#------------------------------------------------------------------------------
#$Date: 2017-07-11 14:26:40 +0300 (Tue, 11 Jul 2017) $
#$Revision: 198632 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/32/60/4326017.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4326017
loop_
_publ_author_name
'Jaime A. Flores'
'José G. Andino'
'Nikolay P. Tsvetkov'
'Maren Pink'
'Robert J. Wolfe'
'Ashley R. Head'
'Dennis L. Lichtenberger'
'Joseph Massa'
'Kenneth G. Caulton'
_publ_section_title
;
 Assessment of the Electronic Structure of 2,2'-Pyridylpyrrolides as
 Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8121
_journal_page_last               8131
_journal_paper_doi               10.1021/ic2005503
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         'C15 H15 F6 K N2 O'
_chemical_formula_sum            'C15 H15 F6 K N2 O'
_chemical_formula_weight         392.39
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           7
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P -2yac'
_symmetry_space_group_name_H-M   'P 1 n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 91.692(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   12.2946(13)
_cell_length_b                   15.6385(15)
_cell_length_c                   18.030(3)
_cell_measurement_reflns_used    4187
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      24.77
_cell_measurement_theta_min      2.26
_cell_volume                     3465.1(8)
_computing_cell_refinement       'APEX II v2009.5.0 (Bruker, 2009)'
_computing_data_collection       'APEX II v2009.5.0 (Bruker, 2009)'
_computing_data_reduction        'APEX II v2009.5.0 (Bruker, 2009)'
_computing_molecular_graphics    'SHELXTL (Bruker, 2008)'
_computing_publication_material  'SHELXTL (Bruker, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR-2004 (Burla et al., 2005)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 'CCD area detector'
_diffrn_detector_area_resol_mean 83.33
_diffrn_detector_type            'Bruker APEXII'
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_details
'0.30 degree frames measured for 15 seconds each'
_diffrn_measurement_device       'APEX Kappa Duo'
_diffrn_measurement_device_type  Kappa
_diffrn_measurement_method       'omega and phi scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0410
_diffrn_reflns_av_sigmaI/netI    0.0553
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            25555
_diffrn_reflns_theta_full        25.04
_diffrn_reflns_theta_max         25.04
_diffrn_reflns_theta_min         1.30
_exptl_absorpt_coefficient_mu    0.372
_exptl_absorpt_correction_T_max  0.9816
_exptl_absorpt_correction_T_min  0.9259
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, R. Blessing; 1995'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.504
_exptl_crystal_description       plate
_exptl_crystal_F_000             1600
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.382
_refine_diff_density_min         -0.270
_refine_diff_density_rms         0.052
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.47(6)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     909
_refine_ls_number_reflns         12113
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.022
_refine_ls_R_factor_all          0.0810
_refine_ls_R_factor_gt           0.0477
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0538P)²+0.1970P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1052
_refine_ls_wR_factor_ref         0.1210
_reflns_number_gt                8457
_reflns_number_total             12113
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic2005503_si_005.cif
_cod_data_source_block           10023
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'multi-scans' was replaced
with the value 'multi-scan' as specified in the replacement file
'src/cod-tools/trunk/data/replacement-values/replacement_values.lst'.

Automatic conversion script
Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius 
;
_cod_original_cell_volume        3465.1(7)
_cod_original_sg_symbol_Hall     '-P 2ybc'
_cod_database_code               4326017
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x+1/2, -y, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
K1 K 0.61832(9) 0.15536(9) 0.70543(6) 0.0272(3) Uani 1 1 d .
F1A F 1.1015(3) 0.0073(3) 0.8657(2) 0.0643(11) Uani 1 1 d .
F2A F 1.1021(3) 0.0953(3) 0.7755(2) 0.0535(11) Uani 1 1 d .
F3A F 1.0911(4) -0.0383(3) 0.7537(3) 0.0639(13) Uani 1 1 d .
F4A F 0.7079(3) 0.0217(2) 0.97049(19) 0.0528(11) Uani 1 1 d .
F5A F 0.6116(3) 0.0934(3) 0.89093(19) 0.0471(10) Uani 1 1 d .
F6A F 0.6109(3) -0.0411(2) 0.8841(2) 0.0527(12) Uani 1 1 d .
N1A N 0.7667(4) 0.0367(3) 0.6245(3) 0.0232(12) Uani 1 1 d .
N2A N 0.7539(4) 0.0345(2) 0.7754(3) 0.0206(12) Uani 1 1 d .
C1A C 0.7705(7) 0.0410(3) 0.5493(3) 0.0339(17) Uani 1 1 d .
H1A H 0.7040 0.0359 0.5215 0.041 Uiso 1 1 calc R
C2A C 0.8630(6) 0.0520(4) 0.5114(3) 0.0464(17) Uani 1 1 d .
H2A H 0.8610 0.0540 0.4587 0.056 Uiso 1 1 calc R
C3A C 0.9614(6) 0.0603(4) 0.5516(3) 0.0515(17) Uani 1 1 d .
H3A H 1.0276 0.0693 0.5269 0.062 Uiso 1 1 calc R
C4A C 0.9599(6) 0.0551(4) 0.6276(4) 0.0457(16) Uani 1 1 d .
H4A H 1.0263 0.0600 0.6557 0.055 Uiso 1 1 calc R
C5A C 0.8638(6) 0.0430(3) 0.6641(4) 0.0287(15) Uani 1 1 d .
C6A C 0.8528(5) 0.0353(3) 0.7452(3) 0.0209(14) Uani 1 1 d .
C7A C 0.9360(5) 0.0271(3) 0.8023(3) 0.0256(14) Uani 1 1 d .
C8A C 0.8805(5) 0.0243(3) 0.8693(3) 0.0285(14) Uani 1 1 d .
H8A H 0.9120 0.0203 0.9179 0.034 Uiso 1 1 calc R
C9A C 0.7725(5) 0.0285(3) 0.8506(3) 0.0218(13) Uani 1 1 d .
C10A C 1.0542(6) 0.0229(5) 0.7998(4) 0.0449(19) Uani 1 1 d .
C11A C 0.6774(5) 0.0263(4) 0.8985(3) 0.0327(16) Uani 1 1 d .
O1A O 0.4505(3) 0.0190(2) 0.7048(2) 0.0454(11) Uani 1 1 d .
C12A C 0.4447(7) 0.0405(4) 0.5756(4) 0.063(2) Uani 1 1 d .
H12A H 0.3987 0.0653 0.5358 0.095 Uiso 1 1 calc R
H12B H 0.4657 -0.0177 0.5619 0.095 Uiso 1 1 calc R
H12C H 0.5102 0.0756 0.5831 0.095 Uiso 1 1 calc R
C13A C 0.3835(6) 0.0380(4) 0.6450(4) 0.0594(19) Uani 1 1 d .
H13A H 0.3488 0.0943 0.6530 0.071 Uiso 1 1 calc R
H13B H 0.3253 -0.0055 0.6405 0.071 Uiso 1 1 calc R
C14A C 0.3916(5) 0.0031(4) 0.7733(4) 0.056(2) Uani 1 1 d .
H14A H 0.4383 -0.0317 0.8073 0.067 Uiso 1 1 calc R
H14B H 0.3255 -0.0307 0.7609 0.067 Uiso 1 1 calc R
C15A C 0.3591(5) 0.0823(4) 0.8126(3) 0.0569(17) Uani 1 1 d .
H15A H 0.3224 0.0670 0.8583 0.085 Uiso 1 1 calc R
H15B H 0.3094 0.1157 0.7804 0.085 Uiso 1 1 calc R
H15C H 0.4239 0.1164 0.8250 0.085 Uiso 1 1 calc R
K2 K 0.63617(10) 0.40565(9) 0.70692(6) 0.0274(3) Uani 1 1 d .
F1B F 0.1524(3) 0.2569(3) 0.5435(2) 0.0670(11) Uani 1 1 d .
F2B F 0.1646(3) 0.2172(2) 0.6576(2) 0.0554(12) Uani 1 1 d .
F3B F 0.1523(3) 0.3509(3) 0.6313(2) 0.0572(11) Uani 1 1 d .
F4B F 0.6372(3) 0.3446(2) 0.50835(19) 0.0440(10) Uani 1 1 d .
F5B F 0.5391(3) 0.2650(3) 0.43536(17) 0.0529(10) Uani 1 1 d .
F6B F 0.6393(3) 0.2083(2) 0.5206(2) 0.0457(11) Uani 1 1 d .
N1B N 0.4905(5) 0.2874(3) 0.7835(3) 0.0333(15) Uani 1 1 d .
N2B N 0.5012(4) 0.2872(3) 0.6312(3) 0.0228(12) Uani 1 1 d .
C1B C 0.4891(7) 0.2942(4) 0.8565(4) 0.0443(18) Uani 1 1 d .
H1B H 0.5558 0.2880 0.8839 0.053 Uiso 1 1 calc R
C2B C 0.3938(6) 0.3102(4) 0.8959(3) 0.0544(18) Uani 1 1 d .
H2B H 0.3950 0.3127 0.9485 0.065 Uiso 1 1 calc R
C3B C 0.2988(6) 0.3220(4) 0.8548(3) 0.0560(18) Uani 1 1 d .
H3B H 0.2333 0.3347 0.8791 0.067 Uiso 1 1 calc R
C4B C 0.2982(5) 0.3156(3) 0.7780(3) 0.0400(14) Uani 1 1 d .
H4B H 0.2331 0.3240 0.7493 0.048 Uiso 1 1 calc R
C5B C 0.3967(5) 0.2964(3) 0.7440(3) 0.0271(15) Uani 1 1 d .
C6B C 0.3997(5) 0.2882(3) 0.6619(3) 0.0231(15) Uani 1 1 d .
C7B C 0.3199(5) 0.2826(3) 0.6061(3) 0.0288(15) Uani 1 1 d .
C8B C 0.3707(5) 0.2747(3) 0.5390(3) 0.0277(14) Uani 1 1 d .
H8B H 0.3375 0.2680 0.4911 0.033 Uiso 1 1 calc R
C9B C 0.4813(5) 0.2787(3) 0.5572(3) 0.0266(15) Uani 1 1 d .
C10B C 0.1988(6) 0.2765(4) 0.6100(4) 0.0402(18) Uani 1 1 d .
C11B C 0.5709(5) 0.2740(4) 0.5062(3) 0.0297(15) Uani 1 1 d .
O1B O 0.7931(3) 0.2725(2) 0.73342(18) 0.0277(9) Uani 1 1 d .
C12B C 0.8624(6) 0.3305(4) 0.8517(3) 0.067(2) Uani 1 1 d .
H12D H 0.8645 0.3181 0.9050 0.100 Uiso 1 1 calc R
H12E H 0.8187 0.3819 0.8421 0.100 Uiso 1 1 calc R
H12F H 0.9366 0.3400 0.8351 0.100 Uiso 1 1 calc R
C13B C 0.8140(5) 0.2581(4) 0.8113(3) 0.0392(15) Uani 1 1 d .
H13C H 0.8632 0.2083 0.8171 0.047 Uiso 1 1 calc R
H13D H 0.7445 0.2431 0.8344 0.047 Uiso 1 1 calc R
C14B C 0.8947(5) 0.2772(3) 0.6948(3) 0.0333(13) Uani 1 1 d .
H14C H 0.9408 0.2270 0.7071 0.040 Uiso 1 1 calc R
H14D H 0.9351 0.3296 0.7094 0.040 Uiso 1 1 calc R
C15B C 0.8662(6) 0.2788(4) 0.6127(3) 0.0421(18) Uani 1 1 d .
H15D H 0.9329 0.2746 0.5845 0.063 Uiso 1 1 calc R
H15E H 0.8287 0.3324 0.6002 0.063 Uiso 1 1 calc R
H15F H 0.8184 0.2304 0.6002 0.063 Uiso 1 1 calc R
K3 K 0.62936(9) 0.65667(9) 0.69344(6) 0.0280(3) Uani 1 1 d .
F1C F 1.1026(3) 0.6062(3) 0.7473(3) 0.0801(15) Uani 1 1 d .
F2C F 1.1116(3) 0.5638(3) 0.8590(2) 0.0880(15) Uani 1 1 d .
F3C F 1.1066(3) 0.4740(2) 0.7714(2) 0.0493(11) Uani 1 1 d .
F4C F 0.7201(3) 0.5598(3) 0.96799(18) 0.0514(10) Uani 1 1 d .
F5C F 0.6181(3) 0.6149(3) 0.8828(2) 0.0510(11) Uani 1 1 d .
F6C F 0.6266(3) 0.4814(2) 0.8919(2) 0.0486(10) Uani 1 1 d .
N1C N 0.7715(5) 0.5291(3) 0.6224(3) 0.0303(14) Uani 1 1 d .
N2C N 0.7610(4) 0.5372(3) 0.7730(3) 0.0206(12) Uani 1 1 d .
C1C C 0.7734(7) 0.5187(4) 0.5469(4) 0.0439(18) Uani 1 1 d .
H1C H 0.7069 0.5234 0.5191 0.053 Uiso 1 1 calc R
C2C C 0.8646(6) 0.5022(4) 0.5105(3) 0.0532(17) Uani 1 1 d .
H2C H 0.8614 0.4937 0.4583 0.064 Uiso 1 1 calc R
C3C C 0.9635(6) 0.4975(5) 0.5492(3) 0.070(2) Uani 1 1 d .
H3C H 1.0292 0.4876 0.5241 0.084 Uiso 1 1 calc R
C4C C 0.9640(5) 0.5075(4) 0.6239(3) 0.0516(16) Uani 1 1 d .
H4C H 1.0309 0.5028 0.6513 0.062 Uiso 1 1 calc R
C5C C 0.8689(6) 0.5243(3) 0.6614(4) 0.0309(15) Uani 1 1 d .
C6C C 0.8593(6) 0.5365(3) 0.7420(3) 0.0230(15) Uani 1 1 d .
C7C C 0.9447(5) 0.5467(3) 0.7981(3) 0.0267(14) Uani 1 1 d .
C8C C 0.8904(5) 0.5574(3) 0.8658(3) 0.0251(12) Uani 1 1 d .
H8C H 0.9223 0.5679 0.9135 0.030 Uiso 1 1 calc R
C9C C 0.7816(5) 0.5495(3) 0.8474(3) 0.0222(13) Uani 1 1 d .
C10C C 1.0627(6) 0.5481(5) 0.7935(4) 0.0444(18) Uani 1 1 d .
C11C C 0.6882(5) 0.5515(4) 0.8971(3) 0.0315(15) Uani 1 1 d .
O1C O 0.4665(3) 0.5240(2) 0.6679(2) 0.0338(10) Uani 1 1 d .
C12C C 0.4128(7) 0.5759(4) 0.5462(3) 0.079(2) Uani 1 1 d .
H12G H 0.4080 0.5597 0.4937 0.119 Uiso 1 1 calc R
H12H H 0.4633 0.6240 0.5527 0.119 Uiso 1 1 calc R
H12I H 0.3407 0.5927 0.5628 0.119 Uiso 1 1 calc R
C13C C 0.4519(5) 0.5040(4) 0.5897(3) 0.0448(15) Uani 1 1 d .
H13E H 0.5223 0.4847 0.5703 0.054 Uiso 1 1 calc R
H13F H 0.3996 0.4562 0.5839 0.054 Uiso 1 1 calc R
C14C C 0.3679(4) 0.5326(3) 0.7063(3) 0.0320(13) Uani 1 1 d .
H14E H 0.3207 0.4825 0.6960 0.038 Uiso 1 1 calc R
H14F H 0.3288 0.5845 0.6890 0.038 Uiso 1 1 calc R
C15C C 0.3927(5) 0.5389(3) 0.7879(3) 0.0379(16) Uani 1 1 d .
H15G H 0.3248 0.5466 0.8143 0.057 Uiso 1 1 calc R
H15H H 0.4408 0.5879 0.7977 0.057 Uiso 1 1 calc R
H15I H 0.4287 0.4863 0.8051 0.057 Uiso 1 1 calc R
K4 K 0.63302(10) 0.90723(9) 0.69633(7) 0.0291(3) Uani 1 1 d .
F1D F 0.1658(3) 0.7185(3) 0.6208(2) 0.0548(11) Uani 1 1 d .
F2D F 0.1616(3) 0.7976(3) 0.5235(2) 0.0738(13) Uani 1 1 d .
F3D F 0.1629(3) 0.8557(3) 0.6321(3) 0.0695(13) Uani 1 1 d .
F4D F 0.6533(3) 0.8637(3) 0.5123(2) 0.0517(11) Uani 1 1 d .
F5D F 0.6467(3) 0.7257(3) 0.5039(2) 0.0543(11) Uani 1 1 d .
F6D F 0.5567(3) 0.8030(3) 0.42561(18) 0.0537(11) Uani 1 1 d .
N1D N 0.4898(5) 0.7809(3) 0.7715(3) 0.0307(14) Uani 1 1 d .
N2D N 0.5077(4) 0.7866(3) 0.6203(3) 0.0247(13) Uani 1 1 d .
C1D C 0.4848(6) 0.7762(4) 0.8444(3) 0.0329(16) Uani 1 1 d .
H1DA H 0.5512 0.7782 0.8727 0.039 Uiso 1 1 calc R
C2D C 0.3885(6) 0.7685(4) 0.8826(3) 0.0481(18) Uani 1 1 d .
H2D H 0.3883 0.7657 0.9352 0.058 Uiso 1 1 calc R
C3D C 0.2956(6) 0.7652(5) 0.8410(3) 0.064(2) Uani 1 1 d .
H3D H 0.2280 0.7590 0.8645 0.076 Uiso 1 1 calc R
C4D C 0.2978(5) 0.7709(4) 0.7641(3) 0.0475(17) Uani 1 1 d .
H4D H 0.2321 0.7701 0.7350 0.057 Uiso 1 1 calc R
C5D C 0.3974(5) 0.7778(3) 0.7307(3) 0.0242(14) Uani 1 1 d .
C6D C 0.4041(5) 0.7842(3) 0.6490(3) 0.0245(15) Uani 1 1 d .
C7D C 0.3273(5) 0.7939(3) 0.5910(3) 0.0244(14) Uani 1 1 d .
C8D C 0.3818(5) 0.8010(3) 0.5253(3) 0.0295(14) Uani 1 1 d .
H8D H 0.3511 0.8074 0.4766 0.035 Uiso 1 1 calc R
C9D C 0.4923(5) 0.7967(3) 0.5463(3) 0.0254(14) Uani 1 1 d .
C11D C 0.5836(6) 0.7976(4) 0.4974(3) 0.0329(16) Uani 1 1 d .
