#------------------------------------------------------------------------------
#$Date: 2016-03-23 14:43:16 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179303 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/00/4320047.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4320047
loop_
_publ_author_name
'Bin Du'
'Edward A. Meyers'
'Sheldon G. Shore'
_publ_section_title
;
 Syntheses and Structural Characterizations of Sheet- and Column-like
 Lanthanide-Transition Metal Arrays: The Effect of Hydrogen Bonding on the
 Structure When K+ Is Replaced by [NH4]+
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4353
_journal_page_last               4360
_journal_paper_doi               10.1021/ic0014787
_journal_volume                  40
_journal_year                    2001
_chemical_formula_sum            'C29 H49 K N15 O7 Pt2 Yb'
_chemical_formula_weight         1322.15
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                105.459(10)
_cell_angle_beta                 99.100(10)
_cell_angle_gamma                98.586(10)
_cell_formula_units_Z            2
_cell_length_a                   8.8515(10)
_cell_length_b                   15.6733(10)
_cell_length_c                   17.9457(10)
_cell_measurement_temperature    213(2)
_cell_volume                     2320.9(4)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      213(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0543
_diffrn_reflns_av_sigmaI/netI    0.0574
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -2
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            6652
_diffrn_reflns_theta_full        22.47
_diffrn_reflns_theta_max         22.47
_diffrn_reflns_theta_min         2.08
_exptl_absorpt_coefficient_mu    8.155
_exptl_absorpt_correction_T_max  0.2086
_exptl_absorpt_correction_T_min  0.1058
_exptl_absorpt_correction_type   empirical
_exptl_crystal_density_diffrn    1.892
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1258
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.36
_exptl_crystal_size_min          0.28
_refine_diff_density_max         2.375
_refine_diff_density_min         -2.276
_refine_diff_density_rms         0.245
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.135
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     502
_refine_ls_number_reflns         6046
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.135
_refine_ls_R_factor_all          0.0831
_refine_ls_R_factor_gt           0.0462
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0582P)²+49.8222P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1249
_refine_ls_wR_factor_ref         0.1428
_reflns_number_gt                4358
_reflns_number_total             6046
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0014787_1.cif
_cod_data_source_block           bd06
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        2320.9(3)
_cod_database_code               4320047
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.5000 0.0000 0.5000 0.0269(3) Uani 1 2 d S . .
Pt2 Pt 0.5000 -0.5000 0.5000 0.0303(3) Uani 1 2 d S . .
Pt3 Pt 0.5000 0.0000 1.0000 0.0297(3) Uani 1 2 d S . .
Pt4 Pt 1.0000 0.5000 1.0000 0.0363(3) Uani 1 2 d S . .
Yb Yb 0.68037(8) -0.16822(5) 0.72548(4) 0.0226(2) Uani 1 1 d . . .
K K 0.4457(5) 0.2937(3) 0.8809(3) 0.0476(11) Uani 1 1 d . . .
C1 C 0.562(2) -0.0624(12) 0.5779(10) 0.031(4) Uani 1 1 d . . .
N1 N 0.5950(16) -0.1016(9) 0.6215(8) 0.027(3) Uani 1 1 d . . .
C2 C 0.314(2) -0.1013(14) 0.4515(12) 0.045(5) Uani 1 1 d . . .
N2 N 0.209(2) -0.1596(15) 0.4242(12) 0.070(6) Uani 1 1 d . . .
C3 C 0.592(2) -0.3755(14) 0.5744(11) 0.033(4) Uani 1 1 d . . .
N3 N 0.6402(17) -0.3057(10) 0.6204(9) 0.033(4) Uani 1 1 d . . .
C4 C 0.671(2) -0.4930(12) 0.4424(12) 0.039(5) Uani 1 1 d . . .
N4 N 0.768(2) -0.4888(11) 0.4055(10) 0.049(4) Uani 1 1 d . . .
C5 C 0.545(2) -0.0626(13) 0.8959(12) 0.038(5) Uani 1 1 d . . .
N5 N 0.5769(18) -0.0968(10) 0.8378(9) 0.039(4) Uani 1 1 d . . .
C6 C 0.405(2) 0.0854(13) 0.9516(11) 0.044(5) Uani 1 1 d . . .
N6 N 0.353(3) 0.1391(13) 0.9249(11) 0.067(6) Uani 1 1 d . . .
C7 C 0.829(2) 0.3947(15) 0.9908(10) 0.042(5) Uani 1 1 d . . .
N7 N 0.734(2) 0.3351(13) 0.9846(11) 0.059(5) Uani 1 1 d . . .
