#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:15:55 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179319 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/16/4321601.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4321601
loop_
_publ_author_name
'Daniel Neuman'
'Patrina Paraskevopoulou'
'Nikos Psaroudakis'
'Konstantinos Mertis'
'Richard J. Staples'
'Pericles Stavropoulos'
_publ_section_title
;
 Structural and Functional Characteristics of Rhenium Clusters Derived
 from Redox Chemistry of the Triangular [ReIII3(μ-Cl)3] Core Unit
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5530
_journal_page_last               5537
_journal_paper_doi               10.1021/ic000449t
_journal_volume                  39
_journal_year                    2000
_chemical_formula_moiety
;
[(C~6~H~5~)~4~P]~2~[Re~3~(\m-Cl)~3~Cl~8~(MeOH)].MeOH 
;
_chemical_formula_sum            'C50 H48 Cl11 O2 P2 Re3'
_chemical_formula_weight         1691.37
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.289(2)
_cell_angle_beta                 93.086(2)
_cell_angle_gamma                107.646(2)
_cell_formula_units_Z            2
_cell_length_a                   10.214(1)
_cell_length_b                   12.944(1)
_cell_length_c                   22.069(2)
_cell_measurement_temperature    213(2)
_cell_volume                     2771.6(4)
_computing_cell_refinement       'SMART (BRUKER, V5.054, 1998)'
_computing_data_collection       'ASTRO (BRUKER, V5.007, 1997)'
_computing_data_reduction        'SAINT (BRUKER, V6.01, 1999)'
_computing_molecular_graphics    'SHELXTL (BRUKER, 1998, V5.1)'
_computing_publication_material  'XCIF (Sheldrick and BRUKER, 1997, V5.1)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      213(2)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_method       'ω, 0.3 deg'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'normal-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0655
_diffrn_reflns_av_sigmaI/netI    0.0839
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            14983
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         0.93
_diffrn_standards_decay_%        <1
_diffrn_standards_interval_count 0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    7.162
_exptl_absorpt_correction_T_max  0.9175
_exptl_absorpt_correction_T_min  0.6939
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.027
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       chunk
_exptl_crystal_F_000             1612
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.406
_refine_diff_density_min         -2.716
_refine_diff_density_rms         0.440
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    fixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     668
_refine_ls_number_reflns         9664
_refine_ls_number_restraints     402
_refine_ls_restrained_S_all      1.016
_refine_ls_R_factor_all          0.1038
_refine_ls_R_factor_gt           0.0610
_refine_ls_shift/su_max          0.032
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1430P)²+58.6662P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1737
_refine_ls_wR_factor_ref         0.2519
_reflns_number_gt                6581
_reflns_number_total             9664
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic000449t_9.cif
_cod_data_source_block           Compound_10
_cod_database_code               4321601
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.65934(8) 0.04721(7) 0.73867(3) 0.0358(2) Uani 1 1 d . . .
Re2 Re 0.90444(7) 0.09762(6) 0.72075(3) 0.0297(2) Uani 1 1 d . . .
Re3 Re 0.79158(7) -0.07520(6) 0.76626(3) 0.0293(2) Uani 1 1 d . . .
Cl1 Cl 0.7737(6) 0.2169(4) 0.6943(3) 0.0511(13) Uani 1 1 d . . .
Cl2 Cl 1.0320(5) -0.0242(4) 0.7479(2) 0.0403(11) Uani 1 1 d . . .
Cl3 Cl 0.5492(5) -0.1218(5) 0.7828(2) 0.0507(13) Uani 1 1 d . . .
Cl4 Cl 0.6683(6) 0.1370(6) 0.8311(3) 0.0613(16) Uani 1 1 d . . .
Cl5 Cl 0.5608(5) -0.0289(4) 0.6446(2) 0.0474(12) Uani 1 1 d . . .
Cl6 Cl 0.9913(5) 0.2042(4) 0.8090(2) 0.0460(12) Uani 1 1 d . . .
Cl7 Cl 1.1241(5) 0.2313(4) 0.6857(2) 0.0444(12) Uani 1 1 d . . .
Cl8 Cl 0.8852(5) 0.0361(4) 0.6196(2) 0.0435(11) Uani 1 1 d . . .
Cl9 Cl 0.8479(5) -0.0161(4) 0.8674(2) 0.0433(11) Uani 1 1 d . . .
Cl10 Cl 0.7990(5) -0.2507(4) 0.8119(2) 0.0450(12) Uani 1 1 d . . .
Cl11 Cl 0.7445(5) -0.1861(4) 0.6789(2) 0.0391(11) Uani 1 1 d . . .
O1 O 0.4576(14) 0.0901(13) 0.7321(7) 0.055(4) Uani 1 1 d . . .
H1 H 0.4057 0.0887 0.7005 0.083 Uiso 1 1 d R . .
C1 C 0.405(3) 0.155(2) 0.7672(13) 0.075(8) Uani 1 1 d . . .
H1A H 0.3150 0.1525 0.7497 0.113 Uiso 1 1 calc R . .
H1B H 0.4660 0.2289 0.7689 0.113 Uiso 1 1 calc R . .
H1C H 0.3968 0.1293 0.8080 0.113 Uiso 1 1 calc R . .
P1A P 0.2898(5) 0.5457(4) 0.5817(2) 0.0325(10) Uani 1 1 d . . .
C1A C 0.419(2) 0.4986(16) 0.6211(9) 0.040(3) Uani 1 1 d U . .
C2A C 0.501(2) 0.5635(16) 0.6660(9) 0.041(3) Uani 1 1 d U . .
H2AA H 0.4887 0.6311 0.6758 0.050 Uiso 1 1 calc R . .
C3A C 0.601(2) 0.5344(16) 0.6979(9) 0.044(3) Uani 1 1 d U . .
H3AA H 0.6584 0.5808 0.7290 0.053 Uiso 1 1 calc R . .
C4A C 0.616(2) 0.4307(15) 0.6820(9) 0.043(3) Uani 1 1 d U . .