C110 C 0.2053(6) 0.7918(5) 0.5928(4) 0.0425(18) Uani 1 1 d .
O1D O 0.8041(4) 0.7735(3) 0.6964(3) 0.0545(13) Uani 1 1 d .
C12D C 0.8138(7) 0.7944(4) 0.8250(4) 0.067(2) Uani 1 1 d .
H12J H 0.8639 0.8043 0.8674 0.100 Uiso 1 1 calc R
H12K H 0.7724 0.7419 0.8331 0.100 Uiso 1 1 calc R
H12L H 0.7635 0.8428 0.8198 0.100 Uiso 1 1 calc R
C13D C 0.8759(6) 0.7858(4) 0.7572(4) 0.068(2) Uani 1 1 d .
H13G H 0.9197 0.8380 0.7497 0.082 Uiso 1 1 calc R
H13H H 0.9262 0.7366 0.7620 0.082 Uiso 1 1 calc R
C14D C 0.8680(6) 0.7510(5) 0.6249(4) 0.068(2) Uani 1 1 d .
H14G H 0.9322 0.7152 0.6377 0.081 Uiso 1 1 calc R
H14H H 0.8205 0.7193 0.5891 0.081 Uiso 1 1 calc R
C15D C 0.9007(5) 0.8294(4) 0.5942(4) 0.082(3) Uani 1 1 d .
H15J H 0.9426 0.8185 0.5497 0.124 Uiso 1 1 calc R
H15K H 0.9461 0.8606 0.6307 0.124 Uiso 1 1 calc R
H15L H 0.8363 0.8636 0.5808 0.124 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2A K1 N2B 174.00(18) . .
N2A K1 O1B 85.33(13) . .
N2B K1 O1B 89.21(13) . .
N2A K1 O1A 85.46(13) . .
N2B K1 O1A 100.24(14) . .
O1B K1 O1A 168.73(12) . .
N2A K1 N1B 124.90(15) . .
N2B K1 N1B 56.59(14) . .
O1B K1 N1B 82.90(14) . .
O1A K1 N1B 97.10(14) . .
N2A K1 N1A 55.93(13) . .
N2B K1 N1A 121.83(14) . .
O1B K1 N1A 91.00(12) . .
O1A K1 N1A 89.22(12) . .
N1B K1 N1A 173.66(16) . .
N2A K1 C13B 70.53(14) . .
N2B K1 C13B 105.14(15) . .
O1B K1 C13B 24.35(12) . .
O1A K1 C13B 144.67(14) . .
N1B K1 C13B 77.45(16) . .
N1A K1 C13B 97.68(14) . .
N2A K1 C6B 162.69(14) . .
N2B K1 C6B 22.49(14) . .
O1B K1 C6B 103.27(13) . .
O1A K1 C6B 84.01(13) . .
N1B K1 C6B 43.51(15) . .
N1A K1 C6B 137.41(14) . .
C13B K1 C6B 111.82(15) . .
N2A K1 C6A 21.19(13) . .
N2B K1 C6A 153.31(15) . .
O1B K1 C6A 72.35(12) . .
O1A K1 C6A 100.60(13) . .
N1B K1 C6A 136.01(15) . .
N1A K1 C6A 42.32(14) . .
C13B K1 C6A 64.94(14) . .
C6B K1 C6A 175.26(14) . .
N2A K1 K4 46.88(10) . 1_545
N2B K1 K4 136.96(11) . 1_545
O1B K1 K4 127.71(8) . 1_545
O1A K1 K4 46.82(8) . 1_545
N1B K1 K4 137.61(10) . 1_545
N1A K1 K4 48.28(9) . 1_545
C13B K1 K4 117.31(10) . 1_545
C6B K1 K4 128.67(11) . 1_545
C6A K1 K4 55.52(10) . 1_545
N2A K1 K2 129.76(10) . .
N2B K1 K2 45.84(10) . .
O1B K1 K2 46.92(8) . .
O1A K1 K2 139.15(8) . .
N1B K1 K2 48.24(10) . .
N1A K1 K2 125.76(9) . .
C13B K1 K2 59.32(10) . .
C6B K1 K2 56.38(10) . .
C6A K1 K2 119.27(10) . .
K4 K1 K2 173.73(3) 1_545 .
C1A N1A C5A 117.3(6) . .
C1A N1A K4 120.7(4) . 1_545
C5A N1A K4 108.0(4) . 1_545
C1A N1A K1 119.5(4) . .
C5A N1A K1 103.4(4) . .
K4 N1A K1 81.71(13) 1_545 .
C6A N2A C9A 105.9(5) . .
C6A N2A K1 110.2(3) . .
C9A N2A K1 124.9(3) . .
C6A N2A K4 105.7(3) . 1_545
C9A N2A K4 121.2(3) . 1_545
K1 N2A K4 87.21(16) . 1_545
C2A C1A N1A 124.3(7) . .
C2A C1A H1A 117.9 . .
N1A C1A H1A 117.9 . .
C1A C2A C3A 118.5(6) . .
C1A C2A H2A 120.7 . .
C3A C2A H2A 120.7 . .
C4A C3A C2A 118.3(6) . .
C4A C3A H3A 120.8 . .
C2A C3A H3A 120.8 . .
C3A C4A C5A 121.3(7) . .
C3A C4A H4A 119.3 . .
C5A C4A H4A 119.3 . .
N1A C5A C4A 120.2(6) . .
N1A C5A C6A 113.8(6) . .
C4A C5A C6A 126.0(6) . .
N2A C6A C7A 110.1(5) . .
N2A C6A C5A 120.7(6) . .
C7A C6A C5A 129.2(6) . .
N2A C6A K4 52.3(3) . 1_545
C7A C6A K4 131.8(3) . 1_545
C5A C6A K4 83.6(3) . 1_545
N2A C6A K1 48.7(3) . .
C7A C6A K1 139.6(4) . .
C5A C6A K1 81.5(3) . .
K4 C6A K1 67.99(13) 1_545 .
C8A C7A C6A 105.3(5) . .
C8A C7A C10A 122.3(6) . .
C6A C7A C10A 132.4(6) . .
C9A C8A C7A 106.3(5) . .
C9A C8A H8A 126.9 . .
C7A C8A H8A 126.9 . .
C8A C9A N2A 112.4(5) . .
C8A C9A C11A 129.6(6) . .
N2A C9A C11A 118.0(6) . .
F1A C10A F3A 105.9(6) . .
F1A C10A F2A 105.0(6) . .
F3A C10A F2A 103.6(6) . .
F1A C10A C7A 113.1(6) . .
F3A C10A C7A 113.8(6) . .
F2A C10A C7A 114.5(6) . .
F5A C11A F4A 107.1(5) . .
F5A C11A F6A 103.4(5) . .
F4A C11A F6A 107.1(5) . .
F5A C11A C9A 114.3(5) . .
F4A C11A C9A 111.4(6) . .
F6A C11A C9A 112.9(5) . .
C13A O1A C14A 113.5(5) . .
C13A O1A K4 123.1(4) . 1_545
C14A O1A K4 110.5(3) . 1_545
C13A O1A K1 104.3(4) . .
C14A O1A K1 118.5(3) . .
K4 O1A K1 83.82(12) 1_545 .
C13A C12A H12A 109.5 . .
C13A C12A H12B 109.5 . .
H12A C12A H12B 109.5 . .
C13A C12A H12C 109.5 . .
H12A C12A H12C 109.5 . .
H12B C12A H12C 109.5 . .
O1A C13A C12A 111.3(6) . .
O1A C13A H13A 109.4 . .
C12A C13A H13A 109.4 . .
O1A C13A H13B 109.4 . .
C12A C13A H13B 109.4 . .
H13A C13A H13B 108.0 . .
O1A C14A C15A 113.9(6) . .
O1A C14A H14A 108.8 . .
C15A C14A H14A 108.8 . .
O1A C14A H14B 108.8 . .
C15A C14A H14B 108.8 . .
H14A C14A H14B 107.7 . .
C14A C15A H15A 109.5 . .
C14A C15A H15B 109.5 . .
H15A C15A H15B 109.5 . .
C14A C15A H15C 109.5 . .
H15A C15A H15C 109.5 . .
H15B C15A H15C 109.5 . .
N2C K2 N2B 173.99(16) . .
N2C K2 O1C 90.89(12) . .
N2B K2 O1C 83.75(13) . .
N2C K2 O1B 96.03(13) . .
N2B K2 O1B 89.26(12) . .
O1C K2 O1B 172.86(13) . .
N2C K2 N1B 126.34(15) . .
N2B K2 N1B 57.06(14) . .
O1C K2 N1B 94.16(14) . .
O1B K2 N1B 83.17(14) . .
N2C K2 N1C 55.89(13) . .
N2B K2 N1C 120.41(15) . .
O1C K2 N1C 82.54(14) . .
O1B K2 N1C 99.88(13) . .
N1B K2 N1C 176.2(2) . .
N2C K2 C13C 106.03(15) . .
N2B K2 C13C 68.00(14) . .
O1C K2 C13C 24.73(12) . .
O1B K2 C13C 149.28(13) . .
N1B K2 C13C 99.88(17) . .
N1C K2 C13C 76.31(16) . .
N2C K2 C6C 21.75(14) . .
N2B K2 C6C 158.39(15) . .
O1C K2 C6C 103.33(13) . .
O1B K2 C6C 82.73(12) . .
N1B K2 C6C 140.71(15) . .
N1C K2 C6C 42.56(14) . .
C13C K2 C6C 110.71(15) . .
N2C K2 C5B 136.99(15) . .
N2B K2 C5B 44.01(14) . .
O1C K2 C5B 75.54(13) . .
O1B K2 C5B 100.35(13) . .
N1B K2 C5B 22.18(15) . .
N1C K2 C5B 154.00(17) . .
C13C K2 C5B 77.94(16) . .
C6C K2 C5B 157.37(15) . .
N2C K2 C6B 156.67(14) . .
N2B K2 C6B 21.79(14) . .
O1C K2 C6B 71.87(12) . .
O1B K2 C6B 101.93(13) . .
N1B K2 C6B 43.12(15) . .
N1C K2 C6B 133.45(15) . .
C13C K2 C6B 64.12(15) . .
C6C K2 C6B 174.83(16) . .
C5B K2 C6B 24.54(14) . .
N2C K2 C5C 43.70(14) . .
N2B K2 C5C 134.78(16) . .
O1C K2 C5C 101.13(13) . .
O1B K2 C5C 82.81(13) . .
N1B K2 C5C 161.39(17) . .
N1C K2 C5C 22.43(15) . .
C13C K2 C5C 98.43(16) . .
C6C K2 C5C 24.30(14) . .
C5B K2 C5C 176.37(19) . .
C6B K2 C5C 153.19(15) . .
N2C K2 K1 139.79(10) . .
N2B K2 K1 46.16(10) . .
O1C K2 K1 127.15(8) . .
O1B K2 K1 46.66(8) . .
N1B K2 K1 48.83(10) . .
N1C K2 K1 132.22(10) . .
C13C K2 K1 114.15(11) . .
C6C K2 K1 129.39(10) . .
C5B K2 K1 57.62(10) . .
C6B K2 K1 55.30(10) . .
C5C K2 K1 124.71(10) . .
C1B N1B C5B 118.9(6) . .
C1B N1B K2 116.3(4) . .
C5B N1B K2 102.1(3) . .
C1B N1B K1 123.4(4) . .
C5B N1B K1 106.2(4) . .
K2 N1B K1 82.93(15) . .
C9B N2B C6B 104.9(5) . .
C9B N2B K2 128.9(4) . .
C6B N2B K2 109.0(4) . .
C9B N2B K1 118.0(3) . .
C6B N2B K1 105.8(3) . .
K2 N2B K1 88.01(16) . .
N1B C1B C2B 123.5(7) . .
N1B C1B H1B 118.3 . .
C2B C1B H1B 118.3 . .
C3B C2B C1B 117.2(6) . .
C3B C2B H2B 121.4 . .
C1B C2B H2B 121.4 . .
C2B C3B C4B 120.4(5) . .
C2B C3B H3B 119.8 . .
C4B C3B H3B 119.8 . .
C3B C4B C5B 118.1(6) . .
C3B C4B H4B 120.9 . .
C5B C4B H4B 120.9 . .
N1B C5B C4B 121.8(6) . .
N1B C5B C6B 118.2(5) . .
C4B C5B C6B 120.0(6) . .
N1B C5B K2 55.8(3) . .
C4B C5B K2 136.2(4) . .
C6B C5B K2 78.8(3) . .
N2B C6B C7B 109.7(5) . .
N2B C6B C5B 116.7(6) . .
C7B C6B C5B 133.6(6) . .
N2B C6B K1 51.7(3) . .
C7B C6B K1 130.8(4) . .
C5B C6B K1 82.4(4) . .
N2B C6B K2 49.2(3) . .
C7B C6B K2 139.8(4) . .
C5B C6B K2 76.7(4) . .
K1 C6B K2 68.31(14) . .
C8B C7B C6B 108.2(5) . .
C8B C7B C10B 120.7(6) . .
C6B C7B C10B 130.8(6) . .
C7B C8B C9B 104.6(5) . .
C7B C8B H8B 127.7 . .
C9B C8B H8B 127.7 . .
N2B C9B C8B 112.5(6) . .
N2B C9B C11B 120.5(6) . .
C8B C9B C11B 126.9(6) . .
F2B C10B F1B 106.2(6) . .
F2B C10B F3B 105.7(5) . .
F1B C10B F3B 106.0(6) . .
F2B C10B C7B 114.0(6) . .
F1B C10B C7B 111.6(5) . .
F3B C10B C7B 112.8(5) . .
F5B C11B F6B 105.5(5) . .
F5B C11B F4B 105.6(4) . .
F6B C11B F4B 104.0(5) . .
F5B C11B C9B 113.8(6) . .
F6B C11B C9B 113.3(5) . .
F4B C11B C9B 113.7(5) . .
C13B O1B C14B 110.2(4) . .
C13B O1B K1 100.6(3) . .
C14B O1B K1 127.0(3) . .
C13B O1B K2 112.1(3) . .
C14B O1B K2 117.9(3) . .
K1 O1B K2 86.42(11) . .
C13B C12B H12D 109.5 . .
C13B C12B H12E 109.5 . .
H12D C12B H12E 109.5 . .
C13B C12B H12F 109.5 . .
H12D C12B H12F 109.5 . .
H12E C12B H12F 109.5 . .
O1B C13B C12B 115.1(5) . .
O1B C13B K1 55.0(2) . .
C12B C13B K1 155.4(4) . .
O1B C13B H13C 108.5 . .
C12B C13B H13C 108.5 . .
K1 C13B H13C 96.1 . .
O1B C13B H13D 108.5 . .
C12B C13B H13D 108.5 . .
K1 C13B H13D 61.5 . .
H13C C13B H13D 107.5 . .
O1B C14B C15B 107.0(5) . .
O1B C14B H14C 110.3 . .
C15B C14B H14C 110.3 . .
O1B C14B H14D 110.3 . .
C15B C14B H14D 110.3 . .
H14C C14B H14D 108.6 . .
C14B C15B H15D 109.5 . .
C14B C15B H15E 109.5 . .
H15D C15B H15E 109.5 . .
C14B C15B H15F 109.5 . .
H15D C15B H15F 109.5 . .
H15E C15B H15F 109.5 . .
O1D K3 N2D 86.30(14) . .
O1D K3 N2C 89.66(14) . .
N2D K3 N2C 175.27(16) . .
O1D K3 O1C 170.12(13) . .
N2D K3 O1C 94.97(14) . .
N2C K3 O1C 89.43(13) . .
O1D K3 N1C 89.20(15) . .
N2D K3 N1C 126.32(15) . .
N2C K3 N1C 55.98(13) . .
O1C K3 N1C 82.15(13) . .
O1D K3 N1D 91.01(15) . .
N2D K3 N1D 56.36(13) . .
N2C K3 N1D 121.34(15) . .
O1C K3 N1D 97.85(14) . .
N1C K3 N1D 177.31(17) . .
O1D K3 C6C 74.50(13) . .
N2D K3 C6C 156.80(15) . .
N2C K3 C6C 21.62(14) . .
O1C K3 C6C 101.79(14) . .
N1C K3 C6C 42.44(15) . .
N1D K3 C6C 135.15(15) . .
O1D K3 C6D 103.50(14) . .
N2D K3 C6D 22.46(14) . .
N2C K3 C6D 158.62(15) . .
O1C K3 C6D 80.40(13) . .
N1C K3 C6D 139.39(15) . .
N1D K3 C6D 43.07(15) . .
C6C K3 C6D 177.59(16) . .
O1D K3 C5D 105.66(14) . .
N2D K3 C5D 43.83(14) . .
N2C K3 C5D 135.63(15) . .
O1C K3 C5D 81.71(13) . .
N1C K3 C5D 159.87(16) . .
N1D K3 C5D 21.86(15) . .
C6C K3 C5D 154.41(15) . .
C6D K3 C5D 24.46(14) . .
O1D K3 C14D 25.53(15) . .
N2D K3 C14D 88.29(17) . .
N2C K3 C14D 89.12(16) . .
O1C K3 C14D 144.61(15) . .
N1C K3 C14D 67.96(16) . .
N1D K3 C14D 112.90(17) . .
C6C K3 C14D 68.77(16) . .
C6D K3 C14D 110.03(16) . .
C5D K3 C14D 121.96(16) . .
O1D K3 K4 48.96(10) . .
N2D K3 K4 45.01(10) . .
N2C K3 K4 130.26(10) . .
O1C K3 K4 136.26(9) . .
N1C K3 K4 132.17(10) . .
N1D K3 K4 49.23(10) . .
C6C K3 K4 121.81(10) . .
C6D K3 K4 55.95(10) . .
C5D K3 K4 57.74(9) . .
C14D K3 K4 65.08(13) . .
O1D K3 K2 129.10(10) . .
N2D K3 K2 139.13(11) . .
N2C K3 K2 45.58(10) . .
O1C K3 K2 46.50(8) . .
N1C K3 K2 49.00(10) . .
N1D K3 K2 129.37(10) . .
C6C K3 K2 55.29(10) . .
C6D K3 K2 126.88(10) . .
C5D K3 K2 122.92(9) . .
C14D K3 K2 114.90(13) . .
K4 K3 K2 175.36(3) . .
C1C N1C C5C 117.5(6) . .
C1C N1C K3 122.4(4) . .
C5C N1C K3 109.3(4) . .
C1C N1C K2 117.0(4) . .
C5C N1C K2 101.2(4) . .
K3 N1C K2 82.57(14) . .
C6C N2C C9C 105.3(5) . .
