#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:19:00 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179371 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/68/4326899.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4326899
loop_
_publ_author_name
'Miriam M. Gillett-Kunnath'
'Joseph I. Paik'
'Sara M. Jensen'
'Jacob D. Taylor'
'Slavi C. Sevov'
_publ_contact_author_address
;
University of Notre Dame
Department of Chemistry and Biochemistry
251 Nieuwland Science Hall
Notre Dame, Indiana 46556
;
_publ_contact_author_email       ssevov@nd.edu
_publ_contact_author_name        'Sevov, S. C.'
_publ_section_title
;
 Metal-Centered Deltahedral Zintl Ions: Synthesis of [Ni@Sn9]4- by direct
 Extraction from Intermetallic Precursors and of the Vertex-Fused Dimer
 [{Ni@Sn8(μ-Ge)1/2}2]4-
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11695
_journal_page_last               11701
_journal_paper_doi               10.1021/ic2016963
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         '(Ni2 Ge Sn16), 2(C18 H36 K N2 O6), N2C2H4'
_chemical_formula_sum            'C76 H160 Ge K4 N12 Ni2 O24 Sn16'
_chemical_formula_weight         3871.61
_chemical_name_systematic
; 
  (K-crypt)2(Ni2@GeSn16)en
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 121.2140(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   30.636(2)
_cell_length_b                   16.5548(12)
_cell_length_c                   28.872(2)
_cell_measurement_reflns_used    9313
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.00
_cell_measurement_theta_min      4.763
_cell_volume                     12523.3(15)
_computing_cell_refinement       'Bruker SAINT v7.60A'
_computing_data_collection       'Bruker APEX-II v2008-6'
_computing_data_reduction        'Bruker SAINT v7.60A'
_computing_molecular_graphics    SHELXL-XP
_computing_publication_material  SHELXTL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 83.33
_diffrn_measured_fraction_theta_full 0.978
_diffrn_measured_fraction_theta_max 0.978
_diffrn_measurement_device_type  'Bruker APEX-II'
_diffrn_measurement_method       'combination of ω/2θ-scans and φ-scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0202
_diffrn_reflns_av_sigmaI/netI    0.0388
_diffrn_reflns_limit_h_max       36
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            17737
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.46
_exptl_absorpt_coefficient_mu    3.848
_exptl_absorpt_correction_T_max  0.8613
_exptl_absorpt_correction_T_min  0.7745
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'Sheldrick, 2008'
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    2.053
_exptl_crystal_description       block
_exptl_crystal_F_000             7424
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.596
_refine_diff_density_min         -1.736
_refine_diff_density_rms         0.162
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.108
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     610
_refine_ls_number_reflns         10799
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.112
_refine_ls_R_factor_all          0.0587
_refine_ls_R_factor_gt           0.0397
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0256P)²+214.4017P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0852
_refine_ls_wR_factor_ref         0.0969
_reflns_number_gt                8606
_reflns_number_total             10799
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic2016963_si_001_1.cif
_cod_data_source_block           compd3
_cod_original_cell_volume        12523.5(15)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4326899
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sn1 Sn 0.05230(2) 0.50633(4) 0.75881(2) 0.03699(15) Uani 1 1 d .
Sn2 Sn 0.03596(2) 0.45452(4) 0.84709(2) 0.03108(14) Uani 1 1 d .
Sn3 Sn 0.096050(19) 0.34114(3) 0.82240(2) 0.02477(13) Uani 1 1 d .
Sn4 Sn 0.05337(2) 0.34093(3) 0.70386(2) 0.02604(13) Uani 1 1 d .
Ni1 Ni 0.0000 0.37660(8) 0.7500 0.0170(3) Uani 1 2 d S
Ge1 Ge 0.0000 0.24229(7) 0.7500 0.0218(2) Uani 1 2 d S
Ni2 Ni 0.0000 0.10762(8) 0.7500 0.0183(3) Uani 1 2 d S
Sn5 Sn 0.02384(2) 0.14385(3) 0.67656(2) 0.02812(13) Uani 1 1 d .
Sn6 Sn -0.08196(2) 0.14644(3) 0.65549(2) 0.02505(13) Uani 1 1 d .
Sn7 Sn -0.02072(2) -0.02207(3) 0.68834(2) 0.03177(14) Uani 1 1 d .
Sn8 Sn -0.08684(2) 0.03061(4) 0.73145(2) 0.03166(14) Uani 1 1 d .
K1 K 0.31062(6) 0.67068(11) 0.94177(7) 0.0295(4) Uani 1 1 d .
N1 N 0.3039(3) 0.5325(5) 1.0053(3) 0.048(2) Uani 1 1 d .
N2 N 0.3151(3) 0.8096(6) 0.8759(3) 0.052(2) Uani 1 1 d .
O1 O 0.3411(3) 0.6940(4) 1.0491(2) 0.0525(18) Uani 1 1 d .
O2 O 0.3298(3) 0.8305(4) 0.9845(3) 0.0490(16) Uani 1 1 d .
O3 O 0.2194(2) 0.5861(4) 0.9019(2) 0.0439(15) Uani 1 1 d .
O4 O 0.2293(2) 0.6958(5) 0.8330(2) 0.0514(18) Uani 1 1 d .
O5 O 0.3684(2) 0.5307(4) 0.9581(2) 0.0427(15) Uani 1 1 d .
O6 O 0.3871(2) 0.6736(4) 0.9150(2) 0.0425(15) Uani 1 1 d .
C1 C 0.3324(4) 0.5545(7) 1.0633(4) 0.063(3) Uani 1 1 d .
H1A H 0.3693 0.5466 1.0778 0.076 Uiso 1 1 calc R
H1B H 0.3222 0.5174 1.0830 0.076 Uiso 1 1 calc R
C2 C 0.3240(5) 0.6388(8) 1.0743(4) 0.068(4) Uani 1 1 d .
H2A H 0.2872 0.6476 1.0602 0.082 Uiso 1 1 calc R
H2B H 0.3429 0.6485 1.1139 0.082 Uiso 1 1 calc R
C3 C 0.3427(5) 0.7750(7) 1.0666(4) 0.070(4) Uani 1 1 d .
H3A H 0.3645 0.7777 1.1065 0.084 Uiso 1 1 calc R
H3B H 0.3079 0.7927 1.0561 0.084 Uiso 1 1 calc R
C4 C 0.3634(5) 0.8291(7) 1.0419(4) 0.067(3) Uani 1 1 d .
H4A H 0.3672 0.8844 1.0567 0.081 Uiso 1 1 calc R
H4B H 0.3975 0.8099 1.0509 0.081 Uiso 1 1 calc R
C5 C 0.3454(5) 0.8896(7) 0.9594(5) 0.070(3) Uani 1 1 d .
H5A H 0.3810 0.8791 0.9693 0.084 Uiso 1 1 calc R
H5B H 0.3438 0.9443 0.9722 0.084 Uiso 1 1 calc R
C6 C 0.3108(5) 0.8848(7) 0.8992(5) 0.066(3) Uani 1 1 d .
H6A H 0.2751 0.8912 0.8902 0.079 Uiso 1 1 calc R
H6B H 0.3186 0.9304 0.8825 0.079 Uiso 1 1 calc R
C7 C 0.2500(4) 0.5196(7) 0.9861(5) 0.061(3) Uani 1 1 d .
H7A H 0.2379 0.5650 0.9988 0.073 Uiso 1 1 calc R
H7B H 0.2467 0.4696 1.0028 0.073 Uiso 1 1 calc R
C8 C 0.2162(4) 0.5129(7) 0.9262(5) 0.062(3) Uani 1 1 d .
H8A H 0.2270 0.4667 0.9127 0.074 Uiso 1 1 calc R
H8B H 0.1805 0.5036 0.9166 0.074 Uiso 1 1 calc R
C9 C 0.1900(4) 0.5805(8) 0.8445(4) 0.065(3) Uani 1 1 d .
H9A H 0.1566 0.5554 0.8330 0.078 Uiso 1 1 calc R
H9B H 0.2079 0.5460 0.8315 0.078 Uiso 1 1 calc R
C10 C 0.1822(3) 0.6619(7) 0.8207(4) 0.053(3) Uani 1 1 d .
