#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:45:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179346 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/43/4324381.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4324381
loop_
_publ_author_name
'Feng Li'
'Jack K. Clegg'
'David Price'
'Cameron J. Kepert'
_publ_section_title
;
 Self-Assembly of a Metallomacrocycle Templated by Iron(II)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              726
_journal_page_last               728
_journal_paper_doi               10.1021/ic102350t
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety
'C84 H68 Ag3 F24 Fe N24 O1, 4(P F6),Cl O4, (C2 H6 O)'
_chemical_formula_sum            'C86 H74 Ag3 Cl F24 Fe N24 O6 P4'
_chemical_formula_weight         2534.48
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           60
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   28.038(3)
_cell_length_b                   22.370(2)
_cell_length_c                   30.391(4)
_cell_measurement_reflns_used    1580
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      16.18
_cell_measurement_theta_min      2.913
_cell_volume                     19062(4)
_computing_cell_refinement       'SAINT (Bruker-Nonius, 2003)'
_computing_data_collection       'APEX (Bruker-Nonius, 2003)'
_computing_data_reduction
'SAINT (Bruker-Nonius, 2003), XPREP (Bruker-Nonius, 2003)'
_computing_molecular_graphics
;ORTEP-3 (Farrugia, 1997)
WINGX-32 (Farrugia, 1999) 
;
_computing_publication_material  'enCIFer 1.1 (CCDC, 2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR97 (Altomare, et. al. 1999)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  APEXII-FR591
_diffrn_measurement_method       ω+φ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1803
_diffrn_reflns_av_sigmaI/netI    0.2010
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            44939
_diffrn_reflns_theta_full        21.44
_diffrn_reflns_theta_max         21.44
_diffrn_reflns_theta_min         1.78
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.966
_exptl_absorpt_correction_T_max  0.7446
_exptl_absorpt_correction_T_min  0.5777
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2007)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.766
_exptl_crystal_description       needle
_exptl_crystal_F_000             10128
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.050
_exptl_crystal_size_min          0.010
_refine_diff_density_max         1.345
_refine_diff_density_min         -1.236
_refine_diff_density_rms         0.188
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1176
_refine_ls_number_reflns         10824
_refine_ls_number_restraints     458
_refine_ls_restrained_S_all      1.015
_refine_ls_R_factor_all          0.2734
_refine_ls_R_factor_gt           0.1484
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1127P)²+1198.8762P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3335
_refine_ls_wR_factor_ref         0.4040
_reflns_number_gt                4902
_reflns_number_total             10824
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic102350t_si_002_3.cif
_cod_data_source_block           fl62
_cod_database_code               4324381
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z-1/2'
'-x-1/2, y-1/2, z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.5254(10) 0.1110(15) 0.6344(13) 0.057(9) Uani 1 1 d U . .
C2 C 0.4990(10) 0.0199(12) 0.6599(14) 0.070(12) Uani 1 1 d . . .
H2 H 0.4960 -0.0072 0.6838 0.084 Uiso 1 1 calc R . .
C3 C 0.4813(12) 0.0034(16) 0.6208(13) 0.070(10) Uani 1 1 d U . .
H3 H 0.4651 -0.0336 0.6174 0.084 Uiso 1 1 calc R . .
C4 C 0.4873(12) 0.0426(15) 0.5848(12) 0.070(10) Uani 1 1 d U . .
H4 H 0.4776 0.0315 0.5560 0.084 Uiso 1 1 calc R . .
C5 C 0.5079(10) 0.0975(14) 0.5928(12) 0.058(9) Uani 1 1 d . . .
H5 H 0.5101 0.1262 0.5698 0.069 Uiso 1 1 calc R . .
C6 C 0.5488(9) 0.1692(11) 0.6442(11) 0.035(7) Uani 1 1 d U . .
C7 C 0.5583(10) 0.2192(13) 0.6148(12) 0.056(9) Uani 1 1 d . . .
H7 H 0.5494 0.2234 0.5848 0.067 Uiso 1 1 calc R . .
C8 C 0.5826(10) 0.2576(11) 0.6398(11) 0.046(8) Uani 1 1 d U . .
H8 H 0.5932 0.2960 0.6307 0.055 Uiso 1 1 calc R . .
C9 C 0.6164(9) 0.2553(10) 0.7161(10) 0.041(8) Uani 1 1 d . . .
H9A H 0.5959 0.2577 0.7426 0.049 Uiso 1 1 calc R . .
H9B H 0.6285 0.2959 0.7095 0.049 Uiso 1 1 calc R . .
C10 C 0.6581(9) 0.2134(11) 0.7249(10) 0.032(7) Uani 1 1 d . . .
C11 C 0.6828(8) 0.1857(9) 0.6894(8) 0.020(6) Uani 1 1 d U . .
H11 H 0.6730 0.1969 0.6607 0.024 Uiso 1 1 calc R . .
C12 C 0.7302(8) 0.1306(10) 0.7357(9) 0.026(6) Uani 1 1 d . . .
C13 C 0.7105(10) 0.1545(10) 0.7697(11) 0.038(8) Uani 1 1 d . . .
H13 H 0.7216 0.1423 0.7978 0.046 Uiso 1 1 calc R . .
C14 C 0.6742(9) 0.1969(11) 0.7684(11) 0.045(8) Uani 1 1 d U . .
H14 H 0.6610 0.2138 0.7943 0.054 Uiso 1 1 calc R . .
C15 C 0.7702(8) 0.0854(9) 0.7358(9) 0.024(6) Uani 1 1 d U . .
C16 C 0.8185(8) 0.0305(9) 0.6885(8) 0.018(6) Uani 1 1 d U . .
H16 H 0.8283 0.0195 0.6597 0.022 Uiso 1 1 calc R . .
C17 C 0.8442(9) 0.0072(10) 0.7241(10) 0.031(7) Uani 1 1 d U . .
C18 C 0.8284(9) 0.0235(11) 0.7666(10) 0.037(8) Uani 1 1 d . . .
H18 H 0.8432 0.0074 0.7921 0.045 Uiso 1 1 calc R . .
C19 C 0.7920(8) 0.0622(11) 0.7701(10) 0.037(7) Uani 1 1 d U . .
H19 H 0.7814 0.0734 0.7987 0.045 Uiso 1 1 calc R . .
C20 C 0.8889(10) -0.0310(12) 0.7158(12) 0.059(10) Uani 1 1 d . . .
H20A H 0.9093 -0.0312 0.7424 0.071 Uiso 1 1 calc R . .
H20B H 0.8795 -0.0728 0.7094 0.071 Uiso 1 1 calc R . .
C21 C 0.9231(11) -0.0307(15) 0.6407(13) 0.057(10) Uani 1 1 d . . .
H21 H 0.9146 -0.0702 0.6323 0.069 Uiso 1 1 calc R . .
C22 C 0.9464(12) 0.0113(18) 0.6130(15) 0.077(12) Uani 1 1 d . . .
H22 H 0.9564 0.0075 0.5833 0.093 Uiso 1 1 calc R . .
C23 C 0.9504(10) 0.0600(17) 0.6417(13) 0.061(10) Uani 1 1 d U . .
C24 C 0.9755(7) 0.1178(8) 0.6327(8) 0.063(10) Uani 1 1 d GU . .
N8 N 0.9805(7) 0.1552(9) 0.6689(6) 0.064(8) Uani 1 1 d GU . .
C25 C 1.0021(8) 0.2108(9) 0.6642(9) 0.110(13) Uani 1 1 d GU . .
H25 H 1.0055 0.2364 0.6889 0.132 Uiso 1 1 calc R . .
C26 C 1.0189(8) 0.2288(10) 0.6232(11) 0.16(2) Uani 1 1 d GU . .
H26 H 1.0337 0.2668 0.6200 0.187 Uiso 1 1 calc R . .
C27 C 1.0139(8) 0.1914(14) 0.5870(8) 0.146(18) Uani 1 1 d GU . .
H27 H 1.0254 0.2038 0.5590 0.176 Uiso 1 1 calc R . .
C28 C 0.9923(9) 0.1359(13) 0.5918(7) 0.085(12) Uani 1 1 d GU . .
H28 H 0.9889 0.1103 0.5670 0.102 Uiso 1 1 calc R . .
C29 C 0.6045(10) 0.1076(12) 0.8259(10) 0.044(8) Uani 1 1 d U . .
C30 C 0.5566(11) 0.1874(14) 0.8145(12) 0.064(10) Uani 1 1 d U . .
H30 H 0.5328 0.2074 0.7977 0.077 Uiso 1 1 calc R . .
C31 C 0.5710(10) 0.2126(13) 0.8506(11) 0.048(8) Uani 1 1 d U . .
H31 H 0.5609 0.2520 0.8575 0.058 Uiso 1 1 calc R . .
C32 C 0.5997(11) 0.1835(13) 0.8778(11) 0.054(9) Uani 1 1 d U . .
H32 H 0.6077 0.2009 0.9053 0.065 Uiso 1 1 calc R . .
C33 C 0.6184(11) 0.1278(13) 0.8667(11) 0.057(9) Uani 1 1 d U . .
H33 H 0.6389 0.1057 0.8856 0.068 Uiso 1 1 calc R . .
C34 C 0.6257(10) 0.0489(12) 0.8080(12) 0.041(8) Uani 1 1 d U . .
C35 C 0.6590(12) 0.0111(14) 0.8277(11) 0.063(10) Uani 1 1 d . . .
H35 H 0.6744 0.0166 0.8553 0.076 Uiso 1 1 calc R . .
C36 C 0.6649(12) -0.0348(13) 0.7996(12) 0.063(10) Uani 1 1 d U . .
H36 H 0.6847 -0.0686 0.8044 0.076 Uiso 1 1 calc R . .
C37 C 0.6333(9) -0.0602(11) 0.7248(10) 0.040(8) Uani 1 1 d U . .
H37A H 0.6008 -0.0776 0.7244 0.048 Uiso 1 1 calc R . .
H37B H 0.6564 -0.0936 0.7254 0.048 Uiso 1 1 calc R . .
C38 C 0.6409(10) -0.0235(11) 0.6823(9) 0.036(7) Uani 1 1 d U . .
C39 C 0.6833(8) 0.0092(10) 0.6803(8) 0.024(6) Uani 1 1 d . . .
H39 H 0.7061 0.0052 0.7032 0.029 Uiso 1 1 calc R . .
C40 C 0.6591(9) 0.0532(11) 0.6150(9) 0.032(7) Uani 1 1 d U . .
C41 C 0.6203(9) 0.0154(10) 0.6136(9) 0.028(7) Uani 1 1 d U . .
H41 H 0.5993 0.0165 0.5890 0.033 Uiso 1 1 calc R . .
C42 C 0.6119(9) -0.0232(11) 0.6470(9) 0.037(7) Uani 1 1 d U . .
H42 H 0.5856 -0.0500 0.6455 0.044 Uiso 1 1 calc R . .
C43 C 0.6694(9) 0.1054(11) 0.5849(10) 0.041(8) Uani 1 1 d . . .
C44 C 0.7186(9) 0.1858(11) 0.5743(9) 0.039(8) Uani 1 1 d . . .
H44 H 0.7465 0.2075 0.5821 0.047 Uiso 1 1 calc R . .
C45 C 0.6913(10) 0.2066(11) 0.5394(9) 0.039(7) Uani 1 1 d U . .
C46 C 0.6503(10) 0.1739(13) 0.5284(9) 0.047(8) Uani 1 1 d . . .
H46 H 0.6296 0.1876 0.5059 0.056 Uiso 1 1 calc R . .
C47 C 0.6409(9) 0.1233(11) 0.5501(9) 0.031(7) Uani 1 1 d U . .
H47 H 0.6144 0.0994 0.5416 0.037 Uiso 1 1 calc R . .
C48 C 0.7068(15) 0.2614(17) 0.5126(12) 0.090(13) Uani 1 1 d . . .