C6C N2C K2 107.6(3) . .
C9C N2C K2 126.9(4) . .
C6C N2C K3 107.6(3) . .
C9C N2C K3 119.3(3) . .
K2 N2C K3 88.37(16) . .
C2C C1C N1C 123.2(7) . .
C2C C1C H1C 118.4 . .
N1C C1C H1C 118.4 . .
C1C C2C C3C 119.8(6) . .
C1C C2C H2C 120.1 . .
C3C C2C H2C 120.1 . .
C4C C3C C2C 118.2(5) . .
C4C C3C H3C 120.9 . .
C2C C3C H3C 120.9 . .
C3C C4C C5C 121.7(6) . .
C3C C4C H4C 119.2 . .
C5C C4C H4C 119.2 . .
N1C C5C C4C 119.6(6) . .
N1C C5C C6C 113.8(6) . .
C4C C5C C6C 126.6(6) . .
N1C C5C K2 56.4(3) . .
C4C C5C K2 135.3(4) . .
C6C C5C K2 75.5(4) . .
N2C C6C C7C 110.6(5) . .
N2C C6C C5C 120.6(6) . .
C7C C6C C5C 128.8(6) . .
N2C C6C K2 50.6(3) . .
C7C C6C K2 138.4(4) . .
C5C C6C K2 80.2(4) . .
N2C C6C K3 50.8(3) . .
C7C C6C K3 133.1(4) . .
C5C C6C K3 84.8(4) . .
K2 C6C K3 68.95(14) . .
C8C C7C C6C 105.3(5) . .
C8C C7C C10C 122.9(6) . .
C6C C7C C10C 131.8(6) . .
C9C C8C C7C 105.2(5) . .
C9C C8C H8C 127.4 . .
C7C C8C H8C 127.4 . .
N2C C9C C8C 113.6(5) . .
N2C C9C C11C 118.1(6) . .
C8C C9C C11C 128.3(6) . .
F2C C10C F1C 105.3(6) . .
F2C C10C F3C 104.3(6) . .
F1C C10C F3C 104.1(6) . .
F2C C10C C7C 112.2(6) . .
F1C C10C C7C 115.5(6) . .
F3C C10C C7C 114.4(6) . .
F4C C11C F6C 107.4(5) . .
F4C C11C F5C 106.4(5) . .
F6C C11C F5C 103.6(5) . .
F4C C11C C9C 111.9(5) . .
F6C C11C C9C 112.9(5) . .
F5C C11C C9C 114.1(5) . .
C14C O1C C13C 114.3(4) . .
C14C O1C K2 124.6(3) . .
C13C O1C K2 99.7(3) . .
C14C O1C K3 116.6(3) . .
C13C O1C K3 111.8(3) . .
K2 O1C K3 85.93(13) . .
C13C C12C H12G 109.5 . .
C13C C12C H12H 109.5 . .
H12G C12C H12H 109.5 . .
C13C C12C H12I 109.5 . .
H12G C12C H12I 109.5 . .
H12H C12C H12I 109.5 . .
C12C C13C O1C 112.9(5) . .
C12C C13C K2 152.8(5) . .
O1C C13C K2 55.6(2) . .
C12C C13C H13E 109.0 . .
O1C C13C H13E 109.0 . .
K2 C13C H13E 60.8 . .
C12C C13C H13F 109.0 . .
O1C C13C H13F 109.0 . .
K2 C13C H13F 98.2 . .
H13E C13C H13F 107.8 . .
O1C C14C C15C 109.5(5) . .
O1C C14C H14E 109.8 . .
C15C C14C H14E 109.8 . .
O1C C14C H14F 109.8 . .
C15C C14C H14F 109.8 . .
H14E C14C H14F 108.2 . .
C14C C15C H15G 109.5 . .
C14C C15C H15H 109.5 . .
H15G C15C H15H 109.5 . .
C14C C15C H15I 109.5 . .
H15G C15C H15I 109.5 . .
H15H C15C H15I 109.5 . .
N2D K4 N2A 177.77(19) . 1_565
N2D K4 O1A 90.97(14) . 1_565
N2A K4 O1A 86.84(13) 1_565 1_565
N2D K4 N1A 124.19(15) . 1_565
N2A K4 N1A 56.39(13) 1_565 1_565
O1A K4 N1A 93.05(13) 1_565 1_565
N2D K4 O1D 84.50(14) . .
N2A K4 O1D 97.64(14) 1_565 .
O1A K4 O1D 172.35(14) 1_565 .
N1A K4 O1D 94.59(14) 1_565 .
N2D K4 N1D 56.59(14) . .
N2A K4 N1D 122.73(15) 1_565 .
O1A K4 N1D 84.59(14) 1_565 .
N1A K4 N1D 177.56(16) 1_565 .
O1D K4 N1D 87.77(14) . .
N2D K4 F4D 55.78(12) . .
N2A K4 F4D 125.21(12) 1_565 .
O1A K4 F4D 104.80(12) 1_565 .
N1A K4 F4D 69.48(11) 1_565 .
O1D K4 F4D 77.71(12) . .
N1D K4 F4D 111.70(12) . .
N2D K4 C6A 159.91(15) . 1_565
N2A K4 C6A 22.02(13) 1_565 1_565
O1A K4 C6A 103.99(13) 1_565 1_565
N1A K4 C6A 42.99(14) 1_565 1_565
O1D K4 C6A 81.92(13) . 1_565
N1D K4 C6A 137.07(15) . 1_565
F4D K4 C6A 106.58(12) . 1_565
N2D K4 C6D 21.99(14) . .
N2A K4 C6D 156.03(15) 1_565 .
O1A K4 C6D 73.81(13) 1_565 .
N1A K4 C6D 136.90(14) 1_565 .
O1D K4 C6D 100.25(14) . .
N1D K4 C6D 42.90(15) . .
F4D K4 C6D 74.54(12) . .
C6A K4 C6D 177.76(15) 1_565 .
N2D K4 K1 132.39(11) . 1_565
N2A K4 K1 45.91(10) 1_565 1_565
O1A K4 K1 49.36(9) 1_565 1_565
N1A K4 K1 50.00(10) 1_565 1_565
O1D K4 K1 137.51(9) . 1_565
N1D K4 K1 127.60(10) . 1_565
F4D K4 K1 104.22(8) . 1_565
C6A K4 K1 56.48(9) 1_565 1_565
C6D K4 K1 121.46(10) . 1_565
N2D K4 K3 46.13(10) . .
N2A K4 K3 135.43(10) 1_565 .
O1A K4 K3 127.19(9) 1_565 .
N1A K4 K3 133.67(10) 1_565 .
O1D K4 K3 45.81(9) . .
N1D K4 K3 48.71(9) . .
F4D K4 K3 77.77(7) . .
C6A K4 K3 126.25(10) 1_565 .
C6D K4 K3 55.75(10) . .
K1 K4 K3 176.24(3) 1_565 .
C11D F4D K4 106.2(3) . .
C1D N1D C5D 118.8(6) . .
C1D N1D K3 118.6(4) . .
C5D N1D K3 102.1(3) . .
C1D N1D K4 122.1(4) . .
C5D N1D K4 106.1(4) . .
K3 N1D K4 82.05(14) . .
C9D N2D C6D 105.5(5) . .
C9D N2D K4 117.9(3) . .
C6D N2D K4 109.7(3) . .
C9D N2D K3 127.0(4) . .
C6D N2D K3 106.6(3) . .
K4 N2D K3 88.85(16) . .
N1D C1D C2D 124.2(7) . .
N1D C1D H1DA 117.9 . .
C2D C1D H1DA 117.9 . .
C3D C2D C1D 116.6(6) . .
C3D C2D H2D 121.7 . .
C1D C2D H2D 121.7 . .
C2D C3D C4D 120.8(6) . .
C2D C3D H3D 119.6 . .
C4D C3D H3D 119.6 . .
C5D C4D C3D 118.8(6) . .
C5D C4D H4D 120.6 . .
C3D C4D H4D 120.6 . .
N1D C5D C4D 120.8(6) . .
N1D C5D C6D 118.3(6) . .
C4D C5D C6D 120.9(6) . .
N1D C5D K3 56.0(3) . .
C4D C5D K3 140.9(4) . .
C6D C5D K3 77.1(3) . .
N2D C6D C7D 109.0(5) . .
N2D C6D C5D 116.8(6) . .
C7D C6D C5D 134.1(6) . .
N2D C6D K3 51.0(3) . .
C7D C6D K3 138.6(4) . .
C5D C6D K3 78.5(3) . .
N2D C6D K4 48.3(3) . .
C7D C6D K4 130.1(4) . .
C5D C6D K4 82.1(4) . .
K3 C6D K4 68.30(14) . .
C8D C7D C6D 108.5(5) . .
C8D C7D C110 122.0(6) . .
C6D C7D C110 129.4(5) . .
C7D C8D C9D 104.7(5) . .
C7D C8D H8D 127.7 . .
C9D C8D H8D 127.7 . .
N2D C9D C8D 112.3(5) . .
N2D C9D C11D 120.9(6) . .
C8D C9D C11D 126.7(6) . .
F6D C11D F4D 106.2(5) . .
F6D C11D F5D 105.0(5) . .
F4D C11D F5D 104.8(6) . .
F6D C11D C9D 114.7(6) . .
F4D C11D C9D 112.5(5) . .
F5D C11D C9D 112.8(5) . .
F3D C110 F1D 106.7(6) . .
F3D C110 F2D 106.8(6) . .
F1D C110 F2D 105.4(6) . .
F3D C110 C7D 113.5(6) . .
F1D C110 C7D 113.4(6) . .
F2D C110 C7D 110.4(5) . .
C13D O1D C14D 110.8(6) . .
C13D O1D K3 124.5(4) . .
C14D O1D K3 103.8(3) . .
C13D O1D K4 109.5(4) . .
C14D O1D K4 122.0(3) . .
K3 O1D K4 85.23(13) . .
C13D C12D H12J 109.5 . .
C13D C12D H12K 109.5 . .
H12J C12D H12K 109.5 . .
C13D C12D H12L 109.5 . .
H12J C12D H12L 109.5 . .
H12K C12D H12L 109.5 . .
O1D C13D C12D 109.4(6) . .
O1D C13D H13G 109.8 . .
C12D C13D H13G 109.8 . .
O1D C13D H13H 109.8 . .
C12D C13D H13H 109.8 . .
H13G C13D H13H 108.2 . .
C15D C14D O1D 106.4(6) . .
C15D C14D K3 138.5(5) . .
O1D C14D K3 50.7(3) . .
C15D C14D H14G 110.4 . .
O1D C14D H14G 110.4 . .
K3 C14D H14G 110.2 . .
C15D C14D H14H 110.4 . .
O1D C14D H14H 110.4 . .
K3 C14D H14H 62.7 . .
H14G C14D H14H 108.6 . .
C14D C15D H15J 109.5 . .
C14D C15D H15K 109.5 . .
H15J C15D H15K 109.5 . .
C14D C15D H15L 109.5 . .
H15J C15D H15L 109.5 . .
H15K C15D H15L 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
K1 N2A 2.796(5) .
K1 N2B 2.829(5) .
K1 O1B 2.857(4) .
K1 O1A 2.968(4) .
K1 N1B 2.974(5) .
K1 N1A 3.010(5) .
K1 C13B 3.426(6) .
K1 C6B 3.469(6) .
K1 C6A 3.497(6) .
K1 K4 3.888(3) 1_545
K1 K2 3.920(2) .
F1A C10A 1.330(8) .
F2A C10A 1.356(8) .
F3A C10A 1.354(8) .
F4A C11A 1.342(7) .
F5A C11A 1.330(7) .
F6A C11A 1.355(7) .
N1A C1A 1.360(8) .
N1A C5A 1.377(8) .
N1A K4 2.933(5) 1_545
N2A C6A 1.346(8) .
N2A C9A 1.372(8) .
N2A K4 2.841(5) 1_545
C1A C2A 1.355(9) .
C1A H1A 0.9500 .
C2A C3A 1.397(9) .
C2A H2A 0.9500 .
C3A C4A 1.375(8) .
C3A H3A 0.9500 .
C4A C5A 1.382(9) .
C4A H4A 0.9500 .
C5A C6A 1.477(9) .
C6A C7A 1.435(9) .
C6A K4 3.457(6) 1_545
C7A C8A 1.406(8) .
C7A C10A 1.456(10) .
C8A C9A 1.361(9) .
C8A H8A 0.9500 .
C9A C11A 1.475(8) .
O1A C13A 1.370(7) .
O1A C14A 1.470(8) .
O1A K4 2.852(4) 1_545
C12A C13A 1.480(10) .
C12A H12A 0.9800 .
C12A H12B 0.9800 .
C12A H12C 0.9800 .
C13A H13A 0.9900 .
C13A H13B 0.9900 .
C14A C15A 1.488(8) .
C14A H14A 0.9900 .
C14A H14B 0.9900 .
C15A H15A 0.9800 .
C15A H15B 0.9800 .
C15A H15C 0.9800 .
K2 N2C 2.811(5) .
K2 N2B 2.814(5) .
K2 O1C 2.861(4) .
K2 O1B 2.869(4) .
K2 N1B 2.947(5) .
K2 N1C 2.994(5) .
K2 C13C 3.418(6) .
K2 C6C 3.465(7) .
K2 C5B 3.485(6) .
K2 C6B 3.513(7) .
K2 C5C 3.528(7) .
F1B C10B 1.349(8) .
F2B C10B 1.339(7) .
F3B C10B 1.357(7) .
F4B C11B 1.372(7) .
F5B C11B 1.333(7) .
F6B C11B 1.348(7) .
N1B C1B 1.321(8) .
N1B C5B 1.345(9) .
N2B C9B 1.355(8) .
N2B C6B 1.379(8) .
C1B C2B 1.410(9) .
C1B H1B 0.9500 .
C2B C3B 1.376(8) .
C2B H2B 0.9500 .
C3B C4B 1.387(8) .
C3B H3B 0.9500 .
C4B C5B 1.406(8) .
C4B H4B 0.9500 .
C5B C6B 1.487(8) .
C6B C7B 1.386(10) .
C7B C8B 1.384(8) .
C7B C10B 1.496(9) .
C8B C9B 1.391(8) .
C8B H8B 0.9500 .
C9B C11B 1.457(9) .
O1B C13B 1.438(6) .
O1B C14B 1.451(6) .
C12B C13B 1.463(8) .
C12B H12D 0.9800 .
C12B H12E 0.9800 .
C12B H12F 0.9800 .
C13B H13C 0.9900 .
C13B H13D 0.9900 .
C14B C15B 1.511(8) .
C14B H14C 0.9900 .
C14B H14D 0.9900 .
C15B H15D 0.9800 .
C15B H15E 0.9800 .
C15B H15F 0.9800 .
K3 O1D 2.820(5) .
K3 N2D 2.826(5) .
K3 N2C 2.833(5) .
K3 O1C 2.911(4) .
K3 N1C 2.968(5) .
K3 N1D 2.973(5) .
K3 C6C 3.485(6) .
K3 C6D 3.487(7) .
K3 C5D 3.505(6) .
K3 C14D 3.539(7) .
K3 K4 3.919(3) .
F1C C10C 1.335(8) .
F2C C10C 1.331(8) .
F3C C10C 1.343(7) .
F4C C11C 1.332(7) .
F5C C11C 1.334(7) .
F6C C11C 1.333(7) .
N1C C1C 1.371(8) .
N1C C5C 1.372(9) .
N2C C6C 1.347(8) .
N2C C9C 1.371(8) .
C1C C2C 1.341(9) .
C1C H1C 0.9500 .
C2C C3C 1.386(9) .
C2C H2C 0.9500 .
C3C C4C 1.354(8) .
C3C H3C 0.9500 .
C4C C5C 1.394(8) .
C4C H4C 0.9500 .
C5C C6C 1.473(9) .
C6C C7C 1.446(9) .
C7C C8C 1.418(8) .
C7C C10C 1.455(10) .
C8C C9C 1.373(8) .
C8C H8C 0.9500 .
C9C C11C 1.479(8) .
O1C C14C 1.420(6) .
O1C C13C 1.450(7) .
C12C C13C 1.444(8) .
C12C H12G 0.9800 .
C12C H12H 0.9800 .
C12C H12I 0.9800 .
C13C H13E 0.9900 .
C13C H13F 0.9900 .
C14C C15C 1.497(8) .
C14C H14E 0.9900 .
C14C H14F 0.9900 .
C15C H15G 0.9800 .
C15C H15H 0.9800 .
C15C H15I 0.9800 .
K4 N2D 2.772(5) .
K4 N2A 2.841(5) 1_565
K4 O1A 2.852(4) 1_565
K4 N1A 2.933(5) 1_565
K4 O1D 2.966(5) .
K4 N1D 2.997(5) .
K4 F4D 3.404(4) .
K4 C6A 3.457(6) 1_565
K4 C6D 3.495(7) .
K4 K1 3.888(3) 1_565
F1D C110 1.348(8) .
F2D C110 1.350(8) .
F3D C110 1.340(8) .
F4D C11D 1.364(7) .
F5D C11D 1.368(7) .
F6D C11D 1.330(7) .
N1D C1D 1.321(7) .
N1D C5D 1.335(9) .
N2D C9D 1.351(8) .
N2D C6D 1.390(8) .
C1D C2D 1.392(9) .
C1D H1DA 0.9500 .
C2D C3D 1.348(9) .
C2D H2D 0.9500 .
C3D C4D 1.390(9) .
C3D H3D 0.9500 .
C4D C5D 1.385(9) .
C4D H4D 0.9500 .
C5D C6D 1.481(9) .
C6D C7D 1.396(9) .
C7D C8D 1.383(8) .
C7D C110 1.502(9) .
C8D C9D 1.402(9) .
C8D H8D 0.9500 .
C9D C11D 1.448(9) .
O1D C13D 1.400(7) .
O1D C14D 1.570(9) .
C12D C13D 1.466(11) .
C12D H12J 0.9800 .
C12D H12K 0.9800 .
C12D H12L 0.9800 .
C13D H13G 0.9900 .
C13D H13H 0.9900 .
C14D C15D 1.409(9) .
C14D H14G 0.9900 .
C14D H14H 0.9900 .
C15D H15J 0.9800 .
C15D H15K 0.9800 .
C15D H15L 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N2A K1 N1A C1A -179.5(5) . .
N2B K1 N1A C1A -6.1(5) . .
O1B K1 N1A C1A -95.8(4) . .
O1A K1 N1A C1A 95.5(5) . .
N1B K1 N1A C1A -79.8(18) . .
C13B K1 N1A C1A -119.3(4) . .