H10A H 0.1592 0.6585 0.7809 0.064 Uiso 1 1 calc R
H10B H 0.1658 0.6970 0.8352 0.064 Uiso 1 1 calc R
C11 C 0.2229(4) 0.7764(8) 0.8144(5) 0.071(4) Uani 1 1 d .
H11A H 0.2148 0.8118 0.8366 0.085 Uiso 1 1 calc R
H11B H 0.1945 0.7798 0.7763 0.085 Uiso 1 1 calc R
C12 C 0.2718(4) 0.8027(8) 0.8191(4) 0.074(4) Uani 1 1 d .
H12A H 0.2810 0.7633 0.7997 0.089 Uiso 1 1 calc R
H12B H 0.2664 0.8557 0.8010 0.089 Uiso 1 1 calc R
C13 C 0.3261(5) 0.4599(6) 0.9961(5) 0.066(3) Uani 1 1 d .
H13A H 0.3016 0.4377 0.9598 0.079 Uiso 1 1 calc R
H13B H 0.3315 0.4185 1.0233 0.079 Uiso 1 1 calc R
C14 C 0.3760(4) 0.4764(7) 0.9996(5) 0.066(3) Uani 1 1 d .
H14A H 0.4006 0.4999 1.0354 0.079 Uiso 1 1 calc R
H14B H 0.3905 0.4251 0.9958 0.079 Uiso 1 1 calc R
C15 C 0.4142(3) 0.5455(6) 0.9584(5) 0.054(3) Uani 1 1 d .
H15A H 0.4293 0.4936 0.9568 0.065 Uiso 1 1 calc R
H15B H 0.4390 0.5732 0.9924 0.065 Uiso 1 1 calc R
C16 C 0.4037(4) 0.5964(6) 0.9114(5) 0.057(3) Uani 1 1 d .
H16A H 0.4351 0.6010 0.9099 0.068 Uiso 1 1 calc R
H16B H 0.3772 0.5701 0.8776 0.068 Uiso 1 1 calc R
C17 C 0.3773(4) 0.7216(7) 0.8698(4) 0.060(3) Uani 1 1 d .
H17A H 0.3491 0.6976 0.8361 0.072 Uiso 1 1 calc R
H17B H 0.4081 0.7234 0.8669 0.072 Uiso 1 1 calc R
C18 C 0.3633(4) 0.8049(7) 0.8768(5) 0.060(3) Uani 1 1 d .
H18A H 0.3909 0.8267 0.9118 0.073 Uiso 1 1 calc R
H18B H 0.3608 0.8396 0.8477 0.073 Uiso 1 1 calc R
K2 K 0.35442(6) 0.23433(10) 0.88735(6) 0.0247(4) Uani 1 1 d .
N3 N 0.2489(3) 0.1978(5) 0.8633(3) 0.0375(17) Uani 1 1 d .
N4 N 0.4598(3) 0.2730(4) 0.9092(3) 0.0334(16) Uani 1 1 d .
O7 O 0.3359(2) 0.2249(4) 0.9729(2) 0.0385(14) Uani 1 1 d .
O8 O 0.4376(2) 0.2297(3) 0.9936(2) 0.0337(13) Uani 1 1 d .
O9 O 0.2732(2) 0.3395(3) 0.8193(2) 0.0350(13) Uani 1 1 d .
O10 O 0.3751(2) 0.3890(4) 0.8574(2) 0.0347(14) Uani 1 1 d .
O11 O 0.3062(2) 0.0849(3) 0.8361(2) 0.0339(13) Uani 1 1 d .
O12 O 0.3967(2) 0.1366(4) 0.8404(2) 0.0392(14) Uani 1 1 d .
C19 C 0.2459(4) 0.2178(7) 0.9112(4) 0.055(3) Uani 1 1 d .
H19A H 0.2141 0.1947 0.9066 0.066 Uiso 1 1 calc R
H19B H 0.2440 0.2772 0.9135 0.066 Uiso 1 1 calc R
C20 C 0.2904(4) 0.1872(7) 0.9632(4) 0.058(3) Uani 1 1 d .
H20A H 0.2850 0.1989 0.9935 0.069 Uiso 1 1 calc R
H20B H 0.2933 0.1279 0.9610 0.069 Uiso 1 1 calc R
C21 C 0.3789(4) 0.1946(6) 1.0214(3) 0.045(2) Uani 1 1 d .
H21A H 0.3844 0.1370 1.0165 0.054 Uiso 1 1 calc R
H21B H 0.3724 0.1983 1.0515 0.054 Uiso 1 1 calc R
C22 C 0.4253(4) 0.2420(6) 1.0349(3) 0.041(2) Uani 1 1 d .
H22A H 0.4191 0.3001 1.0373 0.049 Uiso 1 1 calc R
H22B H 0.4543 0.2246 1.0704 0.049 Uiso 1 1 calc R
C23 C 0.4824(3) 0.2739(6) 1.0051(3) 0.039(2) Uani 1 1 d .
H23A H 0.5107 0.2611 1.0422 0.047 Uiso 1 1 calc R
H23B H 0.4755 0.3326 1.0032 0.047 Uiso 1 1 calc R
C24 C 0.4970(3) 0.2517(6) 0.9651(3) 0.041(2) Uani 1 1 d .
H24A H 0.5297 0.2786 0.9755 0.049 Uiso 1 1 calc R
H24B H 0.5029 0.1927 0.9671 0.049 Uiso 1 1 calc R
C25 C 0.2129(3) 0.2459(6) 0.8162(4) 0.046(2) Uani 1 1 d .
H25A H 0.1788 0.2425 0.8122 0.055 Uiso 1 1 calc R
H25B H 0.2101 0.2219 0.7834 0.055 Uiso 1 1 calc R
C26 C 0.2272(3) 0.3336(6) 0.8192(4) 0.046(2) Uani 1 1 d .
H26A H 0.1997 0.3631 0.7877 0.055 Uiso 1 1 calc R
H26B H 0.2315 0.3582 0.8526 0.055 Uiso 1 1 calc R
C27 C 0.2884(3) 0.4215(5) 0.8220(3) 0.040(2) Uani 1 1 d .
H27A H 0.2989 0.4443 0.8580 0.048 Uiso 1 1 calc R
H27B H 0.2595 0.4538 0.7942 0.048 Uiso 1 1 calc R
C28 C 0.3315(3) 0.4252(6) 0.8128(3) 0.040(2) Uani 1 1 d .
H28A H 0.3225 0.3962 0.7789 0.048 Uiso 1 1 calc R
H28B H 0.3390 0.4822 0.8089 0.048 Uiso 1 1 calc R
C29 C 0.4181(3) 0.3945(6) 0.8513(4) 0.042(2) Uani 1 1 d .
H29A H 0.4246 0.4517 0.8468 0.051 Uiso 1 1 calc R
H29B H 0.4115 0.3642 0.8187 0.051 Uiso 1 1 calc R
C30 C 0.4639(3) 0.3595(5) 0.9010(4) 0.038(2) Uani 1 1 d .
H30A H 0.4945 0.3682 0.8983 0.046 Uiso 1 1 calc R
H30B H 0.4692 0.3893 0.9332 0.046 Uiso 1 1 calc R
C31 C 0.2375(4) 0.1115(6) 0.8505(4) 0.053(3) Uani 1 1 d .
H31A H 0.2004 0.1029 0.8347 0.064 Uiso 1 1 calc R
H31B H 0.2557 0.0801 0.8845 0.064 Uiso 1 1 calc R
C32 C 0.2523(3) 0.0798(6) 0.8118(4) 0.048(3) Uani 1 1 d .
H32A H 0.2412 0.0228 0.8027 0.058 Uiso 1 1 calc R
H32B H 0.2352 0.1118 0.7780 0.058 Uiso 1 1 calc R
C33 C 0.3226(4) 0.0537(6) 0.8020(4) 0.045(2) Uani 1 1 d .
H33A H 0.3086 0.0869 0.7687 0.054 Uiso 1 1 calc R
H33B H 0.3101 -0.0023 0.7912 0.054 Uiso 1 1 calc R
C34 C 0.3793(4) 0.0550(5) 0.8315(4) 0.046(2) Uani 1 1 d .