H48A H 0.6919 0.2602 0.4830 0.109 Uiso 1 1 calc R . .
H48B H 0.6964 0.2985 0.5275 0.109 Uiso 1 1 calc R . .
C49 C 0.7888(14) 0.2949(14) 0.5319(12) 0.069(12) Uani 1 1 d . . .
H49 H 0.7818 0.3260 0.5523 0.082 Uiso 1 1 calc R . .
C50 C 0.8320(16) 0.2739(17) 0.5192(15) 0.090(13) Uani 1 1 d U . .
H50 H 0.8620 0.2887 0.5287 0.108 Uiso 1 1 calc R . .
C51 C 0.8250(17) 0.229(2) 0.4909(15) 0.091(12) Uani 1 1 d U B .
C52 C 0.8578(12) 0.1926(15) 0.4698(11) 0.061(8) Uani 1 1 d U B .
C53 C 0.8754(12) 0.1053(18) 0.4188(13) 0.081(12) Uani 1 1 d . . .
H53 H 0.8639 0.0718 0.4028 0.097 Uiso 1 1 calc R . .
C54 C 0.9244(12) 0.1208(19) 0.4193(15) 0.100(15) Uani 1 1 d . . .
H54 H 0.9463 0.1003 0.4008 0.121 Uiso 1 1 calc R . .
C55 C 0.9405(15) 0.166(2) 0.4470(17) 0.105(15) Uani 1 1 d U . .
H55 H 0.9735 0.1715 0.4528 0.126 Uiso 1 1 calc R . .
C56 C 0.9094(14) 0.201(2) 0.4641(16) 0.108(19) Uani 1 1 d . . .
H56 H 0.9216 0.2374 0.4750 0.130 Uiso 1 1 calc R . .
C57 C 0.8899(8) 0.1304(9) 0.8225(8) 0.068(9) Uani 1 1 d GU . .
N17 N 0.9210(8) 0.0972(11) 0.7965(6) 0.067(8) Uani 1 1 d GU . .
C58 C 0.9409(8) 0.0448(11) 0.8127(9) 0.142(19) Uani 1 1 d GU . .
H58 H 0.9621 0.0222 0.7949 0.171 Uiso 1 1 calc R . .
C59 C 0.9299(10) 0.0255(10) 0.8550(10) 0.139(18) Uani 1 1 d GU . .
H59 H 0.9435 -0.0103 0.8660 0.167 Uiso 1 1 calc R . .
C60 C 0.8988(10) 0.0586(13) 0.8810(7) 0.109(14) Uani 1 1 d GU . .
H60 H 0.8913 0.0454 0.9099 0.131 Uiso 1 1 calc R . .
C61 C 0.8789(9) 0.1111(12) 0.8648(8) 0.127(17) Uani 1 1 d GU . .
H61 H 0.8577 0.1337 0.8826 0.152 Uiso 1 1 calc R . .
C62 C 0.8725(11) 0.1760(14) 0.7979(11) 0.050(8) Uani 1 1 d U . .
C63 C 0.8349(13) 0.2142(14) 0.8063(13) 0.079(11) Uani 1 1 d U . .
H63 H 0.8164 0.2097 0.8322 0.095 Uiso 1 1 calc R . .
C64 C 0.8247(13) 0.2575(15) 0.7777(12) 0.070(9) Uani 1 1 d U . .
H64 H 0.8001 0.2866 0.7788 0.084 Uiso 1 1 calc R . .
C65 C 0.8672(11) 0.2791(13) 0.7024(11) 0.055(8) Uani 1 1 d U . .
H65A H 0.9008 0.2921 0.6996 0.066 Uiso 1 1 calc R . .
H65B H 0.8466 0.3150 0.7006 0.066 Uiso 1 1 calc R . .
C66 C 0.8545(10) 0.2354(11) 0.6647(10) 0.037(7) Uani 1 1 d U . .
C67 C 0.8129(9) 0.2003(10) 0.6679(9) 0.033(7) Uani 1 1 d U . .
H67 H 0.7922 0.2075 0.6921 0.040 Uiso 1 1 calc R . .
C68 C 0.8342(9) 0.1468(11) 0.6080(9) 0.034(7) Uani 1 1 d U . .
C69 C 0.8739(9) 0.1833(12) 0.6025(9) 0.040(8) Uani 1 1 d U . .
H69 H 0.8940 0.1763 0.5779 0.048 Uiso 1 1 calc R . .
C70 C 0.8852(10) 0.2269(10) 0.6294(9) 0.035(8) Uani 1 1 d . . .
H70 H 0.9126 0.2511 0.6250 0.042 Uiso 1 1 calc R . .
C71 C 0.8214(8) 0.0948(10) 0.5810(8) 0.025(6) Uani 1 1 d U . .
C72 C 0.7663(9) 0.0169(10) 0.5714(8) 0.024(6) Uani 1 1 d . . .
H72 H 0.7387 -0.0042 0.5806 0.028 Uiso 1 1 calc R . .
C73 C 0.7900(10) -0.0008(11) 0.5332(9) 0.033(7) Uani 1 1 d U . .
C74 C 0.8299(10) 0.0271(12) 0.5180(10) 0.045(8) Uani 1 1 d U . .
H74 H 0.8452 0.0154 0.4915 0.054 Uiso 1 1 calc R . .
C75 C 0.8470(9) 0.0748(11) 0.5445(9) 0.035(7) Uani 1 1 d U . .
H75 H 0.8764 0.0934 0.5371 0.042 Uiso 1 1 calc R . .
C76 C 0.7661(10) -0.0481(12) 0.5053(10) 0.048(8) Uani 1 1 d . . .
H76A H 0.7868 -0.0582 0.4800 0.058 Uiso 1 1 calc R . .
H76B H 0.7615 -0.0848 0.5230 0.058 Uiso 1 1 calc R . .
C77 C 0.6768(12) -0.0504(13) 0.4978(11) 0.052(9) Uani 1 1 d . . .
H77 H 0.6691 -0.0847 0.5148 0.062 Uiso 1 1 calc R . .
C78 C 0.6454(11) -0.0130(13) 0.4757(11) 0.052(9) Uani 1 1 d . . .
H78 H 0.6118 -0.0178 0.4732 0.063 Uiso 1 1 calc R . .
C79 C 0.6720(11) 0.0316(11) 0.4585(10) 0.039(8) Uani 1 1 d . . .
C80 C 0.6577(10) 0.0836(13) 0.4346(10) 0.048(9) Uani 1 1 d . . .
C81 C 0.6772(12) 0.1741(15) 0.3987(15) 0.088(14) Uani 1 1 d . . .
H81 H 0.7009 0.2022 0.3902 0.105 Uiso 1 1 calc R B .
C82 C 0.6299(15) 0.1833(17) 0.3890(15) 0.109(15) Uani 1 1 d U B .
H82 H 0.6186 0.2232 0.3866 0.131 Uiso 1 1 calc R A 1
C83 C 0.595(2) 0.132(2) 0.382(2) 0.050(9) Uani 0.50 1 d PU B 1
H83 H 0.5672 0.1308 0.3641 0.060 Uiso 0.50 1 calc PR B 1
C84 C 0.615(2) 0.088(3) 0.409(2) 0.050(9) Uani 0.50 1 d PU B 1
H84 H 0.5957 0.0536 0.4111 0.060 Uiso 0.50 1 calc PR B 1
C83A C 0.596(2) 0.158(3) 0.417(2) 0.050(9) Uani 0.50 1 d PU B 2
H83A H 0.5678 0.1801 0.4247 0.060 Uiso 0.50 1 calc PR B 2
C84A C 0.604(2) 0.099(3) 0.432(2) 0.050(9) Uani 0.50 1 d PU B 2
H84A H 0.5789 0.0725 0.4401 0.060 Uiso 0.50 1 calc PR B 2
N1 N 0.5216(7) 0.0745(10) 0.6679(9) 0.044(7) Uani 1 1 d U . .
N2 N 0.5696(7) 0.1784(9) 0.6824(9) 0.039(6) Uani 1 1 d U . .
N3 N 0.5898(8) 0.2334(10) 0.6801(8) 0.037(6) Uani 1 1 d U . .
N4 N 0.7179(6) 0.1463(8) 0.6916(6) 0.018(5) Uani 1 1 d U . .
N5 N 0.7818(7) 0.0663(8) 0.6922(6) 0.023(5) Uani 1 1 d U . .
N6 N 0.9149(9) -0.0069(11) 0.6795(11) 0.053(8) Uani 1 1 d . . .
N7 N 0.9323(8) 0.0481(12) 0.6806(9) 0.056(7) Uani 1 1 d U . .
N9 N 0.5736(7) 0.1335(9) 0.7987(7) 0.031(5) Uani 1 1 d U . .
N10 N 0.6137(7) 0.0268(9) 0.7706(9) 0.037(6) Uani 1 1 d U . .
N11 N 0.6389(7) -0.0249(9) 0.7645(9) 0.036(6) Uani 1 1 d . . .
N12 N 0.6927(7) 0.0475(8) 0.6454(7) 0.026(5) Uani 1 1 d . . .
N13 N 0.7076(7) 0.1361(8) 0.5977(6) 0.022(5) Uani 1 1 d U . .
N14 N 0.7581(13) 0.2607(14) 0.5086(11) 0.084(10) Uani 1 1 d U . .
N15 N 0.7775(11) 0.2187(14) 0.4839(11) 0.077(9) Uani 1 1 d U . .
N16 N 0.8451(9) 0.1418(13) 0.4431(9) 0.064(7) Uani 1 1 d U . .
N18 N 0.8860(10) 0.2023(12) 0.7596(10) 0.064(8) Uani 1 1 d . . .
N19 N 0.8600(9) 0.2490(13) 0.7453(10) 0.065(8) Uani 1 1 d U . .
N20 N 0.8007(6) 0.1578(7) 0.6393(6) 0.019(5) Uani 1 1 d U . .
N21 N 0.7824(7) 0.0646(8) 0.5959(7) 0.025(5) Uani 1 1 d U . .
N22 N 0.7212(9) -0.0275(10) 0.4898(8) 0.042(6) Uani 1 1 d U B .
N23 N 0.7183(8) 0.0253(10) 0.4665(7) 0.040(6) Uani 1 1 d . . .
N24 N 0.6883(8) 0.1265(11) 0.4196(8) 0.049(7) Uani 1 1 d . B .
O1E O 0.7391(10) 0.3893(13) 0.8092(15) 0.19(2) Uani 1 1 d . . .
H1E H 0.7316 0.4151 0.8286 0.282 Uiso 1 1 d R . .
C1E C 0.7075(15) 0.3435(14) 0.8233(11) 0.078(12) Uani 1 1 d . . .
H1E1 H 0.7092 0.3397 0.8557 0.094 Uiso 1 1 calc R . .
H1E2 H 0.7175 0.3049 0.8103 0.094 Uiso 1 1 calc R . .
C2E C 0.6574(13) 0.3567(17) 0.8100(13) 0.090(13) Uani 1 1 d . . .
H2E1 H 0.6484 0.3966 0.8206 0.135 Uiso 1 1 calc R . .
H2E2 H 0.6360 0.3269 0.8229 0.135 Uiso 1 1 calc R . .
H2E3 H 0.6548 0.3555 0.7779 0.135 Uiso 1 1 calc R . .
Fe1 Fe 0.74738(12) 0.10359(14) 0.64404(11) 0.0203(9) Uani 1 1 d . . .
Ag1 Ag 0.55709(8) 0.09305(9) 0.73231(9) 0.0537(8) Uani 1 1 d . . .