H4AA H 0.6880 0.4102 0.7012 0.052 Uiso 1 1 calc R . .
C5A C 0.526(2) 0.3602(15) 0.6391(9) 0.039(3) Uani 1 1 d U . .
H5AA H 0.5301 0.2890 0.6325 0.047 Uiso 1 1 calc R . .
C6A C 0.432(2) 0.3952(15) 0.6062(9) 0.041(3) Uani 1 1 d U . .
H6AA H 0.3761 0.3508 0.5740 0.049 Uiso 1 1 calc R . .
C7A C 0.187(3) 0.582(2) 0.6366(11) 0.060(3) Uani 1 1 d U . .
C8A C 0.224(3) 0.693(2) 0.6586(11) 0.064(3) Uani 1 1 d U . .
H8AA H 0.2965 0.7451 0.6419 0.077 Uiso 1 1 calc R . .
C9A C 0.158(3) 0.724(2) 0.7020(12) 0.067(3) Uani 1 1 d U . .
H9AA H 0.1872 0.7974 0.7163 0.081 Uiso 1 1 calc R . .
C10A C 0.054(3) 0.658(2) 0.7259(12) 0.067(3) Uani 1 1 d U . .
H10B H 0.0078 0.6839 0.7557 0.080 Uiso 1 1 calc R . .
C11A C 0.011(3) 0.544(2) 0.7065(12) 0.066(3) Uani 1 1 d U . .
H11A H -0.0633 0.4942 0.7236 0.080 Uiso 1 1 calc R . .
C12A C 0.080(3) 0.512(2) 0.6628(11) 0.064(3) Uani 1 1 d U . .
H12B H 0.0541 0.4375 0.6500 0.076 Uiso 1 1 calc R . .
C13A C 0.1916(19) 0.4350(16) 0.5280(9) 0.038(3) Uani 1 1 d U . .
C14A C 0.114(2) 0.3399(16) 0.5453(10) 0.044(3) Uani 1 1 d U . .
H14A H 0.0984 0.3315 0.5866 0.053 Uiso 1 1 calc R . .
C15A C 0.055(2) 0.2502(17) 0.5023(9) 0.046(3) Uani 1 1 d U . .
H15A H 0.0015 0.1825 0.5143 0.055 Uiso 1 1 calc R . .
C16A C 0.080(2) 0.2672(17) 0.4444(10) 0.045(3) Uani 1 1 d U . .
H16A H 0.0438 0.2084 0.4158 0.054 Uiso 1 1 calc R . .
C17A C 0.156(2) 0.3647(17) 0.4234(10) 0.045(3) Uani 1 1 d U . .
H17A H 0.1691 0.3730 0.3818 0.053 Uiso 1 1 calc R . .
C18A C 0.2102(19) 0.4489(16) 0.4659(9) 0.039(3) Uani 1 1 d U . .
H18A H 0.2610 0.5171 0.4534 0.047 Uiso 1 1 calc R . .
C19A C 0.369(2) 0.6645(18) 0.5413(10) 0.048(3) Uani 1 1 d U . .
C20A C 0.277(2) 0.7098(18) 0.5099(10) 0.048(3) Uani 1 1 d U . .
H20A H 0.1809 0.6784 0.5089 0.058 Uiso 1 1 calc R . .
C21A C 0.340(2) 0.8050(18) 0.4804(10) 0.050(3) Uani 1 1 d U . .
H21A H 0.2836 0.8392 0.4590 0.060 Uiso 1 1 calc R . .
C22A C 0.477(2) 0.8483(18) 0.4821(10) 0.051(3) Uani 1 1 d U . .
H22A H 0.5164 0.9117 0.4617 0.061 Uiso 1 1 calc R . .
C23A C 0.561(2) 0.8008(18) 0.5131(10) 0.053(3) Uani 1 1 d U . .
H23A H 0.6568 0.8318 0.5131 0.063 Uiso 1 1 calc R . .
C24A C 0.510(2) 0.7114(18) 0.5434(10) 0.049(3) Uani 1 1 d U . .
H24A H 0.5693 0.6813 0.5657 0.059 Uiso 1 1 calc R . .
P1B P 0.6250(6) 0.3230(4) 0.0370(3) 0.0444(13) Uani 1 1 d . . .
C1B C 0.701(5) 0.213(6) 0.061(4) 0.061(4) Uani 0.64(2) 1 d PU A 1
C2B C 0.589(4) 0.117(3) 0.0741(18) 0.061(4) Uani 0.64(2) 1 d PU A 1
H2BA H 0.4950 0.1109 0.0697 0.074 Uiso 0.64(2) 1 calc PR A 1
C3B C 0.646(4) 0.031(3) 0.0953(18) 0.062(5) Uani 0.64(2) 1 d PU A 1
H3BA H 0.5849 -0.0386 0.0999 0.074 Uiso 0.64(2) 1 calc PR A 1
C4B C 0.776(4) 0.049(4) 0.108(2) 0.061(4) Uani 0.64(2) 1 d PU A 1
H4BA H 0.8088 -0.0077 0.1200 0.073 Uiso 0.64(2) 1 calc PR A 1
C5B C 0.867(4) 0.152(3) 0.102(2) 0.061(4) Uani 0.64(2) 1 d PU A 1
H5BA H 0.9596 0.1677 0.1166 0.074 Uiso 0.64(2) 1 calc PR A 1
C6B C 0.823(4) 0.230(3) 0.077(2) 0.061(4) Uani 0.64(2) 1 d PU A 1
H6BA H 0.8869 0.2982 0.0723 0.074 Uiso 0.64(2) 1 calc PR A 1
C1C C 0.674(10) 0.209(11) 0.060(7) 0.061(4) Uani 0.36(2) 1 d PU A 2
C2C C 0.676(7) 0.112(5) 0.019(3) 0.061(4) Uani 0.36(2) 1 d PU A 2
H2CA H 0.6258 0.1042 -0.0191 0.073 Uiso 0.36(2) 1 calc PR A 2
C3C C 0.737(7) 0.037(5) 0.028(3) 0.061(5) Uani 0.36(2) 1 d PU A 2
H3CA H 0.7308 -0.0230 0.0014 0.074 Uiso 0.36(2) 1 calc PR A 2
C4C C 0.820(8) 0.064(7) 0.089(4) 0.061(4) Uani 0.36(2) 1 d PU A 2
H4CA H 0.8770 0.0216 0.1005 0.073 Uiso 0.36(2) 1 calc PR A 2
C5C C 0.816(7) 0.147(6) 0.129(4) 0.061(4) Uani 0.36(2) 1 d PU A 2
H5CA H 0.8507 0.1479 0.1696 0.074 Uiso 0.36(2) 1 calc PR A 2
C6C C 0.766(7) 0.224(6) 0.112(4) 0.061(4) Uani 0.36(2) 1 d PU A 2
H6CA H 0.7925 0.2907 0.1355 0.073 Uiso 0.36(2) 1 calc PR A 2
C7B C 0.732(3) 0.397(2) -0.0177(13) 0.067(3) Uani 1 1 d U A .