H34A H 0.3933 0.0269 0.8667 0.055 Uiso 1 1 calc R
H34B H 0.3914 0.0266 0.8101 0.055 Uiso 1 1 calc R
C35 C 0.4509(4) 0.1394(6) 0.8655(4) 0.047(2) Uani 1 1 d .
H35A H 0.4613 0.1097 0.8431 0.057 Uiso 1 1 calc R
H35B H 0.4671 0.1132 0.9015 0.057 Uiso 1 1 calc R
C36 C 0.4680(3) 0.2249(6) 0.8717(4) 0.046(2) Uani 1 1 d .
H36A H 0.5049 0.2255 0.8845 0.055 Uiso 1 1 calc R
H36B H 0.4498 0.2511 0.8357 0.055 Uiso 1 1 calc R
N5 N 0.5198(4) 0.0826(6) 0.0503(4) 0.078(3) Uani 1 1 d .
H5C H 0.5515 0.0885 0.0582 0.094 Uiso 1 1 calc R
H5D H 0.5080 0.1132 0.0663 0.094 Uiso 1 1 calc R
C37 C 0.4821(6) 0.0130(10) 0.0050(7) 0.104(5) Uani 1 1 d U
H37A H 0.4710 -0.0294 0.0208 0.125 Uiso 1 1 calc R
H37B H 0.4522 0.0369 -0.0273 0.125 Uiso 1 1 calc R
C39 C 0.4751(5) 0.7574(8) 0.2254(6) 0.095(4) Uani 1 1 d U
H39A H 0.4762 0.8065 0.2085 0.113 Uiso 1 1 d .
H39B H 0.4790 0.7152 0.2048 0.113 Uiso 1 1 d .
N7 N 0.4321(6) 0.7522(10) 0.2103(8) 0.212(11) Uani 1 1 d U
H7D H 0.4263 0.7046 0.2213 0.317 Uiso 1 1 d .
H7E H 0.4236 0.7928 0.2249 0.317 Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ni1 Sn1 Sn2 58.531(17) . .
Ni1 Sn1 Sn2 58.479(17) . 2_556
Sn2 Sn1 Sn2 109.38(2) . 2_556
Ni1 Sn1 Sn1 55.31(2) . 2_556
Sn2 Sn1 Sn1 60.02(2) . 2_556
Sn2 Sn1 Sn1 59.89(2) 2_556 2_556
Ni1 Sn1 Sn4 53.60(2) . .
Sn2 Sn1 Sn4 103.31(2) . .
Sn2 Sn1 Sn4 58.407(19) 2_556 .
Sn1 Sn1 Sn4 101.770(19) 2_556 .
Ni1 Sn1 Sn3 53.30(2) . .
Sn2 Sn1 Sn3 57.543(18) . .
Sn2 Sn1 Sn3 103.45(2) 2_556 .
Sn1 Sn1 Sn3 101.154(19) 2_556 .
Sn4 Sn1 Sn3 55.643(18) . .
Ni1 Sn2 Sn3 55.058(19) . .
Ni1 Sn2 Sn1 54.25(2) . .
Sn3 Sn2 Sn1 64.79(2) . .
Ni1 Sn2 Sn1 54.21(2) . 2_556
Sn3 Sn2 Sn1 106.43(2) . 2_556
Sn1 Sn2 Sn1 60.08(2) . 2_556
Ni1 Sn2 Sn4 54.825(18) . 2_556
Sn3 Sn2 Sn4 90.44(2) . 2_556
Sn1 Sn2 Sn4 106.08(2) . 2_556
Sn1 Sn2 Sn4 64.17(2) 2_556 2_556
Ni1 Sn3 Sn2 58.28(2) . .
Ni1 Sn3 Sn4 56.180(15) . .
Sn2 Sn3 Sn4 108.74(2) . .
Ni1 Sn3 Ge1 45.21(3) . .
Sn2 Sn3 Ge1 90.33(2) . .
Sn4 Sn3 Ge1 61.128(15) . .
Ni1 Sn3 Sn1 52.34(3) . .
Sn2 Sn3 Sn1 57.666(19) . .
Sn4 Sn3 Sn1 62.111(19) . .
Ge1 Sn3 Sn1 95.59(2) . .
Ni1 Sn4 Sn3 55.836(14) . .
Ni1 Sn4 Sn2 57.64(2) . 2_556
Sn3 Sn4 Sn2 108.03(2) . 2_556
Ni1 Sn4 Ge1 45.08(3) . .
Sn3 Sn4 Ge1 60.899(15) . .
Sn2 Sn4 Ge1 89.45(2) 2_556 .
Ni1 Sn4 Sn1 52.32(3) . .
Sn3 Sn4 Sn1 62.246(18) . .
Sn2 Sn4 Sn1 57.426(19) 2_556 .
Ge1 Sn4 Sn1 95.53(2) . .
Ge1 Ni1 Sn1 145.31(2) . .
Ge1 Ni1 Sn1 145.31(2) . 2_556
Sn1 Ni1 Sn1 69.38(4) . 2_556
Ge1 Ni1 Sn3 77.18(3) . 2_556
Sn1 Ni1 Sn3 129.38(4) . 2_556
Sn1 Ni1 Sn3 74.37(2) 2_556 2_556
Ge1 Ni1 Sn3 77.18(3) . .
Sn1 Ni1 Sn3 74.36(2) . .
Sn1 Ni1 Sn3 129.38(4) 2_556 .
Sn3 Ni1 Sn3 154.36(6) 2_556 .
Ge1 Ni1 Sn4 77.15(3) . .
Sn1 Ni1 Sn4 74.08(2) . .
Sn1 Ni1 Sn4 129.79(4) 2_556 .
Sn3 Ni1 Sn4 106.03(2) 2_556 .
Sn3 Ni1 Sn4 67.984(19) . .
Ge1 Ni1 Sn4 77.15(3) . 2_556
Sn1 Ni1 Sn4 129.79(4) . 2_556
Sn1 Ni1 Sn4 74.08(2) 2_556 2_556
Sn3 Ni1 Sn4 67.988(19) 2_556 2_556
Sn3 Ni1 Sn4 106.03(2) . 2_556
Sn4 Ni1 Sn4 154.31(6) . 2_556
Ge1 Ni1 Sn2 118.03(3) . .
Sn1 Ni1 Sn2 67.22(3) . .
Sn1 Ni1 Sn2 67.32(3) 2_556 .
Sn3 Ni1 Sn2 127.21(2) 2_556 .
Sn3 Ni1 Sn2 66.667(17) . .
Sn4 Ni1 Sn2 126.23(2) . .
Sn4 Ni1 Sn2 67.537(18) 2_556 .
Ge1 Ni1 Sn2 118.03(3) . 2_556
Sn1 Ni1 Sn2 67.32(3) . 2_556
Sn1 Ni1 Sn2 67.22(3) 2_556 2_556
Sn3 Ni1 Sn2 66.664(17) 2_556 2_556
Sn3 Ni1 Sn2 127.21(2) . 2_556
Sn4 Ni1 Sn2 67.539(18) . 2_556
Sn4 Ni1 Sn2 126.23(2) 2_556 2_556
Sn2 Ni1 Sn2 123.94(5) . 2_556
Ni1 Ge1 Ni2 180.0 . .
Ni1 Ge1 Sn6 121.61(2) . 2_556
Ni2 Ge1 Sn6 58.39(2) . 2_556
Ni1 Ge1 Sn6 121.61(2) . .
Ni2 Ge1 Sn6 58.39(2) . .
Sn6 Ge1 Sn6 116.79(4) 2_556 .
Ni1 Ge1 Sn5 122.32(2) . 2_556
Ni2 Ge1 Sn5 57.68(2) . 2_556
Sn6 Ge1 Sn5 58.57(2) 2_556 2_556
Sn6 Ge1 Sn5 87.76(3) . 2_556
Ni1 Ge1 Sn5 122.32(2) . .
Ni2 Ge1 Sn5 57.68(2) . .
Sn6 Ge1 Sn5 87.77(3) 2_556 .
Sn6 Ge1 Sn5 58.57(2) . .
Sn5 Ge1 Sn5 115.35(4) 2_556 .
Ni1 Ge1 Sn3 57.61(2) . 2_556
Ni2 Ge1 Sn3 122.39(2) . 2_556
Sn6 Ge1 Sn3 162.243(14) 2_556 2_556
Sn6 Ge1 Sn3 66.995(15) . 2_556
Sn5 Ge1 Sn3 105.630(15) 2_556 2_556
Sn5 Ge1 Sn3 107.666(15) . 2_556
Ni1 Ge1 Sn3 57.61(2) . .
