#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:06:29 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179362 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/59/4325995.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4325995
loop_
_publ_author_name
'Dongbin Dang'
'Guangshui Zheng'
'Yan Bai'
'Fan Yang'
'Hui Gao'
'Pengtao Ma'
'Jingyang Niu'
_publ_section_title
;
 Construction of Polyoxometalate-Based Inorganic-Organic Compounds Using
 Silver(I) Double Helicates as Secondary Building Blocks
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              7907
_journal_page_last               7909
_journal_paper_doi               10.1021/ic200159w
_journal_volume                  50
_journal_year                    2011
_chemical_formula_sum            'C303 H257 Ag12 Mo48 N53 O168 P4'
_chemical_formula_weight         13352.06
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.665(3)
_cell_angle_beta                 91.758(4)
_cell_angle_gamma                100.219(4)
_cell_formula_units_Z            1
_cell_length_a                   14.9901(8)
_cell_length_b                   18.0550(9)
_cell_length_c                   45.102(2)
_cell_measurement_reflns_used    7238
_cell_measurement_temperature    273(2)
_cell_measurement_theta_max      18.30
_cell_measurement_theta_min      2.23
_cell_volume                     11887.2(10)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      273(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1412
_diffrn_reflns_av_sigmaI/netI    0.1625
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       53
_diffrn_reflns_limit_l_min       -53
_diffrn_reflns_number            139381
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.37
_exptl_absorpt_coefficient_mu    1.791
_exptl_absorpt_correction_T_max  0.7750
_exptl_absorpt_correction_T_min  0.7048
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.865
_exptl_crystal_description       block
_exptl_crystal_F_000             6430
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.254
_refine_diff_density_min         -1.030
_refine_diff_density_rms         0.167
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.070
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2741
_refine_ls_number_reflns         41744
_refine_ls_number_restraints     114
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.2034
_refine_ls_R_factor_gt           0.0869
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0413P)²+42.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1721
_refine_ls_wR_factor_ref         0.1975
_reflns_number_gt                17768
_reflns_number_total             41744
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic200159w_si_001_1.cif
_cod_data_source_block           1
_cod_original_cell_volume        11887.2(11)
_cod_database_code               4325995
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P -0.0296(2) 0.4980(2) 0.25280(8) 0.0446(9) Uani 1 1 d D . .
Mo1 Mo -0.04999(10) 0.68279(7) 0.28416(3) 0.0647(4) Uani 1 1 d . . .
Mo2 Mo 0.17377(8) 0.63413(7) 0.27268(3) 0.0552(4) Uani 1 1 d . . .
Mo3 Mo -0.07303(9) 0.54063(8) 0.33031(3) 0.0568(4) Uani 1 1 d . . .
Mo4 Mo 0.13297(8) 0.47121(7) 0.30802(3) 0.0517(3) Uani 1 1 d . . .
Mo5 Mo 0.18528(9) 0.45713(8) 0.23228(3) 0.0583(4) Uani 1 1 d . . .
Mo6 Mo -0.08720(9) 0.34654(7) 0.29537(3) 0.0558(4) Uani 1 1 d . . .
Mo7 Mo -0.01775(9) 0.30990(7) 0.22271(3) 0.0556(4) Uani 1 1 d . . .
Mo8 Mo -0.22994(9) 0.35951(8) 0.23380(3) 0.0568(4) Uani 1 1 d . . .
Mo9 Mo 0.00908(9) 0.45940(8) 0.17522(3) 0.0603(4) Uani 1 1 d . . .
Mo10 Mo -0.18617(9) 0.52825(8) 0.19681(3) 0.0558(4) Uani 1 1 d . . .
Mo11 Mo -0.24284(8) 0.54298(7) 0.27550(3) 0.0549(4) Uani 1 1 d . . .
Mo12 Mo 0.02526(10) 0.64739(8) 0.20854(3) 0.0640(4) Uani 1 1 d . . .
O1 O -0.0490(6) 0.7717(5) 0.2986(2) 0.068(3) Uani 1 1 d . A .
O2 O 0.2602(7) 0.7061(7) 0.2797(3) 0.096(4) Uani 1 1 d . A .
O3 O -0.0914(6) 0.5507(6) 0.3665(2) 0.073(3) Uani 1 1 d . A .
O4 O 0.1987(7) 0.4584(6) 0.3368(2) 0.081(3) Uani 1 1 d . A .
O5 O 0.2782(7) 0.4255(5) 0.2207(2) 0.069(3) Uani 1 1 d . A .
O6 O -0.1023(7) 0.2782(5) 0.3173(2) 0.074(3) Uani 1 1 d . A .
O7 O -0.0063(7) 0.2258(5) 0.2050(2) 0.072(3) Uani 1 1 d . A .
O8 O -0.3310(6) 0.3036(5) 0.2258(2) 0.072(3) Uani 1 1 d . A .
O9 O 0.0379(7) 0.4375(6) 0.1400(2) 0.080(3) Uani 1 1 d . A .
O10 O -0.2678(8) 0.5338(6) 0.1721(2) 0.091(4) Uani 1 1 d . A .
O11 O -0.3472(7) 0.5599(6) 0.2808(2) 0.080(3) Uani 1 1 d . A .
O12 O 0.0510(7) 0.7262(6) 0.1930(3) 0.088(4) Uani 1 1 d . A .
O13 O -0.1749(7) 0.6472(6) 0.2805(2) 0.082(3) Uani 1 1 d . A .
O14 O -0.0332(8) 0.6864(7) 0.2449(2) 0.099(4) Uani 1 1 d . A .
O15 O 0.0780(8) 0.6739(6) 0.2886(2) 0.083(4) Uani 1 1 d . A .
O16 O -0.0511(7) 0.6408(6) 0.3233(2) 0.082(3) Uani 1 1 d . A .
O17 O 0.1227(7) 0.6514(6) 0.2322(2) 0.086(4) Uani 1 1 d . A .
O18 O 0.2282(7) 0.5601(5) 0.2462(2) 0.069(3) Uani 1 1 d . A .
O19 O 0.1879(6) 0.5782(5) 0.3033(2) 0.064(3) Uani 1 1 d . A .
O20 O 0.0432(7) 0.5247(6) 0.3297(2) 0.074(3) Uani 1 1 d . A .
O21 O -0.2009(7) 0.5344(6) 0.3134(2) 0.088(3) Uani 1 1 d . A .
O22 O -0.1082(6) 0.4298(5) 0.3191(2) 0.067(3) Uani 1 1 d . A .
O23 O 0.0438(6) 0.3895(5) 0.3045(2) 0.073(3) Uani 1 1 d . A .
O24 O 0.1931(7) 0.4404(5) 0.2753(2) 0.069(3) Uani 1 1 d . A .
O25 O 0.1256(7) 0.4717(6) 0.1983(2) 0.090(4) Uani 1 1 d . A .
O26 O -0.1958(7) 0.3265(6) 0.2719(2) 0.082(3) Uani 1 1 d . A .
O27 O 0.0977(7) 0.3610(6) 0.2303(2) 0.082(3) Uani 1 1 d . A .
O28 O -0.0348(7) 0.2907(6) 0.2613(2) 0.074(3) Uani 1 1 d . A .
O29 O -0.1507(6) 0.3004(6) 0.2172(2) 0.078(3) Uani 1 1 d . A .
O30 O -0.0206(7) 0.3688(6) 0.1887(2) 0.078(3) Uani 1 1 d . A .
O31 O -0.2228(7) 0.4231(5) 0.2050(2) 0.065(3) Uani 1 1 d . A .
O32 O -0.2660(7) 0.4421(5) 0.2615(2) 0.066(3) Uani 1 1 d . A .
O33 O -0.1065(6) 0.4755(5) 0.1704(3) 0.081(3) Uani 1 1 d . A .
O34 O -0.2324(6) 0.5563(5) 0.2324(2) 0.063(3) Uani 1 1 d . A .
O35 O 0.0493(7) 0.5726(6) 0.1801(3) 0.092(4) Uani 1 1 d . A .
O36 O -0.1067(7) 0.6151(6) 0.1949(2) 0.082(3) Uani 1 1 d . A .
O37 O -0.0779(7) 0.5459(6) 0.2755(2) 0.047(3) Uani 0.75 1 d PD A 1
O38 O 0.0698(6) 0.5113(6) 0.2631(2) 0.048(3) Uani 0.75 1 d PD A 1
O39 O -0.0735(7) 0.4148(5) 0.2523(2) 0.045(3) Uani 0.75 1 d PD A 1
O40 O -0.0438(8) 0.5223(6) 0.2220(2) 0.050(3) Uani 0.75 1 d PD A 1
O37' O -0.1343(12) 0.4874(18) 0.2427(7) 0.046(9) Uani 0.25 1 d PDU A 2
O38' O 0.0255(18) 0.5829(11) 0.2545(7) 0.039(8) Uani 0.25 1 d PDU A 2
O39' O 0.0265(17) 0.4504(14) 0.2303(6) 0.031(8) Uani 0.25 1 d PDU A 2
O40' O -0.0126(19) 0.4751(16) 0.2852(4) 0.034(8) Uani 0.25 1 d PDU A 2
P2 P -1.0000 0.0000 0.0000 0.0591(17) Uani 1 2 d SD . .
Mo13 Mo -0.99780(11) -0.14420(11) 0.04597(4) 0.0894(5) Uani 1 1 d . . .
Mo14 Mo -0.85032(11) 0.03518(12) 0.06496(4) 0.0967(6) Uani 1 1 d . . .
Mo15 Mo -0.84321(11) 0.17404(11) 0.01625(4) 0.0950(6) Uani 1 1 d . . .
Mo16 Mo -1.03249(12) 0.13473(11) 0.06107(4) 0.0957(6) Uani 1 1 d . . .
Mo17 Mo -1.18984(10) 0.09351(11) -0.00171(3) 0.0859(5) Uani 1 1 d . . .
Mo18 Mo -1.18193(10) -0.04359(10) 0.04751(4) 0.0826(5) Uani 1 1 d . . .
O41 O -0.9980(10) -0.2111(9) 0.0685(3) 0.140(6) Uani 1 1 d . . .
O42 O -0.7798(7) 0.0500(7) 0.0952(2) 0.100(4) Uani 1 1 d . . .
O43 O -0.7706(8) 0.2552(7) 0.0249(3) 0.115(4) Uani 1 1 d . . .
O44 O -1.0465(8) 0.1964(8) 0.0901(2) 0.106(4) Uani 1 1 d . . .
O45 O -1.2772(7) 0.1376(8) -0.0022(3) 0.121(5) Uani 1 1 d . . .
O46 O -1.2679(8) -0.0624(9) 0.0692(3) 0.122(5) Uani 1 1 d . . .
O47 O -0.8970(8) -0.1523(8) 0.0235(3) 0.128(5) Uani 1 1 d . . .
O48 O -1.0978(8) -0.0978(7) 0.0607(3) 0.101(4) Uani 1 1 d . . .
O49 O -0.9227(8) -0.0550(9) 0.0699(2) 0.126(5) Uani 1 1 d . . .
O50 O -0.8036(9) 0.1153(9) 0.0440(3) 0.133(6) Uani 1 1 d . . .
O51 O -0.9448(9) 0.0831(9) 0.0777(3) 0.140(6) Uani 1 1 d . . .
O52 O -0.7858(7) 0.1227(7) -0.0139(3) 0.104(4) Uani 1 1 d . . .
O53 O -0.9242(7) 0.1951(7) -0.0143(3) 0.095(4) Uani 1 1 d . . .
O54 O -0.9440(8) 0.1879(9) 0.0411(3) 0.126(6) Uani 1 1 d . . .
O55 O -1.1174(9) 0.0446(7) 0.0690(2) 0.103(4) Uani 1 1 d . . .
O56 O -1.1182(9) 0.1487(7) 0.0328(3) 0.109(4) Uani 1 1 d . . .
O57 O -1.2317(9) 0.0174(7) 0.0219(3) 0.107(4) Uani 1 1 d . . .
O58 O -1.2130(7) 0.0237(8) -0.0364(3) 0.126(5) Uani 1 1 d . . .
O59 O -0.9519(10) 0.0614(8) 0.0244(3) 0.064(6) Uani 0.50 1 d PD . .
O60 O -1.0742(9) 0.0263(10) 0.0179(4) 0.053(5) Uani 0.50 1 d PD . .
O61 O -1.0579(12) 0.0417(11) -0.0172(4) 0.077(7) Uani 0.50 1 d PD . .
O62 O -0.9432(11) 0.0569(9) -0.0160(3) 0.061(6) Uani 0.50 1 d PD . .
P3 P 0.0000 0.0000 0.5000 0.0493(14) Uani 1 2 d SD . .
Mo19 Mo -0.03055(12) -0.03305(9) 0.42102(3) 0.0819(5) Uani 1 1 d . . .
Mo20 Mo 0.18981(9) 0.04101(9) 0.45548(3) 0.0659(4) Uani 1 1 d . . .
Mo21 Mo 0.01836(12) 0.15550(9) 0.45870(3) 0.0835(5) Uani 1 1 d . . .
Mo22 Mo 0.03905(12) 0.18876(9) 0.53796(4) 0.0900(5) Uani 1 1 d . . .
Mo23 Mo 0.21759(9) 0.08138(9) 0.53497(4) 0.0750(5) Uani 1 1 d . . .
Mo24 Mo 0.17605(9) -0.10989(9) 0.49939(3) 0.0707(4) Uani 1 1 d . . .
O63 O -0.0387(8) -0.0487(7) 0.3836(2) 0.096(4) Uani 1 1 d . . .
O64 O 0.2773(9) 0.0603(8) 0.4347(3) 0.136(6) Uani 1 1 d . . .
O65 O 0.0268(8) 0.2284(6) 0.4393(3) 0.101(4) Uani 1 1 d . . .
O66 O 0.0599(7) 0.2775(5) 0.5557(2) 0.072(3) Uani 1 1 d . . .
O67 O 0.3209(8) 0.1181(7) 0.5506(3) 0.106(4) Uani 1 1 d . . .
O68 O 0.2568(8) -0.1634(6) 0.4981(3) 0.098(4) Uani 1 1 d . . .
O69 O -0.1514(9) -0.0509(7) 0.4325(3) 0.133(6) Uani 1 1 d . . .
O70 O 0.0995(8) -0.0105(6) 0.4265(3) 0.095(4) Uani 1 1 d . . .
O71 O -0.0285(8) 0.0720(6) 0.4285(2) 0.099(4) Uani 1 1 d . . .
O72 O 0.1333(8) 0.1272(7) 0.4540(2) 0.097(4) Uani 1 1 d . . .
O73 O 0.0568(8) 0.2055(8) 0.4979(2) 0.126(5) Uani 1 1 d . . .
O74 O -0.0877(8) 0.1727(8) 0.5291(2) 0.125(5) Uani 1 1 d . . .
O75 O 0.0204(9) 0.1316(7) 0.5699(3) 0.133(6) Uani 1 1 d . . .
O76 O 0.1608(10) 0.1658(8) 0.5363(3) 0.149(7) Uani 1 1 d . . .
O77 O 0.2379(6) 0.0899(6) 0.4946(2) 0.073(3) Uani 1 1 d . . .
O78 O 0.2285(7) -0.0231(6) 0.5257(2) 0.074(3) Uani 1 1 d . . .
O79 O 0.1035(8) -0.1460(9) 0.5283(3) 0.135(6) Uani 1 1 d . . .
O80 O 0.2051(7) -0.0511(5) 0.4677(2) 0.073(3) Uani 1 1 d . . .
O81 O -0.0307(11) 0.0754(7) 0.4978(3) 0.048(5) Uani 0.50 1 d PD . .
O82 O 0.0558(10) 0.0477(9) 0.5271(3) 0.054(5) Uani 0.50 1 d PD . .
O83 O 0.0986(7) 0.0066(9) 0.4956(4) 0.046(5) Uani 0.50 1 d PD . .
O84 O 0.0405(10) 0.0292(9) 0.4728(3) 0.044(4) Uani 0.50 1 d PD . .
Ag1 Ag -0.62595(9) 0.22031(11) 0.07950(3) 0.1112(6) Uani 1 1 d . . .
Ag2 Ag -0.39143(9) 0.32748(8) 0.15211(3) 0.0867(5) Uani 1 1 d . . .
N1 N -0.5461(10) 0.2213(11) 0.0385(3) 0.099(6) Uani 1 1 d . . .
N2 N -0.5032(10) 0.3384(9) 0.0837(3) 0.093(5) Uani 1 1 d . . .
N3 N -0.4774(9) 0.3752(8) 0.1124(3) 0.087(5) Uani 1 1 d . . .
N4 N -0.4588(8) 0.4199(8) 0.1740(3) 0.073(4) Uani 1 1 d . . .
N5 N -0.7271(10) 0.2408(9) 0.1138(4) 0.094(5) Uani 1 1 d . . .
N6 N -0.5721(8) 0.1959(7) 0.1275(3) 0.076(4) Uani 1 1 d . . .
N7 N -0.4809(8) 0.1984(7) 0.1362(3) 0.073(4) Uani 1 1 d . . .
N8 N -0.2977(8) 0.2454(8) 0.1418(3) 0.061(3) Uani 1 1 d . . .
C1 C -0.5810(11) 0.1738(13) 0.0130(4) 0.112(8) Uani 1 1 d . . .
H1A H -0.6346 0.1395 0.0140 0.135 Uiso 1 1 calc R . .
C2 C -0.5418(15) 0.1744(16) -0.0133(5) 0.133(9) Uani 1 1 d . . .
H2A H -0.5652 0.1412 -0.0305 0.160 Uiso 1 1 calc R . .
C3 C -0.4652(18) 0.2275(16) -0.0128(4) 0.136(9) Uani 1 1 d . . .
H3A H -0.4348 0.2315 -0.0304 0.163 Uiso 1 1 calc R . .
C4 C -0.4300(15) 0.2771(14) 0.0135(4) 0.123(8) Uani 1 1 d . . .
H4A H -0.3778 0.3135 0.0131 0.148 Uiso 1 1 calc R . .
