#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:39:19 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179340 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/37/4323774.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4323774
loop_
_publ_author_name
'F. Albert Cotton'
'John H. Matonic'
'Carlos A. Murillo'
_publ_section_title
;
 Synthesis and Structural Studies of Platinum Complexes Containing
 Monodentate, Bridging, and Chelating Formamidine Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              498
_journal_page_last               503
_journal_paper_doi               10.1021/ic950741e
_journal_volume                  35
_journal_year                    1996
_chemical_formula_analytical     'C47.09 H3.19 N8.22'
_chemical_formula_moiety         'C26 H24 Cl2 Pt'
_chemical_formula_structural     'Pt Cl2 (C13 H12 N2)2'
_chemical_formula_sum            'C26 H24 Cl2 N4 Pt'
_chemical_formula_weight         658.48
_chemical_name_systematic
;
 trans-dichloro-bis-diphenylformamidine-platinate(II)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                90.00
_cell_angle_beta                 96.10(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   23.427(7)
_cell_length_b                   16.677(6)
_cell_length_c                   12.980(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      12.5
_cell_measurement_theta_min      7.5
_cell_volume                     5042(3)
_computing_cell_refinement       'P3 software'
_computing_data_collection       'P3 software'
_computing_data_reduction        'Structure Determination Package'
_computing_molecular_graphics    ORTEP
_computing_publication_material  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       'Syntex P3'
_diffrn_measurement_method       Omega
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0530
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            4511
_diffrn_reflns_theta_max         22.60
_diffrn_reflns_theta_min         2.11
_diffrn_standards_decay_%        -4.6
_diffrn_standards_interval_count 97
_diffrn_standards_number         153
_exptl_absorpt_coefficient_mu    5.798
_exptl_absorpt_correction_T_max  0.9981
_exptl_absorpt_correction_T_min  0.6590
_exptl_absorpt_correction_type   psi-scans
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.735
_exptl_crystal_description       block
_exptl_crystal_F_000             2560
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.742
_refine_diff_density_min         -0.476
_refine_diff_density_rms         0.113
_refine_ls_extinction_coef       none
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.059
_refine_ls_goodness_of_fit_obs   1.044
_refine_ls_hydrogen_treatment    'calculated, ride on carbon atoms'
_refine_ls_matrix_type           full
_refine_ls_number_parameters     595
_refine_ls_number_reflns         4509
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.084
_refine_ls_restrained_S_obs      1.044
_refine_ls_R_factor_all          0.0344
_refine_ls_R_factor_obs          0.0327
_refine_ls_shift/esd_max         -0.228
_refine_ls_shift/esd_mean        0.020
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0241P)²+12.6331P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0773
_refine_ls_wR_factor_obs         0.0737
_reflns_number_observed          4435
_reflns_number_total             4511
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic950741e_1.cif
_cod_data_source_block           C26H24Cl2N4Pt
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0241P)^2^+12.6331P] where P=(Fo^2^+2Fc^2^)/3'
was changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0241P)^2^+12.6331P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        5042.5(28)
_cod_database_code               4323774
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Pt1 Pt 0.09236(2) 0.05863(2) 0.11308(3) 0.03646(13) Uani 1 d . .
Cl1 Cl 0.10313(15) 0.1587(2) 0.2358(2) 0.0672(9) Uani 1 d . .
Cl2 Cl 0.07602(11) -0.0405(2) -0.0119(2) 0.0462(7) Uani 1 d . .
N1 N 0.1054(3) 0.1421(5) 0.0026(6) 0.036(2) Uani 1 d . .
N2 N 0.0118(3) 0.1888(5) -0.0110(7) 0.049(2) Uani 1 d . .
N3 N 0.0923(4) -0.0250(6) 0.2263(7) 0.049(2) Uani 1 d . .
N4 N -0.0058(4) -0.0330(6) 0.2390(7) 0.053(2) Uani 1 d . .
C1 C 0.0652(5) 0.1911(6) -0.0362(8) 0.038(3) Uani 1 d . .
H1 H 0.0744(5) 0.2294(6) -0.0838(8) 0.046 Uiso 1 calc R .
C2 C 0.0478(5) -0.0519(6) 0.2683(8) 0.048(3) Uani 1 d . .
H2 H 0.0547(5) -0.0875(6) 0.3234(8) 0.058 Uiso 1 calc R .
C11 C 0.1621(4) 0.1527(6) -0.0228(7) 0.030(2) Uani 1 d . .
C12 C 0.1978(4) 0.0864(7) -0.0242(7) 0.041(3) Uani 1 d . .
H12 H 0.1850(4) 0.0362(7) -0.0057(7) 0.049 Uiso 1 calc R .
