#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:24:39 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179326 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/23/4322330.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4322330
loop_
_publ_author_name
'Zhiping Zheng'
'Thomas G. Gray'
'R. H. Holm'
_publ_section_title
;
 Synthesis and Structures of Solvated Monoclusters and Bridged Di- and
 Triclusters Based on the cubic Building Block [Re6(μ3-Se)8]2+
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4888
_journal_page_last               4895
_journal_paper_doi               10.1021/ic9906050
_journal_volume                  38
_journal_year                    1999
_chemical_formula_sum            'C38 H70 F12 N2 O P4 Re6 Sb2 Se8'
_chemical_formula_weight         2915.22
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                111.83
_cell_angle_beta                 104.6840(10)
_cell_angle_gamma                94.8030(10)
_cell_formula_units_Z            1
_cell_length_a                   10.6065(2)
_cell_length_b                   13.1141(3)
_cell_length_c                   16.7533(4)
_cell_measurement_temperature    213(2)
_cell_volume                     2051.02(8)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      213(2)
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0509
_diffrn_reflns_av_sigmaI/netI    0.1411
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            13703
_diffrn_reflns_theta_max         28.27
_diffrn_reflns_theta_min         1.38
_exptl_absorpt_coefficient_mu    13.141
_exptl_crystal_density_diffrn    2.360
_exptl_crystal_F_000             1312
_refine_diff_density_max         7.015
_refine_diff_density_min         -6.290
_refine_diff_density_rms         0.545
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   0.938
_refine_ls_goodness_of_fit_obs   1.294
_refine_ls_matrix_type           full
_refine_ls_number_parameters     406
_refine_ls_number_reflns         9508
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.938
_refine_ls_restrained_S_obs      1.294
_refine_ls_R_factor_all          0.1125
_refine_ls_R_factor_obs          0.0675
_refine_ls_shift/esd_max         -0.007
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0826P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1789
_refine_ls_wR_factor_obs         0.1721
_reflns_number_observed          4778
_reflns_number_total             9508
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic9906050_08.cif
_cod_data_source_block           final
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0826P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0826P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2051.07(8)
_cod_database_code               4322330
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Re1 Re 0.16515(6) 0.47273(5) 0.05058(4) 0.0175(2) Uani 1 d . .
Re2 Re -0.04749(6) 0.51158(5) 0.10265(4) 0.0176(2) Uani 1 d . .
Re3 Re 0.07019(6) 0.65337(5) 0.05358(4) 0.0177(2) Uani 1 d . .
Se4 Se 0.1375(2) 0.31691(13) -0.10020(11) 0.0221(4) Uani 1 d . .
Se5 Se 0.1791(2) 0.63097(14) 0.19672(11) 0.0236(4) Uani 1 d . .
Se6 Se 0.2696(2) 0.60828(14) 0.00065(11) 0.0220(4) Uani 1 d . .
Se7 Se 0.0450(2) 0.33794(14) 0.09426(12) 0.0224(4) Uani 1 d . .
Sb1 Sb 0.6916(2) 1.0871(2) 0.24956(13) 0.0722(6) Uani 1 d . .
P1 P 0.3825(4) 0.4430(4) 0.1277(3) 0.0239(10) Uani 1 d . .
P3 P 0.1649(5) 0.8573(4) 0.1246(3) 0.0263(10) Uani 1 d . .
N1 N -0.0973(13) 0.5281(12) 0.2283(9) 0.027(3) Uani 1 d . .
F2 F 0.6221(21) 0.9848(15) 0.1342(11) 0.124(7) Uani 1 d . .
C2 C -0.1503(18) 0.4482(17) 0.3267(11) 0.034(5) Uani 1 d . .
H2A H -0.1782(18) 0.3833(17) 0.3341(11) 0.041 Uiso 1 calc R .
C4 C -0.0927(19) 0.6395(16) 0.3751(12) 0.038(5) Uani 1 d . .
H4A H -0.0801(19) 0.7123(16) 0.4196(12) 0.046 Uiso 1 calc R .
F3 F 0.7566(21) 1.1978(15) 0.3643(10) 0.125(8) Uani 1 d . .
C1 C -0.1338(16) 0.4412(15) 0.2473(12) 0.029(4) Uani 1 d . .
H1A H -0.1493(16) 0.3690(15) 0.2014(12) 0.035 Uiso 1 calc R .
C5 C -0.0764(21) 0.6306(15) 0.2941(11) 0.037(5) Uani 1 d . .
H5A H -0.0511(21) 0.6949(15) 0.2851(11) 0.045 Uiso 1 calc R .
C3 C -0.1250(18) 0.5536(17) 0.3968(12) 0.035(5) Uani 1 d . .
C15 C 0.4347(17) 0.3127(13) 0.0695(12) 0.028(4) Uani 1 d . .
H15A H 0.4342(17) 0.3071(13) 0.0095(12) 0.033 Uiso 1 calc R .
H15B H 0.5262(17) 0.3162(13) 0.1034(12) 0.033 Uiso 1 calc R .
C13 C 0.5296(17) 0.5456(15) 0.1497(14) 0.040(5) Uani 1 d . .
H13A H 0.6090(17) 0.5210(15) 0.1750(14) 0.048 Uiso 1 calc R .
H13B H 0.5335(17) 0.5457(15) 0.0919(14) 0.048 Uiso 1 calc R .
C6 C -0.1380(19) 0.5722(20) 0.4872(14) 0.046(6) Uani 1 d . .
C17 C 0.3046(20) 0.9023(16) 0.0932(14) 0.045(5) Uani 1 d . .
H17A H 0.3393(20) 0.9824(16) 0.1308(14) 0.054 Uiso 1 calc R .
H17B H 0.3753(20) 0.8623(16) 0.1071(14) 0.054 Uiso 1 calc R .
C19 C 0.2428(20) 0.9174(16) 0.2489(13) 0.050(6) Uani 1 d . .
H19A H 0.3063(20) 0.8722(16) 0.2640(13) 0.060 Uiso 1 calc R .
H19B H 0.2925(20) 0.9934(16) 0.2687(13) 0.060 Uiso 1 calc R .
C18 C 0.2737(21) 0.8839(17) -0.0044(14) 0.051(6) Uani 1 d . .
H18A H 0.3536(21) 0.9103(17) -0.0150(14) 0.076 Uiso 1 calc R .
H18B H 0.2058(21) 0.9250(17) -0.0187(14) 0.076 Uiso 1 calc R .
H18C H 0.2419(21) 0.8046(17) -0.0424(14) 0.076 Uiso 1 calc R .
C21 C 0.0390(19) 0.9428(14) 0.1045(12) 0.034(5) Uani 1 d . .
H21A H 0.0013(19) 0.9204(14) 0.0392(12) 0.040 Uiso 1 calc R .
H21B H -0.0334(19) 0.9271(14) 0.1274(12) 0.040 Uiso 1 calc R .
C11 C 0.3837(17) 0.4434(17) 0.2354(11) 0.033(4) Uani 1 d . .
H11A H 0.3622(17) 0.5143(17) 0.2706(11) 0.039 Uiso 1 calc R .
H11B H 0.3120(17) 0.3831(17) 0.2247(11) 0.039 Uiso 1 calc R .
F5 F 0.7465(28) 1.1944(18) 0.2103(13) 0.190(13) Uani 1 d . .