C8B C 0.788(3) 0.340(2) -0.0628(13) 0.070(4) Uani 1 1 d U . .
H8BA H 0.7749 0.2650 -0.0618 0.084 Uiso 1 1 calc R A .
C9B C 0.861(3) 0.401(2) -0.1074(13) 0.070(4) Uani 1 1 d U A .
H9BA H 0.8995 0.3671 -0.1370 0.084 Uiso 1 1 calc R . .
C10B C 0.875(3) 0.504(2) -0.1083(13) 0.069(4) Uani 1 1 d U . .
H10A H 0.9185 0.5396 -0.1415 0.083 Uiso 1 1 calc R A .
C11B C 0.837(3) 0.563(2) -0.0679(12) 0.068(3) Uani 1 1 d U A .
H11B H 0.8551 0.6387 -0.0708 0.081 Uiso 1 1 calc R . .
C12B C 0.762(3) 0.506(2) -0.0176(13) 0.067(3) Uani 1 1 d U . .
H12A H 0.7359 0.5445 0.0141 0.080 Uiso 1 1 calc R A .
C13B C 0.454(2) 0.270(2) 0.0025(11) 0.062(3) Uani 1 1 d U A .
C14B C 0.423(2) 0.286(2) -0.0570(11) 0.059(3) Uani 1 1 d U . .
H14B H 0.4937 0.3233 -0.0811 0.071 Uiso 1 1 calc R A .
C15B C 0.286(2) 0.247(2) -0.0823(11) 0.059(3) Uani 1 1 d U A .
H15B H 0.2636 0.2615 -0.1224 0.071 Uiso 1 1 calc R . .
C16B C 0.193(2) 0.193(2) -0.0494(11) 0.062(3) Uani 1 1 d U . .
H16B H 0.1039 0.1600 -0.0678 0.075 Uiso 1 1 calc R A .
C17B C 0.216(3) 0.178(2) 0.0114(11) 0.066(3) Uani 1 1 d U A .
H17B H 0.1427 0.1404 0.0340 0.079 Uiso 1 1 calc R . .
C18B C 0.342(2) 0.220(2) 0.0378(12) 0.066(3) Uani 1 1 d U . .
H18B H 0.3579 0.2148 0.0799 0.079 Uiso 1 1 calc R A .
C19B C 0.625(3) 0.413(2) 0.1003(12) 0.070(4) Uani 1 1 d U A .
C20B C 0.752(3) 0.459(2) 0.1352(12) 0.074(4) Uani 1 1 d U . .
H20B H 0.8315 0.4406 0.1260 0.089 Uiso 1 1 calc R A .
C21B C 0.755(3) 0.534(2) 0.1847(12) 0.074(4) Uani 1 1 d U A .
H21B H 0.8393 0.5698 0.2063 0.089 Uiso 1 1 calc R . .
C22B C 0.643(3) 0.555(2) 0.2013(13) 0.074(4) Uani 1 1 d U . .
H22B H 0.6455 0.5999 0.2360 0.088 Uiso 1 1 calc R A .
C23B C 0.519(3) 0.507(2) 0.1646(12) 0.075(4) Uani 1 1 d U A .
H23B H 0.4401 0.5265 0.1716 0.090 Uiso 1 1 calc R . .
C24B C 0.517(3) 0.429(2) 0.1182(12) 0.074(4) Uani 1 1 d U . .
H24B H 0.4309 0.3878 0.0995 0.089 Uiso 1 1 calc R A .
O1S O 0.2923(16) 0.0854(14) 0.6314(8) 0.065(4) Uani 1 1 d . . .
H1S H 0.2518 0.1338 0.6330 0.098 Uiso 1 1 d R . .
C1S C 0.217(2) -0.0076(18) 0.5967(11) 0.055(6) Uani 1 1 d . . .
H1SA H 0.1659 0.0123 0.5631 0.082 Uiso 1 1 calc R . .
H1SB H 0.1530 -0.0558 0.6218 0.082 Uiso 1 1 calc R . .
H1SC H 0.2789 -0.0442 0.5809 0.082 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Re1 Cl4 78.3(4) . . ?
O1 Re1 Cl5 77.1(4) . . ?
Cl4 Re1 Cl5 155.33(19) . . ?
O1 Re1 Cl3 91.5(5) . . ?
Cl4 Re1 Cl3 89.5(2) . . ?
Cl5 Re1 Cl3 89.5(2) . . ?
O1 Re1 Cl1 89.4(5) . . ?
Cl4 Re1 Cl1 90.7(2) . . ?
Cl5 Re1 Cl1 90.7(2) . . ?
Cl3 Re1 Cl1 179.11(18) . . ?
O1 Re1 Re2 148.3(4) . . ?
Cl4 Re1 Re2 100.55(15) . . ?
Cl5 Re1 Re2 101.22(14) . . ?
Cl3 Re1 Re2 120.19(13) . . ?
