#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:45:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179346 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/43/4324375.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4324375
loop_
_publ_author_name
'Pei-Pei Yang'
'Xi-Feng Gao'
'Hai-Bin Song'
'Sai Zhang'
'Xue-Lan Mei'
'Li-Cun Li'
'Dai-Zheng Liao'
_publ_section_title
;
 Slow Magnetic Relaxation in Novel Dy4 and Dy8 Compounds
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              720
_journal_page_last               722
_journal_paper_doi               10.1021/ic1021643
_journal_volume                  50
_journal_year                    2011
_chemical_formula_sum            'C146.18 H139.27 Dy8 N17.09 O83'
_chemical_formula_weight         4763.50
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.524(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   18.164(3)
_cell_length_b                   15.223(2)
_cell_length_c                   31.266(5)
_cell_measurement_reflns_used    29450
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      28.0
_cell_measurement_theta_min      1.5
_cell_volume                     8605(2)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean 14.63
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku Saturn CCD area detector'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  multilayer
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0389
_diffrn_reflns_av_sigmaI/netI    0.0396
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            57558
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         1.31
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.533
_exptl_absorpt_correction_T_max  0.6193
_exptl_absorpt_correction_T_min  0.5384
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   CrystalClear
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.838
_exptl_crystal_description       block
_exptl_crystal_F_000             4656
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.674
_refine_diff_density_min         -1.582
_refine_diff_density_rms         0.138
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.161
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1171
_refine_ls_number_reflns         15171
_refine_ls_number_restraints     221
_refine_ls_restrained_S_all      1.165
_refine_ls_R_factor_all          0.0417
_refine_ls_R_factor_gt           0.0393
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0243P)²+51.5007P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0885
_refine_ls_wR_factor_ref         0.0896
_reflns_number_gt                14518
_reflns_number_total             15171
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic1021643_si_002_2.cif
_cod_data_source_block           2
_cod_database_code               4324375
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.542311(15) 0.381104(17) 0.133808(8) 0.01515(7) Uani 1 1 d . A .
Dy2 Dy 0.644878(15) 0.176867(17) 0.098452(8) 0.01523(7) Uani 1 1 d . . .
Dy3 Dy 0.652172(15) 0.217990(17) 0.219682(8) 0.01431(7) Uani 1 1 d . . .
Dy4 Dy 0.683714(15) 0.109698(18) 0.327042(8) 0.01585(7) Uani 1 1 d . . .
N1 N 0.2856(6) 0.8419(8) 0.0984(6) 0.043(4) Uani 0.454(4) 1 d PD A 1
O10 O 0.2186(6) 0.8315(8) 0.0914(5) 0.065(2) Uani 0.454(4) 1 d PDU A 1
O11 O 0.3211(11) 0.9107(17) 0.0960(9) 0.056(4) Uani 0.454(4) 1 d PDU A 1
C19 C 0.4166(9) 0.6206(12) 0.1337(7) 0.0299(19) Uani 0.454(4) 1 d PGU A 1
C20 C 0.4503(6) 0.6991(15) 0.1239(9) 0.031(2) Uani 0.454(4) 1 d PGU A 1
H20A H 0.5026 0.7024 0.1247 0.037 Uiso 0.454(4) 1 calc PR A 1
C21 C 0.4073(8) 0.7727(12) 0.1128(6) 0.036(2) Uani 0.454(4) 1 d PGU A 1
H21A H 0.4303 0.8264 0.1061 0.043 Uiso 0.454(4) 1 calc PR A 1
C22 C 0.3307(8) 0.7679(7) 0.1117(4) 0.034(3) Uani 0.454(4) 1 d PGU A 1
C23 C 0.2971(6) 0.6894(8) 0.1215(4) 0.048(3) Uani 0.454(4) 1 d PGU A 1
H23A H 0.2448 0.6861 0.1208 0.058 Uiso 0.454(4) 1 calc PR A 1
C24 C 0.3400(9) 0.6158(7) 0.1326(5) 0.045(4) Uani 0.454(4) 1 d PGU A 1
H24A H 0.3171 0.5621 0.1393 0.054 Uiso 0.454(4) 1 calc PR A 1
N1' N 0.3055(7) 0.8555(8) 0.1294(5) 0.050(3) Uani 0.546(4) 1 d PD A 2
O10' O 0.2543(6) 0.8659(8) 0.1522(4) 0.065(2) Uani 0.546(4) 1 d PDU A 2
O11' O 0.3176(9) 0.9157(14) 0.1049(7) 0.056(4) Uani 0.546(4) 1 d PDU A 2
C19' C 0.4261(7) 0.6217(10) 0.1359(6) 0.0299(19) Uani 0.546(4) 1 d PG A 2
C20' C 0.4546(6) 0.6966(13) 0.1182(7) 0.031(2) Uani 0.546(4) 1 d PG A 2
H20B H 0.5014 0.6945 0.1069 0.037 Uiso 0.546(4) 1 calc PR A 2
C21' C 0.4148(7) 0.7747(10) 0.1169(5) 0.036(2) Uani 0.546(4) 1 d PG A 2
H21B H 0.4343 0.8259 0.1048 0.043 Uiso 0.546(4) 1 calc PR A 2
C22' C 0.3464(6) 0.7778(6) 0.1333(3) 0.034(3) Uani 0.546(4) 1 d PG A 2
C23' C 0.3178(6) 0.7029(7) 0.1510(4) 0.048(3) Uani 0.546(4) 1 d PG A 2
H23B H 0.2711 0.7050 0.1622 0.058 Uiso 0.546(4) 1 calc PR A 2
C24' C 0.3577(7) 0.6248(6) 0.1523(4) 0.045(4) Uani 0.546(4) 1 d PG A 2
H24B H 0.3382 0.5736 0.1644 0.054 Uiso 0.546(4) 1 calc PR A 2
N2 N 0.8522(3) 0.5891(4) -0.03590(18) 0.0308(13) Uani 1 1 d . . .
N3 N 0.6339(3) 0.7108(4) 0.35561(19) 0.0320(14) Uani 1 1 d . . .
N4 N 0.2728(4) 0.3994(5) 0.3400(2) 0.0446(17) Uani 1 1 d . . .
N5 N 0.5127(3) 0.3325(4) 0.5241(2) 0.0387(15) Uani 1 1 d U . .
N7 N 0.2208(9) -0.0013(10) 0.1866(7) 0.079(2) Uani 0.454(4) 1 d PDU A 1
O34 O 0.1642(8) 0.0380(10) 0.1930(5) 0.069(3) Uani 0.454(4) 1 d PDU A 1
O35 O 0.2308(8) -0.0804(10) 0.1828(5) 0.079(2) Uani 0.454(4) 1 d PDU A 1
C61 C 0.4140(8) 0.1560(10) 0.1840(7) 0.021(2) Uani 0.454(4) 1 d PGU A 1
C62 C 0.3441(9) 0.1939(7) 0.1788(7) 0.035(3) Uani 0.454(4) 1 d PGU A 1
H62A H 0.3390 0.2554 0.1743 0.042 Uiso 0.454(4) 1 calc PR A 1
C63 C 0.2815(7) 0.1417(8) 0.1801(5) 0.038(3) Uani 0.454(4) 1 d PGU A 1
H63A H 0.2337 0.1676 0.1765 0.046 Uiso 0.454(4) 1 calc PR A 1
C64 C 0.2888(6) 0.0517(8) 0.1866(5) 0.040(3) Uani 0.454(4) 1 d PGU A 1
C65 C 0.3588(7) 0.0138(7) 0.1918(4) 0.039(3) Uani 0.454(4) 1 d PGU A 1
H65A H 0.3638 -0.0477 0.1962 0.046 Uiso 0.454(4) 1 calc PR A 1
C66 C 0.4213(5) 0.0660(10) 0.1905(6) 0.031(3) Uani 0.454(4) 1 d PGU A 1
H66A H 0.4691 0.0401 0.1941 0.037 Uiso 0.454(4) 1 calc PR A 1
N7' N 0.1996(8) 0.0487(9) 0.2036(6) 0.079(2) Uani 0.546(4) 1 d PDU A 2
O34' O 0.1454(7) 0.0982(8) 0.2010(4) 0.069(3) Uani 0.546(4) 1 d PDU A 2
O35' O 0.2013(7) -0.0279(8) 0.2167(4) 0.079(2) Uani 0.546(4) 1 d PDU A 2
C61' C 0.4077(6) 0.1682(8) 0.1898(6) 0.021(2) Uani 0.546(4) 1 d PG A 2
C62' C 0.3435(8) 0.2183(6) 0.1851(5) 0.035(3) Uani 0.546(4) 1 d PG A 2
H62B H 0.3461 0.2793 0.1790 0.042 Uiso 0.546(4) 1 calc PR A 2
C63' C 0.2754(6) 0.1793(6) 0.1894(4) 0.038(3) Uani 0.546(4) 1 d PG A 2
H63B H 0.2315 0.2136 0.1863 0.046 Uiso 0.546(4) 1 calc PR A 2
C64' C 0.2716(4) 0.0901(7) 0.1984(4) 0.040(3) Uani 0.546(4) 1 d PG A 2
C65' C 0.3358(6) 0.0399(5) 0.2031(3) 0.039(3) Uani 0.546(4) 1 d PG A 2
H65B H 0.3332 -0.0211 0.2092 0.046 Uiso 0.546(4) 1 calc PR A 2
C66' C 0.4039(5) 0.0789(8) 0.1987(5) 0.031(3) Uani 0.546(4) 1 d PG A 2
H66B H 0.4477 0.0447 0.2019 0.037 Uiso 0.546(4) 1 calc PR A 2
N8 N 0.3500(7) 0.5882(8) 0.3499(6) 0.164(7) Uani 1 1 d . . .
O36 O 0.6438(2) 0.2862(3) 0.15186(12) 0.0182(4) Uani 1 1 d . . .
H36A H 0.6897 0.3219 0.1506 0.022 Uiso 1 1 calc R . .
O1 O 0.4356(2) 0.3694(3) 0.07634(13) 0.0233(9) Uani 1 1 d . . .
O2 O 0.5305(2) 0.2456(3) 0.09478(12) 0.0182(4) Uani 1 1 d . . .
O3 O 0.5561(2) 0.0623(3) 0.10063(13) 0.0215(9) Uani 1 1 d . . .
O4 O 0.9198(2) 0.0089(3) 0.19048(13) 0.0236(10) Uani 1 1 d . . .
O5 O 0.8437(2) 0.0853(3) 0.24557(12) 0.0180(9) Uani 1 1 d . . .
O6 O 0.8179(2) 0.1032(3) 0.33484(12) 0.0182(4) Uani 1 1 d . . .
O7 O 0.7543(2) -0.0182(2) 0.31262(13) 0.0205(9) Uani 1 1 d . . .
O8 O 0.5229(2) 0.5330(3) 0.11657(13) 0.0212(9) Uani 1 1 d . A .
O9 O 0.4415(2) 0.4711(3) 0.15681(12) 0.0182(4) Uani 1 1 d . A .
O12 O 0.6227(2) 0.4210(3) 0.08438(13) 0.0199(9) Uani 1 1 d . . .
O13 O 0.6708(2) 0.3000(3) 0.05775(12) 0.0196(9) Uani 1 1 d . . .
O14 O 0.8917(3) 0.5496(4) -0.05922(16) 0.0411(13) Uani 1 1 d . . .
O15 O 0.8518(3) 0.6698(3) -0.03106(16) 0.0374(12) Uani 1 1 d . . .
O16 O 0.5953(3) 0.4529(3) 0.19294(14) 0.0297(11) Uani 1 1 d . . .
O17 O 0.6637(3) 0.3680(3) 0.23896(13) 0.0266(10) Uani 1 1 d . . .
O18 O 0.6811(3) 0.7069(4) 0.38592(18) 0.0505(15) Uani 1 1 d . . .
O19 O 0.5887(3) 0.7695(3) 0.34993(17) 0.0483(14) Uani 1 1 d . . .
O20 O 0.5611(2) 0.2465(3) 0.26535(13) 0.0263(10) Uani 1 1 d . . .
O21 O 0.5801(2) 0.1949(3) 0.33271(13) 0.0206(9) Uani 1 1 d . . .
O22 O 0.2560(3) 0.3971(4) 0.37702(18) 0.0520(15) Uani 1 1 d . . .
O23 O 0.2346(3) 0.4337(5) 0.31031(19) 0.0630(18) Uani 1 1 d . . .
O24 O 0.7252(2) 0.2079(3) 0.38364(12) 0.0182(4) Uani 1 1 d . . .
O25 O 0.7103(2) 0.3489(3) 0.36460(13) 0.0235(9) Uani 1 1 d . . .
O26 O 0.4851(3) 0.4027(3) 0.52912(17) 0.0421(13) Uani 1 1 d . B .
O28 O 0.6859(2) 0.0255(3) 0.38850(13) 0.0222(9) Uani 1 1 d U . .
O29 O 0.7886(2) 0.0622(3) 0.42971(13) 0.0211(9) Uani 1 1 d . . .
O32 O 0.4784(2) 0.2915(3) 0.17581(13) 0.0211(9) Uani 1 1 d . A .
O33 O 0.5395(2) 0.1654(3) 0.18620(13) 0.0215(9) Uani 1 1 d . A .
O41 O 0.5943(3) 0.1561(3) 0.02505(13) 0.0281(10) Uani 1 1 d . . .
H41 H 0.5667 0.1957 0.0122 0.042 Uiso 1 1 d R . .
O40 O 0.5025(3) 0.2731(4) 0.98663(19) 0.0519(15) Uani 1 1 d . . .
H40 H 0.4657 0.2599 0.9695 0.078 Uiso 1 1 calc R . .
O38 O 0.3980(6) 0.2161(7) 0.9257(3) 0.053(3) Uani 0.60 1 d P . .
O39 O 0.6429(3) 0.6399(3) 0.12128(16) 0.0371(12) Uani 1 1 d . . .
H39 H 0.6040 0.6098 0.1178 0.056 Uiso 1 1 calc R . .
O37 O 0.7214(2) 0.2269(3) 0.28891(12) 0.0182(4) Uani 1 1 d . . .
H37B H 0.7102 0.2831 0.3035 0.022 Uiso 1 1 calc R . .
C1 C 0.3875(4) 0.4374(4) 0.0584(2) 0.0305(15) Uani 1 1 d . . .
H1A H 0.3513 0.4122 0.0365 0.046 Uiso 1 1 calc R . .
H1B H 0.4167 0.4823 0.0452 0.046 Uiso 1 1 calc R . .
H1C H 0.3615 0.4642 0.0812 0.046 Uiso 1 1 calc R . .
C2 C 0.4078(3) 0.2845(4) 0.07286(19) 0.0217(13) Uani 1 1 d . . .
C3 C 0.3350(4) 0.2638(4) 0.0615(2) 0.0294(15) Uani 1 1 d . . .
H3A H 0.3000 0.3090 0.0543 0.035 Uiso 1 1 calc R . .
C4 C 0.3125(4) 0.1761(5) 0.0606(2) 0.0369(17) Uani 1 1 d . . .
H4A H 0.2622 0.1616 0.0527 0.044 Uiso 1 1 calc R . .
C5 C 0.3635(4) 0.1107(4) 0.0710(2) 0.0292(15) Uani 1 1 d . . .
H5A H 0.3478 0.0511 0.0709 0.035 Uiso 1 1 calc R . .
C6 C 0.4388(3) 0.1311(4) 0.08181(19) 0.0228(13) Uani 1 1 d . . .
C7 C 0.4623(3) 0.2197(4) 0.08285(18) 0.0182(12) Uani 1 1 d . . .
C8 C 0.4875(4) 0.0599(4) 0.09375(19) 0.0235(14) Uani 1 1 d . . .
H8A H 0.4699 0.0350 0.1202 0.028 Uiso 1 1 calc R . .
H8B H 0.4769 0.0148 0.0711 0.028 Uiso 1 1 calc R . .
C9 C 0.9766(4) -0.0100(4) 0.16217(19) 0.0263(14) Uani 1 1 d . . .
H9A H 0.9641 0.0187 0.1344 0.039 Uiso 1 1 calc R . .
H9B H 0.9798 -0.0737 0.1579 0.039 Uiso 1 1 calc R . .
