#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:11:56 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179366 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/63/4326379.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4326379
loop_
_publ_author_name
'Santiago Reinoso'
'José Ramón Galán-Mascarós'
'Luis Lezama'
_publ_section_title
;
 New Type of Heterometallic 3d-4f Rhomblike Core in Weakley-Like
 Polyoxometalates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9587
_journal_page_last               9593
_journal_paper_doi               10.1021/ic201331d
_journal_volume                  50
_journal_year                    2011
_chemical_formula_sum            'C2 H45 Ce Cs3 Cu3 Ge2 K4 Na4 O91 W18'
_chemical_formula_weight         5957.69
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                101.966(2)
_cell_angle_beta                 91.712(2)
_cell_angle_gamma                108.183(2)
_cell_formula_units_Z            2
_cell_length_a                   12.5496(2)
_cell_length_b                   17.4025(4)
_cell_length_c                   23.3170(5)
_cell_measurement_reflns_used    17160
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      28.9302
_cell_measurement_theta_min      2.3511
_cell_volume                     4708.32(18)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.41 (release 06-05-2009 CrysAlis171 .NET)
(compiled May  6 2009,17:20:42)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.41 (release 06-05-2009 CrysAlis171 .NET)
(compiled May  6 2009,17:20:42)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.41 (release 06-05-2009 CrysAlis171 .NET)
(compiled May  6 2009,17:20:42)
;
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX  (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR2004 (Burla et al, 2005)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 16.0267
_diffrn_measured_fraction_theta_full 0.895
_diffrn_measured_fraction_theta_max 0.895
_diffrn_measurement_device_type  'Xcalibur, Sapphire3, Gemini'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Enhance (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0303
_diffrn_reflns_av_sigmaI/netI    0.0577
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            34532
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.35
_exptl_absorpt_coefficient_mu    25.097
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.64135
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.41 (release 06-05-2009 CrysAlis171 .NET)
(compiled May  6 2009,17:20:42)
empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    4.202
_exptl_crystal_description       prism
_exptl_crystal_F_000             5222
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.03
_refine_diff_density_max         4.598
_refine_diff_density_min         -3.335
_refine_diff_density_rms         0.397
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.071
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     648
_refine_ls_number_reflns         14834
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.071
_refine_ls_R_factor_all          0.0668
_refine_ls_R_factor_gt           0.0462
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0787P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1330
_refine_ls_wR_factor_ref         0.1381
_reflns_number_gt                10679
_reflns_number_total             14834
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic201331d_si_002.cif
_cod_data_source_block           1a
_cod_original_cell_volume        4708.32(17)
_cod_database_code               4326379
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
W1 W 0.54978(8) -0.38289(5) -0.30896(4) 0.0209(2) Uani 1 1 d .
W2 W 0.39354(7) -0.27377(4) -0.20673(3) 0.0168(2) Uani 1 1 d .
W3 W 0.31797(8) -0.31693(5) -0.36869(4) 0.0192(2) Uani 1 1 d .
W4 W 0.72547(8) -0.27914(5) -0.39576(4) 0.0211(2) Uani 1 1 d .
W5 W 0.79755(8) -0.23450(4) -0.24988(4) 0.0176(2) Uani 1 1 d .
W6 W 0.64124(7) -0.13109(4) -0.14401(3) 0.01391(19) Uani 1 1 d .
W7 W 0.42635(7) -0.07222(4) -0.19908(3) 0.01370(19) Uani 1 1 d .
W8 W 0.36605(7) -0.11299(4) -0.36229(3) 0.01651(19) Uani 1 1 d .
W9 W 0.50080(8) -0.21522(5) -0.45386(3) 0.0211(2) Uani 1 1 d .
W10 W 1.17696(8) 0.27019(5) -0.28014(4) 0.0194(2) Uani 1 1 d .
W11 W 1.03445(8) 0.39167(5) -0.17808(4) 0.0213(2) Uani 1 1 d .
W12 W 0.94468(8) 0.33400(5) -0.33933(4) 0.0208(2) Uani 1 1 d .
W13 W 1.03603(7) 0.07039(4) -0.35025(3) 0.0161(2) Uani 1 1 d .
W14 W 1.10376(7) 0.11901(5) -0.20317(3) 0.01661(19) Uani 1 1 d .
W15 W 0.97011(8) 0.24405(5) -0.09856(3) 0.0185(2) Uani 1 1 d .
W16 W 0.76482(8) 0.30274(4) -0.15313(4) 0.0187(2) Uani 1 1 d .
W17 W 0.67647(8) 0.23619(5) -0.31504(4) 0.0183(2) Uani 1 1 d .
W18 W 0.80836(8) 0.13344(5) -0.40930(3) 0.0167(2) Uani 1 1 d .
Ce1 Ce 0.68272(10) 0.07141(6) -0.14644(4) 0.0135(3) Uani 1 1 d .
Cu1 Cu 0.7661(2) -0.06472(13) -0.39070(10) 0.0164(6) Uani 1 1 d .
Cu2 Cu 0.8299(2) -0.02167(12) -0.24992(9) 0.0119(5) Uani 1 1 d .
Cu3 Cu 0.6397(2) 0.03192(12) -0.29975(9) 0.0121(5) Uani 1 1 d .
Ge1 Ge 0.58569(18) -0.16420(10) -0.29938(8) 0.0107(4) Uani 1 1 d .
Ge2 Ge 0.88163(18) 0.17454(11) -0.25221(8) 0.0112(4) Uani 1 1 d .
O1T O 0.4963(14) -0.4878(8) -0.3085(6) 0.031(4) Uiso 1 1 d .
O2T O 0.2956(12) -0.3433(7) -0.1757(6) 0.021(3) Uiso 1 1 d .
O3T O 0.1943(14) -0.4011(8) -0.3859(6) 0.029(3) Uiso 1 1 d .
O4T O 0.7877(15) -0.3268(9) -0.4520(7) 0.036(4) Uiso 1 1 d .
O5T O 0.9039(14) -0.2524(8) -0.2110(6) 0.027(3) Uiso 1 1 d .
O6T O 0.7009(12) -0.1158(7) -0.0729(5) 0.018(3) Uiso 1 1 d .
O7T O 0.3440(13) -0.0178(7) -0.1638(6) 0.021(3) Uiso 1 1 d .
O8T O 0.2690(14) -0.0660(8) -0.3758(6) 0.028(3) Uiso 1 1 d .
O9T O 0.4846(15) -0.2416(9) -0.5307(6) 0.034(4) Uiso 1 1 d .
O10T O 1.3071(14) 0.3371(8) -0.2904(6) 0.030(3) Uiso 1 1 d .
O11T O 1.1207(13) 0.4954(8) -0.1578(6) 0.027(3) Uiso 1 1 d .
O12T O 1.0042(14) 0.4207(8) -0.3666(6) 0.032(4) Uiso 1 1 d .
O13T O 1.0861(13) 0.0143(7) -0.4066(6) 0.021(3) Uiso 1 1 d .
O14T O 1.1989(14) 0.0900(8) -0.1644(6) 0.028(3) Uiso 1 1 d .
O15T O 1.0247(14) 0.2577(8) -0.0265(6) 0.031(4) Uiso 1 1 d .
O16T O 0.6801(13) 0.3527(8) -0.1180(6) 0.023(3) Uiso 1 1 d .
O17T O 0.5553(13) 0.2623(8) -0.3270(6) 0.023(3) Uiso 1 1 d .
O18T O 0.7863(13) 0.0979(8) -0.4848(6) 0.024(3) Uiso 1 1 d .
O4G2 O 0.7819(12) 0.0826(7) -0.2430(5) 0.015(3) Uiso 1 1 d .
O23 O 0.3220(13) -0.2888(7) -0.2820(6) 0.022(3) Uiso 1 1 d .
O27 O 0.3413(12) -0.1775(7) -0.1824(5) 0.017(3) Uiso 1 1 d .
O49 O 0.5855(13) -0.2838(8) -0.4366(6) 0.024(3) Uiso 1 1 d .
O104 O 1.2211(12) 0.2156(7) -0.2254(5) 0.020(3) Uiso 1 1 d .
O67 O 0.5388(12) -0.0608(7) -0.1347(5) 0.017(3) Uiso 1 1 d .
O101 O 1.1377(12) 0.3422(7) -0.2136(5) 0.020(3) Uiso 1 1 d .
O6C O 0.6843(12) 0.1929(7) -0.1611(5) 0.016(3) Uiso 1 1 d .
O115 O 1.0619(13) 0.3561(8) -0.1097(6) 0.025(3) Uiso 1 1 d .
O13 O 0.4266(12) -0.3682(7) -0.3526(5) 0.017(3) Uiso 1 1 d .
O4C2 O 0.9723(12) 0.0406(7) -0.2034(5) 0.018(3) Uiso 1 1 d .
O116 O 0.8967(13) 0.4010(8) -0.1520(6) 0.025(3) Uiso 1 1 d .
O8CC O 0.7401(12) 0.0428(7) -0.3816(5) 0.019(3) Uiso 1 1 d .
O112 O 0.9737(12) 0.3827(7) -0.2557(5) 0.021(3) Uiso 1 1 d .
O14 O 0.6261(13) -0.3869(8) -0.3757(6) 0.026(3) Uiso 1 1 d .
O3G1 O 0.4736(12) -0.1943(7) -0.3550(5) 0.015(3) Uiso 1 1 d .
O8C3 O 0.4943(13) -0.0268(8) -0.3465(6) 0.023(3) Uiso 1 1 d .
O7CC O 0.5419(12) 0.0128(7) -0.2177(5) 0.016(3) Uiso 1 1 d .
O3CC O 0.9055(13) -0.0024(7) -0.3379(6) 0.021(3) Uiso 1 1 d .
O15 O 0.6831(12) -0.3482(7) -0.2567(6) 0.021(3) Uiso 1 1 d .
O9C1 O 0.6206(12) -0.1247(7) -0.4366(5) 0.020(3) Uiso 1 1 d .
O26 O 0.5082(12) -0.2242(7) -0.1417(5) 0.020(3) Uiso 1 1 d .
O156 O 0.8500(13) 0.2930(8) -0.0842(6) 0.027(3) Uiso 1 1 d .
O145 O 1.0726(13) 0.2007(8) -0.1426(6) 0.023(3) Uiso 1 1 d .
O39 O 0.3665(13) -0.3122(8) -0.4419(6) 0.027(3) Uiso 1 1 d .
O128 O 0.9013(12) 0.2500(7) -0.4094(5) 0.019(3) Uiso 1 1 d .
O167 O 0.7225(13) 0.2973(7) -0.2341(6) 0.022(3) Uiso 1 1 d .
O12 O 0.4822(12) -0.3378(7) -0.2406(5) 0.017(3) Uiso 1 1 d .
O127 O 0.7953(13) 0.3344(8) -0.3351(6) 0.025(3) Uiso 1 1 d .
O78 O 0.3581(12) -0.1054(7) -0.2774(5) 0.018(3) Uiso 1 1 d .
O5C2 O 0.8550(12) -0.1272(7) -0.2529(5) 0.020(3) Uiso 1 1 d .
O38 O 0.2606(13) -0.2281(7) -0.3683(5) 0.021(3) Uiso 1 1 d .
O45 O 0.8259(13) -0.2770(8) -0.3281(6) 0.025(3) Uiso 1 1 d .
O56 O 0.7122(11) -0.2026(7) -0.1857(5) 0.013(3) Uiso 1 1 d .
O6CC O 0.7377(12) -0.0381(7) -0.1671(5) 0.015(3) Uiso 1 1 d .
O2G2 O 0.9063(11) 0.2534(7) -0.1903(5) 0.013(3) Uiso 1 1 d .
O5C O 0.8649(12) 0.1404(7) -0.1152(6) 0.020(3) Uiso 1 1 d .
O138 O 0.9514(12) 0.1194(7) -0.3933(5) 0.016(3) Uiso 1 1 d .
O3G2 O 0.8419(12) 0.2102(7) -0.3115(5) 0.017(3) Uiso 1 1 d .
O1G2 O 1.0107(12) 0.1625(7) -0.2678(5) 0.014(3) Uiso 1 1 d .
O4G1 O 0.6831(11) -0.0697(6) -0.3014(5) 0.010(3) Uiso 1 1 d .
O7C3 O 0.6196(12) 0.1399(7) -0.2953(5) 0.018(3) Uiso 1 1 d .
O2G1 O 0.5274(11) -0.1607(7) -0.2330(5) 0.011(3) Uiso 1 1 d .
O178 O 0.6890(13) 0.1819(7) -0.3943(6) 0.023(3) Uiso 1 1 d .
O134 O 1.1191(13) 0.0599(7) -0.2844(6) 0.022(3) Uiso 1 1 d .
O1G1 O 0.6480(11) -0.2425(7) -0.3105(5) 0.014(3) Uiso 1 1 d .
O4C1 O 0.7873(12) -0.1715(7) -0.3938(5) 0.019(3) Uiso 1 1 d .
O1CU O 0.8491(15) -0.0643(9) -0.4807(7) 0.039(4) Uiso 1 1 d .