Cl1 Re1 Re2 58.92(12) . . ?
O1 Re1 Re3 151.2(4) . . ?
Cl4 Re1 Re3 99.83(16) . . ?
Cl5 Re1 Re3 100.89(13) . . ?
Cl3 Re1 Re3 59.68(13) . . ?
Cl1 Re1 Re3 119.44(13) . . ?
Re2 Re1 Re3 60.51(3) . . ?
Cl6 Re2 Cl8 159.34(19) . . ?
Cl6 Re2 Cl1 89.67(18) . . ?
Cl8 Re2 Cl1 89.41(18) . . ?
Cl6 Re2 Cl2 90.51(18) . . ?
Cl8 Re2 Cl2 90.77(17) . . ?
Cl1 Re2 Cl2 178.99(19) . . ?
Cl6 Re2 Re1 98.72(14) . . ?
Cl8 Re2 Re1 98.69(13) . . ?
Cl1 Re2 Re1 60.12(15) . . ?
Cl2 Re2 Re1 118.87(12) . . ?
Cl6 Re2 Re3 98.86(14) . . ?
Cl8 Re2 Re3 99.47(13) . . ?
Cl1 Re2 Re3 119.88(15) . . ?
Cl2 Re2 Re3 59.11(12) . . ?
Re1 Re2 Re3 59.77(3) . . ?
Cl6 Re2 Cl7 78.52(18) . . ?
Cl8 Re2 Cl7 80.86(18) . . ?
Cl1 Re2 Cl7 91.13(18) . . ?
Cl2 Re2 Cl7 89.88(16) . . ?
Re1 Re2 Cl7 151.22(12) . . ?
Re3 Re2 Cl7 148.96(12) . . ?
Cl11 Re3 Cl9 160.60(18) . . ?
Cl11 Re3 Cl2 89.06(18) . . ?
Cl9 Re3 Cl2 90.01(17) . . ?
Cl11 Re3 Cl3 90.86(18) . . ?
Cl9 Re3 Cl3 90.67(18) . . ?
Cl2 Re3 Cl3 178.17(18) . . ?
Cl11 Re3 Re1 99.00(13) . . ?
Cl9 Re3 Re1 98.41(13) . . ?
Cl2 Re3 Re1 118.88(11) . . ?
Cl3 Re3 Re1 59.33(15) . . ?
Cl11 Re3 Re2 98.08(12) . . ?
Cl9 Re3 Re2 98.06(13) . . ?
Cl2 Re3 Re2 59.16(11) . . ?
Cl3 Re3 Re2 119.05(15) . . ?
Re1 Re3 Re2 59.72(3) . . ?
Cl11 Re3 Cl10 81.10(17) . . ?
Cl9 Re3 Cl10 79.57(18) . . ?
Cl2 Re3 Cl10 92.26(16) . . ?
Cl3 Re3 Cl10 89.54(18) . . ?
Re1 Re3 Cl10 148.85(12) . . ?
Re2 Re3 Cl10 151.40(12) . . ?
Re2 Cl1 Re1 60.96(12) . . ?
Re3 Cl2 Re2 61.73(11) . . ?
Re1 Cl3 Re3 61.00(13) . . ?
C1 O1 Re1 133.4(16) . . ?
C7A P1A C19A 108.0(11) . . ?
C7A P1A C1A 108.6(10) . . ?
C19A P1A C1A 110.7(10) . . ?
C7A P1A C13A 113.2(11) . . ?
C19A P1A C13A 109.8(10) . . ?
C1A P1A C13A 106.6(9) . . ?
C2A C1A C6A 120.7(18) . . ?
C2A C1A P1A 118.4(15) . . ?
C6A C1A P1A 120.9(15) . . ?
C1A C2A C3A 122.1(19) . . ?
C2A C3A C4A 117.3(18) . . ?
C5A C4A C3A 121.0(18) . . ?
C6A C5A C4A 119.3(17) . . ?
C5A C6A C1A 119.2(17) . . ?
C12A C7A C8A 116(2) . . ?
C12A C7A P1A 125(2) . . ?
C8A C7A P1A 118.1(19) . . ?
C9A C8A C7A 121(3) . . ?
C10A C9A C8A 123(3) . . ?
C9A C10A C11A 120(2) . . ?
C12A C11A C10A 118(3) . . ?
C11A C12A C7A 122(3) . . ?
C14A C13A C18A 119.3(18) . . ?
C14A C13A P1A 122.9(16) . . ?
C18A C13A P1A 117.5(14) . . ?
C13A C14A C15A 121(2) . . ?
C16A C15A C14A 117(2) . . ?
C15A C16A C17A 125(2) . . ?
C18A C17A C16A 117(2) . . ?
C17A C18A C13A 121.2(19) . . ?
C24A C19A C20A 122(2) . . ?
C24A C19A P1A 122.3(17) . . ?
C20A C19A P1A 115.4(16) . . ?
C21A C20A C19A 115(2) . . ?
C22A C21A C20A 122(2) . . ?
C21A C22A C23A 120(2) . . ?
C24A C23A C22A 122(2) . . ?
C23A C24A C19A 118(2) . . ?
C19B P1B C7B 109.0(13) . . ?
C19B P1B C1C 111(5) . . ?
C7B P1B C1C 113(5) . . ?
C19B P1B C13B 109.0(13) . . ?
C7B P1B C13B 108.1(12) . . ?
C1C P1B C13B 106(3) . . ?
C19B P1B C1B 111(3) . . ?
C7B P1B C1B 107(3) . . ?
C1C P1B C1B 7(5) . . ?
C13B P1B C1B 113(2) . . ?
C6B C1B C2B 125(6) . . ?
C6B C1B P1B 124(5) . . ?
C2B C1B P1B 109(3) . . ?
C1B C2B C3B 110(4) . . ?
C4B C3B C2B 122(4) . . ?
C3B C4B C5B 120(4) . . ?
C6B C5B C4B 120(4) . . ?
C1B C6B C5B 121(5) . . ?