C20 C 0.1427(17) 0.9218(18) 0.3002(14) 0.048(6) Uani 1 d . .
H20A H 0.1890(17) 0.9538(18) 0.3645(14) 0.071 Uiso 1 calc R .
H20B H 0.0945(17) 0.8465(18) 0.2820(14) 0.071 Uiso 1 calc R .
H20C H 0.0807(17) 0.9678(18) 0.2867(14) 0.071 Uiso 1 calc R .
C14 C 0.5344(19) 0.6674(16) 0.2147(14) 0.048(6) Uani 1 d . .
H14A H 0.6151(19) 0.7154(16) 0.2222(14) 0.072 Uiso 1 calc R .
H14B H 0.5334(19) 0.6691(16) 0.2729(14) 0.072 Uiso 1 calc R .
H14C H 0.4577(19) 0.6939(16) 0.1896(14) 0.072 Uiso 1 calc R .
C7 C -0.2079(22) 0.4873(21) 0.5035(16) 0.055(6) Uani 1 d . .
H7A H -0.2473(22) 0.4169(21) 0.4559(16) 0.066 Uiso 1 calc R .
F4 F 0.6293(22) 0.9907(15) 0.2879(14) 0.134(8) Uani 1 d . .
C10 C -0.0819(23) 0.6721(20) 0.5617(14) 0.053(6) Uani 1 d . .
H10A H -0.0330(23) 0.7328(20) 0.5584(14) 0.064 Uiso 1 calc R .
C16 C 0.3433(18) 0.2039(15) 0.0588(15) 0.045(6) Uani 1 d . .
H16A H 0.3760(18) 0.1383(15) 0.0276(15) 0.067 Uiso 1 calc R .
H16B H 0.2528(18) 0.1988(15) 0.0240(15) 0.067 Uiso 1 calc R .
H16C H 0.3449(18) 0.2079(15) 0.1180(15) 0.067 Uiso 1 calc R .
F1 F 0.5302(19) 1.1368(17) 0.2409(17) 0.166(11) Uani 1 d . .
C12 C 0.5140(21) 0.4291(22) 0.2943(15) 0.064(7) Uani 1 d . .
H12A H 0.5020(21) 0.4307(22) 0.3502(15) 0.096 Uiso 1 calc R .
H12B H 0.5859(21) 0.4896(22) 0.3078(15) 0.096 Uiso 1 calc R .
H12C H 0.5355(21) 0.3579(22) 0.2617(15) 0.096 Uiso 1 calc R .
N2 N -0.1656(25) 0.6012(26) 0.6524(14) 0.086(8) Uani 1 d . .
C9 C -0.1015(26) 0.6773(25) 0.6392(17) 0.070(8) Uani 1 d . .
H9A H -0.0632(26) 0.7453(25) 0.6900(17) 0.084 Uiso 1 calc R .
C8 C -0.2177(28) 0.5072(26) 0.5855(16) 0.072(8) Uani 1 d . .
H8A H -0.2644(28) 0.4501(26) 0.5942(16) 0.086 Uiso 1 calc R .
F6 F 0.8502(20) 1.0475(24) 0.2535(17) 0.187(12) Uani 1 d . .
C22 C 0.0965(26) 1.0700(15) 0.1501(17) 0.069(8) Uani 1 d . .
H22A H 0.0267(26) 1.1102(15) 0.1373(17) 0.104 Uiso 1 calc R .
H22B H 0.1669(26) 1.0865(15) 0.1267(17) 0.104 Uiso 1 calc R .
H22C H 0.1322(26) 1.0932(15) 0.2149(17) 0.104 Uiso 1 calc R .
C24 C 0.4136(47) 1.2122(28) 0.4325(24) 0.143(22) Uani 1 d . .
H24A H 0.4380(47) 1.2184(28) 0.3816(24) 0.171 Uiso 1 calc R .
H24B H 0.3185(47) 1.1800(28) 0.4121(24) 0.171 Uiso 1 calc R .
C23 C 0.4978(49) 1.1371(33) 0.4693(23) 0.186(25) Uani 1 d . .
H23A H 0.4361(49) 1.0811(33) 0.4739(23) 0.223 Uiso 1 calc R .
H23B H 0.5391(49) 1.0964(33) 0.4240(23) 0.223 Uiso 1 calc R .
O O 0.6060(25) 1.1937(18) 0.5593(15) 0.128(10) Uani 1 d . .
C26 C 0.5542(32) 1.2954(26) 0.5737(23) 0.116(13) Uani 1 d . .
H26A H 0.6288(32) 1.3566(26) 0.5908(23) 0.140 Uiso 1 calc R .
H26B H 0.5209(32) 1.3116(26) 0.6257(23) 0.140 Uiso 1 calc R .
C25 C 0.4379(38) 1.2995(38) 0.4922(28) 0.140(17) Uani 1 d . .
H25A H 0.3589(38) 1.3156(38) 0.5110(28) 0.168 Uiso 1 calc R .
H25B H 0.4679(38) 1.3582(38) 0.4744(28) 0.168 Uiso 1 calc R .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Re1 Se5 88.35(12) . . ?
P1 Re1 Se4 95.26(12) . . ?
Se5 Re1 Se4 176.39(6) . . ?
P1 Re1 Se6 93.46(11) . . ?
Se5 Re1 Se6 90.35(6) . . ?
Se4 Re1 Se6 89.37(6) . . ?
P1 Re1 Se7 90.52(11) . . ?
Se5 Re1 Se7 90.13(6) . . ?
Se4 Re1 Se7 89.90(6) . . ?
Se6 Re1 Se7 176.00(6) . . ?
P1 Re1 Re3 136.49(11) . 2_565 ?
Se5 Re1 Re3 118.41(5) . 2_565 ?
Se4 Re1 Re3 58.74(4) . 2_565 ?
Se6 Re1 Re3 118.03(5) . 2_565 ?
Se7 Re1 Re3 58.39(4) . 2_565 ?
P1 Re1 Re3 133.45(11) . . ?
Se5 Re1 Re3 58.50(4) . . ?
Se4 Re1 Re3 118.46(5) . . ?
Se6 Re1 Re3 58.61(4) . . ?
Se7 Re1 Re3 118.51(5) . . ?
Re3 Re1 Re3 89.85(3) 2_565 . ?
P1 Re1 Re2 131.43(11) . . ?
Se5 Re1 Re2 58.39(4) . . ?
Se4 Re1 Re2 118.75(5) . . ?
Se6 Re1 Re2 118.56(5) . . ?
Se7 Re1 Re2 58.56(4) . . ?
Re3 Re1 Re2 60.03(2) 2_565 . ?
Re3 Re1 Re2 59.97(2) . . ?
P1 Re1 Re2 138.53(11) . 2_565 ?
Se5 Re1 Re2 118.43(5) . 2_565 ?
Se4 Re1 Re2 58.53(4) . 2_565 ?
Se6 Re1 Re2 58.15(4) . 2_565 ?
Se7 Re1 Re2 118.27(5) . 2_565 ?
Re3 Re1 Re2 59.89(2) 2_565 2_565 ?
Re3 Re1 Re2 59.94(2) . 2_565 ?
Re2 Re1 Re2 90.00(3) . 2_565 ?
N1 Re2 Se6 93.8(4) . 2_565 ?
N1 Re2 Se5 90.1(4) . . ?
Se6 Re2 Se5 176.09(7) 2_565 . ?
