#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:40:20 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179341 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/38/4323832.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4323832
loop_
_publ_author_name
'Younghun Byun'
'Dongwon Min'
'Junghwan Do'
'Hoseop Yun'
'Youngkyu Do'
_publ_section_title
;
 Mono- and Dinuclear d10 Metal Complexes of
 Hexakis(3,5-dimethylpyrazolyl)cyclotriphosphazene. Synthesis, Structures,
 and Unusual Solution Dynamic Behavior
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3981
_journal_page_last               3989
_journal_paper_doi               10.1021/ic950907b
_journal_volume                  35
_journal_year                    1996
_chemical_formula_sum            'C31 H44 Cd2 Cl6 N15 P3'
_chemical_formula_weight         1157.22
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                90.00
_cell_angle_beta                 102.71(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.585(5)
_cell_length_b                   17.585(4)
_cell_length_c                   14.404(3)
_cell_measurement_temperature    293(2)
_cell_volume                     4592.1(19)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoKa
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0550
_diffrn_reflns_av_sigmaI/netI    0.0229
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            4456
_diffrn_reflns_theta_max         20.00
_diffrn_reflns_theta_min         1.61
_exptl_absorpt_coefficient_mu    1.423
_exptl_crystal_density_diffrn    1.674
_exptl_crystal_F_000             2312
_refine_diff_density_max         1.043
_refine_diff_density_min         -.950
_refine_diff_density_rms         .095
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.055
_refine_ls_goodness_of_fit_obs   1.053
_refine_ls_matrix_type           full
_refine_ls_number_parameters     526
_refine_ls_number_reflns         4286
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.055
_refine_ls_restrained_S_obs      1.053
_refine_ls_R_factor_all          0.0421
_refine_ls_R_factor_obs          0.0365
_refine_ls_shift/esd_max         -0.003
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[s²(Fo²)+( 0.0528P)²+13.7294P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0950
_refine_ls_wR_factor_obs         0.0886
_reflns_number_observed          3814
_reflns_number_total             4286
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic950907b_3.cif
_cod_data_source_block           P3N3(3,5-Me2C3N2H)6(CdCl2)2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc w=1/[s^2^(Fo^2^)+(
0.0528P)^2^+13.7294P] where P=(Fo^2^+2Fc^2^)/3' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/[s^2^(Fo^2^)+( 0.0528P)^2^+13.7294P]
where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        4592.0(19)
_cod_database_code               4323832
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Cd1 Cd 0.12725(2) 0.33400(3) -0.35325(3) 0.0337(2) Uani 1 d . .
Cd2 Cd 0.07976(2) 0.19884(3) 0.10097(3) 0.0354(2) Uani 1 d . .
Cl1 Cl 0.02142(10) 0.29044(10) -0.47352(12) 0.0513(5) Uani 1 d . .
Cl2 Cl 0.22365(10) 0.38459(11) -0.42614(13) 0.0571(5) Uani 1 d . .
Cl3 Cl -0.01674(10) 0.21378(11) 0.18880(13) 0.0582(5) Uani 1 d . .
Cl4 Cl 0.16624(10) 0.09524(10) 0.15410(13) 0.0565(5) Uani 1 d . .
P1 P 0.09516(8) 0.24386(8) -0.13827(10) 0.0239(4) Uani 1 d . .
P2 P 0.05225(8) 0.39286(8) -0.15603(10) 0.0259(4) Uani 1 d . .
P3 P 0.15813(8) 0.34725(9) -0.00769(11) 0.0267(4) Uani 1 d . .
N1 N 0.0699(2) 0.3153(3) -0.2055(3) 0.0270(11) Uani 1 d . .
N2 N 0.1023(2) 0.4109(3) -0.0552(3) 0.0275(12) Uani 1 d . .
N3 N 0.1308(2) 0.2608(3) -0.0285(3) 0.0265(11) Uani 1 d . .
N11 N 0.1514(3) 0.1966(3) -0.1943(3) 0.0283(12) Uani 1 d . .