C8 C 0.879(2) 0.5814(14) 1.0581(12) 0.045(5) Uani 1 1 d . . .
N8 N 0.808(2) 0.6273(14) 1.0904(13) 0.075(6) Uani 1 1 d . . .
O1 O 0.8003(15) -0.0151(8) 0.7683(7) 0.037(3) Uani 1 1 d . . .
C11 C 0.753(2) 0.0546(14) 0.7723(12) 0.047(5) Uani 1 1 d . . .
H11 H 0.6457 0.0526 0.7700 0.056 Uiso 1 1 calc R . .
N10 N 0.8423(18) 0.1329(9) 0.7798(9) 0.034(4) Uani 1 1 d . . .
C12 C 1.006(2) 0.1399(13) 0.7822(14) 0.053(6) Uani 1 1 d . . .
H12A H 1.0536 0.2018 0.7877 0.080 Uiso 1 1 calc R . .
H12B H 1.0222 0.1004 0.7336 0.080 Uiso 1 1 calc R . .
H12C H 1.0539 0.1223 0.8268 0.080 Uiso 1 1 calc R . .
C13 C 0.773(3) 0.2156(13) 0.7816(14) 0.071(8) Uani 1 1 d . . .
H13A H 0.8554 0.2666 0.7873 0.106 Uiso 1 1 calc R . .
H13B H 0.7212 0.2289 0.8259 0.106 Uiso 1 1 calc R . .
H13C H 0.6978 0.2044 0.7328 0.106 Uiso 1 1 calc R . .
O2 O 0.4107(13) -0.2150(8) 0.6897(7) 0.034(3) Uani 1 1 d . . .
C21 C 0.316(2) -0.2449(12) 0.6225(11) 0.032(4) Uani 1 1 d . . .
H21 H 0.3485 -0.2319 0.5787 0.038 Uiso 1 1 calc R . .
N20 N 0.1746(16) -0.2927(9) 0.6115(9) 0.036(4) Uani 1 1 d . . .
C22 C 0.114(2) -0.3213(13) 0.6715(14) 0.051(6) Uani 1 1 d . . .
H22A H 0.0083 -0.3554 0.6502 0.077 Uiso 1 1 calc R . .
H22B H 0.1147 -0.2688 0.7150 0.077 Uiso 1 1 calc R . .
H22C H 0.1790 -0.3592 0.6904 0.077 Uiso 1 1 calc R . .
C23 C 0.071(3) -0.3246(17) 0.5347(15) 0.082(9) Uani 1 1 d . . .
H23A H -0.0272 -0.3584 0.5383 0.123 Uiso 1 1 calc R . .
H23B H 0.1188 -0.3634 0.4976 0.123 Uiso 1 1 calc R . .
H23C H 0.0522 -0.2734 0.5165 0.123 Uiso 1 1 calc R . .
O3 O 0.8943(14) -0.1565(8) 0.6683(7) 0.035(3) Uani 1 1 d . . .
C31 C 1.028(2) -0.1143(12) 0.6969(13) 0.045(5) Uani 1 1 d . . .
H31 H 1.0750 -0.1219 0.7449 0.054 Uiso 1 1 calc R . .
N30 N 1.1122(19) -0.0620(11) 0.6703(10) 0.047(4) Uani 1 1 d . . .
C32 C 1.272(2) -0.0171(13) 0.7100(15) 0.062(7) Uani 1 1 d . . .
H32A H 1.3155 0.0200 0.6800 0.092 Uiso 1 1 calc R . .
H32B H 1.3348 -0.0622 0.7139 0.092 Uiso 1 1 calc R . .
H32C H 1.2730 0.0207 0.7626 0.092 Uiso 1 1 calc R . .
C33 C 1.050(3) -0.0397(19) 0.5983(16) 0.088(9) Uani 1 1 d . . .
H33A H 1.1313 0.0011 0.5871 0.132 Uiso 1 1 calc R . .
H33B H 0.9620 -0.0109 0.6062 0.132 Uiso 1 1 calc R . .
H33C H 1.0171 -0.0946 0.5543 0.132 Uiso 1 1 calc R . .
O4 O 0.6318(15) -0.2829(8) 0.7818(7) 0.040(3) Uani 1 1 d . . .
C41 C 0.519(2) -0.3487(13) 0.7708(12) 0.039(5) Uani 1 1 d . . .
H41 H 0.4593 -0.3760 0.7192 0.047 Uiso 1 1 calc R . .
N40 N 0.4822(19) -0.3794(11) 0.8255(10) 0.047(4) Uani 1 1 d . . .