N1 Re2 Se7 91.8(4) . . ?
Se6 Re2 Se7 90.09(6) 2_565 . ?
Se5 Re2 Se7 89.90(6) . . ?
N1 Re2 Se4 92.4(4) . 2_565 ?
Se6 Re2 Se4 89.26(6) 2_565 2_565 ?
Se5 Re2 Se4 90.47(6) . 2_565 ?
Se7 Re2 Se4 175.85(6) . 2_565 ?
N1 Re2 Re3 133.9(4) . . ?
Se6 Re2 Re3 118.26(5) 2_565 . ?
Se5 Re2 Re3 58.48(4) . . ?
Se7 Re2 Re3 118.31(5) . . ?
Se4 Re2 Re3 58.63(5) 2_565 . ?
N1 Re2 Re1 133.4(3) . . ?
Se6 Re2 Re1 118.63(5) 2_565 . ?
Se5 Re2 Re1 58.26(5) . . ?
Se7 Re2 Re1 58.31(4) . . ?
Se4 Re2 Re1 118.62(5) 2_565 . ?
Re3 Re2 Re1 60.01(2) . . ?
N1 Re2 Re3 136.2(4) . 2_565 ?
Se6 Re2 Re3 58.66(5) 2_565 2_565 ?
Se5 Re2 Re3 118.23(5) . 2_565 ?
Se7 Re2 Re3 58.30(4) . 2_565 ?
Se4 Re2 Re3 118.04(5) 2_565 2_565 ?
Re3 Re2 Re3 89.84(3) . 2_565 ?
Re1 Re2 Re3 59.98(2) . 2_565 ?
N1 Re2 Re1 136.6(3) . 2_565 ?
Se6 Re2 Re1 58.34(4) 2_565 2_565 ?
Se5 Re2 Re1 118.39(5) . 2_565 ?
Se7 Re2 Re1 118.19(5) . 2_565 ?
Se4 Re2 Re1 58.15(4) 2_565 2_565 ?
Re3 Re2 Re1 59.92(2) . 2_565 ?
Re1 Re2 Re1 90.00(3) . 2_565 ?
Re3 Re2 Re1 59.90(2) 2_565 2_565 ?
P3 Re3 Se7 91.78(12) . 2_565 ?
P3 Re3 Se5 92.01(12) . . ?
Se7 Re3 Se5 176.21(6) 2_565 . ?
P3 Re3 Se6 91.88(12) . . ?
Se7 Re3 Se6 89.91(6) 2_565 . ?
Se5 Re3 Se6 89.96(6) . . ?
P3 Re3 Se4 92.40(12) . 2_565 ?
Se7 Re3 Se4 89.57(6) 2_565 2_565 ?
Se5 Re3 Se4 90.27(6) . 2_565 ?
Se6 Re3 Se4 175.70(6) . 2_565 ?
P3 Re3 Re2 135.14(12) . . ?
Se7 Re3 Re2 118.58(5) 2_565 . ?
Se5 Re3 Re2 58.32(4) . . ?
Se6 Re3 Re2 118.27(5) . . ?
Se4 Re3 Re2 58.47(4) 2_565 . ?
P3 Re3 Re1 135.18(11) . 2_565 ?
Se7 Re3 Re1 58.40(4) 2_565 2_565 ?
Se5 Re3 Re1 118.49(5) . 2_565 ?
Se6 Re3 Re1 118.10(5) . 2_565 ?
Se4 Re3 Re1 58.19(4) 2_565 2_565 ?
Re2 Re3 Re1 60.19(2) . 2_565 ?
P3 Re3 Re1 134.67(11) . . ?
Se7 Re3 Re1 118.70(5) 2_565 . ?
Se5 Re3 Re1 58.22(4) . . ?
Se6 Re3 Re1 58.27(4) . . ?
Se4 Re3 Re1 118.46(5) 2_565 . ?
Re2 Re3 Re1 60.02(2) . . ?
Re1 Re3 Re1 90.15(3) 2_565 . ?
P3 Re3 Re2 134.70(12) . 2_565 ?
Se7 Re3 Re2 58.55(4) 2_565 2_565 ?
Se5 Re3 Re2 118.36(5) . 2_565 ?
Se6 Re3 Re2 58.12(4) . 2_565 ?
Se4 Re3 Re2 118.18(5) 2_565 2_565 ?
Re2 Re3 Re2 90.16(3) . 2_565 ?
Re1 Re3 Re2 59.99(2) 2_565 2_565 ?
Re1 Re3 Re2 60.16(2) . 2_565 ?
Re1 Se4 Re2 63.32(4) . 2_565 ?
Re1 Se4 Re3 63.07(5) . 2_565 ?
Re2 Se4 Re3 62.91(4) 2_565 2_565 ?
Re1 Se5 Re2 63.34(4) . . ?
Re1 Se5 Re3 63.28(4) . . ?
Re2 Se5 Re3 63.20(4) . . ?
Re2 Se6 Re1 63.51(4) 2_565 . ?
Re2 Se6 Re3 63.22(4) 2_565 . ?
Re1 Se6 Re3 63.12(5) . . ?
Re3 Se7 Re1 63.21(4) 2_565 . ?
Re3 Se7 Re2 63.15(4) 2_565 . ?
Re1 Se7 Re2 63.12(4) . . ?
F4 Sb1 F6 96.7(12) . . ?
F4 Sb1 F2 90.1(9) . . ?
F6 Sb1 F2 90.3(10) . . ?
F4 Sb1 F3 92.4(8) . . ?
F6 Sb1 F3 92.4(10) . . ?
F2 Sb1 F3 176.1(10) . . ?
F4 Sb1 F5 175.6(13) . . ?
F6 Sb1 F5 87.6(14) . . ?
F2 Sb1 F5 90.8(8) . . ?
F3 Sb1 F5 86.5(8) . . ?
F4 Sb1 F1 88.3(11) . . ?
F6 Sb1 F1 175.0(13) . . ?
F2 Sb1 F1 89.2(10) . . ?
F3 Sb1 F1 87.8(10) . . ?
F5 Sb1 F1 87.4(12) . . ?
C11 P1 C15 105.1(8) . . ?
C11 P1 C13 106.3(9) . . ?
C15 P1 C13 99.9(9) . . ?
C11 P1 Re1 110.4(6) . . ?
C15 P1 Re1 117.4(6) . . ?
C13 P1 Re1 116.3(6) . . ?
C17 P3 C19 98.9(10) . . ?
C17 P3 C21 106.7(9) . . ?
C19 P3 C21 105.2(8) . . ?
C17 P3 Re3 116.5(7) . . ?
C19 P3 Re3 115.3(7) . . ?
C21 P3 Re3 112.8(6) . . ?
C5 N1 C1 116.5(15) . . ?
C5 N1 Re2 118.7(11) . . ?
C1 N1 Re2 124.4(12) . . ?
C1 C2 C3 118.4(19) . . ?
C3 C4 C5 126.1(19) . . ?
N1 C1 C2 126.0(18) . . ?
N1 C5 C4 118.5(17) . . ?
C4 C3 C2 114.4(18) . . ?
C4 C3 C6 122.0(20) . . ?
C2 C3 C6 123.5(19) . . ?
C16 C15 P1 113.5(12) . . ?
C14 C13 P1 115.3(14) . . ?
C10 C6 C7 115.3(20) . . ?