N12 N 0.1886(3) 0.2365(3) -0.2534(3) 0.0357(13) Uani 1 d . .
C13 C 0.2445(4) 0.1933(4) -0.2617(5) 0.046(2) Uani 1 d . .
C14 C 0.2447(4) 0.1253(4) -0.2102(5) 0.046(2) Uani 1 d . .
H14 H 0.2780(4) 0.0854(4) -0.2069(5) 0.055 Uiso 1 calc R .
C15 C 0.1879(4) 0.1287(4) -0.1668(4) 0.037(2) Uani 1 d . .
C16 C 0.2993(5) 0.2167(5) -0.3172(7) 0.089(3) Uani 1 d . .
H16A H 0.2760(10) 0.2494(32) -0.3684(30) 0.133 Uiso 1 calc R .
H16B H 0.3183(28) 0.1724(6) -0.3427(40) 0.133 Uiso 1 calc R .
H16C H 0.3391(19) 0.2435(33) -0.2764(14) 0.133 Uiso 1 calc R .
C17 C 0.1631(4) 0.0716(4) -0.1039(5) 0.056(2) Uani 1 d . .
H17D H 0.1629(24) 0.0945(9) -0.0435(12) 0.084 Uiso 1 calc R .
H17E H 0.1963(15) 0.0291(12) -0.0948(27) 0.084 Uiso 1 calc R .
H17F H 0.1143(11) 0.0546(19) -0.1330(15) 0.084 Uiso 1 calc R .
N21 N 0.0289(2) 0.1795(3) -0.1350(3) 0.0265(12) Uani 1 d . .
N22 N 0.0122(3) 0.1582(3) -0.0485(3) 0.0314(12) Uani 1 d . .
C23 C -0.0418(3) 0.1082(4) -0.0702(5) 0.039(2) Uani 1 d . .
C24 C -0.0598(4) 0.0961(4) -0.1690(5) 0.050(2) Uani 1 d . .
H24 H -0.0958(4) 0.0629(4) -0.2011(5) 0.060 Uiso 1 calc R .
C25 C -0.0158(3) 0.1409(4) -0.2097(4) 0.039(2) Uani 1 d . .
C26 C -0.0750(4) 0.0724(4) 0.0046(5) 0.060(2) Uani 1 d . .
H26A H -0.0389(9) 0.0704(25) 0.0635(10) 0.090 Uiso 1 calc R .
H26B H -0.0909(24) 0.0217(11) -0.0147(17) 0.090 Uiso 1 calc R .
H26C H -0.1165(17) 0.1020(16) 0.0130(25) 0.090 Uiso 1 calc R .
C27 C -0.0107(5) 0.1500(5) -0.3109(5) 0.066(2) Uani 1 d . .
H27D H -0.0161(28) 0.2027(6) -0.3283(12) 0.099 Uiso 1 calc R .
H27E H -0.0491(18) 0.1210(24) -0.3510(6) 0.099 Uiso 1 calc R .
H27F H 0.0365(12) 0.1321(27) -0.3186(9) 0.099 Uiso 1 calc R .
N51 N 0.1784(3) 0.3557(3) 0.1113(3) 0.0346(13) Uani 1 d . .
N52 N 0.1494(3) 0.3053(3) 0.1662(4) 0.0375(13) Uani 1 d . .
C53 C 0.1695(4) 0.3317(4) 0.2547(5) 0.046(2) Uani 1 d . .
C54 C 0.2112(4) 0.3988(4) 0.2567(5) 0.052(2) Uani 1 d . .
H54 H 0.2320(4) 0.4272(4) 0.3104(5) 0.062 Uiso 1 calc R .
C55 C 0.2155(3) 0.4142(4) 0.1659(5) 0.045(2) Uani 1 d . .
C56 C 0.1488(5) 0.2909(5) 0.3362(5) 0.077(3) Uani 1 d . .
H56A H 0.0960(5) 0.2880(30) 0.3259(21) 0.116 Uiso 1 calc R .
