#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:24:39 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179326 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/23/4322319.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4322319
loop_
_publ_author_name
'Corinne Rancurel'
'Daniel B. Leznoff'
'Jean-Pascal Sutter'
'Stéphane Golhen'
'Lahcène Ouahab'
'Janis Kliava'
'Olivier Kahn'
_publ_section_title
;
 Synthesis, Structure, and Magnetism of Mono- and Binuclear Manganese(II)
 Compounds of Nitronyl Nitroxide Substituted Phosphine Oxides
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4753
_journal_page_last               4758
_journal_paper_doi               10.1021/ic990527g
_journal_volume                  38
_journal_year                    1999
_chemical_formula_sum            'C70 H56 F24 Mn2 N4 O14 P2'
_chemical_formula_weight         1805.01
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 98.49(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.463(6)
_cell_length_b                   19.315(3)
_cell_length_c                   17.084(9)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      10.930
_cell_measurement_theta_min      5.240
_cell_volume                     4067(3)
_computing_cell_refinement       'Nonius CAD4'
_computing_data_collection       'Nonius CAD4'
_computing_data_reduction        MolEN
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.968
_diffrn_measured_fraction_theta_max 0.968
_diffrn_measurement_device_type  'Enraf-Nonius CAD4'
_diffrn_measurement_method       q\2q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0294
_diffrn_reflns_av_sigmaI/netI    0.0811
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            8346
_diffrn_reflns_theta_full        25.97
_diffrn_reflns_theta_max         25.97
_diffrn_reflns_theta_min         1.21
_diffrn_standards_decay_%        0.3
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.466
_exptl_absorpt_correction_T_max  0.999837
_exptl_absorpt_correction_T_min  0.983021
_exptl_absorpt_correction_type   '\y scan'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.474
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallelepipedic
_exptl_crystal_F_000             1824
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.644
_refine_diff_density_min         -0.572
_refine_diff_density_rms         0.067
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     523
_refine_ls_number_reflns         7961
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.1706
_refine_ls_R_factor_gt           0.0683
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1089P)²+2.1057P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1775
_refine_ls_wR_factor_ref         0.2213
_reflns_number_gt                3936
_reflns_number_total             7961
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic990527g_2.cif
_cod_data_source_block           4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.1089P)^2^+2.1057P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.1089P)^2^+2.1057P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_database_code               4322319
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x-1/2, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Mn1 Mn 0.88641(6) 0.50868(4) 0.25432(4) 0.0515(3) Uani 1 d . . .
O4 O 0.9913(3) 0.4419(2) 0.3354(2) 0.0644(10) Uani 1 d D . .
C27 C 1.0468(5) 0.3939(3) 0.3153(3) 0.0649(15) Uani 1 d D . .
C26 C 1.0802(9) 0.3421(5) 0.3821(5) 0.114(3) Uani 1 d D . .
F1 F 1.0703(5) 0.3610(3) 0.4509(3) 0.1356(19) Uani 1 d D . .
F2 F 1.1876(8) 0.3344(6) 0.3899(5) 0.264(6) Uani 1 d D . .
F3 F 1.0527(12) 0.2850(4) 0.3698(4) 0.299(8) Uani 1 d D . .
O3 O 1.0005(4) 0.4805(2) 0.1766(2) 0.0717(11) Uani 1 d D . .
C29 C 1.0523(5) 0.4255(3) 0.1793(3) 0.0685(16) Uani 1 d D . .
C30 C 1.0748(12) 0.4023(5) 0.0984(6) 0.184(7) Uani 1 d D . .
F5 F 1.0698(8) 0.4431(4) 0.0463(3) 0.206(4) Uani 1 d D . .
F6 F 1.1861(9) 0.4061(12) 0.1084(5) 0.446(14) Uani 1 d D . .
F4 F 1.0828(16) 0.3464(4) 0.0845(5) 0.360(11) Uani 1 d D . .
C28 C 1.0785(6) 0.3811(3) 0.2432(4) 0.0778(19) Uani 1 d . . .
H28 H 1.1187 0.3415 0.2368 0.093 Uiso 1 calc R . .