C10 C6 C3 122.2(20) . . ?
C7 C6 C3 122.5(21) . . ?
C18 C17 P3 115.1(14) . . ?
C20 C19 P3 113.2(13) . . ?
C22 C21 P3 113.1(15) . . ?
C12 C11 P1 117.4(13) . . ?
C8 C7 C6 120.7(25) . . ?
C9 C10 C6 115.9(24) . . ?
C8 N2 C9 118.0(25) . . ?
N2 C9 C10 128.0(28) . . ?
N2 C8 C7 122.0(27) . . ?
C25 C24 C23 106.1(35) . . ?
O C23 C24 118.2(28) . . ?
C26 O C23 88.8(21) . . ?
O C26 C25 118.7(26) . . ?
C24 C25 C26 106.8(36) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 P1 2.480(4) . ?
Re1 Se5 2.512(2) . ?
Re1 Se4 2.516(2) . ?
Re1 Se6 2.517(2) . ?
Re1 Se7 2.518(2) . ?
Re1 Re3 2.6391(8) 2_565 ?
Re1 Re3 2.6393(9) . ?
Re1 Re2 2.6395(9) . ?
Re1 Re2 2.6461(9) 2_565 ?
Re2 N1 2.237(14) . ?
Re2 Se6 2.511(2) 2_565 ?
Re2 Se5 2.515(2) . ?
Re2 Se7 2.525(2) . ?
Re2 Se4 2.526(2) 2_565 ?
Re2 Re3 2.6382(9) . ?
Re2 Re3 2.6403(9) 2_565 ?
Re2 Re1 2.6461(9) 2_565 ?
Re3 P3 2.481(4) . ?
Re3 Se7 2.518(2) 2_565 ?
Re3 Se5 2.520(2) . ?
Re3 Se6 2.526(2) . ?
Re3 Se4 2.530(2) 2_565 ?
Re3 Re1 2.6391(8) 2_565 ?
Re3 Re2 2.6404(9) 2_565 ?
Se4 Re2 2.526(2) 2_565 ?
Se4 Re3 2.530(2) 2_565 ?
Se6 Re2 2.511(2) 2_565 ?
Se7 Re3 2.518(2) 2_565 ?
Sb1 F4 1.77(2) . ?
Sb1 F6 1.79(2) . ?
Sb1 F2 1.81(2) . ?
Sb1 F3 1.83(2) . ?
Sb1 F5 1.87(2) . ?
Sb1 F1 1.87(2) . ?
P1 C11 1.80(2) . ?
P1 C15 1.83(2) . ?
P1 C13 1.84(2) . ?
P3 C17 1.82(2) . ?
P3 C19 1.85(2) . ?
P3 C21 1.86(2) . ?
N1 C5 1.34(2) . ?
N1 C1 1.34(2) . ?
C2 C1 1.35(2) . ?
C2 C3 1.39(3) . ?
C4 C3 1.35(3) . ?
C4 C5 1.37(2) . ?
C3 C6 1.49(3) . ?
C15 C16 1.58(2) . ?
C13 C14 1.55(3) . ?
C6 C10 1.38(3) . ?
C6 C7 1.43(3) . ?
C17 C18 1.50(3) . ?
C19 C20 1.52(3) . ?
C21 C22 1.54(2) . ?
C11 C12 1.55(2) . ?
C7 C8 1.33(3) . ?
C10 C9 1.34(3) . ?
N2 C8 1.28(3) . ?
N2 C9 1.28(3) . ?
C24 C25 1.16(4) . ?
C24 C23 1.57(4) . ?
C23 O 1.51(4) . ?
O C26 1.45(4) . ?
C26 C25 1.61(4) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P1 Re1 Re2 N1 -0.5(5) . . . . ?
Se5 Re1 Re2 N1 -54.5(5) . . . . ?
Se4 Re1 Re2 N1 128.1(5) . . . . ?
Se6 Re1 Re2 N1 -125.4(5) . . . . ?
Se7 Re1 Re2 N1 57.8(5) . . . . ?
Re3 Re1 Re2 N1 126.9(5) 2_565 . . . ?
Re3 Re1 Re2 N1 -123.8(5) . . . . ?
Re2 Re1 Re2 N1 -178.5(5) 2_565 . . . ?
P1 Re1 Re2 Se6 -128.75(15) . . . 2_565 ?
Se5 Re1 Re2 Se6 177.26(7) . . . 2_565 ?
Se4 Re1 Re2 Se6 -0.18(8) . . . 2_565 ?
Se6 Re1 Re2 Se6 106.35(6) . . . 2_565 ?
Se7 Re1 Re2 Se6 -70.44(7) . . . 2_565 ?
Re3 Re1 Re2 Se6 -1.33(5) 2_565 . . 2_565 ?
Re3 Re1 Re2 Se6 107.93(6) . . . 2_565 ?
Re2 Re1 Re2 Se6 53.28(5) 2_565 . . 2_565 ?
P1 Re1 Re2 Se5 53.98(15) . . . . ?
Se5 Re1 Re2 Se5 0.0 . . . . ?
Se4 Re1 Re2 Se5 -177.44(7) . . . . ?
Se6 Re1 Re2 Se5 -70.92(7) . . . . ?
Se7 Re1 Re2 Se5 112.29(7) . . . . ?
Re3 Re1 Re2 Se5 -178.59(6) 2_565 . . . ?
Re3 Re1 Re2 Se5 -69.34(5) . . . . ?
Re2 Re1 Re2 Se5 -123.99(5) 2_565 . . . ?
P1 Re1 Re2 Se7 -58.31(15) . . . . ?
Se5 Re1 Re2 Se7 -112.29(7) . . . . ?
Se4 Re1 Re2 Se7 70.27(7) . . . . ?
Se6 Re1 Re2 Se7 176.79(7) . . . . ?
Se7 Re1 Re2 Se7 0.0 . . . . ?
Re3 Re1 Re2 Se7 69.11(5) 2_565 . . . ?
Re3 Re1 Re2 Se7 178.37(5) . . . . ?
Re2 Re1 Re2 Se7 123.72(5) 2_565 . . . ?
P1 Re1 Re2 Se4 124.92(15) . . . 2_565 ?
Se5 Re1 Re2 Se4 70.94(7) . . . 2_565 ?
Se4 Re1 Re2 Se4 -106.50(6) . . . 2_565 ?
Se6 Re1 Re2 Se4 0.02(8) . . . 2_565 ?
Se7 Re1 Re2 Se4 -176.77(7) . . . 2_565 ?
Re3 Re1 Re2 Se4 -107.65(5) 2_565 . . 2_565 ?
Re3 Re1 Re2 Se4 1.60(5) . . . 2_565 ?
Re2 Re1 Re2 Se4 -53.05(5) 2_565 . . 2_565 ?
P1 Re1 Re2 Re3 123.32(14) . . . . ?
Se5 Re1 Re2 Re3 69.34(5) . . . . ?
Se4 Re1 Re2 Re3 -108.10(6) . . . . ?
Se6 Re1 Re2 Re3 -1.58(5) . . . . ?
Se7 Re1 Re2 Re3 -178.37(5) . . . . ?
Re3 Re1 Re2 Re3 -109.26(2) 2_565 . . . ?
Re3 Re1 Re2 Re3 0.0 . . . . ?
Re2 Re1 Re2 Re3 -54.65(2) 2_565 . . . ?