O1AC O 0.6910(14) 0.0825(8) -0.0423(6) 0.031(4) Uiso 1 1 d .
O2AC O 0.5454(13) 0.1053(8) -0.0795(6) 0.022(3) Uiso 1 1 d .
O103 O 1.1636(12) 0.1792(7) -0.3433(5) 0.020(3) Uiso 1 1 d .
O89 O 0.3939(12) -0.1553(7) -0.4402(5) 0.021(3) Uiso 1 1 d .
O102 O 1.0743(12) 0.3012(7) -0.3266(5) 0.020(3) Uiso 1 1 d .
C1 C 0.605(2) 0.1014(12) -0.0355(9) 0.026(5) Uiso 1 1 d .
C2 C 0.571(3) 0.1190(18) 0.0279(13) 0.069(9) Uiso 1 1 d .
H2A H 0.5023 0.1329 0.0271 0.104 Uiso 1 1 calc R
H2B H 0.6295 0.1646 0.0523 0.104 Uiso 1 1 calc R
H2C H 0.5584 0.0705 0.0437 0.104 Uiso 1 1 calc R
Cs1 Cs 1.37613(16) 0.11045(10) -0.27853(9) 0.0551(5) Uani 1 1 d .
Cs2 Cs 0.3709(3) -0.50028(16) -0.18485(15) 0.0566(12) Uani 0.608(5) 1 d P
Cs2A Cs 0.2392(5) -0.5021(3) -0.2894(3) 0.081(2) Uani 0.392(5) 1 d P
Cs3 Cs 0.5336(3) -0.0461(2) -0.54258(17) 0.0402(14) Uani 0.452(5) 1 d P
Cs3A Cs 0.5000 0.0000 -0.5000 0.041(11) Uani 0.095(9) 2 d SP
K1 K 0.1214(8) -0.2302(5) -0.2716(4) 0.083(2) Uiso 1 1 d .
Na1 Na 0.8875(10) 0.1122(6) 0.0124(5) 0.053(3) Uiso 1 1 d .
Na2 Na 1.3540(9) 0.1087(5) -0.0971(4) 0.039(2) Uiso 1 1 d .
Na3 Na 0.7320(19) -0.0267(11) -0.5499(8) 0.024(8) Uiso 0.39(3) 1 d P
Na4 Na 0.497(2) -0.6223(12) -0.3225(9) 0.045(9) Uiso 0.46(3) 1 d P
O1W O 1.454(2) 0.2059(13) -0.1524(10) 0.080(6) Uiso 1 1 d .
O2W O 0.0410(12) -0.1290(7) -0.3303(5) 0.017(3) Uiso 1 1 d .
O3W O 0.0794(18) -0.4141(11) -0.2619(8) 0.059(5) Uiso 1 1 d .
O4W O 0.5458(15) -0.5935(8) -0.2177(6) 0.034(4) Uiso 1 1 d .
O5W O 0.971(2) 0.0224(12) -0.0734(9) 0.065(5) Uiso 1 1 d .
O7W O 0.670(2) -0.1674(14) -0.5882(11) 0.095(8) Uiso 1 1 d .
O8W O 0.255(3) -0.5691(17) -0.4097(13) 0.120(10) Uiso 1 1 d .
O9W O 1.218(2) 0.0310(14) -0.0451(11) 0.091(7) Uiso 1 1 d .
O10W O 1.078(4) 0.154(2) 0.0863(16) 0.162(13) Uiso 1 1 d .
O11W O 0.009(4) -0.317(2) -0.3881(16) 0.162(13) Uiso 1 1 d .
O12W O 1.348(4) 0.227(2) -0.0268(16) 0.162(13) Uiso 1 1 d .
O13W O 0.625(4) -0.381(2) -0.1438(18) 0.182(15) Uiso 1 1 d .
O14W O 0.842(3) 0.1914(17) 0.1199(13) 0.117(9) Uiso 1 1 d .
O15W O 0.363(2) -0.4113(12) -0.6043(9) 0.073(6) Uiso 1 1 d .
O16W O 0.908(2) 0.0900(12) 0.1863(9) 0.069(6) Uiso 1 1 d .
O17W O 0.0433(19) -0.1573(11) -0.4395(8) 0.060(5) Uiso 1 1 d .
O18W O 1.111(2) 0.6451(14) -0.1225(11) 0.095(8) Uiso 1 1 d .
O19W O 0.893(3) -0.2174(16) -0.5307(12) 0.106(9) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1T W1 O14 101.1(6) . .
O1T W1 O15 101.4(7) . .
O14 W1 O15 93.7(6) . .
O1T W1 O13 101.5(7) . .
O14 W1 O13 90.0(6) . .
O15 W1 O13 155.7(5) . .
O1T W1 O12 99.0(5) . .
O14 W1 O12 159.7(5) . .
O15 W1 O12 85.4(6) . .
O13 W1 O12 83.0(5) . .
O1T W1 O1G1 171.9(6) . .
O14 W1 O1G1 74.1(5) . .
O15 W1 O1G1 72.8(5) . .
O13 W1 O1G1 85.2(5) . .
O12 W1 O1G1 86.3(4) . .
O1T W1 Cs2A 54.4(5) . .
O14 W1 Cs2A 129.8(5) . .
O15 W1 Cs2A 130.7(4) . .
O13 W1 Cs2A 59.9(4) . .
O12 W1 Cs2A 61.7(4) . .
O1G1 W1 Cs2A 133.7(3) . .
O1T W1 Cs2 49.7(4) . .
O14 W1 Cs2 150.4(4) . .
O15 W1 Cs2 89.2(4) . .
O13 W1 Cs2 99.4(3) . .
O12 W1 Cs2 49.8(3) . .
O1G1 W1 Cs2 134.3(3) . .
Cs2A W1 Cs2 41.74(12) . .
O2T W2 O23 103.1(6) . .
O2T W2 O12 102.1(5) . .
O23 W2 O12 89.3(6) . .
O2T W2 O26 99.9(6) . .
O23 W2 O26 156.9(5) . .
O12 W2 O26 88.1(6) . .
O2T W2 O27 98.3(5) . .
O23 W2 O27 87.0(5) . .
O12 W2 O27 159.6(5) . .
O26 W2 O27 87.5(6) . .
O2T W2 O2G1 169.4(5) . .
O23 W2 O2G1 83.6(5) . .
O12 W2 O2G1 86.1(4) . .
O26 W2 O2G1 73.4(5) . .
O27 W2 O2G1 73.6(4) . .
O2T W2 Cs2A 57.3(4) . .
O23 W2 Cs2A 64.1(4) . .
O12 W2 Cs2A 62.1(4) . .
O26 W2 Cs2A 133.0(4) . .
O27 W2 Cs2A 132.4(4) . .
O2G1 W2 Cs2A 133.3(3) . .
O2T W2 Cs2 48.2(4) . .
O23 W2 Cs2 106.6(4) . .
O12 W2 Cs2 54.5(3) . .
O26 W2 Cs2 90.4(4) . .
O27 W2 Cs2 145.4(3) . .
O2G1 W2 Cs2 138.3(3) . .
Cs2A W2 Cs2 43.03(12) . .
O2T W2 K1 84.1(5) . .
O23 W2 K1 44.2(4) . .
O12 W2 K1 132.6(4) . .
O26 W2 K1 137.7(4) . .
O27 W2 K1 50.5(4) . .
O2G1 W2 K1 95.3(3) . .
Cs2A W2 K1 84.47(15) . .
Cs2 W2 K1 120.49(13) . .
O3T W3 O39 101.7(6) . .
O3T W3 O38 100.6(7) . .
O39 W3 O38 91.5(6) . .
O3T W3 O13 102.0(6) . .
O39 W3 O13 90.2(6) . .
O38 W3 O13 156.4(6) . .
O3T W3 O23 100.0(6) . .
O39 W3 O23 158.2(6) . .
O38 W3 O23 86.6(5) . .
O13 W3 O23 83.2(5) . .
O3T W3 O3G1 171.5(6) . .
O39 W3 O3G1 73.8(5) . .
O38 W3 O3G1 72.6(5) . .
O13 W3 O3G1 85.3(5) . .
O23 W3 O3G1 84.9(5) . .
O3T W3 K1 79.6(4) . .
O39 W3 K1 136.7(5) . .
O38 W3 K1 46.8(4) . .
O13 W3 K1 132.4(4) . .
O23 W3 K1 50.4(5) . .
O3G1 W3 K1 98.7(3) . .
O3T W3 Cs2A 55.4(5) . .
O39 W3 Cs2A 130.1(4) . .
O38 W3 Cs2A 132.8(4) . .
O13 W3 Cs2A 59.1(4) . .
O23 W3 Cs2A 62.9(4) . .
O3G1 W3 Cs2A 133.0(3) . .
K1 W3 Cs2A 86.65(15) . .
O4T W4 O4C1 103.4(6) . .
O4T W4 O49 102.3(7) . .
O4C1 W4 O49 91.9(6) . .
O4T W4 O45 98.4(7) . .
O4C1 W4 O45 94.5(6) . .
O49 W4 O45 156.2(5) . .
O4T W4 O14 96.2(6) . .
O4C1 W4 O14 160.4(5) . .
O49 W4 O14 83.4(6) . .
O45 W4 O14 82.9(6) . .
O4T W4 O1G1 165.3(6) . .
O4C1 W4 O1G1 88.3(5) . .
O49 W4 O1G1 85.9(5) . .
O45 W4 O1G1 71.5(5) . .
O14 W4 O1G1 72.4(4) . .
O5T W5 O5C2 104.2(7) . .
O5T W5 O45 99.0(6) . .
O5C2 W5 O45 95.0(5) . .
O5T W5 O56 100.6(6) . .
O5C2 W5 O56 89.2(5) . .
O45 W5 O56 158.3(6) . .
O5T W5 O15 95.8(6) . .
O5C2 W5 O15 159.6(6) . .
O45 W5 O15 85.8(5) . .
O56 W5 O15 83.0(5) . .
O5T W5 O1G1 166.8(5) . .
O5C2 W5 O1G1 87.4(6) . .
O45 W5 O1G1 73.4(6) . .
O56 W5 O1G1 85.6(5) . .
O15 W5 O1G1 73.2(5) . .
O5T W5 K1 43.2(4) . 1_655
O5C2 W5 K1 82.7(5) . 1_655
O45 W5 K1 64.0(5) . 1_655
O56 W5 K1 137.7(4) . 1_655
O15 W5 K1 115.6(4) . 1_655
O1G1 W5 K1 135.0(3) . 1_655
O6T W6 O56 100.6(6) . .
O6T W6 O6CC 100.8(6) . .
O56 W6 O6CC 92.5(5) . .
O6T W6 O26 97.5(6) . .
O56 W6 O26 91.3(5) . .
O6CC W6 O26 160.3(6) . .
O6T W6 O67 103.7(5) . .
O56 W6 O67 155.6(5) . .
O6CC W6 O67 82.0(5) . .
O26 W6 O67 86.6(5) . .
O6T W6 O2G1 169.1(5) . .
O56 W6 O2G1 85.5(5) . .
O6CC W6 O2G1 87.9(5) . .
O26 W6 O2G1 73.2(5) . .
O67 W6 O2G1 70.7(5) . .
O6T W6 Ce1 98.4(4) . .
O56 W6 Ce1 127.9(3) . .
O6CC W6 Ce1 36.1(4) . .
O26 W6 Ce1 133.4(4) . .
O67 W6 Ce1 47.1(3) . .
O2G1 W6 Ce1 84.6(3) . .
O7T W7 O7CC 101.2(5) . .
O7T W7 O78 101.9(6) . .
O7CC W7 O78 91.2(5) . .
O7T W7 O27 95.4(5) . .
O7CC W7 O27 162.1(6) . .
O78 W7 O27 91.8(5) . .
O7T W7 O67 102.0(6) . .
O7CC W7 O67 82.8(6) . .
O78 W7 O67 156.0(5) . .
O27 W7 O67 87.4(5) . .
O7T W7 O2G1 168.9(5) . .
O7CC W7 O2G1 87.7(5) . .
O78 W7 O2G1 84.3(5) . .
O27 W7 O2G1 75.1(5) . .
O67 W7 O2G1 72.3(5) . .
O7T W7 Ce1 97.9(5) . .
O7CC W7 Ce1 36.9(4) . .
O78 W7 Ce1 127.3(4) . .
O27 W7 Ce1 134.3(4) . .
O67 W7 Ce1 47.1(3) . .
O2G1 W7 Ce1 85.3(3) . .
O7T W7 K1 81.3(5) . .
O7CC W7 K1 138.4(4) . .
O78 W7 K1 48.5(4) . .
O27 W7 K1 50.7(4) . .
O67 W7 K1 137.9(4) . .
O2G1 W7 K1 96.5(3) . .
Ce1 W7 K1 174.99(12) . .
