#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/37/4323790.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4323790
loop_
_publ_author_name
'Mandy W. Avis'
'Cornelis J. Elsevier'
'Nora Veldman'
'Huub Kooijman'
'Anthony L. Spek'
_publ_section_title
;
 Monodentate σ-N and Bidentate σ-N,σ-N' Coordination of
 1,1-Bis((N-p-tolylimino)diphenylphosphoranyl)ethane,
 CHCH3(PPh2NC6H4-4-CH3)2, to Platinum(II)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1518
_journal_page_last               1528
_journal_paper_doi               10.1021/ic950748w
_journal_volume                  35
_journal_year                    1996
_chemical_formula_sum            'C52 H57 Cl2 N2 O P3 Pt'
_chemical_formula_weight         4339.58
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                90.00
_cell_angle_beta                 109.544(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.4021(7)
_cell_length_b                   16.9705(11)
_cell_length_c                   23.760(2)
_cell_measurement_temperature    150(2)
_cell_volume                     4712.6(6)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoKa
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0382
_diffrn_reflns_av_sigmaI/netI    0.1075
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            14499
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         1.51
_exptl_absorpt_coefficient_mu    3.233
_exptl_crystal_density_diffrn    1.529
_exptl_crystal_F_000             2192
_refine_diff_density_max         2.033
_refine_diff_density_min         -0.776
_refine_diff_density_rms         0.164
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   0.996
_refine_ls_goodness_of_fit_obs   1.134
_refine_ls_matrix_type           full
_refine_ls_number_parameters     555
_refine_ls_number_reflns         10778
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      0.999
_refine_ls_restrained_S_obs      1.138
_refine_ls_R_factor_all          0.1135
_refine_ls_R_factor_obs          0.0572
_refine_ls_shift/esd_max         0.079
_refine_ls_shift/esd_mean        0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[s²(Fo²)+( 0.0514P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1215
_refine_ls_wR_factor_obs         0.1088
_reflns_number_observed          6850
_reflns_number_total             10778
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic950748w_2.cif
_cod_data_source_block           3b
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc w=1/[s^2^(Fo^2^)+(
0.0514P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was changed to 'calc'.
New tag '_refine_ls_weighting_details' was created. The value of the
new tag was set to 'w=1/[s^2^(Fo^2^)+( 0.0514P)^2^+0.0000P] where
P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        4712.7(5)
_cod_original_formula_sum        'C52 H57 Cl2 N2 O1 P3 Pt1'
_cod_database_code               4323790
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Pt1 Pt 0.16390(2) 0.28149(2) 0.384635(12) 0.02225(8) Uani 1 d . .
Cl1 Cl -0.0043(2) 0.33960(13) 0.38251(9) 0.0388(5) Uani 1 d . .
P1 P 0.4268(2) 0.24324(10) 0.44542(8) 0.0217(4) Uani 1 d . .
P2 P 0.2980(2) 0.32826(10) 0.51538(8) 0.0234(4) Uani 1 d . .
P3 P 0.1216(2) 0.31213(11) 0.28820(9) 0.0272(4) Uani 1 d . .
N1 N 0.3128(4) 0.2245(3) 0.3898(2) 0.0221(12) Uani 1 d . .
N2 N 0.2055(5) 0.2637(3) 0.4783(3) 0.0236(13) Uani 1 d . .
C1 C 0.3053(6) 0.1558(4) 0.3529(3) 0.024(2) Uani 1 d . .
C2 C 0.2170(6) 0.1033(4) 0.3446(3) 0.029(2) Uani 1 d . .
H2 H 0.1624(6) 0.1120(4) 0.3641(3) 0.035 Uiso 1 calc R .
C3 C 0.2062(6) 0.0373(4) 0.3079(3) 0.032(2) Uani 1 d . .
H3 H 0.1461(6) 0.0007(4) 0.3038(3) 0.039 Uiso 1 calc R .