O6 O 0.7697(3) 0.5527(2) 0.1635(2) 0.0629(10) Uani 1 d . . .
O5 O 0.7976(4) 0.4144(2) 0.2171(3) 0.0864(13) Uani 1 d . . .
F10 F 0.7037(4) 0.6245(2) 0.0323(2) 0.1060(14) Uani 1 d . . .
F11 F 0.5619(4) 0.5976(3) 0.0779(3) 0.139(2) Uani 1 d . . .
F12 F 0.6076(4) 0.5424(3) -0.0189(2) 0.1304(18) Uani 1 d . . .
F7 F 0.7778(10) 0.2952(5) 0.1182(11) 0.318(9) Uani 1 d . . .
F8 F 0.6312(12) 0.3173(4) 0.0869(9) 0.329(9) Uani 1 d . . .
F9 F 0.6832(14) 0.2964(5) 0.1951(7) 0.291(8) Uani 1 d . . .
C35 C 0.6456(6) 0.5706(4) 0.0495(4) 0.0802(19) Uani 1 d . . .
C34 C 0.7086(4) 0.5220(3) 0.1096(3) 0.0616(15) Uani 1 d . . .
C33 C 0.6893(5) 0.4523(4) 0.1006(4) 0.0797(19) Uani 1 d . . .
H33 H 0.6437 0.4372 0.0558 0.096 Uiso 1 calc R . .
C32 C 0.7338(6) 0.4040(4) 0.1539(5) 0.0824(19) Uani 1 d . . .
P1 P 0.71089(10) 0.53483(7) 0.39107(8) 0.0493(4) Uani 1 d . . .
N2 N 0.9411(3) 0.3758(2) 0.7418(2) 0.0481(10) Uani 1 d . . .
N1 N 0.7699(3) 0.3593(3) 0.7456(3) 0.0665(14) Uani 1 d . . .
O1 O 0.6668(4) 0.3556(3) 0.7249(3) 0.1115(19) Uani 1 d . . .
O2 O 0.9694(2) 0.60477(18) 0.28141(19) 0.0503(8) Uani 1 d . . .
O7 O 0.8053(3) 0.5370(2) 0.3472(2) 0.0654(11) Uani 1 d . . .
C31 C 0.7081(14) 0.3285(6) 0.1424(10) 0.151(5) Uani 1 d . . .
C4 C 0.7492(4) 0.4941(3) 0.4860(3) 0.0473(12) Uani 1 d . . .
C5 C 0.8496(4) 0.4622(3) 0.5019(3) 0.0476(12) Uani 1 d . . .
H5 H 0.8956 0.4622 0.4637 0.057 Uiso 1 calc R . .
C6 C 0.8817(4) 0.4306(3) 0.5739(3) 0.0468(12) Uani 1 d . . .
H6 H 0.9503 0.4108 0.5848 0.056 Uiso 1 calc R . .
C1 C 0.8118(4) 0.4282(2) 0.6303(3) 0.0449(12) Uani 1 d . . .
C2 C 0.7134(4) 0.4612(3) 0.6154(3) 0.0578(14) Uani 1 d . . .
H2 H 0.6671 0.4609 0.6534 0.069 Uiso 1 calc R . .
C3 C 0.6828(4) 0.4945(3) 0.5448(3) 0.0650(16) Uani 1 d . . .
H3 H 0.6167 0.5177 0.5360 0.078 Uiso 1 calc R . .
C9 C 0.9410(4) 0.3238(3) 0.8079(3) 0.0574(14) Uani 1 d . . .
C7 C 0.8410(4) 0.3895(3) 0.7046(3) 0.0492(12) Uani 1 d . . .
C8 C 0.8214(5) 0.3334(4) 0.8252(4) 0.0746(19) Uani 1 d . . .
C10 C 0.7685(5) 0.2667(5) 0.8456(6) 0.127(4) Uani 1 d . . .
H10A H 0.7783 0.2320 0.8070 0.191 Uiso 1 calc R . .
H10B H 0.6924 0.2744 0.8457 0.191 Uiso 1 calc R . .