C6B K1 N1A C1A 15.2(5) . .
C6A K1 N1A C1A -157.8(5) . .
K4 K1 N1A C1A 120.7(5) 1_545 .
K2 K1 N1A C1A -61.8(5) . .
N2A K1 N1A C5A -46.8(3) . .
N2B K1 N1A C5A 126.5(3) . .
O1B K1 N1A C5A 36.8(3) . .
O1A K1 N1A C5A -131.9(3) . .
N1B K1 N1A C5A 52.9(18) . .
C13B K1 N1A C5A 13.3(4) . .
C6B K1 N1A C5A 147.8(3) . .
C6A K1 N1A C5A -25.1(3) . .
K4 K1 N1A C5A -106.7(4) 1_545 .
K2 K1 N1A C5A 70.8(4) . .
N2A K1 N1A K4 59.83(14) . 1_545
N2B K1 N1A K4 -126.80(14) . 1_545
O1B K1 N1A K4 143.51(11) . 1_545
O1A K1 N1A K4 -25.22(12) . 1_545
N1B K1 N1A K4 159.5(16) . 1_545
C13B K1 N1A K4 120.00(13) . 1_545
C6B K1 N1A K4 -105.49(19) . 1_545
C6A K1 N1A K4 81.53(18) . 1_545
K2 K1 N1A K4 177.49(3) . 1_545
N2B K1 N2A C6A -26.4(18) . .
O1B K1 N2A C6A -50.9(4) . .
O1A K1 N2A C6A 135.7(4) . .
N1B K1 N2A C6A -128.8(4) . .
N1A K1 N2A C6A 43.5(3) . .
C13B K1 N2A C6A -70.7(4) . .
C6B K1 N2A C6A -171.7(5) . .
K4 K1 N2A C6A 105.7(4) 1_545 .
K2 K1 N2A C6A -67.3(4) . .
N2B K1 N2A C9A 101.3(17) . .
O1B K1 N2A C9A 76.8(4) . .
O1A K1 N2A C9A -96.7(4) . .
N1B K1 N2A C9A -1.2(5) . .
N1A K1 N2A C9A 171.2(5) . .
C13B K1 N2A C9A 57.0(4) . .
C6B K1 N2A C9A -44.0(8) . .
C6A K1 N2A C9A 127.6(6) . .
K4 K1 N2A C9A -126.7(5) 1_545 .
K2 K1 N2A C9A 60.4(5) . .
N2B K1 N2A K4 -132.0(16) . 1_545
O1B K1 N2A K4 -156.53(12) . 1_545
O1A K1 N2A K4 29.99(13) . 1_545
N1B K1 N2A K4 125.48(16) . 1_545
N1A K1 N2A K4 -62.14(14) . 1_545
C13B K1 N2A K4 -176.36(16) . 1_545
C6B K1 N2A K4 82.6(5) . 1_545
C6A K1 N2A K4 -105.7(4) . 1_545
K2 K1 N2A K4 -172.94(4) . 1_545
C5A N1A C1A C2A -0.8(8) . .
K4 N1A C1A C2A -136.2(5) 1_545 .
K1 N1A C1A C2A 125.6(5) . .
N1A C1A C2A C3A -0.6(9) . .
C1A C2A C3A C4A 1.3(9) . .
C2A C3A C4A C5A -0.7(9) . .
C1A N1A C5A C4A 1.4(8) . .
K4 N1A C5A C4A 142.0(5) 1_545 .
K1 N1A C5A C4A -132.5(5) . .
C1A N1A C5A C6A -178.4(4) . .
K4 N1A C5A C6A -37.8(5) 1_545 .
K1 N1A C5A C6A 47.7(5) . .
C3A C4A C5A N1A -0.6(9) . .
C3A C4A C5A C6A 179.1(6) . .
C9A N2A C6A C7A 1.8(5) . .
K1 N2A C6A C7A 139.3(4) . .
K4 N2A C6A C7A -127.9(4) 1_545 .
C9A N2A C6A C5A -178.8(5) . .
K1 N2A C6A C5A -41.3(5) . .
K4 N2A C6A C5A 51.5(5) 1_545 .
C9A N2A C6A K4 129.7(4) . 1_545
K1 N2A C6A K4 -92.8(3) . 1_545
C9A N2A C6A K1 -137.5(4) . .
K4 N2A C6A K1 92.8(3) 1_545 .
N1A C5A C6A N2A -8.7(7) . .
C4A C5A C6A N2A 171.5(5) . .
N1A C5A C6A C7A 170.5(5) . .
C4A C5A C6A C7A -9.2(9) . .
N1A C5A C6A K4 29.8(4) . 1_545
C4A C5A C6A K4 -149.9(6) . 1_545
N1A C5A C6A K1 -38.8(4) . .
C4A C5A C6A K1 141.5(6) . .
N2B K1 C6A N2A 174.1(4) . .
O1B K1 C6A N2A 125.8(4) . .
O1A K1 C6A N2A -45.1(4) . .
N1B K1 C6A N2A 66.9(4) . .
N1A K1 C6A N2A -122.1(4) . .
C13B K1 C6A N2A 100.8(4) . .
C6B K1 C6A N2A 149(2) . .
K4 K1 C6A N2A -58.5(3) 1_545 .
K2 K1 C6A N2A 125.6(3) . .
N2A K1 C6A C7A -70.9(6) . .
N2B K1 C6A C7A 103.2(6) . .
O1B K1 C6A C7A 54.9(6) . .
O1A K1 C6A C7A -116.0(6) . .
N1B K1 C6A C7A -4.0(7) . .
N1A K1 C6A C7A 167.1(7) . .
C13B K1 C6A C7A 30.0(5) . .
C6B K1 C6A C7A 78(2) . .
K4 K1 C6A C7A -129.3(6) 1_545 .
K2 K1 C6A C7A 54.8(6) . .
N2A K1 C6A C5A 145.0(5) . .
N2B K1 C6A C5A -40.9(5) . .
O1B K1 C6A C5A -89.2(3) . .
O1A K1 C6A C5A 99.8(3) . .
N1B K1 C6A C5A -148.1(3) . .
N1A K1 C6A C5A 22.9(3) . .
C13B K1 C6A C5A -114.2(3) . .
C6B K1 C6A C5A -66(2) . .
K4 K1 C6A C5A 86.5(3) 1_545 .
K2 K1 C6A C5A -89.4(3) . .
N2A K1 C6A K4 58.5(3) . 1_545
N2B K1 C6A K4 -127.4(3) . 1_545
O1B K1 C6A K4 -175.73(12) . 1_545
O1A K1 C6A K4 13.34(13) . 1_545
N1B K1 C6A K4 125.36(18) . 1_545
N1A K1 C6A K4 -63.59(16) . 1_545
C13B K1 C6A K4 159.31(15) . 1_545
C6B K1 C6A K4 -153(2) . 1_545
K2 K1 C6A K4 -175.89(4) . 1_545
N2A C6A C7A C8A -2.1(6) . .
C5A C6A C7A C8A 178.6(5) . .
K4 C6A C7A C8A -58.9(6) 1_545 .
K1 C6A C7A C8A 47.0(7) . .
N2A C6A C7A C10A 178.6(6) . .
C5A C6A C7A C10A -0.7(10) . .
K4 C6A C7A C10A 121.7(6) 1_545 .
K1 C6A C7A C10A -132.3(6) . .
C6A C7A C8A C9A 1.5(6) . .
C10A C7A C8A C9A -179.1(5) . .
C7A C8A C9A N2A -0.4(6) . .
C7A C8A C9A C11A 178.7(5) . .
C6A N2A C9A C8A -0.9(6) . .
K1 N2A C9A C8A -130.3(4) . .
K4 N2A C9A C8A 119.1(4) 1_545 .
C6A N2A C9A C11A 179.9(5) . .
K1 N2A C9A C11A 50.5(6) . .
K4 N2A C9A C11A -60.1(6) 1_545 .
C8A C7A C10A F1A 6.6(9) . .
C6A C7A C10A F1A -174.2(6) . .
C8A C7A C10A F3A 127.4(6) . .
C6A C7A C10A F3A -53.4(9) . .
C8A C7A C10A F2A -113.7(7) . .
C6A C7A C10A F2A 65.5(9) . .
C8A C9A C11A F5A 123.4(6) . .
N2A C9A C11A F5A -57.5(7) . .
C8A C9A C11A F4A 1.9(8) . .
N2A C9A C11A F4A -179.0(4) . .
C8A C9A C11A F6A -118.7(7) . .
N2A C9A C11A F6A 60.4(7) . .
N2A K1 O1A C13A -152.7(4) . .
N2B K1 O1A C13A 25.4(4) . .
O1B K1 O1A C13A 172.0(6) . .
N1B K1 O1A C13A 82.7(4) . .
N1A K1 O1A C13A -96.8(4) . .
C13B K1 O1A C13A 161.0(4) . .
C6B K1 O1A C13A 41.1(4) . .
C6A K1 O1A C13A -137.8(4) . .
K4 K1 O1A C13A -122.7(4) 1_545 .
K2 K1 O1A C13A 54.6(4) . .
N2A K1 O1A C14A 79.9(4) . .
N2B K1 O1A C14A -101.9(4) . .
O1B K1 O1A C14A 44.6(8) . .
N1B K1 O1A C14A -44.7(4) . .
N1A K1 O1A C14A 135.8(4) . .
C13B K1 O1A C14A 33.6(5) . .
C6B K1 O1A C14A -86.3(4) . .
C6A K1 O1A C14A 94.8(4) . .
K4 K1 O1A C14A 109.9(4) 1_545 .
K2 K1 O1A C14A -72.8(4) . .
N2A K1 O1A K4 -30.02(13) . 1_545
N2B K1 O1A K4 148.11(13) . 1_545
O1B K1 O1A K4 -65.4(6) . 1_545
N1B K1 O1A K4 -154.67(14) . 1_545
N1A K1 O1A K4 25.86(13) . 1_545
C13B K1 O1A K4 -76.4(3) . 1_545
C6B K1 O1A K4 163.74(14) . 1_545
C6A K1 O1A K4 -15.12(14) . 1_545
K2 K1 O1A K4 177.24(5) . 1_545
C14A O1A C13A C12A -171.4(5) . .
K4 O1A C13A C12A -33.8(6) 1_545 .
K1 O1A C13A C12A 58.2(5) . .
C13A O1A C14A C15A -80.9(6) . .
K4 O1A C14A C15A 136.1(5) 1_545 .
K1 O1A C14A C15A 42.0(6) . .
N2A K1 K2 N2C -4.12(16) . .
N2B K1 K2 N2C -178.6(3) . .
O1B K1 K2 N2C -26.80(18) . .
O1A K1 K2 N2C 139.5(2) . .
N1B K1 K2 N2C 100.7(2) . .
N1A K1 K2 N2C -76.7(2) . .
C13B K1 K2 N2C -0.36(19) . .
C6B K1 K2 N2C 155.6(2) . .
C6A K1 K2 N2C -26.6(2) . .
K4 K1 K2 N2C -59.3(3) 1_545 .
N2A K1 K2 N2B 174.5(3) . .
O1B K1 K2 N2B 151.85(18) . .
O1A K1 K2 N2B -41.9(2) . .
N1B K1 K2 N2B -80.7(2) . .
N1A K1 K2 N2B 101.92(19) . .
C13B K1 K2 N2B 178.28(19) . .
C6B K1 K2 N2B -25.72(18) . .
C6A K1 K2 N2B 152.06(19) . .
K4 K1 K2 N2B 119.3(3) 1_545 .
N2A K1 K2 O1C -161.98(16) . .
N2B K1 K2 O1C 23.49(17) . .
O1B K1 K2 O1C 175.34(18) . .
O1A K1 K2 O1C -18.40(18) . .
N1B K1 K2 O1C -57.20(19) . .
N1A K1 K2 O1C 125.42(16) . .
C13B K1 K2 O1C -158.23(16) . .
C6B K1 K2 O1C -2.23(15) . .
C6A K1 K2 O1C 175.55(15) . .
K4 K1 K2 O1C 142.8(2) 1_545 .
N2A K1 K2 O1B 22.68(17) . .
N2B K1 K2 O1B -151.85(18) . .
O1A K1 K2 O1B 166.26(17) . .
N1B K1 K2 O1B 127.46(19) . .
N1A K1 K2 O1B -49.92(15) . .
C13B K1 K2 O1B 26.43(15) . .
C6B K1 K2 O1B -177.57(16) . .
C6A K1 K2 O1B 0.21(14) . .
K4 K1 K2 O1B -32.5(3) 1_545 .
N2A K1 K2 N1B -104.8(2) . .
N2B K1 K2 N1B 80.7(2) . .
O1B K1 K2 N1B -127.46(19) . .
O1A K1 K2 N1B 38.8(2) . .
N1A K1 K2 N1B -177.4(3) . .
C13B K1 K2 N1B -101.0(2) . .
C6B K1 K2 N1B 55.0(2) . .
C6A K1 K2 N1B -127.24(19) . .
K4 K1 K2 N1B -160.0(3) 1_545 .
N2A K1 K2 N1C 80.2(2) . .
N2B K1 K2 N1C -94.4(2) . .
O1B K1 K2 N1C 57.48(18) . .
O1A K1 K2 N1C -136.3(2) . .
N1B K1 K2 N1C -175.1(3) . .
N1A K1 K2 N1C 7.55(13) . .
C13B K1 K2 N1C 83.91(19) . .
C6B K1 K2 N1C -120.09(19) . .
C6A K1 K2 N1C 57.69(19) . .
K4 K1 K2 N1C 24.9(3) 1_545 .
N2A K1 K2 C13C 173.41(18) . .
N2B K1 K2 C13C -1.12(18) . .
O1B K1 K2 C13C 150.73(16) . .
O1A K1 K2 C13C -43.02(18) . .
N1B K1 K2 C13C -81.8(2) . .
N1A K1 K2 C13C 100.80(17) . .
C13B K1 K2 C13C 177.2(2) . .
C6B K1 K2 C13C -26.84(16) . .
C6A K1 K2 C13C 150.94(17) . .
K4 K1 K2 C13C 118.2(3) 1_545 .
N2A K1 K2 C6C 22.97(19) . .
N2B K1 K2 C6C -151.6(2) . .
O1B K1 K2 C6C 0.29(16) . .
O1A K1 K2 C6C 166.55(19) . .
N1B K1 K2 C6C 127.7(2) . .
N1A K1 K2 C6C -49.63(18) . .
C13B K1 K2 C6C 26.73(17) . .
C6B K1 K2 C6C -177.3(2) . .
C6A K1 K2 C6C 0.51(13) . .
K4 K1 K2 C6C -32.2(3) 1_545 .
N2A K1 K2 C5B -130.3(2) . .
N2B K1 K2 C5B 55.13(19) . .
O1B K1 K2 C5B -153.02(17) . .
O1A K1 K2 C5B 13.23(19) . .
N1B K1 K2 C5B -25.57(19) . .
N1A K1 K2 C5B 157.05(18) . .
C13B K1 K2 C5B -126.59(18) . .
C6B K1 K2 C5B 29.41(17) . .
C6A K1 K2 C5B -152.81(18) . .
K4 K1 K2 C5B 174.4(3) 1_545 .
N2A K1 K2 C6B -159.75(19) . .
N2B K1 K2 C6B 25.72(18) . .
O1B K1 K2 C6B 177.57(16) . .
O1A K1 K2 C6B -16.18(18) . .
N1B K1 K2 C6B -55.0(2) . .
N1A K1 K2 C6B 127.64(17) . .
C13B K1 K2 C6B -156.00(17) . .
C6A K1 K2 C6B 177.8(2) . .
K4 K1 K2 C6B 145.0(3) 1_545 .
N2A K1 K2 C5C 53.00(19) . .
N2B K1 K2 C5C -121.5(2) . .
O1B K1 K2 C5C 30.32(16) . .
O1A K1 K2 C5C -163.42(19) . .
N1B K1 K2 C5C 157.8(2) . .
N1A K1 K2 C5C -19.60(19) . .
C13B K1 K2 C5C 56.76(18) . .
C6B K1 K2 C5C -147.24(18) . .
C6A K1 K2 C5C 30.54(18) . .
K4 K1 K2 C5C -2.2(3) 1_545 .
N2C K2 N1B C1B -4.2(6) . .
N2B K2 N1B C1B -178.1(5) . .
O1C K2 N1B C1B -98.3(5) . .
O1B K2 N1B C1B 88.3(5) . .
N1C K2 N1B C1B -129(2) . .
C13C K2 N1B C1B -122.6(5) . .
C6C K2 N1B C1B 18.7(6) . .
C5B K2 N1B C1B -131.0(7) . .
C6B K2 N1B C1B -156.1(6) . .
C5C K2 N1B C1B 47.0(7) . .
K1 K2 N1B C1B 123.9(5) . .
N2C K2 N1B C5B 126.9(3) . .
N2B K2 N1B C5B -47.1(3) . .
O1C K2 N1B C5B 32.7(4) . .
O1B K2 N1B C5B -140.6(4) . .
N1C K2 N1B C5B 2(2) . .
C13C K2 N1B C5B 8.5(4) . .
C6C K2 N1B C5B 149.7(3) . .
C6B K2 N1B C5B -25.0(3) . .
C5C K2 N1B C5B 178.0(5) . .
K1 K2 N1B C5B -105.1(4) . .
N2C K2 N1B K1 -128.03(15) . .
N2B K2 N1B K1 58.00(14) . .
O1C K2 N1B K1 137.79(12) . .
O1B K2 N1B K1 -35.55(12) . .
N1C K2 N1B K1 108(2) . .
C13C K2 N1B K1 113.54(14) . .
C6C K2 N1B K1 -105.2(2) . .
C5B K2 N1B K1 105.1(4) . .
C6B K2 N1B K1 80.07(18) . .
C5C K2 N1B K1 -76.9(5) . .
N2A K1 N1B C1B -1.9(6) . .
N2B K1 N1B C1B -174.9(6) . .
O1B K1 N1B C1B -81.1(5) . .
O1A K1 N1B C1B 87.5(5) . .
N1A K1 N1B C1B -97.3(16) . .
C13B K1 N1B C1B -57.0(5) . .
C6B K1 N1B C1B 161.0(6) . .
C6A K1 N1B C1B -25.8(6) . .
K4 K1 N1B C1B 59.9(6) 1_545 .
K2 K1 N1B C1B -116.9(6) . .
N2A K1 N1B C5B -144.5(3) . .
N2B K1 N1B C5B 42.6(3) . .
O1B K1 N1B C5B 136.3(4) . .
O1A K1 N1B C5B -55.1(4) . .