C4 C 0.2828(7) 0.0249(5) 0.2776(3) 0.037(2) Uani 1 d . .
C5 C 0.3691(7) 0.0779(4) 0.2855(4) 0.037(2) Uani 1 d . .
H5 H 0.4221(7) 0.0701(4) 0.2649(4) 0.044 Uiso 1 calc R .
C6 C 0.3819(6) 0.1424(4) 0.3222(3) 0.030(2) Uani 1 d . .
H6 H 0.4433(6) 0.1781(4) 0.3266(3) 0.036 Uiso 1 calc R .
C7 C 0.2738(9) -0.0464(5) 0.2384(4) 0.053(3) Uani 1 d . .
H7A H 0.1937(11) -0.0630(22) 0.2218(22) 0.080 Uiso 1 calc R .
H7B H 0.3197(42) -0.0895(13) 0.2621(7) 0.080 Uiso 1 calc R .
H7C H 0.3023(49) -0.0332(11) 0.2057(16) 0.080 Uiso 1 calc R .
C8 C 0.4623(6) 0.1673(4) 0.5019(3) 0.026(2) Uani 1 d . .
C9 C 0.3864(6) 0.1059(4) 0.4973(3) 0.027(2) Uani 1 d . .
H9 H 0.3156(6) 0.1047(4) 0.4653(3) 0.033 Uiso 1 calc R .
C10 C 0.4138(7) 0.0466(4) 0.5392(4) 0.036(2) Uani 1 d . .
H10 H 0.3617(7) 0.0043(4) 0.5355(4) 0.043 Uiso 1 calc R .
C11 C 0.5149(8) 0.0474(5) 0.5859(4) 0.043(2) Uani 1 d . .
H11 H 0.5319(8) 0.0066(5) 0.6150(4) 0.052 Uiso 1 calc R .
C12 C 0.5922(7) 0.1080(5) 0.5906(4) 0.039(2) Uani 1 d . .
H12 H 0.6629(7) 0.1081(5) 0.6227(4) 0.047 Uiso 1 calc R .
C13 C 0.5676(6) 0.1683(5) 0.5491(3) 0.031(2) Uani 1 d . .
H13 H 0.6209(6) 0.2097(5) 0.5523(3) 0.037 Uiso 1 calc R .
C14 C 0.5499(6) 0.2554(5) 0.4218(3) 0.031(2) Uani 1 d . .
C15 C 0.6364(7) 0.1999(7) 0.4338(4) 0.059(3) Uani 1 d . .
H15 H 0.6362(7) 0.1558(7) 0.4584(4) 0.070 Uiso 1 calc R .
C16 C 0.7224(8) 0.2087(9) 0.4103(5) 0.089(5) Uani 1 d . .
H16 H 0.7821(8) 0.1708(9) 0.4183(5) 0.107 Uiso 1 calc R .
C17 C 0.7213(9) 0.2742(10) 0.3741(5) 0.089(5) Uani 1 d . .
H17 H 0.7798(9) 0.2808(10) 0.3570(5) 0.107 Uiso 1 calc R .
C18 C 0.6390(12) 0.3262(7) 0.3642(5) 0.073(4) Uani 1 d . .
H18 H 0.6406(12) 0.3707(7) 0.3402(5) 0.088 Uiso 1 calc R .
C19 C 0.5497(8) 0.3202(5) 0.3867(4) 0.046(2) Uani 1 d . .
H19 H 0.4911(8) 0.3589(5) 0.3783(4) 0.055 Uiso 1 calc R .
C20 C 0.4015(6) 0.3369(4) 0.4763(3) 0.024(2) Uani 1 d . .
H20 H 0.3645(6) 0.3715(4) 0.4411(3) 0.029 Uiso 1 calc R .
C21 C 0.5117(6) 0.3805(4) 0.5135(3) 0.031(2) Uani 1 d . .
H21A H 0.5527(22) 0.3489(14) 0.5487(12) 0.047 Uiso 1 calc R .
