#------------------------------------------------------------------------------
#$Date: 2016-03-23 14:55:18 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179312 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/09/4320956.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4320956
loop_
_publ_author_name
'Owen R. Evans'
'Wenbin Lin'
_publ_section_title
;
 Pillared, 3D Metal-Organic Frameworks with Rectangular Channels.
 Synthesis and Characterization of Coordination Polymers Based on
 Tricadmium Carboxylates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2189
_journal_page_last               2198
_journal_paper_doi               10.1021/ic991360u
_journal_volume                  39
_journal_year                    2000
_chemical_formula_sum            'C37 H35 Cd3 Cl N6 O17'
_chemical_formula_weight         1208.36
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                91.6690(10)
_cell_angle_beta                 96.8500(10)
_cell_angle_gamma                117.9450(10)
_cell_formula_units_Z            2
_cell_length_a                   12.0495(2)
_cell_length_b                   12.2773(2)
_cell_length_c                   19.1028(4)
_cell_measurement_temperature    198(2)
_cell_volume                     2466.97(8)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      198(2)
_diffrn_measured_fraction_theta_full 0.838
_diffrn_measured_fraction_theta_max 0.838
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0887
_diffrn_reflns_av_sigmaI/netI    0.0994
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            14153
_diffrn_reflns_theta_full        28.18
_diffrn_reflns_theta_max         28.18
_diffrn_reflns_theta_min         1.08
_exptl_absorpt_coefficient_mu    1.405
_exptl_crystal_density_diffrn    1.627
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1192
_refine_diff_density_max         2.863
_refine_diff_density_min         -2.931
_refine_diff_density_rms         0.360
_refine_ls_extinction_coef       0.0012(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.835
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     497
_refine_ls_number_reflns         10162
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.835
_refine_ls_R_factor_all          0.1499
_refine_ls_R_factor_gt           0.1079
_refine_ls_shift/su_max          0.460
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2799
_refine_ls_wR_factor_ref         0.3078
_reflns_number_gt                7326
_reflns_number_total             10162
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic991360u_2.cif
_cod_data_source_block           Compound2
_cod_database_code               4320956
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Cd1 Cd -0.76911(9) -0.50233(8) 0.22146(5) 0.0227(3) Uani 1 1 d . . .
Cd2 Cd -0.58859(8) -0.66969(8) 0.30188(4) 0.0172(3) Uani 1 1 d . . .
Cd3 Cd -0.42655(8) -0.32177(8) 0.19801(4) 0.0184(3) Uani 1 1 d . . .
O10 O -0.6170(9) -0.6864(9) 0.1800(4) 0.029(2) Uani 1 1 d . . .
O8 O -0.6133(9) -0.4891(8) 0.3197(4) 0.0240(19) Uani 1 1 d . . .
O4 O -0.3743(9) -0.5631(9) 0.3062(5) 0.031(2) Uani 1 1 d . . .
O9 O -0.6186(8) -0.5083(8) 0.1578(4) 0.0204(18) Uani 1 1 d . . .
O2 O -0.5255(10) -0.2053(9) 0.1819(6) 0.037(2) Uani 1 1 d . . .
O3 O -0.3243(9) -0.4359(9) 0.2189(5) 0.034(2) Uani 1 1 d . . .
O6 O -0.7973(9) -0.7879(9) 0.3066(5) 0.036(2) Uani 1 1 d . . .
O7 O -0.4399(9) -0.3139(8) 0.3159(5) 0.032(2) Uani 1 1 d . . .
O5 O -0.8781(10) -0.7067(9) 0.2261(6) 0.045(3) Uani 1 1 d . . .
O1 O -0.6735(10) -0.2945(9) 0.2525(6) 0.042(3) Uani 1 1 d . . .
C8 C -0.1770(13) -0.4944(12) 0.2656(7) 0.028(3) Uani 1 1 d . . .
C7 C -0.3010(13) -0.4954(11) 0.2625(7) 0.025(3) Uani 1 1 d . . .
C30 C -0.6730(13) -0.5887(12) 0.0125(7) 0.029(3) Uani 1 1 d . . .
H30 H -0.7131 -0.5428 0.0268 0.034 Uiso 1 1 calc R . .
C26 C -0.6179(12) -0.6382(11) 0.0630(7) 0.022(3) Uani 1 1 d . . .