H56B H 0.1680(29) 0.3181(19) 0.3942(8) 0.116 Uiso 1 calc R .
H56C H 0.1690(28) 0.2405(13) 0.3409(27) 0.116 Uiso 1 calc R .
C57 C 0.2508(5) 0.4784(4) 0.1258(5) 0.074(3) Uani 1 d . .
H57D H 0.2159(10) 0.5005(20) 0.0736(26) 0.111 Uiso 1 calc R .
H57E H 0.2927(18) 0.4600(7) 0.1037(36) 0.111 Uiso 1 calc R .
H57F H 0.2665(28) 0.5161(15) 0.1742(12) 0.111 Uiso 1 calc R .
N61 N 0.2401(3) 0.3573(3) -0.0361(3) 0.0320(12) Uani 1 d . .
N62 N 0.2466(3) 0.4077(3) -0.1084(4) 0.0372(13) Uani 1 d . .
C63 C 0.3126(4) 0.3953(4) -0.1225(5) 0.044(2) Uani 1 d . .
C64 C 0.3495(4) 0.3372(4) -0.0622(5) 0.049(2) Uani 1 d . .
H64 H 0.3967(4) 0.3188(4) -0.0602(5) 0.059 Uiso 1 calc R .
C65 C 0.3033(4) 0.3138(4) -0.0086(5) 0.045(2) Uani 1 d . .
C66 C 0.3422(4) 0.4392(5) -0.1957(6) 0.074(3) Uani 1 d . .
H66A H 0.3018(4) 0.4588(27) -0.2430(23) 0.111 Uiso 1 calc R .
H66B H 0.3715(25) 0.4061(9) -0.2255(28) 0.111 Uiso 1 calc R .
H66C H 0.3721(25) 0.4805(19) -0.1654(9) 0.111 Uiso 1 calc R .
C67 C 0.3117(4) 0.2540(5) 0.0673(6) 0.081(3) Uani 1 d . .
H67D H 0.2726(20) 0.2175(19) 0.0505(21) 0.122 Uiso 1 calc R .
H67E H 0.3096(33) 0.2774(7) 0.1268(10) 0.122 Uiso 1 calc R .
H67F H 0.3583(16) 0.2289(24) 0.0730(31) 0.122 Uiso 1 calc R .
N31 N 0.0579(3) 0.4636(3) -0.2316(3) 0.0318(12) Uani 1 d . .
N32 N 0.0792(3) 0.4509(3) -0.3166(3) 0.0327(12) Uani 1 d . .
C33 C 0.0748(3) 0.5182(4) -0.3598(4) 0.036(2) Uani 1 d . .
C34 C 0.0519(3) 0.5739(4) -0.3030(5) 0.043(2) Uani 1 d . .
H34 H 0.0452(3) 0.6253(4) -0.3178(5) 0.052 Uiso 1 calc R .
C35 C 0.0413(4) 0.5397(3) -0.2228(5) 0.039(2) Uani 1 d . .
C36 C 0.0926(4) 0.5275(4) -0.4545(5) 0.056(2) Uani 1 d . .
H36A H 0.0863(24) 0.4797(7) -0.4876(14) 0.084 Uiso 1 calc R .
H36B H 0.1429(9) 0.5440(25) -0.4467(5) 0.084 Uiso 1 calc R .
H36C H 0.0604(17) 0.5647(19) -0.4907(13) 0.084 Uiso 1 calc R .
C37 C 0.0187(4) 0.5713(4) -0.1382(5) 0.060(2) Uani 1 d . .
H37D H 0.0568(12) 0.5619(24) -0.0824(7) 0.089 Uiso 1 calc R .
H37E H -0.0262(15) 0.5474(20) -0.1311(20) 0.089 Uiso 1 calc R .
H37F H 0.0110(26) 0.6251(6) -0.1461(16) 0.089 Uiso 1 calc R .
N41 N -0.0367(3) 0.3938(3) -0.1506(3) 0.0315(12) Uani 1 d . .
N42 N -0.0482(3) 0.3479(3) -0.0758(3) 0.0377(13) Uani 1 d . .