H21B H 0.4915(7) 0.4317(13) 0.5263(18) 0.047 Uiso 1 calc R .
H21C H 0.5607(19) 0.3885(25) 0.4891(8) 0.047 Uiso 1 calc R .
C22 C 0.2445(6) 0.4275(4) 0.5197(3) 0.028(2) Uani 1 d . .
C23 C 0.2112(7) 0.4485(4) 0.5677(4) 0.034(2) Uani 1 d . .
H23 H 0.2254(7) 0.4140(4) 0.6009(4) 0.041 Uiso 1 calc R .
C24 C 0.1584(7) 0.5183(5) 0.5672(4) 0.044(2) Uani 1 d . .
H24 H 0.1342(7) 0.5319(5) 0.6000(4) 0.053 Uiso 1 calc R .
C25 C 0.1389(7) 0.5699(5) 0.5204(4) 0.045(2) Uani 1 d . .
H25 H 0.1006(7) 0.6183(5) 0.5205(4) 0.054 Uiso 1 calc R .
C26 C 0.1748(8) 0.5515(5) 0.4739(4) 0.051(3) Uani 1 d . .
H26 H 0.1651(8) 0.5885(5) 0.4426(4) 0.062 Uiso 1 calc R .
C27 C 0.2259(7) 0.4784(5) 0.4716(4) 0.039(2) Uani 1 d . .
H27 H 0.2471(7) 0.4640(5) 0.4381(4) 0.047 Uiso 1 calc R .
C28 C 0.3720(6) 0.2989(4) 0.5911(3) 0.026(2) Uani 1 d . .
C29 C 0.4444(6) 0.3532(5) 0.6310(3) 0.033(2) Uani 1 d . .
H29 H 0.4507(6) 0.4059(5) 0.6189(3) 0.040 Uiso 1 calc R .
C30 C 0.5063(7) 0.3280(5) 0.6880(4) 0.042(2) Uani 1 d . .
H30 H 0.5580(7) 0.3635(5) 0.7147(4) 0.050 Uiso 1 calc R .
C31 C 0.4949(7) 0.2537(6) 0.7070(4) 0.045(2) Uani 1 d . .
H31 H 0.5364(7) 0.2386(6) 0.7469(4) 0.054 Uiso 1 calc R .
C32 C 0.4235(7) 0.2003(5) 0.6685(4) 0.042(2) Uani 1 d . .
H32 H 0.4167(7) 0.1482(5) 0.6817(4) 0.050 Uiso 1 calc R .
C33 C 0.3610(6) 0.2228(5) 0.6100(3) 0.032(2) Uani 1 d . .
H33 H 0.3115(6) 0.1863(5) 0.5834(3) 0.038 Uiso 1 calc R .
C34 C 0.1218(6) 0.2279(4) 0.4996(3) 0.028(2) Uani 1 d . .
C35 C 0.0827(7) 0.2612(5) 0.5419(4) 0.038(2) Uani 1 d . .
H35 H 0.1079(7) 0.3123(5) 0.5570(4) 0.046 Uiso 1 calc R .
C36 C 0.0058(7) 0.2198(6) 0.5625(4) 0.044(2) Uani 1 d . .
H36 H -0.0191(7) 0.2432(6) 0.5923(4) 0.053 Uiso 1 calc R .
C37 C -0.0349(7) 0.1466(5) 0.5413(4) 0.040(2) Uani 1 d . .
C38 C 0.0027(7) 0.1162(5) 0.4971(4) 0.044(2) Uani 1 d . .
H38 H -0.0250(7) 0.0663(5) 0.4802(4) 0.053 Uiso 1 calc R .
C39 C 0.0783(6) 0.1559(5) 0.4771(4) 0.038(2) Uani 1 d . .
H39 H 0.1016(6) 0.1330(5) 0.4465(4) 0.045 Uiso 1 calc R .
C40 C -0.1181(9) 0.1020(7) 0.5645(5) 0.069(3) Uani 1 d . .