N1A K1 N1B C5B 120.2(16) . .
C13B K1 N1B C5B 160.4(4) . .
C6B K1 N1B C5B 18.5(3) . .
C6A K1 N1B C5B -168.4(3) . .
K4 K1 N1B C5B -82.6(4) 1_545 .
K2 K1 N1B C5B 100.6(4) . .
N2A K1 N1B K2 114.99(16) . .
N2B K1 N1B K2 -58.00(15) . .
O1B K1 N1B K2 35.75(12) . .
O1A K1 N1B K2 -155.60(13) . .
N1A K1 N1B K2 19.6(17) . .
C13B K1 N1B K2 59.86(14) . .
C6B K1 N1B K2 -82.10(18) . .
C6A K1 N1B K2 91.1(2) . .
K4 K1 N1B K2 176.82(5) 1_545 .
N2C K2 N2B C9B 47(2) . .
O1C K2 N2B C9B 73.5(5) . .
O1B K2 N2B C9B -105.0(5) . .
N1B K2 N2B C9B 172.6(5) . .
N1C K2 N2B C9B -4.0(5) . .
C13C K2 N2B C9B 53.8(5) . .
C6C K2 N2B C9B -37.1(7) . .
C5B K2 N2B C9B 149.2(6) . .
C6B K2 N2B C9B 128.9(7) . .
C5C K2 N2B C9B -25.9(6) . .
K1 K2 N2B C9B -125.1(5) . .
N2C K2 N2B C6B -82.3(19) . .
O1C K2 N2B C6B -55.3(4) . .
O1B K2 N2B C6B 126.1(4) . .
N1B K2 N2B C6B 43.8(4) . .
N1C K2 N2B C6B -132.9(4) . .
C13C K2 N2B C6B -75.1(4) . .
C6C K2 N2B C6B -166.0(4) . .
C5B K2 N2B C6B 20.3(3) . .
C5C K2 N2B C6B -154.8(3) . .
K1 K2 N2B C6B 106.0(4) . .
N2C K2 N2B K1 171.6(18) . .
O1C K2 N2B K1 -161.36(13) . .
O1B K2 N2B K1 20.07(12) . .
N1B K2 N2B K1 -62.27(16) . .
N1C K2 N2B K1 121.10(16) . .
C13C K2 N2B K1 178.90(18) . .
C6C K2 N2B K1 88.0(4) . .
C5B K2 N2B K1 -85.72(19) . .
C6B K2 N2B K1 -106.0(4) . .
C5C K2 N2B K1 99.2(2) . .
N2A K1 N2B C9B 89.3(17) . .
O1B K1 N2B C9B 113.7(4) . .
O1A K1 N2B C9B -72.4(4) . .
N1B K1 N2B C9B -164.2(5) . .
N1A K1 N2B C9B 23.0(5) . .
C13B K1 N2B C9B 132.4(4) . .
C6B K1 N2B C9B -116.9(6) . .
C6A K1 N2B C9B 68.4(6) . .
K4 K1 N2B C9B -38.1(5) 1_545 .
K2 K1 N2B C9B 133.9(5) . .
N2A K1 N2B C6B -153.7(15) . .
O1B K1 N2B C6B -129.3(4) . .
O1A K1 N2B C6B 44.5(4) . .
N1B K1 N2B C6B -47.3(4) . .
N1A K1 N2B C6B 140.0(4) . .
C13B K1 N2B C6B -110.7(4) . .
C6A K1 N2B C6B -174.7(4) . .
K4 K1 N2B C6B 78.9(4) 1_545 .
K2 K1 N2B C6B -109.2(4) . .
N2A K1 N2B K2 -44.6(17) . .
O1B K1 N2B K2 -20.16(13) . .
O1A K1 N2B K2 153.65(12) . .
N1B K1 N2B K2 61.85(16) . .
N1A K1 N2B K2 -110.85(15) . .
C13B K1 N2B K2 -1.53(17) . .
C6B K1 N2B K2 109.2(4) . .
C6A K1 N2B K2 -65.5(4) . .
K4 K1 N2B K2 -171.98(5) 1_545 .
C5B N1B C1B C2B 0.3(9) . .
K2 N1B C1B C2B 122.9(6) . .
K1 N1B C1B C2B -137.9(5) . .
N1B C1B C2B C3B -2.3(10) . .
C1B C2B C3B C4B 1.9(10) . .
C2B C3B C4B C5B 0.3(9) . .
C1B N1B C5B C4B 2.1(8) . .
K2 N1B C5B C4B -127.3(5) . .
K1 N1B C5B C4B 146.7(4) . .
C1B N1B C5B C6B -179.8(5) . .
K2 N1B C5B C6B 50.8(5) . .
K1 N1B C5B C6B -35.2(5) . .
C1B N1B C5B K2 129.4(6) . .
K1 N1B C5B K2 -86.0(2) . .
C3B C4B C5B N1B -2.5(8) . .
C3B C4B C5B C6B 179.5(5) . .
C3B C4B C5B K2 -74.4(7) . .
N2C K2 C5B N1B -70.8(4) . .
N2B K2 C5B N1B 117.8(4) . .
O1C K2 C5B N1B -146.2(4) . .
O1B K2 C5B N1B 39.8(4) . .
N1C K2 C5B N1B -179.6(4) . .
C13C K2 C5B N1B -171.5(4) . .
C6C K2 C5B N1B -56.2(5) . .
C6B K2 C5B N1B 135.9(5) . .
C5C K2 C5B N1B -170(3) . .
K1 K2 C5B N1B 59.4(3) . .
N2C K2 C5B C4B 31.3(7) . .
N2B K2 C5B C4B -140.1(7) . .
O1C K2 C5B C4B -44.0(6) . .
O1B K2 C5B C4B 142.0(6) . .
N1B K2 C5B C4B 102.2(7) . .
N1C K2 C5B C4B -77.5(7) . .
C13C K2 C5B C4B -69.3(6) . .
C6C K2 C5B C4B 46.0(8) . .
C6B K2 C5B C4B -122.0(8) . .
C5C K2 C5B C4B -68(3) . .
K1 K2 C5B C4B 161.5(7) . .
N2C K2 C5B C6B 153.3(3) . .
N2B K2 C5B C6B -18.1(3) . .
O1C K2 C5B C6B 77.9(3) . .
O1B K2 C5B C6B -96.1(3) . .
N1B K2 C5B C6B -135.9(5) . .
N1C K2 C5B C6B 44.5(5) . .
C13C K2 C5B C6B 52.6(3) . .
C6C K2 C5B C6B 168.0(4) . .
C5C K2 C5B C6B 54(3) . .
K1 K2 C5B C6B -76.5(3) . .
C9B N2B C6B C7B -1.5(6) . .
K2 N2B C6B C7B 139.7(4) . .
K1 N2B C6B C7B -126.9(4) . .
C9B N2B C6B C5B 179.6(4) . .
K2 N2B C6B C5B -39.3(5) . .
K1 N2B C6B C5B 54.1(5) . .
C9B N2B C6B K1 125.4(4) . .
K2 N2B C6B K1 -93.4(3) . .
C9B N2B C6B K2 -141.2(4) . .
K1 N2B C6B K2 93.4(3) . .
N1B C5B C6B N2B -11.3(7) . .
C4B C5B C6B N2B 166.8(5) . .
K2 C5B C6B N2B 29.5(4) . .
N1B C5B C6B C7B 170.1(6) . .
C4B C5B C6B C7B -11.8(9) . .
K2 C5B C6B C7B -149.1(6) . .
N1B C5B C6B K1 28.6(5) . .
C4B C5B C6B K1 -153.3(5) . .
K2 C5B C6B K1 69.42(10) . .
N1B C5B C6B K2 -40.8(4) . .
C4B C5B C6B K2 137.3(5) . .
N2A K1 C6B N2B 171.1(5) . .
O1B K1 C6B N2B 52.6(4) . .
O1A K1 C6B N2B -136.1(4) . .
N1B K1 C6B N2B 117.0(4) . .
N1A K1 C6B N2B -53.8(4) . .
C13B K1 C6B N2B 76.6(4) . .
C6A K1 C6B N2B 30(2) . .
K4 K1 C6B N2B -120.9(3) 1_545 .
K2 K1 C6B N2B 54.5(3) . .
N2A K1 C6B C7B -105.4(7) . .
N2B K1 C6B C7B 83.5(6) . .
O1B K1 C6B C7B 136.1(5) . .
O1A K1 C6B C7B -52.6(5) . .
N1B K1 C6B C7B -159.5(6) . .
N1A K1 C6B C7B 29.7(6) . .
C13B K1 C6B C7B 160.1(5) . .
C6A K1 C6B C7B 114(2) . .
K4 K1 C6B C7B -37.5(5) 1_545 .
K2 K1 C6B C7B 137.9(5) . .
N2A K1 C6B C5B 38.0(7) . .
N2B K1 C6B C5B -133.1(6) . .
O1B K1 C6B C5B -80.5(3) . .
O1A K1 C6B C5B 90.8(3) . .
N1B K1 C6B C5B -16.1(3) . .
N1A K1 C6B C5B 173.1(3) . .
C13B K1 C6B C5B -56.5(3) . .
C6A K1 C6B C5B -103(2) . .
K4 K1 C6B C5B 106.0(3) 1_545 .
K2 K1 C6B C5B -78.6(3) . .
N2A K1 C6B K2 116.6(5) . .
N2B K1 C6B K2 -54.5(3) . .
O1B K1 C6B K2 -1.83(12) . .
O1A K1 C6B K2 169.44(12) . .
N1B K1 C6B K2 62.52(18) . .
N1A K1 C6B K2 -108.28(18) . .
C13B K1 C6B K2 22.13(15) . .
C6A K1 C6B K2 -24(2) . .
K4 K1 C6B K2 -175.40(4) 1_545 .
N2C K2 C6B N2B 164.8(4) . .
O1C K2 C6B N2B 120.7(4) . .
O1B K2 C6B N2B -55.7(4) . .
N1B K2 C6B N2B -121.9(4) . .
N1C K2 C6B N2B 60.6(4) . .
C13C K2 C6B N2B 95.3(4) . .
C6C K2 C6B N2B 98.4(19) . .
C5B K2 C6B N2B -144.5(5) . .
C5C K2 C6B N2B 42.1(5) . .
K1 K2 C6B N2B -57.5(3) . .
N2C K2 C6B C7B 94.1(7) . .
N2B K2 C6B C7B -70.7(6) . .
O1C K2 C6B C7B 49.9(6) . .
O1B K2 C6B C7B -126.4(6) . .
N1B K2 C6B C7B 167.4(7) . .
N1C K2 C6B C7B -10.2(7) . .
C13C K2 C6B C7B 24.5(6) . .
C6C K2 C6B C7B 28(2) . .
C5B K2 C6B C7B 144.8(7) . .
C5C K2 C6B C7B -28.7(7) . .
K1 K2 C6B C7B -128.2(6) . .
N2C K2 C6B C5B -50.7(5) . .
N2B K2 C6B C5B 144.5(5) . .
O1C K2 C6B C5B -94.8(3) . .
O1B K2 C6B C5B 88.8(3) . .
N1B K2 C6B C5B 22.6(3) . .
N1C K2 C6B C5B -155.0(3) . .
C13C K2 C6B C5B -120.2(3) . .
C6C K2 C6B C5B -117.1(19) . .
C5C K2 C6B C5B -173.5(4) . .
K1 K2 C6B C5B 87.0(3) . .
N2C K2 C6B K1 -137.7(3) . .
N2B K2 C6B K1 57.5(3) . .
O1C K2 C6B K1 178.13(13) . .
O1B K2 C6B K1 1.81(12) . .
N1B K2 C6B K1 -64.41(18) . .
N1C K2 C6B K1 118.03(18) . .
C13C K2 C6B K1 152.75(16) . .
C6C K2 C6B K1 155.9(19) . .
C5B K2 C6B K1 -87.0(3) . .
C5C K2 C6B K1 99.5(3) . .
N2B C6B C7B C8B 2.2(6) . .
C5B C6B C7B C8B -179.2(6) . .
K1 C6B C7B C8B -53.7(6) . .
K2 C6B C7B C8B 51.6(7) . .
N2B C6B C7B C10B 176.3(6) . .
C5B C6B C7B C10B -5.0(10) . .
K1 C6B C7B C10B 120.4(6) . .
K2 C6B C7B C10B -134.3(6) . .
C6B C7B C8B C9B -1.9(6) . .
C10B C7B C8B C9B -176.7(5) . .
C6B N2B C9B C8B 0.3(6) . .
K2 N2B C9B C8B -130.0(5) . .
K1 N2B C9B C8B 117.7(4) . .
C6B N2B C9B C11B -179.1(5) . .
K2 N2B C9B C11B 50.5(7) . .
K1 N2B C9B C11B -61.7(6) . .
C7B C8B C9B N2B 1.0(6) . .
C7B C8B C9B C11B -179.6(5) . .
C8B C7B C10B F2B 124.9(6) . .
C6B C7B C10B F2B -48.7(9) . .
C8B C7B C10B F1B 4.6(8) . .
C6B C7B C10B F1B -169.0(6) . .
C8B C7B C10B F3B -114.7(6) . .
C6B C7B C10B F3B 71.8(8) . .
N2B C9B C11B F5B 179.4(5) . .
C8B C9B C11B F5B 0.1(8) . .
N2B C9B C11B F6B 58.9(7) . .
C8B C9B C11B F6B -120.5(6) . .
N2B C9B C11B F4B -59.6(7) . .
C8B C9B C11B F4B 121.0(6) . .
N2A K1 O1B C13B -50.9(3) . .
N2B K1 O1B C13B 131.6(3) . .
O1A K1 O1B C13B -15.5(7) . .
N1B K1 O1B C13B 75.2(3) . .
N1A K1 O1B C13B -106.6(3) . .
C6B K1 O1B C13B 113.9(3) . .
C6A K1 O1B C13B -68.0(3) . .
K4 K1 O1B C13B -72.4(3) 1_545 .
K2 K1 O1B C13B 111.8(3) . .
N2A K1 O1B C14B 74.7(4) . .
N2B K1 O1B C14B -102.9(4) . .
O1A K1 O1B C14B 110.0(6) . .
N1B K1 O1B C14B -159.3(4) . .
N1A K1 O1B C14B 19.0(4) . .
C13B K1 O1B C14B 125.5(5) . .
C6B K1 O1B C14B -120.6(4) . .
C6A K1 O1B C14B 57.6(3) . .
K4 K1 O1B C14B 53.1(4) 1_545 .
K2 K1 O1B C14B -122.6(4) . .
N2A K1 O1B K2 -162.70(12) . .
N2B K1 O1B K2 19.78(12) . .
O1A K1 O1B K2 -127.3(6) . .
N1B K1 O1B K2 -36.63(12) . .
N1A K1 O1B K2 141.61(11) . .
C13B K1 O1B K2 -111.8(3) . .
C6B K1 O1B K2 2.08(13) . .
C6A K1 O1B K2 -179.81(13) . .
K4 K1 O1B K2 175.74(4) 1_545 .
N2C K2 O1B C13B 63.0(3) . .
N2B K2 O1B C13B -119.9(3) . .
O1C K2 O1B C13B -131.4(10) . .
N1B K2 O1B C13B -63.0(3) . .
N1C K2 O1B C13B 119.3(3) . .
C13C K2 O1B C13B -160.9(4) . .
C6C K2 O1B C13B 80.2(3) . .
C5B K2 O1B C13B -77.1(4) . .
C6B K2 O1B C13B -102.1(3) . .
C5C K2 O1B C13B 104.7(3) . .
K1 K2 O1B C13B -100.0(3) . .
N2C K2 O1B C14B -66.5(3) . .
N2B K2 O1B C14B 110.6(3) . .
O1C K2 O1B C14B 99.1(11) . .
N1B K2 O1B C14B 167.5(3) . .
N1C K2 O1B C14B -10.2(3) . .
C13C K2 O1B C14B 69.6(4) . .
C6C K2 O1B C14B -49.3(3) . .
C5B K2 O1B C14B 153.4(3) . .
C6B K2 O1B C14B 128.4(3) . .
C5C K2 O1B C14B -24.8(3) . .
K1 K2 O1B C14B 130.5(3) . .
N2C K2 O1B K1 162.98(12) . .
N2B K2 O1B K1 -19.90(13) . .
O1C K2 O1B K1 -31.4(11) . .
N1B K2 O1B K1 37.00(12) . .
N1C K2 O1B K1 -140.66(12) . .
C13C K2 O1B K1 -60.9(3) . .
C6C K2 O1B K1 -179.77(12) . .
C5B K2 O1B K1 22.92(14) . .
C6B K2 O1B K1 -2.05(13) . .
C5C K2 O1B K1 -155.27(13) . .
C14B O1B C13B C12B 70.0(6) . .
K1 O1B C13B C12B -153.8(5) . .
K2 O1B C13B C12B -63.4(6) . .
C14B O1B C13B K1 -136.2(4) . .
K2 O1B C13B K1 90.4(2) . .
N2A K1 C13B O1B 124.9(3) . .
N2B K1 C13B O1B -50.8(3) . .
O1A K1 C13B O1B 174.8(2) . .
N1B K1 C13B O1B -100.6(3) . .
N1A K1 C13B O1B 75.2(3) . .
C6B K1 C13B O1B -73.4(3) . .
C6A K1 C13B O1B 102.8(3) . .
K4 K1 C13B O1B 121.9(3) 1_545 .
K2 K1 C13B O1B -52.0(3) . .
N2A K1 C13B C12B -161.6(10) . .
N2B K1 C13B C12B 22.7(10) . .
O1B K1 C13B C12B 73.5(10) . .
O1A K1 C13B C12B -111.7(10) . .
N1B K1 C13B C12B -27.1(10) . .
N1A K1 C13B C12B 148.7(10) . .
C6B K1 C13B C12B 0.1(10) . .
C6A K1 C13B C12B 176.3(10) . .
K4 K1 C13B C12B -164.6(9) 1_545 .
K2 K1 C13B C12B 21.5(9) . .
C13B O1B C14B C15B 171.6(4) . .
K1 O1B C14B C15B 50.0(5) . .
K2 O1B C14B C15B -58.0(5) . .
N2C K2 K3 O1D 36.19(19) . .
N2B K2 K3 O1D -142.60(19) . .
O1C K2 K3 O1D -168.21(17) . .
O1B K2 K3 O1D 6.16(18) . .
N1B K2 K3 O1D 141.6(2) . .
N1C K2 K3 O1D -43.1(2) . .
C13C K2 K3 O1D -141.50(19) . .