C43 C -0.1171(4) 0.3241(4) -0.1033(5) 0.043(2) Uani 1 d . .
C44 C -0.1502(4) 0.3530(4) -0.1947(5) 0.047(2) Uani 1 d . .
H44 H -0.1985(4) 0.3446(4) -0.2276(5) 0.057 Uiso 1 calc R .
C45 C -0.0997(3) 0.3944(4) -0.2249(4) 0.035(2) Uani 1 d . .
C46 C -0.1512(4) 0.2729(5) -0.0417(6) 0.073(3) Uani 1 d . .
H46A H -0.1165(12) 0.2638(27) 0.0172(17) 0.110 Uiso 1 calc R .
H46B H -0.1644(28) 0.2254(13) -0.0739(18) 0.110 Uiso 1 calc R .
H46C H -0.1946(18) 0.2966(15) -0.0291(33) 0.110 Uiso 1 calc R .
C47 C -0.1052(4) 0.4335(5) -0.3183(5) 0.058(2) Uani 1 d . .
H47D H -0.0920(25) 0.4861(7) -0.3075(5) 0.087 Uiso 1 calc R .
H47E H -0.1549(7) 0.4299(24) -0.3551(14) 0.087 Uiso 1 calc R .
H47F H -0.0723(19) 0.4097(17) -0.3523(15) 0.087 Uiso 1 calc R .
ClS1 Cl 0.1604(2) 0.1196(3) 0.5119(3) 0.173(2) Uani 1 d . .
ClS2 Cl 0.0452(3) 0.0383(3) 0.4037(7) 0.315(5) Uani 1 d . .
CS C 0.0817(7) 0.1150(6) 0.4216(10) 0.148(5) Uani 1 d . .
HS1 H 0.0459(7) 0.1506(6) 0.4363(10) 0.177 Uiso 1 calc R .
HS2 H 0.0942(7) 0.1320(6) 0.3631(10) 0.177 Uiso 1 calc R .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C .0033 .0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H .0000 .0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N .0061 .0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P .1023 .0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl .1484 .1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N32 Cd1 N12 130.9(2) . . ?
N32 Cd1 Cl2 97.43(13) . . ?
N12 Cd1 Cl2 103.03(13) . . ?
N32 Cd1 Cl1 98.48(12) . . ?
N12 Cd1 Cl1 114.19(13) . . ?
Cl2 Cd1 Cl1 111.29(7) . . ?
N32 Cd1 N1 71.5(2) . . ?
N12 Cd1 N1 68.9(2) . . ?
Cl2 Cd1 N1 150.61(11) . . ?
Cl1 Cd1 N1 97.45(11) . . ?
N52 Cd2 N22 138.0(2) . . ?
N52 Cd2 Cl3 96.35(13) . . ?
N22 Cd2 Cl3 101.75(13) . . ?
N52 Cd2 Cl4 101.68(13) . . ?
N22 Cd2 Cl4 104.03(13) . . ?
Cl3 Cd2 Cl4 115.42(7) . . ?
N52 Cd2 N3 71.8(2) . . ?
N22 Cd2 N3 70.5(2) . . ?
Cl3 Cd2 N3 141.40(11) . . ?
Cl4 Cd2 N3 103.05(11) . . ?
N1 P1 N3 117.1(2) . . ?
N1 P1 N11 103.3(2) . . ?
N3 P1 N11 113.7(2) . . ?
N1 P1 N21 115.4(2) . . ?
N3 P1 N21 104.2(2) . . ?
N11 P1 N21 102.6(2) . . ?
N1 P1 P3 85.2(2) . . ?
N3 P1 P3 33.2(2) . . ?
N11 P1 P3 116.8(2) . . ?
N21 P1 P3 130.1(2) . . ?
N2 P2 N1 116.3(2) . . ?
N2 P2 N31 110.0(2) . . ?
N1 P2 N31 107.1(2) . . ?
N2 P2 N41 110.1(2) . . ?
N1 P2 N41 109.2(2) . . ?
