#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/24/4322440.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4322440
loop_
_publ_author_name
'Takashi Yoshimura'
'Keisuke Umakoshi'
'Yoichi Sasaki'
'A. Geoffrey Sykes'
_publ_contact_author_address
;
            Pr Yoichi Sasaki
    Division of Chemistry
    Graduate School of Science
    Hokkaido University
    Kita-ku, Sapporo 060-0810
    Japan
;
_publ_contact_author_email       ysasaki@science.hokudai.ac.jp
_publ_contact_author_fax         +81-11-706-3447
_publ_contact_author_name        ' Sasaki, Yoichi '
_publ_contact_author_phone       +81-11-706-3817
_publ_section_title
;
 Synthesis, Structures, and Redox Properties of
 Octa(μ3-sulfido)hexarhenium(III) Complexes Having Terminal Pyridine
 Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5557
_journal_page_last               5564
_journal_paper_doi               10.1021/ic9907922
_journal_volume                  38
_journal_year                    1999
_chemical_formula_sum            'C44 H80 Cl4 N6 Re6 S8'
_chemical_formula_weight         2208.69
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   19.304(3)
_cell_length_b                   17.894(7)
_cell_length_c                   18.773(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      14.9
_cell_measurement_theta_min      12.5
_cell_volume                     6485(3)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
_diffrn_ambient_temperature      296.2
_diffrn_measurement_device_type  'Rigaku AFC5R'
_diffrn_measurement_method       ω-2θ
_diffrn_orient_matrix_UB_11      0.03505
_diffrn_orient_matrix_UB_12      -0.02521
_diffrn_orient_matrix_UB_13      -0.03100
_diffrn_orient_matrix_UB_21      0.01576
_diffrn_orient_matrix_UB_22      0.04979
_diffrn_orient_matrix_UB_23      -0.01795
_diffrn_orient_matrix_UB_31      0.03474
_diffrn_orient_matrix_UB_32      0.00285
_diffrn_orient_matrix_UB_33      0.03943
_diffrn_radiation_detector       'scintillation counter'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.000
_diffrn_reflns_av_sigmaI/netI    0.105
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       0
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            5144
_diffrn_reflns_reduction_process 'Lp corrections applied'
_diffrn_reflns_theta_max         30.00
_diffrn_reflns_theta_min         2.52
_diffrn_standards_decay_%        -0.06
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    11.617
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.427
_exptl_absorpt_correction_type   'psi scans'
_exptl_absorpt_process_details   'North, Phillips & Mathews, 1968'
_exptl_crystal_colour            red-brown
_exptl_crystal_density_diffrn    2.262
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       rhombic
_exptl_crystal_F_000             4128.00
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.40
_refine_diff_density_min         -1.17
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     130
_refine_ls_number_reflns         3124
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0431
_refine_ls_R_factor_gt           0.0431
_refine_ls_shift/su_max          0.0560
_refine_ls_shift/su_mean         0.0080
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[σ²(Fo) + 0.00073|Fo|²]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0509
_refine_ls_wR_factor_ref         0.0509
_reflns_number_gt                3124
_reflns_number_total             5144
_reflns_threshold_expression     >2.0sigma(I)
_cod_data_source_file            ic9907922_2.cif
_cod_data_source_block           (Bu4N)2[trans-Re6S8Cl4(cpy)2]
_cod_original_cell_volume        6484(2)
_cod_original_sg_symbol_H-M      'C m c a '
_cod_original_formula_sum        'C44 H80 Cl4 N6 S8 Re6 '
_cod_database_code               4322440
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
x,-y,-z
x,1/2-y,1/2+z
x,1/2+y,1/2-z
-x,-y,-z
-x,y,z
-x,1/2+y,1/2-z
-x,1/2-y,1/2+z
1/2+x,1/2+y,z
1/2+x,1/2-y,-z
1/2+x,-y,1/2+z
1/2+x,y,1/2-z
1/2-x,1/2-y,-z
1/2-x,1/2+y,z
1/2-x,y,1/2-z
1/2-x,-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.5000 0.09899(3) 0.52190(3) 0.0277(1) Uani 1.00 d S . .
Re2 Re 0.40454(3) 0.0000 0.5000 0.0283(1) Uani 1.00 d S . .
Re3 Re 0.5000 0.02333(3) 0.40459(3) 0.0276(1) Uani 1.00 d S . .