C6C K2 K3 O1D 10.95(18) . .
C5B K2 K3 O1D 165.03(18) . .
C6B K2 K3 O1D -166.79(17) . .
C5C K2 K3 O1D -17.91(18) . .
K1 K2 K3 O1D -142.0(3) . .
N2C K2 K3 N2D -179.5(3) . .
N2B K2 K3 N2D 1.71(16) . .
O1C K2 K3 N2D -23.90(19) . .
O1B K2 K3 N2D 150.47(19) . .
N1B K2 K3 N2D -74.1(2) . .
N1C K2 K3 N2D 101.2(2) . .
C13C K2 K3 N2D 2.8(2) . .
C6C K2 K3 N2D 155.3(2) . .
C5B K2 K3 N2D -50.7(2) . .
C6B K2 K3 N2D -22.5(2) . .
C5C K2 K3 N2D 126.4(2) . .
K1 K2 K3 N2D 2.3(4) . .
N2B K2 K3 N2C -178.8(3) . .
O1C K2 K3 N2C 155.59(18) . .
O1B K2 K3 N2C -30.03(18) . .
N1B K2 K3 N2C 105.4(2) . .
N1C K2 K3 N2C -79.3(2) . .
C13C K2 K3 N2C -177.7(2) . .
C6C K2 K3 N2C -25.24(18) . .
C5B K2 K3 N2C 128.8(2) . .
C6B K2 K3 N2C 157.01(19) . .
C5C K2 K3 N2C -54.11(19) . .
K1 K2 K3 N2C -178.2(4) . .
N2C K2 K3 O1C -155.59(18) . .
N2B K2 K3 O1C 25.61(17) . .
O1B K2 K3 O1C 174.37(19) . .
N1B K2 K3 O1C -50.23(18) . .
N1C K2 K3 O1C 125.14(17) . .
C13C K2 K3 O1C 26.71(15) . .
C6C K2 K3 O1C 179.17(16) . .
C5B K2 K3 O1C -26.76(16) . .
C6B K2 K3 O1C 1.42(15) . .
C5C K2 K3 O1C 150.30(17) . .
K1 K2 K3 O1C 26.2(3) . .
N2C K2 K3 N1C 79.3(2) . .
N2B K2 K3 N1C -99.5(2) . .
O1C K2 K3 N1C -125.14(17) . .
O1B K2 K3 N1C 49.24(18) . .
N1B K2 K3 N1C -175.4(3) . .
C13C K2 K3 N1C -98.43(19) . .
C6C K2 K3 N1C 54.03(19) . .
C5B K2 K3 N1C -151.9(2) . .
C6B K2 K3 N1C -123.72(18) . .
C5C K2 K3 N1C 25.16(19) . .
K1 K2 K3 N1C -99.0(3) . .
N2C K2 K3 N1D -97.9(2) . .
N2B K2 K3 N1D 83.3(2) . .
O1C K2 K3 N1D 57.66(18) . .
O1B K2 K3 N1D -127.97(19) . .
N1B K2 K3 N1D 7.43(16) . .
N1C K2 K3 N1D -177.2(3) . .
C13C K2 K3 N1D 84.37(19) . .
C6C K2 K3 N1D -123.17(19) . .
C5B K2 K3 N1D 30.9(2) . .
C6B K2 K3 N1D 59.08(19) . .
C5C K2 K3 N1D -152.0(2) . .
K1 K2 K3 N1D 83.8(3) . .
N2C K2 K3 C6C 25.24(18) . .
N2B K2 K3 C6C -153.56(19) . .
O1C K2 K3 C6C -179.17(16) . .
O1B K2 K3 C6C -4.79(16) . .
N1B K2 K3 C6C 130.6(2) . .
N1C K2 K3 C6C -54.03(19) . .
C13C K2 K3 C6C -152.46(18) . .
C5B K2 K3 C6C 154.08(18) . .
C6B K2 K3 C6C -177.7(2) . .
C5C K2 K3 C6C -28.87(17) . .
K1 K2 K3 C6C -153.0(3) . .
N2C K2 K3 C6D -153.5(2) . .
N2B K2 K3 C6D 27.73(18) . .
O1C K2 K3 C6D 2.12(16) . .
O1B K2 K3 C6D 176.49(17) . .
N1B K2 K3 C6D -48.1(2) . .
N1C K2 K3 C6D 127.26(19) . .
C13C K2 K3 C6D 28.83(17) . .
C6C K2 K3 C6D -178.7(2) . .
C5B K2 K3 C6D -24.64(18) . .
C6B K2 K3 C6D 3.54(13) . .
C5C K2 K3 C6D 152.42(19) . .
K1 K2 K3 C6D 28.3(4) . .
N2C K2 K3 C5D -123.9(2) . .
N2B K2 K3 C5D 57.29(19) . .
O1C K2 K3 C5D 31.68(16) . .
O1B K2 K3 C5D -153.95(18) . .
N1B K2 K3 C5D -18.5(2) . .
N1C K2 K3 C5D 156.8(2) . .
C13C K2 K3 C5D 58.38(18) . .
C6C K2 K3 C5D -149.16(18) . .
C5B K2 K3 C5D 4.92(14) . .
C6B K2 K3 C5D 33.09(18) . .
C5C K2 K3 C5D -178.0(2) . .
K1 K2 K3 C5D 57.8(3) . .
N2C K2 K3 C14D 61.4(2) . .
N2B K2 K3 C14D -117.4(2) . .
O1C K2 K3 C14D -142.99(17) . .
O1B K2 K3 C14D 31.38(18) . .
N1B K2 K3 C14D 166.8(2) . .
N1C K2 K3 C14D -17.9(2) . .
C13C K2 K3 C14D -116.28(19) . .
C6C K2 K3 C14D 36.17(18) . .
C5B K2 K3 C14D -169.75(19) . .
C6B K2 K3 C14D -141.57(18) . .
C5C K2 K3 C14D 7.31(19) . .
K1 K2 K3 C14D -116.8(3) . .
N2C K2 K3 K4 -27.3(4) . .
N2B K2 K3 K4 153.9(3) . .
O1C K2 K3 K4 128.3(3) . .
O1B K2 K3 K4 -57.4(4) . .
N1B K2 K3 K4 78.0(4) . .
N1C K2 K3 K4 -106.6(4) . .
C13C K2 K3 K4 155.0(4) . .
C6C K2 K3 K4 -52.6(4) . .
C5B K2 K3 K4 101.5(4) . .
C6B K2 K3 K4 129.7(3) . .
C5C K2 K3 K4 -81.4(4) . .
K1 K2 K3 K4 154.4(3) . .
O1D K3 N1C C1C -94.6(5) . .
N2D K3 N1C C1C -9.8(6) . .
N2C K3 N1C C1C 175.3(5) . .
O1C K3 N1C C1C 80.6(5) . .
N1D K3 N1C C1C 171(3) . .
C6C K3 N1C C1C -162.2(6) . .
C6D K3 N1C C1C 15.4(6) . .
C5D K3 N1C C1C 43.6(7) . .
C14D K3 N1C C1C -80.1(5) . .
K4 K3 N1C C1C -68.6(5) . .
K2 K3 N1C C1C 117.4(5) . .
O1D K3 N1C C5C 48.7(4) . .
N2D K3 N1C C5C 133.5(4) . .
N2C K3 N1C C5C -41.5(4) . .
O1C K3 N1C C5C -136.1(4) . .
N1D K3 N1C C5C -46(4) . .
C6C K3 N1C C5C -19.0(3) . .
C6D K3 N1C C5C 158.7(3) . .
C5D K3 N1C C5C -173.1(4) . .
C14D K3 N1C C5C 63.2(4) . .
K4 K3 N1C C5C 74.7(4) . .
K2 K3 N1C C5C -99.3(4) . .
O1D K3 N1C K2 147.99(14) . .
N2D K3 N1C K2 -127.20(15) . .
N2C K3 N1C K2 57.86(14) . .
O1C K3 N1C K2 -36.79(11) . .
N1D K3 N1C K2 54(4) . .
C6C K3 N1C K2 80.36(19) . .
C6D K3 N1C K2 -102.0(2) . .
C5D K3 N1C K2 -73.8(4) . .
C14D K3 N1C K2 162.54(19) . .
K4 K3 N1C K2 173.99(4) . .
N2C K2 N1C C1C 178.7(5) . .
N2B K2 N1C C1C -6.9(5) . .
O1C K2 N1C C1C -85.1(5) . .
O1B K2 N1C C1C 88.1(5) . .
N1B K2 N1C C1C -55(2) . .
C13C K2 N1C C1C -60.8(5) . .
C6C K2 N1C C1C 155.7(6) . .
C5B K2 N1C C1C -52.6(6) . .
C6B K2 N1C C1C -29.0(6) . .
C5C K2 N1C C1C 129.0(7) . .
K1 K2 N1C C1C 49.6(5) . .
N2C K2 N1C C5C 49.6(3) . .
N2B K2 N1C C5C -136.0(3) . .
O1C K2 N1C C5C 145.8(4) . .
O1B K2 N1C C5C -41.0(4) . .
N1B K2 N1C C5C 176(2) . .
C13C K2 N1C C5C 170.2(4) . .
C6C K2 N1C C5C 26.7(3) . .
C5B K2 N1C C5C 178.4(4) . .
C6B K2 N1C C5C -158.0(3) . .
K1 K2 N1C C5C -79.5(4) . .
N2C K2 N1C K3 -58.68(14) . .
N2B K2 N1C K3 115.71(15) . .
O1C K2 N1C K3 37.50(11) . .
O1B K2 N1C K3 -149.30(11) . .
N1B K2 N1C K3 68(2) . .
C13C K2 N1C K3 61.87(14) . .
C6C K2 N1C K3 -81.61(18) . .
C5B K2 N1C K3 70.1(3) . .
C6B K2 N1C K3 93.70(18) . .
C5C K2 N1C K3 -108.3(4) . .
K1 K2 N1C K3 172.21(4) . .
N2B K2 N2C C6C -98.8(19) . .
O1C K2 N2C C6C -125.7(4) . .
O1B K2 N2C C6C 52.6(4) . .
N1B K2 N2C C6C 138.5(3) . .
N1C K2 N2C C6C -45.3(3) . .
C13C K2 N2C C6C -105.8(4) . .
C5B K2 N2C C6C 164.8(3) . .
C6B K2 N2C C6C -167.1(4) . .
C5C K2 N2C C6C -20.4(3) . .
K1 K2 N2C C6C 71.8(4) . .
N2B K2 N2C C9C 135.3(17) . .
O1C K2 N2C C9C 108.5(5) . .
O1B K2 N2C C9C -73.3(5) . .
N1B K2 N2C C9C 12.7(5) . .
N1C K2 N2C C9C -171.1(5) . .
C13C K2 N2C C9C 128.3(5) . .
C6C K2 N2C C9C -125.8(6) . .
C5B K2 N2C C9C 38.9(5) . .
C6B K2 N2C C9C 67.1(6) . .
C5C K2 N2C C9C -146.2(5) . .
K1 K2 N2C C9C -54.0(5) . .
N2B K2 N2C K3 9(2) . .
O1C K2 N2C K3 -17.76(13) . .
O1B K2 N2C K3 160.47(11) . .
N1B K2 N2C K3 -113.58(18) . .
N1C K2 N2C K3 62.60(16) . .
C13C K2 N2C K3 2.07(18) . .
C6C K2 N2C K3 107.9(4) . .
C5B K2 N2C K3 -87.3(2) . .
C6B K2 N2C K3 -59.2(4) . .
C5C K2 N2C K3 87.5(2) . .
K1 K2 N2C K3 179.72(5) . .
O1D K3 N2C C6C -44.8(4) . .
N2D K3 N2C C6C -76(2) . .
O1C K3 N2C C6C 125.4(4) . .
N1C K3 N2C C6C 44.5(3) . .
N1D K3 N2C C6C -135.7(3) . .
C6D K3 N2C C6C -173.5(4) . .
C5D K3 N2C C6C -157.1(3) . .
C14D K3 N2C C6C -19.2(4) . .
K4 K3 N2C C6C -74.8(4) . .
K2 K3 N2C C6C 108.0(4) . .
O1D K3 N2C C9C 75.0(4) . .
N2D K3 N2C C9C 44(2) . .
O1C K3 N2C C9C -114.8(4) . .
N1C K3 N2C C9C 164.3(5) . .
N1D K3 N2C C9C -16.0(5) . .
C6C K3 N2C C9C 119.8(6) . .
C6D K3 N2C C9C -53.7(6) . .
C5D K3 N2C C9C -37.3(5) . .
C14D K3 N2C C9C 100.5(4) . .
K4 K3 N2C C9C 44.9(5) . .
K2 K3 N2C C9C -132.3(5) . .
O1D K3 N2C K2 -152.72(14) . .
N2D K3 N2C K2 176(2) . .
O1C K3 N2C K2 17.44(13) . .
N1C K3 N2C K2 -63.47(15) . .
N1D K3 N2C K2 116.30(16) . .
C6C K3 N2C K2 -108.0(4) . .
C6D K3 N2C K2 78.6(4) . .
C5D K3 N2C K2 94.9(2) . .
C14D K3 N2C K2 -127.20(16) . .
K4 K3 N2C K2 177.21(4) . .
C5C N1C C1C C2C 1.8(9) . .
K3 N1C C1C C2C 142.3(6) . .
K2 N1C C1C C2C -119.0(6) . .
N1C C1C C2C C3C -2.0(11) . .
C1C C2C C3C C4C 1.9(11) . .
C2C C3C C4C C5C -1.8(11) . .
C1C N1C C5C C4C -1.5(8) . .
K3 N1C C5C C4C -146.8(5) . .
K2 N1C C5C C4C 127.2(5) . .
C1C N1C C5C C6C 179.8(5) . .
K3 N1C C5C C6C 34.5(5) . .
K2 N1C C5C C6C -51.4(5) . .
C1C N1C C5C K2 -128.7(5) . .
K3 N1C C5C K2 86.0(2) . .
C3C C4C C5C N1C 1.6(10) . .
C3C C4C C5C C6C -179.9(6) . .
C3C C4C C5C K2 72.2(9) . .
N2C K2 C5C N1C -114.0(4) . .
N2B K2 C5C N1C 57.6(4) . .
O1C K2 C5C N1C -34.6(4) . .
O1B K2 C5C N1C 139.4(4) . .
N1B K2 C5C N1C -179.2(4) . .
C13C K2 C5C N1C -9.6(4) . .
C6C K2 C5C N1C -132.4(5) . .
C5B K2 C5C N1C -11(3) . .
C6B K2 C5C N1C 37.1(5) . .
K1 K2 C5C N1C 117.7(3) . .
N2C K2 C5C C4C 146.2(7) . .
N2B K2 C5C C4C -42.1(7) . .
O1C K2 C5C C4C -134.4(6) . .
O1B K2 C5C C4C 39.6(6) . .
N1B K2 C5C C4C 81.0(8) . .
N1C K2 C5C C4C -99.8(8) . .
C13C K2 C5C C4C -109.4(6) . .
C6C K2 C5C C4C 127.9(8) . .
C5B K2 C5C C4C -111(3) . .
C6B K2 C5C C4C -62.6(7) . .
K1 K2 C5C C4C 17.9(7) . .
N2C K2 C5C C6C 18.3(3) . .
N2B K2 C5C C6C -170.0(3) . .
O1C K2 C5C C6C 97.8(3) . .
O1B K2 C5C C6C -88.3(3) . .
N1B K2 C5C C6C -46.9(6) . .
N1C K2 C5C C6C 132.4(5) . .
C13C K2 C5C C6C 122.7(3) . .
C5B K2 C5C C6C 121(3) . .
C6B K2 C5C C6C 169.5(3) . .
K1 K2 C5C C6C -110.0(3) . .
C9C N2C C6C C7C 1.2(5) . .
K2 N2C C6C C7C -136.6(4) . .
K3 N2C C6C C7C 129.5(4) . .
C9C N2C C6C C5C 179.9(5) . .
K2 N2C C6C C5C 42.2(5) . .
K3 N2C C6C C5C -51.8(5) . .
C9C N2C C6C K2 137.7(4) . .
K3 N2C C6C K2 -94.0(3) . .
C9C N2C C6C K3 -128.3(4) . .
K2 N2C C6C K3 94.0(3) . .
N1C C5C C6C N2C 10.5(7) . .
C4C C5C C6C N2C -168.1(5) . .
K2 C5C C6C N2C -31.8(4) . .
N1C C5C C6C C7C -171.0(5) . .
C4C C5C C6C C7C 10.4(9) . .
K2 C5C C6C C7C 146.7(5) . .
N1C C5C C6C K2 42.3(4) . .
C4C C5C C6C K2 -136.3(6) . .
N1C C5C C6C K3 -27.2(4) . .
C4C C5C C6C K3 154.2(6) . .
K2 C5C C6C K3 -69.49(11) . .
N2B K2 C6C N2C 163.7(4) . .
O1C K2 C6C N2C 56.6(4) . .
O1B K2 C6C N2C -127.3(4) . .
N1B K2 C6C N2C -57.4(4) . .
N1C K2 C6C N2C 119.5(4) . .
C13C K2 C6C N2C 81.3(4) . .
C5B K2 C6C N2C -27.8(6) . .
C6B K2 C6C N2C 78(2) . .
C5C K2 C6C N2C 144.1(5) . .
K1 K2 C6C N2C -127.5(3) . .
N2C K2 C6C C7C 76.1(6) . .
N2B K2 C6C C7C -120.3(6) . .
O1C K2 C6C C7C 132.6(6) . .
O1B K2 C6C C7C -51.2(6) . .
N1B K2 C6C C7C 18.6(7) . .
N1C K2 C6C C7C -164.4(7) . .
C13C K2 C6C C7C 157.4(5) . .
C5B K2 C6C C7C 48.3(8) . .
C6B K2 C6C C7C 154.3(17) . .
C5C K2 C6C C7C -139.8(7) . .
K1 K2 C6C C7C -51.4(6) . .
N2C K2 C6C C5C -144.1(5) . .
N2B K2 C6C C5C 19.5(5) . .
O1C K2 C6C C5C -87.6(3) . .
O1B K2 C6C C5C 88.6(3) . .
N1B K2 C6C C5C 158.4(3) . .
N1C K2 C6C C5C -24.6(3) . .
C13C K2 C6C C5C -62.8(3) . .
C5B K2 C6C C5C -171.9(4) . .
C6B K2 C6C C5C -66(2) . .
K1 K2 C6C C5C 88.4(3) . .
N2C K2 C6C K3 -55.9(3) . .
N2B K2 C6C K3 107.7(3) . .