Ag2 Ag 0.9453(5) 0.1302(5) 0.7361(3) 0.068(2) Uani 0.75 1 d P . 1
Ag2A Ag 0.9424(16) 0.1336(19) 0.7211(12) 0.068(2) Uani 0.25 1 d P . 2
Ag3 Ag 0.7658(3) 0.1171(4) 0.4467(3) 0.040(4) Uani 0.50 1 d P B 1
Ag3A Ag 0.7573(6) 0.1463(6) 0.4492(6) 0.040(4) Uani 0.25 1 d P B 2
Ag3B Ag 0.7711(10) 0.0965(12) 0.4391(8) 0.040(4) Uani 0.25 1 d P B 3
P1 P 0.5000 0.3631(6) 0.7500 0.104(4) Uani 1 2 d S . .
P2 P 1.0000 0.3619(7) 0.7500 0.109(5) Uani 1 2 d S . .
P3 P 0.5869(6) 0.3712(8) 0.5311(7) 0.127(5) Uani 0.50 1 d PG C 1
F8 F 0.6261(9) 0.3486(13) 0.5651(10) 0.127(5) Uani 0.50 1 d PG C 1
F9 F 0.5463(9) 0.3626(14) 0.5680(9) 0.127(5) Uani 0.50 1 d PG C 1
F10 F 0.5778(10) 0.3043(9) 0.5152(11) 0.127(5) Uani 0.50 1 d PG C 1
F11 F 0.5948(10) 0.4383(9) 0.5479(11) 0.127(5) Uani 0.50 1 d PG C 1
F12 F 0.6271(9) 0.3799(14) 0.4950(9) 0.127(5) Uani 0.50 1 d PG C 1
F13 F 0.5467(9) 0.3938(14) 0.4977(10) 0.127(5) Uani 0.50 1 d PG C 1
P3A P 0.5860(5) 0.3674(7) 0.5136(8) 0.127(5) Uani 0.50 1 d PG D 2
F8A F 0.6374(6) 0.3914(13) 0.5270(12) 0.127(5) Uani 0.50 1 d PG D 2
F9A F 0.5699(10) 0.3699(15) 0.5644(8) 0.127(5) Uani 0.50 1 d PG D 2
F10A F 0.6032(10) 0.3003(8) 0.5208(12) 0.127(5) Uani 0.50 1 d PG D 2
F11A F 0.5680(10) 0.4349(8) 0.5077(12) 0.127(5) Uani 0.50 1 d PG D 2
F12A F 0.6020(10) 0.3654(14) 0.4636(8) 0.127(5) Uani 0.50 1 d PG D 2
F13A F 0.5340(6) 0.3433(13) 0.5012(11) 0.127(5) Uani 0.50 1 d PG D 2
P4 P 0.7338(8) 0.3605(8) 0.6647(9) 0.098(4) Uani 0.60 1 d P E 1
F20 F 0.7912(12) 0.3667(12) 0.6544(15) 0.098(4) Uani 0.60 1 d P E 1
F21 F 0.6826(12) 0.3591(13) 0.6788(14) 0.098(4) Uani 0.60 1 d P E 1
F22 F 0.7457(11) 0.4065(12) 0.7097(14) 0.098(4) Uani 0.60 1 d P E 1
F23 F 0.7299(11) 0.4136(13) 0.6334(15) 0.098(4) Uani 0.60 1 d P E 1
F24 F 0.7303(12) 0.3114(13) 0.6321(14) 0.098(4) Uani 0.60 1 d P E 1
F25 F 0.7424(12) 0.3041(12) 0.7059(14) 0.098(4) Uani 0.60 1 d P E 1
P4A P 0.7341(8) 0.3572(8) 0.6537(10) 0.098(4) Uani 0.40 1 d PG F 2
F20A F 0.7304(13) 0.3807(14) 0.6044(11) 0.098(4) Uani 0.40 1 d PG F 2
F22A F 0.6783(8) 0.3711(14) 0.6607(14) 0.098(4) Uani 0.40 1 d PG F 2
F21A F 0.7205(12) 0.2914(9) 0.6373(12) 0.098(4) Uani 0.40 1 d PG F 2
F23A F 0.7462(12) 0.4231(9) 0.6703(14) 0.098(4) Uani 0.40 1 d PG F 2
F24A F 0.7890(8) 0.3434(13) 0.6464(14) 0.098(4) Uani 0.40 1 d PG F 2
F25A F 0.7368(13) 0.3341(14) 0.7034(10) 0.098(4) Uani 0.40 1 d PG F 2
P5 P 0.9573(4) 0.3713(4) 0.5394(4) 0.078(3) Uani 1 1 d . . .
F1 F 0.5000 0.4315(11) 0.7500 0.104(4) Uani 1 2 d S . .
F2 F 0.4574(6) 0.3632(8) 0.7154(9) 0.104(4) Uani 1 1 d . . .
F3 F 0.4607(6) 0.3619(8) 0.7875(9) 0.104(4) Uani 1 1 d . . .
F4 F 0.5000 0.2926(11) 0.7500 0.104(4) Uani 1 2 d S . .
F5 F 0.9716(16) 0.3757(16) 0.706(2) 0.109(5) Uani 0.50 1 d P G 1
F6 F 1.0485(13) 0.3398(17) 0.7323(18) 0.109(5) Uani 0.50 1 d P G 1
F7 F 1.0000 0.4283(11) 0.7500 0.109(5) Uani 1 2 d S G 1
F5A F 1.0452(12) 0.3938(16) 0.7194(18) 0.109(5) Uani 0.50 1 d P G -2
F6A F 1.0221(11) 0.2989(16) 0.7386(18) 0.109(5) Uani 0.50 1 d P G -2
F7A F 0.9761(16) 0.3531(16) 0.701(2) 0.109(5) Uani 0.50 1 d P G -2
F14 F 0.9042(8) 0.3794(10) 0.5624(8) 0.111(3) Uani 1 1 d . . .
F15 F 1.0047(9) 0.3702(10) 0.5238(8) 0.111(3) Uani 1 1 d . . .
F16 F 0.9526(8) 0.4397(10) 0.5372(8) 0.111(3) Uani 1 1 d . . .
F17 F 0.9516(8) 0.3034(10) 0.5484(8) 0.111(3) Uani 1 1 d . . .
F18 F 0.9808(8) 0.3770(10) 0.5885(8) 0.111(3) Uani 1 1 d . . .
F19 F 0.9334(8) 0.3645(10) 0.4929(8) 0.111(3) Uani 1 1 d . . .
O1W O 0.7882(8) 0.0165(9) 0.3812(10) 0.097(9) Uani 1 1 d . . .
O1 O 0.7468(10) 0.1030(11) 0.8733(7) 0.099(4) Uani 1 1 d . H 1
O2 O 0.7312(10) 0.2038(11) 0.8756(8) 0.099(4) Uani 1 1 d . H 1
O3 O 0.7889(11) 0.1655(11) 0.9235(8) 0.099(4) Uani 1 1 d . H 1
O4 O 0.7080(11) 0.1455(11) 0.9352(8) 0.099(4) Uani 1 1 d . H 1
Cl1 Cl 0.7421(4) 0.1552(3) 0.9032(3) 0.061(2) Uani 1 1 d . H 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 C1 C5 123(3) . .
N1 C1 C6 115(3) . .
C5 C1 C6 122(3) . .
C3 C2 N1 124(4) . .
C3 C2 H2 117.9 . .
N1 C2 H2 117.9 . .
C2 C3 C4 118(3) . .
C2 C3 H3 121.0 . .
C4 C3 H3 121.0 . .
C5 C4 C3 118(3) . .
C5 C4 H4 121.1 . .
C3 C4 H4 121.1 . .
C4 C5 C1 120(3) . .
C4 C5 H5 119.9 . .
C1 C5 H5 119.9 . .
N2 C6 C7 110(2) . .
N2 C6 C1 121(3) . .
C7 C6 C1 129(3) . .
C8 C7 C6 104(3) . .
C8 C7 H7 128.1 . .
C6 C7 H7 128.1 . .
C7 C8 N3 109(3) . .
C7 C8 H8 125.3 . .
N3 C8 H8 125.3 . .
N3 C9 C10 109(2) . .
N3 C9 H9A 109.9 . .
C10 C9 H9A 109.9 . .
N3 C9 H9B 109.9 . .
C10 C9 H9B 109.9 . .
H9A C9 H9B 108.3 . .
C11 C10 C14 115(2) . .
C11 C10 C9 121(3) . .
C14 C10 C9 124(3) . .
N4 C11 C10 128(2) . .
N4 C11 H11 116.0 . .
C10 C11 H11 116.0 . .
C13 C12 N4 123(2) . .
C13 C12 C15 126(3) . .
N4 C12 C15 110(2) . .
C12 C13 C14 125(3) . .
C12 C13 H13 117.5 . .
C14 C13 H13 117.5 . .
C13 C14 C10 115(3) . .
C13 C14 H14 122.3 . .
C10 C14 H14 122.3 . .
C19 C15 N5 121(2) . .
C19 C15 C12 128(3) . .
N5 C15 C12 111(2) . .
N5 C16 C17 125(2) . .
N5 C16 H16 117.7 . .
C17 C16 H16 117.7 . .
C16 C17 C18 117(2) . .
C16 C17 C20 120(3) . .
C18 C17 C20 123(3) . .
C19 C18 C17 119(3) . .
C19 C18 H18 120.7 . .
C17 C18 H18 120.7 . .
C15 C19 C18 123(3) . .
C15 C19 H19 118.6 . .
C18 C19 H19 118.6 . .
N6 C20 C17 109(2) . .
N6 C20 H20A 109.8 . .
C17 C20 H20A 109.8 . .
N6 C20 H20B 109.8 . .
C17 C20 H20B 109.8 . .
H20A C20 H20B 108.3 . .
N6 C21 C22 110(3) . .
N6 C21 H21 124.9 . .
C22 C21 H21 124.9 . .
C23 C22 C21 101(4) . .
C23 C22 H22 129.7 . .
C21 C22 H22 129.7 . .
N7 C23 C22 112(3) . .
N7 C23 C24 121(4) . .
C22 C23 C24 127(3) . .
N8 C24 C28 120.0 . .
N8 C24 C23 115(2) . .
C28 C24 C23 125(2) . .
C24 N8 C25 120.0 . .
C24 N8 Ag2A 115.8(18) . .
C25 N8 Ag2A 122.6(19) . .
C24 N8 Ag2 120.4(13) . .
C25 N8 Ag2 119.3(13) . .
C26 C25 N8 120.0 . .
C26 C25 H25 120.0 . .
N8 C25 H25 120.0 . .
C25 C26 C27 120.0 . .
C25 C26 H26 120.0 . .
C27 C26 H26 120.0 . .
C28 C27 C26 120.0 . .
C28 C27 H27 120.0 . .
C26 C27 H27 120.0 . .
C27 C28 C24 120.0 . .
C27 C28 H28 120.0 . .
C24 C28 H28 120.0 . .
N9 C29 C33 127(3) . .
N9 C29 C34 114(3) . .
C33 C29 C34 119(3) . .
C31 C30 N9 124(3) . .
C31 C30 H30 117.8 . .
N9 C30 H30 117.8 . .
C30 C31 C32 120(3) . .
C30 C31 H31 119.9 . .
C32 C31 H31 119.9 . .
C31 C32 C33 121(3) . .
C31 C32 H32 119.4 . .
C33 C32 H32 119.4 . .
C29 C33 C32 114(3) . .
C29 C33 H33 123.1 . .
C32 C33 H33 123.1 . .
N10 C34 C35 109(3) . .
N10 C34 C29 123(3) . .
C35 C34 C29 129(3) . .
C36 C35 C34 106(3) . .
C36 C35 H35 127.1 . .
C34 C35 H35 127.1 . .
N11 C36 C35 109(3) . .
N11 C36 H36 125.6 . .
C35 C36 H36 125.6 . .
N11 C37 C38 113(2) . .
N11 C37 H37A 109.0 . .
C38 C37 H37A 109.0 . .
N11 C37 H37B 109.0 . .
C38 C37 H37B 109.0 . .
H37A C37 H37B 107.8 . .
C42 C38 C39 118(3) . .