C13 C 0.2528(5) 0.0955(8) -0.0535(8) 0.051(3) Uani 1 d . .
H13 H 0.2763(5) 0.0508(8) -0.0575(8) 0.061 Uiso 1 calc R .
C14 C 0.2724(5) 0.1691(8) -0.0762(8) 0.052(3) Uani 1 d . .
H14 H 0.3096(5) 0.1752(8) -0.0938(8) 0.062 Uiso 1 calc R .
C15 C 0.2374(5) 0.2347(7) -0.0731(9) 0.052(3) Uani 1 d . .
H15 H 0.2504(5) 0.2849(7) -0.0915(9) 0.062 Uiso 1 calc R .
C16 C 0.1837(4) 0.2268(7) -0.0432(9) 0.048(3) Uani 1 d . .
H16 H 0.1613(4) 0.2722(7) -0.0365(9) 0.058 Uiso 1 calc R .
C21 C -0.0309(4) 0.2454(6) -0.0485(9) 0.044(3) Uani 1 d . .
C22 C -0.0310(5) 0.2881(7) -0.1405(10) 0.059(3) Uani 1 d . .
H22 H -0.0022(5) 0.2784(7) -0.1830(10) 0.071 Uiso 1 calc R .
C23 C -0.0714(7) 0.3432(8) -0.1696(12) 0.075(4) Uani 1 d . .
H23 H -0.0683(7) 0.3737(8) -0.2287(12) 0.090 Uiso 1 calc R .
C24 C -0.1169(6) 0.3549(8) -0.1142(13) 0.076(4) Uani 1 d . .
H24 H -0.1457(6) 0.3914(8) -0.1358(13) 0.091 Uiso 1 calc R .
C25 C -0.1184(6) 0.3109(8) -0.0255(11) 0.071(4) Uani 1 d . .
H25 H -0.1492(6) 0.3185(8) 0.0133(11) 0.085 Uiso 1 calc R .
C26 C -0.0767(5) 0.2561(7) 0.0092(10) 0.059(3) Uani 1 d . .
H26 H -0.0793(5) 0.2271(7) 0.0697(10) 0.070 Uiso 1 calc R .
C31 C 0.1460(5) -0.0600(8) 0.2597(9) 0.054(3) Uani 1 d . .
C32 C 0.1560(6) -0.1403(10) 0.247(1) 0.076(4) Uani 1 d . .
H32 H 0.1266(6) -0.1727(10) 0.216(1) 0.091 Uiso 1 calc R .
C33 C 0.2087(9) -0.1735(12) 0.278(1) 0.104(6) Uani 1 d . .
H33 H 0.2139(9) -0.2283(12) 0.270(1) 0.125 Uiso 1 calc R .
C34 C 0.2530(8) -0.1294(15) 0.321(1) 0.108(7) Uani 1 d . .
H34 H 0.2880(8) -0.1533(15) 0.344(1) 0.130 Uiso 1 calc R .
C35 C 0.2454(7) -0.0481(13) 0.331(1) 0.098(5) Uani 1 d . .
H35 H 0.2761(7) -0.0157(13) 0.356(1) 0.117 Uiso 1 calc R .
C36 C 0.1905(6) -0.0138(10) 0.302(1) 0.082(4) Uani 1 d . .
H36 H 0.1847(6) 0.0406(10) 0.313(1) 0.098 Uiso 1 calc R .
C41 C 0.0511(5) 0.0543(6) 0.6991(8) 0.044(3) Uani 1 d . .
C42 C 0.1060(5) 0.0550(7) 0.745(1) 0.062(3) Uani 1 d . .
H42 H 0.1131(5) 0.0448(7) 0.815(1) 0.075 Uiso 1 calc R .
C43 C 0.1515(6) 0.0706(7) 0.688(1) 0.068(4) Uani 1 d . .
H43 H 0.1889(6) 0.0709(7) 0.720(1) 0.081 Uiso 1 calc R .
C44 C 0.1408(6) 0.0858(8) 0.583(1) 0.072(4) Uani 1 d . .
H44 H 0.1710(6) 0.0975(8) 0.544(1) 0.087 Uiso 1 calc R .
C45 C 0.0853(6) 0.0837(8) 0.535(1) 0.071(4) Uani 1 d . .
H45 H 0.0782(6) 0.0918(8) 0.464(1) 0.085 Uiso 1 calc R .
C46 C 0.0403(5) 0.0694(7) 0.5939(9) 0.059(3) Uani 1 d . .
H46 H 0.0028(5) 0.0700(7) 0.5624(9) 0.071 Uiso 1 calc R .