H9C H 1.0244 0.0120 0.1751 0.039 Uiso 1 1 calc R . .
C10 C 0.9282(3) -0.0266(4) 0.23167(18) 0.0206(13) Uani 1 1 d . . .
C11 C 0.9733(4) -0.0965(4) 0.2443(2) 0.0259(14) Uani 1 1 d . . .
H11A H 1.0032 -0.1232 0.2246 0.031 Uiso 1 1 calc R . .
C12 C 0.9745(4) -0.1275(4) 0.2860(2) 0.0295(15) Uani 1 1 d . . .
H12A H 1.0059 -0.1751 0.2953 0.035 Uiso 1 1 calc R . .
C13 C 0.9297(4) -0.0889(4) 0.31424(19) 0.0243(14) Uani 1 1 d . . .
H13A H 0.9304 -0.1106 0.3428 0.029 Uiso 1 1 calc R . .
C14 C 0.8833(3) -0.0185(4) 0.30116(18) 0.0189(13) Uani 1 1 d . . .
C15 C 0.8835(3) 0.0150(4) 0.25957(18) 0.0181(12) Uani 1 1 d . . .
C16 C 0.8271(3) 0.0127(4) 0.33048(18) 0.0192(13) Uani 1 1 d . . .
H16A H 0.8390 -0.0138 0.3596 0.023 Uiso 1 1 calc R . .
C17 C 0.7420(4) -0.1103(4) 0.3165(2) 0.0320(16) Uani 1 1 d . . .
H17A H 0.7844 -0.1426 0.3073 0.048 Uiso 1 1 calc R . .
H17B H 0.6972 -0.1269 0.2983 0.048 Uiso 1 1 calc R . .
H17C H 0.7359 -0.1247 0.3465 0.048 Uiso 1 1 calc R . .
C18 C 0.4645(4) 0.5372(4) 0.1371(2) 0.0278(15) Uani 1 1 d . . .
C25 C 0.6648(3) 0.3809(4) 0.06081(18) 0.0182(13) Uani 1 1 d . . .
C26 C 0.7123(3) 0.4374(4) 0.03437(18) 0.0167(12) Uani 1 1 d . . .
C27 C 0.7395(3) 0.4023(4) -0.00205(19) 0.0231(13) Uani 1 1 d . . .
H27A H 0.7267 0.3441 -0.0109 0.028 Uiso 1 1 calc R . .
C28 C 0.7851(3) 0.4522(5) -0.0255(2) 0.0256(14) Uani 1 1 d . . .
H28A H 0.8042 0.4288 -0.0503 0.031 Uiso 1 1 calc R . .
C29 C 0.8020(3) 0.5361(4) -0.0119(2) 0.0238(14) Uani 1 1 d . . .
C30 C 0.7751(3) 0.5736(4) 0.0243(2) 0.0233(14) Uani 1 1 d . . .
H30A H 0.7883 0.6318 0.0330 0.028 Uiso 1 1 calc R . .
C31 C 0.7286(3) 0.5234(4) 0.04716(19) 0.0205(13) Uani 1 1 d . . .
H31A H 0.7080 0.5476 0.0714 0.025 Uiso 1 1 calc R . .
C32 C 0.6295(3) 0.4372(4) 0.22879(18) 0.0179(12) Uani 1 1 d . . .
C33 C 0.6309(3) 0.5087(4) 0.26228(19) 0.0218(13) Uani 1 1 d . . .
C34 C 0.6789(4) 0.5036(4) 0.29942(19) 0.0227(13) Uani 1 1 d . . .
H34A H 0.7111 0.4547 0.3041 0.027 Uiso 1 1 calc R . .
C35 C 0.6798(4) 0.5701(4) 0.3298(2) 0.0273(15) Uani 1 1 d . . .
H35A H 0.7128 0.5670 0.3553 0.033 Uiso 1 1 calc R . .
C36 C 0.6328(4) 0.6404(4) 0.32286(19) 0.0240(14) Uani 1 1 d . . .
C37 C 0.5829(4) 0.6461(4) 0.2867(2) 0.0294(15) Uani 1 1 d . . .
H37A H 0.5496 0.6942 0.2827 0.035 Uiso 1 1 calc R . .
C38 C 0.5828(4) 0.5800(4) 0.2564(2) 0.0291(15) Uani 1 1 d . . .
H38A H 0.5493 0.5831 0.2312 0.035 Uiso 1 1 calc R . .
C39 C 0.5439(3) 0.2380(4) 0.30325(19) 0.0197(13) Uani 1 1 d . . .
C40 C 0.4728(3) 0.2813(4) 0.31322(19) 0.0223(13) Uani 1 1 d . . .
C41 C 0.4476(4) 0.2704(4) 0.3534(2) 0.0244(14) Uani 1 1 d . . .
H41A H 0.4757 0.2368 0.3747 0.029 Uiso 1 1 calc R . .
C42 C 0.3817(4) 0.3084(5) 0.3624(2) 0.0314(16) Uani 1 1 d . . .
H42A H 0.3638 0.3013 0.3898 0.038 Uiso 1 1 calc R . .
C43 C 0.3429(4) 0.3568(5) 0.3307(2) 0.0339(17) Uani 1 1 d . . .
C44 C 0.3660(4) 0.3683(5) 0.2903(2) 0.0392(18) Uani 1 1 d . . .
H44A H 0.3373 0.4013 0.2689 0.047 Uiso 1 1 calc R . .
C45 C 0.4324(4) 0.3304(5) 0.2816(2) 0.0312(16) Uani 1 1 d . . .
H45A H 0.4501 0.3378 0.2542 0.037 Uiso 1 1 calc R . .
C46 C 0.6961(3) 0.2862(4) 0.38701(18) 0.0190(13) Uani 1 1 d . . .
C47 C 0.6458(3) 0.2971(4) 0.42217(19) 0.0216(13) Uani 1 1 d . . .
C48 C 0.6388(5) 0.2305(5) 0.4515(3) 0.046(2) Uani 1 1 d . B .
H48A H 0.6647 0.1769 0.4489 0.055 Uiso 1 1 calc R . .
C49 C 0.5948(5) 0.2413(5) 0.4844(3) 0.059(3) Uani 1 1 d . . .
H49A H 0.5894 0.1953 0.5044 0.070 Uiso 1 1 calc R B .
C50 C 0.5588(4) 0.3200(4) 0.4880(2) 0.0299(16) Uani 1 1 d . B .
C51 C 0.5637(3) 0.3874(4) 0.4596(2) 0.0266(15) Uani 1 1 d . . .
H51A H 0.5376 0.4408 0.4625 0.032 Uiso 1 1 calc R B .
C52 C 0.6084(4) 0.3755(4) 0.4262(2) 0.0257(14) Uani 1 1 d . B .
H52A H 0.6131 0.4214 0.4060 0.031 Uiso 1 1 calc R . .
C53 C 0.7245(4) 0.0297(4) 0.42393(18) 0.0206(13) Uani 1 1 d . . .
C54 C 0.6902(3) -0.0053(4) 0.46263(19) 0.0228(14) Uani 1 1 d . . .
C60 C 0.4811(3) 0.2093(4) 0.18279(18) 0.0189(13) Uani 1 1 d . . .
C67 C 0.4086(8) 0.5594(7) 0.3567(4) 0.083(4) Uani 1 1 d . . .
C68 C 0.4802(5) 0.5251(6) 0.3646(3) 0.058(2) Uani 1 1 d . . .
H68A H 0.5029 0.5205 0.3375 0.087 Uiso 1 1 calc R . .
H68B H 0.4777 0.4667 0.3776 0.087 Uiso 1 1 calc R . .
H68C H 0.5100 0.5641 0.3843 0.087 Uiso 1 1 calc R . .
C74 C 0.5793(4) 0.0819(5) -0.0016(2) 0.0354(17) Uani 1 1 d . . .
H74A H 0.5580 0.1011 -0.0301 0.053 Uiso 1 1 calc R . .
H74B H 0.5441 0.0434 0.0112 0.053 Uiso 1 1 calc R . .
H74C H 0.6253 0.0498 -0.0044 0.053 Uiso 1 1 calc R . .
C73 C 0.5176(4) 0.3626(5) 0.9831(2) 0.0381(18) Uani 1 1 d . . .
H73A H 0.5224 0.3893 1.0117 0.057 Uiso 1 1 calc R . .
H73B H 0.4771 0.3910 0.9652 0.057 Uiso 1 1 calc R . .
H73C H 0.5638 0.3703 0.9698 0.057 Uiso 1 1 calc R . .
O38' O 0.3629(8) 0.2580(11) 0.9508(6) 0.062(5) Uani 0.40 1 d P . .
C72 C 0.6533(4) 0.6709(5) 0.1647(2) 0.0429(19) Uani 1 1 d . . .
H72A H 0.6965 0.7096 0.1681 0.064 Uiso 1 1 calc R . .
H72B H 0.6611 0.6208 0.1843 0.064 Uiso 1 1 calc R . .
H72C H 0.6093 0.7036 0.1713 0.064 Uiso 1 1 calc R . .
C71 C 0.3356(6) 0.1723(6) 0.9437(3) 0.067(3) Uani 1 1 d . . .
C70 C 0.0935(8) 0.8012(11) 0.1328(5) 0.054(4) Uani 0.546(4) 1 d PDU A 2
H70A H 0.1186 0.7874 0.1612 0.081 Uiso 0.546(4) 1 calc PR A 2
H70B H 0.0466 0.7691 0.1288 0.081 Uiso 0.546(4) 1 calc PR A 2
H70C H 0.0838 0.8645 0.1308 0.081 Uiso 0.546(4) 1 calc PR A 2
C69 C 0.1399(10) 0.7756(12) 0.0999(5) 0.070(5) Uani 0.546(4) 1 d PD A 2
N9 N 0.1792(9) 0.7519(12) 0.0731(5) 0.081(5) Uani 0.546(4) 1 d PD A 2
O27 O 0.4929(13) 0.2643(9) 0.5414(7) 0.038(5) Uani 0.58(6) 1 d PU B 1
O27' O 0.522(2) 0.2792(16) 0.5562(11) 0.052(7) Uani 0.42(6) 1 d PU B 2
O1W O 0.5957(8) 0.2848(10) 0.7479(5) 0.084(5) Uani 0.50 1 d P . .
O30 O 0.5145(7) -0.1060(13) 0.5616(6) 0.067(4) Uani 0.480(17) 1 d PDU C 1
O31 O 0.6159(8) -0.0884(15) 0.6049(4) 0.068(3) Uani 0.480(17) 1 d PDU C 1
O30' O 0.5312(8) -0.1373(10) 0.5639(5) 0.067(4) Uani 0.520(17) 1 d PDU C 2
O31' O 0.5997(9) -0.0410(12) 0.6033(4) 0.068(3) Uani 0.520(17) 1 d PDU C 2
N6 N 0.5797(4) -0.0808(6) 0.5693(2) 0.072(2) Uani 1 1 d DU . .
C55 C 0.7138(4) 0.0261(5) 0.5029(2) 0.0287(15) Uani 1 1 d . C .
H55A H 0.7546 0.0654 0.5066 0.034 Uiso 1 1 calc R . .
C56 C 0.6779(4) 0.0001(6) 0.5381(2) 0.045(2) Uani 1 1 d . . .
H56A H 0.6938 0.0212 0.5661 0.054 Uiso 1 1 calc R C .
C57 C 0.6196(4) -0.0559(7) 0.5319(2) 0.050(2) Uani 1 1 d . C .
C58 C 0.5960(5) -0.0908(6) 0.4921(3) 0.052(2) Uani 1 1 d . . .
H58A H 0.5562 -0.1315 0.4888 0.063 Uiso 1 1 calc R C .
C59 C 0.6321(4) -0.0643(5) 0.4569(2) 0.0381(18) Uani 1 1 d . C .
H59A H 0.6170 -0.0867 0.4290 0.046 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O16 Dy1 O32 91.04(16) . .
O16 Dy1 O12 99.91(16) . .
O32 Dy1 O12 158.57(14) . .
O16 Dy1 O36 80.85(15) . .
O32 Dy1 O36 85.72(14) . .
O12 Dy1 O36 78.00(14) . .
O16 Dy1 O8 76.16(15) . .
O32 Dy1 O8 129.37(14) . .
O12 Dy1 O8 71.56(14) . .
O36 Dy1 O8 137.56(14) . .
O16 Dy1 O2 146.73(15) . .
O32 Dy1 O2 75.73(14) . .
O12 Dy1 O2 85.22(14) . .
O36 Dy1 O2 68.00(13) . .
O8 Dy1 O2 135.50(14) . .
O16 Dy1 O9 76.30(15) . .
O32 Dy1 O9 74.31(14) . .
O12 Dy1 O9 126.07(13) . .
O36 Dy1 O9 149.12(13) . .
O8 Dy1 O9 55.11(13) . .
O2 Dy1 O9 126.73(13) . .
O16 Dy1 O1 148.02(15) . .
O32 Dy1 O1 88.24(14) . .
O12 Dy1 O1 91.94(14) . .
O36 Dy1 O1 130.90(14) . .
O8 Dy1 O1 79.71(14) . .
O2 Dy1 O1 63.30(13) . .
O9 Dy1 O1 72.74(14) . .
O16 Dy1 C18 74.66(18) . .
O32 Dy1 C18 101.61(17) . .
O12 Dy1 C18 99.05(17) . .
O36 Dy1 C18 154.48(17) . .
O8 Dy1 C18 27.80(16) . .
O2 Dy1 C18 137.42(17) . .
O9 Dy1 C18 27.31(16) . .
O1 Dy1 C18 74.19(17) . .
O16 Dy1 Dy2 116.29(11) . .
O32 Dy1 Dy2 88.26(10) . .
O12 Dy1 Dy2 70.39(10) . .
O36 Dy1 Dy2 35.56(9) . .
O8 Dy1 Dy2 141.47(9) . .
O2 Dy1 Dy2 34.78(9) . .
O9 Dy1 Dy2 159.07(9) . .
O1 Dy1 Dy2 95.65(10) . .
C18 Dy1 Dy2 165.43(13) . .
O2 Dy2 O13 80.65(14) . .
O2 Dy2 O29 144.08(14) . 2_655
O13 Dy2 O29 104.75(14) . 2_655
O2 Dy2 O36 69.39(14) . .
O13 Dy2 O36 80.54(14) . .
O29 Dy2 O36 146.25(14) 2_655 .
O2 Dy2 O3 74.11(14) . .
O13 Dy2 O3 140.82(14) . .
O29 Dy2 O3 80.80(14) 2_655 .
O36 Dy2 O3 116.40(13) . .
O2 Dy2 O6 115.40(13) . 2_655
O13 Dy2 O6 142.22(14) . 2_655
O29 Dy2 O6 82.31(14) 2_655 2_655
O36 Dy2 O6 74.70(13) . 2_655
O3 Dy2 O6 76.61(14) . 2_655
O2 Dy2 O41 75.77(14) . .
O13 Dy2 O41 70.45(15) . .
O29 Dy2 O41 73.01(15) 2_655 .
O36 Dy2 O41 137.59(14) . .
O3 Dy2 O41 74.56(15) . .
O6 Dy2 O41 144.47(14) 2_655 .
O2 Dy2 O24 140.60(13) . 2_655
O13 Dy2 O24 74.13(14) . 2_655
O29 Dy2 O24 72.85(14) 2_655 2_655
O36 Dy2 O24 76.89(13) . 2_655
O3 Dy2 O24 141.69(14) . 2_655
O6 Dy2 O24 72.77(13) 2_655 2_655
O41 Dy2 O24 121.36(14) . 2_655
O2 Dy2 Dy3 85.46(9) . .
O13 Dy2 Dy3 114.69(10) . .
O29 Dy2 Dy3 121.57(10) 2_655 .
O36 Dy2 Dy3 35.53(9) . .
O3 Dy2 Dy3 92.89(10) . .
O6 Dy2 Dy3 40.44(9) 2_655 .
O41 Dy2 Dy3 159.61(11) . .
O24 Dy2 Dy3 78.41(9) 2_655 .
O2 Dy2 Dy1 36.10(10) . .
O13 Dy2 Dy1 68.68(10) . .
O29 Dy2 Dy1 173.38(10) 2_655 .
O36 Dy2 Dy1 35.70(10) . .