Ni2 Ge1 Sn3 122.39(2) . .
Sn6 Ge1 Sn3 66.995(15) 2_556 .
Sn6 Ge1 Sn3 162.240(14) . .
Sn5 Ge1 Sn3 107.669(15) 2_556 .
Sn5 Ge1 Sn3 105.627(15) . .
Sn3 Ge1 Sn3 115.21(4) 2_556 .
Ni1 Ge1 Sn4 57.76(2) . .
Ni2 Ge1 Sn4 122.24(2) . .
Sn6 Ge1 Sn4 106.933(15) 2_556 .
Sn6 Ge1 Sn4 105.536(15) . .
Sn5 Ge1 Sn4 164.250(15) 2_556 .
Sn5 Ge1 Sn4 66.917(15) . .
Sn3 Ge1 Sn4 87.64(3) 2_556 .
Sn3 Ge1 Sn4 57.973(19) . .
Ni1 Ge1 Sn4 57.77(2) . 2_556
Ni2 Ge1 Sn4 122.23(2) . 2_556
Sn6 Ge1 Sn4 105.534(15) 2_556 2_556
Sn6 Ge1 Sn4 106.932(15) . 2_556
Sn5 Ge1 Sn4 66.916(15) 2_556 2_556
Sn5 Ge1 Sn4 164.249(15) . 2_556
Sn3 Ge1 Sn4 57.977(19) 2_556 2_556
Sn3 Ge1 Sn4 87.64(3) . 2_556
Sn4 Ge1 Sn4 115.53(4) . 2_556
Ge1 Ni2 Sn5 76.89(3) . 2_556
Ge1 Ni2 Sn5 76.89(3) . .
Sn5 Ni2 Sn5 153.79(6) 2_556 .
Ge1 Ni2 Sn7 144.18(2) . 2_556
Sn5 Ni2 Sn7 73.40(2) 2_556 2_556
Sn5 Ni2 Sn7 130.80(4) . 2_556
Ge1 Ni2 Sn7 144.18(2) . .
Sn5 Ni2 Sn7 130.80(4) 2_556 .
Sn5 Ni2 Sn7 73.40(2) . .
Sn7 Ni2 Sn7 71.64(4) 2_556 .
Ge1 Ni2 Sn6 76.01(3) . 2_556
Sn5 Ni2 Sn6 68.18(2) 2_556 2_556
Sn5 Ni2 Sn6 105.18(2) . 2_556
Sn7 Ni2 Sn6 74.69(2) 2_556 2_556
Sn7 Ni2 Sn6 131.01(4) . 2_556
Ge1 Ni2 Sn6 76.01(3) . .
Sn5 Ni2 Sn6 105.18(2) 2_556 .
Sn5 Ni2 Sn6 68.19(2) . .
Sn7 Ni2 Sn6 131.01(4) 2_556 .
Sn7 Ni2 Sn6 74.69(2) . .
Sn6 Ni2 Sn6 152.01(6) 2_556 .
Ge1 Ni2 Sn8 117.72(3) . 2_556
Sn5 Ni2 Sn8 126.31(2) 2_556 2_556
Sn5 Ni2 Sn8 67.595(18) . 2_556
Sn7 Ni2 Sn8 67.74(3) 2_556 2_556
Sn7 Ni2 Sn8 67.94(3) . 2_556
Sn6 Ni2 Sn8 66.855(17) 2_556 2_556
Sn6 Ni2 Sn8 128.17(2) . 2_556
Ge1 Ni2 Sn8 117.72(3) . .
Sn5 Ni2 Sn8 67.594(18) 2_556 .
Sn5 Ni2 Sn8 126.31(2) . .
Sn7 Ni2 Sn8 67.94(3) 2_556 .
Sn7 Ni2 Sn8 67.75(3) . .
Sn6 Ni2 Sn8 128.17(2) 2_556 .
Sn6 Ni2 Sn8 66.854(18) . .
Sn8 Ni2 Sn8 124.56(5) 2_556 .
Ni2 Sn5 Sn6 56.113(15) . .
Ni2 Sn5 Sn8 57.73(2) . 2_556
Sn6 Sn5 Sn8 108.88(2) . 2_556
Ni2 Sn5 Ge1 45.43(3) . .
Sn6 Sn5 Ge1 60.375(15) . .
Sn8 Sn5 Ge1 89.68(2) 2_556 .
Ni2 Sn5 Sn7 53.34(3) . .
Sn6 Sn5 Sn7 63.188(18) . .
Sn8 Sn5 Sn7 58.473(19) 2_556 .
Ge1 Sn5 Sn7 96.73(2) . .
Ni2 Sn6 Sn5 55.701(15) . .
Ni2 Sn6 Sn8 57.92(2) . .
Sn5 Sn6 Sn8 107.82(2) . .
Ni2 Sn6 Ge1 45.60(3) . .
Sn5 Sn6 Ge1 61.055(16) . .
Sn8 Sn6 Ge1 90.48(2) . .
Ni2 Sn6 Sn7 52.52(3) . .
Sn5 Sn6 Sn7 61.302(18) . .
Sn8 Sn6 Sn7 57.883(18) . .
Ge1 Sn6 Sn7 95.98(2) . .
Ni2 Sn7 Sn8 57.605(16) . .
Ni2 Sn7 Sn8 57.500(16) . 2_556
Sn8 Sn7 Sn8 107.53(2) . 2_556
Ni2 Sn7 Sn7 54.18(2) . 2_556
Sn8 Sn7 Sn7 59.12(2) . 2_556
Sn8 Sn7 Sn7 58.87(2) 2_556 2_556
Ni2 Sn7 Sn5 53.25(2) . .
Sn8 Sn7 Sn5 102.34(2) . .
Sn8 Sn7 Sn5 58.006(19) 2_556 .
Sn7 Sn7 Sn5 100.420(18) 2_556 .
Ni2 Sn7 Sn6 52.794(19) . .
Sn8 Sn7 Sn6 56.993(17) . .
Sn8 Sn7 Sn6 102.36(2) 2_556 .
Sn7 Sn7 Sn6 99.656(17) 2_556 .
Sn5 Sn7 Sn6 55.511(18) . .
Ni2 Sn8 Sn6 55.229(19) . .
Ni2 Sn8 Sn5 54.669(19) . 2_556
Sn6 Sn8 Sn5 89.70(2) . 2_556
Ni2 Sn8 Sn7 54.65(2) . .
Sn6 Sn8 Sn7 65.124(19) . .
Sn5 Sn8 Sn7 106.61(2) 2_556 .
Ni2 Sn8 Sn7 54.56(2) . 2_556
Sn6 Sn8 Sn7 107.49(2) . 2_556
Sn5 Sn8 Sn7 63.52(2) 2_556 2_556
Sn7 Sn8 Sn7 62.01(2) . 2_556
O1 K1 O3 102.6(2) . .
O1 K1 O5 96.31(19) . .
O3 K1 O5 93.69(19) . .
O1 K1 O6 117.3(2) . .
O3 K1 O6 133.86(19) . .
O5 K1 O6 61.29(19) . .
O1 K1 O2 60.7(2) . .
O3 K1 O2 125.7(2) . .
O5 K1 O2 136.4(2) . .
O6 K1 O2 95.08(19) . .
O1 K1 O4 144.1(2) . .
O3 K1 O4 60.10(19) . .
O5 K1 O4 114.9(2) . .
O6 K1 O4 94.09(18) . .
O2 K1 O4 102.0(2) . .
O1 K1 N1 60.8(2) . .
O3 K1 N1 59.9(2) . .
O5 K1 N1 60.3(2) . .
O6 K1 N1 120.6(2) . .
O2 K1 N1 120.5(2) . .
O4 K1 N1 119.1(2) . .
O1 K1 N2 119.9(2) . .
O3 K1 N2 118.9(2) . .
O5 K1 N2 120.2(2) . .
O6 K1 N2 60.1(2) . .
O2 K1 N2 60.1(2) . .
O4 K1 N2 59.8(2) . .
N1 K1 N2 178.8(2) . .