C42 C 0.349(2) -0.4527(15) 0.8085(13) 0.056(6) Uani 1 1 d . . .
H42A H 0.3376 -0.4678 0.8566 0.084 Uiso 1 1 calc R . .
H42B H 0.3647 -0.5052 0.7697 0.084 Uiso 1 1 calc R . .
H42C H 0.2552 -0.4343 0.7878 0.084 Uiso 1 1 calc R . .
C43 C 0.574(3) -0.346(2) 0.9061(13) 0.107(12) Uani 1 1 d . . .
H43A H 0.5262 -0.3782 0.9387 0.160 Uiso 1 1 calc R . .
H43B H 0.5763 -0.2820 0.9271 0.160 Uiso 1 1 calc R . .
H43C H 0.6792 -0.3561 0.9063 0.160 Uiso 1 1 calc R . .
O5 O 0.8921(14) -0.1566(9) 0.8233(7) 0.044(3) Uani 1 1 d . . .
C51 C 0.905(3) -0.1478(15) 0.8942(12) 0.054(6) Uani 1 1 d . . .
H51 H 0.8238 -0.1290 0.9184 0.065 Uiso 1 1 calc R . .
N50 N 1.027(2) -0.1634(12) 0.9394(9) 0.051(5) Uani 1 1 d . . .
C52 C 1.035(3) -0.153(2) 1.0226(13) 0.091(9) Uani 1 1 d . . .
H52A H 1.1322 -0.1668 1.0450 0.136 Uiso 1 1 calc R . .
H52B H 0.9476 -0.1934 1.0291 0.136 Uiso 1 1 calc R . .
H52C H 1.0312 -0.0909 1.0495 0.136 Uiso 1 1 calc R . .
C53 C 1.152(3) -0.195(2) 0.9048(15) 0.081(8) Uani 1 1 d . . .
H53A H 1.2307 -0.2020 0.9453 0.121 Uiso 1 1 calc R . .
H53B H 1.1976 -0.1508 0.8813 0.121 Uiso 1 1 calc R . .
H53C H 1.1109 -0.2521 0.8643 0.121 Uiso 1 1 calc R . .
O6 O 0.3696(19) 0.1963(9) 0.7311(9) 0.063(4) Uani 1 1 d . . .
C61 C 0.376(3) 0.2029(17) 0.6663(12) 0.068(7) Uani 1 1 d . . .
H61 H 0.4491 0.1751 0.6410 0.081 Uiso 1 1 calc R . .
N60 N 0.290(2) 0.2453(13) 0.6274(10) 0.060(5) Uani 1 1 d . . .
C62 C 0.176(3) 0.2955(18) 0.6634(15) 0.072(7) Uani 1 1 d . . .
H62A H 0.1240 0.3219 0.6259 0.108 Uiso 1 1 calc R . .
H62B H 0.2305 0.3430 0.7110 0.108 Uiso 1 1 calc R . .
H62C H 0.0990 0.2541 0.6765 0.108 Uiso 1 1 calc R . .
C63 C 0.311(5) 0.2475(19) 0.5491(15) 0.117(13) Uani 1 1 d . . .
H63A H 0.2392 0.2812 0.5290 0.175 Uiso 1 1 calc R . .
H63B H 0.2897 0.1862 0.5139 0.175 Uiso 1 1 calc R . .
H63C H 0.4174 0.2765 0.5521 0.175 Uiso 1 1 calc R . .
O7 O 0.590(2) 0.3994(15) 0.8056(13) 0.090(7) Uani 1 1 d . . .
C71 C 0.707(4) 0.439(3) 0.8064(19) 0.105(11) Uani 1 1 d . . .
H71 H 0.7748 0.4639 0.8562 0.127 Uiso 1 1 calc R . .
N70 N 0.764(3) 0.456(2) 0.745(2) 0.116(11) Uani 1 1 d . . .
C72 C 0.684(5) 0.415(4) 0.670(2) 0.18(2) Uani 1 1 d . . .
H72A H 0.7411 0.4345 0.6334 0.267 Uiso 1 1 calc R . .
H72B H 0.5820 0.4316 0.6634 0.267 Uiso 1 1 calc R . .
H72C H 0.6702 0.3502 0.6587 0.267 Uiso 1 1 calc R . .
C73 C 0.912(5) 0.515(4) 0.755(4) 0.27(4) Uani 1 1 d . . .
H73A H 0.9309 0.5168 0.7032 0.407 Uiso 1 1 calc R . .
H73B H 0.9951 0.4920 0.7806 0.407 Uiso 1 1 calc R . .