P1 Re1 Re2 Re3 -127.42(14) . . . 2_565 ?
Se5 Re1 Re2 Re3 178.59(6) . . . 2_565 ?
Se4 Re1 Re2 Re3 1.15(5) . . . 2_565 ?
Se6 Re1 Re2 Re3 107.68(6) . . . 2_565 ?
Se7 Re1 Re2 Re3 -69.11(5) . . . 2_565 ?
Re3 Re1 Re2 Re3 0.0 2_565 . . 2_565 ?
Re3 Re1 Re2 Re3 109.26(2) . . . 2_565 ?
Re2 Re1 Re2 Re3 54.61(2) 2_565 . . 2_565 ?
P1 Re1 Re2 Re1 177.97(14) . . . 2_565 ?
Se5 Re1 Re2 Re1 123.99(5) . . . 2_565 ?
Se4 Re1 Re2 Re1 -53.45(5) . . . 2_565 ?
Se6 Re1 Re2 Re1 53.07(5) . . . 2_565 ?
Se7 Re1 Re2 Re1 -123.72(5) . . . 2_565 ?
Re3 Re1 Re2 Re1 -54.61(2) 2_565 . . 2_565 ?
Re3 Re1 Re2 Re1 54.65(2) . . . 2_565 ?
Re2 Re1 Re2 Re1 0.0 2_565 . . 2_565 ?
N1 Re2 Re3 P3 -1.8(5) . . . . ?
Se6 Re2 Re3 P3 126.7(2) 2_565 . . . ?
Se5 Re2 Re3 P3 -55.8(2) . . . . ?
Se7 Re2 Re3 P3 -126.4(2) . . . . ?
Se4 Re2 Re3 P3 56.8(2) 2_565 . . . ?
Re1 Re2 Re3 P3 -124.8(2) . . . . ?
Re3 Re2 Re3 P3 -179.6(2) 2_565 . . . ?
Re1 Re2 Re3 P3 125.7(2) 2_565 . . . ?
N1 Re2 Re3 Se7 -128.5(5) . . . 2_565 ?
Se6 Re2 Re3 Se7 -0.05(8) 2_565 . . 2_565 ?
Se5 Re2 Re3 Se7 177.48(8) . . . 2_565 ?
Se7 Re2 Re3 Se7 106.91(6) . . . 2_565 ?
Se4 Re2 Re3 Se7 -69.87(7) 2_565 . . 2_565 ?
Re1 Re2 Re3 Se7 108.48(6) . . . 2_565 ?
Re3 Re2 Re3 Se7 53.66(6) 2_565 . . 2_565 ?
Re1 Re2 Re3 Se7 -1.04(6) 2_565 . . 2_565 ?
N1 Re2 Re3 Se5 54.0(5) . . . . ?
Se6 Re2 Re3 Se5 -177.52(8) 2_565 . . . ?
Se5 Re2 Re3 Se5 0.0 . . . . ?
Se7 Re2 Re3 Se5 -70.57(7) . . . . ?
Se4 Re2 Re3 Se5 112.66(7) 2_565 . . . ?
Re1 Re2 Re3 Se5 -68.99(5) . . . . ?
Re3 Re2 Re3 Se5 -123.82(6) 2_565 . . . ?
Re1 Re2 Re3 Se5 -178.51(6) 2_565 . . . ?
N1 Re2 Re3 Se6 124.6(5) . . . . ?
Se6 Re2 Re3 Se6 -106.96(6) 2_565 . . . ?
Se5 Re2 Re3 Se6 70.56(7) . . . . ?
Se7 Re2 Re3 Se6 -0.01(8) . . . . ?
Se4 Re2 Re3 Se6 -176.78(7) 2_565 . . . ?
Re1 Re2 Re3 Se6 1.57(5) . . . . ?
Re3 Re2 Re3 Se6 -53.26(5) 2_565 . . . ?
Re1 Re2 Re3 Se6 -107.95(6) 2_565 . . . ?
N1 Re2 Re3 Se4 -58.6(5) . . . 2_565 ?
Se6 Re2 Re3 Se4 69.82(7) 2_565 . . 2_565 ?
Se5 Re2 Re3 Se4 -112.66(7) . . . 2_565 ?
Se7 Re2 Re3 Se4 176.77(7) . . . 2_565 ?
Se4 Re2 Re3 Se4 0.0 2_565 . . 2_565 ?
Re1 Re2 Re3 Se4 178.35(5) . . . 2_565 ?
Re3 Re2 Re3 Se4 123.53(5) 2_565 . . 2_565 ?
Re1 Re2 Re3 Se4 68.83(5) 2_565 . . 2_565 ?
N1 Re2 Re3 Re1 -127.5(5) . . . 2_565 ?
Se6 Re2 Re3 Re1 0.99(6) 2_565 . . 2_565 ?
Se5 Re2 Re3 Re1 178.51(6) . . . 2_565 ?
Se7 Re2 Re3 Re1 107.94(6) . . . 2_565 ?
Se4 Re2 Re3 Re1 -68.83(5) 2_565 . . 2_565 ?
Re1 Re2 Re3 Re1 109.52(3) . . . 2_565 ?
Re3 Re2 Re3 Re1 54.69(2) 2_565 . . 2_565 ?
Re1 Re2 Re3 Re1 0.0 2_565 . . 2_565 ?
N1 Re2 Re3 Re1 123.0(5) . . . . ?
Se6 Re2 Re3 Re1 -108.53(6) 2_565 . . . ?
Se5 Re2 Re3 Re1 68.99(5) . . . . ?
Se7 Re2 Re3 Re1 -1.58(5) . . . . ?
Se4 Re2 Re3 Re1 -178.35(5) 2_565 . . . ?
Re1 Re2 Re3 Re1 0.0 . . . . ?
Re3 Re2 Re3 Re1 -54.83(2) 2_565 . . . ?
Re1 Re2 Re3 Re1 -109.52(3) 2_565 . . . ?
N1 Re2 Re3 Re2 177.8(5) . . . 2_565 ?
Se6 Re2 Re3 Re2 -53.71(5) 2_565 . . 2_565 ?
Se5 Re2 Re3 Re2 123.82(6) . . . 2_565 ?
Se7 Re2 Re3 Re2 53.25(5) . . . 2_565 ?
Se4 Re2 Re3 Re2 -123.53(5) 2_565 . . 2_565 ?
Re1 Re2 Re3 Re2 54.82(2) . . . 2_565 ?
Re3 Re2 Re3 Re2 0.0 2_565 . . 2_565 ?
Re1 Re2 Re3 Re2 -54.70(2) 2_565 . . 2_565 ?
P1 Re1 Re3 P3 5.1(2) . . . . ?
Se5 Re1 Re3 P3 56.3(2) . . . . ?
Se4 Re1 Re3 P3 -125.9(2) . . . . ?
Se6 Re1 Re3 P3 -56.1(2) . . . . ?
Se7 Re1 Re3 P3 127.1(2) . . . . ?
Re3 Re1 Re3 P3 -179.7(2) 2_565 . . . ?
Re2 Re1 Re3 P3 125.5(2) . . . . ?
Re2 Re1 Re3 P3 -125.0(2) 2_565 . . . ?
P1 Re1 Re3 Se7 131.4(2) . . . 2_565 ?
Se5 Re1 Re3 Se7 -177.45(7) . . . 2_565 ?