C42 C38 C37 126(2) . .
C39 C38 C37 116(2) . .
N12 C39 C38 121(2) . .
N12 C39 H39 119.4 . .
C38 C39 H39 119.4 . .
N12 C40 C41 122(2) . .
N12 C40 C43 111(2) . .
C41 C40 C43 127(2) . .
C42 C41 C40 120(3) . .
C42 C41 H41 119.8 . .
C40 C41 H41 119.8 . .
C41 C42 C38 120(2) . .
C41 C42 H42 120.2 . .
C38 C42 H42 120.2 . .
N13 C43 C47 123(2) . .
N13 C43 C40 112(2) . .
C47 C43 C40 125(2) . .
N13 C44 C45 123(2) . .
N13 C44 H44 118.4 . .
C45 C44 H44 118.4 . .
C44 C45 C46 117(3) . .
C44 C45 C48 121(3) . .
C46 C45 C48 121(3) . .
C47 C46 C45 119(3) . .
C47 C46 H46 120.4 . .
C45 C46 H46 120.4 . .
C46 C47 C43 120(3) . .
C46 C47 H47 119.8 . .
C43 C47 H47 119.8 . .
N14 C48 C45 108(3) . .
N14 C48 H48A 110.0 . .
C45 C48 H48A 110.0 . .
N14 C48 H48B 110.0 . .
C45 C48 H48B 110.0 . .
H48A C48 H48B 108.4 . .
N14 C49 C50 103(4) . .
N14 C49 H49 128.6 . .
C50 C49 H49 128.6 . .
C51 C50 C49 108(4) . .
C51 C50 H50 125.8 . .
C49 C50 H50 125.8 . .
C50 C51 N15 111(4) . .
C50 C51 C52 130(5) . .
N15 C51 C52 119(4) . .
C51 C52 N16 124(3) . .
C51 C52 C56 130(4) . .
N16 C52 C56 106(4) . .
N16 C53 C54 116(3) . .
N16 C53 H53 121.9 . .
C54 C53 H53 121.9 . .
C55 C54 C53 120(4) . .
C55 C54 H54 120.0 . .
C53 C54 H54 120.0 . .
C56 C55 C54 118(4) . .
C56 C55 H55 121.1 . .
C54 C55 H55 121.1 . .
C55 C56 C52 130(5) . .
C55 C56 H56 114.8 . .
C52 C56 H56 114.8 . .
C62 C57 N17 108(2) . .
C62 C57 C61 132(2) . .
N17 C57 C61 120.0 . .
C57 N17 C58 120.0 . .
C57 N17 Ag2 121.0(16) . .
C58 N17 Ag2 118.5(16) . .
C57 N17 Ag2A 119.8(18) . .
C58 N17 Ag2A 120.1(18) . .
C59 C58 N17 120.0 . .
C59 C58 H58 120.0 . .
N17 C58 H58 120.0 . .
C58 C59 C60 120.0 . .
C58 C59 H59 120.0 . .
C60 C59 H59 120.0 . .
C59 C60 C61 120.0 . .
C59 C60 H60 120.0 . .
C61 C60 H60 120.0 . .
C60 C61 C57 120.0 . .
C60 C61 H61 120.0 . .
C57 C61 H61 120.0 . .
N18 C62 C57 134(3) . .
N18 C62 C63 96(3) . .
C57 C62 C63 130(3) . .
C64 C63 C62 120(4) . .
C64 C63 H63 120.2 . .
C62 C63 H63 120.2 . .
C63 C64 N19 102(3) . .
C63 C64 H64 129.0 . .
N19 C64 H64 129.0 . .
N19 C65 C66 109(2) . .
N19 C65 H65A 109.8 . .
C66 C65 H65A 109.8 . .
N19 C65 H65B 109.8 . .
C66 C65 H65B 109.8 . .
H65A C65 H65B 108.2 . .
C70 C66 C67 119(3) . .
C70 C66 C65 121(2) . .
C67 C66 C65 119(3) . .
N20 C67 C66 124(3) . .
N20 C67 H67 117.9 . .
C66 C67 H67 117.9 . .
N20 C68 C69 122(2) . .
N20 C68 C71 111(2) . .
C69 C68 C71 127(2) . .
C70 C69 C68 124(3) . .
C70 C69 H69 118.1 . .
C68 C69 H69 118.1 . .
C69 C70 C66 116(3) . .
C69 C70 H70 122.1 . .
C66 C70 H70 122.1 . .
N21 C71 C75 121(2) . .
N21 C71 C68 114(2) . .
C75 C71 C68 125(2) . .
N21 C72 C73 121(2) . .
N21 C72 H72 119.6 . .
C73 C72 H72 119.6 . .
C74 C73 C72 123(2) . .
C74 C73 C76 120(3) . .
C72 C73 C76 117(2) . .
C73 C74 C75 116(3) . .
C73 C74 H74 122.2 . .
C75 C74 H74 122.2 . .
C71 C75 C74 121(2) . .
C71 C75 H75 119.4 . .
C74 C75 H75 119.4 . .
N22 C76 C73 111(2) . .
N22 C76 H76A 109.5 . .
C73 C76 H76A 109.5 . .
N22 C76 H76B 109.5 . .
C73 C76 H76B 109.5 . .
H76A C76 H76B 108.1 . .
N22 C77 C78 105(2) . .
N22 C77 H77 127.3 . .
C78 C77 H77 127.3 . .
C79 C78 C77 106(3) . .
C79 C78 H78 126.9 . .
C77 C78 H78 126.9 . .
N23 C79 C78 113(3) . .
N23 C79 C80 117(3) . .
C78 C79 C80 130(3) . .
N24 C80 C79 125(3) . .
N24 C80 C84 107(4) . .
C79 C80 C84 125(3) . .
N24 C80 C84A 116(3) . .
C79 C80 C84A 119(3) . .
N24 C81 C82 118(3) . .
N24 C81 H81 121.1 . .
C82 C81 H81 121.1 . .
C81 C82 C83A 119(4) . .
C81 C82 C83 123(4) . .
C83A C82 C83 49(3) . .
C81 C82 H82 118.6 . .
C83A C82 H82 101.1 . .
C83 C82 H82 118.6 . .
C84 C83 C82 101(5) . .
C84 C83 H83 129.7 . .
C82 C83 H83 129.7 . .
C83 C84 C80 135(6) . .
C83 C84 H84 112.5 . .
C80 C84 H84 112.5 . .
C82 C83A C84A 117(5) . .
C84A C83A H83A 121.3 . .
C83A C84A C80 113(5) . .
C83A C84A H84A 123.7 . .
C1 N1 C2 117(3) . .
C1 N1 Ag1 122(2) . .
C2 N1 Ag1 121(2) . .
C6 N2 N3 106(2) . .
C6 N2 Ag1 111.0(16) . .
N3 N2 Ag1 142.5(19) . .
N2 N3 C8 110(2) . .
N2 N3 C9 120(2) . .
C8 N3 C9 130(2) . .
C11 N4 C12 113.1(19) . .
C11 N4 Fe1 127.9(17) . .
C12 N4 Fe1 118.7(15) . .
C16 N5 C15 116(2) . .
C16 N5 Fe1 126.2(17) . .
C15 N5 Fe1 117.3(15) . .
C21 N6 N7 109(3) . .
C21 N6 C20 129(3) . .
N7 N6 C20 121(3) . .
C23 N7 N6 108(3) . .
C23 N7 Ag2A 105(3) . .
N6 N7 Ag2A 147(3) . .
C23 N7 Ag2 113(2) . .
N6 N7 Ag2 138(2) . .
C29 N9 C30 113(3) . .
C29 N9 Ag1 120.8(18) . .
C30 N9 Ag1 126(2) . .
C34 N10 N11 108(2) . .
C34 N10 Ag1 110.8(18) . .
N11 N10 Ag1 141(2) . .
C36 N11 N10 109(2) . .
C36 N11 C37 130(2) . .
N10 N11 C37 121(2) . .
C40 N12 C39 117(2) . .
C40 N12 Fe1 118.4(17) . .
C39 N12 Fe1 123.5(16) . .
C43 N13 C44 117(2) . .
C43 N13 Fe1 118.8(17) . .
C44 N13 Fe1 123.8(17) . .
N15 N14 C49 116(4) . .
N15 N14 C48 118(3) . .
C49 N14 C48 126(4) . .
N14 N15 C51 101(3) . .
N14 N15 Ag3A 139(3) . .
C51 N15 Ag3A 119(3) . .
N14 N15 Ag3 146(2) . .
C51 N15 Ag3 110(3) . .
C53 N16 C52 128(3) . .
C53 N16 Ag3 118(2) . .
C52 N16 Ag3 114(2) . .
C53 N16 Ag3B 105(2) . .
C52 N16 Ag3B 127(2) . .
C53 N16 Ag3A 132(2) . .
C52 N16 Ag3A 100(2) . .
N19 N18 C62 118(3) . .
N19 N18 Ag2 142(2) . .
C62 N18 Ag2 99(2) . .
N19 N18 Ag2A 132(2) . .
C62 N18 Ag2A 108(2) . .
N18 N19 C64 105(3) . .
N18 N19 C65 124(3) . .
C64 N19 C65 130(3) . .
C67 N20 C68 114(2) . .
C67 N20 Fe1 126.7(17) . .
C68 N20 Fe1 118.2(16) . .
C71 N21 C72 118(2) . .
C71 N21 Fe1 115.4(16) . .
C72 N21 Fe1 125.6(16) . .
C77 N22 N23 111(2) . .
C77 N22 C76 129(3) . .
N23 N22 C76 120(2) . .
C79 N23 N22 104(2) . .
C79 N23 Ag3B 119.0(19) . .
N22 N23 Ag3B 137.0(19) . .
C79 N23 Ag3 112.7(17) . .
N22 N23 Ag3 142.1(18) . .
C81 N24 C80 127(3) . .
C81 N24 Ag3A 104(2) . .
C80 N24 Ag3A 124(2) . .
C81 N24 Ag3 118(2) . .
C80 N24 Ag3 113.7(19) . .
C81 N24 Ag3B 125(2) . .
C80 N24 Ag3B 108.4(19) . .
C1E O1E H1E 97.2 . .
O1E C1E C2E 111(3) . .
O1E C1E H1E1 109.4 . .
C2E C1E H1E1 109.4 . .
O1E C1E H1E2 109.4 . .
C2E C1E H1E2 109.4 . .
H1E1 C1E H1E2 108.0 . .
C1E C2E H2E1 109.5 . .
C1E C2E H2E2 109.5 . .
H2E1 C2E H2E2 109.5 . .
C1E C2E H2E3 109.5 . .
H2E1 C2E H2E3 109.5 . .
H2E2 C2E H2E3 109.5 . .
N4 Fe1 N20 94.5(8) . .
N4 Fe1 N13 96.5(8) . .
N20 Fe1 N13 98.9(8) . .
N4 Fe1 N5 81.9(8) . .
N20 Fe1 N5 86.7(8) . .
N13 Fe1 N5 174.3(8) . .
N4 Fe1 N21 175.0(8) . .
N20 Fe1 N21 80.6(8) . .
N13 Fe1 N21 85.0(8) . .
N5 Fe1 N21 97.0(8) . .
N4 Fe1 N12 88.0(8) . .
N20 Fe1 N12 176.9(9) . .
N13 Fe1 N12 78.8(8) . .
N5 Fe1 N12 95.6(8) . .
N21 Fe1 N12 97.0(8) . .
N1 Ag1 N9 161.4(8) . .
N1 Ag1 N2 70.6(9) . .
N9 Ag1 N2 102.1(8) . .
N1 Ag1 N10 126.1(8) . .
N9 Ag1 N10 71.8(8) . .
N2 Ag1 N10 131.7(7) . .