O3 Dy2 Dy1 103.66(10) . .
O6 Dy2 Dy1 103.38(9) 2_655 .
O41 Dy2 Dy1 103.24(11) . .
O24 Dy2 Dy1 105.36(9) 2_655 .
Dy3 Dy2 Dy1 63.551(7) . .
O2 Dy2 Dy4 145.05(10) . 2_655
O13 Dy2 Dy4 110.44(10) . 2_655
O29 Dy2 Dy4 67.19(10) 2_655 2_655
O36 Dy2 Dy4 79.64(10) . 2_655
O3 Dy2 Dy4 107.40(10) . 2_655
O6 Dy2 Dy4 37.54(9) 2_655 2_655
O41 Dy2 Dy4 139.03(11) . 2_655
O24 Dy2 Dy4 36.51(9) 2_655 2_655
Dy3 Dy2 Dy4 59.665(9) . 2_655
Dy1 Dy2 Dy4 115.338(11) . 2_655
O5 Dy3 O20 82.34(15) 2_655 .
O5 Dy3 O37 96.73(14) 2_655 2_655
O20 Dy3 O37 145.33(15) . 2_655
O5 Dy3 O33 84.16(14) 2_655 .
O20 Dy3 O33 72.33(15) . .
O37 Dy3 O33 142.27(13) 2_655 .
O5 Dy3 O36 144.35(13) 2_655 .
O20 Dy3 O36 118.82(14) . .
O37 Dy3 O36 81.40(14) 2_655 .
O33 Dy3 O36 76.73(14) . .
O5 Dy3 O17 137.05(14) 2_655 .
O20 Dy3 O17 73.42(16) . .
O37 Dy3 O17 84.81(15) 2_655 .
O33 Dy3 O17 119.67(15) . .
O36 Dy3 O17 78.48(14) . .
O5 Dy3 O37 68.38(14) 2_655 .
O20 Dy3 O37 77.19(14) . .
O37 Dy3 O37 70.47(15) 2_655 .
O33 Dy3 O37 141.24(13) . .
O36 Dy3 O37 140.43(14) . .
O17 Dy3 O37 71.94(14) . .
O5 Dy3 O6 73.26(13) 2_655 2_655
O20 Dy3 O6 138.74(15) . 2_655
O37 Dy3 O6 71.73(13) 2_655 2_655
O33 Dy3 O6 72.52(13) . 2_655
O36 Dy3 O6 72.41(13) . 2_655
O17 Dy3 O6 144.75(14) . 2_655
O37 Dy3 O6 121.14(13) . 2_655
O5 Dy3 Dy4 35.84(9) 2_655 .
O20 Dy3 Dy4 65.65(11) . .
O37 Dy3 Dy4 93.51(10) 2_655 .
O33 Dy3 Dy4 107.57(10) . .
O36 Dy3 Dy4 174.91(10) . .
O17 Dy3 Dy4 101.24(10) . .
O37 Dy3 Dy4 36.14(9) . .
O6 Dy3 Dy4 106.01(9) 2_655 .
O5 Dy3 Dy4 79.01(10) 2_655 2_655
O20 Dy3 Dy4 160.47(11) . 2_655
O37 Dy3 Dy4 33.95(10) 2_655 2_655
O33 Dy3 Dy4 111.18(10) . 2_655
O36 Dy3 Dy4 80.27(9) . 2_655
O17 Dy3 Dy4 117.44(11) . 2_655
O37 Dy3 Dy4 90.50(9) . 2_655
O6 Dy3 Dy4 38.70(9) 2_655 2_655
Dy4 Dy3 Dy4 95.478(11) . 2_655
O5 Dy3 Dy2 108.75(9) 2_655 .
O20 Dy3 Dy2 132.70(11) . .
O37 Dy3 Dy2 80.61(9) 2_655 .
O33 Dy3 Dy2 63.74(10) . .
O36 Dy3 Dy2 35.64(9) . .
O17 Dy3 Dy2 113.80(10) . .
O37 Dy3 Dy2 150.06(9) . .
O6 Dy3 Dy2 37.98(9) 2_655 .
Dy4 Dy3 Dy2 143.600(12) . .
Dy4 Dy3 Dy2 60.319(8) 2_655 .
O5 Dy3 Dy3 77.32(10) 2_655 2_655
O20 Dy3 Dy3 111.94(11) . 2_655
O37 Dy3 Dy3 35.94(9) 2_655 2_655
O33 Dy3 Dy3 160.03(10) . 2_655
O36 Dy3 Dy3 114.78(10) . 2_655
O17 Dy3 Dy3 79.63(11) . 2_655
O37 Dy3 Dy3 34.92(9) . 2_655
O6 Dy3 Dy3 94.77(9) 2_655 2_655
Dy4 Dy3 Dy3 60.302(8) . 2_655
Dy4 Dy3 Dy3 58.168(12) 2_655 2_655
Dy2 Dy3 Dy3 115.343(12) . 2_655
O37 Dy4 O21 83.61(14) . .
O37 Dy4 O5 70.09(14) . 2_655
O21 Dy4 O5 93.78(14) . 2_655
O37 Dy4 O28 152.35(15) . .
O21 Dy4 O28 101.37(14) . .
O5 Dy4 O28 135.64(14) 2_655 .
O37 Dy4 O24 78.97(14) . .
O21 Dy4 O24 78.01(14) . .
O5 Dy4 O24 148.73(13) 2_655 .
O28 Dy4 O24 75.60(14) . .
O37 Dy4 O7 110.04(13) . .
O21 Dy4 O7 157.87(14) . .
O5 Dy4 O7 75.69(14) 2_655 .
O28 Dy4 O7 74.87(14) . .
O24 Dy4 O7 120.80(14) . .
O37 Dy4 O6 74.70(13) . .
O21 Dy4 O6 146.48(14) . .
O5 Dy4 O6 102.21(13) 2_655 .
O28 Dy4 O6 87.56(14) . .
O24 Dy4 O6 73.02(13) . .
O7 Dy4 O6 55.65(13) . .
O37 Dy4 O4 129.37(14) . 2_655
O21 Dy4 O4 75.82(14) . 2_655
O5 Dy4 O4 65.83(13) 2_655 2_655
O28 Dy4 O4 77.83(14) . 2_655
O24 Dy4 O4 137.81(13) . 2_655
O7 Dy4 O4 82.09(14) . 2_655
O6 Dy4 O4 137.65(14) . 2_655
O37 Dy4 C16 95.76(15) . .
O21 Dy4 C16 172.02(15) . .
O5 Dy4 C16 93.47(15) 2_655 .
O28 Dy4 C16 75.56(15) . .
O24 Dy4 C16 94.05(14) . .
O7 Dy4 C16 28.97(14) . .
O6 Dy4 C16 27.47(14) . .
O4 Dy4 C16 110.29(15) 2_655 .
O37 Dy4 Dy3 38.25(10) . .
O21 Dy4 Dy3 76.41(10) . .
O5 Dy4 Dy3 35.56(10) 2_655 .
O28 Dy4 Dy3 169.37(11) . .
O24 Dy4 Dy3 113.64(9) . .
O7 Dy4 Dy3 103.18(10) . .
O6 Dy4 Dy3 100.02(9) . .
O4 Dy4 Dy3 91.56(10) 2_655 .
C16 Dy4 Dy3 107.96(11) . .
O37 Dy4 Dy3 34.88(10) . 2_655
O21 Dy4 Dy3 117.34(10) . 2_655
O5 Dy4 Dy3 78.18(10) 2_655 2_655
O28 Dy4 Dy3 127.40(11) . 2_655
O24 Dy4 Dy3 79.07(9) . 2_655
O7 Dy4 Dy3 80.04(9) . 2_655
O6 Dy4 Dy3 40.79(9) . 2_655
O4 Dy4 Dy3 142.77(9) 2_655 2_655
C16 Dy4 Dy3 61.11(11) . 2_655
Dy3 Dy4 Dy3 61.530(10) . 2_655
O37 Dy4 Dy2 80.95(10) . 2_655
O21 Dy4 Dy2 115.02(10) . 2_655
O5 Dy4 Dy2 136.44(10) 2_655 2_655
O28 Dy4 Dy2 72.26(11) . 2_655
O24 Dy4 Dy2 37.14(9) . 2_655
O7 Dy4 Dy2 85.02(10) . 2_655
O6 Dy4 Dy2 37.17(9) . 2_655
O4 Dy4 Dy2 149.61(10) 2_655 2_655
C16 Dy4 Dy2 57.10(11) . 2_655
Dy3 Dy4 Dy2 118.211(11) . 2_655
Dy3 Dy4 Dy2 60.017(12) 2_655 2_655
O10 N1 O11 127.8(14) . .
O10 N1 C22 118.8(13) . .
O11 N1 C22 113.4(17) . .
C20 C19 C24 120.0 . .
C20 C19 C18 117.9(13) . .
C24 C19 C18 121.1(13) . .
C21 C20 C19 120.0 . .
C21 C20 H20A 120.0 . .
C19 C20 H20A 120.0 . .
C20 C21 C22 120.0 . .
C20 C21 H21A 120.0 . .
C22 C21 H21A 120.0 . .
C21 C22 C23 120.0 . .
C21 C22 N1 120.6(11) . .
C23 C22 N1 119.3(11) . .
C24 C23 C22 120.0 . .
C24 C23 H23A 120.0 . .
C22 C23 H23A 120.0 . .
C23 C24 C19 120.0 . .
C23 C24 H24A 120.0 . .
C19 C24 H24A 120.0 . .
O11' N1' O10' 117.0(17) . .
O11' N1' C22' 124.1(16) . .
O10' N1' C22' 118.9(12) . .
C20' C19' C24' 120.0 . .
C20' C19' C18 122.5(11) . .
C24' C19' C18 117.5(11) . .
C19' C20' C21' 120.0 . .
C19' C20' H20B 120.0 . .
C21' C20' H20B 120.0 . .
C20' C21' C22' 120.0 . .
C20' C21' H21B 120.0 . .
C22' C21' H21B 120.0 . .
C23' C22' C21' 120.0 . .
C23' C22' N1' 120.9(9) . .
C21' C22' N1' 119.0(9) . .
C24' C23' C22' 120.0 . .
C24' C23' H23B 120.0 . .
C22' C23' H23B 120.0 . .
C23' C24' C19' 120.0 . .
C23' C24' H24B 120.0 . .
C19' C24' H24B 120.0 . .
O14 N2 O15 124.7(6) . .
O14 N2 C29 117.3(6) . .
O15 N2 C29 118.0(6) . .
O19 N3 O18 124.3(6) . .
O19 N3 C36 117.9(6) . .
O18 N3 C36 117.7(6) . .
O23 N4 O22 123.8(6) . .
O23 N4 C43 118.2(6) . .
O22 N4 C43 118.0(7) . .
O26 N5 O27 123.2(7) . .
O26 N5 O27' 118.9(11) . .
O27 N5 O27' 32.2(10) . .
O26 N5 C50 119.2(6) . .
O27 N5 C50 115.7(8) . .
O27' N5 C50 118.3(10) . .
O34 N7 O35 129.2(14) . .
O34 N7 C64 116.8(13) . .
O35 N7 C64 113.8(13) . .
C62 C61 C66 120.0 . .
C62 C61 C60 121.3(11) . .
C66 C61 C60 118.7(11) . .
C63 C62 C61 120.0 . .
C63 C62 H62A 120.0 . .
C61 C62 H62A 120.0 . .
C64 C63 C62 120.0 . .
C64 C63 H63A 120.0 . .
C62 C63 H63A 120.0 . .
C63 C64 C65 120.0 . .
C63 C64 N7 118.0(10) . .
C65 C64 N7 121.9(10) . .
C66 C65 C64 120.0 . .
C66 C65 H65A 120.0 . .
C64 C65 H65A 120.0 . .
C65 C66 C61 120.0 . .
C65 C66 H66A 120.0 . .
C61 C66 H66A 120.0 . .
O35' N7' O34' 126.3(12) . .
O35' N7' C64' 116.4(12) . .
O34' N7' C64' 116.2(11) . .
C62' C61' C66' 120.0 . .
C62' C61' C60 120.1(9) . .
C66' C61' C60 119.8(9) . .
C61' C62' C63' 120.0 . .
C61' C62' H62B 120.0 . .
C63' C62' H62B 120.0 . .
C64' C63' C62' 120.0 . .
C64' C63' H63B 120.0 . .
C62' C63' H63B 120.0 . .
C63' C64' C65' 120.0 . .
C63' C64' N7' 120.1(8) . .
C65' C64' N7' 119.9(8) . .
C66' C65' C64' 120.0 . .
C66' C65' H65B 120.0 . .
C64' C65' H65B 120.0 . .
C65' C66' C61' 120.0 . .
C65' C66' H66B 120.0 . .
C61' C66' H66B 120.0 . .
Dy3 O36 Dy2 108.82(15) . .
Dy3 O36 Dy1 117.76(16) . .
Dy2 O36 Dy1 108.74(16) . .
Dy3 O36 H36A 107.0 . .
Dy2 O36 H36A 107.0 . .
Dy1 O36 H36A 107.0 . .
C2 O1 C1 116.0(5) . .
C2 O1 Dy1 111.8(3) . .
C1 O1 Dy1 128.8(4) . .
C7 O2 Dy2 133.8(4) . .
C7 O2 Dy1 115.9(3) . .
Dy2 O2 Dy1 109.12(16) . .
C8 O3 Dy2 133.4(4) . .
C10 O4 C9 117.7(5) . .
C10 O4 Dy4 117.7(3) . 2_655
C9 O4 Dy4 124.4(3) . 2_655
C15 O5 Dy3 123.8(3) . 2_655
C15 O5 Dy4 120.5(3) . 2_655
Dy3 O5 Dy4 108.60(16) 2_655 2_655
C16 O6 Dy2 121.2(3) . 2_655
C16 O6 Dy4 99.2(3) . .
Dy2 O6 Dy4 105.29(14) 2_655 .
C16 O6 Dy3 125.3(3) . 2_655
Dy2 O6 Dy3 101.58(14) 2_655 2_655
Dy4 O6 Dy3 100.52(14) . 2_655
C17 O7 C16 115.3(5) . .
C17 O7 Dy4 133.7(4) . .
C16 O7 Dy4 98.5(3) . .
C18 O8 Dy1 92.6(4) . .
C18 O9 Dy1 90.6(3) . .
C25 O12 Dy1 135.9(4) . .
C25 O13 Dy2 136.9(4) . .
C32 O16 Dy1 140.3(4) . .
C32 O17 Dy3 136.0(4) . .
C39 O20 Dy3 144.3(4) . .
C39 O21 Dy4 127.4(4) . .
C46 O24 Dy4 121.9(4) . .
C46 O24 Dy2 123.4(4) . 2_655
Dy4 O24 Dy2 106.36(15) . 2_655
C53 O28 Dy4 132.1(4) . .
C53 O29 Dy2 137.8(4) . 2_655
C60 O32 Dy1 132.3(4) . .
C60 O33 Dy3 123.5(4) . .
C74 O41 Dy2 134.4(4) . .
C74 O41 H41 102.3 . .
Dy2 O41 H41 120.5 . .
C73 O40 H40 109.5 . .
O38' O38 C71 61.8(9) . .
C72 O39 H39 109.5 . .
Dy4 O37 Dy3 111.17(16) . 2_655
Dy4 O37 Dy3 105.61(15) . .
Dy3 O37 Dy3 109.14(15) 2_655 .
Dy4 O37 H37B 110.3 . .
Dy3 O37 H37B 110.3 2_655 .
Dy3 O37 H37B 110.3 . .
O1 C1 H1A 109.5 . .
O1 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
O1 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
C3 C2 O1 124.7(6) . .
C3 C2 C7 122.3(6) . .
O1 C2 C7 113.0(5) . .
C2 C3 C4 119.9(6) . .
C2 C3 H3A 120.0 . .
C4 C3 H3A 120.0 . .
C5 C4 C3 119.8(6) . .
C5 C4 H4A 120.1 . .
C3 C4 H4A 120.1 . .
C4 C5 C6 120.8(6) . .
C4 C5 H5A 119.6 . .
C6 C5 H5A 119.6 . .
C5 C6 C7 119.9(6) . .
C5 C6 C8 117.2(6) . .