C7 N1 C13 110.5(9) . .
C7 N1 C1 110.7(8) . .
C13 N1 C1 110.5(8) . .
C7 N1 K1 107.5(5) . .
C13 N1 K1 109.1(5) . .
C1 N1 K1 108.5(6) . .
C6 N2 C18 111.7(9) . .
C6 N2 C12 109.6(9) . .
C18 N2 C12 109.3(8) . .
C6 N2 K1 108.3(5) . .
C18 N2 K1 108.7(6) . .
C12 N2 K1 109.2(6) . .
C3 O1 C2 112.1(8) . .
C3 O1 K1 117.4(6) . .
C2 O1 K1 118.9(6) . .
C4 O2 C5 111.6(9) . .
C4 O2 K1 110.5(6) . .
C5 O2 K1 117.4(6) . .
C9 O3 C8 110.7(8) . .
C9 O3 K1 114.1(6) . .
C8 O3 K1 122.2(6) . .
C10 O4 C11 111.0(8) . .
C10 O4 K1 114.5(5) . .
C11 O4 K1 115.2(6) . .
C14 O5 C15 112.0(8) . .
C14 O5 K1 118.8(5) . .
C15 O5 K1 113.2(5) . .
C16 O6 C17 110.8(8) . .
C16 O6 K1 112.9(5) . .
C17 O6 K1 116.9(5) . .
N1 C1 C2 114.2(8) . .
O1 C2 C1 110.0(8) . .
O1 C3 C4 110.2(8) . .
O2 C4 C3 109.8(10) . .
O2 C5 C6 109.2(9) . .
N2 C6 C5 113.8(9) . .
N1 C7 C8 115.0(8) . .
O3 C8 C7 108.8(8) . .
O3 C9 C10 109.6(9) . .
O4 C10 C9 110.4(9) . .
O4 C11 C12 107.7(9) . .
N2 C12 C11 113.5(9) . .
N1 C13 C14 112.9(9) . .
O5 C14 C13 109.9(8) . .
O5 C15 C16 110.4(8) . .
O6 C16 C15 111.5(8) . .
O6 C17 C18 109.3(8) . .
N2 C18 C17 114.0(9) . .
O8 K2 O7 61.20(17) . .
O8 K2 O12 97.30(17) . .
O7 K2 O12 137.94(19) . .
O8 K2 O9 138.77(18) . .
O7 K2 O9 97.96(17) . .
O12 K2 O9 118.51(18) . .
O8 K2 O11 118.39(17) . .
O7 K2 O11 96.94(17) . .
O12 K2 O11 59.93(17) . .
O9 K2 O11 98.06(17) . .
O8 K2 O10 97.86(17) . .
O7 K2 O10 119.34(18) . .
O12 K2 O10 97.97(18) . .
O9 K2 O10 59.71(16) . .
O11 K2 O10 138.38(16) . .
O8 K2 N3 120.62(19) . .
O7 K2 N3 60.48(19) . .
O12 K2 N3 118.8(2) . .
O9 K2 N3 60.56(18) . .
O11 K2 N3 60.05(18) . .
O10 K2 N3 119.33(19) . .
O8 K2 N4 60.53(17) . .
O7 K2 N4 120.56(18) . .
O12 K2 N4 61.00(18) . .
O9 K2 N4 118.35(18) . .
O11 K2 N4 120.01(18) . .
O10 K2 N4 59.71(18) . .
N3 K2 N4 178.8(2) . .
C25 N3 C19 111.5(8) . .
C25 N3 C31 109.2(8) . .
C19 N3 C31 109.5(8) . .
C25 N3 K2 107.9(5) . .
C19 N3 K2 108.8(5) . .
C31 N3 K2 109.9(5) . .
C24 N4 C30 109.4(7) . .
C24 N4 C36 110.5(7) . .
C30 N4 C36 110.3(7) . .
C24 N4 K2 108.7(5) . .
C30 N4 K2 110.3(5) . .
C36 N4 K2 107.8(5) . .
C20 O7 C21 110.5(7) . .
C20 O7 K2 118.5(5) . .
C21 O7 K2 112.2(5) . .
C23 O8 C22 111.4(6) . .
C23 O8 K2 117.3(4) . .
C22 O8 K2 115.1(5) . .
C26 O9 C27 111.4(7) . .
C26 O9 K2 118.5(5) . .
C27 O9 K2 113.8(5) . .
C29 O10 C28 111.0(6) . .
C29 O10 K2 117.2(5) . .
C28 O10 K2 113.4(5) . .
C33 O11 C32 112.0(7) . .
C33 O11 K2 113.6(5) . .
C32 O11 K2 117.5(5) . .
C34 O12 C35 110.6(7) . .
C34 O12 K2 114.1(5) . .
C35 O12 K2 116.1(5) . .
N3 C19 C20 113.5(8) . .
O7 C20 C19 109.8(8) . .
O7 C21 C22 109.9(7) . .
O8 C22 C21 109.5(7) . .
O8 C23 C24 109.4(7) . .
N4 C24 C23 115.0(7) . .
N3 C25 C26 114.5(8) . .
O9 C26 C25 109.1(7) . .
O9 C27 C28 109.1(7) . .
O10 C28 C27 109.1(7) . .
O10 C29 C30 108.9(7) . .
N4 C30 C29 114.4(7) . .
N3 C31 C32 113.8(8) . .
O11 C32 C31 109.4(7) . .
O11 C33 C34 109.0(7) . .
O12 C34 C33 109.5(8) . .
O12 C35 C36 109.8(8) . .
N4 C36 C35 114.8(7) . .
C37 C37 N5 94.5(16) 5_655 .
N7 C39 C39 142(3) . 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sn1 Ni1 2.6118(12) .
Sn1 Sn2 2.9672(8) .
Sn1 Sn2 2.9710(8) 2_556
Sn1 Sn1 2.9729(12) 2_556
Sn1 Sn4 3.1733(8) .
Sn1 Sn3 3.1772(8) .
Sn2 Ni1 2.7449(8) .
Sn2 Sn3 2.9632(8) .
Sn2 Sn1 2.9710(8) 2_556
Sn2 Sn4 3.0031(8) 2_556
Sn3 Ni1 2.6453(6) .
Sn3 Sn4 2.9639(8) .
Sn3 Ge1 3.0547(8) .
Sn4 Ni1 2.6561(6) .
Sn4 Sn2 3.0031(8) 2_556
Sn4 Ge1 3.0615(8) .
Ni1 Ge1 2.2235(17) .
Ni1 Sn1 2.6119(12) 2_556
Ni1 Sn3 2.6453(6) 2_556
Ni1 Sn4 2.6562(6) 2_556
Ni1 Sn2 2.7450(8) 2_556
Ge1 Ni2 2.2294(17) .
Ge1 Sn6 3.0277(8) 2_556
Ge1 Sn6 3.0278(8) .
Ge1 Sn5 3.0480(8) 2_556
Ge1 Sn5 3.0480(8) .
Ge1 Sn3 3.0546(8) 2_556
Ge1 Sn4 3.0616(8) 2_556
Ni2 Sn5 2.6445(6) 2_556
Ni2 Sn5 2.6446(6) .
Ni2 Sn7 2.6477(12) 2_556
Ni2 Sn7 2.6477(12) .
Ni2 Sn6 2.6575(6) 2_556
Ni2 Sn6 2.6575(6) .
Ni2 Sn8 2.7410(8) 2_556
Ni2 Sn8 2.7410(8) .
Sn5 Sn6 2.9720(8) .
Sn5 Sn8 2.9968(8) 2_556
Sn5 Sn7 3.1629(8) .
Sn6 Sn8 2.9747(8) .
Sn6 Sn7 3.2182(8) .
Sn7 Sn8 3.0044(8) .
Sn7 Sn8 3.0120(8) 2_556
Sn7 Sn7 3.0991(12) 2_556
Sn8 Sn5 2.9968(8) 2_556
Sn8 Sn7 3.0121(8) 2_556
K1 O1 2.760(6) .
K1 O3 2.786(6) .
K1 O5 2.803(6) .
K1 O6 2.822(6) .
K1 O2 2.849(7) .
K1 O4 2.852(6) .
K1 N1 3.005(7) .
K1 N2 3.033(8) .
N1 C7 1.459(13) .
N1 C13 1.472(13) .