C6C C1C C2C 112(8) . . ?
C6C C1C P1B 118(9) . . ?
C2C C1C P1B 126(9) . . ?
C3C C2C C1C 130(7) . . ?
C2C C3C C4C 109(7) . . ?
C5C C4C C3C 123(7) . . ?
C6C C5C C4C 122(8) . . ?
C5C C6C C1C 121(9) . . ?
C12B C7B C8B 120(2) . . ?
C12B C7B P1B 120(2) . . ?
C8B C7B P1B 120.0(19) . . ?
C9B C8B C7B 117(2) . . ?
C10B C9B C8B 120(3) . . ?
C9B C10B C11B 127(3) . . ?
C10B C11B C12B 116(3) . . ?
C7B C12B C11B 119(3) . . ?
C14B C13B C18B 118(2) . . ?
C14B C13B P1B 121.6(19) . . ?
C18B C13B P1B 120.5(17) . . ?
C13B C14B C15B 120(2) . . ?
C16B C15B C14B 118(2) . . ?
C15B C16B C17B 124(2) . . ?
C18B C17B C16B 119(2) . . ?
C17B C18B C13B 120(2) . . ?
C24B C19B C20B 119(3) . . ?
C24B C19B P1B 123(2) . . ?
C20B C19B P1B 117(2) . . ?
C19B C20B C21B 117(3) . . ?
C22B C21B C20B 122(3) . . ?
C21B C22B C23B 117(3) . . ?
C24B C23B C22B 119(3) . . ?
C19B C24B C23B 123(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 O1 2.289(12) . ?
Re1 Cl4 2.290(5) . ?
Re1 Cl5 2.304(5) . ?
Re1 Cl3 2.407(6) . ?
Re1 Cl1 2.427(6) . ?
Re1 Re2 2.4467(10) . ?
Re1 Re3 2.4478(10) . ?
Re2 Cl6 2.310(5) . ?
Re2 Cl8 2.318(5) . ?
Re2 Cl1 2.397(5) . ?
Re2 Cl2 2.404(4) . ?
Re2 Re3 2.4662(10) . ?
Re2 Cl7 2.563(5) . ?
Re3 Cl11 2.295(4) . ?
Re3 Cl9 2.314(5) . ?
Re3 Cl2 2.403(5) . ?
Re3 Cl3 2.416(5) . ?
Re3 Cl10 2.542(5) . ?
O1 C1 1.36(3) . ?
P1A C7A 1.79(2) . ?
P1A C19A 1.80(2) . ?
P1A C1A 1.813(19) . ?
P1A C13A 1.825(19) . ?
C1A C2A 1.34(3) . ?
C1A C6A 1.41(3) . ?
C2A C3A 1.37(3) . ?
C3A C4A 1.43(3) . ?
C4A C5A 1.38(3) . ?
C5A C6A 1.37(3) . ?
C7A C12A 1.37(4) . ?
C7A C8A 1.43(4) . ?
C8A C9A 1.32(3) . ?
C9A C10A 1.29(4) . ?
C10A C11A 1.44(4) . ?
C11A C12A 1.35(3) . ?
C13A C14A 1.33(3) . ?
C13A C18A 1.40(3) . ?
C14A C15A 1.43(3) . ?
C15A C16A 1.33(3) . ?
C16A C17A 1.38(3) . ?
C17A C18A 1.37(3) . ?
C19A C24A 1.38(3) . ?
C19A C20A 1.42(3) . ?
C20A C21A 1.41(3) . ?
C21A C22A 1.35(3) . ?
C22A C23A 1.36(3) . ?
C23A C24A 1.34(3) . ?
P1B C19B 1.78(3) . ?
P1B C7B 1.78(3) . ?
P1B C1C 1.78(13) . ?
P1B C13B 1.79(2) . ?
P1B C1B 1.89(7) . ?
C1B C6B 1.23(6) . ?
C1B C2B 1.46(8) . ?
C2B C3B 1.48(5) . ?
C3B C4B 1.29(5) . ?
C4B C5B 1.39(6) . ?
C5B C6B 1.34(5) . ?
C1C C6C 1.42(13) . ?
C1C C2C 1.53(17) . ?
C2C C3C 1.32(9) . ?
C3C C4C 1.53(10) . ?
C4C C5C 1.36(13) . ?
C5C C6C 1.31(9) . ?
C7B C12B 1.35(3) . ?
C7B C8B 1.45(4) . ?
C8B C9B 1.39(4) . ?
C9B C10B 1.30(3) . ?
C10B C11B 1.31(4) . ?
C11B C12B 1.48(3) . ?
C13B C14B 1.37(3) . ?
C13B C18B 1.42(3) . ?
C14B C15B 1.41(3) . ?
C15B C16B 1.28(3) . ?
C16B C17B 1.38(3) . ?
C17B C18B 1.33(3) . ?
C19B C24B 1.27(4) . ?
C19B C20B 1.42(3) . ?
C20B C21B 1.43(4) . ?
C21B C22B 1.31(4) . ?
C22B C23B 1.42(3) . ?
C23B C24B 1.39(4) . ?
O1S C1S 1.39(2) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Re1 Re2 Cl6 85.0(7) . . . . ?
Cl4 Re1 Re2 Cl6 0.2(2) . . . . ?
Cl5 Re1 Re2 Cl6 168.52(19) . . . . ?
Cl3 Re1 Re2 Cl6 -95.5(2) . . . . ?
Cl1 Re1 Re2 Cl6 84.6(2) . . . . ?
Re3 Re1 Re2 Cl6 -95.22(13) . . . . ?
O1 Re1 Re2 Cl8 -83.8(7) . . . . ?
Cl4 Re1 Re2 Cl8 -168.7(2) . . . . ?
Cl5 Re1 Re2 Cl8 -0.32(19) . . . . ?
Cl3 Re1 Re2 Cl8 95.7(2) . . . . ?
Cl1 Re1 Re2 Cl8 -84.3(2) . . . . ?