O7T W7 Cs1 64.4(4) . 1_455
O7CC W7 Cs1 55.8(4) . 1_455
O78 W7 Cs1 61.9(4) . 1_455
O27 W7 Cs1 139.7(4) . 1_455
O67 W7 Cs1 129.2(3) . 1_455
O2G1 W7 Cs1 126.7(3) . 1_455
Ce1 W7 Cs1 84.78(4) . 1_455
K1 W7 Cs1 90.42(13) . 1_455
O8T W8 O8C3 101.8(7) . .
O8T W8 O89 101.0(6) . .
O8C3 W8 O89 95.0(6) . .
O8T W8 O78 99.8(6) . .
O8C3 W8 O78 89.6(6) . .
O89 W8 O78 157.3(5) . .
O8T W8 O38 98.9(6) . .
O8C3 W8 O38 159.0(6) . .
O89 W8 O38 84.9(5) . .
O78 W8 O38 82.9(5) . .
O8T W8 O3G1 170.3(6) . .
O8C3 W8 O3G1 86.8(6) . .
O89 W8 O3G1 73.4(5) . .
O78 W8 O3G1 84.7(5) . .
O38 W8 O3G1 73.0(5) . .
O8T W8 Cs3 66.3(4) . 2_654
O8C3 W8 Cs3 54.8(4) . 2_654
O89 W8 Cs3 63.8(4) . 2_654
O78 W8 Cs3 134.4(3) . 2_654
O38 W8 Cs3 140.2(4) . 2_654
O3G1 W8 Cs3 116.4(3) . 2_654
O8T W8 Cs1 55.3(5) . 1_455
O8C3 W8 Cs1 57.9(4) . 1_455
O89 W8 Cs1 132.1(4) . 1_455
O78 W8 Cs1 68.5(3) . 1_455
O38 W8 Cs1 134.8(3) . 1_455
O3G1 W8 Cs1 134.3(3) . 1_455
Cs3 W8 Cs1 68.39(7) 2_654 1_455
O8T W8 K1 82.0(5) . .
O8C3 W8 K1 137.5(4) . .
O89 W8 K1 126.2(4) . .
O78 W8 K1 48.6(4) . .
O38 W8 K1 42.3(3) . .
O3G1 W8 K1 94.9(3) . .
Cs3 W8 K1 148.30(15) 2_654 .
Cs1 W8 K1 93.93(11) 1_455 .
O8T W8 Cs3A 78.4(4) . .
O8C3 W8 Cs3A 60.9(4) . .
O89 W8 Cs3A 46.6(4) . .
O78 W8 Cs3A 148.7(4) . .
O38 W8 Cs3A 128.3(4) . .
O3G1 W8 Cs3A 102.2(3) . .
Cs3 W8 Cs3A 17.84(6) 2_654 .
Cs1 W8 Cs3A 85.95(3) 1_455 .
K1 W8 Cs3A 156.17(14) . .
O9T W9 O9C1 103.6(6) . .
O9T W9 O49 101.4(6) . .
O9C1 W9 O49 92.4(6) . .
O9T W9 O89 99.4(7) . .
O9C1 W9 O89 94.5(6) . .
O49 W9 O89 155.9(5) . .
O9T W9 O39 96.7(6) . .
O9C1 W9 O39 159.6(5) . .
O49 W9 O39 82.9(6) . .
O89 W9 O39 82.6(6) . .
O9T W9 O3G1 165.6(7) . .
O9C1 W9 O3G1 88.6(5) . .
O49 W9 O3G1 85.4(5) . .
O89 W9 O3G1 71.7(5) . .
O39 W9 O3G1 71.3(5) . .
O9T W9 Cs3 59.4(5) . .
O9C1 W9 Cs3 60.6(5) . .
O49 W9 Cs3 137.1(4) . .
O89 W9 Cs3 65.3(4) . .
O39 W9 Cs3 133.6(5) . .
O3G1 W9 Cs3 123.1(3) . .
O9T W9 Cs3A 76.0(5) . .
O9C1 W9 Cs3A 58.6(5) . .
O49 W9 Cs3A 148.3(4) . .
O89 W9 Cs3A 50.2(4) . .
O39 W9 Cs3A 128.8(4) . .
O3G1 W9 Cs3A 104.8(3) . .
Cs3 W9 Cs3A 18.57(6) . .
O10T W10 O103 99.6(6) . .
O10T W10 O104 101.1(7) . .
O103 W10 O104 91.4(5) . .
O10T W10 O102 101.9(6) . .
O103 W10 O102 88.5(6) . .
O104 W10 O102 156.7(6) . .
O10T W10 O101 99.5(6) . .
O103 W10 O101 160.6(6) . .
O104 W10 O101 88.1(5) . .
O102 W10 O101 84.4(6) . .
O10T W10 O1G2 171.6(6) . .
O103 W10 O1G2 74.7(5) . .
O104 W10 O1G2 73.2(5) . .
O102 W10 O1G2 84.3(5) . .
O101 W10 O1G2 86.6(5) . .
O10T W10 Cs2A 54.3(5) . 1_665
O103 W10 Cs2A 126.6(4) . 1_665
O104 W10 Cs2A 135.0(4) . 1_665
O102 W10 Cs2A 59.5(4) . 1_665
O101 W10 Cs2A 64.1(4) . 1_665
O1G2 W10 Cs2A 134.0(3) . 1_665
O10T W10 Cs2 48.2(4) . 1_665
O103 W10 Cs2 147.7(4) . 1_665
O104 W10 Cs2 92.4(4) . 1_665
O102 W10 Cs2 100.1(4) . 1_665
O101 W10 Cs2 51.7(4) . 1_665
O1G2 W10 Cs2 136.8(3) . 1_665
Cs2A W10 Cs2 42.61(12) 1_665 1_665
O10T W10 Cs1 80.6(5) . .
O103 W10 Cs1 57.9(5) . .
O104 W10 Cs1 43.3(4) . .
O102 W10 Cs1 146.0(3) . .
O101 W10 Cs1 129.0(4) . .
O1G2 W10 Cs1 91.0(3) . .
Cs2A W10 Cs1 134.87(10) 1_665 .
Cs2 W10 Cs1 106.10(6) 1_665 .
O11T W11 O115 99.9(6) . .
O11T W11 O101 100.1(6) . .
O115 W11 O101 87.9(6) . .
O11T W11 O116 100.6(6) . .
O115 W11 O116 89.6(6) . .
O101 W11 O116 159.3(6) . .
O11T W11 O112 102.5(6) . .
O115 W11 O112 157.5(5) . .
O101 W11 O112 86.7(6) . .
O116 W11 O112 87.7(6) . .
O11T W11 O2G2 170.7(5) . .
O115 W11 O2G2 73.6(5) . .
O101 W11 O2G2 86.6(5) . .
O116 W11 O2G2 73.0(5) . .
O112 W11 O2G2 84.2(5) . .
O11T W11 Cs2A 58.7(4) . 1_665
O115 W11 Cs2A 132.7(5) . 1_665
O101 W11 Cs2A 59.6(4) . 1_665
O116 W11 Cs2A 132.9(4) . 1_665
O112 W11 Cs2A 61.0(4) . 1_665
O2G2 W11 Cs2A 130.7(3) . 1_665
O11T W11 Cs2 48.7(5) . 1_665
O115 W11 Cs2 91.4(5) . 1_665
O101 W11 Cs2 51.8(4) . 1_665
O116 W11 Cs2 148.9(4) . 1_665
O112 W11 Cs2 102.3(4) . 1_665
O2G2 W11 Cs2 136.7(3) . 1_665
Cs2A W11 Cs2 41.87(12) 1_665 1_665
O12T W12 O127 101.4(7) . .
O12T W12 O128 101.2(6) . .
O127 W12 O128 91.0(6) . .
O12T W12 O102 100.7(7) . .
O127 W12 O102 157.6(5) . .
O128 W12 O102 88.6(6) . .
O12T W12 O112 100.2(6) . .
O127 W12 O112 88.4(6) . .
O128 W12 O112 158.2(5) . .
O102 W12 O112 83.8(6) . .
O12T W12 O3G2 172.3(7) . .
O127 W12 O3G2 73.2(5) . .
O128 W12 O3G2 73.8(5) . .
O102 W12 O3G2 85.3(5) . .
O112 W12 O3G2 85.3(5) . .
O12T W12 Cs2A 53.3(6) . 1_665
O127 W12 Cs2A 134.9(4) . 1_665
O128 W12 Cs2A 127.0(4) . 1_665
O102 W12 Cs2A 59.1(4) . 1_665
O112 W12 Cs2A 65.1(4) . 1_665
O3G2 W12 Cs2A 134.4(4) . 1_665
O13T W13 O3CC 104.5(6) . .
O13T W13 O134 99.8(6) . .
O3CC W13 O134 93.9(6) . .
O13T W13 O138 101.5(6) . .
O3CC W13 O138 89.5(6) . .
O134 W13 O138 156.8(5) . .
O13T W13 O103 95.4(5) . .
O3CC W13 O103 160.0(5) . .
O134 W13 O103 84.5(6) . .
O138 W13 O103 84.6(6) . .
O13T W13 O1G2 167.3(6) . .
O3CC W13 O1G2 86.7(5) . .
O134 W13 O1G2 72.9(5) . .
O138 W13 O1G2 84.4(5) . .
O103 W13 O1G2 73.8(4) . .
O13T W13 Cs1 77.4(5) . .
O3CC W13 Cs1 128.9(5) . .
O134 W13 Cs1 37.8(4) . .
O138 W13 Cs1 141.1(4) . .
O103 W13 Cs1 57.2(4) . .
O1G2 W13 Cs1 90.9(4) . .
O14T W14 O4C2 103.8(6) . .
O14T W14 O145 101.4(6) . .
O4C2 W14 O145 94.5(5) . .
O14T W14 O134 98.2(6) . .
O4C2 W14 O134 89.7(5) . .
O145 W14 O134 158.4(6) . .
O14T W14 O104 95.6(6) . .
O4C2 W14 O104 159.8(6) . .
O145 W14 O104 86.7(5) . .
O134 W14 O104 82.3(5) . .
O14T W14 O1G2 166.9(5) . .
O4C2 W14 O1G2 85.8(5) . .
O145 W14 O1G2 86.5(5) . .
O134 W14 O1G2 72.7(5) . .
O104 W14 O1G2 74.2(5) . .
O14T W14 Cs1 64.0(4) . .
O4C2 W14 Cs1 131.5(4) . .
O145 W14 Cs1 133.2(4) . .
O134 W14 Cs1 50.3(4) . .
O104 W14 Cs1 53.9(4) . .
O1G2 W14 Cs1 103.0(3) . .
O15T W15 O5C 104.2(6) . .
O15T W15 O145 102.0(7) . .
O5C W15 O145 89.9(6) . .
O15T W15 O156 99.9(6) . .
O5C W15 O156 89.8(6) . .
O145 W15 O156 157.5(6) . .
O15T W15 O115 96.7(6) . .
O5C W15 O115 159.0(6) . .
O145 W15 O115 87.2(5) . .
O156 W15 O115 85.1(6) . .
O15T W15 O2G2 168.9(5) . .
O5C W15 O2G2 85.5(5) . .
O145 W15 O2G2 82.9(5) . .
O156 W15 O2G2 74.7(5) . .
O115 W15 O2G2 73.5(5) . .
O16T W16 O6C 103.4(6) . .
O16T W16 O167 101.3(6) . .
O6C W16 O167 91.5(5) . .
O16T W16 O116 98.0(6) . .
O6C W16 O116 157.8(6) . .
O167 W16 O116 89.9(6) . .
O16T W16 O156 99.5(6) . .
O6C W16 O156 86.6(6) . .
O167 W16 O156 159.0(6) . .
O116 W16 O156 84.2(6) . .
O16T W16 O2G2 169.8(6) . .
O6C W16 O2G2 84.5(5) . .
O167 W16 O2G2 84.6(5) . .
O116 W16 O2G2 73.5(5) . .
O156 W16 O2G2 74.4(5) . .
O17T W17 O7C3 101.7(6) . .
O17T W17 O178 100.0(6) . .
O7C3 W17 O178 91.7(5) . .
O17T W17 O167 98.9(6) . .
O7C3 W17 O167 93.4(5) . .
O178 W17 O167 159.0(6) . .
O17T W17 O127 100.1(6) . .
O7C3 W17 O127 158.1(6) . .
O178 W17 O127 82.9(5) . .
O167 W17 O127 84.8(5) . .
O17T W17 O3G2 171.3(5) . .
O7C3 W17 O3G2 85.0(5) . .
O178 W17 O3G2 74.1(6) . .
O167 W17 O3G2 86.0(5) . .
O127 W17 O3G2 73.1(5) . .
O17T W17 Cs1 56.6(4) . 1_455
O7C3 W17 Cs1 45.7(5) . 1_455
O178 W17 Cs1 105.1(4) . 1_455
O167 W17 Cs1 92.9(4) . 1_455
O127 W17 Cs1 156.0(4) . 1_455
O3G2 W17 Cs1 130.7(3) . 1_455
O17T W17 Cs3 73.1(4) . 2_654
O7C3 W17 Cs3 67.4(4) . 2_654
O178 W17 Cs3 41.6(4) . 2_654
O167 W17 Cs3 156.4(4) . 2_654
O127 W17 Cs3 118.2(4) . 2_654
O3G2 W17 Cs3 105.1(3) . 2_654
Cs1 W17 Cs3 63.94(6) 1_455 2_654
O18T W18 O8CC 104.1(6) . .