H10C H 0.8013 0.2514 0.8970 0.191 Uiso 1 calc R . .
C11 C 0.8080(6) 0.3895(5) 0.8843(4) 0.103(3) Uani 1 d . . .
H11A H 0.8418 0.4313 0.8697 0.154 Uiso 1 calc R . .
H11B H 0.8415 0.3752 0.9360 0.154 Uiso 1 calc R . .
H11C H 0.7322 0.3978 0.8849 0.154 Uiso 1 calc R . .
C12 C 0.9652(5) 0.2546(3) 0.7732(4) 0.0769(18) Uani 1 d . . .
H12A H 0.9092 0.2435 0.7302 0.115 Uiso 1 calc R . .
H12B H 0.9680 0.2196 0.8133 0.115 Uiso 1 calc R . .
H12C H 1.0338 0.2569 0.7541 0.115 Uiso 1 calc R . .
C13 C 1.0273(4) 0.3431(3) 0.8759(3) 0.0658(16) Uani 1 d . . .
H13A H 1.0095 0.3868 0.8974 0.099 Uiso 1 calc R . .
H13B H 1.0962 0.3466 0.8574 0.099 Uiso 1 calc R . .
H13C H 1.0311 0.3082 0.9162 0.099 Uiso 1 calc R . .
C14 C 0.6676(4) 0.6206(3) 0.4102(3) 0.0557(14) Uani 1 d . . .
C15 C 0.5673(6) 0.6337(4) 0.4335(4) 0.0805(19) Uani 1 d . . .
H15 H 0.5166 0.5983 0.4333 0.097 Uiso 1 calc R . .
C16 C 0.5435(8) 0.6998(4) 0.4569(5) 0.105(3) Uani 1 d . . .
H16 H 0.4771 0.7089 0.4735 0.126 Uiso 1 calc R . .
C17 C 0.6162(10) 0.7506(5) 0.4557(5) 0.116(3) Uani 1 d . . .
H17 H 0.5996 0.7946 0.4726 0.139 Uiso 1 calc R . .
C18 C 0.7127(8) 0.7403(4) 0.4306(5) 0.103(3) Uani 1 d . . .
H18 H 0.7606 0.7770 0.4284 0.124 Uiso 1 calc R . .
C19 C 0.7390(5) 0.6755(4) 0.4087(4) 0.0778(19) Uani 1 d . . .
H19 H 0.8060 0.6678 0.3924 0.093 Uiso 1 calc R . .
C20 C 0.5972(4) 0.4890(3) 0.3395(3) 0.0549(13) Uani 1 d . . .
C21 C 0.5414(5) 0.5169(4) 0.2717(3) 0.0735(18) Uani 1 d . . .
H21 H 0.5588 0.5610 0.2559 0.088 Uiso 1 calc R . .
C22 C 0.4605(6) 0.4804(5) 0.2272(4) 0.095(2) Uani 1 d . . .
H22 H 0.4241 0.4997 0.1810 0.114 Uiso 1 calc R . .
C23 C 0.4325(7) 0.4159(6) 0.2497(6) 0.113(3) Uani 1 d . . .
H23 H 0.3779 0.3913 0.2186 0.135 Uiso 1 calc R . .
C24 C 0.4843(7) 0.3880(5) 0.3172(7) 0.129(3) Uani 1 d . . .
H24 H 0.4639 0.3445 0.3333 0.155 Uiso 1 calc R . .
C25 C 0.5670(5) 0.4233(4) 0.3624(5) 0.089(2) Uani 1 d . . .
H25 H 0.6030 0.4034 0.4085 0.106 Uiso 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O7 Mn1 O6 95.39(15) . . ?
O7 Mn1 O2 83.13(15) . . ?
O6 Mn1 O2 93.86(14) . . ?
O7 Mn1 O3 167.88(16) . . ?
O6 Mn1 O3 95.36(15) . . ?
O2 Mn1 O3 90.58(15) . . ?
O7 Mn1 O5 99.23(18) . . ?
O6 Mn1 O5 81.88(16) . . ?