Pt2 Pt 0.58931(2) -0.51426(2) 0.41297(3) 0.0361(1) Uani 1 d . .
Cl3 Cl 0.58358(12) -0.4499(2) 0.5680(2) 0.0458(7) Uani 1 d . .
Cl4 Cl 0.5907(2) -0.5811(2) 0.2592(2) 0.0721(1) Uani 1 d . .
N5 N 0.6146(3) -0.6147(5) 0.4909(6) 0.035(2) Uani 1 d . .
N6 N 0.5273(3) -0.6815(5) 0.4818(6) 0.035(2) Uani 1 d . .
N7 N 0.5749(4) -0.4096(5) 0.3340(6) 0.041(2) Uani 1 d . .
N8 N 0.4791(4) -0.4300(5) 0.2774(7) 0.044(2) Uani 1 d . .
C3 C 0.5831(5) -0.6778(6) 0.5094(7) 0.036(3) Uani 1 d . .
H3 H 0.6010(5) -0.7216(6) 0.5434(7) 0.044 Uiso 1 calc R .
C4 C 0.5276(5) -0.3892(6) 0.2826(8) 0.042(3) Uani 1 d . .
H4 H 0.5273(5) -0.3414(6) 0.2457(8) 0.050 Uiso 1 calc R .
C51 C 0.6749(4) -0.6183(6) 0.5299(8) 0.039(3) Uani 1 d . .
C52 C 0.6928(5) -0.6166(7) 0.6321(8) 0.049(3) Uani 1 d . .
H52 H 0.6660(5) -0.6137(7) 0.6798(8) 0.059 Uiso 1 calc R .
C53 C 0.7516(5) -0.6190(8) 0.6671(10) 0.068(4) Uani 1 d . .
H53 H 0.7635(5) -0.6187(8) 0.7378(10) 0.082 Uiso 1 calc R .
C54 C 0.7907(5) -0.6218(7) 0.5986(11) 0.059(3) Uani 1 d . .
H54 H 0.8296(5) -0.6230(7) 0.6215(11) 0.071 Uiso 1 calc R .
C55 C 0.7728(5) -0.6229(7) 0.4948(11) 0.061(3) Uani 1 d . .
H55 H 0.8000(5) -0.6266(7) 0.4478(11) 0.073 Uiso 1 calc R .
C56 C 0.7150(4) -0.6186(6) 0.4579(9) 0.046(3) Uani 1 d . .
H56 H 0.7034(4) -0.6160(6) 0.3872(9) 0.055 Uiso 1 calc R .
C61 C 0.4952(4) -0.7546(6) 0.4837(8) 0.037(3) Uani 1 d . .
C62 C 0.4413(4) -0.7569(6) 0.4294(8) 0.041(3) Uani 1 d . .
H62 H 0.4273(4) -0.7122(6) 0.3921(8) 0.049 Uiso 1 calc R .
C63 C 0.4074(5) -0.8265(8) 0.4300(9) 0.053(3) Uani 1 d . .
H63 H 0.3704(5) -0.8271(8) 0.3962(9) 0.064 Uiso 1 calc R .
C64 C 0.4297(5) -0.8932(7) 0.4809(9) 0.054(3) Uani 1 d . .
H64 H 0.4084(5) -0.9404(7) 0.4781(9) 0.065 Uiso 1 calc R .
C65 C 0.4824(6) -0.8912(6) 0.535(1) 0.064(4) Uani 1 d . .
H65 H 0.4962(6) -0.9367(6) 0.571(1) 0.077 Uiso 1 calc R .
C66 C 0.5168(5) -0.8212(7) 0.5386(9) 0.058(3) Uani 1 d . .
H66 H 0.5528(5) -0.8200(7) 0.5765(9) 0.070 Uiso 1 calc R .
C71 C 0.6241(5) -0.3578(7) 0.3293(8) 0.043(3) Uani 1 d . .
C72 C 0.6749(5) -0.3894(7) 0.3135(8) 0.053(3) Uani 1 d . .
H72 H 0.6786(5) -0.4447(7) 0.3078(8) 0.063 Uiso 1 calc R .
C73 C 0.7222(5) -0.3401(9) 0.3054(9) 0.063(4) Uani 1 d . .
H73 H 0.7574(5) -0.3625(9) 0.2940(9) 0.075 Uiso 1 calc R .
C74 C 0.7169(6) -0.2570(9) 0.3143(9) 0.066(4) Uani 1 d . .
H74 H 0.7483(6) -0.2237(9) 0.3091(9) 0.079 Uiso 1 calc R .