O18T W18 O138 100.8(6) . .
O8CC W18 O138 89.4(6) . .
O18T W18 O178 101.4(7) . .
O8CC W18 O178 94.8(6) . .
O138 W18 O178 155.6(5) . .
O18T W18 O128 96.2(5) . .
O8CC W18 O128 159.5(6) . .
O138 W18 O128 84.3(5) . .
O178 W18 O128 83.4(5) . .
O18T W18 O3G2 167.3(5) . .
O8CC W18 O3G2 87.4(5) . .
O138 W18 O3G2 84.3(5) . .
O178 W18 O3G2 72.0(5) . .
O128 W18 O3G2 72.6(4) . .
O18T W18 Na3 24.6(5) . .
O8CC W18 Na3 80.4(5) . .
O138 W18 Na3 94.3(5) . .
O178 W18 Na3 110.1(5) . .
O128 W18 Na3 119.4(4) . .
O3G2 W18 Na3 167.8(4) . .
O18T W18 Cs3A 56.0(5) . .
O8CC W18 Cs3A 68.3(5) . .
O138 W18 Cs3A 139.1(3) . .
O178 W18 Cs3A 63.7(4) . .
O128 W18 Cs3A 127.4(4) . .
O3G2 W18 Cs3A 126.2(3) . .
Na3 W18 Cs3A 49.7(3) . .
O18T W18 Cs3 71.9(5) . 2_654
O8CC W18 Cs3 68.5(5) . 2_654
O138 W18 Cs3 153.3(3) . 2_654
O178 W18 Cs3 46.7(4) . 2_654
O128 W18 Cs3 121.6(4) . 2_654
O3G2 W18 Cs3 108.6(3) . 2_654
Na3 W18 Cs3 68.1(3) . 2_654
Cs3A W18 Cs3 18.37(6) . 2_654
O18T W18 Cs3 42.5(5) . .
O8CC W18 Cs3 70.2(5) . .
O138 W18 Cs3 124.1(3) . .
O178 W18 Cs3 79.6(4) . .
O128 W18 Cs3 129.0(4) . .
O3G2 W18 Cs3 142.1(3) . .
Na3 W18 Cs3 32.9(3) . .
Cs3A W18 Cs3 16.88(5) . .
Cs3 W18 Cs3 35.25(11) 2_654 .
O6CC Ce1 O6C 150.7(4) . .
O6CC Ce1 O7CC 90.6(5) . .
O6C Ce1 O7CC 87.8(5) . .
O6CC Ce1 O5C 84.6(5) . .
O6C Ce1 O5C 83.0(5) . .
O7CC Ce1 O5C 151.4(4) . .
O6CC Ce1 O1AC 95.7(5) . .
O6C Ce1 O1AC 107.0(4) . .
O7CC Ce1 O1AC 132.1(5) . .
O5C Ce1 O1AC 76.4(5) . .
O6CC Ce1 O2AC 131.4(4) . .
O6C Ce1 O2AC 77.8(4) . .
O7CC Ce1 O2AC 88.4(5) . .
O5C Ce1 O2AC 115.7(5) . .
O1AC Ce1 O2AC 53.1(5) . .
O6CC Ce1 O67 65.6(4) . .
O6C Ce1 O67 137.5(5) . .
O7CC Ce1 O67 64.2(4) . .
O5C Ce1 O67 136.2(5) . .
O1AC Ce1 O67 75.6(4) . .
O2AC Ce1 O67 70.5(4) . .
O6CC Ce1 O4G2 75.2(4) . .
O6C Ce1 O4G2 76.0(4) . .
O7CC Ce1 O4G2 76.3(4) . .
O5C Ce1 O4G2 75.3(4) . .
O1AC Ce1 O4G2 150.9(5) . .
O2AC Ce1 O4G2 150.0(4) . .
O67 Ce1 O4G2 122.4(4) . .
O6CC Ce1 C1 115.1(5) . .
O6C Ce1 C1 92.5(5) . .
O7CC Ce1 C1 111.9(6) . .
O5C Ce1 C1 95.5(6) . .
O1AC Ce1 C1 25.9(6) . .
O2AC Ce1 C1 27.2(6) . .
O67 Ce1 C1 71.6(5) . .
O4G2 Ce1 C1 165.9(5) . .
O6CC Ce1 W7 82.3(4) . .
O6C Ce1 W7 109.1(4) . .
O7CC Ce1 W7 30.1(3) . .
O5C Ce1 W7 166.8(3) . .
O1AC Ce1 W7 104.0(4) . .
O2AC Ce1 W7 73.2(3) . .
O67 Ce1 W7 34.9(3) . .
O4G2 Ce1 W7 102.0(3) . .
C1 Ce1 W7 89.3(5) . .
O6CC Ce1 W6 30.5(3) . .
O6C Ce1 W6 169.5(4) . .
O7CC Ce1 W6 81.7(3) . .
O5C Ce1 W6 106.3(3) . .
O1AC Ce1 W6 80.4(3) . .
O2AC Ce1 W6 101.8(3) . .
O67 Ce1 W6 36.0(3) . .
O4G2 Ce1 W6 101.3(2) . .
C1 Ce1 W6 91.5(4) . .
W7 Ce1 W6 61.21(3) . .
O6CC Ce1 Cu3 81.9(3) . .
O6C Ce1 Cu3 77.8(3) . .
O7CC Ce1 Cu3 41.1(3) . .
O5C Ce1 Cu3 110.4(3) . .
O1AC Ce1 Cu3 172.4(4) . .
O2AC Ce1 Cu3 123.8(4) . .
O67 Ce1 Cu3 96.9(3) . .
O4G2 Ce1 Cu3 35.2(3) . .
C1 Ce1 Cu3 150.6(5) . .
W7 Ce1 Cu3 68.56(4) . .
W6 Ce1 Cu3 94.16(4) . .
O4C1 Cu1 O9C1 87.9(6) . .
O4C1 Cu1 O8CC 175.5(5) . .
O9C1 Cu1 O8CC 92.4(6) . .
O4C1 Cu1 O3CC 93.5(6) . .
O9C1 Cu1 O3CC 174.7(5) . .
O8CC Cu1 O3CC 85.8(6) . .
O4C1 Cu1 O4G1 91.0(4) . .
O9C1 Cu1 O4G1 91.4(5) . .
O8CC Cu1 O4G1 84.5(4) . .
O3CC Cu1 O4G1 83.4(5) . .
O4C1 Cu1 O1CU 87.2(5) . .
O9C1 Cu1 O1CU 88.2(6) . .
O8CC Cu1 O1CU 97.3(5) . .
O3CC Cu1 O1CU 97.0(6) . .
O4G1 Cu1 O1CU 178.1(4) . .
O4C2 Cu2 O5C2 92.5(6) . .
O4C2 Cu2 O4G1 171.1(5) . .
O5C2 Cu2 O4G1 95.8(5) . .
O4C2 Cu2 O4G2 92.6(5) . .
O5C2 Cu2 O4G2 172.0(5) . .
O4G1 Cu2 O4G2 79.5(5) . .
O4C2 Cu2 O6CC 92.2(5) . .
O5C2 Cu2 O6CC 88.7(5) . .
O4G1 Cu2 O6CC 91.0(5) . .
O4G2 Cu2 O6CC 85.0(4) . .
O4C2 Cu2 O3CC 92.7(5) . .
O5C2 Cu2 O3CC 95.3(5) . .
O4G1 Cu2 O3CC 83.6(5) . .
O4G2 Cu2 O3CC 90.6(4) . .
O6CC Cu2 O3CC 173.5(5) . .
O4C2 Cu2 Ce1 91.6(3) . .
O5C2 Cu2 Ce1 126.0(3) . .
O4G1 Cu2 Ce1 86.0(3) . .
O4G2 Cu2 Ce1 47.7(3) . .
O6CC Cu2 Ce1 37.3(3) . .
O3CC Cu2 Ce1 138.2(3) . .
O8C3 Cu3 O7C3 92.1(6) . .
O8C3 Cu3 O4G1 95.4(5) . .
O7C3 Cu3 O4G1 172.0(6) . .
O8C3 Cu3 O4G2 171.8(5) . .
O7C3 Cu3 O4G2 92.4(6) . .
O4G1 Cu3 O4G2 80.5(5) . .
O8C3 Cu3 O8CC 94.1(5) . .
O7C3 Cu3 O8CC 92.1(5) . .
O4G1 Cu3 O8CC 84.8(4) . .
O4G2 Cu3 O8CC 92.6(5) . .
O8C3 Cu3 O7CC 86.1(5) . .
O7C3 Cu3 O7CC 91.8(4) . .
O4G1 Cu3 O7CC 91.3(4) . .
O4G2 Cu3 O7CC 86.8(5) . .
O8CC Cu3 O7CC 176.1(4) . .
O8C3 Cu3 Ce1 124.8(4) . .
O7C3 Cu3 Ce1 91.0(4) . .
O4G1 Cu3 Ce1 86.9(3) . .
O4G2 Cu3 Ce1 48.2(3) . .
O8CC Cu3 Ce1 140.8(4) . .
O7CC Cu3 Ce1 38.7(4) . .
O8C3 Cu3 Cs1 57.5(4) . 1_455
O7C3 Cu3 Cs1 46.9(4) . 1_455
O4G1 Cu3 Cs1 140.5(4) . 1_455
O4G2 Cu3 Cs1 122.0(3) . 1_455
O8CC Cu3 Cs1 122.0(4) . 1_455
O7CC Cu3 Cs1 61.3(3) . 1_455
Ce1 Cu3 Cs1 87.24(6) . 1_455
O8C3 Cu3 Cs3 42.8(4) . 2_654
O7C3 Cu3 Cs3 66.7(4) . 2_654
O4G1 Cu3 Cs3 117.8(4) . 2_654
O4G2 Cu3 Cs3 145.4(3) . 2_654
O8CC Cu3 Cs3 62.6(4) . 2_654
O7CC Cu3 Cs3 119.5(4) . 2_654
Ce1 Cu3 Cs3 150.58(9) . 2_654
Cs1 Cu3 Cs3 63.61(7) 1_455 2_654
O4G1 Ge1 O2G1 111.6(5) . .
O4G1 Ge1 O1G1 110.7(6) . .
O2G1 Ge1 O1G1 109.0(5) . .
O4G1 Ge1 O3G1 111.6(6) . .
O2G1 Ge1 O3G1 106.9(6) . .
O1G1 Ge1 O3G1 106.9(6) . .
O2G2 Ge2 O1G2 107.3(6) . .
O2G2 Ge2 O3G2 107.5(6) . .
O1G2 Ge2 O3G2 104.0(6) . .
O2G2 Ge2 O4G2 111.6(5) . .
O1G2 Ge2 O4G2 112.8(6) . .
O3G2 Ge2 O4G2 113.2(6) . .
W1 O1T Na4 156.1(10) . .
W1 O1T Cs2A 99.4(6) . .
Na4 O1T Cs2A 103.9(8) . .
W1 O1T Cs2 106.9(5) . .
Na4 O1T Cs2 91.6(6) . .
Cs2A O1T Cs2 52.4(3) . .
W2 O2T Cs2 107.5(6) . .
W2 O2T Cs2A 96.5(5) . .
Cs2 O2T Cs2A 53.6(2) . .
W3 O3T Cs2A 98.7(7) . .
W5 O5T K1 114.1(6) . 1_655
W7 O7T Na2 142.7(8) . 1_455
W7 O7T Cs1 91.3(4) . 1_455
Na2 O7T Cs1 84.0(4) 1_455 1_455
W8 O8T Na3 129.3(8) . 2_654
W8 O8T Cs1 99.1(6) . 1_455
Na3 O8T Cs1 84.9(5) 2_654 1_455
W8 O8T Cs3 87.1(5) . 2_654
Na3 O8T Cs3 43.5(5) 2_654 2_654
Cs1 O8T Cs3 79.9(3) 1_455 2_654
W9 O9T Cs3 93.8(5) . .
W10 O10T Na4 157.2(8) . 1_665
W10 O10T Cs2A 99.1(6) . 1_665
Na4 O10T Cs2A 101.6(6) 1_665 1_665
W10 O10T Cs2 107.9(5) . 1_665
Na4 O10T Cs2 92.2(6) 1_665 1_665
Cs2A O10T Cs2 54.0(3) 1_665 1_665
W11 O11T Cs2 107.1(6) . 1_665
W11 O11T Cs2A 95.7(5) . 1_665
Cs2 O11T Cs2A 51.4(2) 1_665 1_665
W12 O12T Cs2A 100.8(7) . 1_665
W13 O13T Na3 137.6(8) . 2_754
W14 O14T Na2 156.9(8) . .
W14 O14T Cs1 89.8(5) . .
Na2 O14T Cs1 90.4(5) . .