H73C H 0.9110 0.5752 0.7865 0.407 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 C1 180.000(4) 2_656 . ?
C1 Pt1 C2 88.2(8) 2_656 2_656 ?
C1 Pt1 C2 91.8(8) . 2_656 ?
C1 Pt1 C2 91.8(8) 2_656 . ?
C1 Pt1 C2 88.2(8) . . ?
C2 Pt1 C2 180.0(19) 2_656 . ?
C4 Pt2 C4 180.0(10) . 2_646 ?
C4 Pt2 C3 91.1(7) . . ?
C4 Pt2 C3 88.9(7) 2_646 . ?
C4 Pt2 C3 88.9(7) . 2_646 ?
C4 Pt2 C3 91.1(7) 2_646 2_646 ?
C3 Pt2 C3 180.0(11) . 2_646 ?
C5 Pt3 C5 180.000(8) . 2_657 ?
C5 Pt3 C6 89.7(7) . . ?
C5 Pt3 C6 90.3(7) 2_657 . ?
C5 Pt3 C6 90.3(7) . 2_657 ?
C5 Pt3 C6 89.7(7) 2_657 2_657 ?
C6 Pt3 C6 180.000(8) . 2_657 ?
C8 Pt4 C8 180.0(12) . 2_767 ?
C8 Pt4 C7 91.4(8) . 2_767 ?
C8 Pt4 C7 88.6(8) 2_767 2_767 ?
C8 Pt4 C7 88.6(8) . . ?
C8 Pt4 C7 91.4(8) 2_767 . ?
C7 Pt4 C7 180.000(2) 2_767 . ?
O3 Yb O5 74.4(4) . . ?
O3 Yb O4 119.1(4) . . ?
O5 Yb O4 70.6(5) . . ?
O3 Yb O2 140.0(4) . . ?
O5 Yb O2 142.4(4) . . ?
O4 Yb O2 76.7(4) . . ?
O3 Yb O1 73.6(4) . . ?
O5 Yb O1 75.0(5) . . ?
O4 Yb O1 137.1(4) . . ?
O2 Yb O1 121.7(4) . . ?
O3 Yb N3 74.2(4) . . ?
O5 Yb N3 111.3(5) . . ?
O4 Yb N3 74.3(5) . . ?
O2 Yb N3 76.0(5) . . ?
O1 Yb N3 143.9(5) . . ?
O3 Yb N5 142.9(5) . . ?
O5 Yb N5 82.1(5) . . ?
O4 Yb N5 77.7(5) . . ?
O2 Yb N5 73.2(5) . . ?
O1 Yb N5 72.9(5) . . ?
N3 Yb N5 142.1(5) . . ?
O3 Yb N1 77.5(4) . . ?
O5 Yb N1 141.5(5) . . ?
O4 Yb N1 147.6(5) . . ?
O2 Yb N1 74.1(4) . . ?
O1 Yb N1 72.0(4) . . ?
N3 Yb N1 85.4(5) . . ?
N5 Yb N1 106.4(5) . . ?
O6 K O7 75.9(6) . . ?
O6 K N8 105.5(6) . 2_667 ?
O7 K N8 102.0(6) . 2_667 ?
O6 K N7 128.4(5) . . ?
O7 K N7 85.1(6) . . ?
N8 K N7 125.4(6) 2_667 . ?
O6 K N6 89.9(5) . . ?
O7 K N6 158.4(7) . . ?
N8 K N6 97.4(6) 2_667 . ?
N7 K N6 91.5(6) . . ?
O6 K C7 126.0(5) . . ?
O7 K C7 70.6(6) . . ?
N8 K C7 121.9(6) 2_667 . ?
N7 K C7 15.3(5) . . ?
N6 K C7 106.8(6) . . ?
N1 C1 Pt1 177.4(16) . . ?
C1 N1 Yb 173.3(14) . . ?
N2 C2 Pt1 179(2) . . ?
N3 C3 Pt2 175.8(15) . . ?
C3 N3 Yb 165.9(14) . . ?
N4 C4 Pt2 177.1(18) . . ?
N5 C5 Pt3 176.9(18) . . ?
C5 N5 Yb 172.1(16) . . ?
N6 C6 Pt3 177.1(19) . . ?
C6 N6 K 141.7(18) . . ?
N7 C7 Pt4 178.9(19) . . ?
N7 C7 K 40.8(13) . . ?
Pt4 C7 K 138.9(8) . . ?
C7 N7 K 123.9(16) . . ?
N8 C8 Pt4 179(2) . . ?