C25 C -0.6184(12) -0.6085(13) 0.1398(6) 0.028(3) Uani 1 1 d . . .
C13 C -0.8822(11) -0.7902(11) 0.2647(7) 0.026(3) Uani 1 1 d . . .
C19 C -0.5168(12) -0.3888(11) 0.3467(7) 0.022(3) Uani 1 1 d . . .
C29 C -0.6668(13) -0.6094(12) -0.0605(7) 0.028(3) Uani 1 1 d . . .
H29 H -0.7018 -0.5754 -0.0950 0.033 Uiso 1 1 calc R . .
C12 C -0.0760(13) -0.3982(12) 0.2396(8) 0.033(3) Uani 1 1 d . . .
H12 H -0.0853 -0.3305 0.2226 0.040 Uiso 1 1 calc R . .
C14 C -1.0078(11) -0.9107(11) 0.2521(7) 0.023(3) Uani 1 1 d . . .
C1 C -0.5953(13) -0.2031(11) 0.2245(8) 0.027(3) Uani 1 1 d . . .
C9 C -0.1515(15) -0.5844(14) 0.2941(9) 0.043(4) Uani 1 1 d . . .
H9 H -0.2139 -0.6473 0.3168 0.051 Uiso 1 1 calc R . .
C2 C -0.5916(14) -0.0839(12) 0.2426(7) 0.031(3) Uani 1 1 d . . .
C6 C -0.6668(15) -0.0732(14) 0.2906(9) 0.038(4) Uani 1 1 d . . .
H6 H -0.7221 -0.1444 0.3114 0.046 Uiso 1 1 calc R . .
C3 C -0.5123(14) 0.0212(13) 0.2167(9) 0.037(4) Uani 1 1 d . . .
H3 H -0.4574 0.0185 0.1856 0.045 Uiso 1 1 calc R . .
C4 C -0.5087(15) 0.1349(14) 0.2345(8) 0.035(3) Uani 1 1 d . . .
H4 H -0.4537 0.2063 0.2138 0.042 Uiso 1 1 calc R . .
C5 C -0.6613(18) 0.0376(13) 0.3077(8) 0.045(4) Uani 1 1 d . . .
H5 H -0.7146 0.0407 0.3397 0.054 Uiso 1 1 calc R . .
N1 N -0.5823(12) 0.1459(11) 0.2809(6) 0.033(3) Uani 1 1 d . . .
C11 C 0.0383(14) -0.4009(14) 0.2383(9) 0.037(4) Uani 1 1 d . . .
H11 H 0.1043 -0.3347 0.2195 0.045 Uiso 1 1 calc R . .
C10 C -0.0391(15) -0.5851(16) 0.2904(11) 0.054(5) Uani 1 1 d . . .
H10 H -0.0281 -0.6517 0.3078 0.065 Uiso 1 1 calc R . .
N2 N 0.0596(12) -0.4914(12) 0.2621(7) 0.041(3) Uani 1 1 d . . .
C18 C -1.0298(14) -1.0101(12) 0.2921(8) 0.035(3) Uani 1 1 d . . .
H18 H -0.9668 -1.0044 0.3293 0.041 Uiso 1 1 calc R . .
C15 C -1.1067(14) -0.9255(13) 0.1995(9) 0.039(4) Uani 1 1 d . . .
H15 H -1.0979 -0.8589 0.1725 0.047 Uiso 1 1 calc R . .
C17 C -1.1439(14) -1.1162(13) 0.2769(7) 0.035(3) Uani 1 1 d . . .
H17 H -1.1566 -1.1825 0.3050 0.042 Uiso 1 1 calc R . .
C16 C -1.2175(14) -1.0379(14) 0.1872(8) 0.039(4) Uani 1 1 d . . .
H16 H -1.2820 -1.0482 0.1498 0.047 Uiso 1 1 calc R . .
N3 N -1.2374(11) -1.1345(11) 0.2269(6) 0.032(3) Uani 1 1 d . . .
C20 C -0.4966(13) -0.3655(12) 0.4269(6) 0.023(3) Uani 1 1 d . . .
C24 C -0.3744(12) -0.2872(12) 0.4656(7) 0.025(3) Uani 1 1 d . . .
H24 H -0.3049 -0.2423 0.4410 0.030 Uiso 1 1 calc R . .
C21 C -0.5977(13) -0.4233(11) 0.4655(7) 0.027(3) Uani 1 1 d . . .