C75 C 0.6647(6) -0.2255(8) 0.3309(9) 0.067(4) Uani 1 d . .
H75 H 0.6605(6) -0.1702(8) 0.3362(9) 0.080 Uiso 1 calc R .
C76 C 0.6180(5) -0.2757(7) 0.3398(8) 0.052(3) Uani 1 d . .
H76 H 0.5829(5) -0.2541(7) 0.3529(8) 0.063 Uiso 1 calc R .
C81 C 0.4281(5) -0.4055(7) 0.2161(8) 0.047(3) Uani 1 d . .
C82 C 0.4140(5) -0.3256(7) 0.203(1) 0.058(3) Uani 1 d . .
H82 H 0.4388(5) -0.2861(7) 0.232(1) 0.070 Uiso 1 calc R .
C83 C 0.3616(7) -0.3041(11) 0.145(1) 0.087(5) Uani 1 d . .
H83 H 0.3514(7) -0.2503(11) 0.138(1) 0.104 Uiso 1 calc R .
C84 C 0.3257(7) -0.3618(14) 0.099(1) 0.094(6) Uani 1 d . .
H84 H 0.2920(7) -0.3473(14) 0.059(1) 0.113 Uiso 1 calc R .
C85 C 0.3398(7) -0.4402(12) 0.113(1) 0.092(5) Uani 1 d . .
H85 H 0.3151(7) -0.4795(12) 0.084(1) 0.111 Uiso 1 calc R .
C86 C 0.3910(5) -0.4631(8) 0.1721(9) 0.064(4) Uani 1 d . .
H86 H 0.3999(5) -0.5171(8) 0.1811(9) 0.076 Uiso 1 calc R .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N3 Pt1 N1 171.5(3) . . y
N3 Pt1 Cl1 90.4(3) . . y
N1 Pt1 Cl1 88.7(2) . . y
N3 Pt1 Cl2 90.2(3) . . y
N1 Pt1 Cl2 91.2(2) . . y
Cl1 Pt1 Cl2 176.8(1) . . y
C1 N1 C11 119.3(8) . . ?
C1 N1 Pt1 122.7(7) . . ?
C11 N1 Pt1 117.5(6) . . ?
C1 N2 C21 123.0(9) . . ?
C2 N3 C31 117(1) . . ?
C2 N3 Pt1 127.0(8) . . ?
C31 N3 Pt1 115.9(7) . . ?
C2 N4 C41 121.2(9) . 3_556 ?
N1 C1 N2 123.1(9) . . y
N3 C2 N4 125(1) . . y
C16 C11 C12 118.7(9) . . ?
C16 C11 N1 122.1(9) . . ?
C12 C11 N1 119.1(9) . . ?
C11 C12 C13 119(1) . . ?
C14 C13 C12 120(1) . . ?
C13 C14 C15 120(1) . . ?
C16 C15 C14 120(1) . . ?
C15 C16 C11 121(1) . . ?
C26 C21 C22 118(1) . . ?
C26 C21 N2 117(1) . . ?
C22 C21 N2 125(1) . . ?
C23 C22 C21 122(1) . . ?
C22 C23 C24 121(1) . . ?
C23 C24 C25 117(1) . . ?
C24 C25 C26 123(1) . . ?
C25 C26 C21 118(1) . . ?
C36 C31 C32 118(1) . . ?
C36 C31 N3 120(1) . . ?
C32 C31 N3 121(1) . . ?
C31 C32 C33 121(2) . . ?
C34 C33 C32 122(2) . . ?
C33 C34 C35 118(2) . . ?
C34 C35 C36 120(2) . . ?
C31 C36 C35 121(2) . . ?
C42 C41 C46 120(1) . . ?
C42 C41 N4 118(1) . 3_556 ?
C46 C41 N4 122(1) . 3_556 ?
C41 C42 C43 121(1) . . ?
C44 C43 C42 119(1) . . ?
C45 C44 C43 120(1) . . ?
C44 C45 C46 120(1) . . ?
C45 C46 C41 120(1) . . ?
N5 Pt2 N7 172.5(3) . . y
N5 Pt2 Cl4 90.1(2) . . y
N7 Pt2 Cl4 89.7(3) . . y
N5 Pt2 Cl3 89.4(2) . . y
N7 Pt2 Cl3 91.0(2) . . y
Cl4 Pt2 Cl3 177(1) . . y
C3 N5 C51 116.5(8) . . ?
C3 N5 Pt2 127.8(7) . . ?
C51 N5 Pt2 115.7(6) . . ?
C3 N6 C61 122.7(9) . . ?
C4 N7 C71 117.9(9) . . ?
C4 N7 Pt2 125.5(7) . . ?