Re3 Re1 Re2 Cl8 95.94(12) . . . . ?
O1 Re1 Re2 Cl1 0.5(7) . . . . ?
Cl4 Re1 Re2 Cl1 -84.4(2) . . . . ?
Cl5 Re1 Re2 Cl1 84.0(2) . . . . ?
Cl3 Re1 Re2 Cl1 180.0(2) . . . . ?
Re3 Re1 Re2 Cl1 -179.78(16) . . . . ?
O1 Re1 Re2 Cl2 -179.5(7) . . . . ?
Cl4 Re1 Re2 Cl2 95.6(2) . . . . ?
Cl5 Re1 Re2 Cl2 -96.0(2) . . . . ?
Cl3 Re1 Re2 Cl2 0.0(2) . . . . ?
Cl1 Re1 Re2 Cl2 180.0(2) . . . . ?
Re3 Re1 Re2 Cl2 0.22(14) . . . . ?
O1 Re1 Re2 Re3 -179.8(7) . . . . ?
Cl4 Re1 Re2 Re3 95.40(18) . . . . ?
Cl5 Re1 Re2 Re3 -96.26(14) . . . . ?
Cl3 Re1 Re2 Re3 -0.23(15) . . . . ?
Cl1 Re1 Re2 Re3 179.78(16) . . . . ?
O1 Re1 Re2 Cl7 3.0(8) . . . . ?
Cl4 Re1 Re2 Cl7 -81.8(3) . . . . ?
Cl5 Re1 Re2 Cl7 86.5(3) . . . . ?
Cl3 Re1 Re2 Cl7 -177.5(3) . . . . ?
Cl1 Re1 Re2 Cl7 2.5(3) . . . . ?
Re3 Re1 Re2 Cl7 -177.2(3) . . . . ?
O1 Re1 Re3 Cl11 85.6(8) . . . . ?
Cl4 Re1 Re3 Cl11 169.2(2) . . . . ?
Cl5 Re1 Re3 Cl11 2.69(19) . . . . ?
Cl3 Re1 Re3 Cl11 85.6(2) . . . . ?
Cl1 Re1 Re3 Cl11 -94.4(2) . . . . ?
Re2 Re1 Re3 Cl11 -94.14(13) . . . . ?
O1 Re1 Re3 Cl9 -85.8(8) . . . . ?
Cl4 Re1 Re3 Cl9 -2.2(2) . . . . ?
Cl5 Re1 Re3 Cl9 -168.71(19) . . . . ?
Cl3 Re1 Re3 Cl9 -85.8(2) . . . . ?
Cl1 Re1 Re3 Cl9 94.3(2) . . . . ?
Re2 Re1 Re3 Cl9 94.47(13) . . . . ?
O1 Re1 Re3 Cl2 179.5(8) . . . . ?
Cl4 Re1 Re3 Cl2 -96.9(2) . . . . ?
Cl5 Re1 Re3 Cl2 96.6(2) . . . . ?
Cl3 Re1 Re3 Cl2 179.6(2) . . . . ?
Cl1 Re1 Re3 Cl2 -0.4(2) . . . . ?
Re2 Re1 Re3 Cl2 -0.22(14) . . . . ?
O1 Re1 Re3 Cl3 0.0(8) . . . . ?
Cl4 Re1 Re3 Cl3 83.6(2) . . . . ?
Cl5 Re1 Re3 Cl3 -82.9(2) . . . . ?
Cl1 Re1 Re3 Cl3 -180.0(2) . . . . ?
Re2 Re1 Re3 Cl3 -179.77(15) . . . . ?
O1 Re1 Re3 Re2 179.7(8) . . . . ?
Cl4 Re1 Re3 Re2 -96.63(17) . . . . ?
Cl5 Re1 Re3 Re2 96.83(15) . . . . ?
Cl3 Re1 Re3 Re2 179.77(15) . . . . ?
Cl1 Re1 Re3 Re2 -0.21(15) . . . . ?
O1 Re1 Re3 Cl10 -2.1(8) . . . . ?
Cl4 Re1 Re3 Cl10 81.6(3) . . . . ?
Cl5 Re1 Re3 Cl10 -85.0(3) . . . . ?
Cl3 Re1 Re3 Cl10 -2.0(3) . . . . ?
Cl1 Re1 Re3 Cl10 178.0(3) . . . . ?
Re2 Re1 Re3 Cl10 178.2(2) . . . . ?
Cl6 Re2 Re3 Cl11 -169.28(18) . . . . ?
Cl8 Re2 Re3 Cl11 1.15(18) . . . . ?
Cl1 Re2 Re3 Cl11 96.0(2) . . . . ?
Cl2 Re2 Re3 Cl11 -84.03(19) . . . . ?
Re1 Re2 Re3 Cl11 95.75(13) . . . . ?
Cl7 Re2 Re3 Cl11 -86.8(3) . . . . ?
Cl6 Re2 Re3 Cl9 -0.09(18) . . . . ?
Cl8 Re2 Re3 Cl9 170.34(18) . . . . ?
Cl1 Re2 Re3 Cl9 -94.8(2) . . . . ?
Cl2 Re2 Re3 Cl9 85.16(19) . . . . ?
Re1 Re2 Re3 Cl9 -95.06(13) . . . . ?
Cl7 Re2 Re3 Cl9 82.4(3) . . . . ?
Cl6 Re2 Re3 Cl2 -85.2(2) . . . . ?
Cl8 Re2 Re3 Cl2 85.18(19) . . . . ?
Cl1 Re2 Re3 Cl2 180.0(2) . . . . ?
Re1 Re2 Re3 Cl2 179.78(15) . . . . ?
Cl7 Re2 Re3 Cl2 -2.8(3) . . . . ?
Cl6 Re2 Re3 Cl3 95.2(2) . . . . ?
Cl8 Re2 Re3 Cl3 -94.4(2) . . . . ?
Cl1 Re2 Re3 Cl3 0.4(2) . . . . ?
Cl2 Re2 Re3 Cl3 -179.6(2) . . . . ?