C5 C -0.4707(14) 0.2712(12) 0.0376(4) 0.086(6) Uani 1 1 d . . .
C6 C -0.4409(12) 0.3214(9) 0.0672(4) 0.083(6) Uani 1 1 d . . .
C7 C -0.3413(13) 0.3408(12) 0.0745(4) 0.084(6) Uani 1 1 d . . .
C8 C -0.2845(13) 0.2895(11) 0.0660(4) 0.084(5) Uani 1 1 d . . .
H8A H -0.3101 0.2438 0.0543 0.101 Uiso 1 1 calc R . .
C9 C -0.1934(16) 0.3019(15) 0.0736(5) 0.115(7) Uani 1 1 d . . .
H9A H -0.1580 0.2659 0.0674 0.138 Uiso 1 1 calc R . .
C10 C -0.1575(16) 0.3677(17) 0.0905(5) 0.118(9) Uani 1 1 d . . .
H10A H -0.0957 0.3762 0.0958 0.142 Uiso 1 1 calc R . .
C11 C -0.2030(18) 0.4218(18) 0.1003(5) 0.150(11) Uani 1 1 d . . .
H11A H -0.1747 0.4664 0.1122 0.180 Uiso 1 1 calc R . .
C12 C -0.3034(14) 0.4077(13) 0.0912(4) 0.099(6) Uani 1 1 d . . .
H12A H -0.3383 0.4444 0.0970 0.119 Uiso 1 1 calc R . .
C13 C -0.5241(12) 0.4224(11) 0.1236(4) 0.094(6) Uani 1 1 d . . .
C14 C -0.6020(13) 0.4440(12) 0.1068(5) 0.124(8) Uani 1 1 d D . .
C15 C -0.5878(18) 0.4695(17) 0.0793(6) 0.202(16) Uani 1 1 d D . .
H15A H -0.5317 0.4698 0.0710 0.242 Uiso 1 1 calc R . .
C16 C -0.656(2) 0.494(2) 0.0641(6) 0.26(2) Uani 1 1 d D . .
H16A H -0.6440 0.5194 0.0476 0.310 Uiso 1 1 calc R . .
C17 C -0.7423(19) 0.480(2) 0.0745(7) 0.22(2) Uani 1 1 d D . .
H17A H -0.7910 0.4872 0.0625 0.261 Uiso 1 1 calc R . .
C18 C -0.7590(16) 0.457(2) 0.1021(7) 0.23(2) Uani 1 1 d D . .
H18A H -0.8170 0.4509 0.1092 0.273 Uiso 1 1 calc R . .
C19 C -0.6866(14) 0.4421(13) 0.1188(5) 0.178(13) Uani 1 1 d D . .
H19A H -0.6947 0.4309 0.1382 0.213 Uiso 1 1 calc R . .
C20 C -0.5028(11) 0.4553(11) 0.1563(4) 0.079(5) Uani 1 1 d . . .
C21 C -0.5266(15) 0.5250(11) 0.1673(5) 0.120(8) Uani 1 1 d . . .
H21A H -0.5552 0.5512 0.1546 0.144 Uiso 1 1 calc R . .
C22 C -0.5077(17) 0.5545(14) 0.1968(5) 0.146(11) Uani 1 1 d . . .
H22A H -0.5222 0.6013 0.2042 0.175 Uiso 1 1 calc R . .
C23 C -0.4670(13) 0.5142(10) 0.2154(4) 0.097(6) Uani 1 1 d . . .
H23A H -0.4564 0.5317 0.2358 0.117 Uiso 1 1 calc R . .
C24 C -0.4428(10) 0.4481(10) 0.2033(4) 0.075(5) Uani 1 1 d . . .
H24A H -0.4139 0.4213 0.2157 0.090 Uiso 1 1 calc R . .
C25 C -0.8024(12) 0.2657(14) 0.1062(4) 0.130(9) Uani 1 1 d . . .
H25A H -0.8092 0.2794 0.0872 0.156 Uiso 1 1 calc R . .
C26 C -0.8682(15) 0.2714(14) 0.1254(6) 0.131(10) Uani 1 1 d . . .
H26A H -0.9200 0.2886 0.1195 0.157 Uiso 1 1 calc R . .
C27 C -0.8600(16) 0.2519(14) 0.1542(7) 0.148(12) Uani 1 1 d . . .
H27A H -0.9047 0.2553 0.1679 0.177 Uiso 1 1 calc R . .
C28 C -0.7826(11) 0.2278(10) 0.1606(4) 0.093(6) Uani 1 1 d . . .
H28A H -0.7753 0.2124 0.1792 0.112 Uiso 1 1 calc R . .
C29 C -0.7133(11) 0.2242(9) 0.1412(5) 0.072(5) Uani 1 1 d . . .
C30 C -0.6231(11) 0.2066(10) 0.1487(4) 0.078(5) Uani 1 1 d . . .
C31 C -0.5964(12) 0.2113(11) 0.1807(5) 0.087(6) Uani 1 1 d . . .
C32 C -0.6036(13) 0.2748(11) 0.2022(5) 0.105(7) Uani 1 1 d . . .
H32A H -0.6272 0.3157 0.1968 0.125 Uiso 1 1 calc R . .
C33 C -0.5739(18) 0.2733(16) 0.2317(6) 0.131(10) Uani 1 1 d . . .
H33A H -0.5802 0.3129 0.2464 0.157 Uiso 1 1 calc R . .
C34 C -0.5352(14) 0.2135(18) 0.2393(6) 0.115(8) Uani 1 1 d . . .
H34A H -0.5140 0.2146 0.2590 0.138 Uiso 1 1 calc R . .
C35 C -0.5280(13) 0.1561(13) 0.2194(6) 0.116(9) Uani 1 1 d . . .
H35A H -0.5045 0.1155 0.2252 0.139 Uiso 1 1 calc R . .
C36 C -0.5548(11) 0.1551(12) 0.1903(5) 0.085(6) Uani 1 1 d . . .
H36A H -0.5449 0.1152 0.1763 0.102 Uiso 1 1 calc R . .
C37 C -0.4334(11) 0.1560(9) 0.1199(3) 0.067(4) Uani 1 1 d . . .
C38 C -0.4675(10) 0.0981(10) 0.0936(4) 0.072(5) Uani 1 1 d . . .
C39 C -0.5551(12) 0.0537(11) 0.0943(5) 0.097(6) Uani 1 1 d . . .
H39A H -0.5901 0.0609 0.1107 0.116 Uiso 1 1 calc R . .
C40 C -0.5881(13) -0.0018(13) 0.0694(5) 0.119(8) Uani 1 1 d . . .
H40A H -0.6446 -0.0327 0.0698 0.142 Uiso 1 1 calc R . .
C41 C -0.5379(14) -0.0110(14) 0.0445(5) 0.127(9) Uani 1 1 d . . .
H41A H -0.5595 -0.0483 0.0284 0.153 Uiso 1 1 calc R . .
C42 C -0.4526(14) 0.0377(13) 0.0440(4) 0.108(7) Uani 1 1 d . . .
H42A H -0.4188 0.0349 0.0271 0.129 Uiso 1 1 calc R . .
C43 C -0.4207(11) 0.0892(10) 0.0692(3) 0.075(5) Uani 1 1 d . . .
H43A H -0.3636 0.1193 0.0690 0.090 Uiso 1 1 calc R . .
C44 C -0.3338(9) 0.1755(11) 0.1292(3) 0.063(5) Uani 1 1 d . . .
C45 C -0.2826(10) 0.1176(8) 0.1243(3) 0.060(4) Uani 1 1 d . . .
H45A H -0.3092 0.0688 0.1154 0.071 Uiso 1 1 calc R . .
C46 C -0.1924(11) 0.1350(11) 0.1331(3) 0.073(5) Uani 1 1 d . . .
H46A H -0.1564 0.0979 0.1304 0.088 Uiso 1 1 calc R . .
C47 C -0.1560(12) 0.2070(12) 0.1457(3) 0.082(6) Uani 1 1 d . . .
H47A H -0.0944 0.2202 0.1513 0.098 Uiso 1 1 calc R . .
C48 C -0.2109(10) 0.2596(10) 0.1502(3) 0.072(5) Uani 1 1 d . . .
H48A H -0.1857 0.3081 0.1596 0.086 Uiso 1 1 calc R . .
Ag3 Ag 0.03458(8) -0.10121(8) 0.25553(4) 0.0862(4) Uani 1 1 d . . .
Ag4 Ag -0.02486(9) 0.13772(7) 0.29039(3) 0.0767(4) Uani 1 1 d . . .
N9 N 0.1739(8) -0.0794(8) 0.2432(3) 0.061(3) Uani 1 1 d . . .
N10 N 0.0689(8) 0.0238(7) 0.2343(3) 0.064(3) Uani 1 1 d . . .
N11 N 0.0026(8) 0.0666(6) 0.2416(3) 0.051(3) Uani 1 1 d . . .
N12 N -0.1491(8) 0.1209(7) 0.2592(3) 0.054(3) Uani 1 1 d . . .
N13 N 0.0622(8) 0.1667(7) 0.3311(3) 0.059(3) Uani 1 1 d . . .
N14 N -0.0269(8) 0.0170(7) 0.3152(3) 0.058(3) Uani 1 1 d . . .
N15 N -0.0522(8) -0.0481(7) 0.2947(3) 0.055(3) Uani 1 1 d . . .
N16 N -0.1122(8) -0.1509(7) 0.2454(3) 0.064(3) Uani 1 1 d . . .
C49 C 0.2227(13) -0.1389(10) 0.2385(4) 0.081(5) Uani 1 1 d . . .
H49A H 0.1996 -0.1877 0.2424 0.097 Uiso 1 1 calc R . .
C50 C 0.3110(14) -0.1191(13) 0.2271(5) 0.107(7) Uani 1 1 d . . .
H50A H 0.3430 -0.1582 0.2220 0.128 Uiso 1 1 calc R . .
C51 C 0.3500(13) -0.0504(14) 0.2232(6) 0.131(9) Uani 1 1 d . . .
H51A H 0.4100 -0.0407 0.2179 0.157 Uiso 1 1 calc R . .
C52 C 0.2989(11) 0.0092(10) 0.2272(4) 0.095(6) Uani 1 1 d . . .
H52A H 0.3219 0.0581 0.2234 0.114 Uiso 1 1 calc R . .
C53 C 0.2099(11) -0.0111(9) 0.2376(3) 0.062(4) Uani 1 1 d . . .
C54 C 0.1545(11) 0.0535(9) 0.2439(3) 0.058(4) Uani 1 1 d . . .
C55 C 0.1926(10) 0.1274(9) 0.2595(3) 0.054(4) Uani 1 1 d . . .
C56 C 0.2651(11) 0.1378(10) 0.2801(4) 0.074(5) Uani 1 1 d . . .
H56A H 0.2918 0.0964 0.2829 0.088 Uiso 1 1 calc R . .
C57 C 0.2977(12) 0.2044(11) 0.2959(4) 0.084(6) Uani 1 1 d . . .
H57A H 0.3475 0.2092 0.3093 0.101 Uiso 1 1 calc R . .
C58 C 0.2597(12) 0.2665(11) 0.2929(4) 0.080(5) Uani 1 1 d . . .
H58A H 0.2804 0.3127 0.3049 0.096 Uiso 1 1 calc R . .
C59 C 0.1904(11) 0.2588(9) 0.2718(4) 0.077(5) Uani 1 1 d . . .
H59A H 0.1657 0.3013 0.2690 0.092 Uiso 1 1 calc R . .
C60 C 0.1559(11) 0.1905(9) 0.2545(4) 0.072(5) Uani 1 1 d . . .
H60A H 0.1095 0.1866 0.2399 0.086 Uiso 1 1 calc R . .
C61 C -0.0626(10) 0.0616(8) 0.2217(4) 0.057(4) Uani 1 1 d . . .
C62 C -0.0606(13) 0.0208(12) 0.1914(4) 0.075(5) Uani 1 1 d . . .
C63 C 0.0030(13) 0.0544(11) 0.1730(4) 0.095(6) Uani 1 1 d . . .
H63A H 0.0424 0.0994 0.1803 0.114 Uiso 1 1 calc R . .
C64 C 0.008(3) 0.0207(19) 0.1434(6) 0.171(16) Uani 1 1 d . . .
H64A H 0.0514 0.0422 0.1313 0.205 Uiso 1 1 calc R . .
C65 C -0.049(3) -0.040(3) 0.1331(7) 0.19(2) Uani 1 1 d . . .
H65A H -0.0470 -0.0606 0.1131 0.233 Uiso 1 1 calc R . .
C66 C -0.117(2) -0.0786(17) 0.1520(8) 0.162(13) Uani 1 1 d . . .
H66A H -0.1547 -0.1244 0.1447 0.195 Uiso 1 1 calc R . .
C67 C -0.1205(15) -0.0415(13) 0.1820(4) 0.108(7) Uani 1 1 d . . .
H67A H -0.1643 -0.0609 0.1945 0.129 Uiso 1 1 calc R . .
C68 C -0.1431(9) 0.0936(8) 0.2314(3) 0.052(4) Uani 1 1 d . . .
C69 C -0.2136(10) 0.0932(9) 0.2093(4) 0.073(5) Uani 1 1 d . . .
H69A H -0.2092 0.0732 0.1894 0.088 Uiso 1 1 calc R . .
C70 C -0.2890(12) 0.1235(10) 0.2184(4) 0.084(5) Uani 1 1 d . . .
H70A H -0.3341 0.1281 0.2045 0.101 Uiso 1 1 calc R . .
C71 C -0.2950(9) 0.1466(8) 0.2484(4) 0.061(4) Uani 1 1 d . . .
H71A H -0.3481 0.1610 0.2553 0.073 Uiso 1 1 calc R . .
C72 C -0.2232(10) 0.1487(8) 0.2685(3) 0.058(4) Uani 1 1 d . . .
H72A H -0.2257 0.1692 0.2884 0.070 Uiso 1 1 calc R . .
C73 C 0.0885(10) 0.2370(10) 0.3456(4) 0.070(5) Uani 1 1 d . . .
H73A H 0.0736 0.2775 0.3369 0.085 Uiso 1 1 calc R . .
C74 C 0.1373(11) 0.2526(11) 0.3732(4) 0.083(6) Uani 1 1 d . . .
H74A H 0.1570 0.3024 0.3824 0.100 Uiso 1 1 calc R . .
C75 C 0.1554(12) 0.1934(12) 0.3865(4) 0.079(5) Uani 1 1 d . . .
H75A H 0.1862 0.2023 0.4052 0.095 Uiso 1 1 calc R . .
C76 C 0.1280(12) 0.1204(11) 0.3723(4) 0.077(5) Uani 1 1 d . . .
H76A H 0.1395 0.0793 0.3813 0.092 Uiso 1 1 calc R . .
C77 C 0.0843(9) 0.1094(10) 0.3450(3) 0.061(4) Uani 1 1 d . . .
C78 C 0.0563(10) 0.0309(9) 0.3283(3) 0.055(4) Uani 1 1 d . . .
C79 C 0.1232(10) -0.0187(10) 0.3273(3) 0.060(4) Uani 1 1 d . . .
C80 C 0.2153(11) 0.0130(9) 0.3277(3) 0.067(4) Uani 1 1 d . . .
H80A H 0.2338 0.0655 0.3313 0.080 Uiso 1 1 calc R . .
C81 C 0.2801(12) -0.0341(12) 0.3227(4) 0.083(5) Uani 1 1 d . . .
H81A H 0.3412 -0.0126 0.3226 0.100 Uiso 1 1 calc R . .
C82 C 0.2540(15) -0.1101(11) 0.3181(4) 0.086(6) Uani 1 1 d . . .
H82A H 0.2974 -0.1411 0.3156 0.103 Uiso 1 1 calc R . .
C83 C 0.1655(15) -0.1416(12) 0.3170(4) 0.093(6) Uani 1 1 d . . .
H83A H 0.1491 -0.1941 0.3124 0.112 Uiso 1 1 calc R . .
C84 C 0.0982(11) -0.0996(9) 0.3224(3) 0.064(4) Uani 1 1 d . . .
H84A H 0.0379 -0.1232 0.3228 0.077 Uiso 1 1 calc R . .
C85 C -0.1377(10) -0.0720(8) 0.2904(3) 0.054(4) Uani 1 1 d . . .
C86 C -0.2088(11) -0.0426(9) 0.3090(4) 0.067(4) Uani 1 1 d . . .
C87 C -0.2026(12) -0.0439(11) 0.3403(5) 0.098(6) Uani 1 1 d . . .
H87A H -0.1547 -0.0608 0.3493 0.118 Uiso 1 1 calc R . .
C88 C -0.2727(16) -0.0183(12) 0.3580(5) 0.116(7) Uani 1 1 d . . .
H88A H -0.2743 -0.0230 0.3783 0.139 Uiso 1 1 calc R . .
C89 C -0.3357(15) 0.0125(12) 0.3446(6) 0.110(8) Uani 1 1 d . . .
H89A H -0.3780 0.0324 0.3564 0.132 Uiso 1 1 calc R . .
C90 C -0.3409(12) 0.0162(11) 0.3141(6) 0.097(6) Uani 1 1 d . . .
H90A H -0.3851 0.0385 0.3057 0.117 Uiso 1 1 calc R . .
C91 C -0.2806(11) -0.0134(9) 0.2970(4) 0.070(5) Uani 1 1 d . . .
H91A H -0.2865 -0.0145 0.2763 0.084 Uiso 1 1 calc R . .
C92 C -0.1715(10) -0.1355(8) 0.2656(3) 0.055(4) Uani 1 1 d . . .
C93 C -0.2589(10) -0.1766(10) 0.2641(4) 0.073(5) Uani 1 1 d . . .
H93A H -0.2990 -0.1681 0.2790 0.087 Uiso 1 1 calc R . .
C94 C -0.2840(12) -0.2326(10) 0.2386(4) 0.088(6) Uani 1 1 d . . .
H94A H -0.3428 -0.2605 0.2363 0.106 Uiso 1 1 calc R . .
C95 C -0.2244(14) -0.2459(11) 0.2180(4) 0.091(6) Uani 1 1 d . . .