Se4 Re1 Re3 Se7 0.29(8) . . . 2_565 ?
Se6 Re1 Re3 Se7 70.09(7) . . . 2_565 ?
Se7 Re1 Re3 Se7 -106.70(7) . . . 2_565 ?
Re3 Re1 Re3 Se7 -53.42(5) 2_565 . . 2_565 ?
Re2 Re1 Re3 Se7 -108.29(6) . . . 2_565 ?
Re2 Re1 Re3 Se7 1.26(5) 2_565 . . 2_565 ?
P1 Re1 Re3 Se5 -51.2(2) . . . . ?
Se5 Re1 Re3 Se5 0.0 . . . . ?
Se4 Re1 Re3 Se5 177.74(7) . . . . ?
Se6 Re1 Re3 Se5 -112.46(7) . . . . ?
Se7 Re1 Re3 Se5 70.75(7) . . . . ?
Re3 Re1 Re3 Se5 124.03(6) 2_565 . . . ?
Re2 Re1 Re3 Se5 69.16(5) . . . . ?
Re2 Re1 Re3 Se5 178.71(6) 2_565 . . . ?
P1 Re1 Re3 Se6 61.3(2) . . . . ?
Se5 Re1 Re3 Se6 112.46(7) . . . . ?
Se4 Re1 Re3 Se6 -69.80(7) . . . . ?
Se6 Re1 Re3 Se6 0.0 . . . . ?
Se7 Re1 Re3 Se6 -176.79(7) . . . . ?
Re3 Re1 Re3 Se6 -123.51(5) 2_565 . . . ?
Re2 Re1 Re3 Se6 -178.38(5) . . . . ?
Re2 Re1 Re3 Se6 -68.83(5) 2_565 . . . ?
P1 Re1 Re3 Se4 -121.9(2) . . . 2_565 ?
Se5 Re1 Re3 Se4 -70.76(7) . . . 2_565 ?
Se4 Re1 Re3 Se4 106.98(7) . . . 2_565 ?
Se6 Re1 Re3 Se4 176.78(7) . . . 2_565 ?
Se7 Re1 Re3 Se4 -0.01(8) . . . 2_565 ?
Re3 Re1 Re3 Se4 53.27(5) 2_565 . . 2_565 ?
Re2 Re1 Re3 Se4 -1.60(5) . . . 2_565 ?
Re2 Re1 Re3 Se4 107.95(5) 2_565 . . 2_565 ?
P1 Re1 Re3 Re2 -120.3(2) . . . . ?
Se5 Re1 Re3 Re2 -69.16(5) . . . . ?
Se4 Re1 Re3 Re2 108.58(6) . . . . ?
Se6 Re1 Re3 Re2 178.38(5) . . . . ?
Se7 Re1 Re3 Re2 1.58(5) . . . . ?
Re3 Re1 Re3 Re2 54.86(2) 2_565 . . . ?
Re2 Re1 Re3 Re2 0.0 . . . . ?
Re2 Re1 Re3 Re2 109.55(3) 2_565 . . . ?
P1 Re1 Re3 Re1 -175.2(2) . . . 2_565 ?
Se5 Re1 Re3 Re1 -124.03(6) . . . 2_565 ?
Se4 Re1 Re3 Re1 53.72(5) . . . 2_565 ?
Se6 Re1 Re3 Re1 123.51(5) . . . 2_565 ?
Se7 Re1 Re3 Re1 -53.28(5) . . . 2_565 ?
Re3 Re1 Re3 Re1 0.0 2_565 . . 2_565 ?
Re2 Re1 Re3 Re1 -54.86(2) . . . 2_565 ?
Re2 Re1 Re3 Re1 54.69(2) 2_565 . . 2_565 ?
P1 Re1 Re3 Re2 130.1(2) . . . 2_565 ?
Se5 Re1 Re3 Re2 -178.71(6) . . . 2_565 ?
Se4 Re1 Re3 Re2 -0.97(5) . . . 2_565 ?
Se6 Re1 Re3 Re2 68.83(5) . . . 2_565 ?
Se7 Re1 Re3 Re2 -107.97(6) . . . 2_565 ?
Re3 Re1 Re3 Re2 -54.69(2) 2_565 . . 2_565 ?
Re2 Re1 Re3 Re2 -109.55(3) . . . 2_565 ?
Re2 Re1 Re3 Re2 0.0 2_565 . . 2_565 ?
P1 Re1 Se4 Re2 -145.68(11) . . . 2_565 ?
Se5 Re1 Se4 Re2 33.2(10) . . . 2_565 ?
Se6 Re1 Se4 Re2 -52.26(5) . . . 2_565 ?
Se7 Re1 Se4 Re2 123.81(5) . . . 2_565 ?
Re3 Re1 Se4 Re2 71.55(4) 2_565 . . 2_565 ?
Re3 Re1 Se4 Re2 0.98(6) . . . 2_565 ?
Re2 Re1 Se4 Re2 70.38(5) . . . 2_565 ?
Re2 Re1 Se4 Re2 0.0 2_565 . . 2_565 ?
P1 Re1 Se4 Re3 142.77(11) . . . 2_565 ?
Se5 Re1 Se4 Re3 -38.3(10) . . . 2_565 ?
Se6 Re1 Se4 Re3 -123.81(5) . . . 2_565 ?
Se7 Re1 Se4 Re3 52.26(5) . . . 2_565 ?
Re3 Re1 Se4 Re3 0.0 2_565 . . 2_565 ?
Re3 Re1 Se4 Re3 -70.57(5) . . . 2_565 ?
Re2 Re1 Se4 Re3 -1.17(5) . . . 2_565 ?
Re2 Re1 Se4 Re3 -71.55(4) 2_565 . . 2_565 ?
P1 Re1 Se5 Re2 -142.65(11) . . . . ?
Se4 Re1 Se5 Re2 38.4(10) . . . . ?
Se6 Re1 Se5 Re2 123.90(5) . . . . ?
Se7 Re1 Se5 Re2 -52.13(5) . . . . ?
Re3 Re1 Se5 Re2 1.38(6) 2_565 . . . ?
Re3 Re1 Se5 Re2 71.81(4) . . . . ?
Re2 Re1 Se5 Re2 0.0 . . . . ?
Re2 Re1 Se5 Re2 70.54(5) 2_565 . . . ?
P1 Re1 Se5 Re3 145.54(11) . . . . ?
Se4 Re1 Se5 Re3 -33.4(10) . . . . ?
Se6 Re1 Se5 Re3 52.08(5) . . . . ?
Se7 Re1 Se5 Re3 -123.95(5) . . . . ?
Re3 Re1 Se5 Re3 -70.43(5) 2_565 . . . ?
Re3 Re1 Se5 Re3 0.0 . . . . ?
Re2 Re1 Se5 Re3 -71.81(4) . . . . ?
Re2 Re1 Se5 Re3 -1.27(6) 2_565 . . . ?
N1 Re2 Se5 Re1 143.7(4) . . . . ?
Se6 Re2 Se5 Re1 -38.0(9) 2_565 . . . ?
Se7 Re2 Se5 Re1 51.94(5) . . . . ?
Se4 Re2 Se5 Re1 -123.93(5) 2_565 . . . ?
Re3 Re2 Se5 Re1 -71.94(4) . . . . ?
Re1 Re2 Se5 Re1 0.0 . . . . ?