O2 Mn1 O5 175.28(16) . . ?
O3 Mn1 O5 87.82(18) . . ?
O7 Mn1 O4 89.09(15) . . ?
O6 Mn1 O4 167.17(15) . . ?
O2 Mn1 O4 98.62(14) . . ?
O3 Mn1 O4 81.60(15) . . ?
O5 Mn1 O4 85.54(16) . . ?
C27 O4 Mn1 125.1(4) . . ?
O4 C27 C28 129.2(5) . . ?
O4 C27 C26 112.7(6) . . ?
C28 C27 C26 118.1(6) . . ?
F3 C26 F1 112.3(10) . . ?
F3 C26 F2 100.2(10) . . ?
F1 C26 F2 100.1(9) . . ?
F3 C26 C27 116.4(8) . . ?
F1 C26 C27 117.0(7) . . ?
F2 C26 C27 107.8(8) . . ?
C29 O3 Mn1 125.5(4) . . ?
O3 C29 C28 128.3(5) . . ?
O3 C29 C30 112.6(6) . . ?
C28 C29 C30 118.7(6) . . ?
F4 C30 F5 118.8(10) . . ?
F4 C30 F6 87.6(12) . . ?
F5 C30 F6 89.9(11) . . ?
F4 C30 C29 121.0(9) . . ?
F5 C30 C29 119.5(7) . . ?
F6 C30 C29 100.9(11) . . ?
C30 F6 F4 39.9(6) . . ?
C30 F4 F6 52.4(9) . . ?
C27 C28 C29 122.0(6) . . ?
C34 O6 Mn1 128.2(4) . . ?
C32 O5 Mn1 127.8(5) . . ?
F12 C35 F10 105.4(6) . . ?
F12 C35 F11 106.9(6) . . ?
F10 C35 F11 105.0(7) . . ?
F12 C35 C34 115.3(6) . . ?
F10 C35 C34 112.9(5) . . ?
F11 C35 C34 110.6(6) . . ?
O6 C34 C33 128.5(6) . . ?
O6 C34 C35 113.6(6) . . ?
C33 C34 C35 117.8(6) . . ?
C32 C33 C34 123.3(6) . . ?
O5 C32 C33 127.4(7) . . ?
O5 C32 C31 111.3(9) . . ?
C33 C32 C31 121.3(9) . . ?
O7 P1 C14 110.4(3) . . ?
O7 P1 C20 113.2(2) . . ?
C14 P1 C20 108.1(2) . . ?
O7 P1 C4 110.0(2) . . ?
C14 P1 C4 106.7(2) . . ?
C20 P1 C4 108.2(2) . . ?
O2 N2 C7 125.5(4) 3_766 . ?
O2 N2 C9 121.2(4) 3_766 . ?
C7 N2 C9 112.5(4) . . ?
O1 N1 C7 126.3(5) . . ?
O1 N1 C8 120.5(4) . . ?
C7 N1 C8 113.0(4) . . ?
N2 O2 Mn1 126.6(3) 3_766 . ?
P1 O7 Mn1 152.7(3) . . ?
F9 C31 F7 105.5(16) . . ?
F9 C31 F8 103.3(14) . . ?
F7 C31 F8 99.1(13) . . ?
F9 C31 C32 119.3(13) . . ?
F7 C31 C32 114.5(13) . . ?
F8 C31 C32 112.9(13) . . ?
C5 C4 C3 118.5(5) . . ?
C5 C4 P1 118.8(4) . . ?
C3 C4 P1 122.7(4) . . ?
C6 C5 C4 120.4(4) . . ?
C5 C6 C1 120.2(4) . . ?
C2 C1 C6 119.3(4) . . ?
C2 C1 C7 119.8(4) . . ?
C6 C1 C7 120.9(4) . . ?
C3 C2 C1 120.4(5) . . ?
C2 C3 C4 121.0(5) . . ?
C13 C9 C12 111.1(5) . . ?
C13 C9 N2 109.4(4) . . ?
C12 C9 N2 105.8(5) . . ?
C13 C9 C8 114.5(5) . . ?