H21 H -0.6822 -0.4745 0.4424 0.032 Uiso 1 1 calc R . .
C22 C -0.5688(13) -0.4022(13) 0.5398(6) 0.027(3) Uani 1 1 d . . .
H22 H -0.6360 -0.4428 0.5666 0.032 Uiso 1 1 calc R . .
N4 N -0.4530(10) -0.3289(10) 0.5748(5) 0.023(2) Uani 1 1 d . . .
C23 C -0.3555(13) -0.2755(13) 0.5380(7) 0.032(3) Uani 1 1 d . . .
H23 H -0.2716 -0.2287 0.5628 0.038 Uiso 1 1 calc R . .
C27 C -0.5731(14) -0.7132(12) 0.0396(6) 0.028(3) Uani 1 1 d . . .
H27 H -0.5450 -0.7551 0.0723 0.034 Uiso 1 1 calc R . .
C28 C -0.5681(17) -0.7289(13) -0.0325(7) 0.039(4) Uani 1 1 d . . .
H28 H -0.5321 -0.7784 -0.0472 0.047 Uiso 1 1 calc R . .
N5 N -0.6116(11) -0.6776(11) -0.0816(6) 0.032(3) Uani 1 1 d . . .
O11 O -0.866(2) -0.489(3) 0.1075(8) 0.120(9) Uani 1 1 d . . .
C34 C -0.874(6) -0.394(4) 0.007(2) 0.072(17) Uani 0.48(3) 1 d P A 1
C33 C -0.814(3) -0.394(3) 0.0787(17) 0.034(9) Uani 0.48(3) 1 d P A 1
C31 C -0.979(4) -0.588(4) 0.0942(19) 0.09(2) Uani 0.52(3) 1 d P A 2
C32 C -1.025(6) -0.540(6) 0.022(2) 0.11(3) Uani 0.52(3) 1 d P . 2
C37 C -1.012(4) -0.897(4) 0.000(3) 0.073(12) Uiso 0.50 1 d P . .
C36 C -0.941(4) -0.903(4) 0.057(2) 0.070(12) Uiso 0.50 1 d P . .
C35 C -0.927(6) -0.992(5) 0.062(3) 0.105(18) Uiso 0.50 1 d P . .
O12 O -0.587(4) -1.054(4) -0.012(2) 0.122(14) Uiso 0.50 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O5 Cd1 O1 161.6(4) . . ?
O5 Cd1 O9 95.7(4) . . ?
O1 Cd1 O9 98.9(3) . . ?
O5 Cd1 N2 86.7(4) . 1_455 ?
O1 Cd1 N2 81.4(4) . 1_455 ?
O9 Cd1 N2 167.7(4) . 1_455 ?
O5 Cd1 O11 98.9(8) . . ?
O1 Cd1 O11 93.9(8) . . ?
O9 Cd1 O11 83.4(4) . . ?
N2 Cd1 O11 84.4(5) 1_455 . ?
O5 Cd1 O8 89.9(4) . . ?
O1 Cd1 O8 81.4(4) . . ?
O9 Cd1 O8 80.7(3) . . ?
N2 Cd1 O8 111.3(4) 1_455 . ?
O11 Cd1 O8 162.5(5) . . ?
O6 Cd2 O4 173.7(4) . . ?
O6 Cd2 O10 93.5(4) . . ?
O4 Cd2 O10 90.8(3) . . ?
O6 Cd2 N1 86.6(4) . 1_545 ?
O4 Cd2 N1 89.6(4) . 1_545 ?
O10 Cd2 N1 80.7(4) . 1_545 ?
O6 Cd2 N4 88.9(4) . 2_446 ?
O4 Cd2 N4 86.2(3) . 2_446 ?
O10 Cd2 N4 172.0(4) . 2_446 ?
N1 Cd2 N4 91.9(4) 1_545 2_446 ?
O6 Cd2 O8 89.1(3) . . ?
O4 Cd2 O8 94.9(3) . . ?
O10 Cd2 O8 97.7(3) . . ?
N1 Cd2 O8 175.3(4) 1_545 . ?
N4 Cd2 O8 90.0(3) 2_446 . ?
O2 Cd3 O3 177.7(4) . . ?
O2 Cd3 O7 89.8(4) . . ?
O3 Cd3 O7 88.1(4) . . ?
O2 Cd3 N5 94.3(4) . 2_445 ?