N31 P2 N41 103.2(2) . . ?
N2 P2 P3 31.4(2) . . ?
N1 P2 P3 85.1(2) . . ?
N31 P2 P3 126.9(2) . . ?
N41 P2 P3 121.6(2) . . ?
N2 P3 N3 116.0(2) . . ?
N2 P3 N61 111.5(2) . . ?
N3 P3 N61 108.7(2) . . ?
N2 P3 N51 111.0(3) . . ?
N3 P3 N51 105.4(3) . . ?
N61 P3 N51 103.3(2) . . ?
N2 P3 P2 31.4(2) . . ?
N3 P3 P2 89.3(2) . . ?
N61 P3 P2 108.7(2) . . ?
N51 P3 P2 138.2(2) . . ?
N2 P3 P1 91.9(2) . . ?
N3 P3 P1 33.0(2) . . ?
N61 P3 P1 100.4(2) . . ?
N51 P3 P1 137.6(2) . . ?
P2 P3 P1 61.09(6) . . ?
P1 N1 P2 117.5(3) . . ?
P1 N1 Cd1 118.6(2) . . ?
P2 N1 Cd1 114.6(2) . . ?
P2 N2 P3 117.2(3) . . ?
P1 N3 P3 113.9(3) . . ?
P1 N3 Cd2 120.6(2) . . ?
P3 N3 Cd2 115.2(2) . . ?
C15 N11 N12 109.3(4) . . ?
C15 N11 P1 127.4(4) . . ?
N12 N11 P1 119.2(4) . . ?
C13 N12 N11 105.8(5) . . ?
C13 N12 Cd1 130.5(4) . . ?
N11 N12 Cd1 119.9(3) . . ?
N12 C13 C14 110.7(6) . . ?
N12 C13 C16 122.6(6) . . ?
C14 C13 C16 126.7(6) . . ?
C15 C14 C13 107.3(6) . . ?
C14 C15 N11 106.9(5) . . ?
C14 C15 C17 129.3(6) . . ?
N11 C15 C17 123.8(5) . . ?
C25 N21 N22 110.3(4) . . ?
C25 N21 P1 128.9(4) . . ?
N22 N21 P1 120.8(4) . . ?
C23 N22 N21 105.9(5) . . ?
C23 N22 Cd2 130.1(4) . . ?
N21 N22 Cd2 123.7(3) . . ?
N22 C23 C24 109.9(5) . . ?
N22 C23 C26 121.6(6) . . ?
C24 C23 C26 128.5(6) . . ?
C25 C24 C23 108.5(6) . . ?
C24 C25 N21 105.4(5) . . ?
C24 C25 C27 131.2(6) . . ?
N21 C25 C27 123.4(6) . . ?
N52 N51 C55 111.2(5) . . ?
N52 N51 P3 120.1(4) . . ?
C55 N51 P3 128.2(5) . . ?
C53 N52 N51 105.3(5) . . ?
C53 N52 Cd2 132.4(5) . . ?
N51 N52 Cd2 122.3(4) . . ?
N52 C53 C54 110.4(6) . . ?
N52 C53 C56 121.2(7) . . ?
C54 C53 C56 128.4(7) . . ?
C55 C54 C53 107.2(6) . . ?
C54 C55 N51 105.9(6) . . ?
C54 C55 C57 130.7(6) . . ?
N51 C55 C57 123.4(6) . . ?
C65 N61 N62 110.9(5) . . ?
C65 N61 P3 129.3(4) . . ?
N62 N61 P3 119.0(4) . . ?
C63 N62 N61 104.5(5) . . ?
N62 C63 C64 111.6(6) . . ?
N62 C63 C66 121.7(6) . . ?
C64 C63 C66 126.7(7) . . ?
C65 C64 C63 106.9(6) . . ?
C64 C65 N61 106.1(6) . . ?
C64 C65 C67 131.1(6) . . ?
N61 C65 C67 122.8(6) . . ?
N32 N31 C35 110.4(5) . . ?