C12 C9 C8 115.3(5) . . ?
N2 C9 C8 99.6(4) . . ?
N2 C7 N1 107.8(4) . . ?
N2 C7 C1 127.2(4) . . ?
N1 C7 C1 125.0(4) . . ?
N1 C8 C11 107.1(6) . . ?
N1 C8 C10 110.5(5) . . ?
C11 C8 C10 111.3(7) . . ?
N1 C8 C9 99.2(4) . . ?
C11 C8 C9 114.3(6) . . ?
C10 C8 C9 113.6(6) . . ?
C19 C14 C15 118.2(6) . . ?
C19 C14 P1 119.5(5) . . ?
C15 C14 P1 122.0(5) . . ?
C16 C15 C14 119.4(7) . . ?
C17 C16 C15 119.9(8) . . ?
C16 C17 C18 122.2(8) . . ?
C17 C18 C19 119.0(8) . . ?
C18 C19 C14 121.2(7) . . ?
C21 C20 C25 118.1(6) . . ?
C21 C20 P1 119.2(5) . . ?
C25 C20 P1 122.6(4) . . ?
C22 C21 C20 120.5(7) . . ?
C21 C22 C23 120.9(7) . . ?
C24 C23 C22 119.7(8) . . ?
C23 C24 C25 120.4(8) . . ?
C24 C25 C20 120.3(7) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Mn1 O7 2.076(4) . ?
Mn1 O6 2.140(4) . ?
Mn1 O2 2.142(3) . ?
Mn1 O3 2.153(4) . ?
Mn1 O5 2.177(4) . ?
Mn1 O4 2.181(4) . ?
O4 C27 1.236(6) . ?
C27 C28 1.371(8) . ?
C27 C26 1.528(9) . ?
C26 F3 1.164(10) . ?
C26 F1 1.254(8) . ?
C26 F2 1.333(12) . ?
O3 C29 1.241(6) . ?
C29 C28 1.388(8) . ?
C29 C30 1.519(9) . ?
C30 F4 1.113(9) . ?
C30 F5 1.184(9) . ?
C30 F6 1.373(15) . ?
F6 F4 1.732(18) . ?
O6 C34 1.254(6) . ?
O5 C32 1.259(8) . ?
F10 C35 1.324(8) . ?
F11 C35 1.321(8) . ?
F12 C35 1.313(7) . ?
F7 C31 1.201(16) . ?
F8 C31 1.263(14) . ?
F9 C31 1.172(16) . ?
C35 C34 1.521(9) . ?
C34 C33 1.373(9) . ?
C33 C32 1.362(10) . ?
C32 C31 1.500(12) . ?
P1 O7 1.486(4) . ?
P1 C14 1.787(6) . ?
P1 C20 1.789(5) . ?
P1 C4 1.802(5) . ?
N2 O2 1.294(5) 3_766 ?
N2 C7 1.340(6) . ?
N2 C9 1.510(6) . ?
N1 O1 1.283(6) . ?
N1 C7 1.342(6) . ?
N1 C8 1.501(7) . ?
O2 N2 1.294(5) 3_766 ?
C4 C5 1.384(7) . ?
C4 C3 1.392(7) . ?
C5 C6 1.380(7) . ?
C6 C1 1.392(7) . ?
C1 C2 1.373(7) . ?
C1 C7 1.471(7) . ?
C2 C3 1.371(7) . ?
C9 C13 1.509(7) . ?
C9 C12 1.510(8) . ?
C9 C8 1.573(8) . ?
C8 C11 1.508(10) . ?
C8 C10 1.511(9) . ?
C14 C19 1.387(8) . ?
C14 C15 1.390(8) . ?
C15 C16 1.383(10) . ?
C16 C17 1.339(11) . ?
C17 C18 1.350(12) . ?
C18 C19 1.361(10) . ?
C20 C21 1.370(8) . ?
C20 C25 1.395(8) . ?
C21 C22 1.366(9) . ?
C22 C23 1.364(11) . ?
C23 C24 1.347(12) . ?
C24 C25 1.375(10) . ?