W15 O15T Na1 105.1(7) . .
W17 O17T Na4 141.0(10) . 1_565
W17 O17T Cs1 97.3(5) . 1_455
Na4 O17T Cs1 113.8(7) 1_565 1_455
W18 O18T Na3 136.9(8) . .
W18 O18T Cs3 117.5(6) . .
Na3 O18T Cs3 45.4(6) . .
W18 O18T Cs3A 99.4(5) . .
Na3 O18T Cs3A 67.1(7) . .
Cs3 O18T Cs3A 22.08(12) . .
Ge2 O4G2 Cu3 118.3(7) . .
Ge2 O4G2 Cu2 118.4(7) . .
Cu3 O4G2 Cu2 98.5(5) . .
Ge2 O4G2 Ce1 123.0(5) . .
Cu3 O4G2 Ce1 96.6(5) . .
Cu2 O4G2 Ce1 96.7(4) . .
W2 O23 W3 150.8(8) . .
W2 O23 K1 109.8(5) . .
W3 O23 K1 99.1(6) . .
W2 O23 Cs2A 87.0(4) . .
W3 O23 Cs2A 86.9(4) . .
K1 O23 Cs2A 110.0(4) . .
W7 O27 W2 119.2(6) . .
W7 O27 K1 101.1(5) . .
W2 O27 K1 100.9(5) . .
W9 O49 W4 142.5(7) . .
W10 O104 W14 119.3(8) . .
W10 O104 Cs1 112.5(5) . .
W14 O104 Cs1 95.1(4) . .
W7 O67 W6 121.0(6) . .
W7 O67 Ce1 98.1(5) . .
W6 O67 Ce1 96.9(5) . .
W11 O101 W10 150.3(9) . .
W11 O101 Cs2 101.2(5) . 1_665
W10 O101 Cs2 100.2(5) . 1_665
W11 O101 Cs2A 92.5(4) . 1_665
W10 O101 Cs2A 85.3(4) . 1_665
Cs2 O101 Cs2A 50.8(2) 1_665 1_665
W16 O6C Ce1 147.0(8) . .
W11 O115 W15 120.9(8) . .
W3 O13 W1 156.7(7) . .
W3 O13 Cs2A 91.6(5) . .
W1 O13 Cs2A 90.3(4) . .
W14 O4C2 Cu2 143.1(7) . .
W11 O116 W16 122.0(6) . .
W18 O8CC Cu1 131.8(7) . .
W18 O8CC Cu3 129.4(6) . .
Cu1 O8CC Cu3 96.0(5) . .
W11 O112 W12 153.1(8) . .
W11 O112 Cs2A 90.8(5) . 1_665
W12 O112 Cs2A 85.1(4) . 1_665
W1 O14 W4 120.4(6) . .
Ge1 O3G1 W8 121.5(6) . .
Ge1 O3G1 W9 122.3(6) . .
W8 O3G1 W9 93.5(5) . .
Ge1 O3G1 W3 124.2(6) . .
W8 O3G1 W3 94.0(5) . .
W9 O3G1 W3 93.4(4) . .
W8 O8C3 Cu3 149.5(8) . .
W8 O8C3 Cs3 97.6(6) . 2_654
Cu3 O8C3 Cs3 112.4(5) . 2_654
W8 O8C3 Cs1 95.2(5) . 1_455
Cu3 O8C3 Cs1 93.0(4) . 1_455
Cs3 O8C3 Cs1 84.2(3) 2_654 1_455
W8 O8C3 Cs3A 94.2(5) . .
Cu3 O8C3 Cs3A 112.2(5) . .
Cs3 O8C3 Cs3A 20.06(11) 2_654 .
Cs1 O8C3 Cs3A 104.2(4) 1_455 .
W7 O7CC Ce1 113.0(6) . .
W7 O7CC Cu3 135.8(6) . .
Ce1 O7CC Cu3 100.2(5) . .
W7 O7CC Cs1 98.2(5) . 1_455
Ce1 O7CC Cs1 127.0(4) . 1_455
Cu3 O7CC Cs1 83.0(4) . 1_455
W13 O3CC Cu1 131.0(7) . .
W13 O3CC Cu2 129.8(7) . .
Cu1 O3CC Cu2 97.0(5) . .
W1 O15 W5 119.9(7) . .
W9 O9C1 Cu1 148.1(8) . .
W9 O9C1 Cs3 92.2(6) . .
Cu1 O9C1 Cs3 119.5(5) . .
W9 O9C1 Cs3A 96.1(6) . .
Cu1 O9C1 Cs3A 114.6(5) . .
Cs3 O9C1 Cs3A 21.74(11) . .
W2 O26 W6 122.0(6) . .
W15 O156 W16 117.7(6) . .
W15 O145 W14 151.5(9) . .
W3 O39 W9 121.5(7) . .
W12 O128 W18 121.6(6) . .
W16 O167 W17 151.3(7) . .
W2 O12 W1 150.3(8) . .
W2 O12 Cs2 97.7(4) . .
W1 O12 Cs2 103.0(4) . .
W2 O12 Cs2A 88.8(5) . .
W1 O12 Cs2A 88.0(4) . .
Cs2 O12 Cs2A 51.0(2) . .
W12 O127 W17 119.7(7) . .
W7 O78 W8 151.5(8) . .
W7 O78 K1 104.5(5) . .
W8 O78 K1 103.2(6) . .
W7 O78 Cs1 91.3(4) . 1_455
W8 O78 Cs1 81.9(4) . 1_455
K1 O78 Cs1 117.5(4) . 1_455
W5 O5C2 Cu2 148.0(8) . .
W3 O38 W8 120.3(8) . .
W3 O38 K1 104.6(5) . .
W8 O38 K1 110.0(5) . .
W5 O45 W4 119.5(7) . .
W6 O56 W5 152.1(6) . .
W6 O6CC Ce1 113.4(6) . .
W6 O6CC Cu2 133.3(6) . .
Ce1 O6CC Cu2 103.0(5) . .
Ge2 O2G2 W15 123.1(6) . .
Ge2 O2G2 W16 122.2(7) . .
W15 O2G2 W16 92.9(4) . .
Ge2 O2G2 W11 125.9(5) . .
W15 O2G2 W11 91.9(5) . .
W16 O2G2 W11 91.5(4) . .
W15 O5C Ce1 142.7(7) . .
W18 O138 W13 146.8(6) . .
Ge2 O3G2 W17 119.7(6) . .
Ge2 O3G2 W18 123.6(6) . .
W17 O3G2 W18 93.3(5) . .
Ge2 O3G2 W12 125.7(7) . .
W17 O3G2 W12 94.0(5) . .
W18 O3G2 W12 92.1(4) . .
Ge2 O1G2 W14 119.0(5) . .
Ge2 O1G2 W13 124.2(7) . .
W14 O1G2 W13 94.3(4) . .
Ge2 O1G2 W10 126.0(6) . .
W14 O1G2 W10 93.3(5) . .
W13 O1G2 W10 91.6(4) . .
Ge1 O4G1 Cu3 122.3(7) . .
Ge1 O4G1 Cu2 122.6(6) . .
Cu3 O4G1 Cu2 101.3(5) . .
Ge1 O4G1 Cu1 115.2(5) . .
Cu3 O4G1 Cu1 93.9(4) . .
Cu2 O4G1 Cu1 95.0(5) . .
W17 O7C3 Cu3 143.4(7) . .
W17 O7C3 Cs1 109.3(6) . 1_455
Cu3 O7C3 Cs1 104.6(5) . 1_455
Ge1 O2G1 W7 123.2(6) . .
Ge1 O2G1 W6 120.7(7) . .
W7 O2G1 W6 95.9(4) . .
Ge1 O2G1 W2 125.2(6) . .
W7 O2G1 W2 92.0(4) . .
W6 O2G1 W2 91.4(4) . .
W17 O178 W18 119.7(8) . .
W17 O178 Cs3 114.2(6) . 2_654
W18 O178 Cs3 106.3(5) . 2_654
W17 O178 Cs3A 132.9(6) . .
W18 O178 Cs3A 87.9(4) . .
Cs3 O178 Cs3A 20.25(11) 2_654 .
W13 O134 W14 119.4(7) . .
W13 O134 Cs1 119.7(5) . .
W14 O134 Cs1 99.3(6) . .
Ge1 O1G1 W5 121.3(6) . .
Ge1 O1G1 W4 122.6(6) . .
W5 O1G1 W4 94.7(5) . .
Ge1 O1G1 W1 123.5(6) . .
W5 O1G1 W1 93.8(4) . .
W4 O1G1 W1 93.1(4) . .
W4 O4C1 Cu1 148.0(9) . .
Cu1 O1CU Na3 108.9(8) . .
C1 O1AC Ce1 95.8(14) . .
C1 O1AC Na1 140.1(14) . .
Ce1 O1AC Na1 116.8(6) . .
C1 O2AC Na2 135.2(13) . 1_455
C1 O2AC Ce1 90.3(13) . .
Na2 O2AC Ce1 132.8(6) 1_455 .
W10 O103 W13 119.9(6) . .
W10 O103 Cs1 96.1(5) . .
W13 O103 Cs1 94.9(4) . .
W8 O89 W9 120.5(8) . .
W8 O89 Cs3A 108.2(5) . .
W9 O89 Cs3A 102.4(5) . .
W8 O89 Cs3 86.6(4) . 2_654
W9 O89 Cs3 119.7(5) . 2_654
Cs3A O89 Cs3 22.30(10) . 2_654
W8 O89 Cs3 129.0(5) . .
W9 O89 Cs3 84.7(4) . .
Cs3A O89 Cs3 21.79(10) . .
Cs3 O89 Cs3 44.09(19) 2_654 .
W12 O102 W10 154.0(7) . .
W12 O102 Cs2A 91.2(4) . 1_665
W10 O102 Cs2A 90.4(5) . 1_665
O1AC C1 O2AC 120.7(18) . .
O1AC C1 C2 118(2) . .
O2AC C1 C2 121(2) . .
O1AC C1 Ce1 58.3(10) . .
O2AC C1 Ce1 62.5(10) . .
C2 C1 Ce1 176(2) . .
C1 C2 H2A 109.5 . .
C1 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C1 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
O7C3 Cs1 O1W 86.8(5) 1_655 .
O7C3 Cs1 O134 169.4(3) 1_655 .
O1W Cs1 O134 103.8(5) . .
O7C3 Cs1 O104 137.9(3) 1_655 .
O1W Cs1 O104 66.5(5) . .
O134 Cs1 O104 50.4(3) . .
O7C3 Cs1 O8T 98.6(4) 1_655 1_655
O1W Cs1 O8T 150.3(5) . 1_655
O134 Cs1 O8T 71.6(3) . 1_655
O104 Cs1 O8T 120.9(4) . 1_655
O7C3 Cs1 O17T 50.9(3) 1_655 1_655
O1W Cs1 O17T 90.6(5) . 1_655
O134 Cs1 O17T 128.9(4) . 1_655
O104 Cs1 O17T 95.5(3) . 1_655
O8T Cs1 O17T 115.5(3) 1_655 1_655
O7C3 Cs1 O8C3 52.4(3) 1_655 1_655
O1W Cs1 O8C3 121.6(5) . 1_655
O134 Cs1 O8C3 119.0(3) . 1_655
O104 Cs1 O8C3 169.3(4) . 1_655
O8T Cs1 O8C3 48.5(4) 1_655 1_655
O17T Cs1 O8C3 91.4(3) 1_655 1_655
O7C3 Cs1 O7CC 56.2(3) 1_655 1_655
O1W Cs1 O7CC 72.7(5) . 1_655
O134 Cs1 O7CC 125.4(3) . 1_655
O104 Cs1 O7CC 133.9(3) . 1_655
O8T Cs1 O7CC 86.1(3) 1_655 1_655
O17T Cs1 O7CC 105.7(3) 1_655 1_655
O8C3 Cs1 O7CC 50.8(3) 1_655 1_655
O7C3 Cs1 O14T 138.7(4) 1_655 .
O1W Cs1 O14T 57.4(5) . .
O134 Cs1 O14T 50.3(4) . .
O104 Cs1 O14T 49.0(3) . .
O8T Cs1 O14T 103.8(3) 1_655 .
O17T Cs1 O14T 137.9(3) 1_655 .
O8C3 Cs1 O14T 127.5(3) 1_655 .
O7CC Cs1 O14T 91.0(3) 1_655 .
O7C3 Cs1 O7W 91.1(5) 1_655 2_754
O1W Cs1 O7W 134.2(6) . 2_754
O134 Cs1 O7W 82.5(5) . 2_754
O104 Cs1 O7W 86.0(5) . 2_754
O8T Cs1 O7W 75.1(5) 1_655 2_754
O17T Cs1 O7W 54.9(5) 1_655 2_754
O8C3 Cs1 O7W 91.4(5) 1_655 2_754
O7CC Cs1 O7W 139.5(4) 1_655 2_754
O14T Cs1 O7W 127.9(5) . 2_754
O7C3 Cs1 O103 132.0(3) 1_655 .