H95A H -0.2404 -0.2836 0.2016 0.109 Uiso 1 1 calc R . .
C96 C -0.1402(12) -0.2028(10) 0.2217(4) 0.066(4) Uani 1 1 d . . .
H96A H -0.0997 -0.2100 0.2068 0.079 Uiso 1 1 calc R . .
Ag5 Ag 0.57191(8) 0.74774(9) 0.42650(3) 0.0900(5) Uani 1 1 d . . .
Ag6 Ag 0.34010(8) 0.64558(7) 0.35352(3) 0.0724(4) Uani 1 1 d . . .
N17 N 0.2487(7) 0.7269(7) 0.3679(2) 0.049(3) Uani 1 1 d . . .
N18 N 0.4291(8) 0.7731(6) 0.3717(2) 0.056(3) Uani 1 1 d . . .
N19 N 0.5222(7) 0.7796(6) 0.3796(2) 0.053(3) Uani 1 1 d . . .
N20 N 0.6800(8) 0.7394(7) 0.3933(3) 0.063(3) Uani 1 1 d . . .
N21 N 0.4957(10) 0.7398(9) 0.4673(3) 0.079(4) Uani 1 1 d . . .
N22 N 0.4512(8) 0.6276(7) 0.4209(3) 0.056(3) Uani 1 1 d . . .
N23 N 0.4275(7) 0.5952(7) 0.3914(3) 0.055(3) Uani 1 1 d . . .
N24 N 0.4071(7) 0.5538(7) 0.3308(3) 0.057(3) Uani 1 1 d . . .
C97 C 0.1581(9) 0.7081(9) 0.3634(3) 0.060(4) Uani 1 1 d . . .
H97A H 0.1347 0.6605 0.3527 0.072 Uiso 1 1 calc R . .
C98 C 0.0986(11) 0.7523(10) 0.3729(3) 0.074(5) Uani 1 1 d . . .
H98A H 0.0363 0.7369 0.3688 0.088 Uiso 1 1 calc R . .
C99 C 0.1349(12) 0.8213(13) 0.3890(4) 0.100(7) Uani 1 1 d . . .
H99A H 0.0967 0.8527 0.3974 0.120 Uiso 1 1 calc R . .
C100 C 0.2292(11) 0.8452(9) 0.3929(3) 0.073(5) Uani 1 1 d . . .
H10B H 0.2536 0.8944 0.4018 0.088 Uiso 1 1 calc R . .
C101 C 0.2847(9) 0.7961(8) 0.3835(3) 0.049(4) Uani 1 1 d . . .
C102 C 0.3852(9) 0.8160(8) 0.3880(3) 0.050(4) Uani 1 1 d . . .
C103 C 0.4284(11) 0.8810(9) 0.4097(3) 0.057(4) Uani 1 1 d . . .
C104 C 0.4007(10) 0.8893(10) 0.4394(4) 0.079(5) Uani 1 1 d . . .
H10C H 0.3527 0.8542 0.4447 0.094 Uiso 1 1 calc R . .
C105 C 0.4437(13) 0.9495(12) 0.4613(4) 0.088(6) Uani 1 1 d . . .
H10D H 0.4235 0.9551 0.4806 0.106 Uiso 1 1 calc R . .
C106 C 0.5143(13) 0.9983(10) 0.4535(5) 0.092(6) Uani 1 1 d . . .
H10E H 0.5444 1.0372 0.4678 0.110 Uiso 1 1 calc R . .
C107 C 0.5431(14) 0.9924(13) 0.4251(5) 0.124(8) Uani 1 1 d . . .
H10F H 0.5912 1.0275 0.4199 0.149 Uiso 1 1 calc R . .
C108 C 0.5003(12) 0.9343(11) 0.4047(4) 0.086(6) Uani 1 1 d . . .
H10G H 0.5220 0.9306 0.3856 0.103 Uiso 1 1 calc R . .
C109 C 0.5729(9) 0.7681(8) 0.3577(3) 0.052(4) Uani 1 1 d . . .
C110 C 0.5438(9) 0.7674(9) 0.3256(3) 0.053(4) Uani 1 1 d . . .
C111 C 0.5103(11) 0.8268(9) 0.3157(4) 0.075(5) Uani 1 1 d . . .
H11B H 0.5081 0.8704 0.3290 0.090 Uiso 1 1 calc R . .
C112 C 0.4795(12) 0.8215(13) 0.2857(5) 0.097(7) Uani 1 1 d . . .
H11C H 0.4583 0.8613 0.2783 0.116 Uiso 1 1 calc R . .
C113 C 0.4823(13) 0.7537(15) 0.2675(4) 0.098(7) Uani 1 1 d . . .
H11D H 0.4588 0.7464 0.2478 0.118 Uiso 1 1 calc R . .
C114 C 0.5171(14) 0.7002(11) 0.2776(5) 0.102(7) Uani 1 1 d . . .
H11E H 0.5223 0.6577 0.2641 0.122 Uiso 1 1 calc R . .
C115 C 0.5461(12) 0.7025(10) 0.3063(4) 0.082(5) Uani 1 1 d . . .
H11F H 0.5669 0.6615 0.3128 0.098 Uiso 1 1 calc R . .
C116 C 0.6648(9) 0.7574(8) 0.3654(3) 0.050(4) Uani 1 1 d . . .
C117 C 0.7332(12) 0.7641(11) 0.3466(4) 0.090(6) Uani 1 1 d . . .
H11G H 0.7229 0.7770 0.3277 0.108 Uiso 1 1 calc R . .
C118 C 0.8181(13) 0.7520(12) 0.3550(5) 0.100(6) Uani 1 1 d . . .
H11H H 0.8655 0.7571 0.3421 0.120 Uiso 1 1 calc R . .
C119 C 0.8302(12) 0.7323(12) 0.3828(5) 0.100(7) Uani 1 1 d . . .
H11I H 0.8873 0.7250 0.3891 0.120 Uiso 1 1 calc R . .
C120 C 0.7627(11) 0.7231(10) 0.4015(4) 0.086(6) Uani 1 1 d . . .
H12B H 0.7715 0.7059 0.4197 0.103 Uiso 1 1 calc R . .
C121 C 0.5253(12) 0.7836(11) 0.4932(4) 0.092(6) Uani 1 1 d . . .
H12C H 0.5777 0.8201 0.4934 0.111 Uiso 1 1 calc R . .
C122 C 0.4821(15) 0.7778(12) 0.5200(4) 0.096(6) Uani 1 1 d . . .
H12D H 0.5040 0.8097 0.5376 0.115 Uiso 1 1 calc R . .
C123 C 0.4068(16) 0.7236(14) 0.5191(4) 0.105(7) Uani 1 1 d . . .
H12E H 0.3765 0.7171 0.5365 0.126 Uiso 1 1 calc R . .
C124 C 0.3746(11) 0.6777(10) 0.4926(4) 0.077(5) Uani 1 1 d . . .
H12F H 0.3223 0.6409 0.4918 0.092 Uiso 1 1 calc R . .
C125 C 0.4223(11) 0.6882(10) 0.4674(3) 0.058(4) Uani 1 1 d . . .
C126 C 0.3858(10) 0.6410(8) 0.4380(3) 0.052(4) Uani 1 1 d . . .
C127 C 0.2900(10) 0.6206(10) 0.4321(3) 0.063(4) Uani 1 1 d . . .
C128 C 0.2350(13) 0.6699(11) 0.4410(4) 0.086(6) Uani 1 1 d . . .
H12G H 0.2596 0.7157 0.4527 0.103 Uiso 1 1 calc R . .
C129 C 0.1418(16) 0.6543(16) 0.4330(5) 0.109(7) Uani 1 1 d . . .
H12H H 0.1047 0.6894 0.4385 0.131 Uiso 1 1 calc R . .
C130 C 0.1079(15) 0.5841(18) 0.4167(6) 0.119(8) Uani 1 1 d . . .
H13A H 0.0455 0.5714 0.4123 0.142 Uiso 1 1 calc R . .
C131 C 0.1592(15) 0.5330(14) 0.4066(4) 0.112(7) Uani 1 1 d . . .
H13B H 0.1343 0.4874 0.3947 0.135 Uiso 1 1 calc R . .
C132 C 0.2522(13) 0.5521(12) 0.4150(4) 0.090(6) Uani 1 1 d . . .
H13C H 0.2896 0.5175 0.4090 0.108 Uiso 1 1 calc R . .
C133 C 0.4765(10) 0.5485(8) 0.3793(3) 0.056(4) Uani 1 1 d . . .
C134 C 0.5473(11) 0.5203(9) 0.3957(4) 0.065(4) Uani 1 1 d . . .
C135 C 0.5267(15) 0.4808(13) 0.4194(5) 0.116(7) Uani 1 1 d . . .
H13D H 0.4672 0.4707 0.4251 0.139 Uiso 1 1 calc R . .
C136 C 0.598(2) 0.4550(14) 0.4354(6) 0.137(8) Uani 1 1 d U . .
H13E H 0.5871 0.4267 0.4512 0.164 Uiso 1 1 calc R . .
C137 C 0.684(2) 0.476(2) 0.4255(8) 0.167(13) Uani 1 1 d . . .
H13F H 0.7308 0.4616 0.4365 0.201 Uiso 1 1 calc R . .
C138 C 0.711(2) 0.512(2) 0.4028(8) 0.169(14) Uani 1 1 d . . .
H13G H 0.7709 0.5224 0.3972 0.202 Uiso 1 1 calc R . .
C139 C 0.6374(13) 0.5347(10) 0.3880(4) 0.092(6) Uani 1 1 d . . .
H13H H 0.6503 0.5611 0.3718 0.110 Uiso 1 1 calc R . .
C140 C 0.4590(9) 0.5189(8) 0.3473(3) 0.051(4) Uani 1 1 d . . .
C141 C 0.4938(11) 0.4592(9) 0.3339(4) 0.075(5) Uani 1 1 d . . .
H14A H 0.5275 0.4341 0.3455 0.090 Uiso 1 1 calc R . .
C142 C 0.4803(11) 0.4346(10) 0.3032(4) 0.091(6) Uani 1 1 d . . .
H14B H 0.5070 0.3954 0.2940 0.110 Uiso 1 1 calc R . .
C143 C 0.4289(11) 0.4683(9) 0.2878(4) 0.076(5) Uani 1 1 d . . .
H14C H 0.4169 0.4527 0.2673 0.091 Uiso 1 1 calc R . .
C144 C 0.3924(10) 0.5273(9) 0.3021(4) 0.069(5) Uani 1 1 d . . .
H14D H 0.3550 0.5500 0.2908 0.082 Uiso 1 1 calc R . .
O85 O 0.699(3) 0.655(2) 0.5618(8) 0.184(14) Uiso 0.50 1 d PD . .
N25 N 0.7022(16) 0.6455(13) 0.5138(5) 0.075(8) Uiso 0.50 1 d PD . .
C145 C 0.707(3) 0.6989(18) 0.5395(6) 0.154(18) Uiso 0.50 1 d PD . .
H14E H 0.7138 0.7515 0.5410 0.185 Uiso 0.50 1 calc PR . .
C146 C 0.643(3) 0.5761(19) 0.5126(9) 0.22(3) Uiso 0.50 1 d PD . .
H14F H 0.6298 0.5665 0.5326 0.328 Uiso 0.50 1 calc PR . .
H14G H 0.6705 0.5361 0.5028 0.328 Uiso 0.50 1 calc PR . .
H14H H 0.5876 0.5779 0.5017 0.328 Uiso 0.50 1 calc PR . .
C147 C 0.728(2) 0.6709(18) 0.4868(5) 0.105(13) Uiso 0.50 1 d PD . .
H14I H 0.7233 0.6281 0.4713 0.157 Uiso 0.50 1 calc PR . .
H14J H 0.7903 0.6974 0.4892 0.157 Uiso 0.50 1 calc PR . .
H14K H 0.6899 0.7047 0.4814 0.157 Uiso 0.50 1 calc PR . .
O86 O -0.333(2) 0.188(2) 0.4180(8) 0.180(12) Uiso 0.50 1 d PDU . .
N26 N -0.2084(19) 0.1986(15) 0.3901(7) 0.120(9) Uiso 0.50 1 d PDU . .
C148 C -0.253(2) 0.166(2) 0.4132(8) 0.128(10) Uiso 0.50 1 d PDU . .
H14L H -0.2300 0.1327 0.4242 0.154 Uiso 0.50 1 calc PR . .
C149 C -0.213(3) 0.2741(18) 0.3873(11) 0.192(16) Uiso 0.50 1 d PDU . .
H14M H -0.2707 0.2847 0.3935 0.288 Uiso 0.50 1 calc PR . .
H14N H -0.2062 0.2818 0.3668 0.288 Uiso 0.50 1 calc PR . .
H14O H -0.1653 0.3075 0.3997 0.288 Uiso 0.50 1 calc PR . .
C150 C -0.1297(18) 0.1732(17) 0.3807(7) 0.085(10) Uiso 0.50 1 d PDU . .
H15B H -0.1400 0.1186 0.3783 0.128 Uiso 0.50 1 calc PR . .
H15C H -0.0807 0.1933 0.3954 0.128 Uiso 0.50 1 calc PR . .
H15D H -0.1142 0.1901 0.3619 0.128 Uiso 0.50 1 calc PR . .
O87 O -0.525(3) 0.114(2) 0.3355(9) 0.199(13) Uiso 0.50 1 d PDU . .
N27 N -0.535(3) 0.1963(17) 0.3689(7) 0.153(11) Uiso 0.50 1 d PDU . .
C151 C -0.491(3) 0.188(2) 0.3424(8) 0.165(12) Uiso 0.50 1 d PDU . .
H15E H -0.4517 0.2221 0.3328 0.198 Uiso 0.50 1 calc PR . .
C152 C -0.572(3) 0.135(2) 0.3830(10) 0.179(16) Uiso 0.50 1 d PDU . .
H15F H -0.6079 0.0969 0.3687 0.268 Uiso 0.50 1 calc PR . .
H15G H -0.6087 0.1521 0.3986 0.268 Uiso 0.50 1 calc PR . .
H15H H -0.5235 0.1147 0.3916 0.268 Uiso 0.50 1 calc PR . .
C153 C -0.540(4) 0.2690(19) 0.3825(10) 0.196(17) Uiso 0.50 1 d PDU . .
H15I H -0.5805 0.2658 0.3985 0.294 Uiso 0.50 1 calc PR . .
H15J H -0.5619 0.2968 0.3680 0.294 Uiso 0.50 1 calc PR . .
H15K H -0.4806 0.2948 0.3904 0.294 Uiso 0.50 1 calc PR . .
O88 O 0.442(2) 0.7417(17) 0.1920(6) 0.133(10) Uiso 0.50 1 d PD . .
N28 N 0.3222(18) 0.6768(17) 0.1623(6) 0.107(10) Uiso 0.50 1 d PD . .
C154 C 0.411(2) 0.717(2) 0.1635(7) 0.160(19) Uiso 0.50 1 d PD . .
H15L H 0.4436 0.7256 0.1468 0.191 Uiso 0.50 1 calc PR . .
C155 C 0.280(3) 0.645(3) 0.1346(7) 0.24(3) Uiso 0.50 1 d PD . .
H15M H 0.3076 0.6717 0.1193 0.358 Uiso 0.50 1 calc PR . .
H15N H 0.2165 0.6485 0.1347 0.358 Uiso 0.50 1 calc PR . .
H15O H 0.2854 0.5924 0.1307 0.358 Uiso 0.50 1 calc PR . .
C156 C 0.289(3) 0.648(3) 0.1878(8) 0.19(2) Uiso 0.50 1 d PD . .
H15P H 0.2272 0.6227 0.1836 0.287 Uiso 0.50 1 calc PR . .
H15Q H 0.2915 0.6895 0.2038 0.287 Uiso 0.50 1 calc PR . .
H15R H 0.3253 0.6133 0.1935 0.287 Uiso 0.50 1 calc PR . .
O89 O -0.416(4) -0.072(4) 0.2133(12) 0.16(2) Uiso 0.25 1 d PD . .
N29 N -0.421(5) -0.071(3) 0.1652(8) 0.17(3) Uiso 0.25 1 d PD . .
C157 C -0.401(5) -0.114(3) 0.1874(10) 0.11(3) Uiso 0.25 1 d PD . .
H15S H -0.3821 -0.1606 0.1850 0.134 Uiso 0.25 1 calc PR . .
C158 C -0.418(4) -0.101(3) 0.1351(8) 0.08(2) Uiso 0.25 1 d PD . .
H15T H -0.4387 -0.0672 0.1227 0.120 Uiso 0.25 1 calc PR . .
H15U H -0.4555 -0.1499 0.1311 0.120 Uiso 0.25 1 calc PR . .
H15V H -0.3561 -0.1046 0.1309 0.120 Uiso 0.25 1 calc PR . .
C159 C -0.464(3) -0.009(2) 0.1729(8) 0.020(10) Uiso 0.25 1 d PD . .
H15W H -0.4792 0.0106 0.1551 0.031 Uiso 0.25 1 calc PR . .
H15X H -0.4233 0.0296 0.1860 0.031 Uiso 0.25 1 calc PR . .
H15Y H -0.5179 -0.0250 0.1830 0.031 Uiso 0.25 1 calc PR . .
O90 O -0.676(4) -0.018(3) 0.1495(16) 0.18(3) Uiso 0.25 1 d PD . .
N30 N -0.785(3) -0.118(3) 0.1423(11) 0.11(2) Uiso 0.25 1 d PD . .
C160 C -0.764(4) -0.042(3) 0.1541(17) 0.14(3) Uiso 0.25 1 d PD . .
H16B H -0.8035 -0.0124 0.1633 0.166 Uiso 0.25 1 calc PR . .
C161 C -0.875(3) -0.154(4) 0.1437(18) 0.15(4) Uiso 0.25 1 d PD . .
H16C H -0.8802 -0.2076 0.1374 0.222 Uiso 0.25 1 calc PR . .
H16D H -0.9128 -0.1333 0.1307 0.222 Uiso 0.25 1 calc PR . .