C7 C6 C8 122.8(6) . .
O2 C7 C2 118.3(5) . .
O2 C7 C6 124.4(5) . .
C2 C7 C6 117.2(5) . .
O3 C8 C6 127.4(6) . .
O3 C8 H8A 105.4 . .
C6 C8 H8A 105.4 . .
O3 C8 H8B 105.4 . .
C6 C8 H8B 105.4 . .
H8A C8 H8B 106.0 . .
O4 C9 H9A 109.5 . .
O4 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
O4 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
C11 C10 O4 125.1(5) . .
C11 C10 C15 122.4(6) . .
O4 C10 C15 112.5(5) . .
C10 C11 C12 119.2(6) . .
C10 C11 H11A 120.4 . .
C12 C11 H11A 120.4 . .
C11 C12 C13 119.9(6) . .
C11 C12 H12A 120.1 . .
C13 C12 H12A 120.1 . .
C12 C13 C14 120.8(6) . .
C12 C13 H13A 119.6 . .
C14 C13 H13A 119.6 . .
C15 C14 C13 119.8(5) . .
C15 C14 C16 120.8(5) . .
C13 C14 C16 119.0(5) . .
O5 C15 C14 123.1(5) . .
O5 C15 C10 119.0(5) . .
C14 C15 C10 118.0(5) . .
O6 C16 O7 104.0(4) . .
O6 C16 C14 117.6(5) . .
O7 C16 C14 107.8(4) . .
O6 C16 Dy4 53.3(3) . .
O7 C16 Dy4 52.5(2) . .
C14 C16 Dy4 140.4(4) . .
O6 C16 H16A 109.0 . .
O7 C16 H16A 109.0 . .
C14 C16 H16A 109.0 . .
Dy4 C16 H16A 110.1 . .
O7 C17 H17A 109.5 . .
O7 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
O7 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
O9 C18 O8 121.7(6) . .
O9 C18 C19' 122.0(8) . .
O8 C18 C19' 116.3(8) . .
O9 C18 C19 118.5(9) . .
O8 C18 C19 119.5(10) . .
C19' C18 C19 6.2(14) . .
O9 C18 Dy1 62.1(3) . .
O8 C18 Dy1 59.6(3) . .
C19' C18 Dy1 175.5(8) . .
C19 C18 Dy1 173.1(9) . .
O13 C25 O12 125.8(5) . .
O13 C25 C26 117.5(5) . .
O12 C25 C26 116.8(5) . .
C27 C26 C31 121.0(5) . .
C27 C26 C25 119.6(5) . .
C31 C26 C25 119.5(5) . .
C28 C27 C26 120.0(6) . .
C28 C27 H27A 120.0 . .
C26 C27 H27A 120.0 . .
C29 C28 C27 118.4(6) . .
C29 C28 H28A 120.8 . .
C27 C28 H28A 120.8 . .
C28 C29 C30 123.0(6) . .
C28 C29 N2 118.9(6) . .
C30 C29 N2 118.0(6) . .
C31 C30 C29 118.1(6) . .
C31 C30 H30A 121.0 . .
C29 C30 H30A 121.0 . .
C30 C31 C26 119.5(6) . .
C30 C31 H31A 120.2 . .
C26 C31 H31A 120.2 . .
O17 C32 O16 125.6(6) . .
O17 C32 C33 117.2(5) . .
O16 C32 C33 117.2(5) . .
C34 C33 C38 119.3(6) . .
C34 C33 C32 120.6(5) . .
C38 C33 C32 120.1(6) . .
C33 C34 C35 120.0(6) . .
C33 C34 H34A 120.0 . .
C35 C34 H34A 120.0 . .
C36 C35 C34 119.5(6) . .
C36 C35 H35A 120.2 . .
C34 C35 H35A 120.2 . .
C35 C36 C37 121.9(6) . .
C35 C36 N3 119.2(6) . .
C37 C36 N3 118.9(6) . .
C38 C37 C36 118.1(6) . .
C38 C37 H37A 120.9 . .
C36 C37 H37A 120.9 . .
C37 C38 C33 121.2(6) . .
C37 C38 H38A 119.4 . .
C33 C38 H38A 119.4 . .
O20 C39 O21 125.5(6) . .
O20 C39 C40 116.3(5) . .
O21 C39 C40 118.2(5) . .
C41 C40 C45 120.7(6) . .
C41 C40 C39 119.9(6) . .
C45 C40 C39 119.4(5) . .
C42 C41 C40 120.1(6) . .
C42 C41 H41A 119.9 . .
C40 C41 H41A 119.9 . .
C43 C42 C41 118.1(6) . .
C43 C42 H42A 121.0 . .
C41 C42 H42A 121.0 . .
C42 C43 C44 123.3(6) . .
C42 C43 N4 118.9(6) . .
C44 C43 N4 117.9(7) . .
C43 C44 C45 118.2(7) . .
C43 C44 H44A 120.9 . .
C45 C44 H44A 120.9 . .
C44 C45 C40 119.6(6) . .
C44 C45 H45A 120.2 . .
C40 C45 H45A 120.2 . .
O25 C46 O24 123.6(5) . .
O25 C46 C47 120.5(5) . .
O24 C46 C47 115.9(5) . .
C48 C47 C52 119.7(6) . .
C48 C47 C46 120.3(6) . .
C52 C47 C46 119.9(6) . .
C49 C48 C47 120.5(7) . .
C49 C48 H48A 119.8 . .
C47 C48 H48A 119.8 . .
C48 C49 C50 118.8(7) . .
C48 C49 H49A 120.6 . .
C50 C49 H49A 120.6 . .
C51 C50 C49 122.7(6) . .
C51 C50 N5 118.5(6) . .
C49 C50 N5 118.8(6) . .
C50 C51 C52 118.0(6) . .
C50 C51 H51A 121.0 . .
C52 C51 H51A 121.0 . .
C47 C52 C51 120.4(6) . .
C47 C52 H52A 119.8 . .
C51 C52 H52A 119.8 . .
O28 C53 O29 125.2(5) . .
O28 C53 C54 116.8(6) . .
O29 C53 C54 118.0(5) . .
C55 C54 C59 120.8(6) . .
C55 C54 C53 119.6(6) . .
C59 C54 C53 119.5(6) . .
O33 C60 O32 124.1(6) . .
O33 C60 C61 113.7(8) . .
O32 C60 C61 122.0(9) . .
O33 C60 C61' 121.3(7) . .
O32 C60 C61' 114.5(7) . .
C61 C60 C61' 11.0(13) . .
N8 C67 C68 179.4(18) . .
C67 C68 H68A 109.5 . .
C67 C68 H68B 109.5 . .
H68A C68 H68B 109.5 . .
C67 C68 H68C 109.5 . .
H68A C68 H68C 109.5 . .
H68B C68 H68C 109.5 . .
O41 C74 H74A 109.5 . .
O41 C74 H74B 109.5 . .
H74A C74 H74B 109.5 . .
O41 C74 H74C 109.5 . .
H74A C74 H74C 109.5 . .
H74B C74 H74C 109.5 . .
O40 C73 H73A 109.5 . .
O40 C73 H73B 109.5 . .
H73A C73 H73B 109.5 . .
O40 C73 H73C 109.5 . .
H73A C73 H73C 109.5 . .
H73B C73 H73C 109.5 . .
O38 O38' C71 67.4(11) . .
O39 C72 H72A 109.5 . .
O39 C72 H72B 109.5 . .
H72A C72 H72B 109.5 . .
O39 C72 H72C 109.5 . .
H72A C72 H72C 109.5 . .
H72B C72 H72C 109.5 . .
O38' C71 O38 50.7(8) . .
C69 C70 H70A 109.5 . .
C69 C70 H70B 109.5 . .
H70A C70 H70B 109.5 . .
C69 C70 H70C 109.5 . .
H70A C70 H70C 109.5 . .
H70B C70 H70C 109.5 . .
N9 C69 C70 178(2) . .
O30' N6 O31 111.5(13) . .
O30' N6 O30 26.4(12) . .
O31 N6 O30 123.7(10) . .
O30' N6 O31' 126.9(10) . .
O31 N6 O31' 36.5(9) . .
O30 N6 O31' 120.4(14) . .
O30' N6 C57 118.0(10) . .
O31 N6 C57 118.2(9) . .
O30 N6 C57 117.1(10) . .
O31' N6 C57 115.1(9) . .
C54 C55 C56 119.7(7) . .
C54 C55 H55A 120.1 . .
C56 C55 H55A 120.1 . .
C57 C56 C55 119.0(7) . .
C57 C56 H56A 120.5 . .
C55 C56 H56A 120.5 . .
C56 C57 C58 122.7(7) . .
C56 C57 N6 118.7(8) . .
C58 C57 N6 118.6(8) . .
C57 C58 C59 118.0(8) . .
C57 C58 H58A 121.0 . .
C59 C58 H58A 121.0 . .
C54 C59 C58 119.7(7) . .
C54 C59 H59A 120.1 . .
C58 C59 H59A 120.1 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O16 2.280(4) .
Dy1 O32 2.286(4) .
Dy1 O12 2.307(4) .
Dy1 O36 2.367(4) .
Dy1 O8 2.392(4) .
Dy1 O2 2.395(4) .
Dy1 O9 2.450(4) .
Dy1 O1 2.519(4) .
Dy1 C18 2.772(6) .
Dy1 Dy2 3.8413(6) .
Dy2 O2 2.319(4) .
Dy2 O13 2.339(4) .
Dy2 O29 2.343(4) 2_655
Dy2 O36 2.359(4) .
Dy2 O3 2.380(4) .
Dy2 O6 2.407(4) 2_655
Dy2 O41 2.410(4) .
Dy2 O24 2.418(4) 2_655
Dy2 Dy3 3.8315(7) .
Dy2 Dy4 3.8431(6) 2_655
Dy3 O5 2.291(4) 2_655
Dy3 O20 2.328(4) .
Dy3 O37 2.341(4) 2_655
Dy3 O33 2.349(4) .
Dy3 O36 2.353(4) .
Dy3 O17 2.366(4) .
Dy3 O37 2.400(4) .
Dy3 O6 2.537(4) 2_655
Dy3 Dy4 3.7341(6) .
Dy3 Dy4 3.8179(5) 2_655
Dy3 Dy3 3.8636(7) 2_655
Dy4 O37 2.287(4) .
Dy4 O21 2.306(4) .
Dy4 O5 2.307(4) 2_655
Dy4 O28 2.307(4) .
Dy4 O24 2.383(4) .
Dy4 O7 2.398(4) .
Dy4 O6 2.428(4) .
Dy4 O4 2.447(4) 2_655
Dy4 C16 2.987(6) .
Dy4 Dy3 3.8178(5) 2_655
Dy4 Dy2 3.8431(5) 2_655
N1 O10 1.226(9) .
N1 O11 1.237(9) .
N1 C22 1.431(17) .
C19 C20 1.3900 .
C19 C24 1.3900 .
C19 C18 1.537(13) .
C20 C21 1.3900 .
C20 H20A 0.9500 .
C21 C22 1.3900 .
C21 H21A 0.9500 .
C22 C23 1.3900 .
C23 C24 1.3900 .
C23 H23A 0.9500 .
C24 H24A 0.9500 .
N1' O11' 1.229(10) .
N1' O10' 1.236(9) .
N1' C22' 1.396(16) .
C19' C20' 1.3900 .
C19' C24' 1.3900 .
C19' C18 1.462(12) .
C20' C21' 1.3900 .
C20' H20B 0.9500 .
C21' C22' 1.3900 .
C21' H21B 0.9500 .
C22' C23' 1.3900 .
C23' C24' 1.3900 .
C23' H23B 0.9500 .
C24' H24B 0.9500 .
N2 O14 1.228(7) .
N2 O15 1.238(8) .
N2 C29 1.475(8) .
N3 O19 1.215(8) .
N3 O18 1.216(8) .
N3 C36 1.481(8) .
N4 O23 1.221(8) .
N4 O22 1.225(8) .
N4 C43 1.483(9) .
N5 O26 1.197(8) .
N5 O27 1.239(14) .
N5 O27' 1.29(2) .
N5 C50 1.481(8) .
N7 O34 1.222(9) .
N7 O35 1.226(9) .
N7 C64 1.476(18) .
C61 C62 1.3900 .
C61 C66 1.3900 .
C61 C60 1.468(11) .
C62 C63 1.3900 .
C62 H62A 0.9500 .
C63 C64 1.3900 .
C63 H63A 0.9500 .
C64 C65 1.3900 .
C65 C66 1.3900 .
C65 H65A 0.9500 .
C66 H66A 0.9500 .
N7' O35' 1.236(9) .
N7' O34' 1.236(9) .
N7' C64' 1.474(16) .
C61' C62' 1.3900 .
C61' C66' 1.3900 .
C61' C60 1.508(10) .
C62' C63' 1.3900 .
C62' H62B 0.9500 .
C63' C64' 1.3900 .
C63' H63B 0.9500 .
C64' C65' 1.3900 .
C65' C66' 1.3900 .
C65' H65B 0.9500 .
C66' H66B 0.9500 .
N8 C67 1.152(15) .
O36 H36A 1.0000 .
O1 C2 1.388(7) .
O1 C1 1.434(7) .
O2 C7 1.319(7) .
O3 C8 1.245(7) .
O4 C10 1.391(7) .
O4 C9 1.452(7) .
O4 Dy4 2.447(4) 2_655
O5 C15 1.342(7) .
O5 Dy3 2.291(4) 2_655
O5 Dy4 2.307(4) 2_655
O6 C16 1.396(7) .
O6 Dy2 2.407(4) 2_655
O6 Dy3 2.537(4) 2_655
O7 C17 1.427(7) .
O7 C16 1.463(7) .
O8 C18 1.294(7) .
O9 C18 1.272(8) .
O12 C25 1.268(7) .
O13 C25 1.241(7) .
O16 C32 1.251(7) .
O17 C32 1.248(7) .
O20 C39 1.261(7) .
O21 C39 1.263(7) .
O24 C46 1.312(7) .
O24 Dy2 2.418(4) 2_655
O25 C46 1.226(7) .
O28 C53 1.255(7) .
O29 C53 1.261(7) .
O29 Dy2 2.343(4) 2_655
O32 C60 1.270(7) .
O33 C60 1.249(7) .
O41 C74 1.414(8) .
O41 H41 0.8585 .
O40 C73 1.396(9) .
O40 H40 0.8400 .
O38 O38' 1.234(19) .
O38 C71 1.472(13) .
O39 C72 1.431(9) .
O39 H39 0.8400 .
O37 Dy3 2.341(4) 2_655
O37 H37B 1.0000 .
C1 H1A 0.9800 .
C1 H1B 0.9800 .
C1 H1C 0.9800 .
C2 C3 1.372(9) .
C2 C7 1.410(8) .
C3 C4 1.395(10) .
C3 H3A 0.9500 .
C4 C5 1.378(10) .
C4 H4A 0.9500 .
C5 C6 1.411(9) .
C5 H5A 0.9500 .
C6 C7 1.415(9) .
C6 C8 1.426(9) .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 C11 1.378(9) .
C10 C15 1.399(8) .
C11 C12 1.386(9) .
C11 H11A 0.9500 .
C12 C13 1.387(9) .
C12 H12A 0.9500 .
C13 C14 1.399(8) .
C13 H13A 0.9500 .
C14 C15 1.397(8) .
C14 C16 1.513(8) .
C16 H16A 1.0000 .
C17 H17A 0.9800 .
C17 H17B 0.9800 .
C17 H17C 0.9800 .
C25 C26 1.519(8) .
C26 C27 1.390(8) .
C26 C31 1.393(8) .
C27 C28 1.385(9) .
C27 H27A 0.9500 .
C28 C29 1.371(9) .
C28 H28A 0.9500 .
C29 C30 1.398(9) .
C30 C31 1.388(8) .
C30 H30A 0.9500 .
C31 H31A 0.9500 .
C32 C33 1.509(8) .
C33 C34 1.385(9) .
C33 C38 1.394(9) .
C34 C35 1.388(8) .
C34 H34A 0.9500 .
C35 C36 1.373(9) .
C35 H35A 0.9500 .
C36 C37 1.383(9) .
C37 C38 1.381(9) .
C37 H37A 0.9500 .