N1 C1 1.478(13) .
N2 C6 1.454(14) .
N2 C18 1.464(12) .
N2 C12 1.485(13) .
O1 C3 1.424(13) .
O1 C2 1.427(13) .
O2 C4 1.429(12) .
O2 C5 1.439(12) .
O3 C9 1.421(11) .
O3 C8 1.428(12) .
O4 C10 1.412(11) .
O4 C11 1.414(13) .
O5 C14 1.417(12) .
O5 C15 1.421(11) .
O6 C16 1.400(12) .
O6 C17 1.420(12) .
C1 C2 1.483(16) .
C3 C4 1.476(16) .
C5 C6 1.495(16) .
C7 C8 1.489(15) .
C9 C10 1.474(16) .
C11 C12 1.499(15) .
C13 C14 1.503(15) .
C15 C16 1.482(15) .
C17 C18 1.489(16) .
K2 O8 2.795(5) .
K2 O7 2.809(5) .
K2 O12 2.819(6) .
K2 O9 2.831(6) .
K2 O11 2.868(6) .
K2 O10 2.877(6) .
K2 N3 2.997(7) .
K2 N4 3.018(7) .
N3 C25 1.465(11) .
N3 C19 1.468(11) .
N3 C31 1.471(12) .
N4 C24 1.456(11) .
N4 C30 1.467(11) .
N4 C36 1.470(11) .
O7 C20 1.418(11) .
O7 C21 1.428(11) .
O8 C23 1.433(10) .
O8 C22 1.438(10) .
O9 C26 1.412(10) .
O9 C27 1.425(10) .
O10 C29 1.418(10) .
O10 C28 1.421(10) .
O11 C33 1.416(10) .
O11 C32 1.425(10) .
O12 C34 1.424(11) .
O12 C35 1.428(11) .
C19 C20 1.499(14) .
C21 C22 1.488(13) .
C23 C24 1.486(12) .
C25 C26 1.505(13) .
C27 C28 1.477(13) .
C29 C30 1.509(12) .
C31 C32 1.500(14) .
C33 C34 1.486(13) .
C35 C36 1.487(14) .
N5 C37 1.68(2) .
C37 C37 1.34(3) 5_655
C39 N7 1.16(2) .
C39 C39 1.45(3) 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Sn2 Sn1 Sn2 Ni1 30.11(3) 2_556 .
Sn1 Sn1 Sn2 Ni1 65.34(3) 2_556 .
Sn4 Sn1 Sn2 Ni1 -30.72(2) . .
Sn3 Sn1 Sn2 Ni1 -63.82(2) . .
Ni1 Sn1 Sn2 Sn3 63.82(2) . .
Sn2 Sn1 Sn2 Sn3 93.93(2) 2_556 .
Sn1 Sn1 Sn2 Sn3 129.17(2) 2_556 .
Sn4 Sn1 Sn2 Sn3 33.11(2) . .
Ni1 Sn1 Sn2 Sn1 -65.34(3) . 2_556
Sn2 Sn1 Sn2 Sn1 -35.23(3) 2_556 2_556
Sn4 Sn1 Sn2 Sn1 -96.06(2) . 2_556
Sn3 Sn1 Sn2 Sn1 -129.17(2) . 2_556
Ni1 Sn1 Sn2 Sn4 -18.89(3) . 2_556
Sn2 Sn1 Sn2 Sn4 11.22(3) 2_556 2_556
Sn1 Sn1 Sn2 Sn4 46.455(17) 2_556 2_556
Sn4 Sn1 Sn2 Sn4 -49.60(3) . 2_556
Sn3 Sn1 Sn2 Sn4 -82.71(2) . 2_556
Sn1 Sn2 Sn3 Ni1 -62.69(3) . .
Sn1 Sn2 Sn3 Ni1 -18.21(3) 2_556 .
Sn4 Sn2 Sn3 Ni1 44.92(3) 2_556 .
Ni1 Sn2 Sn3 Sn4 25.75(3) . .
Sn1 Sn2 Sn3 Sn4 -36.94(2) . .
Sn1 Sn2 Sn3 Sn4 7.54(3) 2_556 .
Sn4 Sn2 Sn3 Sn4 70.67(2) 2_556 .
Ni1 Sn2 Sn3 Ge1 -33.72(3) . .
Sn1 Sn2 Sn3 Ge1 -96.41(2) . .
Sn1 Sn2 Sn3 Ge1 -51.93(3) 2_556 .
Sn4 Sn2 Sn3 Ge1 11.20(2) 2_556 .
Ni1 Sn2 Sn3 Sn1 62.69(3) . .
Sn1 Sn2 Sn3 Sn1 44.48(2) 2_556 .
Sn4 Sn2 Sn3 Sn1 107.61(2) 2_556 .
Sn2 Sn1 Sn3 Ni1 72.69(2) . .
Sn2 Sn1 Sn3 Ni1 -31.92(2) 2_556 .
Sn1 Sn1 Sn3 Ni1 29.49(2) 2_556 .
Sn4 Sn1 Sn3 Ni1 -67.23(2) . .
Ni1 Sn1 Sn3 Sn2 -72.69(2) . .
Sn2 Sn1 Sn3 Sn2 -104.61(2) 2_556 .
Sn1 Sn1 Sn3 Sn2 -43.20(2) 2_556 .
Sn4 Sn1 Sn3 Sn2 -139.92(2) . .
Ni1 Sn1 Sn3 Sn4 67.23(2) . .
Sn2 Sn1 Sn3 Sn4 139.92(2) . .
Sn2 Sn1 Sn3 Sn4 35.31(2) 2_556 .
Sn1 Sn1 Sn3 Sn4 96.72(3) 2_556 .
Ni1 Sn1 Sn3 Ge1 14.152(16) . .
Sn2 Sn1 Sn3 Ge1 86.84(2) . .
Sn2 Sn1 Sn3 Ge1 -17.77(2) 2_556 .
Sn1 Sn1 Sn3 Ge1 43.64(3) 2_556 .
Sn4 Sn1 Sn3 Ge1 -53.080(16) . .
Sn2 Sn3 Sn4 Ni1 -26.41(4) . .
Ge1 Sn3 Sn4 Ni1 53.21(4) . .
Sn1 Sn3 Sn4 Ni1 -61.47(4) . .
Ni1 Sn3 Sn4 Sn2 25.68(4) . 2_556
Sn2 Sn3 Sn4 Sn2 -0.73(3) . 2_556
Ge1 Sn3 Sn4 Sn2 78.89(3) . 2_556
Sn1 Sn3 Sn4 Sn2 -35.79(2) . 2_556
Ni1 Sn3 Sn4 Ge1 -53.21(4) . .
Sn2 Sn3 Sn4 Ge1 -79.62(3) . .
Sn1 Sn3 Sn4 Ge1 -114.68(3) . .
Ni1 Sn3 Sn4 Sn1 61.47(4) . .
Sn2 Sn3 Sn4 Sn1 35.06(2) . .
Ge1 Sn3 Sn4 Sn1 114.68(3) . .
Sn2 Sn1 Sn4 Ni1 32.77(2) . .
Sn2 Sn1 Sn4 Ni1 -71.99(2) 2_556 .
Sn1 Sn1 Sn4 Ni1 -28.85(2) 2_556 .
Sn3 Sn1 Sn4 Ni1 66.709(19) . .
Ni1 Sn1 Sn4 Sn3 -66.709(19) . .
Sn2 Sn1 Sn4 Sn3 -33.94(2) . .
Sn2 Sn1 Sn4 Sn3 -138.70(2) 2_556 .
Sn1 Sn1 Sn4 Sn3 -95.56(3) 2_556 .
Ni1 Sn1 Sn4 Sn2 71.99(2) . 2_556
Sn2 Sn1 Sn4 Sn2 104.77(2) . 2_556
Sn1 Sn1 Sn4 Sn2 43.14(2) 2_556 2_556
Sn3 Sn1 Sn4 Sn2 138.70(2) . 2_556
Ni1 Sn1 Sn4 Ge1 -13.804(16) . .
Sn2 Sn1 Sn4 Ge1 18.97(2) . .
Sn2 Sn1 Sn4 Ge1 -85.80(2) 2_556 .
Sn1 Sn1 Sn4 Ge1 -42.66(3) 2_556 .