O1C K2 C6C K3 0.63(12) . .
O1B K2 C6C K3 176.79(11) . .
N1B K2 C6C K3 -113.4(2) . .
N1C K2 C6C K3 63.54(18) . .
C13C K2 C6C K3 25.35(15) . .
C5B K2 C6C K3 -83.7(4) . .
C6B K2 C6C K3 22(2) . .
C5C K2 C6C K3 88.2(3) . .
K1 K2 C6C K3 176.58(4) . .
O1D K3 C6C N2C 133.1(4) . .
N2D K3 C6C N2C 168.3(4) . .
O1C K3 C6C N2C -56.4(4) . .
N1C K3 C6C N2C -120.6(4) . .
N1D K3 C6C N2C 57.7(4) . .
C6D K3 C6C N2C 99(4) . .
C5D K3 C6C N2C 39.1(5) . .
C14D K3 C6C N2C 159.3(4) . .
K4 K3 C6C N2C 119.9(3) . .
K2 K3 C6C N2C -55.7(3) . .
O1D K3 C6C C7C 51.2(5) . .
N2D K3 C6C C7C 86.5(7) . .
N2C K3 C6C C7C -81.8(6) . .
O1C K3 C6C C7C -138.2(5) . .
N1C K3 C6C C7C 157.6(6) . .
N1D K3 C6C C7C -24.1(6) . .
C6D K3 C6C C7C 17(4) . .
C5D K3 C6C C7C -42.7(7) . .
C14D K3 C6C C7C 77.5(5) . .
K4 K3 C6C C7C 38.1(5) . .
K2 K3 C6C C7C -137.6(6) . .
O1D K3 C6C C5C -89.7(3) . .
N2D K3 C6C C5C -54.5(6) . .
N2C K3 C6C C5C 137.2(5) . .
O1C K3 C6C C5C 80.9(3) . .
N1C K3 C6C C5C 16.7(3) . .
N1D K3 C6C C5C -165.1(3) . .
C6D K3 C6C C5C -124(4) . .
C5D K3 C6C C5C 176.3(3) . .
C14D K3 C6C C5C -63.4(3) . .
K4 K3 C6C C5C -102.8(3) . .
K2 K3 C6C C5C 81.5(3) . .
O1D K3 C6C K2 -171.20(14) . .
N2D K3 C6C K2 -136.0(3) . .
N2C K3 C6C K2 55.7(3) . .
O1C K3 C6C K2 -0.62(12) . .
N1C K3 C6C K2 -64.84(17) . .
N1D K3 C6C K2 113.44(18) . .
C6D K3 C6C K2 155(4) . .
C5D K3 C6C K2 94.8(3) . .
C14D K3 C6C K2 -144.95(17) . .
K4 K3 C6C K2 175.66(3) . .
N2C C6C C7C C8C -2.3(6) . .
C5C C6C C7C C8C 179.1(5) . .
K2 C6C C7C C8C -55.6(7) . .
K3 C6C C7C C8C 52.7(6) . .
N2C C6C C7C C10C 178.3(6) . .
C5C C6C C7C C10C -0.2(9) . .
K2 C6C C7C C10C 125.1(6) . .
K3 C6C C7C C10C -126.6(6) . .
C6C C7C C8C C9C 2.5(6) . .
C10C C7C C8C C9C -178.1(5) . .
C6C N2C C9C C8C 0.5(6) . .
K2 N2C C9C C8C 127.3(5) . .
K3 N2C C9C C8C -120.4(4) . .
C6C N2C C9C C11C -178.8(5) . .
K2 N2C C9C C11C -52.0(7) . .
K3 N2C C9C C11C 60.4(6) . .
C7C C8C C9C N2C -2.0(6) . .
C7C C8C C9C C11C 177.2(6) . .
C8C C7C C10C F2C -2.5(9) . .
C6C C7C C10C F2C 176.7(6) . .
C8C C7C C10C F1C -123.1(7) . .
C6C C7C C10C F1C 56.1(9) . .
C8C C7C C10C F3C 116.0(7) . .
C6C C7C C10C F3C -64.8(9) . .
N2C C9C C11C F4C 177.1(5) . .
C8C C9C C11C F4C -2.0(9) . .
N2C C9C C11C F6C 55.9(7) . .
C8C C9C C11C F6C -123.3(6) . .
N2C C9C C11C F5C -62.0(7) . .
C8C C9C C11C F5C 118.8(7) . .
N2C K2 O1C C14C -102.5(4) . .
N2B K2 O1C C14C 80.2(4) . .
O1B K2 O1C C14C 91.8(11) . .
N1B K2 O1C C14C 24.0(4) . .
N1C K2 O1C C14C -157.9(4) . .
C13C K2 O1C C14C 128.7(5) . .
C6C K2 O1C C14C -120.5(3) . .
C5B K2 O1C C14C 36.2(3) . .
C6B K2 O1C C14C 61.5(3) . .
C5C K2 O1C C14C -145.3(3) . .
K1 K2 O1C C14C 63.4(4) . .
N2C K2 O1C C13C 128.8(3) . .
N2B K2 O1C C13C -48.5(3) . .
O1B K2 O1C C13C -36.9(12) . .
N1B K2 O1C C13C -104.7(3) . .
N1C K2 O1C C13C 73.4(3) . .
C6C K2 O1C C13C 110.8(3) . .
C5B K2 O1C C13C -92.5(3) . .
C6B K2 O1C C13C -67.2(3) . .
C5C K2 O1C C13C 86.0(3) . .
K1 K2 O1C C13C -65.3(3) . .
N2C K2 O1C K3 17.31(13) . .
N2B K2 O1C K3 -159.97(13) . .
O1B K2 O1C K3 -148.4(10) . .
N1B K2 O1C K3 143.84(12) . .
N1C K2 O1C K3 -38.10(11) . .
C13C K2 O1C K3 -111.5(3) . .
C6C K2 O1C K3 -0.71(14) . .
C5B K2 O1C K3 156.00(13) . .
C6B K2 O1C K3 -178.70(13) . .
C5C K2 O1C K3 -25.48(14) . .
K1 K2 O1C K3 -176.78(4) . .
O1D K3 O1C C14C -165.4(7) . .
N2D K3 O1C C14C -68.5(3) . .
N2C K3 O1C C14C 109.8(3) . .
N1C K3 O1C C14C 165.5(3) . .
N1D K3 O1C C14C -11.8(3) . .
C6C K3 O1C C14C 127.7(3) . .
C6D K3 O1C C14C -51.3(3) . .
C5D K3 O1C C14C -26.6(3) . .
C14D K3 O1C C14C -162.5(3) . .
K4 K3 O1C C14C -47.7(4) . .
K2 K3 O1C C14C 127.0(4) . .
O1D K3 O1C C13C -31.2(9) . .
N2D K3 O1C C13C 65.8(3) . .
N2C K3 O1C C13C -116.0(3) . .
N1C K3 O1C C13C -60.3(3) . .
N1D K3 O1C C13C 122.5(3) . .
C6C K3 O1C C13C -98.1(3) . .
C6D K3 O1C C13C 82.9(3) . .
C5D K3 O1C C13C 107.7(3) . .
C14D K3 O1C C13C -28.3(5) . .
K4 K3 O1C C13C 86.5(3) . .
K2 K3 O1C C13C -98.8(3) . .
O1D K3 O1C K2 67.6(8) . .
N2D K3 O1C K2 164.57(12) . .
N2C K3 O1C K2 -17.17(12) . .
N1C K3 O1C K2 38.54(12) . .
N1D K3 O1C K2 -138.75(12) . .
C6C K3 O1C K2 0.70(14) . .
C6D K3 O1C K2 -178.28(13) . .
C5D K3 O1C K2 -153.55(13) . .
C14D K3 O1C K2 70.5(3) . .
K4 K3 O1C K2 -174.73(4) . .
C14C O1C C13C C12C 73.0(7) . .
K2 O1C C13C C12C -151.8(5) . .
K3 O1C C13C C12C -62.3(6) . .
C14C O1C C13C K2 -135.2(4) . .
K3 O1C C13C K2 89.5(2) . .
N2C K2 C13C C12C 18.3(10) . .
N2B K2 C13C C12C -160.9(10) . .
O1C K2 C13C C12C 72.5(10) . .
O1B K2 C13C C12C -115.9(9) . .
N1B K2 C13C C12C 150.8(10) . .
N1C K2 C13C C12C -29.6(10) . .
C6C K2 C13C C12C -4.1(10) . .
C5B K2 C13C C12C 154.1(10) . .
C6B K2 C13C C12C 175.6(10) . .
C5C K2 C13C C12C -25.8(10) . .
K1 K2 C13C C12C -160.0(9) . .
N2C K2 C13C O1C -54.2(3) . .
N2B K2 C13C O1C 126.6(3) . .
O1B K2 C13C O1C 171.6(3) . .
N1B K2 C13C O1C 78.3(3) . .
N1C K2 C13C O1C -102.1(3) . .
C6C K2 C13C O1C -76.6(3) . .
C5B K2 C13C O1C 81.6(3) . .
C6B K2 C13C O1C 103.1(3) . .
C5C K2 C13C O1C -98.3(3) . .
K1 K2 C13C O1C 127.5(3) . .
C13C O1C C14C C15C 170.9(4) . .
K2 O1C C14C C15C 48.5(5) . .
K3 O1C C14C C15C -56.0(4) . .
O1D K3 K4 N2D 138.5(2) . .
N2C K3 K4 N2D -179.9(2) . .
O1C K3 K4 N2D -29.86(18) . .
N1C K3 K4 N2D 103.0(2) . .
N1D K3 K4 N2D -80.1(2) . .
C6C K3 K4 N2D 155.40(19) . .
C6D K3 K4 N2D -25.64(18) . .
C5D K3 K4 N2D -54.88(19) . .
C14D K3 K4 N2D 114.7(2) . .
K2 K3 K4 N2D -154.4(4) . .
O1D K3 K4 N2A -43.7(2) . 1_565
N2D K3 K4 N2A 177.8(3) . 1_565
N2C K3 K4 N2A -2.08(15) . 1_565
O1C K3 K4 N2A 147.91(18) . 1_565
N1C K3 K4 N2A -79.2(2) . 1_565
N1D K3 K4 N2A 97.7(2) . 1_565
C6C K3 K4 N2A -26.82(19) . 1_565
C6D K3 K4 N2A 152.1(2) . 1_565
C5D K3 K4 N2A 122.9(2) . 1_565
C14D K3 K4 N2A -67.5(2) . 1_565
K2 K3 K4 N2A 23.4(4) . 1_565
O1D K3 K4 O1A -175.9(2) . 1_565
N2D K3 K4 O1A 45.56(19) . 1_565
N2C K3 K4 O1A -134.29(18) . 1_565
O1C K3 K4 O1A 15.70(17) . 1_565
N1C K3 K4 O1A 148.55(18) . 1_565
N1D K3 K4 O1A -34.51(19) . 1_565
C6C K3 K4 O1A -159.04(17) . 1_565
C6D K3 K4 O1A 19.93(17) . 1_565
C5D K3 K4 O1A -9.32(17) . 1_565
C14D K3 K4 O1A 160.25(19) . 1_565
K2 K3 K4 O1A -108.9(3) . 1_565
O1D K3 K4 N1A 39.3(2) . 1_565
N2D K3 K4 N1A -99.2(2) . 1_565
N2C K3 K4 N1A 80.94(19) . 1_565
O1C K3 K4 N1A -129.07(18) . 1_565
N1C K3 K4 N1A 3.78(14) . 1_565
N1D K3 K4 N1A -179.3(3) . 1_565
C6C K3 K4 N1A 56.20(19) . 1_565
C6D K3 K4 N1A -124.84(18) . 1_565
C5D K3 K4 N1A -154.08(19) . 1_565
C14D K3 K4 N1A 15.5(2) . 1_565
K2 K3 K4 N1A 106.4(4) . 1_565
N2D K3 K4 O1D -138.5(2) . .
N2C K3 K4 O1D 41.63(19) . .
O1C K3 K4 O1D -168.38(17) . .
N1C K3 K4 O1D -35.5(2) . .
N1D K3 K4 O1D 141.4(2) . .
C6C K3 K4 O1D 16.88(18) . .
C6D K3 K4 O1D -164.15(18) . .
C5D K3 K4 O1D 166.60(19) . .
C14D K3 K4 O1D -23.83(18) . .
K2 K3 K4 O1D 67.1(4) . .
O1D K3 K4 N1D -141.4(2) . .
N2D K3 K4 N1D 80.1(2) . .
N2C K3 K4 N1D -99.8(2) . .
O1C K3 K4 N1D 50.21(18) . .
N1C K3 K4 N1D -176.9(3) . .
C6C K3 K4 N1D -124.52(19) . .
C6D K3 K4 N1D 54.44(19) . .
C5D K3 K4 N1D 25.20(19) . .
C14D K3 K4 N1D -165.2(2) . .
K2 K3 K4 N1D -74.3(4) . .
O1D K3 K4 F4D 84.66(15) . .
N2D K3 K4 F4D -53.85(16) . .
N2C K3 K4 F4D 126.29(16) . .
O1C K3 K4 F4D -83.72(13) . .
N1C K3 K4 F4D 49.13(16) . .
N1D K3 K4 F4D -133.93(17) . .
C6C K3 K4 F4D 101.55(14) . .
C6D K3 K4 F4D -79.49(14) . .
C5D K3 K4 F4D -108.73(15) . .
C14D K3 K4 F4D 60.84(15) . .
K2 K3 K4 F4D 151.7(3) . .
O1D K3 K4 C6A -17.05(18) . 1_565
N2D K3 K4 C6A -155.6(2) . 1_565
N2C K3 K4 C6A 24.57(18) . 1_565
O1C K3 K4 C6A 174.57(17) . 1_565
N1C K3 K4 C6A -52.6(2) . 1_565
N1D K3 K4 C6A 124.35(19) . 1_565
C6C K3 K4 C6A -0.17(12) . 1_565
C6D K3 K4 C6A 178.8(2) . 1_565
C5D K3 K4 C6A 149.55(18) . 1_565
C14D K3 K4 C6A -40.88(19) . 1_565
K2 K3 K4 C6A 50.0(4) . 1_565
O1D K3 K4 C6D 164.15(18) . .
N2D K3 K4 C6D 25.64(18) . .
N2C K3 K4 C6D -154.22(19) . .
O1C K3 K4 C6D -4.23(16) . .
N1C K3 K4 C6D 128.62(19) . .
N1D K3 K4 C6D -54.44(19) . .
C6C K3 K4 C6D -179.0(2) . .
C5D K3 K4 C6D -29.24(17) . .
C14D K3 K4 C6D 140.33(18) . .
K2 K3 K4 C6D -128.8(4) . .
O1D K3 K4 K1 -153.0(5) . 1_565
N2D K3 K4 K1 68.5(5) . 1_565
N2C K3 K4 K1 -111.3(5) . 1_565
O1C K3 K4 K1 38.6(5) . 1_565
N1C K3 K4 K1 171.5(4) . 1_565
N1D K3 K4 K1 -11.6(5) . 1_565
C6C K3 K4 K1 -136.1(4) . 1_565
C6D K3 K4 K1 42.9(5) . 1_565
C5D K3 K4 K1 13.6(5) . 1_565
C14D K3 K4 K1 -176.8(5) . 1_565
K2 K3 K4 K1 -85.9(5) . 1_565
N2D K4 F4D C11D -3.7(4) . .
N2A K4 F4D C11D 178.7(4) 1_565 .
O1A K4 F4D C11D -84.6(4) 1_565 .
N1A K4 F4D C11D -172.3(4) 1_565 .
O1D K4 F4D C11D 88.0(4) . .
N1D K4 F4D C11D 5.4(4) . .
C6A K4 F4D C11D 165.5(4) 1_565 .
C6D K4 F4D C11D -16.5(4) . .
K1 K4 F4D C11D -135.7(4) 1_565 .
K3 K4 F4D C11D 41.0(4) . .
O1D K3 N1D C1D -94.3(5) . .
N2D K3 N1D C1D -179.2(5) . .
N2C K3 N1D C1D -4.1(5) . .
O1C K3 N1D C1D 90.0(5) . .
N1C K3 N1D C1D 0(4) . .
C6C K3 N1D C1D -25.5(6) . .
C6D K3 N1D C1D 156.8(6) . .
C5D K3 N1D C1D 132.8(7) . .
C14D K3 N1D C1D -107.9(5) . .
K4 K3 N1D C1D -122.4(5) . .
K2 K3 N1D C1D 51.8(5) . .
O1D K3 N1D C5D 132.9(4) . .
N2D K3 N1D C5D 48.0(3) . .
N2C K3 N1D C5D -136.9(3) . .
O1C K3 N1D C5D -42.7(4) . .
N1C K3 N1D C5D -133(4) . .
C6C K3 N1D C5D -158.3(3) . .
C6D K3 N1D C5D 24.1(3) . .
C14D K3 N1D C5D 119.4(4) . .
K4 K3 N1D C5D 104.8(4) . .
K2 K3 N1D C5D -81.0(4) . .
O1D K3 N1D K4 28.07(14) . .
N2D K3 N1D K4 -56.81(14) . .
N2C K3 N1D K4 118.29(15) . .
O1C K3 N1D K4 -147.57(12) . .
N1C K3 N1D K4 122(4) . .
C6C K3 N1D K4 96.90(19) . .
C6D K3 N1D K4 -80.78(18) . .
C5D K3 N1D K4 -104.8(4) . .
C14D K3 N1D K4 14.53(19) . .
K2 K3 N1D K4 174.21(3) . .
N2D K4 N1D C1D 177.2(5) . .
N2A K4 N1D C1D -5.3(5) 1_565 .
O1A K4 N1D C1D -88.0(5) 1_565 .
N1A K4 N1D C1D -73(5) 1_565 .
O1D K4 N1D C1D 92.3(5) . .
F4D K4 N1D C1D 168.2(5) . .
C6A K4 N1D C1D 16.7(6) 1_565 .
C6D K4 N1D C1D -160.0(6) . .
K1 K4 N1D C1D -62.0(5) 1_565 .
K3 K4 N1D C1D 118.9(5) . .
N2D K4 N1D C5D -42.1(3) . .
N2A K4 N1D C5D 135.4(3) 1_565 .
O1A K4 N1D C5D 52.7(3) 1_565 .
N1A K4 N1D C5D 67(5) 1_565 .
O1D K4 N1D C5D -127.0(4) . .
F4D K4 N1D C5D -51.1(4) . .
C6A K4 N1D C5D 157.4(3) 1_565 .
C6D K4 N1D C5D -19.3(3) . .