Re1 Re2 Re3 Cl3 0.23(15) . . . . ?
Cl7 Re2 Re3 Cl3 177.7(3) . . . . ?
Cl6 Re2 Re3 Re1 94.98(13) . . . . ?
Cl8 Re2 Re3 Re1 -94.60(13) . . . . ?
Cl1 Re2 Re3 Re1 0.22(16) . . . . ?
Cl2 Re2 Re3 Re1 -179.78(15) . . . . ?
Cl7 Re2 Re3 Re1 177.4(2) . . . . ?
Cl6 Re2 Re3 Cl10 -83.1(3) . . . . ?
Cl8 Re2 Re3 Cl10 87.4(3) . . . . ?
Cl1 Re2 Re3 Cl10 -177.8(3) . . . . ?
Cl2 Re2 Re3 Cl10 2.2(3) . . . . ?
Re1 Re2 Re3 Cl10 -178.0(3) . . . . ?
Cl7 Re2 Re3 Cl10 -0.6(4) . . . . ?
Cl6 Re2 Cl1 Re1 -100.26(16) . . . . ?
Cl8 Re2 Cl1 Re1 100.38(15) . . . . ?
Cl2 Re2 Cl1 Re1 0(11) . . . . ?
Re3 Re2 Cl1 Re1 -0.22(16) . . . . ?
Cl7 Re2 Cl1 Re1 -178.78(14) . . . . ?
O1 Re1 Cl1 Re2 -179.8(4) . . . . ?
Cl4 Re1 Cl1 Re2 101.92(16) . . . . ?
Cl5 Re1 Cl1 Re2 -102.71(15) . . . . ?
Cl3 Re1 Cl1 Re2 -1(12) . . . . ?
Re3 Re1 Cl1 Re2 0.22(16) . . . . ?
Cl11 Re3 Cl2 Re2 99.99(14) . . . . ?
Cl9 Re3 Cl2 Re2 -99.40(15) . . . . ?
Cl3 Re3 Cl2 Re2 12(6) . . . . ?
Re1 Re3 Cl2 Re2 0.22(14) . . . . ?
Cl10 Re3 Cl2 Re2 -178.95(14) . . . . ?
Cl6 Re2 Cl2 Re3 100.04(16) . . . . ?
Cl8 Re2 Cl2 Re3 -100.59(15) . . . . ?
Cl1 Re2 Cl2 Re3 0(11) . . . . ?
Re1 Re2 Cl2 Re3 -0.22(14) . . . . ?
Cl7 Re2 Cl2 Re3 178.56(14) . . . . ?
O1 Re1 Cl3 Re3 180.0(4) . . . . ?
Cl4 Re1 Cl3 Re3 -101.70(16) . . . . ?
Cl5 Re1 Cl3 Re3 102.94(15) . . . . ?
Cl1 Re1 Cl3 Re3 1(12) . . . . ?
Re2 Re1 Cl3 Re3 0.23(16) . . . . ?
Cl11 Re3 Cl3 Re1 -99.96(14) . . . . ?
Cl9 Re3 Cl3 Re1 99.38(15) . . . . ?
Cl2 Re3 Cl3 Re1 -12(6) . . . . ?
Re2 Re3 Cl3 Re1 -0.23(15) . . . . ?
Cl10 Re3 Cl3 Re1 178.94(15) . . . . ?
Cl4 Re1 O1 C1 10(2) . . . . ?
Cl5 Re1 O1 C1 -172(2) . . . . ?
Cl3 Re1 O1 C1 99(2) . . . . ?
Cl1 Re1 O1 C1 -81(2) . . . . ?
Re2 Re1 O1 C1 -81(2) . . . . ?
Re3 Re1 O1 C1 99(2) . . . . ?
C7A P1A C1A C2A -54(2) . . . . ?
C19A P1A C1A C2A 64(2) . . . . ?
C13A P1A C1A C2A -176.3(17) . . . . ?
C7A P1A C1A C6A 124.4(19) . . . . ?
C19A P1A C1A C6A -117.3(18) . . . . ?
C13A P1A C1A C6A 2(2) . . . . ?
C6A C1A C2A C3A 2(3) . . . . ?
P1A C1A C2A C3A -179.8(17) . . . . ?
C1A C2A C3A C4A -1(3) . . . . ?
C2A C3A C4A C5A -4(3) . . . . ?
C3A C4A C5A C6A 8(3) . . . . ?
C4A C5A C6A C1A -6(3) . . . . ?
C2A C1A C6A C5A 2(3) . . . . ?
P1A C1A C6A C5A -176.7(16) . . . . ?
C19A P1A C7A C12A 159(2) . . . . ?
C1A P1A C7A C12A -81(2) . . . . ?
C13A P1A C7A C12A 37(3) . . . . ?
C19A P1A C7A C8A -26(2) . . . . ?
C1A P1A C7A C8A 94(2) . . . . ?
C13A P1A C7A C8A -147.6(19) . . . . ?
C12A C7A C8A C9A 0(4) . . . . ?
P1A C7A C8A C9A -175(2) . . . . ?
C7A C8A C9A C10A -2(4) . . . . ?
C8A C9A C10A C11A 3(4) . . . . ?
C9A C10A C11A C12A -1(4) . . . . ?
C10A C11A C12A C7A -1(4) . . . . ?
C8A C7A C12A C11A 1(4) . . . . ?
P1A C7A C12A C11A 177(2) . . . . ?
C7A P1A C13A C14A -55(2) . . . . ?
C19A P1A C13A C14A -175.2(18) . . . . ?
C1A P1A C13A C14A 65(2) . . . . ?
C7A P1A C13A C18A 131.7(16) . . . . ?
C19A P1A C13A C18A 11.0(18) . . . . ?
C1A P1A C13A C18A -108.9(16) . . . . ?
C18A C13A C14A C15A 3(3) . . . . ?
P1A C13A C14A C15A -170.7(16) . . . . ?
C13A C14A C15A C16A -1(3) . . . . ?