C8 N8 K 159.1(19) . 2_667 ?
C11 O1 Yb 134.1(12) . . ?
O1 C11 N10 124.3(18) . . ?
C11 N10 C12 120.4(16) . . ?
C11 N10 C13 120.9(18) . . ?
C12 N10 C13 118.7(17) . . ?
C21 O2 Yb 132.5(11) . . ?
O2 C21 N20 123.5(18) . . ?
C21 N20 C22 123.7(16) . . ?
C21 N20 C23 121.5(19) . . ?
C22 N20 C23 114.7(17) . . ?
C31 O3 Yb 130.2(12) . . ?
O3 C31 N30 128(2) . . ?
C31 N30 C32 123(2) . . ?
C31 N30 C33 121(2) . . ?
C32 N30 C33 116.0(18) . . ?
C41 O4 Yb 135.0(11) . . ?
N40 C41 O4 123.6(18) . . ?
C41 N40 C42 120.2(17) . . ?
C41 N40 C43 122.4(19) . . ?
C42 N40 C43 117.4(18) . . ?
C51 O5 Yb 132.0(14) . . ?
O5 C51 N50 124(2) . . ?
C51 N50 C53 119.9(18) . . ?
C51 N50 C52 121.7(19) . . ?
C53 N50 C52 118.4(18) . . ?
C61 O6 K 140.7(16) . . ?
O6 C61 N60 126(2) . . ?
C61 N60 C63 120(2) . . ?
C61 N60 C62 121.5(19) . . ?
C63 N60 C62 118(2) . . ?
C71 O7 K 142(2) . . ?
O7 C71 N70 128(3) . . ?
C71 N70 C72 120(3) . . ?
C71 N70 C73 123(4) . . ?
C72 N70 C73 117(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.965(18) 2_656 ?
Pt1 C1 1.965(18) . ?
Pt1 C2 2.00(2) 2_656 ?
Pt1 C2 2.00(2) . ?
Pt2 C4 1.97(2) . ?
Pt2 C4 1.97(2) 2_646 ?
Pt2 C3 2.01(2) . ?
Pt2 C3 2.01(2) 2_646 ?
Pt3 C5 2.00(2) . ?
Pt3 C5 2.00(2) 2_657 ?
Pt3 C6 2.00(2) . ?
Pt3 C6 2.00(2) 2_657 ?
Pt4 C8 1.98(2) . ?
Pt4 C8 1.98(2) 2_767 ?
Pt4 C7 2.02(2) 2_767 ?
Pt4 C7 2.02(2) . ?
Yb O3 2.298(11) . ?
Yb O5 2.305(12) . ?
Yb O4 2.305(12) . ?
Yb O2 2.322(11) . ?
Yb O1 2.340(12) . ?
Yb N3 2.391(15) . ?
Yb N5 2.417(16) . ?
Yb N1 2.445(14) . ?
K O6 2.636(16) . ?
K O7 2.704(18) . ?
K N8 2.77(2) 2_667 ?
K N7 2.78(2) . ?
K N6 2.793(19) . ?
K C7 3.54(2) . ?
C1 N1 1.14(2) . ?
C2 N2 1.14(2) . ?
C3 N3 1.15(2) . ?
C4 N4 1.17(2) . ?
C5 N5 1.14(2) . ?
C6 N6 1.18(3) . ?
C7 N7 1.13(2) . ?
C8 N8 1.13(2) . ?
N8 K 2.77(2) 2_667 ?
O1 C11 1.22(2) . ?
C11 N10 1.32(2) . ?
N10 C12 1.43(2) . ?
N10 C13 1.51(2) . ?
O2 C21 1.28(2) . ?
C21 N20 1.31(2) . ?
N20 C22 1.42(2) . ?
N20 C23 1.44(3) . ?
O3 C31 1.23(2) . ?
C31 N30 1.26(2) . ?
N30 C32 1.46(3) . ?
N30 C33 1.47(3) . ?
O4 C41 1.27(2) . ?
C41 N40 1.27(2) . ?
N40 C42 1.45(3) . ?
N40 C43 1.46(3) . ?
O5 C51 1.23(2) . ?
C51 N50 1.34(3) . ?
N50 C53 1.43(3) . ?
N50 C52 1.45(3) . ?
O6 C61 1.20(2) . ?
C61 N60 1.32(3) . ?
N60 C63 1.45(3) . ?
N60 C62 1.50(3) . ?
O7 C71 1.13(4) . ?
C71 N70 1.35(4) . ?
N70 C72 1.35(4) . ?
N70 C73 1.45(4) . ?