O3 Cd3 N5 87.7(4) . 2_445 ?
O7 Cd3 N5 173.5(4) . 2_445 ?
O2 Cd3 N3 86.6(4) . 1_665 ?
O3 Cd3 N3 92.3(4) . 1_665 ?
O7 Cd3 N3 85.6(4) . 1_665 ?
N5 Cd3 N3 89.6(4) 2_445 1_665 ?
O2 Cd3 O9 92.0(3) . . ?
O3 Cd3 O9 89.2(3) . . ?
O7 Cd3 O9 99.4(3) . . ?
N5 Cd3 O9 85.6(3) 2_445 . ?
N3 Cd3 O9 174.9(3) 1_665 . ?
C25 O10 Cd2 128.1(8) . . ?
C19 O8 Cd2 118.5(8) . . ?
C19 O8 Cd1 124.1(8) . . ?
Cd2 O8 Cd1 106.1(3) . . ?
C7 O4 Cd2 133.4(9) . . ?
C25 O9 Cd1 122.5(7) . . ?
C25 O9 Cd3 121.9(8) . . ?
Cd1 O9 Cd3 105.5(3) . . ?
C1 O2 Cd3 120.3(9) . . ?
C7 O3 Cd3 143.2(9) . . ?
C13 O6 Cd2 124.6(9) . . ?
C19 O7 Cd3 128.2(8) . . ?
C13 O5 Cd1 140.7(10) . . ?
C1 O1 Cd1 132.0(9) . . ?
C9 C8 C12 115.6(13) . . ?
C9 C8 C7 124.0(11) . . ?
C12 C8 C7 120.4(12) . . ?
O3 C7 O4 127.3(13) . . ?
O3 C7 C8 117.1(11) . . ?
O4 C7 C8 115.6(12) . . ?
C26 C30 C29 118.2(12) . . ?
C27 C26 C30 118.7(12) . . ?
C27 C26 C25 124.0(12) . . ?
C30 C26 C25 117.2(12) . . ?
O10 C25 O9 126.5(11) . . ?
O10 C25 C26 115.3(12) . . ?
O9 C25 C26 118.2(12) . . ?
O6 C13 O5 127.9(12) . . ?
O6 C13 C14 117.2(12) . . ?
O5 C13 C14 114.7(12) . . ?
O7 C19 O8 126.7(12) . . ?
O7 C19 C20 117.4(11) . . ?
O8 C19 C20 115.9(10) . . ?
N5 C29 C30 121.2(12) . . ?
C11 C12 C8 120.5(13) . . ?
C18 C14 C15 117.1(11) . . ?
C18 C14 C13 122.0(12) . . ?
C15 C14 C13 120.9(11) . . ?
O2 C1 O1 126.5(12) . . ?
O2 C1 C2 117.8(12) . . ?
O1 C1 C2 115.6(12) . . ?
C10 C9 C8 121.9(13) . . ?
C3 C2 C6 116.7(13) . . ?
C3 C2 C1 121.9(13) . . ?
C6 C2 C1 121.3(12) . . ?
C5 C6 C2 120.9(14) . . ?
C2 C3 C4 121.6(13) . . ?
N1 C4 C3 122.1(13) . . ?
C6 C5 N1 123.4(14) . . ?
C4 N1 C5 115.4(12) . . ?
C4 N1 Cd2 121.4(9) . 1_565 ?
C5 N1 Cd2 122.8(9) . 1_565 ?
N2 C11 C12 123.5(12) . . ?
C9 C10 N2 122.1(14) . . ?
C11 N2 C10 116.2(12) . . ?
C11 N2 Cd1 114.7(9) . 1_655 ?
C10 N2 Cd1 126.6(10) . 1_655 ?
C17 C18 C14 118.7(13) . . ?
C16 C15 C14 119.6(12) . . ?
N3 C17 C18 125.8(12) . . ?
N3 C16 C15 122.5(14) . . ?
C17 N3 C16 116.2(12) . . ?
C17 N3 Cd3 124.7(9) . 1_445 ?
C16 N3 Cd3 118.9(9) . 1_445 ?
C21 C20 C24 117.5(11) . . ?
C21 C20 C19 121.1(12) . . ?
C24 C20 C19 121.4(11) . . ?
C23 C24 C20 120.8(11) . . ?
C20 C21 C22 117.2(12) . . ?