C38 H38A 0.9500 .
C39 C40 1.509(8) .
C40 C41 1.387(8) .
C40 C45 1.391(9) .
C41 C42 1.382(9) .
C41 H41A 0.9500 .
C42 C43 1.375(10) .
C42 H42A 0.9500 .
C43 C44 1.381(10) .
C44 C45 1.386(9) .
C44 H44A 0.9500 .
C45 H45A 0.9500 .
C46 C47 1.505(8) .
C47 C48 1.380(9) .
C47 C52 1.385(9) .
C48 C49 1.373(10) .
C48 H48A 0.9500 .
C49 C50 1.374(10) .
C49 H49A 0.9500 .
C50 C51 1.365(9) .
C51 C52 1.395(9) .
C51 H51A 0.9500 .
C52 H52A 0.9500 .
C53 C54 1.510(8) .
C54 C55 1.376(9) .
C54 C59 1.384(10) .
C67 C68 1.401(15) .
C68 H68A 0.9800 .
C68 H68B 0.9800 .
C68 H68C 0.9800 .
C74 H74A 0.9800 .
C74 H74B 0.9800 .
C74 H74C 0.9800 .
C73 H73A 0.9800 .
C73 H73B 0.9800 .
C73 H73C 0.9800 .
O38' C71 1.405(18) .
C72 H72A 0.9800 .
C72 H72B 0.9800 .
C72 H72C 0.9800 .
C70 C69 1.446(9) .
C70 H70A 0.9800 .
C70 H70B 0.9800 .
C70 H70C 0.9800 .
C69 N9 1.207(9) .
O30 N6 1.246(9) .
O31 N6 1.243(8) .
O30' N6 1.231(8) .
O31' N6 1.248(8) .
N6 C57 1.483(9) .
C55 C56 1.391(9) .
C55 H55A 0.9500 .
C56 C57 1.358(12) .
C56 H56A 0.9500 .
C57 C58 1.383(12) .
C58 C59 1.395(9) .
C58 H58A 0.9500 .
C59 H59A 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O16 Dy1 Dy2 O2 157.4(2) . .
O32 Dy1 Dy2 O2 67.15(19) . .
O12 Dy1 Dy2 O2 -110.96(19) . .
O36 Dy1 Dy2 O2 152.2(2) . .
O8 Dy1 Dy2 O2 -101.5(2) . .
O9 Dy1 Dy2 O2 34.0(3) . .
O1 Dy1 Dy2 O2 -20.91(18) . .
C18 Dy1 Dy2 O2 -65.9(6) . .
O16 Dy1 Dy2 O13 -98.71(17) . .
O32 Dy1 Dy2 O13 170.99(15) . .
O12 Dy1 Dy2 O13 -7.12(15) . .
O36 Dy1 Dy2 O13 -103.93(19) . .
O8 Dy1 Dy2 O13 2.36(19) . .
O2 Dy1 Dy2 O13 103.84(19) . .
O9 Dy1 Dy2 O13 137.8(3) . .
O1 Dy1 Dy2 O13 82.93(14) . .
C18 Dy1 Dy2 O13 37.9(6) . .
O16 Dy1 Dy2 O29 -106.4(9) . 2_655
O32 Dy1 Dy2 O29 163.3(9) . 2_655
O12 Dy1 Dy2 O29 -14.8(9) . 2_655
O36 Dy1 Dy2 O29 -111.6(9) . 2_655
O8 Dy1 Dy2 O29 -5.4(9) . 2_655
O2 Dy1 Dy2 O29 96.1(9) . 2_655
O9 Dy1 Dy2 O29 130.1(9) . 2_655
O1 Dy1 Dy2 O29 75.2(9) . 2_655
C18 Dy1 Dy2 O29 30.2(11) . 2_655
O16 Dy1 Dy2 O36 5.2(2) . .
O32 Dy1 Dy2 O36 -85.08(19) . .
O12 Dy1 Dy2 O36 96.8(2) . .
O8 Dy1 Dy2 O36 106.3(2) . .
O2 Dy1 Dy2 O36 -152.2(2) . .
O9 Dy1 Dy2 O36 -118.3(3) . .
O1 Dy1 Dy2 O36 -173.14(19) . .
C18 Dy1 Dy2 O36 141.9(6) . .
O16 Dy1 Dy2 O3 121.69(17) . .
O32 Dy1 Dy2 O3 31.39(15) . .
O12 Dy1 Dy2 O3 -146.71(15) . .
O36 Dy1 Dy2 O3 116.47(19) . .
O8 Dy1 Dy2 O3 -137.24(19) . .
O2 Dy1 Dy2 O3 -35.75(19) . .
O9 Dy1 Dy2 O3 -1.8(3) . .
O1 Dy1 Dy2 O3 -56.66(14) . .
C18 Dy1 Dy2 O3 -101.7(6) . .
O16 Dy1 Dy2 O6 42.48(17) . 2_655
O32 Dy1 Dy2 O6 -47.82(14) . 2_655
O12 Dy1 Dy2 O6 134.07(15) . 2_655
O36 Dy1 Dy2 O6 37.26(19) . 2_655
O8 Dy1 Dy2 O6 143.55(19) . 2_655
O2 Dy1 Dy2 O6 -114.97(19) . 2_655
O9 Dy1 Dy2 O6 -81.0(3) . 2_655
O1 Dy1 Dy2 O6 -135.88(13) . 2_655
C18 Dy1 Dy2 O6 179.1(6) . 2_655
O16 Dy1 Dy2 O41 -161.27(17) . .
O32 Dy1 Dy2 O41 108.43(16) . .
O12 Dy1 Dy2 O41 -69.67(16) . .
O36 Dy1 Dy2 O41 -166.5(2) . .
O8 Dy1 Dy2 O41 -60.2(2) . .
O2 Dy1 Dy2 O41 41.29(19) . .
O9 Dy1 Dy2 O41 75.2(3) . .
O1 Dy1 Dy2 O41 20.38(15) . .
C18 Dy1 Dy2 O41 -24.6(6) . .
O16 Dy1 Dy2 O24 -33.02(16) . 2_655
O32 Dy1 Dy2 O24 -123.32(14) . 2_655
O12 Dy1 Dy2 O24 58.58(14) . 2_655
O36 Dy1 Dy2 O24 -38.24(19) . 2_655
O8 Dy1 Dy2 O24 68.05(19) . 2_655
O2 Dy1 Dy2 O24 169.54(19) . 2_655
O9 Dy1 Dy2 O24 -156.5(3) . 2_655
O1 Dy1 Dy2 O24 148.63(13) . 2_655
C18 Dy1 Dy2 O24 103.6(6) . 2_655
O16 Dy1 Dy2 Dy3 35.31(13) . .
O32 Dy1 Dy2 Dy3 -55.00(11) . .
O12 Dy1 Dy2 Dy3 126.90(11) . .
O36 Dy1 Dy2 Dy3 30.08(16) . .
O8 Dy1 Dy2 Dy3 136.37(16) . .
O2 Dy1 Dy2 Dy3 -122.14(16) . .
O9 Dy1 Dy2 Dy3 -88.2(3) . .
O1 Dy1 Dy2 Dy3 -143.05(9) . .
C18 Dy1 Dy2 Dy3 171.9(6) . .
O16 Dy1 Dy2 Dy4 4.59(13) . 2_655
O32 Dy1 Dy2 Dy4 -85.71(11) . 2_655
O12 Dy1 Dy2 Dy4 96.18(11) . 2_655
O36 Dy1 Dy2 Dy4 -0.63(16) . 2_655
O8 Dy1 Dy2 Dy4 105.65(16) . 2_655
O2 Dy1 Dy2 Dy4 -152.86(16) . 2_655
O9 Dy1 Dy2 Dy4 -118.9(3) . 2_655
O1 Dy1 Dy2 Dy4 -173.77(9) . 2_655
C18 Dy1 Dy2 Dy4 141.2(6) . 2_655
O2 Dy2 Dy3 O5 117.47(14) . 2_655
O13 Dy2 Dy3 O5 -165.00(15) . 2_655
O29 Dy2 Dy3 O5 -37.31(16) 2_655 2_655
O36 Dy2 Dy3 O5 177.7(2) . 2_655
O3 Dy2 Dy3 O5 43.67(15) . 2_655
O6 Dy2 Dy3 O5 -21.71(18) 2_655 2_655
O41 Dy2 Dy3 O5 94.7(3) . 2_655
O24 Dy2 Dy3 O5 -98.68(14) 2_655 2_655
Dy1 Dy2 Dy3 O5 147.50(11) . 2_655
Dy4 Dy2 Dy3 O5 -64.84(11) 2_655 2_655
O2 Dy2 Dy3 O20 20.48(18) . .
O13 Dy2 Dy3 O20 98.01(19) . .
O29 Dy2 Dy3 O20 -134.30(19) 2_655 .
O36 Dy2 Dy3 O20 80.7(2) . .
O3 Dy2 Dy3 O20 -53.32(18) . .
O6 Dy2 Dy3 O20 -118.7(2) 2_655 .
O41 Dy2 Dy3 O20 -2.3(3) . .
O24 Dy2 Dy3 O20 164.34(18) 2_655 .
Dy1 Dy2 Dy3 O20 50.51(16) . .
Dy4 Dy2 Dy3 O20 -161.83(16) 2_655 .
O2 Dy2 Dy3 O37 -148.56(14) . 2_655
O13 Dy2 Dy3 O37 -71.02(15) . 2_655
O29 Dy2 Dy3 O37 56.66(15) 2_655 2_655
O36 Dy2 Dy3 O37 -88.31(19) . 2_655
O3 Dy2 Dy3 O37 137.64(14) . 2_655
O6 Dy2 Dy3 O37 72.27(17) 2_655 2_655
O41 Dy2 Dy3 O37 -171.4(3) . 2_655
O24 Dy2 Dy3 O37 -4.70(14) 2_655 2_655
Dy1 Dy2 Dy3 O37 -118.53(10) . 2_655
Dy4 Dy2 Dy3 O37 29.14(10) 2_655 2_655
O2 Dy2 Dy3 O33 44.16(15) . .
O13 Dy2 Dy3 O33 121.69(16) . .
O29 Dy2 Dy3 O33 -110.62(16) 2_655 .
O36 Dy2 Dy3 O33 104.4(2) . .
O3 Dy2 Dy3 O33 -29.64(15) . .
O6 Dy2 Dy3 O33 -95.02(18) 2_655 .
O41 Dy2 Dy3 O33 21.3(3) . .
O24 Dy2 Dy3 O33 -171.98(15) 2_655 .
Dy1 Dy2 Dy3 O33 74.19(11) . .
Dy4 Dy2 Dy3 O33 -138.15(11) 2_655 .
O2 Dy2 Dy3 O36 -60.25(19) . .
O13 Dy2 Dy3 O36 17.3(2) . .
O29 Dy2 Dy3 O36 145.0(2) 2_655 .
O3 Dy2 Dy3 O36 -134.05(19) . .
O6 Dy2 Dy3 O36 160.6(2) 2_655 .
O41 Dy2 Dy3 O36 -83.1(3) . .
O24 Dy2 Dy3 O36 83.61(19) 2_655 .
Dy1 Dy2 Dy3 O36 -30.22(17) . .
Dy4 Dy2 Dy3 O36 117.45(17) 2_655 .
O2 Dy2 Dy3 O17 -68.53(16) . .
O13 Dy2 Dy3 O17 9.01(17) . .
O29 Dy2 Dy3 O17 136.69(17) 2_655 .
O36 Dy2 Dy3 O17 -8.3(2) . .
O3 Dy2 Dy3 O17 -142.33(16) . .
O6 Dy2 Dy3 O17 152.30(19) 2_655 .
O41 Dy2 Dy3 O17 -91.3(3) . .
O24 Dy2 Dy3 O17 75.33(16) 2_655 .
Dy1 Dy2 Dy3 O17 -38.50(12) . .
Dy4 Dy2 Dy3 O17 109.16(12) 2_655 .
O2 Dy2 Dy3 O37 -163.5(2) . .
O13 Dy2 Dy3 O37 -86.0(2) . .
O29 Dy2 Dy3 O37 41.7(2) 2_655 .
O36 Dy2 Dy3 O37 -103.3(3) . .
O3 Dy2 Dy3 O37 122.7(2) . .
O6 Dy2 Dy3 O37 57.3(2) 2_655 .
O41 Dy2 Dy3 O37 173.7(4) . .
O24 Dy2 Dy3 O37 -19.6(2) 2_655 .
Dy1 Dy2 Dy3 O37 -133.47(19) . .
Dy4 Dy2 Dy3 O37 14.19(19) 2_655 .
O2 Dy2 Dy3 O6 139.17(17) . 2_655
O13 Dy2 Dy3 O6 -143.29(18) . 2_655
O29 Dy2 Dy3 O6 -15.61(19) 2_655 2_655
O36 Dy2 Dy3 O6 -160.6(2) . 2_655
O3 Dy2 Dy3 O6 65.37(18) . 2_655
O41 Dy2 Dy3 O6 116.4(3) . 2_655
O24 Dy2 Dy3 O6 -76.97(17) 2_655 2_655
Dy1 Dy2 Dy3 O6 169.20(14) . 2_655
Dy4 Dy2 Dy3 O6 -43.13(14) 2_655 2_655
O2 Dy2 Dy3 Dy4 128.31(10) . .
O13 Dy2 Dy3 Dy4 -154.15(11) . .
O29 Dy2 Dy3 Dy4 -26.46(12) 2_655 .
O36 Dy2 Dy3 Dy4 -171.44(17) . .
O3 Dy2 Dy3 Dy4 54.51(10) . .
O6 Dy2 Dy3 Dy4 -10.86(14) 2_655 .
O41 Dy2 Dy3 Dy4 105.5(3) . .
O24 Dy2 Dy3 Dy4 -87.83(10) 2_655 .
Dy1 Dy2 Dy3 Dy4 158.346(17) . .
Dy4 Dy2 Dy3 Dy4 -53.992(16) 2_655 .
O2 Dy2 Dy3 Dy4 -177.69(10) . 2_655
O13 Dy2 Dy3 Dy4 -100.16(11) . 2_655
O29 Dy2 Dy3 Dy4 27.53(12) 2_655 2_655
O36 Dy2 Dy3 Dy4 -117.45(17) . 2_655
O3 Dy2 Dy3 Dy4 108.51(10) . 2_655
O6 Dy2 Dy3 Dy4 43.13(14) 2_655 2_655
O41 Dy2 Dy3 Dy4 159.5(3) . 2_655
O24 Dy2 Dy3 Dy4 -33.83(9) 2_655 2_655
Dy1 Dy2 Dy3 Dy4 -147.662(9) . 2_655
O2 Dy2 Dy3 Dy3 -158.03(10) . 2_655
O13 Dy2 Dy3 Dy3 -80.49(11) . 2_655
O29 Dy2 Dy3 Dy3 47.19(12) 2_655 2_655
O36 Dy2 Dy3 Dy3 -97.78(16) . 2_655
O3 Dy2 Dy3 Dy3 128.17(10) . 2_655
O6 Dy2 Dy3 Dy3 62.80(14) 2_655 2_655
O41 Dy2 Dy3 Dy3 179.2(3) . 2_655
O24 Dy2 Dy3 Dy3 -14.17(9) 2_655 2_655
Dy1 Dy2 Dy3 Dy3 -127.995(8) . 2_655
Dy4 Dy2 Dy3 Dy3 19.667(7) 2_655 2_655
O5 Dy3 Dy4 O37 145.9(2) 2_655 .
O20 Dy3 Dy4 O37 -101.9(2) . .
O37 Dy3 Dy4 O37 49.30(15) 2_655 .
O33 Dy3 Dy4 O37 -162.42(19) . .
O36 Dy3 Dy4 O37 50.2(11) . .
O17 Dy3 Dy4 O37 -36.10(19) . .
O6 Dy3 Dy4 O37 121.29(18) 2_655 .
Dy4 Dy3 Dy4 O37 83.31(16) 2_655 .
Dy2 Dy3 Dy4 O37 128.22(16) . .
Dy3 Dy3 Dy4 O37 34.96(16) 2_655 .
O5 Dy3 Dy4 O21 -117.1(2) 2_655 .
O20 Dy3 Dy4 O21 -4.95(16) . .