H16E H -0.8928 -0.1453 0.1639 0.222 Uiso 0.25 1 calc PR . .
C162 C -0.743(4) -0.140(3) 0.1160(11) 0.09(2) Uiso 0.25 1 d PD . .
H16F H -0.6816 -0.1129 0.1172 0.136 Uiso 0.25 1 calc PR . .
H16G H -0.7757 -0.1270 0.0992 0.136 Uiso 0.25 1 calc PR . .
H16H H -0.7441 -0.1934 0.1134 0.136 Uiso 0.25 1 calc PR . .
O1W O -0.123(5) 0.363(4) -0.0012(16) 0.17(3) Uiso 0.25 1 d P . .
O2W O 0.054(5) 0.601(4) 0.5203(17) 0.19(3) Uiso 0.25 1 d P . .
O3W O -0.358(4) 0.324(3) 0.3146(12) 0.127(19) Uiso 0.25 1 d P . .
O4W O 0.185(3) 0.574(3) 0.5147(11) 0.112(17) Uiso 0.25 1 d P . .
O5W O -1.255(6) -0.309(5) 0.1315(19) 0.21(3) Uiso 0.25 1 d P B 1
O6W O -1.130(4) -0.326(3) 0.1215(13) 0.13(2) Uiso 0.25 1 d P C 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O38 P1 O39 110.9(6) . .
O38 P1 O40 112.3(6) . .
O39 P1 O40 110.0(6) . .
O38 P1 O37 107.9(6) . .
O39 P1 O37 107.7(6) . .
O40 P1 O37 107.9(6) . .
O38 P1 O37' 177.5(13) . .
O39 P1 O37' 71.1(12) . .
O40 P1 O37' 67.9(12) . .
O37 P1 O37' 69.8(12) . .
O38 P1 O40' 66.4(11) . .
O39 P1 O40' 71.8(12) . .
O40 P1 O40' 178.2(13) . .
O37 P1 O40' 71.6(10) . .
O37' P1 O40' 113.3(16) . .
O38 P1 O38' 63.4(11) . .
O39 P1 O38' 174.3(12) . .
O40 P1 O38' 73.3(12) . .
O37 P1 O38' 75.0(11) . .
O37' P1 O38' 114.6(16) . .
O40' P1 O38' 104.8(16) . .
O38 P1 O39' 68.6(11) . .
O39 P1 O39' 74.4(11) . .
O40 P1 O39' 73.7(11) . .
O37 P1 O39' 176.5(12) . .
O37' P1 O39' 113.7(16) . .
O40' P1 O39' 106.7(14) . .
O38' P1 O39' 102.7(15) . .
O1 Mo1 O14 104.6(5) . .
O1 Mo1 O13 99.4(5) . .
O14 Mo1 O13 97.3(5) . .
O1 Mo1 O15 102.7(5) . .
O14 Mo1 O15 87.4(4) . .
O13 Mo1 O15 155.5(4) . .
O1 Mo1 O16 96.5(5) . .
O14 Mo1 O16 157.6(5) . .
O13 Mo1 O16 86.8(4) . .
O15 Mo1 O16 80.4(4) . .
O1 Mo1 O37 163.1(4) . .
O14 Mo1 O37 90.8(4) . .
O13 Mo1 O37 71.1(4) . .
O15 Mo1 O37 84.8(4) . .
O16 Mo1 O37 69.6(4) . .
O1 Mo1 O38' 150.3(6) . .
O14 Mo1 O38' 60.5(7) . .
O13 Mo1 O38' 107.6(6) . .
O15 Mo1 O38' 54.1(7) . .
O16 Mo1 O38' 97.2(7) . .
O37 Mo1 O38' 45.2(5) . .
O2 Mo2 O15 103.4(6) . .
O2 Mo2 O19 102.8(5) . .
O15 Mo2 O19 95.1(4) . .
O2 Mo2 O18 101.2(5) . .
O15 Mo2 O18 153.9(5) . .
O19 Mo2 O18 88.0(4) . .
O2 Mo2 O17 101.5(5) . .
O15 Mo2 O17 85.9(4) . .
O19 Mo2 O17 154.8(5) . .
O18 Mo2 O17 80.7(4) . .
O2 Mo2 O38' 151.3(7) . .
O15 Mo2 O38' 59.7(8) . .
O19 Mo2 O38' 101.8(7) . .
O18 Mo2 O38' 94.3(8) . .
O17 Mo2 O38' 57.2(7) . .
O2 Mo2 O38 168.2(5) . .
O15 Mo2 O38 87.0(4) . .
O19 Mo2 O38 70.1(4) . .
O18 Mo2 O38 69.7(4) . .
O17 Mo2 O38 84.8(4) . .
O38' Mo2 O38 40.0(6) . .
O3 Mo3 O20 102.9(5) . .
O3 Mo3 O16 101.4(5) . .
O20 Mo3 O16 98.0(5) . .
O3 Mo3 O22 101.6(5) . .
O20 Mo3 O22 85.8(4) . .
O16 Mo3 O22 155.2(4) . .
O3 Mo3 O21 99.5(5) . .
O20 Mo3 O21 155.6(5) . .
O16 Mo3 O21 87.0(4) . .
O22 Mo3 O21 80.2(4) . .
O3 Mo3 O37 164.7(4) . .
O20 Mo3 O37 91.1(4) . .
O16 Mo3 O37 70.0(4) . .
O22 Mo3 O37 85.5(4) . .
O21 Mo3 O37 68.1(4) . .
O3 Mo3 O40' 151.6(6) . .
O20 Mo3 O40' 57.8(7) . .
O16 Mo3 O40' 101.9(7) . .
O22 Mo3 O40' 59.5(7) . .
O21 Mo3 O40' 97.8(7) . .
O37 Mo3 O40' 43.2(5) . .
O4 Mo4 O23 102.9(5) . .
O4 Mo4 O24 103.3(5) . .
O23 Mo4 O24 97.1(4) . .
O4 Mo4 O20 100.6(5) . .
O23 Mo4 O20 84.5(4) . .
O24 Mo4 O20 154.9(4) . .
O4 Mo4 O19 100.0(5) . .
O23 Mo4 O19 154.9(4) . .
O24 Mo4 O19 87.4(4) . .
O20 Mo4 O19 81.2(4) . .
O4 Mo4 O40' 151.7(6) . .
O23 Mo4 O40' 59.8(7) . .
O24 Mo4 O40' 101.1(6) . .
O20 Mo4 O40' 58.1(7) . .
O19 Mo4 O40' 95.1(7) . .
O4 Mo4 O38 166.0(5) . .
O23 Mo4 O38 90.4(4) . .
O24 Mo4 O38 70.1(4) . .
O20 Mo4 O38 84.9(4) . .
O19 Mo4 O38 67.8(4) . .
O40' Mo4 O38 41.1(6) . .
O5 Mo5 O25 105.3(5) . .
O5 Mo5 O18 103.5(4) . .
O25 Mo5 O18 96.3(5) . .
O5 Mo5 O27 101.2(4) . .
O25 Mo5 O27 86.5(4) . .
O18 Mo5 O27 153.4(4) . .
O5 Mo5 O24 99.3(4) . .
O25 Mo5 O24 153.8(5) . .
O18 Mo5 O24 86.5(4) . .
O27 Mo5 O24 79.9(4) . .
O5 Mo5 O39' 151.4(6) . .
O25 Mo5 O39' 59.4(7) . .
O18 Mo5 O39' 102.2(6) . .
O27 Mo5 O39' 56.8(7) . .
O24 Mo5 O39' 94.5(7) . .
O5 Mo5 O38 164.3(4) . .
O25 Mo5 O38 89.8(5) . .
O18 Mo5 O38 69.8(4) . .
O27 Mo5 O38 83.8(4) . .
O24 Mo5 O38 66.7(3) . .
O39' Mo5 O38 42.2(6) . .
O6 Mo6 O22 104.2(5) . .
O6 Mo6 O26 102.8(5) . .
O22 Mo6 O26 97.6(4) . .
O6 Mo6 O28 98.3(5) . .
O22 Mo6 O28 155.5(4) . .
O26 Mo6 O28 86.8(4) . .
O6 Mo6 O23 100.8(5) . .
O22 Mo6 O23 85.9(4) . .
O26 Mo6 O23 154.5(5) . .
O28 Mo6 O23 80.3(4) . .
O6 Mo6 O39 163.6(4) . .
O22 Mo6 O39 91.1(4) . .
O26 Mo6 O39 68.8(4) . .
O28 Mo6 O39 67.9(4) . .
O23 Mo6 O39 85.9(4) . .
O6 Mo6 O40' 151.0(6) . .
O22 Mo6 O40' 60.8(6) . .
O26 Mo6 O40' 103.8(6) . .
O28 Mo6 O40' 94.7(6) . .
O23 Mo6 O40' 56.0(6) . .
O39 Mo6 O40' 43.6(5) . .
O7 Mo7 O27 104.1(5) . .
O7 Mo7 O28 102.7(5) . .
O27 Mo7 O28 95.2(5) . .
O7 Mo7 O29 99.3(5) . .
O27 Mo7 O29 155.1(5) . .
O28 Mo7 O29 87.7(4) . .
O7 Mo7 O30 101.1(5) . .
O27 Mo7 O30 85.5(4) . .
O28 Mo7 O30 155.3(4) . .
O29 Mo7 O30 81.8(4) . .
O7 Mo7 O39 164.6(4) . .
O27 Mo7 O39 90.0(4) . .
O28 Mo7 O39 69.3(4) . .
O29 Mo7 O39 67.9(4) . .
O30 Mo7 O39 86.0(4) . .
O7 Mo7 O39' 149.8(6) . .
O27 Mo7 O39' 55.6(7) . .
O28 Mo7 O39' 101.5(7) . .
O29 Mo7 O39' 99.5(6) . .
O30 Mo7 O39' 58.8(7) . .
O39 Mo7 O39' 45.0(5) . .
O8 Mo8 O31 103.2(5) . .
O8 Mo8 O29 103.1(5) . .
O31 Mo8 O29 96.3(4) . .
O8 Mo8 O26 100.1(5) . .
O31 Mo8 O26 155.7(5) . .
O29 Mo8 O26 84.9(4) . .
O8 Mo8 O32 99.5(4) . .
O31 Mo8 O32 87.5(4) . .
O29 Mo8 O32 155.4(4) . .
O26 Mo8 O32 81.9(4) . .
O8 Mo8 O39 165.2(4) . .
O31 Mo8 O39 90.6(4) . .
O29 Mo8 O39 69.7(4) . .
O26 Mo8 O39 66.9(4) . .
O32 Mo8 O39 86.1(4) . .
O8 Mo8 O37' 150.4(6) . .
O31 Mo8 O37' 59.0(7) . .
O29 Mo8 O37' 102.4(7) . .
O26 Mo8 O37' 96.9(7) . .
O32 Mo8 O37' 59.1(7) . .
O39 Mo8 O37' 43.2(6) . .
O9 Mo9 O30 104.6(5) . .
O9 Mo9 O33 103.2(5) . .
O30 Mo9 O33 96.2(5) . .
O9 Mo9 O25 102.4(5) . .
O30 Mo9 O25 86.7(4) . .
O33 Mo9 O25 152.6(5) . .
O9 Mo9 O35 99.3(5) . .
O30 Mo9 O35 154.2(5) . .
O33 Mo9 O35 87.4(4) . .
O25 Mo9 O35 78.9(5) . .
O9 Mo9 O40 164.5(4) . .
O30 Mo9 O40 89.3(4) . .
O33 Mo9 O40 67.9(4) . .
O25 Mo9 O40 84.9(4) . .
O35 Mo9 O40 68.4(4) . .
O9 Mo9 O39' 150.2(6) . .
O30 Mo9 O39' 59.5(7) . .
O33 Mo9 O39' 103.5(6) . .
O25 Mo9 O39' 54.9(7) . .
O35 Mo9 O39' 94.8(7) . .
O40 Mo9 O39' 44.1(5) . .
O10 Mo10 O36 101.8(6) . .
O10 Mo10 O34 103.1(5) . .
O36 Mo10 O34 98.3(4) . .
O10 Mo10 O31 101.0(5) . .
O36 Mo10 O31 155.0(4) . .
O34 Mo10 O31 86.1(4) . .
O10 Mo10 O33 100.3(5) . .
O36 Mo10 O33 87.0(4) . .
O34 Mo10 O33 154.3(4) . .
O31 Mo10 O33 79.1(4) . .
O10 Mo10 O40 165.4(5) . .
O36 Mo10 O40 70.8(4) . .
O34 Mo10 O40 90.6(4) . .
O31 Mo10 O40 84.6(4) . .
O33 Mo10 O40 67.3(4) . .
O10 Mo10 O37' 151.3(7) . .
O36 Mo10 O37' 102.9(7) . .
O34 Mo10 O37' 59.0(7) . .
O31 Mo10 O37' 58.4(7) . .
O33 Mo10 O37' 95.3(7) . .
O40 Mo10 O37' 42.1(6) . .
O11 Mo11 O32 101.4(5) . .
O11 Mo11 O21 103.0(5) . .
O32 Mo11 O21 96.7(5) . .
O11 Mo11 O13 99.9(5) . .
O32 Mo11 O13 156.1(5) . .
O21 Mo11 O13 88.8(4) . .
O11 Mo11 O34 100.4(4) . .
O32 Mo11 O34 84.7(4) . .
O21 Mo11 O34 155.8(4) . .
O13 Mo11 O34 81.0(4) . .
O11 Mo11 O37 166.7(4) . .
O32 Mo11 O37 91.3(4) . .
O21 Mo11 O37 71.1(4) . .
O13 Mo11 O37 68.5(4) . .
O34 Mo11 O37 84.7(4) . .
O11 Mo11 O37' 149.5(6) . .
O32 Mo11 O37' 60.3(7) . .
O21 Mo11 O37' 103.3(7) . .
O13 Mo11 O37' 95.8(8) . .
O34 Mo11 O37' 56.5(7) . .
O37 Mo11 O37' 42.4(6) . .
O12 Mo12 O17 102.5(5) . .
O12 Mo12 O35 104.2(6) . .
O17 Mo12 O35 96.1(5) . .
O12 Mo12 O14 100.5(5) . .
O17 Mo12 O14 86.9(5) . .
O35 Mo12 O14 153.9(5) . .
O12 Mo12 O36 100.3(5) . .
O17 Mo12 O36 155.2(5) . .
O35 Mo12 O36 87.7(5) . .
O14 Mo12 O36 79.4(5) . .
O12 Mo12 O40 165.8(5) . .
O17 Mo12 O40 91.4(4) . .
O35 Mo12 O40 71.0(4) . .
O14 Mo12 O40 83.0(4) . .
O36 Mo12 O40 66.7(4) . .
O12 Mo12 O38' 148.7(7) . .
O17 Mo12 O38' 55.9(7) . .
O35 Mo12 O38' 100.8(7) . .
O14 Mo12 O38' 59.8(7) . .
O36 Mo12 O38' 99.3(7) . .
O40 Mo12 O38' 44.1(5) . .
Mo1 O13 Mo11 129.8(6) . .
Mo1 O14 Mo12 147.0(6) . .
Mo2 O15 Mo1 147.7(6) . .
Mo3 O16 Mo1 129.3(6) . .
Mo12 O17 Mo2 147.3(6) . .
Mo5 O18 Mo2 130.7(5) . .
Mo2 O19 Mo4 130.8(5) . .
Mo3 O20 Mo4 146.5(6) . .
Mo11 O21 Mo3 130.5(6) . .
Mo6 O22 Mo3 146.2(5) . .
Mo4 O23 Mo6 147.7(6) . .
Mo4 O24 Mo5 132.9(5) . .
Mo5 O25 Mo9 147.4(6) . .
Mo6 O26 Mo8 132.2(6) . .
Mo7 O27 Mo5 148.6(6) . .
Mo7 O28 Mo6 131.5(5) . .
Mo8 O29 Mo7 131.9(6) . .
Mo9 O30 Mo7 147.5(6) . .
Mo8 O31 Mo10 145.4(5) . .
Mo11 O32 Mo8 145.9(5) . .
Mo9 O33 Mo10 133.4(6) . .
Mo10 O34 Mo11 147.7(5) . .
Mo12 O35 Mo9 131.0(6) . .
Mo10 O36 Mo12 131.4(6) . .
P1 O37 Mo1 124.7(6) . .
P1 O37 Mo11 125.7(6) . .
Mo1 O37 Mo11 90.5(3) . .
P1 O37 Mo3 124.3(5) . .
Mo1 O37 Mo3 91.0(3) . .
Mo11 O37 Mo3 90.1(3) . .
P1 O38 Mo2 126.6(6) . .
P1 O38 Mo4 126.3(6) . .
Mo2 O38 Mo4 90.9(3) . .
P1 O38 Mo5 122.3(6) . .
Mo2 O38 Mo5 89.7(3) . .
Mo4 O38 Mo5 90.2(3) . .
P1 O39 Mo6 125.8(6) . .
P1 O39 Mo8 124.7(6) . .
Mo6 O39 Mo8 92.0(3) . .
P1 O39 Mo7 122.8(6) . .
Mo6 O39 Mo7 91.0(3) . .
Mo8 O39 Mo7 90.6(3) . .
P1 O40 Mo10 127.3(6) . .
P1 O40 Mo12 123.9(6) . .
Mo10 O40 Mo12 90.9(3) . .
P1 O40 Mo9 123.4(6) . .
Mo10 O40 Mo9 91.1(3) . .
Mo12 O40 Mo9 89.5(3) . .
P1 O37' Mo10 122.4(16) . .
P1 O37' Mo8 120.5(16) . .
Mo10 O37' Mo8 95.6(8) . .
P1 O37' Mo11 121.4(16) . .
Mo10 O37' Mo11 96.1(8) . .
Mo8 O37' Mo11 94.1(8) . .
P1 O38' Mo2 129.6(16) . .
P1 O38' Mo12 118.6(15) . .
Mo2 O38' Mo12 98.1(7) . .
P1 O38' Mo1 113.9(13) . .
Mo2 O38' Mo1 96.8(8) . .
Mo12 O38' Mo1 91.9(8) . .