H40A H -0.1630(42) 0.1396(7) 0.5788(29) 0.103 Uiso 1 calc R .
H40B H -0.0752(9) 0.0674(31) 0.5974(21) 0.103 Uiso 1 calc R .
H40C H -0.1697(40) 0.0702(32) 0.5322(10) 0.103 Uiso 1 calc R .
C41 C 0.0096(7) 0.2512(5) 0.2388(3) 0.034(2) Uani 1 d . .
C42 C -0.1032(8) 0.2713(6) 0.2273(4) 0.055(3) Uani 1 d . .
H42 H -0.1219(8) 0.3189(6) 0.2430(4) 0.066 Uiso 1 calc R .
C43 C -0.1906(9) 0.2220(7) 0.1926(4) 0.068(3) Uani 1 d . .
H43 H -0.2684(9) 0.2361(7) 0.1847(4) 0.082 Uiso 1 calc R .
C44 C -0.1634(10) 0.1527(7) 0.1697(4) 0.066(3) Uani 1 d . .
H44 H -0.2222(10) 0.1189(7) 0.1460(4) 0.080 Uiso 1 calc R .
C45 C -0.0529(10) 0.1337(6) 0.1813(4) 0.058(3) Uani 1 d . .
H45 H -0.0342(10) 0.0856(6) 0.1664(4) 0.070 Uiso 1 calc R .
C46 C 0.0349(9) 0.1830(5) 0.2149(4) 0.047(2) Uani 1 d . .
H46 H 0.1124(9) 0.1694(5) 0.2212(4) 0.057 Uiso 1 calc R .
C47 C 0.2367(7) 0.3083(5) 0.2579(3) 0.037(2) Uani 1 d . .
H47A H 0.2695(29) 0.2552(9) 0.2631(21) 0.056 Uiso 1 calc R .
H47B H 0.2960(21) 0.3464(22) 0.2788(16) 0.056 Uiso 1 calc R .
H47C H 0.2073(11) 0.3214(30) 0.2153(6) 0.056 Uiso 1 calc R .
C48 C 0.0724(7) 0.4133(4) 0.2724(4) 0.037(2) Uani 1 d . .
H48A H 0.0097(30) 0.4229(10) 0.2879(21) 0.055 Uiso 1 calc R .
H48B H 0.0453(41) 0.4220(10) 0.2291(4) 0.055 Uiso 1 calc R .
H48C H 0.1357(13) 0.4494(4) 0.2916(20) 0.055 Uiso 1 calc R .
O1 O 0.1007(5) 0.5892(4) 0.1747(3) 0.0440(15) Uani 1 d D .
C49 C 0.2322(11) 0.5675(11) 0.1997(6) 0.122(6) Uani 1 d D .
H49A H 0.2728(11) 0.6181(11) 0.2125(6) 0.146 Uiso 1 calc R .
H49B H 0.2428(11) 0.5371(11) 0.2368(6) 0.146 Uiso 1 calc R .
C50 C 0.2968(12) 0.5258(11) 0.1685(7) 0.133(7) Uani 1 d D .
H50A H 0.3208(12) 0.5609(11) 0.1416(7) 0.159 Uiso 1 calc R .
H50B H 0.3647(12) 0.4991(11) 0.1964(7) 0.159 Uiso 1 calc R .
C51 C 0.2206(11) 0.4768(6) 0.1396(5) 0.049(3) Uani 1 d D .
H51A H 0.2343(11) 0.4237(6) 0.1580(5) 0.059 Uiso 1 calc R .
H51B H 0.2162(11) 0.4729(6) 0.0973(5) 0.059 Uiso 1 calc R .
C52 C 0.1188(18) 0.5125(12) 0.1452(8) 0.270(19) Uani 1 d D .
H52A H 0.0862(18) 0.4713(12) 0.1642(8) 0.324 Uiso 1 calc R .
H52B H 0.0658(18) 0.5166(12) 0.1036(8) 0.324 Uiso 1 calc R .