Cl1 Cl 0.2791(2) 0.0000 0.5000 0.054(1) Uani 1.00 d S . .
Cl2 Cl 0.5000 0.0545(3) 0.2789(2) 0.055(1) Uani 1.00 d S . .
S1 S 0.4123(1) 0.0716(2) 0.6080(1) 0.0376(7) Uani 1.00 d . . .
S2 S 0.4127(1) 0.1142(2) 0.4328(1) 0.0368(7) Uani 1.00 d . . .
N11 N 0.5000 0.2195(7) 0.5482(7) 0.037(4) Uani 1.00 d S . .
N18 N 0.5000 0.510(1) 0.599(1) 0.13(1) Uani 1.00 d S . .
N101 N 0.2500 0.0276(10) 0.2500 0.067(4) Uiso 1.00 d S . .
C12 C 0.5000 0.2682(10) 0.4949(9) 0.058(6) Uani 1.00 d S . .
C13 C 0.5000 0.344(1) 0.508(1) 0.067(7) Uani 1.00 d S . .
C14 C 0.5000 0.369(1) 0.576(1) 0.078(8) Uani 1.00 d S . .
C15 C 0.5000 0.317(1) 0.632(1) 0.065(7) Uani 1.00 d S . .
C16 C 0.5000 0.2420(9) 0.6147(8) 0.040(4) Uani 1.00 d S . .
C17 C 0.5000 0.446(2) 0.591(1) 0.10(1) Uani 1.00 d S . .
C101 C 0.2678(8) 0.0744(9) 0.3166(8) 0.076(4) Uiso 1.00 d . . .
C102 C 0.2100(10) 0.127(1) 0.3378(10) 0.094(5) Uiso 1.00 d . . .
C103 C 0.2359(9) 0.180(1) 0.3949(9) 0.088(5) Uiso 1.00 d . . .
C104 C 0.185(1) 0.236(1) 0.416(1) 0.110(6) Uiso 1.00 d . . .
C105 C 0.1850(8) -0.0242(9) 0.2646(8) 0.073(4) Uiso 1.00 d . . .
C106 C 0.196(1) -0.077(1) 0.327(1) 0.113(7) Uiso 1.00 d . . .
C107 C 0.127(1) -0.131(1) 0.336(1) 0.23(1) Uiso 1.49 d P . .
C108 C 0.116(2) -0.185(2) 0.279(2) 0.14(1) Uiso 0.66 d P . .
H12 H 0.5000 0.2498 0.4462 0.0685 Uiso 1.00 calc S . .
H13 H 0.5000 0.3791 0.4686 0.0805 Uiso 1.00 calc S . .
H15 H 0.5000 0.3325 0.6821 0.0768 Uiso 1.00 calc S . .
H16 H 0.5000 0.2049 0.6527 0.0484 Uiso 1.00 calc S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.003 0.002
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
H H 0.000 0.000
;International Tables for Crystallography
(1992, Vol. C, Table 6.1.1.2)
;
N N 0.006 0.003
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
Re Re -1.018 7.231
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
S S 0.125 0.123
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
Cl Cl 0.148 0.159
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
8 0 0
0 10 0
0 0 10
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
RE2 RE1 RE2 90.76(3) 1_555 1_555 5_656 yes
RE2 RE1 RE3 60.42(1) 1_555 1_555 1_555 yes
RE2 RE1 RE3 60.39(1) 1_555 1_555 2_556 yes
RE2 RE1 S1 57.52(7) 1_555 1_555 1_555 yes
RE2 RE1 S1 118.08(7) 1_555 1_555 6_655 yes
RE2 RE1 S2 57.64(7) 1_555 1_555 1_555 yes
RE2 RE1 S2 117.96(7) 1_555 1_555 6_655 yes