K1 K4 N1D C5D 78.7(4) 1_565 .
K3 K4 N1D C5D -100.4(4) . .
N2D K4 N1D K3 58.29(15) . .
N2A K4 N1D K3 -124.24(14) 1_565 .
O1A K4 N1D K3 153.04(14) 1_565 .
N1A K4 N1D K3 168(4) 1_565 .
O1D K4 N1D K3 -26.59(13) . .
F4D K4 N1D K3 49.25(16) . .
C6A K4 N1D K3 -102.21(19) 1_565 .
C6D K4 N1D K3 81.07(18) . .
K1 K4 N1D K3 179.05(4) 1_565 .
N2A K4 N2D C9D 92(5) 1_565 .
O1A K4 N2D C9D 82.6(4) 1_565 .
N1A K4 N2D C9D -11.8(5) 1_565 .
O1D K4 N2D C9D -103.6(4) . .
N1D K4 N2D C9D 165.4(5) . .
F4D K4 N2D C9D -24.7(4) . .
C6A K4 N2D C9D -56.0(6) 1_565 .
C6D K4 N2D C9D 120.7(6) . .
K1 K4 N2D C9D 52.6(5) 1_565 .
K3 K4 N2D C9D -132.1(5) . .
N2A K4 N2D C6D -28(5) 1_565 .
O1A K4 N2D C6D -38.1(4) 1_565 .
N1A K4 N2D C6D -132.5(4) 1_565 .
O1D K4 N2D C6D 135.7(4) . .
N1D K4 N2D C6D 44.7(4) . .
F4D K4 N2D C6D -145.4(4) . .
C6A K4 N2D C6D -176.7(5) 1_565 .
K1 K4 N2D C6D -68.1(4) 1_565 .
K3 K4 N2D C6D 107.2(4) . .
N2A K4 N2D K3 -135(4) 1_565 .
O1A K4 N2D K3 -145.33(14) 1_565 .
N1A K4 N2D K3 120.32(16) 1_565 .
O1D K4 N2D K3 28.50(13) . .
N1D K4 N2D K3 -62.46(16) . .
F4D K4 N2D K3 107.37(17) . .
C6A K4 N2D K3 76.1(4) 1_565 .
C6D K4 N2D K3 -107.2(4) . .
K1 K4 N2D K3 -175.27(4) 1_565 .
O1D K3 N2D C9D 94.8(5) . .
N2C K3 N2D C9D 126(2) . .
O1C K3 N2D C9D -75.4(5) . .
N1C K3 N2D C9D 8.5(6) . .
N1D K3 N2D C9D -171.5(5) . .
C6C K3 N2D C9D 61.0(7) . .
C6D K3 N2D C9D -124.9(7) . .
C5D K3 N2D C9D -147.9(6) . .
C14D K3 N2D C9D 69.3(5) . .
K4 K3 N2D C9D 124.8(5) . .
K2 K3 N2D C9D -58.2(5) . .
O1D K3 N2D C6D -140.3(4) . .
N2C K3 N2D C6D -109(2) . .
O1C K3 N2D C6D 49.6(4) . .
N1C K3 N2D C6D 133.5(3) . .
N1D K3 N2D C6D -46.6(4) . .
C6C K3 N2D C6D -174.1(4) . .
C5D K3 N2D C6D -23.0(3) . .
C14D K3 N2D C6D -165.7(4) . .
K4 K3 N2D C6D -110.2(4) . .
K2 K3 N2D C6D 66.7(4) . .
O1D K3 N2D K4 -30.04(15) . .
N2C K3 N2D K4 1(2) . .
O1C K3 N2D K4 159.78(12) . .
N1C K3 N2D K4 -116.31(16) . .
N1D K3 N2D K4 63.65(16) . .
C6C K3 N2D K4 -63.9(4) . .
C6D K3 N2D K4 110.2(4) . .
C5D K3 N2D K4 87.2(2) . .
C14D K3 N2D K4 -55.52(16) . .
K2 K3 N2D K4 176.94(5) . .
C5D N1D C1D C2D -0.3(8) . .
K3 N1D C1D C2D -125.3(6) . .
K4 N1D C1D C2D 135.7(5) . .
N1D C1D C2D C3D 0.4(9) . .
C1D C2D C3D C4D -1.1(10) . .
C2D C3D C4D C5D 1.6(10) . .
C1D N1D C5D C4D 0.8(8) . .
K3 N1D C5D C4D 133.5(5) . .
K4 N1D C5D C4D -141.4(5) . .
C1D N1D C5D C6D 179.3(5) . .
K3 N1D C5D C6D -48.0(5) . .
K4 N1D C5D C6D 37.1(5) . .
C1D N1D C5D K3 -132.6(5) . .
K4 N1D C5D K3 85.1(2) . .
C3D C4D C5D N1D -1.5(9) . .
C3D C4D C5D C6D -179.9(6) . .
C3D C4D C5D K3 71.2(9) . .
O1D K3 C5D N1D -49.5(4) . .
N2D K3 C5D N1D -116.6(4) . .
N2C K3 C5D N1D 56.6(4) . .
O1C K3 C5D N1D 137.2(4) . .
N1C K3 C5D N1D 174.3(4) . .
C6C K3 C5D N1D 37.2(5) . .
C6D K3 C5D N1D -137.8(5) . .
C14D K3 C5D N1D -71.1(4) . .
K4 K3 C5D N1D -60.0(3) . .
K2 K3 C5D N1D 114.6(3) . .
O1D K3 C5D C4D -148.2(7) . .
N2D K3 C5D C4D 144.7(8) . .
N2C K3 C5D C4D -42.1(8) . .
O1C K3 C5D C4D 38.5(7) . .
N1C K3 C5D C4D 75.6(9) . .
N1D K3 C5D C4D -98.7(8) . .
C6C K3 C5D C4D -61.5(8) . .
C6D K3 C5D C4D 123.5(8) . .
C14D K3 C5D C4D -169.8(7) . .
K4 K3 C5D C4D -158.7(8) . .
K2 K3 C5D C4D 15.9(8) . .
O1D K3 C5D C6D 88.3(3) . .
N2D K3 C5D C6D 21.1(3) . .
N2C K3 C5D C6D -165.6(3) . .
O1C K3 C5D C6D -85.0(3) . .
N1C K3 C5D C6D -48.0(5) . .
N1D K3 C5D C6D 137.8(5) . .
C6C K3 C5D C6D 175.0(3) . .
C14D K3 C5D C6D 66.6(4) . .
K4 K3 C5D C6D 77.8(3) . .
K2 K3 C5D C6D -107.7(3) . .
C9D N2D C6D C7D -0.6(6) . .
K4 N2D C6D C7D 127.3(4) . .
K3 N2D C6D C7D -137.8(4) . .
C9D N2D C6D C5D -177.0(4) . .
K4 N2D C6D C5D -49.0(5) . .
K3 N2D C6D C5D 45.8(5) . .
C9D N2D C6D K3 137.2(5) . .
K4 N2D C6D K3 -94.8(3) . .
C9D N2D C6D K4 -128.0(5) . .
K3 N2D C6D K4 94.8(3) . .
N1D C5D C6D N2D 4.6(7) . .
C4D C5D C6D N2D -176.9(5) . .
K3 C5D C6D N2D -34.6(4) . .
N1D C5D C6D C7D -170.6(6) . .
C4D C5D C6D C7D 7.9(9) . .
K3 C5D C6D C7D 150.2(6) . .
N1D C5D C6D K3 39.3(4) . .
C4D C5D C6D K3 -142.3(5) . .
N1D C5D C6D K4 -30.1(4) . .
C4D C5D C6D K4 148.4(5) . .
K3 C5D C6D K4 -69.35(11) . .
O1D K3 C6D N2D 41.0(4) . .
N2C K3 C6D N2D 167.6(4) . .
O1C K3 C6D N2D -129.7(4) . .
N1C K3 C6D N2D -63.9(4) . .
N1D K3 C6D N2D 117.7(4) . .
C6C K3 C6D N2D 75(4) . .
C5D K3 C6D N2D 139.2(5) . .
C14D K3 C6D N2D 15.2(4) . .
K4 K3 C6D N2D 53.2(3) . .
K2 K3 C6D N2D -131.3(3) . .
O1D K3 C6D C7D 114.5(6) . .
N2D K3 C6D C7D 73.5(6) . .
N2C K3 C6D C7D -118.9(6) . .
O1C K3 C6D C7D -56.3(6) . .
N1C K3 C6D C7D 9.5(7) . .
N1D K3 C6D C7D -168.8(7) . .
C6C K3 C6D C7D 148(4) . .
C5D K3 C6D C7D -147.3(7) . .
C14D K3 C6D C7D 88.7(6) . .
K4 K3 C6D C7D 126.7(6) . .
K2 K3 C6D C7D -57.8(6) . .
O1D K3 C6D C5D -98.2(3) . .
N2D K3 C6D C5D -139.2(5) . .
N2C K3 C6D C5D 28.5(6) . .
O1C K3 C6D C5D 91.1(3) . .
N1C K3 C6D C5D 156.9(3) . .
N1D K3 C6D C5D -21.5(3) . .
C6C K3 C6D C5D -64(4) . .
C14D K3 C6D C5D -124.0(3) . .
K4 K3 C6D C5D -86.0(3) . .
K2 K3 C6D C5D 89.5(3) . .
O1D K3 C6D K4 -12.23(14) . .
N2D K3 C6D K4 -53.2(3) . .
N2C K3 C6D K4 114.4(4) . .
O1C K3 C6D K4 177.04(11) . .
N1C K3 C6D K4 -117.17(19) . .
N1D K3 C6D K4 64.46(18) . .
C6C K3 C6D K4 22(4) . .
C5D K3 C6D K4 86.0(3) . .
C14D K3 C6D K4 -38.04(17) . .
K2 K3 C6D K4 175.48(4) . .
N2A K4 C6D N2D 177.4(4) 1_565 .
O1A K4 C6D N2D 140.0(4) 1_565 .
N1A K4 C6D N2D 63.3(4) 1_565 .
O1D K4 C6D N2D -44.9(4) . .
N1D K4 C6D N2D -120.3(4) . .
F4D K4 C6D N2D 29.1(4) . .
C6A K4 C6D N2D 149(4) 1_565 .
K1 K4 C6D N2D 126.6(3) 1_565 .
K3 K4 C6D N2D -56.4(3) . .
N2D K4 C6D C7D -79.6(6) . .
N2A K4 C6D C7D 97.8(6) 1_565 .
O1A K4 C6D C7D 60.4(5) 1_565 .
N1A K4 C6D C7D -16.4(6) 1_565 .
O1D K4 C6D C7D -124.6(5) . .
N1D K4 C6D C7D 160.1(6) . .
F4D K4 C6D C7D -50.5(5) . .
C6A K4 C6D C7D 70(5) 1_565 .
K1 K4 C6D C7D 47.0(5) 1_565 .
K3 K4 C6D C7D -136.0(5) . .
N2D K4 C6D C5D 137.1(5) . .
N2A K4 C6D C5D -45.5(5) 1_565 .
O1A K4 C6D C5D -82.9(3) 1_565 .
N1A K4 C6D C5D -159.6(3) 1_565 .
O1D K4 C6D C5D 92.2(3) . .
N1D K4 C6D C5D 16.8(3) . .
F4D K4 C6D C5D 166.2(3) . .
C6A K4 C6D C5D -74(5) 1_565 .
K1 K4 C6D C5D -96.3(3) 1_565 .
K3 K4 C6D C5D 80.7(3) . .
N2D K4 C6D K3 56.4(3) . .
N2A K4 C6D K3 -126.2(3) 1_565 .
O1A K4 C6D K3 -163.58(14) 1_565 .
N1A K4 C6D K3 119.67(18) 1_565 .
O1D K4 C6D K3 11.48(13) . .
N1D K4 C6D K3 -63.90(17) . .
F4D K4 C6D K3 85.55(10) . .
C6A K4 C6D K3 -154(5) 1_565 .
K1 K4 C6D K3 -177.01(4) 1_565 .
N2D C6D C7D C8D 1.0(6) . .
C5D C6D C7D C8D 176.5(6) . .
K3 C6D C7D C8D -50.9(7) . .
K4 C6D C7D C8D 52.0(6) . .
N2D C6D C7D C110 177.0(5) . .
C5D C6D C7D C110 -7.6(10) . .
K3 C6D C7D C110 125.0(6) . .
K4 C6D C7D C110 -132.0(5) . .
C6D C7D C8D C9D -1.0(6) . .
C110 C7D C8D C9D -177.3(5) . .
C6D N2D C9D C8D 0.0(6) . .
K4 N2D C9D C8D -122.8(4) . .
K3 N2D C9D C8D 125.4(5) . .
C6D N2D C9D C11D -176.9(5) . .
K4 N2D C9D C11D 60.3(6) . .
K3 N2D C9D C11D -51.5(7) . .
C7D C8D C9D N2D 0.6(6) . .
C7D C8D C9D C11D 177.3(6) . .
K4 F4D C11D F6D 155.0(4) . .
K4 F4D C11D F5D -94.2(4) . .
K4 F4D C11D C9D 28.7(6) . .
N2D C9D C11D F6D 176.3(5) . .
C8D C9D C11D F6D -0.1(9) . .
N2D C9D C11D F4D -62.2(7) . .
C8D C9D C11D F4D 121.4(6) . .
N2D C9D C11D F5D 56.1(8) . .
C8D C9D C11D F5D -120.3(6) . .
C8D C7D C110 F3D -119.8(7) . .
C6D C7D C110 F3D 64.7(8) . .
C8D C7D C110 F1D 118.1(6) . .
C6D C7D C110 F1D -57.4(8) . .
C8D C7D C110 F2D 0.1(8) . .
C6D C7D C110 F2D -175.4(5) . .
N2D K3 O1D C13D 138.5(5) . .
N2C K3 O1D C13D -39.1(5) . .
O1C K3 O1D C13D -123.8(8) . .
N1C K3 O1D C13D -95.0(5) . .
N1D K3 O1D C13D 82.3(5) . .
C6C K3 O1D C13D -54.7(5) . .
C6D K3 O1D C13D 123.9(5) . .
C5D K3 O1D C13D 98.7(5) . .
C14D K3 O1D C13D -127.7(6) . .
K4 K3 O1D C13D 110.5(5) . .
K2 K3 O1D C13D -64.0(5) . .
N2D K3 O1D C14D -93.8(4) . .
N2C K3 O1D C14D 88.7(4) . .
O1C K3 O1D C14D 3.9(9) . .
N1C K3 O1D C14D 32.7(4) . .
N1D K3 O1D C14D -150.0(4) . .
C6C K3 O1D C14D 73.1(4) . .
C6D K3 O1D C14D -108.3(4) . .
C5D K3 O1D C14D -133.5(4) . .
K4 K3 O1D C14D -121.8(4) . .
K2 K3 O1D C14D 63.7(4) . .
N2D K3 O1D K4 28.00(13) . .
N2C K3 O1D K4 -149.54(13) . .
O1C K3 O1D K4 125.7(7) . .
N1C K3 O1D K4 154.48(14) . .
N1D K3 O1D K4 -28.20(13) . .
C6C K3 O1D K4 -165.16(16) . .
C6D K3 O1D K4 13.45(15) . .
C5D K3 O1D K4 -11.74(16) . .
C14D K3 O1D K4 121.8(4) . .
K2 K3 O1D K4 -174.49(4) . .
N2D K4 O1D C13D -153.7(4) . .
N2A K4 O1D C13D 25.7(4) 1_565 .
O1A K4 O1D C13D -99.8(13) 1_565 .
N1A K4 O1D C13D 82.4(4) 1_565 .
N1D K4 O1D C13D -97.0(4) . .
F4D K4 O1D C13D 150.2(4) . .
C6A K4 O1D C13D 41.2(4) 1_565 .
C6D K4 O1D C13D -138.3(4) . .
K1 K4 O1D C13D 52.5(5) 1_565 .
K3 K4 O1D C13D -125.0(5) . .
N2D K4 O1D C14D 74.6(4) . .
N2A K4 O1D C14D -106.0(4) 1_565 .
O1A K4 O1D C14D 128.5(12) 1_565 .
N1A K4 O1D C14D -49.4(4) 1_565 .
N1D K4 O1D C14D 131.2(4) . .
F4D K4 O1D C14D 18.5(4) . .
C6A K4 O1D C14D -90.6(4) 1_565 .
C6D K4 O1D C14D 90.0(4) . .
K1 K4 O1D C14D -79.3(4) 1_565 .
K3 K4 O1D C14D 103.3(4) . .
N2D K4 O1D K3 -28.67(13) . .
N2A K4 O1D K3 150.71(13) 1_565 .
O1A K4 O1D K3 25.2(13) 1_565 .
N1A K4 O1D K3 -152.63(13) 1_565 .
N1D K4 O1D K3 27.98(14) . .
F4D K4 O1D K3 -84.80(12) . .
C6A K4 O1D K3 166.18(15) 1_565 .
C6D K4 O1D K3 -13.26(15) . .
K1 K4 O1D K3 177.47(5) 1_565 .
C14D O1D C13D C12D -171.9(5) . .
K3 O1D C13D C12D -47.1(6) . .
K4 O1D C13D C12D 50.7(5) . .
C13D O1D C14D C15D -84.0(6) . .
K3 O1D C14D C15D 140.2(5) . .
K4 O1D C14D C15D 47.2(7) . .
C13D O1D C14D K3 135.8(5) . .
K4 O1D C14D K3 -93.0(3) . .
O1D K3 C14D C15D -68.1(8) . .
N2D K3 C14D C15D 16.9(8) . .
N2C K3 C14D C15D -159.1(8) . .
O1C K3 C14D C15D 113.1(8) . .
N1C K3 C14D C15D 147.6(8) . .
N1D K3 C14D C15D -35.2(8) . .
C6C K3 C14D C15D -166.6(8) . .
C6D K3 C14D C15D 11.2(8) . .
C5D K3 C14D C15D -12.7(9) . .
K4 K3 C14D C15D -23.1(7) . .
K2 K3 C14D C15D 162.1(7) . .
N2D K3 C14D O1D 85.0(3) . .
N2C K3 C14D O1D -91.0(3) . .
O1C K3 C14D O1D -178.8(3) . .
N1C K3 C14D O1D -144.4(4) . .
N1D K3 C14D O1D 32.9(4) . .
C6C K3 C14D O1D -98.5(4) . .
C6D K3 C14D O1D 79.2(4) . .
C5D K3 C14D O1D 55.4(4) . .
K4 K3 C14D O1D 45.0(3) . .
K2 K3 C14D O1D -129.9(3) . .