P1 O39' Mo5 126.6(15) . .
P1 O39' Mo7 117.8(14) . .
Mo5 O39' Mo7 97.6(8) . .
P1 O39' Mo9 118.0(14) . .
Mo5 O39' Mo9 96.5(7) . .
Mo7 O39' Mo9 93.5(8) . .
P1 O40' Mo4 125.4(14) . .
P1 O40' Mo3 120.8(13) . .
Mo4 O40' Mo3 96.6(8) . .
P1 O40' Mo6 118.3(15) . .
Mo4 O40' Mo6 95.7(7) . .
Mo3 O40' Mo6 92.8(8) . .
O62 P2 O62 180.0(11) . 2_355
O62 P2 O60 62.9(9) . 2_355
O62 P2 O60 117.1(9) 2_355 2_355
O62 P2 O60 117.1(9) . .
O62 P2 O60 62.9(9) 2_355 .
O60 P2 O60 180.0(13) 2_355 .
O62 P2 O61 68.6(11) . .
O62 P2 O61 111.4(11) 2_355 .
O60 P2 O61 112.9(10) 2_355 .
O60 P2 O61 67.1(10) . .
O62 P2 O61 111.4(11) . 2_355
O62 P2 O61 68.6(11) 2_355 2_355
O60 P2 O61 67.1(10) 2_355 2_355
O60 P2 O61 112.9(10) . 2_355
O61 P2 O61 180.0(10) . 2_355
O62 P2 O59 105.5(9) . 2_355
O62 P2 O59 74.5(9) 2_355 2_355
O60 P2 O59 74.7(9) 2_355 2_355
O60 P2 O59 105.3(9) . 2_355
O61 P2 O59 76.9(10) . 2_355
O61 P2 O59 103.1(10) 2_355 2_355
O62 P2 O59 74.5(9) . .
O62 P2 O59 105.5(9) 2_355 .
O60 P2 O59 105.3(9) 2_355 .
O60 P2 O59 74.7(9) . .
O61 P2 O59 103.1(10) . .
O61 P2 O59 76.9(10) 2_355 .
O59 P2 O59 180.0(14) 2_355 .
O41 Mo13 O53 102.2(7) . 2_355
O41 Mo13 O47 103.4(7) . .
O53 Mo13 O47 91.6(5) 2_355 .
O41 Mo13 O48 100.8(6) . .
O53 Mo13 O48 87.4(5) 2_355 .
O47 Mo13 O48 155.4(6) . .
O41 Mo13 O49 102.1(7) . .
O53 Mo13 O49 155.4(6) 2_355 .
O47 Mo13 O49 86.9(5) . .
O48 Mo13 O49 83.9(5) . .
O41 Mo13 O61 160.4(6) . 2_355
O53 Mo13 O61 91.6(6) 2_355 2_355
O47 Mo13 O61 61.9(6) . 2_355
O48 Mo13 O61 93.6(5) . 2_355
O49 Mo13 O61 66.1(6) . 2_355
O41 Mo13 O62 159.1(6) . 2_355
O53 Mo13 O62 67.5(5) 2_355 2_355
O47 Mo13 O62 95.3(6) . 2_355
O48 Mo13 O62 61.7(5) . 2_355
O49 Mo13 O62 88.1(6) . 2_355
O61 Mo13 O62 40.3(5) 2_355 2_355
O42 Mo14 O49 101.2(6) . .
O42 Mo14 O51 103.4(6) . .
O49 Mo14 O51 87.6(6) . .
O42 Mo14 O50 102.8(6) . .
O49 Mo14 O50 155.5(6) . .
O51 Mo14 O50 91.4(6) . .
O42 Mo14 O58 101.5(5) . 2_355
O49 Mo14 O58 87.0(6) . 2_355
O51 Mo14 O58 155.1(6) . 2_355
O50 Mo14 O58 83.6(6) . 2_355
O42 Mo14 O59 160.1(5) . .
O49 Mo14 O59 94.3(5) . .
O51 Mo14 O59 64.5(5) . .
O50 Mo14 O59 63.5(6) . .
O58 Mo14 O59 91.7(5) 2_355 .
O43 Mo15 O52 102.1(6) . .
O43 Mo15 O50 101.1(7) . .
O52 Mo15 O50 89.9(6) . .
O43 Mo15 O53 103.6(6) . .
O52 Mo15 O53 88.3(5) . .
O50 Mo15 O53 155.0(6) . .
O43 Mo15 O54 103.5(6) . .
O52 Mo15 O54 154.2(6) . .
O50 Mo15 O54 88.7(5) . .
O53 Mo15 O54 82.2(5) . .
O43 Mo15 O59 157.9(6) . .
O52 Mo15 O59 94.7(5) . .
O50 Mo15 O59 64.4(6) . .
O53 Mo15 O59 90.9(5) . .
O54 Mo15 O59 61.6(6) . .
O43 Mo15 O62 159.9(5) . .
O52 Mo15 O62 63.8(5) . .
O50 Mo15 O62 93.5(6) . .
O53 Mo15 O62 63.5(5) . .
O54 Mo15 O62 90.5(6) . .
O59 Mo15 O62 42.2(5) . .
O44 Mo16 O54 103.6(7) . .
O44 Mo16 O56 102.5(6) . .
O54 Mo16 O56 89.1(6) . .
O44 Mo16 O51 101.4(6) . .
O54 Mo16 O51 90.6(5) . .
O56 Mo16 O51 155.5(6) . .
O44 Mo16 O55 100.8(6) . .
O54 Mo16 O55 155.6(6) . .
O56 Mo16 O55 87.9(5) . .
O51 Mo16 O55 82.3(6) . .
O44 Mo16 O59 158.4(5) . .
O54 Mo16 O59 62.5(6) . .
O56 Mo16 O59 94.1(5) . .
O51 Mo16 O59 64.4(6) . .
O55 Mo16 O59 93.6(5) . .
O44 Mo16 O60 158.6(5) . .
O54 Mo16 O60 93.8(6) . .
O56 Mo16 O60 64.9(5) . .
O51 Mo16 O60 90.7(6) . .
O55 Mo16 O60 63.0(5) . .
O59 Mo16 O60 42.9(5) . .
O45 Mo17 O58 102.5(6) . .
O45 Mo17 O57 101.2(6) . .
O58 Mo17 O57 91.1(6) . .
O45 Mo17 O47 102.9(7) . 2_355
O58 Mo17 O47 86.5(5) . 2_355
O57 Mo17 O47 155.7(6) . 2_355
O45 Mo17 O56 102.1(6) . .
O58 Mo17 O56 155.1(6) . .
O57 Mo17 O56 87.9(5) . .
O47 Mo17 O56 84.2(5) 2_355 .
O45 Mo17 O61 161.1(6) . .
O58 Mo17 O61 67.1(6) . .
O57 Mo17 O61 95.0(6) . .
O47 Mo17 O61 61.9(6) 2_355 .
O56 Mo17 O61 88.2(6) . .
O45 Mo17 O60 159.3(6) . .
O58 Mo17 O60 91.9(6) . .
O57 Mo17 O60 63.3(5) . .
O47 Mo17 O60 92.6(6) 2_355 .
O56 Mo17 O60 65.5(5) . .
O61 Mo17 O60 39.5(5) . .
O46 Mo18 O55 100.8(6) . .
O46 Mo18 O48 103.4(6) . .
O55 Mo18 O48 90.1(5) . .
O46 Mo18 O57 100.1(6) . .
O55 Mo18 O57 88.5(5) . .
O48 Mo18 O57 156.3(6) . .
O46 Mo18 O52 101.9(6) . 2_355
O55 Mo18 O52 157.0(5) . 2_355
O48 Mo18 O52 88.3(5) . 2_355
O57 Mo18 O52 83.9(5) . 2_355
O46 Mo18 O62 162.5(6) . 2_355
O55 Mo18 O62 91.5(6) . 2_355
O48 Mo18 O62 63.7(5) . 2_355
O57 Mo18 O62 92.7(6) . 2_355
O52 Mo18 O62 67.3(5) 2_355 2_355
O46 Mo18 O60 159.8(6) . .
O55 Mo18 O60 67.3(5) . .
O48 Mo18 O60 93.2(5) . .
O57 Mo18 O60 64.5(6) . .
O52 Mo18 O60 89.9(5) 2_355 .
O62 Mo18 O60 37.7(5) 2_355 .
Mo13 O47 Mo17 141.1(9) . 2_355
Mo18 O48 Mo13 139.6(7) . .
Mo14 O49 Mo13 139.9(7) . .
Mo14 O50 Mo15 139.7(8) . .
Mo14 O51 Mo16 138.5(7) . .
Mo15 O52 Mo18 138.4(6) . 2_355
Mo13 O53 Mo15 139.7(7) 2_355 .
Mo16 O54 Mo15 141.4(8) . .
Mo18 O55 Mo16 137.8(6) . .
Mo16 O56 Mo17 139.7(7) . .
Mo17 O57 Mo18 138.4(8) . .
Mo17 O58 Mo14 140.3(6) . 2_355
P2 O59 Mo15 125.5(9) . .
P2 O59 Mo16 123.3(8) . .
Mo15 O59 Mo16 93.0(5) . .
P2 O59 Mo14 122.9(9) . .
Mo15 O59 Mo14 91.5(4) . .
Mo16 O59 Mo14 91.2(5) . .
P2 O60 O62 58.2(5) . 2_355
P2 O60 O61 56.6(6) . .
O62 O60 O61 100.3(9) 2_355 .
P2 O60 Mo18 129.3(10) . .
O62 O60 Mo18 71.0(8) 2_355 .
O61 O60 Mo18 141.2(12) . .
P2 O60 Mo17 124.4(10) . .
O62 O60 Mo17 137.8(12) 2_355 .
O61 O60 Mo17 67.9(8) . .
Mo18 O60 Mo17 92.8(4) . .
P2 O60 Mo16 119.1(9) . .
O62 O60 Mo16 128.4(12) 2_355 .
O61 O60 Mo16 120.5(12) . .
Mo18 O60 Mo16 91.2(5) . .
Mo17 O60 Mo16 89.3(5) . .
P2 O61 O60 56.4(6) . .
P2 O61 O62 55.3(6) . .
O60 O61 O62 99.3(9) . .
P2 O61 Mo17 128.9(10) . .
O60 O61 Mo17 72.6(8) . .
O62 O61 Mo17 145.3(12) . .
P2 O61 Mo13 125.9(11) . 2_355
O60 O61 Mo13 140.7(13) . 2_355
O62 O61 Mo13 70.6(8) . 2_355
Mo17 O61 Mo13 94.1(5) . 2_355
P2 O61 Mo14 116.8(10) . 2_355
O60 O61 Mo14 126.1(13) . 2_355
O62 O61 Mo14 119.4(10) . 2_355
Mo17 O61 Mo14 90.4(5) . 2_355
Mo13 O61 Mo14 89.8(5) 2_355 2_355
P2 O62 O60 58.9(6) . 2_355
P2 O62 O61 56.1(6) . .
O60 O62 O61 100.8(10) 2_355 .
P2 O62 Mo18 130.1(10) . 2_355
O60 O62 Mo18 71.2(8) 2_355 2_355
O61 O62 Mo18 141.4(11) . 2_355
P2 O62 Mo13 125.2(10) . 2_355
O60 O62 Mo13 142.0(12) 2_355 2_355
O61 O62 Mo13 69.1(8) . 2_355
Mo18 O62 Mo13 93.7(4) 2_355 2_355
P2 O62 Mo15 117.7(8) . .
O60 O62 Mo15 124.5(12) 2_355 .
O61 O62 Mo15 122.7(11) . .
Mo18 O62 Mo15 89.7(4) 2_355 .
Mo13 O62 Mo15 88.8(5) 2_355 .
O83 P3 O83 180.0(13) 2_556 .
O83 P3 O84 121.0(8) 2_556 .
O83 P3 O84 59.0(8) . .
O83 P3 O84 59.0(8) 2_556 2_556
O83 P3 O84 121.0(8) . 2_556
O84 P3 O84 180.000(5) . 2_556
O83 P3 O81 110.9(9) 2_556 2_556
O83 P3 O81 69.1(9) . 2_556
O84 P3 O81 107.0(8) . 2_556
O84 P3 O81 73.0(8) 2_556 2_556
O83 P3 O81 69.1(9) 2_556 .
O83 P3 O81 110.9(9) . .
O84 P3 O81 73.0(8) . .
O84 P3 O81 107.0(8) 2_556 .
O81 P3 O81 180.0(11) 2_556 .
O83 P3 O82 69.2(8) 2_556 2_556
O83 P3 O82 110.8(8) . 2_556
O84 P3 O82 73.7(9) . 2_556
O84 P3 O82 106.3(9) 2_556 2_556
O81 P3 O82 81.5(9) 2_556 2_556
O81 P3 O82 98.5(9) . 2_556
O83 P3 O82 110.8(8) 2_556 .
O83 P3 O82 69.2(8) . .
O84 P3 O82 106.3(9) . .
O84 P3 O82 73.7(9) 2_556 .
O81 P3 O82 98.5(9) 2_556 .
O81 P3 O82 81.5(9) . .
O82 P3 O82 180.0(7) 2_556 .
O63 Mo19 O71 101.5(5) . .
O63 Mo19 O69 104.7(6) . .
O71 Mo19 O69 89.6(5) . .
O63 Mo19 O75 101.1(6) . 2_556
O71 Mo19 O75 157.1(6) . 2_556
O69 Mo19 O75 88.3(5) . 2_556
O63 Mo19 O70 98.2(5) . .
O71 Mo19 O70 87.5(5) . .
O69 Mo19 O70 157.0(6) . .
O75 Mo19 O70 85.5(5) 2_556 .
O63 Mo19 O82 161.3(6) . 2_556
O71 Mo19 O82 92.1(5) . 2_556
O69 Mo19 O82 62.2(6) . 2_556
O75 Mo19 O82 66.8(5) 2_556 2_556
O70 Mo19 O82 95.0(5) . 2_556
O63 Mo19 O84 155.8(5) . .
O71 Mo19 O84 66.3(4) . .
O69 Mo19 O84 96.3(6) . .
O75 Mo19 O84 91.3(6) 2_556 .
O70 Mo19 O84 61.7(5) . .
O82 Mo19 O84 42.6(5) 2_556 .
O64 Mo20 O80 102.6(6) . .
O64 Mo20 O70 101.4(7) . .
O80 Mo20 O70 90.6(5) . .
O64 Mo20 O72 101.7(7) . .
O80 Mo20 O72 155.7(5) . .
O70 Mo20 O72 86.0(5) . .
O64 Mo20 O77 102.3(6) . .
O80 Mo20 O77 87.6(4) . .
O70 Mo20 O77 156.1(5) . .
O72 Mo20 O77 85.8(4) . .
O64 Mo20 O84 161.3(6) . .
O80 Mo20 O84 92.1(5) . .
O70 Mo20 O84 66.4(5) . .
O72 Mo20 O84 64.5(5) . .
O77 Mo20 O84 89.8(5) . .
O64 Mo20 O83 162.6(7) . .
O80 Mo20 O83 66.2(5) . .
O70 Mo20 O83 92.3(5) . .
O72 Mo20 O83 89.8(5) . .
O77 Mo20 O83 65.2(5) . .
O84 Mo20 O83 36.0(5) . .
O65 Mo21 O72 101.6(5) . .
O65 Mo21 O73 101.7(6) . .
O72 Mo21 O73 90.2(5) . .
O65 Mo21 O71 101.5(6) . .
O72 Mo21 O71 87.2(5) . .
O73 Mo21 O71 156.7(6) . .
O65 Mo21 O79 103.0(6) . 2_556
O72 Mo21 O79 155.4(6) . 2_556
O73 Mo21 O79 86.9(5) . 2_556
O71 Mo21 O79 86.0(5) . 2_556
O65 Mo21 O81 158.8(4) . .
O72 Mo21 O81 96.7(5) . .
O73 Mo21 O81 67.5(5) . .
O71 Mo21 O81 89.8(5) . .
O79 Mo21 O81 59.6(6) 2_556 .
O66 Mo22 O75 102.1(6) . .
O66 Mo22 O73 101.1(5) . .
O75 Mo22 O73 156.5(6) . .
O66 Mo22 O74 102.0(5) . .
O75 Mo22 O74 90.4(6) . .
O73 Mo22 O74 88.6(5) . .
O66 Mo22 O76 101.3(6) . .
O75 Mo22 O76 88.3(5) . .
O73 Mo22 O76 83.3(6) . .
O74 Mo22 O76 156.4(7) . .
O66 Mo22 O81 158.0(4) . .
O75 Mo22 O81 93.8(6) . .
O73 Mo22 O81 65.0(5) . .
O74 Mo22 O81 62.5(5) . .
O76 Mo22 O81 94.1(6) . .
O66 Mo22 O82 156.6(4) . .
O75 Mo22 O82 63.4(5) . .
O73 Mo22 O82 93.4(6) . .
O74 Mo22 O82 96.7(5) . .
O76 Mo22 O82 61.9(6) . .
O81 Mo22 O82 45.4(4) . .
O67 Mo23 O76 103.3(7) . .
O67 Mo23 O77 100.4(5) . .
O76 Mo23 O77 87.8(5) . .
O67 Mo23 O69 103.3(7) . 2_556
O76 Mo23 O69 89.7(5) . 2_556
O77 Mo23 O69 156.2(6) . 2_556
O67 Mo23 O78 100.2(5) . .
O76 Mo23 O78 156.5(6) . .
O77 Mo23 O78 87.1(4) . .
O69 Mo23 O78 85.8(5) 2_556 .
O67 Mo23 O82 161.9(5) . .
O76 Mo23 O82 67.0(7) . .
O77 Mo23 O82 94.6(5) . .
O69 Mo23 O82 62.8(6) 2_556 .
O78 Mo23 O82 90.6(5) . .
O68 Mo24 O79 103.2(7) . .
O68 Mo24 O78 103.1(5) . .
O79 Mo24 O78 91.6(5) . .
O68 Mo24 O80 102.4(5) . .
O79 Mo24 O80 154.0(6) . .