Re3 Re2 Se5 Re1 -1.38(6) 2_565 . . . ?
Re1 Re2 Se5 Re1 -70.47(5) 2_565 . . . ?
N1 Re2 Se5 Re3 -144.3(4) . . . . ?
Se6 Re2 Se5 Re3 34.0(9) 2_565 . . . ?
Se7 Re2 Se5 Re3 123.87(5) . . . . ?
Se4 Re2 Se5 Re3 -51.99(5) 2_565 . . . ?
Re3 Re2 Se5 Re3 0.0 . . . . ?
Re1 Re2 Se5 Re3 71.94(4) . . . . ?
Re3 Re2 Se5 Re3 70.55(5) 2_565 . . . ?
Re1 Re2 Se5 Re3 1.46(6) 2_565 . . . ?
P3 Re3 Se5 Re1 -143.69(12) . . . . ?
Se7 Re3 Se5 Re1 36.2(10) 2_565 . . . ?
Se6 Re3 Se5 Re1 -51.81(5) . . . . ?
Se4 Re3 Se5 Re1 123.90(5) 2_565 . . . ?
Re2 Re3 Se5 Re1 72.03(4) . . . . ?
Re1 Re3 Se5 Re1 70.56(5) 2_565 . . . ?
Re1 Re3 Se5 Re1 0.0 . . . . ?
Re2 Re3 Se5 Re1 1.27(6) 2_565 . . . ?
P3 Re3 Se5 Re2 144.28(12) . . . . ?
Se7 Re3 Se5 Re2 -35.8(10) 2_565 . . . ?
Se6 Re3 Se5 Re2 -123.84(5) . . . . ?
Se4 Re3 Se5 Re2 51.87(5) 2_565 . . . ?
Re2 Re3 Se5 Re2 0.0 . . . . ?
Re1 Re3 Se5 Re2 -1.47(6) 2_565 . . . ?
Re1 Re3 Se5 Re2 -72.03(4) . . . . ?
Re2 Re3 Se5 Re2 -70.76(5) 2_565 . . . ?
P1 Re1 Se6 Re2 147.79(11) . . . 2_565 ?
Se5 Re1 Se6 Re2 -123.83(5) . . . 2_565 ?
Se4 Re1 Se6 Re2 52.57(5) . . . 2_565 ?
Se7 Re1 Se6 Re2 -27.0(10) . . . 2_565 ?
Re3 Re1 Se6 Re2 -1.01(6) 2_565 . . 2_565 ?
Re3 Re1 Se6 Re2 -71.84(4) . . . 2_565 ?
Re2 Re1 Se6 Re2 -70.24(5) . . . 2_565 ?
Re2 Re1 Se6 Re2 0.0 2_565 . . 2_565 ?
P1 Re1 Se6 Re3 -140.37(11) . . . . ?
Se5 Re1 Se6 Re3 -52.00(5) . . . . ?
Se4 Re1 Se6 Re3 124.40(5) . . . . ?
Se7 Re1 Se6 Re3 44.9(9) . . . . ?
Re3 Re1 Se6 Re3 70.83(5) 2_565 . . . ?
Re3 Re1 Se6 Re3 0.0 . . . . ?
Re2 Re1 Se6 Re3 1.60(5) . . . . ?
Re2 Re1 Se6 Re3 71.84(4) 2_565 . . . ?
P3 Re3 Se6 Re2 -143.94(11) . . . 2_565 ?
Se7 Re3 Se6 Re2 -52.16(5) 2_565 . . 2_565 ?
Se5 Re3 Se6 Re2 124.05(5) . . . 2_565 ?
Se4 Re3 Se6 Re2 31.0(8) 2_565 . . 2_565 ?
Re2 Re3 Se6 Re2 70.68(5) . . . 2_565 ?
Re1 Re3 Se6 Re2 1.34(5) 2_565 . . 2_565 ?
Re1 Re3 Se6 Re2 72.28(4) . . . 2_565 ?
Re2 Re3 Se6 Re2 0.0 2_565 . . 2_565 ?
P3 Re3 Se6 Re1 143.78(11) . . . . ?
Se7 Re3 Se6 Re1 -124.44(5) 2_565 . . . ?
Se5 Re3 Se6 Re1 51.77(5) . . . . ?
Se4 Re3 Se6 Re1 -41.3(8) 2_565 . . . ?
Re2 Re3 Se6 Re1 -1.60(5) . . . . ?
Re1 Re3 Se6 Re1 -70.94(5) 2_565 . . . ?
Re1 Re3 Se6 Re1 0.0 . . . . ?
Re2 Re3 Se6 Re1 -72.28(4) 2_565 . . . ?
P1 Re1 Se7 Re3 -147.79(11) . . . 2_565 ?
Se5 Re1 Se7 Re3 123.86(5) . . . 2_565 ?
Se4 Re1 Se7 Re3 -52.53(5) . . . 2_565 ?
Se6 Re1 Se7 Re3 27.0(10) . . . 2_565 ?
Re3 Re1 Se7 Re3 0.0 2_565 . . 2_565 ?
Re3 Re1 Se7 Re3 70.25(5) . . . 2_565 ?
Re2 Re1 Se7 Re3 71.86(4) . . . 2_565 ?
Re2 Re1 Se7 Re3 1.05(6) 2_565 . . 2_565 ?
P1 Re1 Se7 Re2 140.36(11) . . . . ?
Se5 Re1 Se7 Re2 52.00(5) . . . . ?
Se4 Re1 Se7 Re2 -124.39(5) . . . . ?
Se6 Re1 Se7 Re2 -44.9(9) . . . . ?
Re3 Re1 Se7 Re2 -71.86(4) 2_565 . . . ?
Re3 Re1 Se7 Re2 -1.61(5) . . . . ?
Re2 Re1 Se7 Re2 0.0 . . . . ?
Re2 Re1 Se7 Re2 -70.81(5) 2_565 . . . ?
N1 Re2 Se7 Re3 146.0(3) . . . 2_565 ?
Se6 Re2 Se7 Re3 52.25(5) 2_565 . . 2_565 ?
Se5 Re2 Se7 Re3 -123.85(5) . . . 2_565 ?
Se4 Re2 Se7 Re3 -28.8(9) 2_565 . . 2_565 ?
Re3 Re2 Se7 Re3 -70.35(5) . . . 2_565 ?
Re1 Re2 Se7 Re3 -71.95(4) . . . 2_565 ?
Re3 Re2 Se7 Re3 0.0 2_565 . . 2_565 ?
Re1 Re2 Se7 Re3 -1.27(5) 2_565 . . 2_565 ?
N1 Re2 Se7 Re1 -142.0(3) . . . . ?
Se6 Re2 Se7 Re1 124.20(5) 2_565 . . . ?
Se5 Re2 Se7 Re1 -51.90(5) . . . . ?
Se4 Re2 Se7 Re1 43.2(9) 2_565 . . . ?
Re3 Re2 Se7 Re1 1.60(5) . . . . ?
Re1 Re2 Se7 Re1 0.0 . . . . ?
Re3 Re2 Se7 Re1 71.95(4) 2_565 . . . ?
Re1 Re2 Se7 Re1 70.68(5) 2_565 . . . ?
Se5 Re1 P1 C11 46.5(7) . . . . ?
Se4 Re1 P1 C11 -133.5(7) . . . . ?