N1 Ag1 Ag1 81.8(6) . 4_656
N9 Ag1 Ag1 84.8(5) . 4_656
N2 Ag1 Ag1 109.3(5) . 4_656
N10 Ag1 Ag1 117.4(5) . 4_656
N17 Ag2 N8 171.5(11) . .
N17 Ag2 N18 75.6(11) . .
N8 Ag2 N18 112.8(9) . .
N17 Ag2 N7 106.4(10) . .
N8 Ag2 N7 69.6(8) . .
N18 Ag2 N7 125.6(9) . .
N17 Ag2 Ag2 94.7(7) . 4_756
N8 Ag2 Ag2 80.0(7) . 4_756
N18 Ag2 Ag2 125.7(7) . 4_756
N7 Ag2 Ag2 108.5(7) . 4_756
N8 Ag2A N7 80.8(18) . .
N8 Ag2A N18 125(2) . .
N7 Ag2A N18 133(2) . .
N8 Ag2A N17 161(2) . .
N7 Ag2A N17 101.0(17) . .
N18 Ag2A N17 67.6(15) . .
N16 Ag3 N24 149.7(10) . .
N16 Ag3 N23 136.1(10) . .
N24 Ag3 N23 70.5(8) . .
N16 Ag3 N15 71.5(11) . .
N24 Ag3 N15 101.3(10) . .
N23 Ag3 N15 133.3(9) . .
N15 Ag3A N24 129.0(13) . .
N15 Ag3A N16 78.0(13) . .
N24 Ag3A N16 147.6(12) . .
N16 Ag3B N23 148.5(16) . .
N16 Ag3B N24 137.0(15) . .
N23 Ag3B N24 71.1(11) . .
N16 Ag3B O1W 100.0(13) . .
N23 Ag3B O1W 83.5(11) . .
N24 Ag3B O1W 101.4(12) . .
F1 P1 F4 180.000(10) . .
F1 P1 F3 91.0(8) . .
F4 P1 F3 89.0(8) . .
F1 P1 F3 91.0(8) . 4_656
F4 P1 F3 89.0(8) . 4_656
F3 P1 F3 178.0(16) . 4_656
F1 P1 F2 89.9(8) . .
F4 P1 F2 90.1(8) . .
F3 P1 F2 87.3(11) . .
F3 P1 F2 92.7(11) 4_656 .
F1 P1 F2 89.9(8) . 4_656
F4 P1 F2 90.1(8) . 4_656
F3 P1 F2 92.7(11) . 4_656
F3 P1 F2 87.3(11) 4_656 4_656
F2 P1 F2 179.9(18) . 4_656
F7 P2 F6 108.7(15) . 4_756
F7 P2 F6 108.7(15) . .
F6 P2 F6 143(3) 4_756 .
F7 P2 F6A 153.2(15) . .
F6 P2 F6A 98(2) 4_756 .
F7 P2 F6A 153.2(15) . 4_756
F6 P2 F6A 98(2) . 4_756
F6A P2 F6A 54(3) . 4_756
F7 P2 F5 78.8(15) . 4_756
F6 P2 F5 102(3) 4_756 4_756
F6 P2 F5 85(3) . 4_756
F6A P2 F5 99(2) . 4_756
F6A P2 F5 101(2) 4_756 4_756
F7 P2 F5 78.8(15) . .
F6 P2 F5 85(3) 4_756 .
F6 P2 F5 102(3) . .
F6A P2 F5 101(2) . .
F6A P2 F5 99(2) 4_756 .
F5 P2 F5 158(3) 4_756 .
F7 P2 F7A 96.9(15) . 4_756
F6 P2 F7A 90(2) 4_756 4_756
F6 P2 F7A 85(3) . 4_756
F6A P2 F7A 86(3) . 4_756
F6A P2 F7A 82(2) 4_756 4_756
F5 P2 F7A 172(3) . 4_756
F7 P2 F7A 96.9(15) . .
F6 P2 F7A 85(3) 4_756 .
F6 P2 F7A 90(2) . .
F6A P2 F7A 82(2) . .
F6A P2 F7A 86(3) 4_756 .
F5 P2 F7A 172(3) 4_756 .
F7A P2 F7A 166(3) 4_756 .
F7 P2 F5A 65.6(14) . 4_756
F6 P2 F5A 45.4(17) 4_756 4_756
F6 P2 F5A 165(2) . 4_756
F6A P2 F5A 141(2) . 4_756
F6A P2 F5A 88(2) 4_756 4_756
F5 P2 F5A 80(2) 4_756 4_756
F5 P2 F5A 90(2) . 4_756
F7A P2 F5A 82(3) 4_756 4_756
F7A P2 F5A 104(2) . 4_756
F7 P2 F5A 65.6(14) . .
F6 P2 F5A 165(2) 4_756 .
F6 P2 F5A 45.4(17) . .
F6A P2 F5A 88(2) . .
F6A P2 F5A 141(2) 4_756 .
F5 P2 F5A 90(2) 4_756 .
F5 P2 F5A 80(2) . .
F7A P2 F5A 104(2) 4_756 .
F7A P2 F5A 82(3) . .
F5A P2 F5A 131(3) 4_756 .
F12 P3 F8 89.8 . .
F12 P3 F10 91.1 . .
F8 P3 F10 90.5 . .
F12 P3 F13 91.3 . .
F8 P3 F13 178.87(9) . .
F10 P3 F13 89.5 . .
F12 P3 F11 90.5 . .
F8 P3 F11 89.7 . .
F10 P3 F11 178.47(6) . .
F13 P3 F11 90.3 . .
F12 P3 F9 179.53(12) . .
F8 P3 F9 89.8 . .
F10 P3 F9 89.2 . .
F13 P3 F9 89.0 . .
F11 P3 F9 89.2 . .
F12A P3A F8A 89.8 . .
F12A P3A F10A 91.1 . .
F8A P3A F10A 90.5 . .
F12A P3A F13A 91.3 . .
F8A P3A F13A 178.9(2) . .
F10A P3A F13A 89.5 . .
F12A P3A F11A 90.5 . .
F8A P3A F11A 89.7 . .
F10A P3A F11A 178.47(7) . .
F13A P3A F11A 90.3 . .
F12A P3A F9A 179.53(8) . .
F8A P3A F9A 89.8 . .
F10A P3A F9A 89.2 . .
F13A P3A F9A 89.0 . .
F11A P3A F9A 89.2 . .
F24 P4 F21 96(2) . .
F24 P4 F23 99(3) . .
F21 P4 F23 97(2) . .
F24 P4 F20 90(2) . .
F21 P4 F20 173(3) . .
F23 P4 F20 83(2) . .
F24 P4 F22 167(2) . .
F21 P4 F22 88(2) . .
F23 P4 F22 93(2) . .
F20 P4 F22 85(2) . .
F24 P4 F25 87(2) . .
F21 P4 F25 85(2) . .
F23 P4 F25 173(3) . .
F20 P4 F25 93.4(19) . .
F22 P4 F25 81(2) . .
F24A P4A F20A 89.8 . .
F24A P4A F23A 91.1 . .
F20A P4A F23A 90.5 . .
F24A P4A F25A 91.3 . .
F20A P4A F25A 178.86(9) . .
F23A P4A F25A 89.5 . .
F24A P4A F21A 90.5 . .
F20A P4A F21A 89.7 . .
F23A P4A F21A 178.47(15) . .
F25A P4A F21A 90.3 . .
F24A P4A F22A 179.53(14) . .
F20A P4A F22A 89.8 . .
F23A P4A F22A 89.2 . .
F25A P4A F22A 89.0 . .
F21A P4A F22A 89.2 . .
F15 P5 F16 94.9(14) . .
F15 P5 F17 98.0(14) . .
F16 P5 F17 166.6(16) . .
F15 P5 F19 95.6(15) . .
F16 P5 F19 91.2(13) . .
F17 P5 F19 91.1(12) . .
F15 P5 F18 85.8(13) . .
F16 P5 F18 89.9(12) . .
F17 P5 F18 87.5(12) . .
F19 P5 F18 178.1(15) . .
F15 P5 F14 172.4(14) . .
F16 P5 F14 80.3(13) . .
F17 P5 F14 86.5(13) . .
F19 P5 F14 90.4(12) . .
F18 P5 F14 88.2(13) . .
O4 Cl1 O2 113.1(18) . .
O4 Cl1 O3 110.4(15) . .
O2 Cl1 O3 108.9(16) . .
O4 Cl1 O1 111.6(15) . .
O2 Cl1 O1 105.1(14) . .
O3 Cl1 O1 107.4(15) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N1 1.31(4) .
C1 C5 1.39(4) .
C1 C6 1.49(4) .
C2 C3 1.34(4) .
C2 N1 1.40(3) .
C2 H2 0.9500 .
C3 C4 1.41(4) .
C3 H3 0.9500 .
C4 C5 1.38(4) .
C4 H4 0.9500 .
C5 H5 0.9500 .
C6 N2 1.31(3) .
C6 C7 1.46(4) .
C7 C8 1.33(4) .
C7 H7 0.9500 .
C8 N3 1.36(3) .
C8 H8 0.9500 .
C9 N3 1.41(3) .
C9 C10 1.52(3) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 C11 1.42(3) .
C10 C14 1.45(4) .
C11 N4 1.32(3) .
C11 H11 0.9500 .
C12 C13 1.29(4) .
C12 N4 1.43(3) .
C12 C15 1.51(3) .
C13 C14 1.39(4) .
C13 H13 0.9500 .
C14 H14 0.9500 .
C15 C19 1.31(3) .
C15 N5 1.43(3) .
C16 N5 1.31(3) .
C16 C17 1.40(3) .
C16 H16 0.9500 .
C17 C18 1.41(4) .
C17 C20 1.54(3) .
C18 C19 1.34(3) .
C18 H18 0.9500 .
C19 H19 0.9500 .
C20 N6 1.43(4) .
C20 H20A 0.9900 .
C20 H20B 0.9900 .
C21 N6 1.31(4) .
C21 C22 1.42(4) .
C21 H21 0.9500 .
C22 C23 1.40(5) .
C22 H22 0.9500 .
C23 N7 1.31(4) .
C23 C24 1.50(4) .
C24 N8 1.3900 .
C24 C28 1.3900 .
N8 C25 1.3900 .
N8 Ag2A 1.97(5) .
N8 Ag2 2.33(2) .
C25 C26 1.3900 .
C25 H25 0.9500 .
C26 C27 1.3900 .
C26 H26 0.9500 .
C27 C28 1.3900 .
C27 H27 0.9500 .
C28 H28 0.9500 .
C29 N9 1.33(3) .
C29 C33 1.38(4) .
C29 C34 1.54(4) .
C30 C31 1.30(4) .
C30 N9 1.38(3) .
C30 H30 0.9500 .
C31 C32 1.33(4) .
C31 H31 0.9500 .
C32 C33 1.39(4) .
C32 H32 0.9500 .
C33 H33 0.9500 .
C34 N10 1.28(3) .
C34 C35 1.40(4) .
C35 C36 1.35(4) .
C35 H35 0.9500 .
C36 N11 1.31(4) .
C36 H36 0.9500 .
C37 N11 1.45(3) .
C37 C38 1.54(4) .
C37 H37A 0.9900 .
C37 H37B 0.9900 .
C38 C42 1.35(4) .
C38 C39 1.40(3) .
C39 N12 1.39(3) .
C39 H39 0.9500 .
C40 N12 1.33(3) .
C40 C41 1.38(3) .
C40 C43 1.51(4) .
C41 C42 1.35(3) .
C41 H41 0.9500 .
C42 H42 0.9500 .
C43 N13 1.33(3) .
C43 C47 1.38(3) .
C44 N13 1.36(3) .
C44 C45 1.39(4) .
C44 H44 0.9500 .
C45 C46 1.40(4) .
C45 C48 1.54(4) .
C46 C47 1.34(4) .
C46 H46 0.9500 .
C47 H47 0.9500 .
C48 N14 1.44(4) .
C48 H48A 0.9900 .