O37 Dy3 Dy4 O21 146.29(14) 2_655 .
O33 Dy3 Dy4 O21 -65.42(15) . .
O36 Dy3 Dy4 O21 147.2(11) . .
O17 Dy3 Dy4 O21 60.90(16) . .
O37 Dy3 Dy4 O21 96.99(19) . .
O6 Dy3 Dy4 O21 -141.71(14) 2_655 .
Dy4 Dy3 Dy4 O21 -179.70(10) 2_655 .
Dy2 Dy3 Dy4 O21 -134.79(11) . .
Dy3 Dy3 Dy4 O21 131.96(10) 2_655 .
O20 Dy3 Dy4 O5 112.1(2) . 2_655
O37 Dy3 Dy4 O5 -96.64(19) 2_655 2_655
O33 Dy3 Dy4 O5 51.6(2) . 2_655
O36 Dy3 Dy4 O5 -95.7(11) . 2_655
O17 Dy3 Dy4 O5 178.0(2) . 2_655
O37 Dy3 Dy4 O5 -145.9(2) . 2_655
O6 Dy3 Dy4 O5 -24.65(19) 2_655 2_655
Dy4 Dy3 Dy4 O5 -62.63(17) 2_655 2_655
Dy2 Dy3 Dy4 O5 -17.72(17) . 2_655
Dy3 Dy3 Dy4 O5 -110.98(17) 2_655 2_655
O5 Dy3 Dy4 O28 -37.9(6) 2_655 .
O20 Dy3 Dy4 O28 74.2(6) . .
O37 Dy3 Dy4 O28 -134.6(6) 2_655 .
O33 Dy3 Dy4 O28 13.7(6) . .
O36 Dy3 Dy4 O28 -133.7(12) . .
O17 Dy3 Dy4 O28 140.0(6) . .
O37 Dy3 Dy4 O28 176.1(6) . .
O6 Dy3 Dy4 O28 -62.6(6) 2_655 .
Dy4 Dy3 Dy4 O28 -100.6(6) 2_655 .
Dy2 Dy3 Dy4 O28 -55.7(6) . .
Dy3 Dy3 Dy4 O28 -148.9(6) 2_655 .
O5 Dy3 Dy4 O24 172.8(2) 2_655 .
O20 Dy3 Dy4 O24 -75.13(16) . .
O37 Dy3 Dy4 O24 76.12(14) 2_655 .
O33 Dy3 Dy4 O24 -135.60(15) . .
O36 Dy3 Dy4 O24 77.0(11) . .
O17 Dy3 Dy4 O24 -9.28(15) . .
O37 Dy3 Dy4 O24 26.81(19) . .
O6 Dy3 Dy4 O24 148.11(14) 2_655 .
Dy4 Dy3 Dy4 O24 110.12(10) 2_655 .
Dy2 Dy3 Dy4 O24 155.03(10) . .
Dy3 Dy3 Dy4 O24 61.78(10) 2_655 .
O5 Dy3 Dy4 O7 40.2(2) 2_655 .
O20 Dy3 Dy4 O7 152.30(16) . .
O37 Dy3 Dy4 O7 -56.46(14) 2_655 .
O33 Dy3 Dy4 O7 91.83(14) . .
O36 Dy3 Dy4 O7 -55.6(11) . .
O17 Dy3 Dy4 O7 -141.85(15) . .
O37 Dy3 Dy4 O7 -105.76(19) . .
O6 Dy3 Dy4 O7 15.54(14) 2_655 .
Dy4 Dy3 Dy4 O7 -22.45(10) 2_655 .
Dy2 Dy3 Dy4 O7 22.46(10) . .
Dy3 Dy3 Dy4 O7 -70.79(10) 2_655 .
O5 Dy3 Dy4 O6 97.01(19) 2_655 .
O20 Dy3 Dy4 O6 -150.87(16) . .
O37 Dy3 Dy4 O6 0.38(13) 2_655 .
O33 Dy3 Dy4 O6 148.66(14) . .
O36 Dy3 Dy4 O6 1.3(11) . .
O17 Dy3 Dy4 O6 -85.02(15) . .
O37 Dy3 Dy4 O6 -48.93(18) . .
O6 Dy3 Dy4 O6 72.37(12) 2_655 .
Dy4 Dy3 Dy4 O6 34.38(9) 2_655 .
Dy2 Dy3 Dy4 O6 79.29(9) . .
Dy3 Dy3 Dy4 O6 -13.96(9) 2_655 .
O5 Dy3 Dy4 O4 -42.06(19) 2_655 2_655
O20 Dy3 Dy4 O4 70.06(16) . 2_655
O37 Dy3 Dy4 O4 -138.70(14) 2_655 2_655
O33 Dy3 Dy4 O4 9.58(14) . 2_655
O36 Dy3 Dy4 O4 -137.8(11) . 2_655
O17 Dy3 Dy4 O4 135.90(15) . 2_655
O37 Dy3 Dy4 O4 172.00(19) . 2_655
O6 Dy3 Dy4 O4 -66.71(14) 2_655 2_655
Dy4 Dy3 Dy4 O4 -104.69(10) 2_655 2_655
Dy2 Dy3 Dy4 O4 -59.78(10) . 2_655
Dy3 Dy3 Dy4 O4 -153.04(10) 2_655 2_655
O5 Dy3 Dy4 C16 69.9(2) 2_655 .
O20 Dy3 Dy4 C16 -178.01(17) . .
O37 Dy3 Dy4 C16 -26.76(15) 2_655 .
O33 Dy3 Dy4 C16 121.52(16) . .
O36 Dy3 Dy4 C16 -25.9(11) . .
O17 Dy3 Dy4 C16 -112.16(16) . .
O37 Dy3 Dy4 C16 -76.06(19) . .
O6 Dy3 Dy4 C16 45.23(15) 2_655 .
Dy4 Dy3 Dy4 C16 7.24(12) 2_655 .
Dy2 Dy3 Dy4 C16 52.16(12) . .
Dy3 Dy3 Dy4 C16 -41.10(12) 2_655 .
O5 Dy3 Dy4 Dy3 110.98(17) 2_655 2_655
O20 Dy3 Dy4 Dy3 -136.90(13) . 2_655
O37 Dy3 Dy4 Dy3 14.34(10) 2_655 2_655
O33 Dy3 Dy4 Dy3 162.62(10) . 2_655
O36 Dy3 Dy4 Dy3 15.2(11) . 2_655
O17 Dy3 Dy4 Dy3 -71.06(11) . 2_655
O37 Dy3 Dy4 Dy3 -34.96(16) . 2_655
O6 Dy3 Dy4 Dy3 86.33(9) 2_655 2_655
Dy4 Dy3 Dy4 Dy3 48.344(12) 2_655 2_655
Dy2 Dy3 Dy4 Dy3 93.256(18) . 2_655
O5 Dy3 Dy4 Dy2 131.58(17) 2_655 2_655
O20 Dy3 Dy4 Dy2 -116.30(13) . 2_655
O37 Dy3 Dy4 Dy2 34.94(10) 2_655 2_655
O33 Dy3 Dy4 Dy2 -176.78(10) . 2_655
O36 Dy3 Dy4 Dy2 35.8(11) . 2_655
O17 Dy3 Dy4 Dy2 -50.46(12) . 2_655
O37 Dy3 Dy4 Dy2 -14.36(16) . 2_655
O6 Dy3 Dy4 Dy2 106.93(9) 2_655 2_655
Dy4 Dy3 Dy4 Dy2 68.947(16) 2_655 2_655
Dy2 Dy3 Dy4 Dy2 113.859(16) . 2_655
Dy3 Dy3 Dy4 Dy2 20.604(8) 2_655 2_655
C24 C19 C20 C21 0.0 . .
C18 C19 C20 C21 168.4(15) . .
C19 C20 C21 C22 0.0 . .
C20 C21 C22 C23 0.0 . .
C20 C21 C22 N1 -177.0(14) . .
O10 N1 C22 C21 168.8(15) . .
O11 N1 C22 C21 -12(3) . .
O10 N1 C22 C23 -8(2) . .
O11 N1 C22 C23 171(2) . .
C21 C22 C23 C24 0.0 . .
N1 C22 C23 C24 177.0(13) . .
C22 C23 C24 C19 0.0 . .
C20 C19 C24 C23 0.0 . .
C18 C19 C24 C23 -168.1(16) . .
C24' C19' C20' C21' 0.0 . .
C18 C19' C20' C21' 178.4(14) . .
C19' C20' C21' C22' 0.0 . .
C20' C21' C22' C23' 0.0 . .
C20' C21' C22' N1' -176.4(12) . .
O11' N1' C22' C23' -160.4(14) . .
O10' N1' C22' C23' 21(2) . .
O11' N1' C22' C21' 16(2) . .
O10' N1' C22' C21' -163.1(13) . .
C21' C22' C23' C24' 0.0 . .
N1' C22' C23' C24' 176.4(12) . .
C22' C23' C24' C19' 0.0 . .
C20' C19' C24' C23' 0.0 . .
C18 C19' C24' C23' -178.5(13) . .
C66 C61 C62 C63 0.0 . .
C60 C61 C62 C63 179.9(18) . .
C61 C62 C63 C64 0.0 . .
C62 C63 C64 C65 0.0 . .
C62 C63 C64 N7 -178.6(15) . .
O34 N7 C64 C63 -20(2) . .
O35 N7 C64 C63 164.4(16) . .
O34 N7 C64 C65 161.6(16) . .
O35 N7 C64 C65 -14(2) . .
C63 C64 C65 C66 0.0 . .
N7 C64 C65 C66 178.5(16) . .
C64 C65 C66 C61 0.0 . .
C62 C61 C66 C65 0.0 . .
C60 C61 C66 C65 -179.9(17) . .
C66' C61' C62' C63' 0.0 . .
C60 C61' C62' C63' 176.8(14) . .
C61' C62' C63' C64' 0.0 . .
C62' C63' C64' C65' 0.0 . .
C62' C63' C64' N7' 179.1(13) . .
O35' N7' C64' C63' -171.4(13) . .
O34' N7' C64' C63' -2(2) . .
O35' N7' C64' C65' 8(2) . .
O34' N7' C64' C65' 176.8(13) . .
C63' C64' C65' C66' 0.0 . .
N7' C64' C65' C66' -179.1(13) . .
C64' C65' C66' C61' 0.0 . .
C62' C61' C66' C65' 0.0 . .
C60 C61' C66' C65' -176.8(14) . .
O5 Dy3 O36 Dy2 -3.7(3) 2_655 .
O20 Dy3 O36 Dy2 -124.12(17) . .
O37 Dy3 O36 Dy2 85.86(16) 2_655 .
O33 Dy3 O36 Dy2 -63.18(16) . .
O17 Dy3 O36 Dy2 172.27(19) . .
O37 Dy3 O36 Dy2 130.30(18) . .
O6 Dy3 O36 Dy2 12.40(14) 2_655 .
Dy4 Dy3 O36 Dy2 85.0(11) . .
Dy4 Dy3 O36 Dy2 51.47(12) 2_655 .
Dy3 Dy3 O36 Dy2 99.51(14) 2_655 .
O5 Dy3 O36 Dy1 120.6(2) 2_655 .
O20 Dy3 O36 Dy1 0.1(2) . .
O37 Dy3 O36 Dy1 -149.9(2) 2_655 .
O33 Dy3 O36 Dy1 61.09(18) . .
O17 Dy3 O36 Dy1 -63.46(19) . .
O37 Dy3 O36 Dy1 -105.4(2) . .
O6 Dy3 O36 Dy1 136.7(2) 2_655 .
Dy4 Dy3 O36 Dy1 -150.8(9) . .
Dy4 Dy3 O36 Dy1 175.74(18) 2_655 .
Dy2 Dy3 O36 Dy1 124.3(3) . .
Dy3 Dy3 O36 Dy1 -136.22(13) 2_655 .
O2 Dy2 O36 Dy3 112.39(18) . .
O13 Dy2 O36 Dy3 -164.11(18) . .
O29 Dy2 O36 Dy3 -61.7(3) 2_655 .
O3 Dy2 O36 Dy3 53.3(2) . .
O6 Dy2 O36 Dy3 -12.92(15) 2_655 .
O41 Dy2 O36 Dy3 149.16(18) . .
O24 Dy2 O36 Dy3 -88.35(17) 2_655 .
Dy1 Dy2 O36 Dy3 129.4(2) . .
Dy4 Dy2 O36 Dy3 -51.14(12) 2_655 .
O2 Dy2 O36 Dy1 -17.06(14) . .
O13 Dy2 O36 Dy1 66.44(16) . .
O29 Dy2 O36 Dy1 168.87(18) 2_655 .
O3 Dy2 O36 Dy1 -76.18(19) . .
O6 Dy2 O36 Dy1 -142.37(18) 2_655 .
O41 Dy2 O36 Dy1 19.7(3) . .
O24 Dy2 O36 Dy1 142.21(17) 2_655 .
Dy3 Dy2 O36 Dy1 -129.4(2) . .
Dy4 Dy2 O36 Dy1 179.42(15) 2_655 .
O16 Dy1 O36 Dy3 60.4(2) . .
O32 Dy1 O36 Dy3 -31.32(19) . .
O12 Dy1 O36 Dy3 162.7(2) . .
O8 Dy1 O36 Dy3 118.1(2) . .
O2 Dy1 O36 Dy3 -107.6(2) . .
O9 Dy1 O36 Dy3 17.9(4) . .
O1 Dy1 O36 Dy3 -115.26(19) . .
C18 Dy1 O36 Dy3 76.8(4) . .
Dy2 Dy1 O36 Dy3 -124.3(3) . .
O16 Dy1 O36 Dy2 -175.26(19) . .
O32 Dy1 O36 Dy2 92.99(17) . .
O12 Dy1 O36 Dy2 -72.99(16) . .
O8 Dy1 O36 Dy2 -117.61(19) . .
O2 Dy1 O36 Dy2 16.66(14) . .
O9 Dy1 O36 Dy2 142.2(2) . .
O1 Dy1 O36 Dy2 9.1(2) . .
C18 Dy1 O36 Dy2 -158.9(3) . .
O16 Dy1 O1 C2 -130.2(4) . .
O32 Dy1 O1 C2 -41.0(4) . .
O12 Dy1 O1 C2 117.5(4) . .
O36 Dy1 O1 C2 41.7(4) . .
O8 Dy1 O1 C2 -171.6(4) . .
O2 Dy1 O1 C2 33.9(3) . .
O9 Dy1 O1 C2 -115.2(4) . .
C18 Dy1 O1 C2 -143.6(4) . .
Dy2 Dy1 O1 C2 47.0(4) . .
O16 Dy1 O1 C1 27.6(6) . .
O32 Dy1 O1 C1 116.7(5) . .
O12 Dy1 O1 C1 -84.7(5) . .
O36 Dy1 O1 C1 -160.5(4) . .
O8 Dy1 O1 C1 -13.8(5) . .
O2 Dy1 O1 C1 -168.4(5) . .
O9 Dy1 O1 C1 42.6(5) . .
C18 Dy1 O1 C1 14.2(5) . .
Dy2 Dy1 O1 C1 -155.2(5) . .
O13 Dy2 O2 C7 127.2(5) . .
O29 Dy2 O2 C7 24.9(6) 2_655 .
O36 Dy2 O2 C7 -149.5(5) . .
O3 Dy2 O2 C7 -22.6(5) . .
O6 Dy2 O2 C7 -88.9(5) 2_655 .
O41 Dy2 O2 C7 55.1(5) . .
O24 Dy2 O2 C7 177.6(4) 2_655 .
Dy3 Dy2 O2 C7 -116.9(5) . .
Dy1 Dy2 O2 C7 -166.4(6) . .
Dy4 Dy2 O2 C7 -120.3(4) 2_655 .
O13 Dy2 O2 Dy1 -66.45(16) . .
O29 Dy2 O2 Dy1 -168.73(17) 2_655 .
O36 Dy2 O2 Dy1 16.89(14) . .
O3 Dy2 O2 Dy1 143.82(18) . .
O6 Dy2 O2 Dy1 77.51(18) 2_655 .
O41 Dy2 O2 Dy1 -138.50(18) . .
O24 Dy2 O2 Dy1 -16.0(3) 2_655 .
Dy3 Dy2 O2 Dy1 49.51(12) . .