O78 Mo24 O80 87.0(4) . .
O68 Mo24 O74 99.8(6) . 2_556
O79 Mo24 O74 86.3(5) . 2_556
O78 Mo24 O74 156.9(6) . 2_556
O80 Mo24 O74 85.0(5) . 2_556
O68 Mo24 O81 160.3(6) . 2_556
O79 Mo24 O81 62.8(6) . 2_556
O78 Mo24 O81 91.5(5) . 2_556
O80 Mo24 O81 91.3(4) . 2_556
O74 Mo24 O81 67.0(6) 2_556 2_556
O68 Mo24 O83 159.6(5) . .
O79 Mo24 O83 94.8(6) . .
O78 Mo24 O83 66.2(4) . .
O80 Mo24 O83 61.0(4) . .
O74 Mo24 O83 91.0(6) 2_556 .
O81 Mo24 O83 39.9(5) 2_556 .
Mo19 O69 Mo23 139.4(9) . 2_556
Mo20 O70 Mo19 139.2(7) . .
Mo19 O71 Mo21 138.4(5) . .
Mo21 O72 Mo20 139.8(7) . .
Mo22 O73 Mo21 138.3(7) . .
Mo22 O74 Mo24 138.4(7) . 2_556
Mo22 O75 Mo19 139.1(7) . 2_556
Mo23 O76 Mo22 138.8(9) . .
Mo23 O77 Mo20 139.0(6) . .
Mo24 O78 Mo23 139.4(5) . .
Mo24 O79 Mo21 142.4(9) . 2_556
Mo20 O80 Mo24 140.7(5) . .
P3 O81 O83 54.2(5) . 2_556
P3 O81 O84 52.8(5) . .
O83 O81 O84 95.4(7) 2_556 .
P3 O81 Mo24 131.4(10) . 2_556
O83 O81 Mo24 77.2(7) 2_556 2_556
O84 O81 Mo24 142.7(10) . 2_556
P3 O81 Mo21 123.0(8) . .
O83 O81 Mo21 144.1(10) 2_556 .
O84 O81 Mo21 70.2(6) . .
Mo24 O81 Mo21 94.4(4) 2_556 .
P3 O81 Mo22 116.6(8) . .
O83 O81 Mo22 125.9(9) 2_556 .
O84 O81 Mo22 120.7(10) . .
Mo24 O81 Mo22 91.6(4) 2_556 .
Mo21 O81 Mo22 88.7(5) . .
P3 O82 O83 54.1(5) . .
P3 O82 O84 52.5(5) . 2_556
O83 O82 O84 94.8(7) . 2_556
P3 O82 Mo23 128.6(8) . .
O83 O82 Mo23 74.4(7) . .
O84 O82 Mo23 143.7(10) 2_556 .
P3 O82 Mo19 125.3(10) . 2_556
O83 O82 Mo19 142.2(11) . 2_556
O84 O82 Mo19 72.9(7) 2_556 2_556
Mo23 O82 Mo19 94.4(4) . 2_556
P3 O82 Mo22 116.5(8) . .
O83 O82 Mo22 125.3(11) . .
O84 O82 Mo22 121.7(9) 2_556 .
Mo23 O82 Mo22 91.4(5) . .
Mo19 O82 Mo22 90.3(4) 2_556 .
O84 O83 P3 61.1(5) . .
O84 O83 O81 99.7(9) . 2_556
P3 O83 O81 56.6(5) . 2_556
O84 O83 O82 99.1(9) . .
P3 O83 O82 56.7(5) . .
O81 O83 O82 85.2(9) 2_556 .
O84 O83 Mo20 71.8(8) . .
P3 O83 Mo20 132.7(10) . .
O81 O83 Mo20 134.0(9) 2_556 .
O82 O83 Mo20 140.2(11) . .
O84 O83 Mo24 135.2(10) . .
P3 O83 Mo24 119.5(9) . .
O81 O83 Mo24 62.9(7) 2_556 .
O82 O83 Mo24 118.5(10) . .
Mo20 O83 Mo24 91.0(4) . .
O83 O84 P3 59.9(5) . .
O83 O84 O81 98.0(8) . .
P3 O84 O81 54.1(5) . .
O83 O84 O82 97.3(9) . 2_556
P3 O84 O82 53.8(5) . 2_556
O81 O84 O82 79.5(8) . 2_556
O83 O84 Mo20 72.2(7) . .
P3 O84 Mo20 132.0(9) . .
O81 O84 Mo20 143.3(10) . .
O82 O84 Mo20 135.9(9) 2_556 .
O83 O84 Mo19 134.6(11) . .
P3 O84 Mo19 118.3(8) . .
O81 O84 Mo19 117.1(9) . .
O82 O84 Mo19 64.5(6) 2_556 .
Mo20 O84 Mo19 92.1(4) . .
N1 Ag1 N5 163.5(6) . .
N1 Ag1 N6 125.1(4) . .
N5 Ag1 N6 70.1(5) . .
N1 Ag1 N2 68.8(6) . .
N5 Ag1 N2 108.2(5) . .
N6 Ag1 N2 89.4(5) . .
N8 Ag2 N4 163.8(5) . .
N8 Ag2 N7 70.4(4) . .
N4 Ag2 N7 120.1(4) . .
N8 Ag2 N3 123.0(4) . .
N4 Ag2 N3 71.5(5) . .
N7 Ag2 N3 89.1(5) . .
C5 N1 C1 119.5(17) . .
C5 N1 Ag1 121.4(12) . .
C1 N1 Ag1 118.8(14) . .
C6 N2 N3 117.2(15) . .
C6 N2 Ag1 106.7(12) . .
N3 N2 Ag1 116.3(11) . .
C13 N3 N2 117.4(15) . .
C13 N3 Ag2 111.5(12) . .
N2 N3 Ag2 126.6(10) . .
C20 N4 C24 119.7(13) . .
C20 N4 Ag2 117.2(11) . .
C24 N4 Ag2 122.1(10) . .
C29 N5 C25 120.8(16) . .
C29 N5 Ag1 119.0(11) . .
C25 N5 Ag1 120.1(14) . .
C30 N6 N7 115.0(14) . .
C30 N6 Ag1 115.6(12) . .
N7 N6 Ag1 125.2(9) . .
C37 N7 N6 119.2(13) . .
C37 N7 Ag2 110.8(10) . .
N6 N7 Ag2 115.1(9) . .
C48 N8 C44 117.9(13) . .
C48 N8 Ag2 124.0(11) . .
C44 N8 Ag2 117.7(9) . .
C2 C1 N1 123(2) . .
C2 C1 H1A 118.4 . .
N1 C1 H1A 118.4 . .
C1 C2 C3 114(2) . .
C1 C2 H2A 122.8 . .
C3 C2 H2A 122.8 . .
C2 C3 C4 122(2) . .
C2 C3 H3A 118.9 . .
C4 C3 H3A 118.9 . .
C5 C4 C3 119(2) . .
C5 C4 H4A 120.4 . .
C3 C4 H4A 120.4 . .
C4 C5 N1 121.6(19) . .
C4 C5 C6 124(2) . .
N1 C5 C6 113.9(18) . .
N2 C6 C7 127.3(17) . .
N2 C6 C5 116.7(16) . .
C7 C6 C5 115.9(16) . .
C12 C7 C8 117.5(19) . .
C12 C7 C6 120.9(16) . .
C8 C7 C6 121.5(19) . .
C9 C8 C7 124(2) . .
C9 C8 H8A 117.8 . .
C7 C8 H8A 117.8 . .
C10 C9 C8 117(2) . .
C10 C9 H9A 121.4 . .
C8 C9 H9A 121.4 . .
C11 C10 C9 125(3) . .
C11 C10 H10A 117.4 . .
C9 C10 H10A 117.4 . .
C10 C11 C12 117(2) . .
C10 C11 H11A 121.5 . .
C12 C11 H11A 121.5 . .
C7 C12 C11 119(2) . .
C7 C12 H12A 120.6 . .
C11 C12 H12A 120.6 . .
N3 C13 C14 123.7(17) . .
N3 C13 C20 117.2(15) . .
C14 C13 C20 119.1(16) . .
C15 C14 C19 119(2) . .
C15 C14 C13 119.2(19) . .
C19 C14 C13 121(2) . .
C16 C15 C14 121(2) . .
C16 C15 H15A 119.5 . .
C14 C15 H15A 119.5 . .
C17 C16 C15 117(2) . .
C17 C16 H16A 121.3 . .
C15 C16 H16A 121.3 . .
C16 C17 C18 122(2) . .
C16 C17 H17A 118.8 . .
C18 C17 H17A 118.8 . .
C17 C18 C19 118(2) . .
C17 C18 H18A 121.0 . .
C19 C18 H18A 121.0 . .
C18 C19 C14 120(2) . .
C18 C19 H19A 119.8 . .
C14 C19 H19A 119.8 . .
N4 C20 C21 120.0(15) . .
N4 C20 C13 120.0(15) . .
C21 C20 C13 119.9(19) . .
C22 C21 C20 120.0(19) . .
C22 C21 H21A 120.0 . .
C20 C21 H21A 120.0 . .
C21 C22 C23 119.1(18) . .
C21 C22 H22A 120.4 . .
C23 C22 H22A 120.4 . .
C24 C23 C22 118.4(18) . .
C24 C23 H23A 120.8 . .
C22 C23 H23A 120.8 . .
N4 C24 C23 122.6(17) . .
N4 C24 H24A 118.7 . .
C23 C24 H24A 118.7 . .
N5 C25 C26 121(2) . .
N5 C25 H25A 119.3 . .
C26 C25 H25A 119.3 . .
C25 C26 C27 121(2) . .
C25 C26 H26A 119.6 . .
C27 C26 H26A 119.6 . .
C28 C27 C26 115(2) . .
C28 C27 H27A 122.5 . .
C26 C27 H27A 122.5 . .
C27 C28 C29 124(2) . .
C27 C28 H28A 117.8 . .
C29 C28 H28A 117.8 . .
N5 C29 C28 117.4(16) . .
N5 C29 C30 116.9(16) . .
C28 C29 C30 125.6(19) . .
N6 C30 C31 125.0(16) . .
N6 C30 C29 117.3(17) . .
C31 C30 C29 117.3(16) . .
C36 C31 C32 117(2) . .
C36 C31 C30 119.5(18) . .
C32 C31 C30 123(2) . .
C33 C32 C31 117(2) . .
C33 C32 H32A 121.3 . .
C31 C32 H32A 121.3 . .
C34 C33 C32 121(2) . .
C34 C33 H33A 119.5 . .
C32 C33 H33A 119.5 . .
C35 C34 C33 121(3) . .
C35 C34 H34A 119.4 . .
C33 C34 H34A 119.4 . .
C34 C35 C36 120(3) . .
C34 C35 H35A 119.9 . .
C36 C35 H35A 119.9 . .
C35 C36 C31 123(2) . .
C35 C36 H36A 118.7 . .
C31 C36 H36A 118.7 . .
N7 C37 C38 126.8(14) . .
N7 C37 C44 112.2(13) . .
C38 C37 C44 120.9(13) . .
C43 C38 C39 119.5(16) . .
C43 C38 C37 122.4(16) . .
C39 C38 C37 118.0(15) . .
C40 C39 C38 118.4(17) . .
C40 C39 H39A 120.8 . .
C38 C39 H39A 120.8 . .
C41 C40 C39 121(2) . .
C41 C40 H40A 119.5 . .
C39 C40 H40A 119.5 . .
C40 C41 C42 118.7(19) . .
C40 C41 H41A 120.6 . .
C42 C41 H41A 120.6 . .
C43 C42 C41 118.6(17) . .
C43 C42 H42A 120.7 . .
C41 C42 H42A 120.7 . .
C38 C43 C42 123.5(17) . .
C38 C43 H43A 118.3 . .
C42 C43 H43A 118.3 . .
N8 C44 C45 122.4(13) . .
N8 C44 C37 119.8(13) . .
C45 C44 C37 117.8(16) . .
C46 C45 C44 117.8(15) . .
C46 C45 H45A 121.1 . .
C44 C45 H45A 121.1 . .
C47 C46 C45 119.3(15) . .
C47 C46 H46A 120.4 . .
C45 C46 H46A 120.4 . .
C46 C47 C48 119.2(16) . .
C46 C47 H47A 120.4 . .
C48 C47 H47A 120.4 . .
N8 C48 C47 123.3(16) . .
N8 C48 H48A 118.3 . .
C47 C48 H48A 118.3 . .
N9 Ag3 N16 152.1(5) . .
N9 Ag3 N15 135.7(5) . .
N16 Ag3 N15 71.3(5) . .
N9 Ag3 N10 69.7(4) . .
N16 Ag3 N10 108.4(4) . .
N15 Ag3 N10 92.2(4) . .
N13 Ag4 N12 160.3(4) . .
N13 Ag4 N11 129.0(4) . .
N12 Ag4 N11 70.3(4) . .
N13 Ag4 N14 71.3(4) . .
N12 Ag4 N14 108.9(4) . .
N11 Ag4 N14 89.8(4) . .
C53 N9 C49 120.2(13) . .
C53 N9 Ag3 119.2(9) . .
C49 N9 Ag3 120.4(12) . .
C54 N10 N11 118.1(12) . .
C54 N10 Ag3 104.8(9) . .
N11 N10 Ag3 110.1(8) . .
C61 N11 N10 116.7(13) . .
C61 N11 Ag4 112.8(10) . .
N10 N11 Ag4 129.8(9) . .
C68 N12 C72 121.3(12) . .
C68 N12 Ag4 118.1(9) . .
C72 N12 Ag4 120.0(10) . .
C73 N13 C77 116.2(13) . .
C73 N13 Ag4 124.7(11) . .
C77 N13 Ag4 118.7(10) . .
C78 N14 N15 118.3(12) . .
C78 N14 Ag4 101.0(9) . .
N15 N14 Ag4 111.6(8) . .
C85 N15 N14 115.3(12) . .
C85 N15 Ag3 113.2(10) . .
N14 N15 Ag3 128.7(9) . .
C92 N16 C96 118.8(14) . .
C92 N16 Ag3 118.9(11) . .
C96 N16 Ag3 121.7(11) . .
N9 C49 C50 115.2(16) . .
N9 C49 H49A 122.4 . .
C50 C49 H49A 122.4 . .
C51 C50 C49 125.2(17) . .
C51 C50 H50A 117.4 . .
C49 C50 H50A 117.4 . .
C50 C51 C52 118.9(18) . .
C50 C51 H51A 120.6 . .
C52 C51 H51A 120.6 . .
C51 C52 C53 115.5(17) . .
C51 C52 H52A 122.2 . .
C53 C52 H52A 122.2 . .
N9 C53 C52 124.7(14) . .
N9 C53 C54 118.4(14) . .
C52 C53 C54 116.8(15) . .
N10 C54 C55 130.0(13) . .
N10 C54 C53 106.6(14) . .
C55 C54 C53 123.1(14) . .
C56 C55 C60 118.2(16) . .
C56 C55 C54 121.3(14) . .
C60 C55 C54 120.5(15) . .
C57 C56 C55 122.3(16) . .
C57 C56 H56A 118.9 . .
C55 C56 H56A 118.9 . .
C56 C57 C58 120.9(17) . .
C56 C57 H57A 119.5 . .
C58 C57 H57A 119.5 . .
C59 C58 C57 118.2(17) . .
C59 C58 H58A 120.9 . .
C57 C58 H58A 120.9 . .
C58 C59 C60 122.3(15) . .
C58 C59 H59A 118.9 . .
C60 C59 H59A 118.9 . .
C59 C60 C55 117.9(15) . .
C59 C60 H60A 121.1 . .
C55 C60 H60A 121.1 . .
N11 C61 C62 121.7(14) . .
N11 C61 C68 117.0(14) . .
C62 C61 C68 121.1(13) . .
C67 C62 C63 122.7(19) . .
C67 C62 C61 120.7(18) . .
C63 C62 C61 116.4(18) . .
C62 C63 C64 120(2) . .
C62 C63 H63A 119.8 . .
C64 C63 H63A 119.8 . .
C65 C64 C63 120(4) . .
C65 C64 H64A 120.2 . .
C63 C64 H64A 120.2 . .
C64 C65 C66 122(3) . .
C64 C65 H65A 119.0 . .
C66 C65 H65A 119.0 . .
C67 C66 C65 117(3) . .
C67 C66 H66A 121.7 . .
C65 C66 H66A 121.7 . .
C62 C67 C66 119(2) . .
C62 C67 H67A 120.7 . .
C66 C67 H67A 120.7 . .
N12 C68 C69 121.2(13) . .
N12 C68 C61 120.7(13) . .
C69 C68 C61 118.1(13) . .
C70 C69 C68 118.1(15) . .
C70 C69 H69A 120.9 . .
C68 C69 H69A 120.9 . .
C71 C70 C69 118.2(15) . .
C71 C70 H70A 120.9 . .
C69 C70 H70A 120.9 . .
C70 C71 C72 120.7(14) . .
C70 C71 H71A 119.7 . .
C72 C71 H71A 119.7 . .
N12 C72 C71 120.1(14) . .
N12 C72 H72A 120.0 . .
C71 C72 H72A 120.0 . .
N13 C73 C74 123.0(15) . .
N13 C73 H73A 118.5 . .
C74 C73 H73A 118.5 . .
C75 C74 C73 118.4(17) . .
C75 C74 H74A 120.8 . .
C73 C74 H74A 120.8 . .
C74 C75 C76 119.9(17) . .
C74 C75 H75A 120.0 . .
C76 C75 H75A 120.0 . .
C77 C76 C75 118.7(16) . .
C77 C76 H76A 120.6 . .
C75 C76 H76A 120.6 . .
C76 C77 N13 123.7(16) . .
C76 C77 C78 120.3(16) . .
N13 C77 C78 116.0(13) . .
N14 C78 C79 128.5(14) . .
N14 C78 C77 114.3(13) . .
C79 C78 C77 117.2(13) . .
C80 C79 C84 117.9(14) . .
C80 C79 C78 119.3(15) . .
C84 C79 C78 122.3(14) . .
C79 C80 C81 120.2(16) . .