Se6 Re1 P1 C11 136.8(7) . . . . ?
Se7 Re1 P1 C11 -43.6(7) . . . . ?
Re3 Re1 P1 C11 -84.8(7) 2_565 . . . ?
Re3 Re1 P1 C11 88.2(7) . . . . ?
Re2 Re1 P1 C11 3.0(7) . . . . ?
Re2 Re1 P1 C11 179.9(7) 2_565 . . . ?
Se5 Re1 P1 C15 167.1(6) . . . . ?
Se4 Re1 P1 C15 -13.0(6) . . . . ?
Se6 Re1 P1 C15 -102.7(6) . . . . ?
Se7 Re1 P1 C15 76.9(6) . . . . ?
Re3 Re1 P1 C15 35.7(6) 2_565 . . . ?
Re3 Re1 P1 C15 -151.3(6) . . . . ?
Re2 Re1 P1 C15 123.5(6) . . . . ?
Re2 Re1 P1 C15 -59.6(6) 2_565 . . . ?
Se5 Re1 P1 C13 -74.7(8) . . . . ?
Se4 Re1 P1 C13 105.2(8) . . . . ?
Se6 Re1 P1 C13 15.5(8) . . . . ?
Se7 Re1 P1 C13 -164.9(8) . . . . ?
Re3 Re1 P1 C13 153.9(8) 2_565 . . . ?
Re3 Re1 P1 C13 -33.1(8) . . . . ?
Re2 Re1 P1 C13 -118.3(8) . . . . ?
Re2 Re1 P1 C13 58.6(8) 2_565 . . . ?
Se7 Re3 P3 C17 -75.8(7) 2_565 . . . ?
Se5 Re3 P3 C17 104.2(7) . . . . ?
Se6 Re3 P3 C17 14.1(7) . . . . ?
Se4 Re3 P3 C17 -165.5(7) 2_565 . . . ?
Re2 Re3 P3 C17 149.0(7) . . . . ?
Re1 Re3 P3 C17 -120.4(7) 2_565 . . . ?
Re1 Re3 P3 C17 59.1(8) . . . . ?
Re2 Re3 P3 C17 -30.5(8) 2_565 . . . ?
Se7 Re3 P3 C19 169.0(8) 2_565 . . . ?
Se5 Re3 P3 C19 -11.0(8) . . . . ?
Se6 Re3 P3 C19 -101.0(8) . . . . ?
Se4 Re3 P3 C19 79.3(8) 2_565 . . . ?
Re2 Re3 P3 C19 33.8(8) . . . . ?
Re1 Re3 P3 C19 124.4(7) 2_565 . . . ?
Re1 Re3 P3 C19 -56.1(8) . . . . ?
Re2 Re3 P3 C19 -145.7(7) 2_565 . . . ?
Se7 Re3 P3 C21 48.1(7) 2_565 . . . ?
Se5 Re3 P3 C21 -132.0(7) . . . . ?
Se6 Re3 P3 C21 138.0(7) . . . . ?
Se4 Re3 P3 C21 -41.6(7) 2_565 . . . ?
Re2 Re3 P3 C21 -87.2(7) . . . . ?
Re1 Re3 P3 C21 3.5(7) 2_565 . . . ?
Re1 Re3 P3 C21 -177.0(7) . . . . ?
Re2 Re3 P3 C21 93.3(7) 2_565 . . . ?
Se6 Re2 N1 C5 -129.6(13) 2_565 . . . ?
Se5 Re2 N1 C5 50.3(14) . . . . ?
Se7 Re2 N1 C5 140.2(13) . . . . ?
Se4 Re2 N1 C5 -40.2(14) 2_565 . . . ?
Re3 Re2 N1 C5 6.6(16) . . . . ?
Re1 Re2 N1 C5 94.1(14) . . . . ?
Re3 Re2 N1 C5 -176.5(11) 2_565 . . . ?
Re1 Re2 N1 C5 -83.7(14) 2_565 . . . ?
Se6 Re2 N1 C1 57.9(13) 2_565 . . . ?
Se5 Re2 N1 C1 -122.2(13) . . . . ?
Se7 Re2 N1 C1 -32.3(13) . . . . ?
Se4 Re2 N1 C1 147.4(13) 2_565 . . . ?
Re3 Re2 N1 C1 -165.8(11) . . . . ?
Re1 Re2 N1 C1 -78.4(14) . . . . ?
Re3 Re2 N1 C1 11.1(16) 2_565 . . . ?
Re1 Re2 N1 C1 103.9(13) 2_565 . . . ?
C5 N1 C1 C2 -0.4(27) . . . . ?
Re2 N1 C1 C2 172.2(14) . . . . ?
C3 C2 C1 N1 -1.6(29) . . . . ?
C1 N1 C5 C4 0.3(27) . . . . ?
Re2 N1 C5 C4 -172.7(14) . . . . ?
C3 C4 C5 N1 1.9(33) . . . . ?
C5 C4 C3 C2 -3.8(31) . . . . ?
C5 C4 C3 C6 178.9(19) . . . . ?
C1 C2 C3 C4 3.4(27) . . . . ?
C1 C2 C3 C6 -179.3(16) . . . . ?
C11 P1 C15 C16 57.4(15) . . . . ?
C13 P1 C15 C16 167.5(14) . . . . ?
Re1 P1 C15 C16 -65.8(14) . . . . ?
C11 P1 C13 C14 -60.0(16) . . . . ?
C15 P1 C13 C14 -169.1(14) . . . . ?
Re1 P1 C13 C14 63.4(16) . . . . ?
C4 C3 C6 C10 -19.5(31) . . . . ?
C2 C3 C6 C10 163.4(20) . . . . ?
C4 C3 C6 C7 161.5(21) . . . . ?
C2 C3 C6 C7 -15.6(30) . . . . ?
C19 P3 C17 C18 -171.1(15) . . . . ?
C21 P3 C17 C18 -62.1(17) . . . . ?
Re3 P3 C17 C18 64.8(16) . . . . ?
C17 P3 C19 C20 165.0(15) . . . . ?
C21 P3 C19 C20 54.9(17) . . . . ?
Re3 P3 C19 C20 -70.1(15) . . . . ?
C17 P3 C21 C22 -52.1(17) . . . . ?
C19 P3 C21 C22 52.3(18) . . . . ?
Re3 P3 C21 C22 178.8(13) . . . . ?
C15 P1 C11 C12 54.0(18) . . . . ?
C13 P1 C11 C12 -51.3(18) . . . . ?
Re1 P1 C11 C12 -178.4(15) . . . . ?
C10 C6 C7 C8 1.0(34) . . . . ?
C3 C6 C7 C8 -179.9(22) . . . . ?
C7 C6 C10 C9 -0.8(32) . . . . ?
C3 C6 C10 C9 -179.9(21) . . . . ?
C8 N2 C9 C10 0.8(48) . . . . ?
C6 C10 C9 N2 0.0(44) . . . . ?
C9 N2 C8 C7 -0.6(44) . . . . ?
C6 C7 C8 N2 -0.3(42) . . . . ?
C25 C24 C23 O -12.4(73) . . . . ?
C24 C23 O C26 11.0(49) . . . . ?
C23 O C26 C25 -7.4(41) . . . . ?
C23 C24 C25 C26 5.7(61) . . . . ?
O C26 C25 C24 1.3(62) . . . . ?