Cl2 Cl 0.3625(2) 0.48241(13) 0.35721(11) 0.0521(6) Uani 1 d . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Pt1 N2 88.4(2) . . ?
N1 Pt1 P3 93.9(2) . . ?
N2 Pt1 P3 174.7(2) . . ?
N1 Pt1 Cl1 176.6(2) . . ?
N2 Pt1 Cl1 89.1(2) . . ?
P3 Pt1 Cl1 88.71(7) . . ?
N1 P1 C8 113.5(3) . . ?
N1 P1 C14 111.6(3) . . ?
C8 P1 C14 106.9(3) . . ?
N1 P1 C20 106.3(3) . . ?
C8 P1 C20 110.8(3) . . ?
C14 P1 C20 107.7(3) . . ?
N2 P2 C28 113.0(3) . . ?
N2 P2 C20 105.6(3) . . ?
C28 P2 C20 108.7(3) . . ?
N2 P2 C22 116.8(3) . . ?
C28 P2 C22 105.8(3) . . ?
C20 P2 C22 106.6(3) . . ?
C47 P3 C41 105.0(4) . . ?
C47 P3 C48 101.9(4) . . ?
C41 P3 C48 105.9(4) . . ?
C47 P3 Pt1 117.1(3) . . ?
C41 P3 Pt1 113.4(3) . . ?
C48 P3 Pt1 112.3(3) . . ?
C1 N1 P1 121.2(4) . . ?
C1 N1 Pt1 118.1(4) . . ?
P1 N1 Pt1 118.7(3) . . ?
C34 N2 P2 124.0(5) . . ?
C34 N2 Pt1 118.6(4) . . ?
P2 N2 Pt1 110.7(3) . . ?
C2 C1 C6 117.9(7) . . ?
C2 C1 N1 119.9(6) . . ?
C6 C1 N1 122.2(6) . . ?
C1 C2 C3 121.0(7) . . ?
C4 C3 C2 120.4(7) . . ?
C5 C4 C3 118.2(7) . . ?
C5 C4 C7 120.4(8) . . ?
C3 C4 C7 121.4(8) . . ?
C4 C5 C6 122.1(8) . . ?
C5 C6 C1 120.5(7) . . ?
C9 C8 C13 119.8(7) . . ?
C9 C8 P1 119.2(6) . . ?
C13 C8 P1 121.0(5) . . ?
C10 C9 C8 119.8(7) . . ?
C11 C10 C9 121.1(8) . . ?
C10 C11 C12 119.6(8) . . ?
C13 C12 C11 120.7(8) . . ?
C12 C13 C8 119.0(7) . . ?
C19 C14 C15 120.8(8) . . ?
C19 C14 P1 116.6(7) . . ?
C15 C14 P1 122.4(6) . . ?
C16 C15 C14 119.9(10) . . ?
C15 C16 C17 119.2(11) . . ?
C18 C17 C16 119.5(9) . . ?
C17 C18 C19 123.8(11) . . ?
C14 C19 C18 116.9(10) . . ?
C21 C20 P1 114.2(5) . . ?
C21 C20 P2 112.7(5) . . ?
P1 C20 P2 112.4(4) . . ?
C23 C22 C27 120.3(7) . . ?
C23 C22 P2 120.0(6) . . ?
C27 C22 P2 119.3(6) . . ?
C24 C23 C22 119.9(8) . . ?
C23 C24 C25 121.2(8) . . ?
C26 C25 C24 119.8(8) . . ?
C25 C26 C27 120.7(9) . . ?
C22 C27 C26 118.0(8) . . ?
C33 C28 C29 120.0(7) . . ?
C33 C28 P2 120.6(5) . . ?
C29 C28 P2 119.4(5) . . ?
C30 C29 C28 118.5(8) . . ?
C31 C30 C29 121.7(8) . . ?
C30 C31 C32 120.3(8) . . ?