Sn3 Sn1 Sn4 Ge1 52.905(16) . .
Sn2 Sn1 Ni1 Ge1 -106.79(2) . .
Sn2 Sn1 Ni1 Ge1 106.93(2) 2_556 .
Sn1 Sn1 Ni1 Ge1 180.0 2_556 .
Sn4 Sn1 Ni1 Ge1 35.07(3) . .
Sn3 Sn1 Ni1 Ge1 -35.97(3) . .
Sn2 Sn1 Ni1 Sn1 73.21(2) . 2_556
Sn2 Sn1 Ni1 Sn1 -73.07(2) 2_556 2_556
Sn4 Sn1 Ni1 Sn1 -144.93(3) . 2_556
Sn3 Sn1 Ni1 Sn1 144.03(3) . 2_556
Sn2 Sn1 Ni1 Sn3 120.25(4) . 2_556
Sn2 Sn1 Ni1 Sn3 -26.03(3) 2_556 2_556
Sn1 Sn1 Ni1 Sn3 47.04(4) 2_556 2_556
Sn4 Sn1 Ni1 Sn3 -97.89(3) . 2_556
Sn3 Sn1 Ni1 Sn3 -168.93(3) . 2_556
Sn2 Sn1 Ni1 Sn3 -70.819(19) . .
Sn2 Sn1 Ni1 Sn3 142.90(3) 2_556 .
Sn1 Sn1 Ni1 Sn3 -144.03(3) 2_556 .
Sn4 Sn1 Ni1 Sn3 71.04(2) . .
Sn2 Sn1 Ni1 Sn4 -141.86(3) . .
Sn2 Sn1 Ni1 Sn4 71.86(2) 2_556 .
Sn1 Sn1 Ni1 Sn4 144.93(3) 2_556 .
Sn3 Sn1 Ni1 Sn4 -71.04(2) . .
Sn2 Sn1 Ni1 Sn4 27.23(3) . 2_556
Sn2 Sn1 Ni1 Sn4 -119.05(4) 2_556 2_556
Sn1 Sn1 Ni1 Sn4 -45.98(4) 2_556 2_556
Sn4 Sn1 Ni1 Sn4 169.09(3) . 2_556
Sn3 Sn1 Ni1 Sn4 98.05(3) . 2_556
Sn2 Sn1 Ni1 Sn2 -146.28(3) 2_556 .
Sn1 Sn1 Ni1 Sn2 -73.21(2) 2_556 .
Sn4 Sn1 Ni1 Sn2 141.86(3) . .
Sn3 Sn1 Ni1 Sn2 70.819(19) . .
Sn2 Sn1 Ni1 Sn2 146.28(3) . 2_556
Sn1 Sn1 Ni1 Sn2 73.07(2) 2_556 2_556
Sn4 Sn1 Ni1 Sn2 -71.86(2) . 2_556
Sn3 Sn1 Ni1 Sn2 -142.90(3) . 2_556
Sn2 Sn3 Ni1 Ge1 -128.54(2) . .
Sn4 Sn3 Ni1 Ge1 81.14(2) . .
Sn1 Sn3 Ni1 Ge1 159.950(17) . .
Sn2 Sn3 Ni1 Sn1 71.51(3) . .
Sn4 Sn3 Ni1 Sn1 -78.81(2) . .
Ge1 Sn3 Ni1 Sn1 -159.950(17) . .
Sn2 Sn3 Ni1 Sn1 26.17(3) . 2_556
Sn4 Sn3 Ni1 Sn1 -124.14(5) . 2_556
Ge1 Sn3 Ni1 Sn1 154.71(3) . 2_556
Sn1 Sn3 Ni1 Sn1 -45.34(5) . 2_556
Sn2 Sn3 Ni1 Sn3 -128.55(2) . 2_556
Sn4 Sn3 Ni1 Sn3 81.14(2) . 2_556
Ge1 Sn3 Ni1 Sn3 0.0 . 2_556
Sn1 Sn3 Ni1 Sn3 159.943(17) . 2_556
Sn2 Sn3 Ni1 Sn4 150.31(4) . .
Ge1 Sn3 Ni1 Sn4 -81.14(2) . .
Sn1 Sn3 Ni1 Sn4 78.81(2) . .
Sn2 Sn3 Ni1 Sn4 -56.16(3) . 2_556
Sn4 Sn3 Ni1 Sn4 153.53(6) . 2_556
Ge1 Sn3 Ni1 Sn4 72.38(4) . 2_556
Sn1 Sn3 Ni1 Sn4 -127.67(5) . 2_556
Sn4 Sn3 Ni1 Sn2 -150.31(4) . .
Ge1 Sn3 Ni1 Sn2 128.54(2) . .
Sn1 Sn3 Ni1 Sn2 -71.51(3) . .
Sn2 Sn3 Ni1 Sn2 115.84(7) . 2_556
Sn4 Sn3 Ni1 Sn2 -34.47(4) . 2_556
Ge1 Sn3 Ni1 Sn2 -115.62(5) . 2_556
Sn1 Sn3 Ni1 Sn2 44.33(5) . 2_556
Sn3 Sn4 Ni1 Ge1 -81.18(2) . .
Sn2 Sn4 Ni1 Ge1 128.02(2) 2_556 .
Sn1 Sn4 Ni1 Ge1 -160.404(17) . .
Sn3 Sn4 Ni1 Sn1 79.22(2) . .
Sn2 Sn4 Ni1 Sn1 -71.58(3) 2_556 .
Ge1 Sn4 Ni1 Sn1 160.404(17) . .
Sn3 Sn4 Ni1 Sn1 123.64(5) . 2_556
Sn2 Sn4 Ni1 Sn1 -27.17(3) 2_556 2_556
Ge1 Sn4 Ni1 Sn1 -155.18(3) . 2_556
Sn1 Sn4 Ni1 Sn1 44.41(5) . 2_556
Sn3 Sn4 Ni1 Sn3 -153.58(6) . 2_556
Sn2 Sn4 Ni1 Sn3 55.62(3) 2_556 2_556
Ge1 Sn4 Ni1 Sn3 -72.40(4) . 2_556
Sn1 Sn4 Ni1 Sn3 127.19(4) . 2_556
Sn2 Sn4 Ni1 Sn3 -150.80(4) 2_556 .
Ge1 Sn4 Ni1 Sn3 81.18(2) . .
Sn1 Sn4 Ni1 Sn3 -79.22(2) . .
Sn3 Sn4 Ni1 Sn4 -81.18(2) . 2_556
Sn2 Sn4 Ni1 Sn4 128.02(2) 2_556 2_556
Ge1 Sn4 Ni1 Sn4 0.0 . 2_556
Sn1 Sn4 Ni1 Sn4 -160.404(17) . 2_556
Sn3 Sn4 Ni1 Sn2 34.32(4) . .
Sn2 Sn4 Ni1 Sn2 -116.49(7) 2_556 .
Ge1 Sn4 Ni1 Sn2 115.50(5) . .
Sn1 Sn4 Ni1 Sn2 -44.91(5) . .
Sn3 Sn4 Ni1 Sn2 150.80(4) . 2_556
Ge1 Sn4 Ni1 Sn2 -128.02(2) . 2_556
Sn1 Sn4 Ni1 Sn2 71.58(3) . 2_556
Sn3 Sn2 Ni1 Ge1 59.77(2) . .
Sn1 Sn2 Ni1 Ge1 141.883(19) . .
Sn1 Sn2 Ni1 Ge1 -141.915(19) 2_556 .
Sn4 Sn2 Ni1 Ge1 -60.48(2) 2_556 .
Sn3 Sn2 Ni1 Sn1 -82.11(2) . .
Sn1 Sn2 Ni1 Sn1 76.20(4) 2_556 .
Sn4 Sn2 Ni1 Sn1 157.64(3) 2_556 .
Sn3 Sn2 Ni1 Sn1 -158.31(3) . 2_556
Sn1 Sn2 Ni1 Sn1 -76.20(4) . 2_556
Sn4 Sn2 Ni1 Sn1 81.43(2) 2_556 2_556
Sn3 Sn2 Ni1 Sn3 154.85(7) . 2_556
Sn1 Sn2 Ni1 Sn3 -123.04(6) . 2_556
Sn1 Sn2 Ni1 Sn3 -46.84(5) 2_556 2_556
Sn4 Sn2 Ni1 Sn3 34.60(4) 2_556 2_556
Sn1 Sn2 Ni1 Sn3 82.11(2) . .