N4 C22 C21 124.0(11) . . ?
C22 N4 C23 118.9(10) . . ?
C22 N4 Cd2 120.0(7) . 2_446 ?
C23 N4 Cd2 119.5(8) . 2_446 ?
N4 C23 C24 121.4(12) . . ?
C26 C27 C28 120.2(13) . . ?
N5 C28 C27 123.0(14) . . ?
C28 N5 C29 118.3(12) . . ?
C28 N5 Cd3 122.3(10) . 2_445 ?
C29 N5 Cd3 118.9(9) . 2_445 ?
C33 O11 C31 134(3) . . ?
C33 O11 Cd1 119(2) . . ?
C31 O11 Cd1 107(3) . . ?
O11 C33 C34 116(3) . . ?
O11 C31 C32 95(4) . . ?
C32 C32 C31 138(7) 2_345 . ?
C36 C37 C35 120(4) . 2_335 ?
C35 C36 C37 120(5) . . ?
C36 C35 C37 120(5) . 2_335 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cd1 O5 2.232(9) . ?
Cd1 O1 2.277(10) . ?
Cd1 O9 2.328(8) . ?
Cd1 N2 2.348(12) 1_455 ?
Cd1 O11 2.392(15) . ?
Cd1 O8 2.435(9) . ?
Cd2 O6 2.254(9) . ?
Cd2 O4 2.272(9) . ?
Cd2 O10 2.302(8) . ?
Cd2 N1 2.326(11) 1_545 ?
Cd2 N4 2.352(9) 2_446 ?
Cd2 O8 2.392(9) . ?
Cd3 O2 2.257(10) . ?
Cd3 O3 2.275(9) . ?
Cd3 O7 2.279(8) . ?
Cd3 N5 2.324(10) 2_445 ?
Cd3 N3 2.345(11) 1_665 ?
Cd3 O9 2.387(8) . ?
O10 C25 1.248(16) . ?
O8 C19 1.269(15) . ?
O4 C7 1.301(14) . ?
O9 C25 1.269(16) . ?
O2 C1 1.248(15) . ?
O3 C7 1.215(16) . ?
O6 C13 1.209(17) . ?
O7 C19 1.189(14) . ?
O5 C13 1.266(17) . ?
O1 C1 1.264(16) . ?
C8 C9 1.387(19) . ?
C8 C12 1.398(17) . ?
C8 C7 1.48(2) . ?
C30 C26 1.415(18) . ?
C30 C29 1.427(17) . ?
C26 C27 1.355(18) . ?
C26 C25 1.505(16) . ?
C13 C14 1.526(16) . ?
C19 C20 1.518(15) . ?
C29 N5 1.368(17) . ?
C12 C11 1.396(19) . ?
C14 C18 1.395(18) . ?
C14 C15 1.401(19) . ?
C1 C2 1.472(17) . ?
C9 C10 1.37(2) . ?
C2 C3 1.35(2) . ?
C2 C6 1.408(18) . ?
C6 C5 1.36(2) . ?
C3 C4 1.407(19) . ?
C4 N1 1.371(17) . ?
C5 N1 1.380(18) . ?
N1 Cd2 2.326(11) 1_565 ?
C11 N2 1.333(19) . ?
C10 N2 1.393(17) . ?
N2 Cd1 2.348(12) 1_655 ?
C18 C17 1.370(19) . ?
C15 C16 1.39(2) . ?
C17 N3 1.314(18) . ?
C16 N3 1.366(18) . ?
N3 Cd3 2.345(11) 1_445 ?
C20 C21 1.402(16) . ?
C20 C24 1.419(19) . ?
C24 C23 1.366(17) . ?
C21 C22 1.407(16) . ?
C22 N4 1.330(16) . ?
N4 C23 1.344(16) . ?
N4 Cd2 2.352(9) 2_446 ?
C27 C28 1.398(17) . ?
C28 N5 1.333(18) . ?
N5 Cd3 2.324(10) 2_445 ?
O11 C33 1.22(4) . ?
O11 C31 1.31(4) . ?
C34 C33 1.46(6) . ?
C31 C32 1.66(6) . ?
C32 C32 1.28(13) 2_345 ?
C37 C36 1.32(6) . ?
C37 C35 1.60(7) 2_335 ?
C36 C35 1.19(6) . ?
C35 C37 1.60(7) 2_335 ?