C71 N7 Pt2 116.3(7) . . ?
C4 N8 C81 123.2(9) . . ?
N6 C3 N5 123(1) . . y
N7 C4 N8 126(1) . . y
C52 C51 C56 120(1) . . ?
C52 C51 N5 122.1(9) . . ?
C56 C51 N5 117.9(9) . . ?
C51 C52 C53 121(1) . . ?
C54 C53 C52 120(1) . . ?
C53 C54 C55 120(1) . . ?
C54 C55 C56 122(1) . . ?
C55 C56 C51 118(1) . . ?
C62 C61 C66 120(1) . . ?
C62 C61 N6 117.9(9) . . ?
C66 C61 N6 122(1) . . ?
C61 C62 C63 121(1) . . ?
C64 C63 C62 119(1) . . ?
C65 C64 C63 121(1) . . ?
C64 C65 C66 121(1) . . ?
C61 C66 C65 118(1) . . ?
C72 C71 C76 121(1) . . ?
C72 C71 N7 120(1) . . ?
C76 C71 N7 120(1) . . ?
C71 C72 C73 121(1) . . ?
C72 C73 C74 120(1) . . ?
C75 C74 C73 119(1) . . ?
C74 C75 C76 120(1) . . ?
C71 C76 C75 120(1) . . ?
C86 C81 C82 119(1) . . ?
C86 C81 N8 119(1) . . ?
C82 C81 N8 121(1) . . ?
C81 C82 C83 119(1) . . ?
C84 C83 C82 121(2) . . ?
C85 C84 C83 119(2) . . ?
C84 C85 C86 121(2) . . ?
C81 C86 C85 120(1) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N3 2.026(9) . y
Pt1 N1 2.045(8) . y
Pt1 Cl1 2.302(3) . y
Pt1 Cl2 2.319(3) . y
N1 C1 1.31(1) . ?
N1 C11 1.41(1) . ?
N2 C1 1.33(1) . ?
N2 C21 1.42(1) . ?
N3 C2 1.31(1) . ?
N3 C31 1.41(1) . ?
N4 C2 1.31(1) . ?
N4 C41 1.44(1) 3_556 ?
C11 C16 1.37(1) . ?
C11 C12 1.39(1) . ?
C12 C13 1.39(1) . ?
C13 C14 1.35(1) . ?
C14 C15 1.37(1) . ?
C15 C16 1.36(1) . ?
C21 C26 1.38(2) . ?
C21 C22 1.39(2) . ?
C22 C23 1.34(2) . ?
C23 C24 1.36(2) . ?
C24 C25 1.37(2) . ?
C25 C26 1.38(2) . ?
C31 C36 1.37(2) . ?
C31 C32 1.37(2) . ?
C32 C33 1.38(2) . ?
C33 C34 1.34(2) . ?
C34 C35 1.37(2) . ?
C35 C36 1.42(2) . ?
C41 C42 1.36(2) . ?
C41 C46 1.39(2) . ?
C41 N4 1.44(1) 3_556 ?
C42 C43 1.39(2) . ?
C43 C44 1.38(2) . ?
C44 C45 1.38(2) . ?
C45 C46 1.38(2) . ?
Pt2 N5 2.014(8) . y
Pt2 N7 2.033(8) . y
Pt2 Cl4 2.289(3) . y
Pt2 Cl3 2.297(3) . y
N5 C3 1.32(1) . ?
N5 C51 1.45(1) . ?
N6 C3 1.32(1) . ?
N6 C61 1.44(1) . ?
N7 C4 1.28(1) . ?
N7 C71 1.45(1) . ?
N8 C4 1.32(1) . ?
N8 C81 1.42(1) . ?
C51 C52 1.35(1) . ?
C51 C56 1.39(1) . ?
C52 C53 1.40(2) . ?
C53 C54 1.34(2) . ?
C54 C55 1.37(2) . ?
C55 C56 1.39(2) . ?
C61 C62 1.38(1) . ?
C61 C66 1.39(1) . ?
C62 C63 1.41(1) . ?
C63 C64 1.37(2) . ?
C64 C65 1.36(2) . ?
C65 C66 1.42(1) . ?
C71 C72 1.34(1) . ?
C71 C76 1.39(2) . ?
C72 C73 1.39(2) . ?
C73 C74 1.40(2) . ?
C74 C75 1.37(2) . ?
C75 C76 1.39(2) . ?
C81 C86 1.38(2) . ?
C81 C82 1.38(2) . ?
C82 C83 1.42(2) . ?
C83 C84 1.37(2) . ?
C84 C85 1.36(2) . ?
C85 C86 1.40(2) . ?