O1W Cs1 O103 111.1(5) . .
O134 Cs1 O103 45.4(3) . .
O104 Cs1 O103 46.2(3) . .
O8T Cs1 O103 86.9(3) 1_655 .
O17T Cs1 O103 83.6(3) 1_655 .
O8C3 Cs1 O103 127.1(3) 1_655 .
O7CC Cs1 O103 170.2(3) 1_655 .
O14T Cs1 O103 83.9(3) . .
O7W Cs1 O103 44.1(5) 2_754 .
O7C3 Cs1 O78 86.5(3) 1_655 1_655
O1W Cs1 O78 104.6(5) . 1_655
O134 Cs1 O78 89.6(3) . 1_655
O104 Cs1 O78 130.2(3) . 1_655
O8T Cs1 O78 47.3(3) 1_655 1_655
O17T Cs1 O78 134.2(3) 1_655 1_655
O8C3 Cs1 O78 43.8(3) 1_655 1_655
O7CC Cs1 O78 43.5(3) 1_655 1_655
O14T Cs1 O78 84.0(3) . 1_655
O7W Cs1 O78 120.9(4) 2_754 1_655
O103 Cs1 O78 127.2(3) . 1_655
Cs2A Cs2 O2T 66.0(3) . .
Cs2A Cs2 O4W 110.8(3) . .
O2T Cs2 O4W 150.6(4) . .
Cs2A Cs2 O10T 62.2(3) . 1_445
O2T Cs2 O10T 128.1(4) . 1_445
O4W Cs2 O10T 59.4(4) . 1_445
Cs2A Cs2 O11T 68.8(3) . 1_445
O2T Cs2 O11T 58.5(3) . 1_445
O4W Cs2 O11T 150.0(4) . 1_445
O10T Cs2 O11T 98.4(4) 1_445 1_445
Cs2A Cs2 O13W 124.3(8) . .
O2T Cs2 O13W 89.2(8) . .
O4W Cs2 O13W 68.1(8) . .
O10T Cs2 O13W 122.8(7) 1_445 .
O11T Cs2 O13W 138.5(7) 1_445 .
Cs2A Cs2 O101 68.4(3) . 1_445
O2T Cs2 O101 105.2(4) . 1_445
O4W Cs2 O101 99.8(4) . 1_445
O10T Cs2 O101 51.9(3) 1_445 1_445
O11T Cs2 O101 51.1(3) 1_445 1_445
O13W Cs2 O101 164.4(8) . 1_445
Cs2A Cs2 O12 67.1(3) . .
O2T Cs2 O12 51.9(3) . .
O4W Cs2 O12 99.1(3) . .
O10T Cs2 O12 107.8(3) 1_445 .
O11T Cs2 O12 107.4(3) 1_445 .
O13W Cs2 O12 58.8(8) . .
O101 Cs2 O12 135.3(4) 1_445 .
Cs2A Cs2 O1T 61.5(3) . .
O2T Cs2 O1T 96.9(3) . .
O4W Cs2 O1T 60.0(4) . .
O10T Cs2 O1T 61.4(3) 1_445 .
O11T Cs2 O1T 130.2(4) 1_445 .
O13W Cs2 O1T 74.2(7) . .
O101 Cs2 O1T 109.0(3) 1_445 .
O12 Cs2 O1T 50.3(3) . .
Cs2A Cs2 W2 66.24(11) . .
O2T Cs2 W2 24.3(2) . .
O4W Cs2 W2 126.3(3) . .
O10T Cs2 W2 123.9(3) 1_445 .
O11T Cs2 W2 82.0(2) 1_445 .
O13W Cs2 W2 71.9(8) . .
O101 Cs2 W2 123.6(3) 1_445 .
O12 Cs2 W2 27.9(2) . .
O1T Cs2 W2 75.9(2) . .
Cs2A Cs2 W11 68.12(12) . 1_445
O2T Cs2 W11 81.2(3) . 1_445
O4W Cs2 W11 126.1(3) . 1_445
O10T Cs2 W11 77.0(3) 1_445 1_445
O11T Cs2 W11 24.2(2) 1_445 1_445
O13W Cs2 W11 159.2(7) . 1_445
O101 Cs2 W11 27.1(2) 1_445 1_445
O12 Cs2 W11 124.8(3) . 1_445
O1T Cs2 W11 125.0(3) . 1_445
W2 Cs2 W11 103.21(8) . 1_445
Cs2A Cs2 W10 64.14(11) . 1_445
O2T Cs2 W10 122.1(3) . 1_445
O4W Cs2 W10 76.2(3) . 1_445
O10T Cs2 W10 23.9(3) 1_445 1_445
O11T Cs2 W10 77.2(2) 1_445 1_445
O13W Cs2 W10 144.0(7) . 1_445
O101 Cs2 W10 28.1(2) 1_445 1_445
O12 Cs2 W10 124.9(2) . 1_445
O1T Cs2 W10 83.9(3) . 1_445
W2 Cs2 W10 130.24(10) . 1_445
W11 Cs2 W10 54.25(4) 1_445 1_445
O8W Cs2A Cs2 129.4(7) . .
O8W Cs2A O3W 118.6(8) . .
Cs2 Cs2A O3W 112.0(5) . .
O8W Cs2A O12T 66.4(8) . 1_445
Cs2 Cs2A O12T 146.3(3) . 1_445
O3W Cs2A O12T 64.2(5) . 1_445
O8W Cs2A O10T 74.4(7) . 1_445
Cs2 Cs2A O10T 63.8(3) . 1_445
O3W Cs2A O10T 148.5(5) . 1_445
O12T Cs2A O10T 101.2(4) 1_445 1_445
O8W Cs2A O1T 70.4(8) . .
Cs2 Cs2A O1T 66.1(3) . .
O3W Cs2A O1T 146.5(5) . .
O12T Cs2A O1T 136.7(4) 1_445 .
O10T Cs2A O1T 63.3(4) 1_445 .
O8W Cs2A O3T 62.5(7) . .
Cs2 Cs2A O3T 147.7(3) . .
O3W Cs2A O3T 64.2(5) . .
O12T Cs2A O3T 63.9(4) 1_445 .
O10T Cs2A O3T 136.9(4) 1_445 .
O1T Cs2A O3T 98.9(4) . .
O8W Cs2A O2T 150.6(6) . .
Cs2 Cs2A O2T 60.4(3) . .
O3W Cs2A O2T 59.4(5) . .
O12T Cs2A O2T 123.3(4) 1_445 .
O10T Cs2A O2T 124.1(4) 1_445 .
O1T Cs2A O2T 96.4(4) . .
O3T Cs2A O2T 95.3(3) . .
O8W Cs2A O102 70.8(6) . 1_445
Cs2 Cs2A O102 101.6(3) . 1_445
O3W Cs2A O102 102.5(5) . 1_445
O12T Cs2A O102 51.3(4) 1_445 1_445
O10T Cs2A O102 52.2(4) 1_445 1_445
O1T Cs2A O102 110.7(4) . 1_445
O3T Cs2A O102 110.6(4) . 1_445
O2T Cs2A O102 138.2(3) . 1_445
O8W Cs2A O13 66.6(6) . .
Cs2 Cs2A O13 102.6(3) . .
O3W Cs2A O13 100.2(4) . .
O12T Cs2A O13 111.1(4) 1_445 .
O10T Cs2A O13 111.2(4) 1_445 .
O1T Cs2A O13 51.3(4) . .
O3T Cs2A O13 50.7(4) . .
O2T Cs2A O13 84.5(3) . .
O102 Cs2A O13 137.3(4) 1_445 .
O8W Cs2A O12 106.7(7) . .
Cs2 Cs2A O12 61.9(3) . .
O3W Cs2A O12 98.1(5) . .
O12T Cs2A O12 149.5(4) 1_445 .
O10T Cs2A O12 105.4(4) 1_445 .
O1T Cs2A O12 50.1(3) . .
O3T Cs2A O12 86.3(4) . .
O2T Cs2A O12 49.4(3) . .
O102 Cs2A O12 157.5(4) 1_445 .
O13 Cs2A O12 44.7(3) . .
O8W Cs2A O11T 153.9(7) . 1_445
Cs2 Cs2A O11T 59.8(3) . 1_445
O3W Cs2A O11T 61.2(5) . 1_445
O12T Cs2A O11T 93.8(4) 1_445 1_445
O10T Cs2A O11T 94.2(4) 1_445 1_445
O1T Cs2A O11T 125.9(4) . 1_445
O3T Cs2A O11T 125.3(4) . 1_445
O2T Cs2A O11T 54.6(3) . 1_445
O102 Cs2A O11T 83.6(3) 1_445 1_445
O13 Cs2A O11T 139.1(4) . 1_445
O12 Cs2A O11T 98.9(4) . 1_445
Cs3A Cs3 Na3 121.2(5) . .
Cs3A Cs3 Cs3 0.00(19) . 2_654
Na3 Cs3 Cs3 121.2(5) . 2_654
Cs3A Cs3 O178 104.1(3) . 2_654
Na3 Cs3 O178 134.1(5) . 2_654
Cs3 Cs3 O178 104.1(3) 2_654 2_654
Cs3A Cs3 O7W 151.6(6) . .
Na3 Cs3 O7W 46.3(7) . .
Cs3 Cs3 O7W 151.6(6) 2_654 .
O178 Cs3 O7W 89.9(6) 2_654 .
Cs3A Cs3 O8C3 104.0(3) . 2_654
Na3 Cs3 O8C3 94.0(5) . 2_654
Cs3 Cs3 O8C3 104.0(3) 2_654 2_654
O178 Cs3 O8C3 81.1(4) 2_654 2_654
O7W Cs3 O8C3 102.5(5) . 2_654
Cs3A Cs3 O9T 114.6(3) . .
Na3 Cs3 O9T 91.3(5) . .
Cs3 Cs3 O9T 114.6(3) 2_654 .
O178 Cs3 O9T 61.2(4) 2_654 .
O7W Cs3 O9T 51.3(5) . .
O8C3 Cs3 O9T 130.8(4) 2_654 .
Cs3A Cs3 O9C1 86.0(3) . .
Na3 Cs3 O9C1 73.0(5) . .
Cs3 Cs3 O9C1 86.0(3) 2_654 .
O178 Cs3 O9C1 105.4(3) 2_654 .
O7W Cs3 O9C1 66.3(5) . .
O8C3 Cs3 O9C1 166.6(4) 2_654 .
O9T Cs3 O9C1 48.6(4) . .
Cs3A Cs3 O18T 80.5(3) . .
Na3 Cs3 O18T 41.7(5) . .
Cs3 Cs3 O18T 80.5(3) 2_654 .
O178 Cs3 O18T 175.0(3) 2_654 .
O7W Cs3 O18T 86.6(6) . .
O8C3 Cs3 O18T 96.1(4) 2_654 .
O9T Cs3 O18T 118.7(4) . .
O9C1 Cs3 O18T 76.4(3) . .
Cs3A Cs3 O89 69.5(2) . 2_654
Na3 Cs3 O89 83.9(5) . 2_654
Cs3 Cs3 O89 69.5(2) 2_654 2_654
O178 Cs3 O89 121.5(4) 2_654 2_654
O7W Cs3 O89 123.7(5) . 2_654
O8C3 Cs3 O89 48.4(3) 2_654 2_654
O9T Cs3 O89 175.0(4) . 2_654
O9C1 Cs3 O89 130.6(3) . 2_654
O18T Cs3 O89 58.1(4) . 2_654
Cs3A Cs3 O8T 114.5(3) . 2_654
Na3 Cs3 O8T 47.7(5) . 2_654
Cs3 Cs3 O8T 114.5(3) 2_654 2_654
O178 Cs3 O8T 120.6(4) 2_654 2_654
O7W Cs3 O8T 76.9(5) . 2_654
O8C3 Cs3 O8T 47.7(4) 2_654 2_654
O9T Cs3 O8T 127.8(4) . 2_654
O9C1 Cs3 O8T 120.0(4) . 2_654
O18T Cs3 O8T 55.1(3) . 2_654
O89 Cs3 O8T 47.3(3) 2_654 2_654
Cs3A Cs3 O89 66.4(2) . .
Na3 Cs3 O89 119.3(5) . .
Cs3 Cs3 O89 66.4(2) 2_654 .
O178 Cs3 O89 70.7(3) 2_654 .
O7W Cs3 O89 96.3(5) . .
O8C3 Cs3 O89 146.0(4) 2_654 .
O9T Cs3 O89 48.3(3) . .
O9C1 Cs3 O89 46.5(3) . .
O18T Cs3 O89 113.2(3) . .
O89 Cs3 O89 135.91(19) 2_654 .
O8T Cs3 O89 166.3(4) 2_654 .
Cs3 Cs3A Cs3 180.0(3) . 2_654
Cs3 Cs3A O89 91.8(2) . .
Cs3 Cs3A O89 88.2(2) 2_654 .
Cs3 Cs3A O89 88.2(2) . 2_654
Cs3 Cs3A O89 91.8(2) 2_654 2_654
O89 Cs3A O89 180.0(3) . 2_654
Cs3 Cs3A Na3 38.9(4) . .