C48 H48B 0.9900 .
C49 N14 1.35(4) .
C49 C50 1.35(5) .
C49 H49 0.9500 .
C50 C51 1.34(5) .
C50 H50 0.9500 .
C51 N15 1.37(5) .
C51 C52 1.38(5) .
C52 N16 1.44(4) .
C52 C56 1.47(5) .
C53 N16 1.39(4) .
C53 C54 1.42(4) .
C53 H53 0.9500 .
C54 C55 1.39(6) .
C54 H54 0.9500 .
C55 C56 1.27(6) .
C55 H55 0.9500 .
C56 H56 0.9500 .
C57 C62 1.36(4) .
C57 N17 1.3900 .
C57 C61 1.3900 .
N17 C58 1.3900 .
N17 Ag2 2.09(2) .
N17 Ag2A 2.50(4) .
C58 C59 1.3900 .
C58 H58 0.9500 .
C59 C60 1.3900 .
C59 H59 0.9500 .
C60 C61 1.3900 .
C60 H60 0.9500 .
C61 H61 0.9500 .
C62 N18 1.36(4) .
C62 C63 1.38(4) .
C63 C64 1.33(4) .
C63 H63 0.9500 .
C64 N19 1.41(4) .
C64 H64 0.9500 .
C65 N19 1.48(4) .
C65 C66 1.55(4) .
C65 H65A 0.9900 .
C65 H65B 0.9900 .
C66 C70 1.39(4) .
C66 C67 1.41(3) .
C67 N20 1.33(3) .
C67 H67 0.9500 .
C68 N20 1.36(3) .
C68 C69 1.39(3) .
C68 C71 1.47(3) .
C69 C70 1.31(3) .
C69 H69 0.9500 .
C70 H70 0.9500 .
C71 N21 1.36(3) .
C71 C75 1.40(3) .
C72 N21 1.38(3) .
C72 C73 1.40(3) .
C72 H72 0.9500 .
C73 C74 1.36(4) .
C73 C76 1.51(4) .
C74 C75 1.42(4) .
C74 H74 0.9500 .
C75 H75 0.9500 .
C76 N22 1.42(3) .
C76 H76A 0.9900 .
C76 H76B 0.9900 .
C77 N22 1.37(3) .
C77 C78 1.39(4) .
C77 H77 0.9500 .
C78 C79 1.35(4) .
C78 H78 0.9500 .
C79 N23 1.33(3) .
C79 C80 1.43(4) .
C80 N24 1.37(3) .
C80 C84 1.43(7) .
C80 C84A 1.56(7) .
C81 N24 1.28(4) .
C81 C82 1.37(5) .
C81 H81 0.9500 .
C82 C83A 1.39(7) .
C82 C83 1.52(7) .
C82 H82 0.9500 .
C83 C84 1.40(8) .
C83 H83 0.9500 .
C84 H84 0.9500 .
C83A C84A 1.42(8) .
C83A H83A 0.9500 .
C84A H84A 0.9500 .
N1 Ag1 2.24(2) .
N2 N3 1.36(3) .
N2 Ag1 2.46(2) .
N4 Fe1 1.921(18) .
N5 Fe1 1.940(19) .
N6 N7 1.32(3) .
N7 Ag2A 2.29(5) .
N7 Ag2 2.52(3) .
N9 Ag1 2.26(2) .
N10 N11 1.37(3) .
N10 Ag1 2.46(2) .
N12 Fe1 1.981(19) .
N13 Fe1 1.939(19) .
N14 N15 1.32(4) .
N15 Ag3A 2.01(4) .
N15 Ag3 2.56(3) .
N16 Ag3 2.29(2) .
N16 Ag3B 2.31(4) .
N16 Ag3A 2.47(3) .
N18 N19 1.35(4) .
N18 Ag2 2.42(3) .
N18 Ag2A 2.50(6) .
N20 Fe1 1.931(18) .
N21 Fe1 1.966(19) .
N22 N23 1.38(3) .
N23 Ag3B 2.33(4) .
N23 Ag3 2.52(2) .
N24 Ag3A 2.18(3) .
N24 Ag3 2.34(2) .
N24 Ag3B 2.49(4) .
O1E C1E 1.42(4) .
O1E H1E 0.8514 .
C1E C2E 1.49(4) .
C1E H1E1 0.9900 .
C1E H1E2 0.9900 .
C2E H2E1 0.9800 .
C2E H2E2 0.9800 .
C2E H2E3 0.9800 .
Ag1 Ag1 3.377(5) 4_656
Ag2 Ag2 3.18(2) 4_756
Ag3B O1W 2.56(3) .
P1 F1 1.53(3) .
P1 F4 1.58(3) .
P1 F3 1.59(2) .
P1 F3 1.59(2) 4_656
P1 F2 1.59(2) .
P1 F2 1.59(2) 4_656
P2 F7 1.49(3) .
P2 F6 1.54(4) 4_756
P2 F6 1.54(4) .
P2 F6A 1.58(4) .
P2 F6A 1.58(4) 4_756
P2 F5 1.59(6) 4_756
P2 F5 1.59(6) .
P2 F7A 1.64(6) 4_756
P2 F7A 1.64(6) .
P2 F5A 1.73(4) 4_756
P2 F5A 1.73(5) .
P3 F12 1.5848 .
P3 F8 1.5910 .
P3 F10 1.5934 .
P3 F13 1.5981 .
P3 F11 1.6016 .
P3 F9 1.6102 .
P3A F12A 1.5847 .
P3A F8A 1.5912 .
P3A F10A 1.5933 .
P3A F13A 1.5981 .
P3A F11A 1.6016 .
P3A F9A 1.6103 .
P4 F24 1.49(4) .
P4 F21 1.50(4) .
P4 F23 1.53(4) .
P4 F20 1.65(4) .
P4 F22 1.74(5) .
P4 F25 1.79(4) .
P4A F24A 1.5848 .
P4A F20A 1.5911 .
P4A F23A 1.5933 .
P4A F25A 1.5981 .
P4A F21A 1.6016 .
P4A F22A 1.6102 .
P5 F15 1.41(3) .
P5 F16 1.54(2) .
P5 F17 1.55(2) .
P5 F19 1.57(2) .
P5 F18 1.64(2) .
P5 F14 1.65(3) .
O1 Cl1 1.49(2) .
O2 Cl1 1.41(3) .
O3 Cl1 1.47(3) .
O4 Cl1 1.38(3) .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O1E H1E O1W 0.85 2.28 3.13(5) 179.3 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_4
N1 C2 C3 C4 3(5) .
C2 C3 C4 C5 -5(5) .
C3 C4 C5 C1 5(5) .
N1 C1 C5 C4 -3(5) .
C6 C1 C5 C4 179(3) .
N1 C1 C6 N2 9(4) .
C5 C1 C6 N2 -173(3) .
N1 C1 C6 C7 -180(3) .
C5 C1 C6 C7 -1(4) .
N2 C6 C7 C8 -4(3) .
C1 C6 C7 C8 -176(3) .
C6 C7 C8 N3 3(3) .
N3 C9 C10 C11 37(3) .
N3 C9 C10 C14 -140(2) .
C14 C10 C11 N4 1(3) .
C9 C10 C11 N4 -176(2) .
N4 C12 C13 C14 2(4) .
C15 C12 C13 C14 179(2) .
C12 C13 C14 C10 1(4) .
C11 C10 C14 C13 -2(3) .
C9 C10 C14 C13 175(2) .
C13 C12 C15 C19 0(4) .
N4 C12 C15 C19 178(2) .
C13 C12 C15 N5 177(2) .
N4 C12 C15 N5 -6(3) .
N5 C16 C17 C18 1(4) .
N5 C16 C17 C20 -176(2) .
C16 C17 C18 C19 -4(3) .
C20 C17 C18 C19 173(2) .
N5 C15 C19 C18 5(4) .
C12 C15 C19 C18 -178(2) .
C17 C18 C19 C15 0(4) .
C16 C17 C20 N6 38(3) .
C18 C17 C20 N6 -138(3) .
N6 C21 C22 C23 1(3) .
C21 C22 C23 N7 0(3) .
C21 C22 C23 C24 175(3) .
N7 C23 C24 N8 4(3) .
C22 C23 C24 N8 -171(3) .
N7 C23 C24 C28 -175(2) .
C22 C23 C24 C28 11(4) .
C28 C24 N8 C25 0.0 .
C23 C24 N8 C25 -178(2) .
C28 C24 N8 Ag2A 165.9(18) .
C23 C24 N8 Ag2A -12(2) .
C28 C24 N8 Ag2 173.3(13) .
C23 C24 N8 Ag2 -5(2) .
C24 N8 C25 C26 0.0 .
Ag2A N8 C25 C26 -165.0(18) .
Ag2 N8 C25 C26 -173.4(13) .
N8 C25 C26 C27 0.0 .
C25 C26 C27 C28 0.0 .
C26 C27 C28 C24 0.0 .
N8 C24 C28 C27 0.0 .
C23 C24 C28 C27 178(2) .
N9 C30 C31 C32 -8(5) .
C30 C31 C32 C33 6(5) .
N9 C29 C33 C32 -5(4) .
C34 C29 C33 C32 175(2) .
C31 C32 C33 C29 0(4) .
N9 C29 C34 N10 -1(4) .
C33 C29 C34 N10 179(3) .
N9 C29 C34 C35 179(3) .
C33 C29 C34 C35 -1(4) .
N10 C34 C35 C36 -1(4) .
C29 C34 C35 C36 179(3) .
C34 C35 C36 N11 3(4) .
N11 C37 C38 C42 -132(3) .
N11 C37 C38 C39 52(3) .
C42 C38 C39 N12 8(4) .
C37 C38 C39 N12 -175(2) .
N12 C40 C41 C42 9(4) .
C43 C40 C41 C42 -169(2) .
C40 C41 C42 C38 2(4) .
C39 C38 C42 C41 -10(4) .
C37 C38 C42 C41 174(2) .
N12 C40 C43 N13 -4(3) .
C41 C40 C43 N13 174(2) .
N12 C40 C43 C47 -179(2) .
C41 C40 C43 C47 -1(4) .
N13 C44 C45 C46 0(4) .
N13 C44 C45 C48 -177(3) .
C44 C45 C46 C47 -3(4) .
C48 C45 C46 C47 174(3) .
C45 C46 C47 C43 4(4) .
N13 C43 C47 C46 -2(4) .
C40 C43 C47 C46 173(2) .
C44 C45 C48 N14 36(4) .
C46 C45 C48 N14 -141(3) .
N14 C49 C50 C51 -2(4) .
C49 C50 C51 N15 0(5) .
C49 C50 C51 C52 -178(4) .
C50 C51 C52 N16 174(4) .
N15 C51 C52 N16 -4(5) .
C50 C51 C52 C56 -15(7) .
N15 C51 C52 C56 166(3) .
N16 C53 C54 C55 7(6) .
C53 C54 C55 C56 -14(7) .
C54 C55 C56 C52 18(8) .
C51 C52 C56 C55 176(5) .
N16 C52 C56 C55 -12(6) .
C62 C57 N17 C58 -175(2) .
C61 C57 N17 C58 0.0 .
C62 C57 N17 Ag2 13(2) .
C61 C57 N17 Ag2 -172.0(14) .
C62 C57 N17 Ag2A 7(2) .
C61 C57 N17 Ag2A -178.4(16) .
C57 N17 C58 C59 0.0 .
Ag2 N17 C58 C59 172.2(14) .
Ag2A N17 C58 C59 178.4(17) .
N17 C58 C59 C60 0.0 .
C58 C59 C60 C61 0.0 .
C59 C60 C61 C57 0.0 .
C62 C57 C61 C60 173(3) .
N17 C57 C61 C60 0.0 .
N17 C57 C62 N18 -17(4) .
C61 C57 C62 N18 169(3) .
N17 C57 C62 C63 167(3) .