C79 C80 H80A 119.9 . .
C81 C80 H80A 119.9 . .
C82 C81 C80 120.2(17) . .
C82 C81 H81A 119.9 . .
C80 C81 H81A 119.9 . .
C83 C82 C81 120.4(18) . .
C83 C82 H82A 119.8 . .
C81 C82 H82A 119.8 . .
C82 C83 C84 123.0(19) . .
C82 C83 H83A 118.5 . .
C84 C83 H83A 118.5 . .
C83 C84 C79 118.2(15) . .
C83 C84 H84A 120.9 . .
C79 C84 H84A 120.9 . .
N15 C85 C92 118.7(13) . .
N15 C85 C86 125.0(14) . .
C92 C85 C86 116.3(13) . .
C91 C86 C87 118.4(16) . .
C91 C86 C85 123.4(15) . .
C87 C86 C85 118.2(15) . .
C86 C87 C88 118.2(18) . .
C86 C87 H87A 120.9 . .
C88 C87 H87A 120.9 . .
C89 C88 C87 119(2) . .
C89 C88 H88A 120.7 . .
C87 C88 H88A 120.7 . .
C88 C89 C90 124(2) . .
C88 C89 H89A 118.2 . .
C90 C89 H89A 118.2 . .
C91 C90 C89 118.3(19) . .
C91 C90 H90A 120.9 . .
C89 C90 H90A 120.9 . .
C90 C91 C86 122.6(18) . .
C90 C91 H91A 118.7 . .
C86 C91 H91A 118.7 . .
N16 C92 C93 122.1(15) . .
N16 C92 C85 116.3(14) . .
C93 C92 C85 121.7(14) . .
C92 C93 C94 116.2(15) . .
C92 C93 H93A 121.9 . .
C94 C93 H93A 121.9 . .
C95 C94 C93 121.0(17) . .
C95 C94 H94A 119.5 . .
C93 C94 H94A 119.5 . .
C94 C95 C96 118.0(18) . .
C94 C95 H95A 121.0 . .
C96 C95 H95A 121.0 . .
N16 C96 C95 123.6(16) . .
N16 C96 H96A 118.2 . .
C95 C96 H96A 118.2 . .
N21 Ag5 N20 161.8(5) . .
N21 Ag5 N19 127.9(4) . .
N20 Ag5 N19 70.1(4) . .
N21 Ag5 N22 68.6(5) . .
N20 Ag5 N22 112.1(4) . .
N19 Ag5 N22 91.7(4) . .
N17 Ag6 N24 166.9(4) . .
N17 Ag6 N18 69.3(4) . .
N24 Ag6 N18 120.7(4) . .
N17 Ag6 N23 120.3(4) . .
N24 Ag6 N23 70.4(4) . .
N18 Ag6 N23 88.1(4) . .
C97 N17 C101 118.4(11) . .
C97 N17 Ag6 122.0(10) . .
C101 N17 Ag6 119.4(8) . .
C102 N18 N19 116.9(11) . .
C102 N18 Ag6 113.7(9) . .
N19 N18 Ag6 118.3(7) . .
C109 N19 N18 115.6(11) . .
C109 N19 Ag5 115.9(9) . .
N18 N19 Ag5 121.1(8) . .
C116 N20 C120 120.2(13) . .
C116 N20 Ag5 118.3(9) . .
C120 N20 Ag5 121.2(12) . .
C125 N21 C121 117.5(15) . .
C125 N21 Ag5 120.7(11) . .
C121 N21 Ag5 121.7(13) . .
C126 N22 N23 117.6(12) . .
C126 N22 Ag5 107.9(9) . .
N23 N22 Ag5 114.1(8) . .
C133 N23 N22 116.8(12) . .
C133 N23 Ag6 112.6(9) . .
N22 N23 Ag6 127.1(8) . .
C144 N24 C140 117.4(12) . .
C144 N24 Ag6 122.9(10) . .
C140 N24 Ag6 119.4(9) . .
N17 C97 C98 125.4(15) . .
N17 C97 H97A 117.3 . .
C98 C97 H97A 117.3 . .
C97 C98 C99 115.9(15) . .
C97 C98 H98A 122.0 . .
C99 C98 H98A 122.0 . .
C98 C99 C100 120.6(15) . .
C98 C99 H99A 119.7 . .
C100 C99 H99A 119.7 . .
C101 C100 C99 119.5(16) . .
C101 C100 H10B 120.3 . .
C99 C100 H10B 120.3 . .
C100 C101 N17 119.7(13) . .
C100 C101 C102 122.7(14) . .
N17 C101 C102 117.5(11) . .
N18 C102 C103 123.8(13) . .
N18 C102 C101 115.3(12) . .
C103 C102 C101 120.9(12) . .
C108 C103 C104 113.9(15) . .
C108 C103 C102 125.7(14) . .
C104 C103 C102 120.2(15) . .
C103 C104 C105 121.9(16) . .
C103 C104 H10C 119.0 . .
C105 C104 H10C 119.0 . .
C106 C105 C104 118.1(17) . .
C106 C105 H10D 121.0 . .
C104 C105 H10D 121.0 . .
C105 C106 C107 121.9(18) . .
C105 C106 H10E 119.1 . .
C107 C106 H10E 119.1 . .
C108 C107 C106 118(2) . .
C108 C107 H10F 120.8 . .
C106 C107 H10F 120.8 . .
C107 C108 C103 125.8(17) . .
C107 C108 H10G 117.1 . .
C103 C108 H10G 117.1 . .
N19 C109 C116 116.6(13) . .
N19 C109 C110 123.7(12) . .
C116 C109 C110 119.7(12) . .
C115 C110 C111 120.5(15) . .
C115 C110 C109 117.0(14) . .
C111 C110 C109 122.4(14) . .
C110 C111 C112 120.1(16) . .
C110 C111 H11B 119.9 . .
C112 C111 H11B 119.9 . .
C113 C112 C111 116.3(17) . .
C113 C112 H11C 121.8 . .
C111 C112 H11C 121.8 . .
C114 C113 C112 121.3(19) . .
C114 C113 H11D 119.4 . .
C112 C113 H11D 119.4 . .
C113 C114 C115 124.0(19) . .
C113 C114 H11E 118.0 . .
C115 C114 H11E 118.0 . .
C114 C115 C110 117.5(17) . .
C114 C115 H11F 121.2 . .
C110 C115 H11F 121.2 . .
C117 C116 N20 119.6(14) . .
C117 C116 C109 123.7(15) . .
N20 C116 C109 116.7(12) . .
C116 C117 C118 121.1(17) . .
C116 C117 H11G 119.5 . .
C118 C117 H11G 119.5 . .
C119 C118 C117 117.6(17) . .
C119 C118 H11H 121.2 . .
C117 C118 H11H 121.2 . .
C120 C119 C118 122.3(17) . .
C120 C119 H11I 118.8 . .
C118 C119 H11I 118.8 . .
C119 C120 N20 118.9(17) . .
C119 C120 H12B 120.5 . .
N20 C120 H12B 120.5 . .
N21 C121 C122 123.8(18) . .
N21 C121 H12C 118.1 . .
C122 C121 H12C 118.1 . .
C123 C122 C121 116.7(18) . .
C123 C122 H12D 121.6 . .
C121 C122 H12D 121.6 . .
C122 C123 C124 120.7(18) . .
C122 C123 H12E 119.7 . .
C124 C123 H12E 119.7 . .
C125 C124 C123 117.9(18) . .
C125 C124 H12F 121.0 . .
C123 C124 H12F 121.0 . .
N21 C125 C124 123.4(15) . .
N21 C125 C126 117.9(14) . .
C124 C125 C126 118.6(16) . .
N22 C126 C127 129.4(14) . .
N22 C126 C125 111.4(13) . .
C127 C126 C125 119.2(12) . .
C128 C127 C132 118.5(16) . .
C128 C127 C126 120.7(16) . .
C132 C127 C126 120.6(14) . .
C127 C128 C129 122.0(19) . .
C127 C128 H12G 119.0 . .
C129 C128 H12G 119.0 . .
C130 C129 C128 117(2) . .
C130 C129 H12H 121.6 . .
C128 C129 H12H 121.6 . .
C131 C130 C129 124(2) . .
C131 C130 H13A 117.9 . .
C129 C130 H13A 117.9 . .
C130 C131 C132 116(2) . .
C130 C131 H13B 121.8 . .
C132 C131 H13B 121.8 . .
C127 C132 C131 122.0(18) . .
C127 C132 H13C 119.0 . .
C131 C132 H13C 119.0 . .
N23 C133 C140 118.2(13) . .
N23 C133 C134 124.6(14) . .
C140 C133 C134 117.1(12) . .
C135 C134 C139 118.3(17) . .
C135 C134 C133 121.0(16) . .
C139 C134 C133 120.7(17) . .
C134 C135 C136 120(2) . .
C134 C135 H13D 120.2 . .
C136 C135 H13D 120.2 . .
C137 C136 C135 115(3) . .
C137 C136 H13E 122.5 . .
C135 C136 H13E 122.5 . .
C138 C137 C136 130(3) . .
C138 C137 H13F 115.0 . .
C136 C137 H13F 115.0 . .
C137 C138 C139 112(3) . .
C137 C138 H13G 124.2 . .
C139 C138 H13G 124.2 . .
C134 C139 C138 125(2) . .
C134 C139 H13H 117.3 . .
C138 C139 H13H 117.3 . .
N24 C140 C141 119.5(13) . .
N24 C140 C133 117.9(12) . .
C141 C140 C133 122.6(14) . .
C140 C141 C142 121.7(14) . .
C140 C141 H14A 119.2 . .
C142 C141 H14A 119.2 . .
C143 C142 C141 117.7(15) . .
C143 C142 H14B 121.1 . .
C141 C142 H14B 121.1 . .
C142 C143 C144 119.2(16) . .
C142 C143 H14C 120.4 . .
C144 C143 H14C 120.4 . .
N24 C144 C143 124.3(15) . .
N24 C144 H14D 117.8 . .
C143 C144 H14D 117.8 . .
C146 N25 C145 118.6(13) . .
C146 N25 C147 118.5(13) . .
C145 N25 C147 118.7(12) . .
O85 C145 N25 103(3) . .
O85 C145 H14E 128.6 . .
N25 C145 H14E 128.6 . .
N25 C146 H14F 109.5 . .
N25 C146 H14G 109.5 . .
H14F C146 H14G 109.5 . .
N25 C146 H14H 109.5 . .
H14F C146 H14H 109.5 . .
H14G C146 H14H 109.5 . .
N25 C147 H14I 109.5 . .
N25 C147 H14J 109.5 . .
H14I C147 H14J 109.5 . .
N25 C147 H14K 109.5 . .
H14I C147 H14K 109.5 . .
H14J C147 H14K 109.5 . .
C148 N26 C150 117.8(14) . .
C148 N26 C149 118.5(15) . .
C150 N26 C149 116.4(14) . .
O86 C148 N26 112(3) . .
O86 C148 H14L 123.8 . .
N26 C148 H14L 123.8 . .
N26 C149 H14M 109.5 . .
N26 C149 H14N 109.5 . .
H14M C149 H14N 109.5 . .
N26 C149 H14O 109.5 . .
H14M C149 H14O 109.5 . .
H14N C149 H14O 109.5 . .
N26 C150 H15B 109.5 . .
N26 C150 H15C 109.5 . .
H15B C150 H15C 109.5 . .
N26 C150 H15D 109.5 . .
H15B C150 H15D 109.5 . .
H15C C150 H15D 109.5 . .
C152 N27 C151 123.0(15) . .
C152 N27 C153 118.3(14) . .
C151 N27 C153 118.7(14) . .
O87 C151 N27 94(3) . .
O87 C151 H15E 132.8 . .
N27 C151 H15E 132.8 . .
N27 C152 H15F 109.5 . .
N27 C152 H15G 109.5 . .
H15F C152 H15G 109.5 . .
N27 C152 H15H 109.5 . .
H15F C152 H15H 109.5 . .
H15G C152 H15H 109.5 . .
N27 C153 H15I 109.5 . .
N27 C153 H15J 109.5 . .
H15I C153 H15J 109.5 . .
N27 C153 H15K 109.5 . .
H15I C153 H15K 109.5 . .
H15J C153 H15K 109.5 . .
C156 N28 C155 118.6(13) . .
C156 N28 C154 119.1(13) . .
C155 N28 C154 119.0(13) . .
O88 C154 N28 111(3) . .
O88 C154 H15L 124.4 . .
N28 C154 H15L 124.4 . .
N28 C155 H15M 109.5 . .
N28 C155 H15N 109.5 . .
H15M C155 H15N 109.5 . .
N28 C155 H15O 109.5 . .
H15M C155 H15O 109.5 . .
H15N C155 H15O 109.5 . .
N28 C156 H15P 109.5 . .
N28 C156 H15Q 109.5 . .
H15P C156 H15Q 109.5 . .
N28 C156 H15R 109.5 . .
H15P C156 H15R 109.5 . .
H15Q C156 H15R 109.5 . .
C158 N29 C159 119.8(15) . .
C158 N29 C157 119.4(15) . .
C159 N29 C157 119.2(15) . .
O89 C157 N29 104(4) . .
O89 C157 H15S 128.0 . .
N29 C157 H15S 128.0 . .
N29 C158 H15T 109.5 . .
N29 C158 H15U 109.5 . .
H15T C158 H15U 109.5 . .
N29 C158 H15V 109.5 . .
H15T C158 H15V 109.5 . .
H15U C158 H15V 109.5 . .
N29 C159 H15W 109.5 . .
N29 C159 H15X 109.5 . .
H15W C159 H15X 109.5 . .
N29 C159 H15Y 109.5 . .
H15W C159 H15Y 109.5 . .
H15X C159 H15Y 109.5 . .
C162 N30 C160 116(3) . .
C162 N30 C161 115(2) . .
C160 N30 C161 116(2) . .
O90 C160 N30 105.9(16) . .
O90 C160 H16B 127.1 . .
N30 C160 H16B 127.1 . .
N30 C161 H16C 109.5 . .
N30 C161 H16D 109.5 . .
H16C C161 H16D 109.5 . .
N30 C161 H16E 109.5 . .
H16C C161 H16E 109.5 . .
H16D C161 H16E 109.5 . .
N30 C162 H16F 109.5 . .
N30 C162 H16G 109.5 . .
H16F C162 H16G 109.5 . .
N30 C162 H16H 109.5 . .
H16F C162 H16H 109.5 . .
H16G C162 H16H 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
P1 O38 1.515(8) .
P1 O39 1.526(8) .
P1 O40 1.531(8) .
P1 O37 1.533(7) .
P1 O37' 1.592(16) .
P1 O40' 1.596(16) .
P1 O38' 1.599(16) .
P1 O39' 1.599(16) .
Mo1 O1 1.647(9) .
Mo1 O14 1.803(11) .
Mo1 O13 1.863(11) .
Mo1 O15 1.961(11) .
Mo1 O16 2.011(10) .
Mo1 O37 2.408(10) .
Mo1 O38' 2.55(3) .
Mo2 O2 1.654(10) .
Mo2 O15 1.839(9) .
Mo2 O19 1.844(9) .
Mo2 O18 1.975(9) .
Mo2 O17 2.041(11) .
Mo2 O38' 2.33(3) .
Mo2 O38 2.451(10) .
Mo3 O3 1.654(9) .
Mo3 O20 1.817(10) .
Mo3 O16 1.851(10) .
Mo3 O22 1.968(9) .
Mo3 O21 2.020(10) .
Mo3 O37 2.487(10) .
Mo3 O40' 2.49(2) .
Mo4 O4 1.671(9) .
Mo4 O23 1.792(10) .
Mo4 O24 1.827(8) .
Mo4 O20 1.997(9) .
Mo4 O19 2.002(10) .
Mo4 O40' 2.40(2) .
Mo4 O38 2.458(10) .
Mo5 O5 1.669(9) .
Mo5 O25 1.825(10) .
Mo5 O18 1.872(10) .
Mo5 O27 1.972(10) .
Mo5 O24 2.006(9) .
Mo5 O39' 2.36(2) .
Mo5 O38 2.505(10) .
Mo6 O6 1.670(9) .
Mo6 O22 1.807(9) .
Mo6 O26 1.868(10) .
Mo6 O28 1.984(9) .
Mo6 O23 1.989(10) .
Mo6 O39 2.431(10) .
Mo6 O40' 2.50(3) .
Mo7 O7 1.659(8) .
Mo7 O27 1.810(10) .
Mo7 O28 1.836(9) .
Mo7 O29 1.974(9) .
Mo7 O30 1.983(9) .
Mo7 O39 2.454(10) .
Mo7 O39' 2.48(3) .
Mo8 O8 1.665(9) .
Mo8 O31 1.839(9) .
Mo8 O29 1.845(9) .
Mo8 O26 1.973(10) .
Mo8 O32 1.976(8) .
Mo8 O39 2.453(10) .
Mo8 O37' 2.47(3) .
Mo9 O9 1.676(9) .
Mo9 O30 1.807(9) .
Mo9 O33 1.818(9) .
Mo9 O25 1.968(10) .
Mo9 O35 2.007(11) .
Mo9 O40 2.481(10) .
Mo9 O39' 2.52(3) .
Mo10 O10 1.657(10) .
Mo10 O36 1.806(10) .
Mo10 O34 1.812(9) .
Mo10 O31 1.967(9) .
Mo10 O33 1.984(9) .
Mo10 O40 2.413(10) .
Mo10 O37' 2.44(3) .
Mo11 O11 1.665(9) .
Mo11 O32 1.815(9) .
Mo11 O21 1.837(10) .
Mo11 O13 1.956(10) .
Mo11 O34 1.999(9) .
Mo11 O37 2.463(9) .
Mo11 O37' 2.48(3) .
Mo12 O12 1.659(9) .
Mo12 O17 1.767(11) .
Mo12 O35 1.825(10) .
Mo12 O14 1.989(10) .
Mo12 O36 2.012(10) .
Mo12 O40 2.473(11) .
Mo12 O38' 2.51(3) .
P2 O62 1.492(10) .