Dy4 Dy2 O2 Dy1 46.0(2) 2_655 .
O16 Dy1 O2 C7 130.3(4) . .
O32 Dy1 O2 C7 61.0(4) . .
O12 Dy1 O2 C7 -128.9(4) . .
O36 Dy1 O2 C7 152.1(4) . .
O8 Dy1 O2 C7 -71.5(4) . .
O9 Dy1 O2 C7 3.5(4) . .
O1 Dy1 O2 C7 -34.3(4) . .
C18 Dy1 O2 C7 -30.8(5) . .
Dy2 Dy1 O2 C7 169.1(5) . .
O16 Dy1 O2 Dy2 -38.8(3) . .
O32 Dy1 O2 Dy2 -108.12(18) . .
O12 Dy1 O2 Dy2 61.98(16) . .
O36 Dy1 O2 Dy2 -16.99(14) . .
O8 Dy1 O2 Dy2 119.42(18) . .
O9 Dy1 O2 Dy2 -165.58(13) . .
O1 Dy1 O2 Dy2 156.6(2) . .
C18 Dy1 O2 Dy2 160.2(2) . .
O2 Dy2 O3 C8 11.9(5) . .
O13 Dy2 O3 C8 -40.1(6) . .
O29 Dy2 O3 C8 -142.2(5) 2_655 .
O36 Dy2 O3 C8 68.5(5) . .
O6 Dy2 O3 C8 133.6(5) 2_655 .
O41 Dy2 O3 C8 -67.4(5) . .
O24 Dy2 O3 C8 171.2(5) 2_655 .
Dy3 Dy2 O3 C8 96.3(5) . .
Dy1 Dy2 O3 C8 32.8(5) . .
Dy4 Dy2 O3 C8 155.4(5) 2_655 .
O37 Dy4 O6 C16 -138.7(3) . .
O21 Dy4 O6 C16 169.7(3) . .
O5 Dy4 O6 C16 -73.6(3) 2_655 .
O28 Dy4 O6 C16 62.7(3) . .
O24 Dy4 O6 C16 138.4(3) . .
O7 Dy4 O6 C16 -10.6(3) . .
O4 Dy4 O6 C16 -6.2(4) 2_655 .
Dy3 Dy4 O6 C16 -109.8(3) . .
Dy3 Dy4 O6 C16 -128.8(4) 2_655 .
Dy2 Dy4 O6 C16 126.0(4) 2_655 .
O37 Dy4 O6 Dy2 95.22(16) . 2_655
O21 Dy4 O6 Dy2 43.7(3) . 2_655
O5 Dy4 O6 Dy2 160.36(14) 2_655 2_655
O28 Dy4 O6 Dy2 -63.35(16) . 2_655
O24 Dy4 O6 Dy2 12.33(13) . 2_655
O7 Dy4 O6 Dy2 -136.7(2) . 2_655
O4 Dy4 O6 Dy2 -132.25(17) 2_655 2_655
C16 Dy4 O6 Dy2 -126.0(4) . 2_655
Dy3 Dy4 O6 Dy2 124.16(11) . 2_655
Dy3 Dy4 O6 Dy2 105.21(18) 2_655 2_655
O37 Dy4 O6 Dy3 -9.99(13) . 2_655
O21 Dy4 O6 Dy3 -61.5(3) . 2_655
O5 Dy4 O6 Dy3 55.14(15) 2_655 2_655
O28 Dy4 O6 Dy3 -168.56(15) . 2_655
O24 Dy4 O6 Dy3 -92.88(15) . 2_655
O7 Dy4 O6 Dy3 118.13(19) . 2_655
O4 Dy4 O6 Dy3 122.54(17) 2_655 2_655
C16 Dy4 O6 Dy3 128.8(4) . 2_655
Dy3 Dy4 O6 Dy3 18.95(12) . 2_655
Dy2 Dy4 O6 Dy3 -105.21(18) 2_655 2_655
O37 Dy4 O7 C17 -158.3(5) . .
O21 Dy4 O7 C17 -32.7(7) . .
O5 Dy4 O7 C17 -96.1(5) 2_655 .
O28 Dy4 O7 C17 50.3(5) . .
O24 Dy4 O7 C17 112.8(5) . .
O6 Dy4 O7 C17 147.8(6) . .
O4 Dy4 O7 C17 -29.2(5) 2_655 .
C16 Dy4 O7 C17 137.7(7) . .
Dy3 Dy4 O7 C17 -118.9(5) . .
Dy3 Dy4 O7 C17 -176.4(5) 2_655 .
Dy2 Dy4 O7 C17 123.2(5) 2_655 .
O37 Dy4 O7 C16 64.0(3) . .
O21 Dy4 O7 C16 -170.4(4) . .
O5 Dy4 O7 C16 126.1(3) 2_655 .
O28 Dy4 O7 C16 -87.4(3) . .
O24 Dy4 O7 C16 -24.9(3) . .
O6 Dy4 O7 C16 10.1(3) . .
O4 Dy4 O7 C16 -166.9(3) 2_655 .
Dy3 Dy4 O7 C16 103.4(3) . .
Dy3 Dy4 O7 C16 45.9(3) 2_655 .
Dy2 Dy4 O7 C16 -14.5(3) 2_655 .
O16 Dy1 O8 C18 -83.3(4) . .
O32 Dy1 O8 C18 -3.5(4) . .
O12 Dy1 O8 C18 171.1(4) . .
O36 Dy1 O8 C18 -142.5(3) . .
O2 Dy1 O8 C18 108.8(4) . .
O9 Dy1 O8 C18 -0.5(3) . .
O1 Dy1 O8 C18 75.6(4) . .
Dy2 Dy1 O8 C18 161.7(3) . .
O16 Dy1 O9 C18 83.0(4) . .
O32 Dy1 O9 C18 178.1(4) . .
O12 Dy1 O9 C18 -9.4(4) . .
O36 Dy1 O9 C18 126.4(4) . .
O8 Dy1 O9 C18 0.5(4) . .
O2 Dy1 O9 C18 -123.9(4) . .
O1 Dy1 O9 C18 -88.8(4) . .
Dy2 Dy1 O9 C18 -147.3(3) . .
O16 Dy1 O12 C25 120.4(5) . .
O32 Dy1 O12 C25 0.7(8) . .
O36 Dy1 O12 C25 42.1(5) . .
O8 Dy1 O12 C25 -167.9(6) . .
O2 Dy1 O12 C25 -26.4(5) . .
O9 Dy1 O12 C25 -159.4(5) . .
O1 Dy1 O12 C25 -89.4(5) . .
C18 Dy1 O12 C25 -163.7(5) . .
Dy2 Dy1 O12 C25 5.9(5) . .
O2 Dy2 O13 C25 52.5(6) . .
O29 Dy2 O13 C25 -163.9(6) 2_655 .
O36 Dy2 O13 C25 -18.0(6) . .
O3 Dy2 O13 C25 102.6(6) . .
O6 Dy2 O13 C25 -67.3(6) 2_655 .
O41 Dy2 O13 C25 130.6(6) . .
O24 Dy2 O13 C25 -96.9(6) 2_655 .
Dy3 Dy2 O13 C25 -28.1(6) . .
Dy1 Dy2 O13 C25 17.1(5) . .
Dy4 Dy2 O13 C25 -93.1(6) 2_655 .
O32 Dy1 O16 C32 50.4(6) . .
O12 Dy1 O16 C32 -111.1(6) . .
O36 Dy1 O16 C32 -35.1(6) . .
O8 Dy1 O16 C32 -179.1(7) . .
O2 Dy1 O16 C32 -14.7(8) . .
O9 Dy1 O16 C32 124.0(6) . .
O1 Dy1 O16 C32 138.7(6) . .
C18 Dy1 O16 C32 152.2(7) . .
Dy2 Dy1 O16 C32 -38.2(7) . .
O5 Dy3 O17 C32 -134.3(5) 2_655 .
O20 Dy3 O17 C32 -75.9(6) . .
O37 Dy3 O17 C32 131.4(6) 2_655 .
O33 Dy3 O17 C32 -18.2(6) . .
O36 Dy3 O17 C32 49.1(5) . .
O37 Dy3 O17 C32 -157.5(6) . .
O6 Dy3 O17 C32 83.7(6) 2_655 .
Dy4 Dy3 O17 C32 -136.1(5) . .
Dy4 Dy3 O17 C32 121.6(5) 2_655 .
Dy2 Dy3 O17 C32 54.0(6) . .
Dy3 Dy3 O17 C32 167.3(6) 2_655 .
O5 Dy3 O20 C39 42.2(7) 2_655 .
O37 Dy3 O20 C39 -48.5(8) 2_655 .
O33 Dy3 O20 C39 128.5(7) . .
O36 Dy3 O20 C39 -168.2(7) . .
O17 Dy3 O20 C39 -101.9(7) . .
O37 Dy3 O20 C39 -27.2(7) . .
O6 Dy3 O20 C39 95.8(7) 2_655 .
Dy4 Dy3 O20 C39 9.0(7) . .
Dy4 Dy3 O20 C39 24.9(10) 2_655 .
Dy2 Dy3 O20 C39 150.7(6) . .
Dy3 Dy3 O20 C39 -30.7(7) 2_655 .
O37 Dy4 O21 C39 45.2(5) . .
O5 Dy4 O21 C39 -24.3(5) 2_655 .
O28 Dy4 O21 C39 -162.3(5) . .
O24 Dy4 O21 C39 125.2(5) . .
O7 Dy4 O21 C39 -84.6(6) . .
O6 Dy4 O21 C39 94.7(5) . .
O4 Dy4 O21 C39 -88.2(5) 2_655 .
C16 Dy4 O21 C39 131.1(10) . .
Dy3 Dy4 O21 C39 7.0(4) . .
Dy3 Dy4 O21 C39 54.4(5) 2_655 .
Dy2 Dy4 O21 C39 122.1(4) 2_655 .
O37 Dy4 O24 C46 59.5(4) . .
O21 Dy4 O24 C46 -26.2(4) . .
O5 Dy4 O24 C46 51.1(5) 2_655 .
O28 Dy4 O24 C46 -131.4(4) . .
O7 Dy4 O24 C46 166.4(4) . .
O6 Dy4 O24 C46 136.7(4) . .
O4 Dy4 O24 C46 -78.8(4) 2_655 .
C16 Dy4 O24 C46 154.6(4) . .
Dy3 Dy4 O24 C46 43.0(4) . .
Dy3 Dy4 O24 C46 95.1(4) 2_655 .
Dy2 Dy4 O24 C46 149.1(5) 2_655 .
O37 Dy4 O24 Dy2 -89.54(16) . 2_655
O21 Dy4 O24 Dy2 -175.26(17) . 2_655
O5 Dy4 O24 Dy2 -97.9(3) 2_655 2_655
O28 Dy4 O24 Dy2 79.51(16) . 2_655
O7 Dy4 O24 Dy2 17.3(2) . 2_655
O6 Dy4 O24 Dy2 -12.34(13) . 2_655
O4 Dy4 O24 Dy2 132.12(18) 2_655 2_655
C16 Dy4 O24 Dy2 5.55(17) . 2_655
Dy3 Dy4 O24 Dy2 -106.07(12) . 2_655
Dy3 Dy4 O24 Dy2 -53.98(11) 2_655 2_655
O37 Dy4 O28 C53 -4.9(7) . .
O21 Dy4 O28 C53 -102.9(5) . .
O5 Dy4 O28 C53 149.5(5) 2_655 .
O24 Dy4 O28 C53 -28.6(5) . .
O7 Dy4 O28 C53 99.5(5) . .
O6 Dy4 O28 C53 44.5(5) . .
O4 Dy4 O28 C53 -175.5(5) 2_655 .
C16 Dy4 O28 C53 69.6(5) . .
Dy3 Dy4 O28 C53 -179.7(4) . .
Dy3 Dy4 O28 C53 35.1(6) 2_655 .
Dy2 Dy4 O28 C53 10.0(5) 2_655 .
O16 Dy1 O32 C60 -115.2(5) . .
O12 Dy1 O32 C60 6.0(8) . .
O36 Dy1 O32 C60 -34.4(5) . .
O8 Dy1 O32 C60 172.0(5) . .
O2 Dy1 O32 C60 34.0(5) . .
O9 Dy1 O32 C60 169.4(6) . .
O1 Dy1 O32 C60 96.8(5) . .
C18 Dy1 O32 C60 170.3(5) . .
Dy2 Dy1 O32 C60 1.1(5) . .
O5 Dy3 O33 C60 132.2(4) 2_655 .
O20 Dy3 O33 C60 48.4(4) . .
O37 Dy3 O33 C60 -134.3(4) 2_655 .
O36 Dy3 O33 C60 -78.1(4) . .
O17 Dy3 O33 C60 -9.8(5) . .
O37 Dy3 O33 C60 88.2(5) . .
O6 Dy3 O33 C60 -153.5(4) 2_655 .
Dy4 Dy3 O33 C60 104.7(4) . .
Dy4 Dy3 O33 C60 -152.0(4) 2_655 .
Dy2 Dy3 O33 C60 -113.5(4) . .
Dy3 Dy3 O33 C60 154.2(3) 2_655 .
O2 Dy2 O41 C74 -123.6(6) . .
O13 Dy2 O41 C74 151.5(6) . .
O29 Dy2 O41 C74 38.4(6) 2_655 .
O36 Dy2 O41 C74 -158.9(5) . .
O3 Dy2 O41 C74 -46.4(6) . .
O6 Dy2 O41 C74 -9.6(7) 2_655 .
O24 Dy2 O41 C74 95.3(6) 2_655 .
Dy3 Dy2 O41 C74 -100.1(6) . .
Dy1 Dy2 O41 C74 -147.2(6) . .
Dy4 Dy2 O41 C74 52.5(6) 2_655 .
O21 Dy4 O37 Dy3 165.64(18) . 2_655
O5 Dy4 O37 Dy3 -97.98(18) 2_655 2_655
O28 Dy4 O37 Dy3 63.3(4) . 2_655
O24 Dy4 O37 Dy3 86.65(17) . 2_655
O7 Dy4 O37 Dy3 -32.3(2) . 2_655
O6 Dy4 O37 Dy3 11.43(15) . 2_655
O4 Dy4 O37 Dy3 -128.61(17) 2_655 2_655
C16 Dy4 O37 Dy3 -6.37(19) . 2_655
Dy3 Dy4 O37 Dy3 -118.2(2) . 2_655
Dy2 Dy4 O37 Dy3 48.97(13) 2_655 2_655
O21 Dy4 O37 Dy3 -76.12(16) . .
O5 Dy4 O37 Dy3 20.27(14) 2_655 .
O28 Dy4 O37 Dy3 -178.5(2) . .
O24 Dy4 O37 Dy3 -155.10(17) . .
O7 Dy4 O37 Dy3 85.94(17) . .
O6 Dy4 O37 Dy3 129.68(17) . .
O4 Dy4 O37 Dy3 -10.4(2) 2_655 .
C16 Dy4 O37 Dy3 111.88(16) . .
Dy3 Dy4 O37 Dy3 118.2(2) 2_655 .
Dy2 Dy4 O37 Dy3 167.21(14) 2_655 .
O5 Dy3 O37 Dy4 -20.66(14) 2_655 .
O20 Dy3 O37 Dy4 66.08(17) . .
O37 Dy3 O37 Dy4 -126.59(11) 2_655 .
O33 Dy3 O37 Dy4 27.4(3) . .
O36 Dy3 O37 Dy4 -173.86(15) . .
O17 Dy3 O37 Dy4 142.57(19) . .
O6 Dy3 O37 Dy4 -73.68(18) 2_655 .
Dy4 Dy3 O37 Dy4 -98.63(13) 2_655 .
Dy2 Dy3 O37 Dy4 -110.92(16) . .
Dy3 Dy3 O37 Dy4 -119.6(2) 2_655 .