Cs3 Cs3A Na3 141.1(4) 2_654 .
O89 Cs3A Na3 104.5(4) . .
O89 Cs3A Na3 75.5(4) 2_654 .
Cs3 Cs3A Na3 141.1(4) . 2_654
Cs3 Cs3A Na3 38.9(4) 2_654 2_654
O89 Cs3A Na3 75.5(4) . 2_654
O89 Cs3A Na3 104.5(4) 2_654 2_654
Na3 Cs3A Na3 180.0(6) . 2_654
Cs3 Cs3A O18T 102.6(3) . 2_654
Cs3 Cs3A O18T 77.4(3) 2_654 2_654
O89 Cs3A O18T 59.8(4) . 2_654
O89 Cs3A O18T 120.2(4) 2_654 2_654
Na3 Cs3A O18T 140.8(4) . 2_654
Na3 Cs3A O18T 39.2(4) 2_654 2_654
Cs3 Cs3A O18T 77.4(3) . .
Cs3 Cs3A O18T 102.6(3) 2_654 .
O89 Cs3A O18T 120.2(4) . .
O89 Cs3A O18T 59.8(4) 2_654 .
Na3 Cs3A O18T 39.2(4) . .
Na3 Cs3A O18T 140.8(4) 2_654 .
O18T Cs3A O18T 180.000(1) 2_654 .
Cs3 Cs3A O9C1 107.7(2) . 2_654
Cs3 Cs3A O9C1 72.3(2) 2_654 2_654
O89 Cs3A O9C1 132.7(3) . 2_654
O89 Cs3A O9C1 47.3(3) 2_654 2_654
Na3 Cs3A O9C1 117.9(4) . 2_654
Na3 Cs3A O9C1 62.1(4) 2_654 2_654
O18T Cs3A O9C1 73.9(3) 2_654 2_654
O18T Cs3A O9C1 106.1(3) . 2_654
Cs3 Cs3A O9C1 72.3(2) . .
Cs3 Cs3A O9C1 107.7(2) 2_654 .
O89 Cs3A O9C1 47.3(3) . .
O89 Cs3A O9C1 132.7(3) 2_654 .
Na3 Cs3A O9C1 62.1(4) . .
Na3 Cs3A O9C1 117.9(4) 2_654 .
O18T Cs3A O9C1 106.1(3) 2_654 .
O18T Cs3A O9C1 73.9(3) . .
O9C1 Cs3A O9C1 180.0(3) 2_654 .
Cs3 Cs3A O178 55.6(3) . 2_654
Cs3 Cs3A O178 124.4(3) 2_654 2_654
O89 Cs3A O178 67.7(3) . 2_654
O89 Cs3A O178 112.3(3) 2_654 2_654
Na3 Cs3A O178 94.3(4) . 2_654
Na3 Cs3A O178 85.7(4) 2_654 2_654
O18T Cs3A O178 47.0(3) 2_654 2_654
O18T Cs3A O178 133.0(3) . 2_654
O9C1 Cs3A O178 88.2(3) 2_654 2_654
O9C1 Cs3A O178 91.8(3) . 2_654
Cs3 Cs3A O178 124.4(3) . .
Cs3 Cs3A O178 55.6(3) 2_654 .
O89 Cs3A O178 112.3(3) . .
O89 Cs3A O178 67.7(3) 2_654 .
Na3 Cs3A O178 85.7(4) . .
Na3 Cs3A O178 94.3(4) 2_654 .
O18T Cs3A O178 133.0(3) 2_654 .
O18T Cs3A O178 47.0(3) . .
O9C1 Cs3A O178 91.8(3) 2_654 .
O9C1 Cs3A O178 88.2(3) . .
O178 Cs3A O178 180.0(3) 2_654 .
O2W K1 O11W 67.0(8) . .
O2W K1 O38 81.0(4) . .
O11W K1 O38 62.9(8) . .
O2W K1 O16W 69.4(5) . 2_655
O11W K1 O16W 131.4(10) . 2_655
O38 K1 O16W 129.1(5) . 2_655
O2W K1 O23 133.3(4) . .
O11W K1 O23 97.0(8) . .
O38 K1 O23 53.6(4) . .
O16W K1 O23 129.0(7) 2_655 .
O2W K1 O5T 84.5(4) . 1_455
O11W K1 O5T 95.2(8) . 1_455
O38 K1 O5T 157.2(6) . 1_455
O16W K1 O5T 59.9(5) 2_655 1_455
O23 K1 O5T 142.0(5) . 1_455
O2W K1 O78 84.5(4) . .
O11W K1 O78 111.6(8) . .
O38 K1 O78 51.7(4) . .
O16W K1 O78 84.2(5) 2_655 .
O23 K1 O78 60.1(4) . .
O5T K1 O78 144.0(4) 1_455 .
O2W K1 O3W 143.5(6) . .
O11W K1 O3W 80.3(8) . .
O38 K1 O3W 98.5(4) . .
O16W K1 O3W 129.8(6) 2_655 .
O23 K1 O3W 64.1(5) . .
O5T K1 O3W 82.8(5) 1_455 .
O78 K1 O3W 123.9(5) . .
O2W K1 O27 128.3(4) . .
O11W K1 O27 147.3(9) . .
O38 K1 O27 89.2(4) . .
O16W K1 O27 78.9(6) 2_655 .
O23 K1 O27 50.7(4) . .
O5T K1 O27 113.6(4) 1_455 .
O78 K1 O27 51.8(4) . .
O3W K1 O27 88.0(5) . .
O2W K1 W3 108.5(3) . .
O11W K1 W3 68.9(8) . .
O38 K1 W3 28.6(3) . .
O16W K1 W3 147.8(5) 2_655 .
O23 K1 W3 30.5(3) . .
O5T K1 W3 151.8(3) 1_455 .
O78 K1 W3 63.8(3) . .
O3W K1 W3 71.8(4) . .
O27 K1 W3 78.5(3) . .
O2W K1 W7 101.2(3) . .
O11W K1 W7 138.0(8) . .
O38 K1 W7 75.7(3) . .
O16W K1 W7 70.9(5) 2_655 .
O23 K1 W7 60.8(3) . .
O5T K1 W7 124.7(4) 1_455 .
O78 K1 W7 27.0(2) . .
O3W K1 W7 114.2(5) . .
O27 K1 W7 28.2(2) . .
W3 K1 W7 78.41(17) . .
O2W K1 W2 146.6(4) . .
O11W K1 W2 121.5(8) . .
O38 K1 W2 76.7(4) . .
O16W K1 W2 106.8(6) 2_655 .
O23 K1 W2 25.9(3) . .
O5T K1 W2 123.4(4) 1_455 .
O78 K1 W2 62.2(3) . .
O3W K1 W2 65.3(4) . .
O27 K1 W2 28.6(2) . .
W3 K1 W2 56.41(13) . .
W7 K1 W2 49.39(12) . .
O1AC Na1 O9W 82.7(8) . 2_755
O1AC Na1 O10W 170.1(9) . .
O9W Na1 O10W 95.8(10) 2_755 .
O1AC Na1 O5W 98.0(7) . .
O9W Na1 O5W 87.9(7) 2_755 .
O10W Na1 O5W 91.7(9) . .
O1AC Na1 O14W 95.9(9) . .
O9W Na1 O14W 85.8(8) 2_755 .
O10W Na1 O14W 74.3(11) . .
O5W Na1 O14W 163.9(10) . .
O1AC Na1 O15T 102.2(6) . .
O9W Na1 O15T 172.6(8) 2_755 .
O10W Na1 O15T 80.2(9) . .
O5W Na1 O15T 86.0(5) . .
O14W Na1 O15T 99.0(7) . .
O9W Na2 O14T 85.0(9) . .
O9W Na2 O12W 85.5(10) . .
O14T Na2 O12W 100.1(12) . .
O9W Na2 O7T 88.7(7) . 1_655
O14T Na2 O7T 78.4(6) . 1_655
O12W Na2 O7T 174.1(10) . 1_655
O9W Na2 O1W 164.3(10) . .
O14T Na2 O1W 83.6(8) . .
O12W Na2 O1W 85.9(10) . .
O7T Na2 O1W 99.5(6) 1_655 .
O9W Na2 O2AC 115.3(9) . 1_655
O14T Na2 O2AC 149.0(6) . 1_655
O12W Na2 O2AC 104.5(12) . 1_655
O7T Na2 O2AC 78.9(5) 1_655 1_655
O1W Na2 O2AC 79.7(8) . 1_655
O9W Na2 Cs1 133.7(7) . .
O14T Na2 Cs1 55.9(4) . .
O12W Na2 Cs1 121.8(10) . .
O7T Na2 Cs1 62.1(4) 1_655 .
O1W Na2 Cs1 44.0(6) . .
O2AC Na2 Cs1 94.7(4) 1_655 .
O18T Na3 O7W 161.5(12) . .
O18T Na3 Cs3 92.9(8) . .
O7W Na3 Cs3 83.8(10) . .
O18T Na3 O1CU 84.3(9) . .
O7W Na3 O1CU 82.4(10) . .
Cs3 Na3 O1CU 123.1(8) . .
O18T Na3 O13T 98.2(9) . 2_754
O7W Na3 O13T 90.5(9) . 2_754
Cs3 Na3 O13T 160.4(10) . 2_754
O1CU Na3 O13T 74.3(8) . 2_754
O18T Na3 O8T 81.9(7) . 2_654
O7W Na3 O8T 116.2(11) . 2_654
Cs3 Na3 O8T 88.8(8) . 2_654
O1CU Na3 O8T 145.8(10) . 2_654
O13T Na3 O8T 77.0(7) 2_754 2_654
O18T Na3 Cs3A 73.7(6) . .
O7W Na3 Cs3A 100.6(10) . .
Cs3 Na3 Cs3A 19.85(19) . .
O1CU Na3 Cs3A 114.9(7) . .
O13T Na3 Cs3A 166.4(8) 2_754 .
O8T Na3 Cs3A 90.9(7) 2_654 .
O18T Na3 W18 18.5(4) . .
O7W Na3 W18 143.1(10) . .
Cs3 Na3 W18 90.8(5) . .
O1CU Na3 W18 70.1(6) . .
O13T Na3 W18 104.7(7) 2_754 .
O8T Na3 W18 100.2(6) 2_654 .
Cs3A Na3 W18 71.0(3) . .
O18T Na3 Cs1 136.2(8) . 2_754
O7W Na3 Cs1 61.5(8) . 2_754
Cs3 Na3 Cs1 81.7(6) . 2_754
O1CU Na3 Cs1 134.5(7) . 2_754
O13T Na3 Cs1 79.1(6) 2_754 2_754
O8T Na3 Cs1 54.7(5) 2_654 2_754
Cs3A Na3 Cs1 99.0(6) . 2_754
W18 Na3 Cs1 153.7(6) . 2_754
O18T Na3 Cs3 63.2(6) . 2_654
O7W Na3 Cs3 109.6(9) . 2_654
Cs3 Na3 Cs3 30.6(3) . 2_654
O1CU Na3 Cs3 109.3(6) . 2_654
O13T Na3 Cs3 159.9(7) 2_754 2_654
O8T Na3 Cs3 92.0(6) 2_654 2_654
Cs3A Na3 Cs3 10.79(11) . 2_654
W18 Na3 Cs3 60.3(3) . 2_654
Cs1 Na3 Cs3 108.4(5) 2_754 2_654
O1T Na4 O17T 162.5(13) . 1_545
O1T Na4 O4W 87.0(8) . .
O17T Na4 O4W 85.5(9) 1_545 .
O1T Na4 O10T 89.5(9) . 1_445
O17T Na4 O10T 104.9(9) 1_545 1_445
O4W Na4 O10T 80.7(8) . 1_445
O1T Na4 O15W 87.1(8) . 2_644
O17T Na4 O15W 84.0(9) 1_545 2_644
O4W Na4 O15W 124.2(12) . 2_644
O10T Na4 O15W 154.7(13) 1_445 2_644
O1T Na4 Cs2 54.4(5) . .
O17T Na4 Cs2 128.3(8) 1_545 .
O4W Na4 Cs2 49.6(5) . .
O10T Na4 Cs2 51.3(5) 1_445 .
O15W Na4 Cs2 139.0(8) 2_644 .
O1T Na4 Cs2A 45.4(6) . .
O17T Na4 Cs2A 150.0(8) 1_545 .
O4W Na4 Cs2A 89.3(7) . .
O10T Na4 Cs2A 45.2(5) 1_445 .
O15W Na4 Cs2A 122.5(9) 2_644 .
Cs2 Na4 Cs2A 39.7(2) . .
O1T Na4 Cs1 151.6(8) . 1_445
O17T Na4 Cs1 39.6(5) 1_545 1_445
O4W Na4 Cs1 76.3(6) . 1_445
O10T Na4 Cs1 65.4(5) 1_445 1_445
O15W Na4 Cs1 121.3(8) 2_644 1_445
Cs2 Na4 Cs1 97.8(4) . 1_445
Cs2A Na4 Cs1 110.6(4) . 1_445
Na2 O1W Cs1 102.6(8) . .