C31 C32 C33 119.8(8) . . ?
C28 C33 C32 119.6(8) . . ?
C39 C34 C35 117.6(7) . . ?
C39 C34 N2 118.4(7) . . ?
C35 C34 N2 124.0(7) . . ?
C34 C35 C36 119.9(8) . . ?
C37 C36 C35 122.5(8) . . ?
C36 C37 C38 116.1(7) . . ?
C36 C37 C40 121.8(8) . . ?
C38 C37 C40 122.0(8) . . ?
C39 C38 C37 121.8(8) . . ?
C38 C39 C34 122.1(8) . . ?
C46 C41 C42 119.0(8) . . ?
C46 C41 P3 121.2(7) . . ?
C42 C41 P3 119.7(7) . . ?
C41 C42 C43 120.3(10) . . ?
C44 C43 C42 119.8(10) . . ?
C45 C44 C43 119.2(9) . . ?
C44 C45 C46 121.5(10) . . ?
C41 C46 C45 120.0(10) . . ?
C52 O1 C49 71.5(10) . . ?
C50 C49 O1 126.8(11) . . ?
C51 C50 C49 99.1(12) . . ?
C50 C51 C52 100.9(12) . . ?
C51 C52 O1 131.8(15) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 2.052(5) . ?
Pt1 N2 2.130(6) . ?
Pt1 P3 2.234(2) . ?
Pt1 Cl1 2.293(2) . ?
P1 N1 1.612(6) . ?
P1 C8 1.805(7) . ?
P1 C14 1.806(8) . ?
P1 C20 1.821(7) . ?
P2 N2 1.618(6) . ?
P2 C28 1.796(7) . ?
P2 C20 1.825(7) . ?
P2 C22 1.826(7) . ?
P3 C47 1.803(8) . ?
P3 C41 1.812(8) . ?
P3 C48 1.818(8) . ?
N1 C1 1.441(9) . ?
N2 C34 1.434(9) . ?
C1 C2 1.374(10) . ?
C1 C6 1.398(10) . ?
C2 C3 1.399(10) . ?
C3 C4 1.386(11) . ?
C4 C5 1.363(11) . ?
C4 C7 1.510(11) . ?
C5 C6 1.375(10) . ?
C8 C9 1.384(10) . ?
C8 C13 1.408(10) . ?
C9 C10 1.376(10) . ?
C10 C11 1.369(11) . ?
C11 C12 1.385(12) . ?
C12 C13 1.384(10) . ?
C14 C19 1.380(11) . ?
C14 C15 1.384(12) . ?
C15 C16 1.368(13) . ?
C16 C17 1.40(2) . ?
C17 C18 1.31(2) . ?
C18 C19 1.384(14) . ?
C20 C21 1.545(9) . ?
C22 C23 1.382(10) . ?
C22 C27 1.390(11) . ?
C23 C24 1.352(10) . ?
C24 C25 1.373(12) . ?
C25 C26 1.358(12) . ?
C26 C27 1.403(11) . ?
C28 C33 1.389(10) . ?
C28 C29 1.407(10) . ?
C29 C30 1.383(11) . ?
C30 C31 1.362(12) . ?
C31 C32 1.378(12) . ?
C32 C33 1.400(10) . ?
C34 C39 1.371(10) . ?
C34 C35 1.374(10) . ?
C35 C36 1.399(11) . ?
C36 C37 1.372(12) . ?
C37 C38 1.383(12) . ?
C37 C40 1.524(11) . ?
C38 C39 1.363(11) . ?
C41 C46 1.371(12) . ?
C41 C42 1.376(12) . ?
C42 C43 1.399(12) . ?
C43 C44 1.39(2) . ?
C44 C45 1.344(15) . ?
C45 C46 1.393(12) . ?
O1 C52 1.53(2) . ?
O1 C49 1.582(14) . ?
C49 C50 1.45(2) . ?
C50 C51 1.27(2) . ?
C51 C52 1.45(2) . ?