C14A C15A C16A C17A -1(3) . . . . ?
C15A C16A C17A C18A 1(3) . . . . ?
C16A C17A C18A C13A 1(3) . . . . ?
C14A C13A C18A C17A -3(3) . . . . ?
P1A C13A C18A C17A 170.8(16) . . . . ?
C7A P1A C19A C24A 117(2) . . . . ?
C1A P1A C19A C24A -2(2) . . . . ?
C13A P1A C19A C24A -119.3(19) . . . . ?
C7A P1A C19A C20A -60(2) . . . . ?
C1A P1A C19A C20A -178.6(16) . . . . ?
C13A P1A C19A C20A 64.0(19) . . . . ?
C24A C19A C20A C21A 1(3) . . . . ?
P1A C19A C20A C21A 177.6(16) . . . . ?
C19A C20A C21A C22A 0(3) . . . . ?
C20A C21A C22A C23A 0(3) . . . . ?
C21A C22A C23A C24A -1(4) . . . . ?
C22A C23A C24A C19A 2(3) . . . . ?
C20A C19A C24A C23A -2(3) . . . . ?
P1A C19A C24A C23A -178.7(17) . . . . ?
C19B P1B C1B C6B -69(8) . . . . ?
C7B P1B C1B C6B 50(8) . . . . ?
C1C P1B C1B C6B -165(66) . . . . ?
C13B P1B C1B C6B 169(7) . . . . ?
C19B P1B C1B C2B 95(5) . . . . ?
C7B P1B C1B C2B -146(4) . . . . ?
C1C P1B C1B C2B -2(55) . . . . ?
C13B P1B C1B C2B -27(6) . . . . ?
C6B C1B C2B C3B -14(10) . . . . ?
P1B C1B C2B C3B -178(4) . . . . ?
C1B C2B C3B C4B 9(7) . . . . ?
C2B C3B C4B C5B 2(8) . . . . ?
C3B C4B C5B C6B -9(8) . . . . ?
C2B C1B C6B C5B 9(12) . . . . ?
P1B C1B C6B C5B 170(5) . . . . ?
C4B C5B C6B C1B 3(9) . . . . ?
C19B P1B C1C C6C -30(11) . . . . ?
C7B P1B C1C C6C 92(11) . . . . ?
C13B P1B C1C C6C -149(9) . . . . ?
C1B P1B C1C C6C 56(52) . . . . ?
C19B P1B C1C C2C 176(7) . . . . ?
C7B P1B C1C C2C -61(9) . . . . ?
C13B P1B C1C C2C 57(9) . . . . ?
C1B P1B C1C C2C -98(63) . . . . ?
C6C C1C C2C C3C 8(15) . . . . ?
P1B C1C C2C C3C 163(7) . . . . ?
C1C C2C C3C C4C -3(12) . . . . ?
C2C C3C C4C C5C 6(11) . . . . ?
C3C C4C C5C C6C -16(13) . . . . ?
C4C C5C C6C C1C 21(14) . . . . ?
C2C C1C C6C C5C -17(14) . . . . ?
P1B C1C C6C C5C -174(8) . . . . ?
C19B P1B C7B C12B -21(3) . . . . ?
C1C P1B C7B C12B -145(5) . . . . ?
C13B P1B C7B C12B 97(3) . . . . ?
C1B P1B C7B C12B -141(3) . . . . ?
C19B P1B C7B C8B 159(2) . . . . ?
C1C P1B C7B C8B 35(5) . . . . ?
C13B P1B C7B C8B -83(3) . . . . ?
C1B P1B C7B C8B 40(3) . . . . ?
C12B C7B C8B C9B -5(4) . . . . ?
P1B C7B C8B C9B 175(2) . . . . ?
C7B C8B C9B C10B -1(4) . . . . ?
C8B C9B C10B C11B 5(5) . . . . ?
C9B C10B C11B C12B -3(5) . . . . ?
C8B C7B C12B C11B 7(4) . . . . ?
P1B C7B C12B C11B -172.4(19) . . . . ?
C10B C11B C12B C7B -3(4) . . . . ?
C19B P1B C13B C14B 120(3) . . . . ?
C7B P1B C13B C14B 2(3) . . . . ?
C1C P1B C13B C14B -120(6) . . . . ?
C1B P1B C13B C14B -116(4) . . . . ?
C19B P1B C13B C18B -54(3) . . . . ?
C7B P1B C13B C18B -172(2) . . . . ?
C1C P1B C13B C18B 67(6) . . . . ?
C1B P1B C13B C18B 70(4) . . . . ?
C18B C13B C14B C15B -3(4) . . . . ?
P1B C13B C14B C15B -178(2) . . . . ?
C13B C14B C15B C16B -3(4) . . . . ?
C14B C15B C16B C17B 7(5) . . . . ?
C15B C16B C17B C18B -3(5) . . . . ?
C16B C17B C18B C13B -4(4) . . . . ?
C14B C13B C18B C17B 7(4) . . . . ?
P1B C13B C18B C17B -179(2) . . . . ?
C7B P1B C19B C24B 121(3) . . . . ?
C1C P1B C19B C24B -113(5) . . . . ?
C13B P1B C19B C24B 4(3) . . . . ?
C1B P1B C19B C24B -121(3) . . . . ?
C7B P1B C19B C20B -65(3) . . . . ?
C1C P1B C19B C20B 60(5) . . . . ?
C13B P1B C19B C20B 177(2) . . . . ?
C1B P1B C19B C20B 52(3) . . . . ?
C24B C19B C20B C21B -8(5) . . . . ?
P1B C19B C20B C21B 178(2) . . . . ?
C19B C20B C21B C22B 5(5) . . . . ?
C20B C21B C22B C23B -5(5) . . . . ?
C21B C22B C23B C24B 8(5) . . . . ?
C20B C19B C24B C23B 12(5) . . . . ?
P1B C19B C24B C23B -175(2) . . . . ?
C22B C23B C24B C19B -12(5) . . . . ?