Cs2A O3W K1 124.0(7) . .
Na4 O4W Cs2 94.6(8) . .
Na3 O7W Cs3 49.9(7) . .
Na3 O7W Cs1 83.8(9) . 2_754
Cs3 O7W Cs1 81.3(6) . 2_754
Na2 O9W Na1 151.1(10) . 2_755
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O1T 1.740(13) .
W1 O14 1.852(12) .
W1 O15 1.894(15) .
W1 O13 1.937(15) .
W1 O12 1.963(11) .
W1 O1G1 2.376(11) .
W1 Cs2A 3.893(6) .
W1 Cs2 4.191(3) .
W2 O2T 1.727(12) .
W2 O23 1.877(14) .
W2 O12 1.888(12) .
W2 O26 1.915(15) .
W2 O27 1.968(12) .
W2 O2G1 2.360(11) .
W2 Cs2A 3.881(6) .
W2 Cs2 4.003(3) .
W2 K1 4.038(10) .
W3 O3T 1.737(15) .
W3 O39 1.838(12) .
W3 O38 1.896(13) .
W3 O13 1.914(14) .
W3 O23 1.975(12) .
W3 O3G1 2.356(12) .
W3 K1 3.838(8) .
W3 Cs2A 3.921(5) .
W4 O4T 1.742(14) .
W4 O4C1 1.779(12) .
W4 O49 1.943(16) .
W4 O45 1.976(16) .
W4 O14 2.057(13) .
W4 O1G1 2.298(11) .
W5 O5T 1.733(17) .
W5 O5C2 1.797(12) .
W5 O45 1.910(12) .
W5 O56 1.953(11) .
W5 O15 2.021(13) .
W5 O1G1 2.266(14) .
W5 K1 4.090(9) 1_655
W6 O6T 1.732(14) .
W6 O56 1.879(11) .
W6 O6CC 1.885(11) .
W6 O26 1.941(13) .
W6 O67 2.021(13) .
W6 O2G1 2.353(13) .
W6 Ce1 3.4106(12) .
W7 O7T 1.726(13) .
W7 O7CC 1.855(12) .
W7 O78 1.888(14) .
W7 O27 1.936(11) .
W7 O67 1.965(15) .
W7 O2G1 2.319(11) .
W7 Ce1 3.4027(14) .
W7 K1 4.022(9) .
W7 Cs1 4.190(2) 1_455
W8 O8T 1.720(16) .
W8 O8C3 1.790(14) .
W8 O89 1.900(12) .
W8 O78 1.963(12) .
W8 O38 2.000(13) .
W8 O3G1 2.265(13) .
W8 Cs3 3.836(3) 2_654
W8 Cs1 3.9343(17) 1_455
W8 K1 4.040(8) .
W8 Cs3A 4.2285(7) .
W9 O9T 1.743(15) .
W9 O9C1 1.768(13) .
W9 O49 1.919(15) .
W9 O89 1.937(14) .
W9 O39 2.053(14) .
W9 O3G1 2.310(11) .
W9 Cs3 3.863(3) .
W9 Cs3A 4.1083(8) .
W10 O10T 1.742(15) .
W10 O103 1.886(12) .
W10 O104 1.904(14) .
W10 O102 1.929(15) .
W10 O101 1.961(11) .
W10 O1G2 2.401(12) .
W10 Cs2A 3.846(5) 1_665
W10 Cs2 4.092(3) 1_665
W10 Cs1 4.284(2) .
W11 O11T 1.746(13) .
W11 O115 1.884(14) .
W11 O101 1.890(13) .
W11 O116 1.893(14) .
W11 O112 1.900(14) .
W11 O2G2 2.395(11) .
W11 Cs2A 4.023(5) 1_665
W11 Cs2 4.074(3) 1_665
W12 O12T 1.721(14) .
W12 O127 1.882(15) .
W12 O128 1.888(12) .
W12 O102 1.918(15) .
W12 O112 1.932(13) .
W12 O3G2 2.371(11) .
W12 Cs2A 3.865(6) 1_665
W13 O13T 1.724(12) .
W13 O3CC 1.805(13) .
W13 O134 1.901(15) .
W13 O138 1.929(14) .
W13 O103 2.035(13) .
W13 O1G2 2.333(11) .
W13 Cs1 4.328(2) .
W14 O14T 1.731(16) .
W14 O4C2 1.782(13) .
W14 O145 1.927(12) .
W14 O134 2.006(12) .
W14 O104 2.031(12) .
W14 O1G2 2.266(13) .
W14 Cs1 3.9193(18) .
W15 O15T 1.736(16) .
W15 O5C 1.828(13) .
W15 O145 1.909(13) .
W15 O156 1.955(15) .
W15 O115 2.005(13) .
W15 O2G2 2.316(13) .
W16 O16T 1.699(13) .
W16 O6C 1.830(11) .
W16 O167 1.921(14) .
W16 O116 1.969(14) .
W16 O156 1.969(16) .
W16 O2G2 2.318(12) .
W17 O17T 1.748(15) .
W17 O7C3 1.767(11) .
W17 O178 1.929(12) .
W17 O167 1.935(13) .
W17 O127 2.037(13) .
W17 O3G2 2.261(14) .
W17 Cs1 3.9416(18) 1_455
W17 Cs3 4.288(4) 2_654
W18 O18T 1.723(13) .
W18 O8CC 1.804(12) .
W18 O138 1.921(14) .
W18 O178 1.942(14) .
W18 O128 2.000(12) .
W18 O3G2 2.343(12) .
W18 Na3 3.714(19) .
W18 Cs3A 4.0874(9) .
W18 Cs3 4.113(4) 2_654
W18 Cs3 4.464(4) .
Ce1 O6CC 2.190(12) .
Ce1 O6C 2.204(12) .
Ce1 O7CC 2.218(14) .
Ce1 O5C 2.242(15) .
Ce1 O1AC 2.393(14) .
Ce1 O2AC 2.483(13) .
Ce1 O67 2.516(12) .
Ce1 O4G2 2.618(11) .
Ce1 C1 2.799(19) .
Ce1 Cu3 3.490(2) .
Cu1 O4C1 1.945(12) .
Cu1 O9C1 1.950(15) .
Cu1 O8CC 1.968(12) .
Cu1 O3CC 1.971(15) .
Cu1 O4G1 2.362(10) .
Cu1 O1CU 2.370(14) .
Cu2 O4C2 1.931(15) .
Cu2 O5C2 1.946(13) .
Cu2 O4G1 2.006(14) .
Cu2 O4G2 2.061(12) .
Cu2 O6CC 2.303(11) .
Cu2 O3CC 2.328(12) .
Cu3 O8C3 1.955(16) .
Cu3 O7C3 1.955(12) .
Cu3 O4G1 2.000(11) .
Cu3 O4G2 2.026(14) .
Cu3 O8CC 2.325(12) .
Cu3 O7CC 2.331(11) .
Cu3 Cs1 3.962(3) 1_455
Cu3 Cs3 4.306(4) 2_654
Ge1 O4G1 1.727(11) .
Ge1 O2G1 1.729(10) .
Ge1 O1G1 1.751(12) .
Ge1 O3G1 1.756(14) .
Ge2 O2G2 1.718(11) .
Ge2 O1G2 1.736(13) .
Ge2 O3G2 1.748(13) .
Ge2 O4G2 1.755(12) .
O1T Na4 2.30(2) .
O1T Cs2A 3.209(17) .
O1T Cs2 3.341(13) .
O2T Cs2 3.128(13) .
O2T Cs2A 3.286(14) .
O3T Cs2A 3.263(16) .
O5T K1 3.065(16) 1_655
O7T Na2 2.382(14) 1_455
O7T Cs1 3.779(13) 1_455
O8T Na3 2.60(2) 2_654
O8T Cs1 3.277(13) 1_455
O8T Cs3 3.517(13) 2_654
O9T Cs3 3.334(14) .
O10T Na4 2.45(3) 1_665
O10T Cs2A 3.164(15) 1_665
O10T Cs2 3.207(14) 1_665
O11T Cs2 3.203(15) 1_665
O11T Cs2A 3.454(14) 1_665
O12T Cs2A 3.154(19) 1_665
O13T Na3 2.49(2) 2_754
O14T Na2 2.36(2) .
O14T Cs1 3.522(13) .
O15T Na1 2.920(17) .
O17T Na4 2.33(2) 1_565
O17T Cs1 3.317(13) 1_455
O18T Na3 2.26(2) .
O18T Cs3 3.397(15) .
O18T Cs3A 3.434(15) .
O23 K1 2.995(17) .
O23 Cs2A 3.495(13) .
O27 K1 3.173(18) .
O104 Cs1 3.178(13) .
O101 Cs2 3.261(14) 1_665
O101 Cs2A 3.471(13) 1_665
O13 Cs2A 3.367(12) .
O112 Cs2A 3.518(14) 1_665
O8C3 Cs3 3.163(14) 2_654
O8C3 Cs1 3.347(13) 1_455
O8C3 Cs3A 3.704(13) .
O7CC Cs1 3.502(14) 1_455
O9C1 Cs3 3.367(14) .
O9C1 Cs3A 3.526(14) .
O12 Cs2 3.287(12) .
O12 Cs2A 3.431(14) .
O78 K1 3.111(16) .
O78 Cs1 3.697(12) 1_455
O38 K1 2.893(14) .
O7C3 Cs1 2.989(14) 1_455
O178 Cs3 3.121(15) 2_654
O178 Cs3A 3.667(14) .
O134 Cs1 3.058(15) .
O1CU Na3 2.47(3) .
O1AC C1 1.23(3) .
O1AC Na1 2.59(2) .
O2AC C1 1.28(3) .
O2AC Na2 2.446(19) 1_455
O103 Cs1 3.651(15) .
O89 Cs3A 3.232(12) .
O89 Cs3 3.448(12) 2_654
O89 Cs3 3.525(12) .
O102 Cs2A 3.315(13) 1_665
C1 C2 1.55(3) .
C2 H2A 0.9600 .
C2 H2B 0.9600 .
C2 H2C 0.9600 .
Cs1 O7C3 2.989(14) 1_655
Cs1 O1W 3.03(2) .
Cs1 O8T 3.277(14) 1_655
Cs1 O17T 3.317(13) 1_655
Cs1 O8C3 3.347(13) 1_655
Cs1 O7CC 3.502(14) 1_655
Cs1 O7W 3.53(3) 2_754
Cs1 O78 3.697(12) 1_655
Cs2 Cs2A 2.893(8) .
Cs2 O4W 3.139(16) .
Cs2 O10T 3.207(14) 1_445
Cs2 O11T 3.203(16) 1_445
Cs2 O13W 3.21(5) .
Cs2 O101 3.261(14) 1_445
Cs2 W11 4.074(3) 1_445
Cs2 W10 4.092(3) 1_445
Cs2A O8W 2.84(3) .
Cs2A O3W 2.89(2) .
Cs2A O12T 3.154(19) 1_445
Cs2A O10T 3.164(15) 1_445
Cs2A O102 3.315(13) 1_445
Cs2A O11T 3.454(14) 1_445
Cs3 Cs3A 1.309(4) .
Cs3 Na3 2.42(2) .
Cs3 Cs3 2.618(8) 2_654
Cs3 O178 3.121(15) 2_654
Cs3 O7W 3.15(3) .
Cs3 O8C3 3.163(14) 2_654
Cs3 O89 3.448(12) 2_654
Cs3 O8T 3.517(13) 2_654
Cs3A Cs3 1.309(4) 2_654
Cs3A O89 3.232(12) 2_654
Cs3A Na3 3.30(2) .
Cs3A Na3 3.30(2) 2_654
Cs3A O18T 3.434(15) 2_654
Cs3A O9C1 3.526(14) 2_654
Cs3A O178 3.667(14) 2_654
K1 O2W 2.831(16) .
K1 O11W 2.90(4) .
K1 O16W 2.94(2) 2_655
K1 O5T 3.065(16) 1_455
K1 O3W 3.135(19) .
Na1 O9W 2.71(2) 2_755
Na1 O10W 2.71(5) .
Na1 O5W 2.72(2) .
Na1 O14W 2.77(3) .
Na2 O9W 2.36(2) .
Na2 O12W 2.37(3) .
Na2 O7T 2.382(14) 1_655
Na2 O1W 2.40(2) .
Na2 O2AC 2.446(19) 1_655
Na3 O7W 2.29(3) .
Na3 O13T 2.49(2) 2_754
Na3 O8T 2.60(2) 2_654
Na3 Cs1 4.00(2) 2_754
Na3 Cs3 4.39(2) 2_654
Na4 O17T 2.33(2) 1_545
Na4 O4W 2.41(3) .
Na4 O10T 2.45(3) 1_445
Na4 O15W 2.51(3) 2_644
Na4 Cs1 4.759(19) 1_445
O7W Cs1 3.53(3) 2_754
O9W Na1 2.71(2) 2_755
O15W Na4 2.51(3) 2_644
O16W K1 2.94(2) 2_655