C61 C57 C62 C63 -7(5) .
N18 C62 C63 C64 1(4) .
C57 C62 C63 C64 178(3) .
C62 C63 C64 N19 -1(4) .
N19 C65 C66 C70 -131(3) .
N19 C65 C66 C67 44(3) .
C70 C66 C67 N20 1(4) .
C65 C66 C67 N20 -174(2) .
N20 C68 C69 C70 8(4) .
C71 C68 C69 C70 -175(2) .
C68 C69 C70 C66 0(4) .
C67 C66 C70 C69 -4(4) .
C65 C66 C70 C69 171(2) .
N20 C68 C71 N21 -7(3) .
C69 C68 C71 N21 175(2) .
N20 C68 C71 C75 175(2) .
C69 C68 C71 C75 -2(4) .
N21 C72 C73 C74 0(4) .
N21 C72 C73 C76 -172(2) .
C72 C73 C74 C75 2(4) .
C76 C73 C74 C75 174(2) .
N21 C71 C75 C74 8(4) .
C68 C71 C75 C74 -175(2) .
C73 C74 C75 C71 -6(4) .
C74 C73 C76 N22 -111(3) .
C72 C73 C76 N22 62(3) .
N22 C77 C78 C79 -4(3) .
C77 C78 C79 N23 2(4) .
C77 C78 C79 C80 -177(3) .
N23 C79 C80 N24 0(4) .
C78 C79 C80 N24 179(3) .
N23 C79 C80 C84 156(4) .
C78 C79 C80 C84 -26(6) .
N23 C79 C80 C84A -169(3) .
C78 C79 C80 C84A 10(5) .
N24 C81 C82 C83A 28(7) .
N24 C81 C82 C83 -29(7) .
C81 C82 C83 C84 30(7) .
C83A C82 C83 C84 -71(5) .
C82 C83 C84 C80 -6(9) .
N24 C80 C84 C83 -18(8) .
C79 C80 C84 C83 -177(6) .
C84A C80 C84 C83 94(10) .
C81 C82 C83A C84A -41(8) .
C83 C82 C83A C84A 69(6) .
C82 C83A C84A C80 27(7) .
N24 C80 C84A C83A -3(6) .
C79 C80 C84A C83A 166(4) .
C84 C80 C84A C83A -83(8) .
C5 C1 N1 C2 0(4) .
C6 C1 N1 C2 179(2) .
C5 C1 N1 Ag1 173(2) .
C6 C1 N1 Ag1 -8(3) .
C3 C2 N1 C1 0(4) .
C3 C2 N1 Ag1 -173(2) .
C7 C6 N2 N3 4(3) .
C1 C6 N2 N3 176(2) .
C7 C6 N2 Ag1 -177.8(16) .
C1 C6 N2 Ag1 -5(3) .
C6 N2 N3 C8 -2(3) .
Ag1 N2 N3 C8 -180(2) .
C6 N2 N3 C9 -178(2) .
Ag1 N2 N3 C9 4(4) .
C7 C8 N3 N2 -1(3) .
C7 C8 N3 C9 175(2) .
C10 C9 N3 N2 60(3) .
C10 C9 N3 C8 -115(3) .
C10 C11 N4 C12 1(3) .
C10 C11 N4 Fe1 173.9(17) .
C13 C12 N4 C11 -3(3) .
C15 C12 N4 C11 179.9(18) .
C13 C12 N4 Fe1 -176.3(19) .
C15 C12 N4 Fe1 6(2) .
C17 C16 N5 C15 4(3) .
C17 C16 N5 Fe1 176.0(17) .
C19 C15 N5 C16 -8(3) .
C12 C15 N5 C16 175.1(19) .
C19 C15 N5 Fe1 179.9(18) .
C12 C15 N5 Fe1 3(2) .
C22 C21 N6 N7 -2(3) .
C22 C21 N6 C20 174(3) .
C17 C20 N6 C21 -115(3) .
C17 C20 N6 N7 61(3) .
C22 C23 N7 N6 -1(3) .
C24 C23 N7 N6 -177(2) .
C22 C23 N7 Ag2A -180(2) .
C24 C23 N7 Ag2A 5(3) .
C22 C23 N7 Ag2 175(2) .
C24 C23 N7 Ag2 -1(3) .
C21 N6 N7 C23 2(3) .
C20 N6 N7 C23 -174(2) .
C21 N6 N7 Ag2A 179(3) .
C20 N6 N7 Ag2A 2(5) .
C21 N6 N7 Ag2 -172(2) .
C20 N6 N7 Ag2 11(4) .
C33 C29 N9 C30 3(4) .
C34 C29 N9 C30 -177(2) .
C33 C29 N9 Ag1 179(2) .
C34 C29 N9 Ag1 -1(3) .
C31 C30 N9 C29 4(4) .
C31 C30 N9 Ag1 -172(2) .
C35 C34 N10 N11 -1(3) .
C29 C34 N10 N11 180(2) .
C35 C34 N10 Ag1 -177.8(19) .
C29 C34 N10 Ag1 3(3) .
C35 C36 N11 N10 -3(4) .
C35 C36 N11 C37 179(3) .
C34 N10 N11 C36 2(3) .
Ag1 N10 N11 C36 178(2) .
C34 N10 N11 C37 -180(2) .
Ag1 N10 N11 C37 -4(4) .
C38 C37 N11 C36 -129(3) .
C38 C37 N11 N10 54(3) .
C41 C40 N12 C39 -11(3) .
C43 C40 N12 C39 168(2) .
C41 C40 N12 Fe1 179.3(18) .
C43 C40 N12 Fe1 -2(3) .
C38 C39 N12 C40 2(3) .
C38 C39 N12 Fe1 171.3(17) .
C47 C43 N13 C44 -2(4) .
C40 C43 N13 C44 -177(2) .
C47 C43 N13 Fe1 -176(2) .
C40 C43 N13 Fe1 9(3) .
C45 C44 N13 C43 2(4) .
C45 C44 N13 Fe1 176(2) .
C50 C49 N14 N15 3(4) .
C50 C49 N14 C48 175(3) .
C45 C48 N14 N15 69(4) .
C45 C48 N14 C49 -103(4) .
C49 N14 N15 C51 -3(4) .
C48 N14 N15 C51 -175(3) .
C49 N14 N15 Ag3A 168(3) .
C48 N14 N15 Ag3A -4(5) .
C49 N14 N15 Ag3 154(3) .
C48 N14 N15 Ag3 -18(6) .
C50 C51 N15 N14 1(4) .
C52 C51 N15 N14 -180(3) .
C50 C51 N15 Ag3A -172(3) .
C52 C51 N15 Ag3A 7(5) .
C50 C51 N15 Ag3 -165(3) .
C52 C51 N15 Ag3 14(4) .
C54 C53 N16 C52 -2(5) .
C54 C53 N16 Ag3 -177(3) .
C54 C53 N16 Ag3B -175(3) .
C54 C53 N16 Ag3A 172(3) .
C51 C52 N16 C53 176(4) .
C56 C52 N16 C53 4(4) .
C51 C52 N16 Ag3 -9(4) .
C56 C52 N16 Ag3 178.7(19) .
C51 C52 N16 Ag3B -13(4) .
C56 C52 N16 Ag3B 175(2) .
C51 C52 N16 Ag3A 0(4) .
C56 C52 N16 Ag3A -172(2) .
C57 C62 N18 N19 -178(3) .
C63 C62 N18 N19 -2(3) .
C57 C62 N18 Ag2 11(4) .
C63 C62 N18 Ag2 -172.4(18) .
C57 C62 N18 Ag2A 17(4) .
C63 C62 N18 Ag2A -167(2) .
C62 N18 N19 C64 1(3) .
Ag2 N18 N19 C64 166(2) .
Ag2A N18 N19 C64 162(2) .
C62 N18 N19 C65 -174(2) .
Ag2 N18 N19 C65 -9(5) .
Ag2A N18 N19 C65 -14(4) .
C63 C64 N19 N18 0(3) .
C63 C64 N19 C65 175(3) .
C66 C65 N19 N18 66(3) .
C66 C65 N19 C64 -108(3) .
C66 C67 N20 C68 6(3) .
C66 C67 N20 Fe1 174.4(18) .
C69 C68 N20 C67 -10(3) .
C71 C68 N20 C67 173(2) .
C69 C68 N20 Fe1 -179.5(19) .
C71 C68 N20 Fe1 3(3) .
C75 C71 N21 C72 -6(3) .
C68 C71 N21 C72 177(2) .
C75 C71 N21 Fe1 -174.3(18) .
C68 C71 N21 Fe1 8(3) .
C73 C72 N21 C71 2(3) .
C73 C72 N21 Fe1 168.7(18) .
C78 C77 N22 N23 5(3) .
C78 C77 N22 C76 179(3) .
C73 C76 N22 C77 -118(3) .
C73 C76 N22 N23 55(3) .
C78 C79 N23 N22 1(3) .
C80 C79 N23 N22 180(2) .
C78 C79 N23 Ag3B 179(2) .
C80 C79 N23 Ag3B -2(3) .
C78 C79 N23 Ag3 -170(2) .
C80 C79 N23 Ag3 9(3) .
C77 N22 N23 C79 -3(3) .
C76 N22 N23 C79 -178(2) .
C77 N22 N23 Ag3B 179(2) .
C76 N22 N23 Ag3B 4(4) .
C77 N22 N23 Ag3 162(2) .
C76 N22 N23 Ag3 -13(4) .
C82 C81 N24 C80 -2(6) .
C82 C81 N24 Ag3A -159(4) .
C82 C81 N24 Ag3 -170(3) .
C82 C81 N24 Ag3B 178(3) .
C79 C80 N24 C81 -179(3) .
C84 C80 N24 C81 22(5) .
C84A C80 N24 C81 -10(5) .
C79 C80 N24 Ag3A -26(4) .
C84 C80 N24 Ag3A 175(3) .
C84A C80 N24 Ag3A 143(3) .
C79 C80 N24 Ag3 -10(4) .
C84 C80 N24 Ag3 -169(3) .
C84A C80 N24 Ag3 159(3) .
C79 C80 N24 Ag3B 2(3) .
C84 C80 N24 Ag3B -158(3) .
C84A C80 N24 Ag3B 171(3) .
C11 N4 Fe1 N20 97.6(18) .
C12 N4 Fe1 N20 -90.0(16) .
C11 N4 Fe1 N13 -1.9(19) .
C12 N4 Fe1 N13 170.5(16) .
C11 N4 Fe1 N5 -176.4(19) .
C12 N4 Fe1 N5 -4.0(16) .
C11 N4 Fe1 N12 -80.5(19) .
C12 N4 Fe1 N12 91.9(16) .
C67 N20 Fe1 N4 12(2) .
C68 N20 Fe1 N4 -179.7(17) .
C67 N20 Fe1 N13 109.3(19) .
C68 N20 Fe1 N13 -82.4(17) .
C67 N20 Fe1 N5 -69.7(19) .
C68 N20 Fe1 N5 98.7(17) .
C67 N20 Fe1 N21 -167(2) .
C68 N20 Fe1 N21 1.0(17) .
C44 N13 Fe1 N4 91.6(19) .
C43 N13 Fe1 N20 169.5(19) .
C44 N13 Fe1 N20 -4(2) .
C43 N13 Fe1 N12 -8.2(19) .
C44 N13 Fe1 N12 178(2) .
C16 N5 Fe1 N4 -171.0(19) .
C15 N5 Fe1 N4 0.5(16) .
C16 N5 Fe1 N20 -76.0(19) .
C15 N5 Fe1 N20 95.4(16) .
C16 N5 Fe1 N12 101.8(19) .
C15 N5 Fe1 N12 -86.8(16) .
C72 N21 Fe1 N20 -172.7(19) .
C71 N21 Fe1 N13 94.6(17) .
C72 N21 Fe1 N13 -72.7(19) .
C71 N21 Fe1 N5 -90.7(17) .