O5 Dy3 O37 Dy3 98.93(18) 2_655 2_655
O20 Dy3 O37 Dy3 -174.33(19) . 2_655
O37 Dy3 O37 Dy3 -7.0(2) 2_655 2_655
O33 Dy3 O37 Dy3 146.98(17) . 2_655
O36 Dy3 O37 Dy3 -54.3(3) . 2_655
O17 Dy3 O37 Dy3 -97.84(18) . 2_655
O6 Dy3 O37 Dy3 45.9(2) 2_655 2_655
Dy4 Dy3 O37 Dy3 119.6(2) . 2_655
Dy4 Dy3 O37 Dy3 20.96(14) 2_655 2_655
Dy2 Dy3 O37 Dy3 8.7(3) . 2_655
C1 O1 C2 C3 -13.2(9) . .
Dy1 O1 C2 C3 147.7(5) . .
C1 O1 C2 C7 167.7(5) . .
Dy1 O1 C2 C7 -31.5(6) . .
O1 C2 C3 C4 -177.6(6) . .
C7 C2 C3 C4 1.5(10) . .
C2 C3 C4 C5 0.0(11) . .
C3 C4 C5 C6 -1.4(11) . .
C4 C5 C6 C7 1.3(10) . .
C4 C5 C6 C8 177.7(6) . .
Dy2 O2 C7 C2 -162.0(4) . .
Dy1 O2 C7 C2 32.3(6) . .
Dy2 O2 C7 C6 22.0(8) . .
Dy1 O2 C7 C6 -143.7(5) . .
C3 C2 C7 O2 -177.9(6) . .
O1 C2 C7 O2 1.3(8) . .
C3 C2 C7 C6 -1.5(9) . .
O1 C2 C7 C6 177.7(5) . .
C5 C6 C7 O2 176.2(5) . .
C8 C6 C7 O2 0.0(9) . .
C5 C6 C7 C2 0.1(9) . .
C8 C6 C7 C2 -176.1(6) . .
Dy2 O3 C8 C6 -0.3(9) . .
C5 C6 C8 O3 173.0(6) . .
C7 C6 C8 O3 -10.6(10) . .
C9 O4 C10 C11 -19.0(9) . .
Dy4 O4 C10 C11 166.4(5) 2_655 .
C9 O4 C10 C15 162.9(5) . .
Dy4 O4 C10 C15 -11.7(6) 2_655 .
O4 C10 C11 C12 -177.6(6) . .
C15 C10 C11 C12 0.3(10) . .
C10 C11 C12 C13 1.0(10) . .
C11 C12 C13 C14 -0.3(10) . .
C12 C13 C14 C15 -1.7(10) . .
C12 C13 C14 C16 170.8(6) . .
Dy3 O5 C15 C14 52.9(7) 2_655 .
Dy4 O5 C15 C14 -159.9(4) 2_655 .
Dy3 O5 C15 C10 -126.3(5) 2_655 .
Dy4 O5 C15 C10 20.9(7) 2_655 .
C13 C14 C15 O5 -176.2(6) . .
C16 C14 C15 O5 11.4(9) . .
C13 C14 C15 C10 2.9(9) . .
C16 C14 C15 C10 -169.5(5) . .
C11 C10 C15 O5 176.9(6) . .
O4 C10 C15 O5 -4.9(8) . .
C11 C10 C15 C14 -2.3(9) . .
O4 C10 C15 C14 175.9(5) . .
Dy2 O6 C16 O7 129.1(3) 2_655 .
Dy4 O6 C16 O7 14.9(4) . .
Dy3 O6 C16 O7 -95.1(4) 2_655 .
Dy2 O6 C16 C14 -111.8(5) 2_655 .
Dy4 O6 C16 C14 134.0(5) . .
Dy3 O6 C16 C14 24.0(7) 2_655 .
Dy2 O6 C16 Dy4 114.2(3) 2_655 .
Dy3 O6 C16 Dy4 -110.0(4) 2_655 .
C17 O7 C16 O6 -162.5(5) . .
Dy4 O7 C16 O6 -15.1(4) . .
C17 O7 C16 C14 71.9(6) . .
Dy4 O7 C16 C14 -140.7(4) . .
C17 O7 C16 Dy4 -147.4(5) . .
C15 C14 C16 O6 -49.4(8) . .
C13 C14 C16 O6 138.2(6) . .
C15 C14 C16 O7 67.6(7) . .
C13 C14 C16 O7 -104.8(6) . .
C15 C14 C16 Dy4 15.5(9) . .
C13 C14 C16 Dy4 -156.9(5) . .
O37 Dy4 C16 O6 39.7(3) . .
O21 Dy4 C16 O6 -45.3(12) . .
O5 Dy4 C16 O6 110.0(3) 2_655 .
O28 Dy4 C16 O6 -113.6(3) . .
O24 Dy4 C16 O6 -39.6(3) . .
O7 Dy4 C16 O6 161.7(5) . .
O4 Dy4 C16 O6 175.5(3) 2_655 .
Dy3 Dy4 C16 O6 76.9(3) . .
Dy3 Dy4 C16 O6 35.6(3) 2_655 .
Dy2 Dy4 C16 O6 -35.6(3) 2_655 .
O37 Dy4 C16 O7 -121.9(3) . .
O21 Dy4 C16 O7 153.0(10) . .
O5 Dy4 C16 O7 -51.6(3) 2_655 .
O28 Dy4 C16 O7 84.8(3) . .
O24 Dy4 C16 O7 158.7(3) . .
O6 Dy4 C16 O7 -161.7(5) . .
O4 Dy4 C16 O7 13.9(3) 2_655 .
Dy3 Dy4 C16 O7 -84.8(3) . .
Dy3 Dy4 C16 O7 -126.1(3) 2_655 .
Dy2 Dy4 C16 O7 162.7(3) 2_655 .
O37 Dy4 C16 C14 -50.7(6) . .
O21 Dy4 C16 C14 -135.7(10) . .
O5 Dy4 C16 C14 19.6(6) 2_655 .
O28 Dy4 C16 C14 156.0(6) . .
O24 Dy4 C16 C14 -130.0(6) . .
O7 Dy4 C16 C14 71.2(6) . .
O6 Dy4 C16 C14 -90.4(7) . .
O4 Dy4 C16 C14 85.1(6) 2_655 .
Dy3 Dy4 C16 C14 -13.6(6) . .
Dy3 Dy4 C16 C14 -54.9(6) 2_655 .
Dy2 Dy4 C16 C14 -126.0(6) 2_655 .
Dy1 O9 C18 O8 -0.9(6) . .
Dy1 O9 C18 C19' 178.1(10) . .
Dy1 O9 C18 C19 172.2(10) . .
Dy1 O8 C18 O9 0.9(6) . .
Dy1 O8 C18 C19' -178.1(9) . .
Dy1 O8 C18 C19 -172.1(10) . .
C20' C19' C18 O9 173.5(7) . .
C24' C19' C18 O9 -8.1(16) . .
C20' C19' C18 O8 -7.5(11) . .
C24' C19' C18 O8 171.0(8) . .
C20' C19' C18 C19 -130(14) . .
C24' C19' C18 C19 48(13) . .
C20' C19' C18 Dy1 -29(11) . .
C24' C19' C18 Dy1 150(10) . .
C20 C19 C18 O9 161.6(7) . .
C24 C19 C18 O9 -30.1(17) . .
C20 C19 C18 O8 -25.2(12) . .
C24 C19 C18 O8 143.1(10) . .
C20 C19 C18 C19' 35(14) . .
C24 C19 C18 C19' -157(15) . .
C20 C19 C18 Dy1 -105(7) . .
C24 C19 C18 Dy1 63(8) . .
O16 Dy1 C18 O9 -89.8(4) . .
O32 Dy1 C18 O9 -1.9(4) . .
O12 Dy1 C18 O9 172.4(3) . .
O36 Dy1 C18 O9 -106.6(5) . .
O8 Dy1 C18 O9 -179.1(6) . .
O2 Dy1 C18 O9 79.6(4) . .
O1 Dy1 C18 O9 82.9(4) . .
Dy2 Dy1 C18 O9 129.9(5) . .
O16 Dy1 C18 O8 89.3(4) . .
O32 Dy1 C18 O8 177.2(3) . .
O12 Dy1 C18 O8 -8.5(4) . .
O36 Dy1 C18 O8 72.5(5) . .
O2 Dy1 C18 O8 -101.3(4) . .
O9 Dy1 C18 O8 179.1(6) . .
O1 Dy1 C18 O8 -98.0(4) . .
Dy2 Dy1 C18 O8 -51.0(8) . .
O16 Dy1 C18 C19' 111(11) . .
O32 Dy1 C18 C19' -161(11) . .
O12 Dy1 C18 C19' 14(11) . .
O36 Dy1 C18 C19' 95(11) . .
O8 Dy1 C18 C19' 22(10) . .
O2 Dy1 C18 C19' -79(11) . .
O9 Dy1 C18 C19' -159(11) . .
O1 Dy1 C18 C19' -76(11) . .
Dy2 Dy1 C18 C19' -29(11) . .
O16 Dy1 C18 C19 174(8) . .
O32 Dy1 C18 C19 -99(8) . .
O12 Dy1 C18 C19 76(8) . .
O36 Dy1 C18 C19 157(7) . .
O8 Dy1 C18 C19 84(8) . .
O2 Dy1 C18 C19 -17(8) . .
O9 Dy1 C18 C19 -97(8) . .
O1 Dy1 C18 C19 -14(8) . .
Dy2 Dy1 C18 C19 33(8) . .
Dy2 O13 C25 O12 -19.9(10) . .
Dy2 O13 C25 C26 159.5(4) . .
Dy1 O12 C25 O13 3.0(10) . .
Dy1 O12 C25 C26 -176.5(4) . .
O13 C25 C26 C27 22.6(8) . .
O12 C25 C26 C27 -157.9(5) . .
O13 C25 C26 C31 -156.9(5) . .
O12 C25 C26 C31 22.6(8) . .
C31 C26 C27 C28 1.9(9) . .
C25 C26 C27 C28 -177.6(5) . .
C26 C27 C28 C29 -0.4(9) . .
C27 C28 C29 C30 -0.2(10) . .
C27 C28 C29 N2 178.3(6) . .
O14 N2 C29 C28 -19.0(9) . .
O15 N2 C29 C28 161.2(6) . .
O14 N2 C29 C30 159.6(6) . .
O15 N2 C29 C30 -20.2(9) . .
C28 C29 C30 C31 -0.6(10) . .
N2 C29 C30 C31 -179.2(5) . .
C29 C30 C31 C26 2.1(9) . .
C27 C26 C31 C30 -2.7(9) . .
C25 C26 C31 C30 176.8(5) . .
Dy3 O17 C32 O16 -30.6(9) . .
Dy3 O17 C32 C33 150.8(4) . .
Dy1 O16 C32 O17 21.3(10) . .
Dy1 O16 C32 C33 -160.2(4) . .
O17 C32 C33 C34 11.4(8) . .
O16 C32 C33 C34 -167.3(6) . .
O17 C32 C33 C38 -167.5(6) . .
O16 C32 C33 C38 13.8(8) . .
C38 C33 C34 C35 -1.5(9) . .
C32 C33 C34 C35 179.7(6) . .
C33 C34 C35 C36 0.2(10) . .
C34 C35 C36 C37 1.6(10) . .
C34 C35 C36 N3 179.6(6) . .
O19 N3 C36 C35 -175.6(6) . .
O18 N3 C36 C35 6.1(9) . .
O19 N3 C36 C37 2.4(9) . .
O18 N3 C36 C37 -175.9(6) . .
C35 C36 C37 C38 -2.1(10) . .
N3 C36 C37 C38 179.9(6) . .
C36 C37 C38 C33 0.8(10) . .
C34 C33 C38 C37 1.0(10) . .
C32 C33 C38 C37 179.8(6) . .
Dy3 O20 C39 O21 -6.8(11) . .
Dy3 O20 C39 C40 175.0(5) . .
Dy4 O21 C39 O20 -4.8(9) . .
Dy4 O21 C39 C40 173.4(4) . .
O20 C39 C40 C41 176.0(6) . .
O21 C39 C40 C41 -2.4(9) . .
O20 C39 C40 C45 -2.7(9) . .
O21 C39 C40 C45 178.9(6) . .
C45 C40 C41 C42 0.0(10) . .
C39 C40 C41 C42 -178.7(6) . .
C40 C41 C42 C43 -0.2(10) . .
C41 C42 C43 C44 0.8(11) . .
C41 C42 C43 N4 -179.0(6) . .
O23 N4 C43 C42 -171.8(7) . .
O22 N4 C43 C42 7.2(11) . .
O23 N4 C43 C44 8.4(11) . .
O22 N4 C43 C44 -172.6(7) . .
C42 C43 C44 C45 -1.2(12) . .
N4 C43 C44 C45 178.6(7) . .
C43 C44 C45 C40 0.9(11) . .
C41 C40 C45 C44 -0.4(11) . .
C39 C40 C45 C44 178.3(6) . .
Dy4 O24 C46 O25 -77.0(7) . .
Dy2 O24 C46 O25 66.8(7) 2_655 .
Dy4 O24 C46 C47 106.0(5) . .
Dy2 O24 C46 C47 -110.2(5) 2_655 .
O25 C46 C47 C48 -170.0(7) . .
O24 C46 C47 C48 7.1(9) . .
O25 C46 C47 C52 7.5(9) . .
O24 C46 C47 C52 -175.3(5) . .
C52 C47 C48 C49 0.3(13) . .
C46 C47 C48 C49 177.9(8) . .
C47 C48 C49 C50 -1.0(15) . .
C48 C49 C50 C51 1.4(14) . .
C48 C49 C50 N5 -178.6(8) . .
O26 N5 C50 C51 -4.9(10) . .
O27 N5 C50 C51 160.3(16) . .
O27' N5 C50 C51 -163(2) . .
O26 N5 C50 C49 175.1(8) . .
O27 N5 C50 C49 -19.6(18) . .
O27' N5 C50 C49 17(3) . .
C49 C50 C51 C52 -1.1(12) . .
N5 C50 C51 C52 178.9(6) . .
C48 C47 C52 C51 -0.1(10) . .
C46 C47 C52 C51 -177.6(6) . .
C50 C51 C52 C47 0.4(10) . .
Dy4 O28 C53 O29 -26.4(9) . .
Dy4 O28 C53 C54 152.2(4) . .
Dy2 O29 C53 O28 33.9(9) 2_655 .
Dy2 O29 C53 C54 -144.6(4) 2_655 .
O28 C53 C54 C55 -154.7(6) . .
O29 C53 C54 C55 24.0(9) . .
O28 C53 C54 C59 21.2(9) . .
O29 C53 C54 C59 -160.2(6) . .
Dy3 O33 C60 O32 37.1(7) . .
Dy3 O33 C60 C61 -147.7(10) . .
Dy3 O33 C60 C61' -138.7(9) . .
Dy1 O32 C60 O33 38.0(9) . .
Dy1 O32 C60 C61 -136.7(11) . .
Dy1 O32 C60 C61' -145.8(8) . .
C62 C61 C60 O33 -177.2(7) . .
C66 C61 C60 O33 2.8(15) . .
C62 C61 C60 O32 -1.9(16) . .
C66 C61 C60 O32 178.0(7) . .
C62 C61 C60 C61' 47(7) . .
C66 C61 C60 C61' -133(8) . .
C62' C61' C60 O33 -179.0(6) . .
C66' C61' C60 O33 -2.2(14) . .
C62' C61' C60 O32 4.8(11) . .
C66' C61' C60 O32 -178.5(7) . .
C62' C61' C60 C61 -131(8) . .
C66' C61' C60 C61 46(7) . .
C59 C54 C55 C56 -1.7(10) . .
C53 C54 C55 C56 174.2(6) . .
C54 C55 C56 C57 -0.2(11) . .
C55 C56 C57 C58 2.2(13) . .
C55 C56 C57 N6 -177.7(7) . .
O30' N6 C57 C56 -173.9(13) . .
O31 N6 C57 C56 -34.8(18) . .
O30 N6 C57 C56 156.2(14) . .
O31' N6 C57 C56 6.1(16) . .
O30' N6 C57 C58 6.2(16) . .
O31 N6 C57 C58 145.3(15) . .
O30 N6 C57 C58 -23.7(18) . .
O31' N6 C57 C58 -173.8(13) . .
C56 C57 C58 C59 -2.3(14) . .
N6 C57 C58 C59 177.6(8) . .
C55 C54 C59 C58 1.6(11) . .
C53 C54 C59 C58 -174.3(7) . .
C57 C58 C59 C54 0.4(13) . .