P2 O62 1.492(10) 2_355
P2 O60 1.502(10) 2_355
P2 O60 1.502(10) .
P2 O61 1.506(11) .
P2 O61 1.506(11) 2_355
P2 O59 1.517(11) 2_355
P2 O59 1.517(11) .
Mo13 O41 1.680(13) .
Mo13 O53 1.847(11) 2_355
Mo13 O47 1.861(11) .
Mo13 O48 1.936(12) .
Mo13 O49 1.961(12) .
Mo13 O61 2.443(19) 2_355
Mo13 O62 2.466(17) 2_355
Mo14 O42 1.661(11) .
Mo14 O49 1.834(14) .
Mo14 O51 1.855(10) .
Mo14 O50 1.877(13) .
Mo14 O58 1.937(12) 2_355
Mo14 O59 2.492(16) .
Mo15 O43 1.656(12) .
Mo15 O52 1.862(11) .
Mo15 O50 1.891(12) .
Mo15 O53 1.930(11) .
Mo15 O54 1.941(10) .
Mo15 O59 2.446(16) .
Mo15 O62 2.600(16) .
Mo16 O44 1.645(10) .
Mo16 O54 1.829(11) .
Mo16 O56 1.854(11) .
Mo16 O51 1.929(11) .
Mo16 O55 1.961(13) .
Mo16 O59 2.461(15) .
Mo16 O60 2.547(16) .
Mo17 O45 1.650(10) .
Mo17 O58 1.856(11) .
Mo17 O57 1.883(13) .
Mo17 O47 1.911(12) 2_355
Mo17 O56 1.918(11) .
Mo17 O61 2.417(16) .
Mo17 O60 2.490(16) .
Mo18 O46 1.658(10) .
Mo18 O55 1.842(12) .
Mo18 O48 1.858(12) .
Mo18 O57 1.918(12) .
Mo18 O52 1.924(11) 2_355
Mo18 O62 2.414(14) 2_355
Mo18 O60 2.417(16) .
O47 Mo17 1.911(12) 2_355
O52 Mo18 1.924(11) 2_355
O53 Mo13 1.847(11) 2_355
O58 Mo14 1.937(12) 2_355
O60 O62 1.56(2) 2_355
O60 O61 1.66(2) .
O61 O62 1.69(2) .
O61 Mo13 2.443(19) 2_355
O61 Mo14 2.608(18) 2_355
O62 O60 1.56(2) 2_355
O62 Mo18 2.414(14) 2_355
O62 Mo13 2.466(17) 2_355
P3 O83 1.484(9) 2_556
P3 O83 1.484(9) .
P3 O84 1.502(10) .
P3 O84 1.502(10) 2_556
P3 O81 1.527(10) 2_556
P3 O81 1.527(10) .
P3 O82 1.529(10) 2_556
P3 O82 1.529(10) .
Mo19 O63 1.670(10) .
Mo19 O71 1.877(11) .
Mo19 O69 1.884(12) .
Mo19 O75 1.908(11) 2_556
Mo19 O70 1.921(12) .
Mo19 O82 2.422(16) 2_556
Mo19 O84 2.565(15) .
Mo20 O64 1.650(10) .
Mo20 O80 1.869(9) .
Mo20 O70 1.878(11) .
Mo20 O72 1.906(11) .
Mo20 O77 1.921(10) .
Mo20 O84 2.376(13) .
Mo20 O83 2.383(15) .
Mo21 O65 1.664(10) .
Mo21 O72 1.893(11) .
Mo21 O73 1.897(11) .
Mo21 O71 1.906(11) .
Mo21 O79 1.921(11) 2_556
Mo21 O81 2.476(15) .
Mo22 O66 1.664(9) .
Mo22 O75 1.882(11) .
Mo22 O73 1.890(11) .
Mo22 O74 1.892(13) .
Mo22 O76 1.944(12) .
Mo22 O81 2.587(15) .
Mo22 O82 2.587(16) .
Mo23 O67 1.667(11) .
Mo23 O76 1.868(10) .
Mo23 O77 1.878(10) .
Mo23 O69 1.886(10) 2_556
Mo23 O78 1.914(10) .
Mo23 O82 2.396(14) .
Mo24 O68 1.675(9) .
Mo24 O79 1.835(11) .
Mo24 O78 1.869(10) .
Mo24 O80 1.907(10) .
Mo24 O74 1.914(11) 2_556
Mo24 O81 2.372(14) 2_556
Mo24 O83 2.598(15) .
O69 Mo23 1.886(10) 2_556
O74 Mo24 1.914(11) 2_556
O75 Mo19 1.908(11) 2_556
O79 Mo21 1.921(11) 2_556
O81 O83 1.71(2) 2_556
O81 O84 1.802(19) .
O81 Mo24 2.372(14) 2_556
O82 O83 1.71(2) .
O82 O84 1.82(2) 2_556
O82 Mo19 2.422(16) 2_556
O83 O84 1.47(2) .
O83 O81 1.71(2) 2_556
O84 O82 1.82(2) 2_556
Ag1 N1 2.232(15) .
Ag1 N5 2.240(14) .
Ag1 N6 2.409(14) .
Ag1 N2 2.539(16) .
Ag2 N8 2.233(12) .
Ag2 N4 2.236(12) .
Ag2 N7 2.475(13) .
Ag2 N3 2.506(15) .
N1 C5 1.32(2) .
N1 C1 1.37(2) .
N2 C6 1.27(2) .
N2 N3 1.382(17) .
N3 C13 1.260(18) .
N4 C20 1.32(2) .
N4 C24 1.350(17) .
N5 C29 1.33(2) .
N5 C25 1.34(2) .
N6 C30 1.261(18) .
N6 N7 1.402(15) .
N7 C37 1.309(16) .
N8 C48 1.314(16) .
N8 C44 1.325(18) .
C1 C2 1.34(2) .
C1 H1A 0.9300 .
C2 C3 1.36(3) .
C2 H2A 0.9300 .
C3 C4 1.41(3) .
C3 H3A 0.9300 .
C4 C5 1.27(2) .
C4 H4A 0.9300 .
C5 C6 1.52(2) .
C6 C7 1.49(2) .
C7 C12 1.36(2) .
C7 C8 1.39(2) .
C8 C9 1.37(2) .
C8 H8A 0.9300 .
C9 C10 1.34(3) .
C9 H9A 0.9300 .
C10 C11 1.32(3) .
C10 H10A 0.9300 .
C11 C12 1.51(3) .
C11 H11A 0.9300 .
C12 H12A 0.9300 .
C13 C14 1.51(2) .
C13 C20 1.52(2) .
C14 C15 1.386(10) .
C14 C19 1.392(9) .
C15 C16 1.385(10) .
C15 H15A 0.9300 .
C16 C17 1.384(10) .
C16 H16A 0.9300 .
C17 C18 1.385(10) .
C17 H17A 0.9300 .
C18 C19 1.385(10) .
C18 H18A 0.9300 .
C19 H19A 0.9300 .
C20 C21 1.40(2) .
C21 C22 1.36(2) .
C21 H21A 0.9300 .
C22 C23 1.38(2) .
C22 H22A 0.9300 .
C23 C24 1.36(2) .
C23 H23A 0.9300 .
C24 H24A 0.9300 .
C25 C26 1.34(3) .
C25 H25A 0.9300 .
C26 C27 1.40(3) .
C26 H26A 0.9300 .
C27 C28 1.35(3) .
C27 H27A 0.9300 .
C28 C29 1.38(2) .
C28 H28A 0.9300 .
C29 C30 1.48(2) .
C30 C31 1.47(2) .
C31 C36 1.39(2) .
C31 C32 1.42(2) .
C32 C33 1.39(3) .
C32 H32A 0.9300 .
C33 C34 1.39(3) .
C33 H33A 0.9300 .
C34 C35 1.30(3) .
C34 H34A 0.9300 .
C35 C36 1.36(3) .
C35 H35A 0.9300 .
C36 H36A 0.9300 .
C37 C38 1.484(19) .
C37 C44 1.51(2) .
C38 C43 1.331(19) .
C38 C39 1.42(2) .
C39 C40 1.41(2) .
C39 H39A 0.9300 .
C40 C41 1.38(3) .
C40 H40A 0.9300 .
C41 C42 1.42(3) .
C41 H41A 0.9300 .
C42 C43 1.38(2) .
C42 H42A 0.9300 .
C43 H43A 0.9300 .
C44 C45 1.401(19) .
C45 C46 1.365(19) .
C45 H45A 0.9300 .
C46 C47 1.36(2) .
C46 H46A 0.9300 .
C47 C48 1.36(2) .
C47 H47A 0.9300 .
C48 H48A 0.9300 .
Ag3 N9 2.160(11) .
Ag3 N16 2.232(13) .
Ag3 N15 2.422(12) .
Ag3 N10 2.543(12) .
Ag4 N13 2.167(12) .
Ag4 N12 2.251(11) .
Ag4 N11 2.478(11) .
Ag4 N14 2.575(12) .
N9 C53 1.316(17) .
N9 C49 1.399(17) .
N10 C54 1.334(18) .
N10 N11 1.385(14) .
N11 C61 1.290(16) .
N12 C68 1.297(15) .
N12 C72 1.353(16) .
N13 C73 1.336(18) .
N13 C77 1.364(18) .
N14 C78 1.333(16) .
N14 N15 1.380(15) .
N15 C85 1.278(16) .
N16 C92 1.327(17) .
N16 C96 1.329(18) .
C49 C50 1.44(2) .
C49 H49A 0.9300 .
C50 C51 1.31(2) .
C50 H50A 0.9300 .
C51 C52 1.42(2) .
C51 H51A 0.9300 .
C52 C53 1.43(2) .
C52 H52A 0.9300 .
C53 C54 1.549(18) .
C54 C55 1.43(2) .
C55 C56 1.38(2) .
C55 C60 1.391(18) .
C56 C57 1.32(2) .
C56 H56A 0.9300 .
C57 C58 1.36(2) .
C57 H57A 0.9300 .
C58 C59 1.36(2) .
C58 H58A 0.9300 .
C59 C60 1.38(2) .
C59 H59A 0.9300 .
C60 H60A 0.9300 .
C61 C62 1.47(2) .
C61 C68 1.480(18) .
C62 C67 1.32(2) .
C62 C63 1.40(2) .
C63 C64 1.40(3) .
C63 H63A 0.9300 .
C64 C65 1.28(5) .
C64 H64A 0.9300 .
C65 C66 1.49(4) .
C65 H65A 0.9300 .
C66 C67 1.44(3) .
C66 H66A 0.9300 .
C67 H67A 0.9300 .
C68 C69 1.429(19) .
C69 C70 1.39(2) .
C69 H69A 0.9300 .
C70 C71 1.38(2) .
C70 H70A 0.9300 .
C71 C72 1.375(18) .
C71 H71A 0.9300 .
C72 H72A 0.9300 .
C73 C74 1.39(2) .
C73 H73A 0.9300 .
C74 C75 1.35(2) .
C74 H74A 0.9300 .
C75 C76 1.37(2) .
C75 H75A 0.9300 .
C76 C77 1.35(2) .
C76 H76A 0.9300 .
C77 C78 1.49(2) .
C78 C79 1.456(19) .
C79 C80 1.396(19) .
C79 C84 1.427(19) .
C80 C81 1.40(2) .
C80 H80A 0.9300 .
C81 C82 1.34(2) .
C81 H81A 0.9300 .
C82 C83 1.34(2) .
C82 H82A 0.9300 .
C83 C84 1.37(2) .
C83 H83A 0.9300 .
C84 H84A 0.9300 .
C85 C92 1.499(19) .
C85 C86 1.50(2) .
C86 C91 1.40(2) .
C86 C87 1.42(2) .
C87 C88 1.44(2) .
C87 H87A 0.9300 .
C88 C89 1.35(3) .
C88 H88A 0.9300 .
C89 C90 1.38(3) .
C89 H89A 0.9300 .
C90 C91 1.34(2) .
C90 H90A 0.9300 .
C91 H91A 0.9300 .
C92 C93 1.381(19) .
C93 C94 1.42(2) .
C93 H93A 0.9300 .
C94 C95 1.34(2) .
C94 H94A 0.9300 .
C95 C96 1.35(2) .
C95 H95A 0.9300 .
C96 H96A 0.9300 .
Ag5 N21 2.202(13) .
Ag5 N20 2.251(12) .
Ag5 N19 2.397(11) .
Ag5 N22 2.544(12) .
Ag6 N17 2.229(10) .
Ag6 N24 2.238(11) .
Ag6 N18 2.469(11) .
Ag6 N23 2.481(11) .
N17 C97 1.343(16) .
N17 C101 1.359(16) .
N18 C102 1.278(15) .
N18 N19 1.410(14) .
N19 C109 1.280(15) .
N20 C116 1.362(16) .
N20 C120 1.375(18) .
N21 C125 1.310(19) .
N21 C121 1.34(2) .
N22 C126 1.304(15) .
N22 N23 1.389(14) .
N23 C133 1.291(16) .
N24 C144 1.315(16) .
N24 C140 1.348(16) .
C97 C98 1.343(19) .
C97 H97A 0.9300 .
C98 C99 1.37(2) .
C98 H98A 0.9300 .
C99 C100 1.40(2) .
C99 H99A 0.9300 .
C100 C101 1.357(17) .
C100 H10B 0.9300 .
C101 C102 1.487(17) .
C102 C103 1.461(19) .
C103 C108 1.36(2) .
C103 C104 1.412(19) .
C104 C105 1.42(2) .
C104 H10C 0.9300 .
C105 C106 1.34(2) .
C105 H10D 0.9300 .
C106 C107 1.36(2) .
C106 H10E 0.9300 .
C107 C108 1.35(2) .
C107 H10F 0.9300 .
C108 H10G 0.9300 .
C109 C116 1.461(18) .
C109 C110 1.500(18) .
C110 C115 1.37(2) .
C110 C111 1.379(19) .
C111 C112 1.40(2) .
C111 H11B 0.9300 .
C112 C113 1.39(3) .
C112 H11C 0.9300 .
C113 C114 1.30(2) .
C113 H11D 0.9300 .
C114 C115 1.35(2) .
C114 H11E 0.9300 .
C115 H11F 0.9300 .
C116 C117 1.352(18) .
C117 C118 1.38(2) .
C117 H11G 0.9300 .
C118 C119 1.37(2) .
C118 H11H 0.9300 .
C119 C120 1.34(2) .
C119 H11I 0.9300 .
C120 H12B 0.9300 .
C121 C122 1.40(2) .
C121 H12C 0.9300 .
C122 C123 1.35(2) .
C122 H12D 0.9300 .
C123 C124 1.38(2) .
C123 H12E 0.9300 .
C124 C125 1.38(2) .
C124 H12F 0.9300 .
C125 C126 1.506(19) .
C126 C127 1.426(19) .
C127 C128 1.35(2) .
C127 C132 1.38(2) .
C128 C129 1.40(2) .
C128 H12G 0.9300 .
C129 C130 1.38(3) .
C129 H12H 0.9300 .
C130 C131 1.35(3) .
C130 H13A 0.9300 .
C131 C132 1.40(2) .
C131 H13B 0.9300 .
C132 H13C 0.9300 .
C133 C140 1.472(18) .
C133 C134 1.475(19) .
C134 C135 1.37(2) .
C134 C139 1.39(2) .
C135 C136 1.45(3) .
C135 H13D 0.9300 .
C136 C137 1.38(3) .
C136 H13E 0.9300 .
C137 C138 1.33(4) .
C137 H13F 0.9300 .
C138 C139 1.42(3) .
C138 H13G 0.9300 .
C139 H13H 0.9300 .
C140 C141 1.359(18) .
C141 C142 1.39(2) .
C141 H14A 0.9300 .
C142 C143 1.30(2) .
C142 H14B 0.9300 .
C143 C144 1.378(19) .
C143 H14C 0.9300 .
C144 H14D 0.9300 .
O85 C145 1.352(10) .
N25 C146 1.395(10) .
N25 C145 1.398(10) .
N25 C147 1.402(10) .
C145 H14E 0.9300 .
C146 H14F 0.9600 .
C146 H14G 0.9600 .
C146 H14H 0.9600 .
C147 H14I 0.9600 .
C147 H14J 0.9600 .
C147 H14K 0.9600 .
O86 C148 1.349(10) .
N26 C148 1.395(10) .
N26 C150 1.398(10) .
N26 C149 1.400(10) .
C148 H14L 0.9300 .
C149 H14M 0.9600 .
C149 H14N 0.9600 .
C149 H14O 0.9600 .
C150 H15B 0.9600 .
C150 H15C 0.9600 .
C150 H15D 0.9600 .
O87 C151 1.339(10) .
N27 C152 1.383(9) .
N27 C151 1.388(9) .
N27 C153 1.389(10) .
C151 H15E 0.9300 .
C152 H15F 0.9600 .
C152 H15G 0.9600 .
C152 H15H 0.9600 .
C153 H15I 0.9600 .
C153 H15J 0.9600 .
C153 H15K 0.9600 .
O88 C154 1.343(10) .
N28 C156 1.389(10) .
N28 C155 1.390(10) .
N28 C154 1.390(10) .
C154 H15L 0.9300 .
C155 H15M 0.9600 .
C155 H15N 0.9600 .
C155 H15O 0.9600 .
C156 H15P 0.9600 .
C156 H15Q 0.9600 .
C156 H15R 0.9600 .
O89 C157 1.352(10) .
N29 C158 1.395(10) .
N29 C159 1.395(10) .
N29 C157 1.399(10) .
C157 H15S 0.9300 .
C158 H15T 0.9600 .
C158 H15U 0.9600 .
C158 H15V 0.9600 .
C159 H15W 0.9600 .
C159 H15X 0.9600 .
C159 H15Y 0.9600 .
O90 C160 1.349(10) .
N30 C162 1.394(10) .
N30 C160 1.394(10) .
N30 C161 1.395(10) .
C160 H16B 0.9300 .
C161 H16C 0.9600 .
C161 H16D 0.9600 .
C161 H16E 0.9600 .
C162 H16F 0.9600 .
C162 H16G 0.9600 .
C162 H16H 0.9600 .