C72 N21 Fe1 N5 101.9(19) .
C71 N21 Fe1 N12 172.7(16) .
C72 N21 Fe1 N12 5(2) .
C40 N12 Fe1 N4 102.3(18) .
C39 N12 Fe1 N4 -66.6(18) .
C40 N12 Fe1 N13 5.3(18) .
C39 N12 Fe1 N13 -163.6(19) .
C40 N12 Fe1 N5 -176.0(18) .
C39 N12 Fe1 N5 15.2(19) .
C40 N12 Fe1 N21 -78.2(18) .
C39 N12 Fe1 N21 112.9(18) .
C1 N1 Ag1 N9 74(4) .
C2 N1 Ag1 N9 -114(3) .
C1 N1 Ag1 N2 4(2) .
C2 N1 Ag1 N2 177(2) .
C1 N1 Ag1 N10 -123(2) .
C2 N1 Ag1 N10 49(2) .
C1 N1 Ag1 Ag1 118(2) 4_656
C2 N1 Ag1 Ag1 -69.2(19) 4_656
C29 N9 Ag1 N1 167(3) .
C30 N9 Ag1 N1 -18(4) .
C29 N9 Ag1 N2 -128.2(18) .
C30 N9 Ag1 N2 47(2) .
C29 N9 Ag1 N10 1.9(17) .
C30 N9 Ag1 N10 177(2) .
C29 N9 Ag1 Ag1 123.1(18) 4_656
C30 N9 Ag1 Ag1 -61.5(19) 4_656
C6 N2 Ag1 N1 0.5(16) .
N3 N2 Ag1 N1 178(3) .
C6 N2 Ag1 N9 -161.7(17) .
N3 N2 Ag1 N9 16(3) .
C6 N2 Ag1 N10 122.0(17) .
N3 N2 Ag1 N10 -60(3) .
C6 N2 Ag1 Ag1 -73.0(17) 4_656
N3 N2 Ag1 Ag1 105(2) 4_656
C34 N10 Ag1 N1 -176.5(17) .
N11 N10 Ag1 N1 8(3) .
C34 N10 Ag1 N9 -2.3(17) .
N11 N10 Ag1 N9 -178(2) .
C34 N10 Ag1 N2 88(2) .
N11 N10 Ag1 N2 -88(2) .
C34 N10 Ag1 Ag1 -76.1(18) 4_656
N11 N10 Ag1 Ag1 108(2) 4_656
C57 N17 Ag2 N18 -7.0(13) .
C58 N17 Ag2 N18 -179.2(12) .
Ag2A N17 Ag2 N18 73(14) .
C57 N17 Ag2 N7 -130.4(13) .
C58 N17 Ag2 N7 57.4(13) .
Ag2A N17 Ag2 N7 -51(14) .
C57 N17 Ag2 Ag2 118.7(12) 4_756
C58 N17 Ag2 Ag2 -53.5(11) 4_756
Ag2A N17 Ag2 Ag2 -162(14) 4_756
C24 N8 Ag2 N18 -117.7(12) .
C25 N8 Ag2 N18 55.7(13) .
Ag2A N8 Ag2 N18 -61(11) .
C24 N8 Ag2 N7 3.5(11) .
C25 N8 Ag2 N7 176.8(12) .
Ag2A N8 Ag2 N7 60(11) .
C24 N8 Ag2 Ag2 117.7(11) 4_756
C25 N8 Ag2 Ag2 -69.0(10) 4_756
Ag2A N8 Ag2 Ag2 174(11) 4_756
N19 N18 Ag2 N17 -168(3) .
C62 N18 Ag2 N17 -0.9(18) .
Ag2A N18 Ag2 N17 -150(7) .
N19 N18 Ag2 N8 13(3) .
C62 N18 Ag2 N8 179.7(17) .
Ag2A N18 Ag2 N8 31(6) .
N19 N18 Ag2 N7 -67(3) .
C62 N18 Ag2 N7 99(2) .
Ag2A N18 Ag2 N7 -50(6) .
N19 N18 Ag2 Ag2 107(3) 4_756
C62 N18 Ag2 Ag2 -86.3(18) 4_756
Ag2A N18 Ag2 Ag2 125(7) 4_756
C23 N7 Ag2 N17 -173(2) .
N6 N7 Ag2 N17 1(3) .
Ag2A N7 Ag2 N17 151(9) .
C23 N7 Ag2 N8 -1.3(19) .
N6 N7 Ag2 N8 173(3) .
Ag2A N7 Ag2 N8 -37(8) .
C23 N7 Ag2 N18 103(2) .
N6 N7 Ag2 N18 -83(3) .
Ag2A N7 Ag2 N18 67(8) .
C23 N7 Ag2 Ag2 -73(2) 4_756
N6 N7 Ag2 Ag2 101(3) 4_756
Ag2A N7 Ag2 Ag2 -109(9) 4_756
C24 N8 Ag2A N7 11.6(17) .
C25 N8 Ag2A N7 177.1(13) .
Ag2 N8 Ag2A N7 -115(12) .
C24 N8 Ag2A N18 -126(2) .
C25 N8 Ag2A N18 40(3) .
Ag2 N8 Ag2A N18 107(12) .
C24 N8 Ag2A N17 109(7) .
C25 N8 Ag2A N17 -86(7) .
Ag2 N8 Ag2A N17 -19(6) .
C23 N7 Ag2A N8 -9(2) .
N6 N7 Ag2A N8 174(3) .
Ag2 N7 Ag2A N8 137(9) .
C23 N7 Ag2A N18 121(3) .
N6 N7 Ag2A N18 -56(4) .
Ag2 N7 Ag2A N18 -93(9) .
C23 N7 Ag2A N17 -170(2) .
N6 N7 Ag2A N17 13(4) .
Ag2 N7 Ag2A N17 -24(7) .
N19 N18 Ag2A N8 28(4) .
C62 N18 Ag2A N8 -170(2) .
Ag2 N18 Ag2A N8 -137(8) .
N19 N18 Ag2A N7 -84(3) .
C62 N18 Ag2A N7 78(3) .
Ag2 N18 Ag2A N7 110(8) .
N19 N18 Ag2A N17 -168(3) .
C62 N18 Ag2A N17 -6(2) .
Ag2 N18 Ag2A N17 26(6) .
C57 N17 Ag2A N8 134(7) .
C58 N17 Ag2A N8 -45(8) .
Ag2 N17 Ag2A N8 30(9) .
C57 N17 Ag2A N7 -132.8(16) .
C58 N17 Ag2A N7 49(2) .
Ag2 N17 Ag2A N7 123(15) .
C57 N17 Ag2A N18 -0.2(16) .
C58 N17 Ag2A N18 -178.6(13) .
Ag2 N17 Ag2A N18 -104(14) .
C53 N16 Ag3 N24 -93(3) .
C52 N16 Ag3 N24 91(3) .
Ag3B N16 Ag3 N24 -103(4) .
Ag3A N16 Ag3 N24 58(2) .
C53 N16 Ag3 N23 52(3) .
C52 N16 Ag3 N23 -123.2(19) .
Ag3B N16 Ag3 N23 42(4) .
Ag3A N16 Ag3 N23 -157(2) .
C53 N16 Ag3 N15 -174(3) .
C52 N16 Ag3 N15 10.9(19) .
Ag3B N16 Ag3 N15 176(4) .
Ag3A N16 Ag3 N15 -22.8(17) .
C81 N24 Ag3 N16 -25(4) .
C80 N24 Ag3 N16 165(2) .
Ag3A N24 Ag3 N16 -64(3) .
Ag3B N24 Ag3 N16 99(4) .
C81 N24 Ag3 N23 180(3) .
C80 N24 Ag3 N23 10.0(19) .
Ag3A N24 Ag3 N23 140.3(18) .
Ag3B N24 Ag3 N23 -56(4) .
C81 N24 Ag3 N15 47(3) .
C80 N24 Ag3 N15 -122(2) .
Ag3A N24 Ag3 N15 8.1(18) .
Ag3B N24 Ag3 N15 171(4) .
C79 N23 Ag3 N16 -172.8(19) .
N22 N23 Ag3 N16 22(3) .
Ag3B N23 Ag3 N16 -49(4) .
C79 N23 Ag3 N24 -10.5(19) .
N22 N23 Ag3 N24 -175(3) .
Ag3B N23 Ag3 N24 114(4) .
C79 N23 Ag3 N15 77(2) .
N22 N23 Ag3 N15 -88(3) .
Ag3B N23 Ag3 N15 -159(5) .
N14 N15 Ag3 N16 -169(4) .
C51 N15 Ag3 N16 -13(2) .
Ag3A N15 Ag3 N16 136(3) .
N14 N15 Ag3 N24 42(4) .
C51 N15 Ag3 N24 -163(3) .
Ag3A N15 Ag3 N24 -14(3) .
N14 N15 Ag3 N23 -32(5) .
C51 N15 Ag3 N23 124(3) .
Ag3A N15 Ag3 N23 -87(3) .
N14 N15 Ag3A N24 25(4) .
C51 N15 Ag3A N24 -165(3) .
Ag3 N15 Ag3A N24 161(4) .
N14 N15 Ag3A N16 -175(4) .
C51 N15 Ag3A N16 -5(3) .
Ag3 N15 Ag3A N16 -39(3) .
C81 N24 Ag3A N15 48(3) .
C80 N24 Ag3A N15 -109(3) .
Ag3 N24 Ag3A N15 -167(3) .
Ag3B N24 Ag3A N15 -174(3) .
C81 N24 Ag3A N16 -93(3) .
C80 N24 Ag3A N16 110(3) .
Ag3 N24 Ag3A N16 52(2) .
Ag3B N24 Ag3A N16 44.9(19) .
C53 N16 Ag3A N15 -173(3) .
C52 N16 Ag3A N15 2.5(18) .
Ag3 N16 Ag3A N15 151(2) .
Ag3B N16 Ag3A N15 160(2) .
C53 N16 Ag3A N24 -23(4) .
C52 N16 Ag3A N24 153(2) .
Ag3 N16 Ag3A N24 -58(2) .
Ag3B N16 Ag3A N24 -49(2) .
C53 N16 Ag3B N23 84(3) .
C52 N16 Ag3B N23 -88(4) .
Ag3 N16 Ag3B N23 -105(5) .
Ag3A N16 Ag3B N23 -116(4) .
C53 N16 Ag3B N24 -128(3) .
C52 N16 Ag3B N24 59(3) .
Ag3 N16 Ag3B N24 42(3) .
Ag3A N16 Ag3B N24 31.5(15) .
C53 N16 Ag3B O1W -9(2) .
C52 N16 Ag3B O1W 178(2) .
Ag3 N16 Ag3B O1W 161(5) .
Ag3A N16 Ag3B O1W 151(3) .
C79 N23 Ag3B N16 159(3) .
N22 N23 Ag3B N16 -23(4) .
Ag3 N23 Ag3B N16 98(5) .
C79 N23 Ag3B N24 2(2) .
N22 N23 Ag3B N24 180(3) .
Ag3 N23 Ag3B N24 -59(4) .
C79 N23 Ag3B O1W -102(2) .
N22 N23 Ag3B O1W 75(3) .
Ag3 N23 Ag3B O1W -163(5) .
C81 N24 Ag3B N16 16(4) .
C80 N24 Ag3B N16 -164(2) .
Ag3A N24 Ag3B N16 -36.3(18) .
Ag3 N24 Ag3B N16 -46(3) .
C81 N24 Ag3B N23 179(3) .
C80 N24 Ag3B N23 -1.7(19) .
Ag3A N24 Ag3B N23 126(2) .
Ag3 N24 Ag3B N23 116(4) .
C81 N24 Ag3B O1W -103(3) .
C80 N24 Ag3B O1W 77(2) .
Ag3A N24 Ag3B O1W -155(3) .
Ag3 N24 Ag3B O1W -165(5) .