RE2 RE1 N11 134.62(1) 1_555 1_555 1_555 yes
RE2 RE1 RE3 60.42(1) 5_656 1_555 1_555 yes
RE2 RE1 RE3 60.39(1) 5_656 1_555 2_556 yes
RE2 RE1 S1 118.08(7) 5_656 1_555 1_555 yes
RE2 RE1 S1 57.52(7) 5_656 1_555 6_655 yes
RE2 RE1 S2 117.96(7) 5_656 1_555 1_555 yes
RE2 RE1 S2 57.64(7) 5_656 1_555 6_655 yes
RE2 RE1 N11 134.62(1) 5_656 1_555 1_555 yes
RE3 RE1 RE3 90.65(2) 1_555 1_555 2_556 yes
RE3 RE1 S1 117.92(7) 1_555 1_555 1_555 yes
RE3 RE1 S1 117.92(7) 1_555 1_555 6_655 yes
RE3 RE1 S2 57.56(7) 1_555 1_555 1_555 yes
RE3 RE1 S2 57.56(7) 1_555 1_555 6_655 yes
RE3 RE1 N11 134.5(3) 1_555 1_555 1_555 yes
RE3 RE1 S1 57.72(7) 2_556 1_555 1_555 yes
RE3 RE1 S1 57.72(7) 2_556 1_555 6_655 yes
RE3 RE1 S2 118.00(7) 2_556 1_555 1_555 yes
RE3 RE1 S2 118.00(7) 2_556 1_555 6_655 yes
RE3 RE1 N11 134.9(3) 2_556 1_555 1_555 yes
S1 RE1 S1 90.1(1) 1_555 1_555 6_655 yes
S1 RE1 S2 89.83(9) 1_555 1_555 1_555 yes
S1 RE1 S2 174.58(10) 1_555 1_555 6_655 yes
S1 RE1 N11 92.8(2) 1_555 1_555 1_555 yes
S1 RE1 S2 174.58(10) 6_655 1_555 1_555 yes
S1 RE1 S2 89.83(9) 6_655 1_555 6_655 yes
S1 RE1 N11 92.8(2) 6_655 1_555 1_555 yes
S2 RE1 S2 89.7(1) 1_555 1_555 6_655 yes
S2 RE1 N11 92.6(2) 1_555 1_555 1_555 yes
S2 RE1 N11 92.6(2) 6_655 1_555 1_555 yes
RE1 RE2 RE1 89.24(3) 1_555 1_555 2_556 yes
RE1 RE2 RE3 59.72(2) 1_555 1_555 1_555 yes
RE1 RE2 RE3 59.77(2) 1_555 1_555 2_556 yes
RE1 RE2 CL1 135.38(1) 1_555 1_555 1_555 yes
RE1 RE2 S1 57.10(7) 1_555 1_555 1_555 yes
RE1 RE2 S1 117.01(7) 1_555 1_555 2_556 yes
RE1 RE2 S2 57.04(6) 1_555 1_555 1_555 yes
RE1 RE2 S2 116.83(6) 1_555 1_555 2_556 yes
RE1 RE2 RE3 59.77(2) 2_556 1_555 1_555 yes
RE1 RE2 RE3 59.72(2) 2_556 1_555 2_556 yes
RE1 RE2 CL1 135.38(1) 2_556 1_555 1_555 yes
RE1 RE2 S1 117.01(7) 2_556 1_555 1_555 yes
RE1 RE2 S1 57.10(7) 2_556 1_555 2_556 yes
RE1 RE2 S2 116.83(6) 2_556 1_555 1_555 yes
RE1 RE2 S2 57.04(6) 2_556 1_555 2_556 yes
RE3 RE2 RE3 89.88(2) 1_555 1_555 2_556 yes
RE3 RE2 CL1 135.06(1) 1_555 1_555 1_555 yes
RE3 RE2 S1 116.80(7) 1_555 1_555 1_555 yes
RE3 RE2 S1 57.37(7) 1_555 1_555 2_556 yes
RE3 RE2 S2 57.12(6) 1_555 1_555 1_555 yes
RE3 RE2 S2 116.79(6) 1_555 1_555 2_556 yes
RE3 RE2 CL1 135.06(1) 2_556 1_555 1_555 yes
RE3 RE2 S1 57.36(7) 2_556 1_555 1_555 yes
RE3 RE2 S1 116.80(7) 2_556 1_555 2_556 yes
RE3 RE2 S2 116.79(6) 2_556 1_555 1_555 yes
RE3 RE2 S2 57.12(6) 2_556 1_555 2_556 yes