N32 N31 P2 121.8(4) . . ?
C35 N31 P2 127.8(4) . . ?
C33 N32 N31 105.6(5) . . ?
C33 N32 Cd1 131.4(4) . . ?
N31 N32 Cd1 122.5(3) . . ?
N32 C33 C34 110.2(5) . . ?
N32 C33 C36 121.6(6) . . ?
C34 C33 C36 128.2(6) . . ?
C35 C34 C33 107.9(6) . . ?
C34 C35 N31 105.9(5) . . ?
C34 C35 C37 131.0(6) . . ?
N31 C35 C37 123.1(6) . . ?
N42 N41 C45 110.4(4) . . ?
N42 N41 P2 110.5(4) . . ?
C45 N41 P2 129.3(4) . . ?
C43 N42 N41 104.8(5) . . ?
N42 C43 C44 111.0(6) . . ?
N42 C43 C46 121.4(6) . . ?
C44 C43 C46 127.6(7) . . ?
C45 C44 C43 107.8(6) . . ?
C44 C45 N41 106.0(5) . . ?
C44 C45 C47 129.1(6) . . ?
N41 C45 C47 124.8(6) . . ?
ClS2 CS ClS1 116.4(7) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cd1 N32 2.347(5) . ?
Cd1 N12 2.363(5) . ?
Cd1 Cl2 2.435(2) . ?
Cd1 Cl1 2.441(2) . ?
Cd1 N1 2.601(4) . ?
Cd2 N52 2.351(5) . ?
Cd2 N22 2.353(5) . ?
Cd2 Cl3 2.426(2) . ?
Cd2 Cl4 2.438(2) . ?
Cd2 N3 2.519(4) . ?
P1 N1 1.593(5) . ?
P1 N3 1.602(5) . ?
P1 N11 1.676(5) . ?
P1 N21 1.680(5) . ?
P1 P3 2.692(2) . ?
P2 N2 1.575(5) . ?
P2 N1 1.606(5) . ?
P2 N31 1.671(5) . ?
P2 N41 1.672(5) . ?
P2 P3 2.689(2) . ?
P3 N2 1.576(5) . ?
P3 N3 1.610(5) . ?
P3 N61 1.671(5) . ?
P3 N51 1.679(5) . ?
N11 C15 1.387(8) . ?
N11 N12 1.397(7) . ?
N12 C13 1.315(8) . ?
C13 C14 1.406(9) . ?
C13 C16 1.485(10) . ?
C14 C15 1.342(9) . ?
C15 C17 1.490(9) . ?
N21 C25 1.384(8) . ?
N21 N22 1.400(6) . ?
N22 C23 1.319(8) . ?
C23 C24 1.405(9) . ?
C23 C26 1.493(9) . ?
C24 C25 1.358(9) . ?
C25 C27 1.490(9) . ?
N51 N52 1.374(7) . ?
N51 C55 1.383(8) . ?
N52 C53 1.330(8) . ?
C53 C54 1.409(10) . ?
C53 C56 1.497(10) . ?
C54 C55 1.354(9) . ?
C55 C57 1.485(10) . ?
N61 C65 1.385(8) . ?
N61 N62 1.393(7) . ?
N62 C63 1.304(8) . ?
C63 C64 1.417(9) . ?
C63 C66 1.503(9) . ?
C64 C65 1.339(9) . ?
C65 C67 1.500(10) . ?
N31 N32 1.385(7) . ?
N31 C35 1.386(8) . ?
N32 C33 1.332(8) . ?
C33 C34 1.400(9) . ?
C33 C36 1.483(9) . ?
C34 C35 1.354(9) . ?
C35 C37 1.483(9) . ?
N41 N42 1.399(7) . ?
N41 C45 1.402(7) . ?
N42 C43 1.321(8) . ?
C43 C44 1.419(9) . ?
C43 C46 1.500(10) . ?
C44 C45 1.335(9) . ?
C45 C47 1.494(9) . ?
ClS1 CS 1.733(12) . ?
ClS2 CS 1.507(12) . ?