CL1 RE2 S1 93.58(6) 1_555 1_555 1_555 yes
CL1 RE2 S1 93.58(6) 1_555 1_555 2_556 yes
CL1 RE2 S2 93.73(6) 1_555 1_555 1_555 yes
CL1 RE2 S2 93.73(6) 1_555 1_555 2_556 yes
S1 RE2 S1 172.8(1) 1_555 1_555 2_556 yes
S1 RE2 S2 89.18(9) 1_555 1_555 1_555 yes
S1 RE2 S2 90.35(9) 1_555 1_555 2_556 yes
S1 RE2 S2 90.35(9) 2_556 1_555 1_555 yes
S1 RE2 S2 89.18(9) 2_556 1_555 2_556 yes
S2 RE2 S2 172.5(1) 1_555 1_555 2_556 yes
RE1 RE3 RE1 89.35(2) 1_555 1_555 2_556 yes
RE1 RE3 RE2 59.86(1) 1_555 1_555 1_555 yes
RE1 RE3 RE2 59.86(1) 1_555 1_555 5_656 yes
RE1 RE3 CL2 135.1(1) 1_555 1_555 1_555 yes
RE1 RE3 S1 116.91(6) 1_555 1_555 2_556 yes
RE1 RE3 S1 116.91(6) 1_555 1_555 5_656 yes
RE1 RE3 S2 57.15(6) 1_555 1_555 1_555 yes
RE1 RE3 S2 57.15(6) 1_555 1_555 6_655 yes
RE1 RE3 RE2 59.83(1) 2_556 1_555 1_555 yes
RE1 RE3 RE2 59.83(1) 2_556 1_555 5_656 yes
RE1 RE3 CL2 135.5(1) 2_556 1_555 1_555 yes
RE1 RE3 S1 57.05(6) 2_556 1_555 2_556 yes
RE1 RE3 S1 57.05(6) 2_556 1_555 5_656 yes
RE1 RE3 S2 117.08(7) 2_556 1_555 1_555 yes
RE1 RE3 S2 117.08(7) 2_556 1_555 6_655 yes
RE2 RE3 RE2 90.12(2) 1_555 1_555 5_656 yes
RE2 RE3 CL2 134.94(1) 1_555 1_555 1_555 yes
RE2 RE3 S1 57.12(6) 1_555 1_555 2_556 yes
RE2 RE3 S1 116.86(7) 1_555 1_555 5_656 yes
RE2 RE3 S2 57.31(7) 1_555 1_555 1_555 yes
RE2 RE3 S2 116.99(6) 1_555 1_555 6_655 yes
RE2 RE3 CL2 134.94(1) 5_656 1_555 1_555 yes
RE2 RE3 S1 116.86(7) 5_656 1_555 2_556 yes
RE2 RE3 S1 57.12(6) 5_656 1_555 5_656 yes
RE2 RE3 S2 116.99(6) 5_656 1_555 1_555 yes
RE2 RE3 S2 57.31(7) 5_656 1_555 6_655 yes
CL2 RE3 S1 93.8(1) 1_555 1_555 2_556 yes
CL2 RE3 S1 93.8(1) 1_555 1_555 5_656 yes
CL2 RE3 S2 93.4(1) 1_555 1_555 1_555 yes
CL2 RE3 S2 93.4(1) 1_555 1_555 6_655 yes
S1 RE3 S1 89.3(1) 2_556 1_555 5_656 yes
S1 RE3 S2 90.31(9) 2_556 1_555 1_555 yes
S1 RE3 S2 172.81(9) 2_556 1_555 6_655 yes
S1 RE3 S2 172.81(9) 5_656 1_555 1_555 yes
S1 RE3 S2 90.31(9) 5_656 1_555 6_655 yes
S2 RE3 S2 89.2(1) 1_555 1_555 6_655 yes
RE1 S1 RE2 65.37(6) 1_555 1_555 1_555 yes
RE1 S1 RE3 65.23(7) 1_555 1_555 2_556 yes
RE2 S1 RE3 65.51(7) 1_555 1_555 2_556 yes
RE1 S2 RE2 65.32(7) 1_555 1_555 1_555 yes
RE1 S2 RE3 65.29(7) 1_555 1_555 1_555 yes
RE2 S2 RE3 65.56(7) 1_555 1_555 1_555 yes
RE1 N11 C12 118(1) 1_555 1_555 1_555 yes
RE1 N11 C13 148.6(8) 1_555 1_555 1_555 yes
RE1 N11 C15 150.7(8) 1_555 1_555 1_555 yes
RE1 N11 C16 120(1) 1_555 1_555 1_555 yes
RE1 N11 H12 92.9(5) 1_555 1_555 1_555 no
RE1 N11 H16 95.3(5) 1_555 1_555 1_555 no
C12 N11 C16 121(1) 1_555 1_555 1_555 yes
C101 N101 C101 114(1) 1_555 1_555 15_555 yes
C101 N101 C105 110.7(8) 1_555 1_555 1_555 yes
C101 N101 C105 106.3(8) 1_555 1_555 15_555 yes
C101 N101 C105 110.7(8) 15_555 1_555 15_555 yes
C105 N101 C105 108(1) 1_555 1_555 15_555 yes
N11 C12 C13 120(1) 1_555 1_555 1_555 yes
N11 C12 H12 119(1) 1_555 1_555 1_555 no
C13 C12 H12 120(1) 1_555 1_555 1_555 no
C12 C13 C14 119(1) 1_555 1_555 1_555 yes
C12 C13 H13 119(2) 1_555 1_555 1_555 no
C14 C13 H13 120(2) 1_555 1_555 1_555 no
C13 C14 C17 120(2) 1_555 1_555 1_555 yes
C15 C14 C17 120(2) 1_555 1_555 1_555 yes
C16 C15 H15 120(2) 1_555 1_555 1_555 no
N11 C16 C15 121(1) 1_555 1_555 1_555 yes
N11 C16 H16 119(1) 1_555 1_555 1_555 no
C15 C16 H16 119(1) 1_555 1_555 1_555 no
N101 C101 C102 112(1) 1_555 1_555 1_555 yes
C101 C102 C103 109(1) 1_555 1_555 1_555 yes
C102 C103 C104 113(1) 1_555 1_555 1_555 yes
N101 C105 C106 112(1) 1_555 1_555 1_555 yes
C105 C106 C107 108(1) 1_555 1_555 1_555 yes
C106 C107 C108 115(2) 1_555 1_555 1_555 yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
RE1 RE2 2.5889(6) 1_555 1_555 yes
RE1 RE2 2.5889(6) 1_555 5_656 yes
RE1 RE3 2.5851(8) 1_555 1_555 yes
RE1 RE3 2.5873(8) 1_555 2_556 yes
RE1 S1 2.391(3) 1_555 1_555 yes
RE1 S1 2.391(3) 1_555 6_655 yes
RE1 S2 2.391(3) 1_555 1_555 yes
RE1 S2 2.391(3) 1_555 6_655 yes
RE1 N11 2.21(1) 1_555 1_555 yes
RE2 RE3 2.6034(6) 1_555 1_555 yes
RE2 RE3 2.6034(6) 1_555 2_556 yes
RE2 CL1 2.422(4) 1_555 1_555 yes
RE2 S1 2.402(3) 1_555 1_555 yes
RE2 S1 2.402(3) 1_555 2_556 yes
RE2 S2 2.407(3) 1_555 1_555 yes
RE2 S2 2.407(3) 1_555 2_556 yes
RE3 CL2 2.424(4) 1_555 1_555 yes
RE3 S1 2.409(3) 1_555 2_556 yes
RE3 S1 2.409(3) 1_555 5_656 yes
RE3 S2 2.402(3) 1_555 1_555 yes
RE3 S2 2.402(3) 1_555 6_655 yes
N11 C12 1.33(2) 1_555 1_555 yes
N11 C16 1.31(2) 1_555 1_555 yes
N18 C17 1.16(3) 1_555 1_555 yes
N101 C101 1.54(2) 1_555 1_555 yes
N101 C105 1.58(2) 1_555 1_555 yes
C12 C13 1.37(3) 1_555 1_555 yes
C13 C14 1.35(3) 1_555 1_555 yes
C14 C15 1.40(3) 1_555 1_555 yes
C14 C17 1.41(3) 1_555 1_555 yes
C15 C16 1.38(2) 1_555 1_555 yes
C101 C102 1.51(2) 1_555 1_555 yes
C102 C103 1.52(2) 1_555 1_555 yes
C103 C104 1.46(3) 1_555 1_555 yes
C105 C106 1.53(2) 1_555 1_555 yes
C106 C107 1.66(3) 1_555 1_555 yes
C107 C108 1.46(4) 1_555 1_555 yes