Sn1 Sn2 Ni1 Sn3 158.31(3) 2_556 .
Sn4 Sn2 Ni1 Sn3 -120.25(4) 2_556 .
Sn3 Sn2 Ni1 Sn4 -34.69(4) . .
Sn1 Sn2 Ni1 Sn4 47.42(4) . .
Sn1 Sn2 Ni1 Sn4 123.62(6) 2_556 .
Sn4 Sn2 Ni1 Sn4 -154.95(7) 2_556 .
Sn3 Sn2 Ni1 Sn4 120.25(4) . 2_556
Sn1 Sn2 Ni1 Sn4 -157.64(3) . 2_556
Sn1 Sn2 Ni1 Sn4 -81.43(2) 2_556 2_556
Sn3 Sn2 Ni1 Sn2 -120.23(2) . 2_556
Sn1 Sn2 Ni1 Sn2 -38.119(19) . 2_556
Sn1 Sn2 Ni1 Sn2 38.083(19) 2_556 2_556
Sn4 Sn2 Ni1 Sn2 119.52(2) 2_556 2_556
Sn1 Ni1 Ge1 Ni2 172(100) . .
Sn1 Ni1 Ge1 Ni2 -8(49) 2_556 .
Sn3 Ni1 Ge1 Ni2 -44(65) 2_556 .
Sn3 Ni1 Ge1 Ni2 136(49) . .
Sn4 Ni1 Ge1 Ni2 -154(65) . .
Sn4 Ni1 Ge1 Ni2 26(49) 2_556 .
Sn2 Ni1 Ge1 Ni2 82(49) . .
Sn2 Ni1 Ge1 Ni2 -98(65) 2_556 .
Sn1 Ni1 Ge1 Sn6 56.41(3) . 2_556
Sn1 Ni1 Ge1 Sn6 -123.59(3) 2_556 2_556
Sn3 Ni1 Ge1 Sn6 -159.048(16) 2_556 2_556
Sn3 Ni1 Ge1 Sn6 20.955(16) . 2_556
Sn4 Ni1 Ge1 Sn6 90.932(18) . 2_556
Sn4 Ni1 Ge1 Sn6 -89.068(18) 2_556 2_556
Sn2 Ni1 Ge1 Sn6 -33.498(18) . 2_556
Sn2 Ni1 Ge1 Sn6 146.504(18) 2_556 2_556
Sn1 Ni1 Ge1 Sn6 -123.59(3) . .
Sn1 Ni1 Ge1 Sn6 56.41(3) 2_556 .
Sn3 Ni1 Ge1 Sn6 20.951(16) 2_556 .
Sn3 Ni1 Ge1 Sn6 -159.045(16) . .
Sn4 Ni1 Ge1 Sn6 -89.069(18) . .
Sn4 Ni1 Ge1 Sn6 90.931(18) 2_556 .
Sn2 Ni1 Ge1 Sn6 146.501(18) . .
Sn2 Ni1 Ge1 Sn6 -33.497(18) 2_556 .
Sn1 Ni1 Ge1 Sn5 126.83(3) . 2_556
Sn1 Ni1 Ge1 Sn5 -53.17(3) 2_556 2_556
Sn3 Ni1 Ge1 Sn5 -88.632(18) 2_556 2_556
Sn3 Ni1 Ge1 Sn5 91.371(18) . 2_556
Sn4 Ni1 Ge1 Sn5 161.347(17) . 2_556
Sn4 Ni1 Ge1 Sn5 -18.653(17) 2_556 2_556
Sn2 Ni1 Ge1 Sn5 36.917(19) . 2_556
Sn2 Ni1 Ge1 Sn5 -143.081(19) 2_556 2_556
Sn1 Ni1 Ge1 Sn5 -53.17(3) . .
Sn1 Ni1 Ge1 Sn5 126.83(3) 2_556 .
Sn3 Ni1 Ge1 Sn5 91.368(18) 2_556 .
Sn3 Ni1 Ge1 Sn5 -88.629(18) . .
Sn4 Ni1 Ge1 Sn5 -18.653(17) . .
Sn4 Ni1 Ge1 Sn5 161.347(17) 2_556 .
Sn2 Ni1 Ge1 Sn5 -143.083(19) . .
Sn2 Ni1 Ge1 Sn5 36.919(19) 2_556 .
Sn1 Ni1 Ge1 Sn3 -144.54(3) . 2_556
Sn1 Ni1 Ge1 Sn3 35.46(3) 2_556 2_556
Sn3 Ni1 Ge1 Sn3 180.0 . 2_556
Sn4 Ni1 Ge1 Sn3 -110.020(18) . 2_556
Sn4 Ni1 Ge1 Sn3 69.980(18) 2_556 2_556
Sn2 Ni1 Ge1 Sn3 125.550(18) . 2_556
Sn2 Ni1 Ge1 Sn3 -54.448(18) 2_556 2_556
Sn1 Ni1 Ge1 Sn3 35.46(3) . .
Sn1 Ni1 Ge1 Sn3 -144.54(3) 2_556 .
Sn3 Ni1 Ge1 Sn3 180.0 2_556 .
Sn4 Ni1 Ge1 Sn3 69.976(18) . .
Sn4 Ni1 Ge1 Sn3 -110.024(18) 2_556 .
Sn2 Ni1 Ge1 Sn3 -54.454(18) . .
Sn2 Ni1 Ge1 Sn3 125.548(18) 2_556 .
Sn1 Ni1 Ge1 Sn4 -34.52(3) . .
Sn1 Ni1 Ge1 Sn4 145.48(3) 2_556 .
Sn3 Ni1 Ge1 Sn4 110.020(18) 2_556 .
Sn3 Ni1 Ge1 Sn4 -69.976(18) . .
Sn4 Ni1 Ge1 Sn4 180.0 2_556 .
Sn2 Ni1 Ge1 Sn4 -124.430(19) . .
Sn2 Ni1 Ge1 Sn4 55.572(19) 2_556 .
Sn1 Ni1 Ge1 Sn4 145.48(3) . 2_556
Sn1 Ni1 Ge1 Sn4 -34.52(3) 2_556 2_556
Sn3 Ni1 Ge1 Sn4 -69.980(18) 2_556 2_556
Sn3 Ni1 Ge1 Sn4 110.024(17) . 2_556
Sn4 Ni1 Ge1 Sn4 180.0 . 2_556
Sn2 Ni1 Ge1 Sn4 55.570(19) . 2_556
Sn2 Ni1 Ge1 Sn4 -124.428(19) 2_556 2_556
Sn2 Sn3 Ge1 Ni1 41.706(13) . .
Sn4 Sn3 Ge1 Ni1 -69.621(17) . .
Sn1 Sn3 Ge1 Ni1 -15.824(12) . .
Ni1 Sn3 Ge1 Ni2 180.0 . .
Sn2 Sn3 Ge1 Ni2 -138.294(13) . .
Sn4 Sn3 Ge1 Ni2 110.379(17) . .
Sn1 Sn3 Ge1 Ni2 164.176(12) . .
Ni1 Sn3 Ge1 Sn6 -160.676(15) . 2_556
Sn2 Sn3 Ge1 Sn6 -118.97(2) . 2_556
Sn4 Sn3 Ge1 Sn6 129.70(2) . 2_556
Sn1 Sn3 Ge1 Sn6 -176.50(2) . 2_556
Ni1 Sn3 Ge1 Sn6 93.09(12) . .
Sn2 Sn3 Ge1 Sn6 134.80(12) . .
Sn4 Sn3 Ge1 Sn6 23.47(12) . .
Sn1 Sn3 Ge1 Sn6 77.27(12) . .
Ni1 Sn3 Ge1 Sn5 -117.55(2) . 2_556
Sn2 Sn3 Ge1 Sn5 -75.84(3) . 2_556
Sn4 Sn3 Ge1 Sn5 172.83(3) . 2_556
Sn1 Sn3 Ge1 Sn5 -133.37(3) . 2_556
Ni1 Sn3 Ge1 Sn5 118.69(2) . .
Sn2 Sn3 Ge1 Sn5 160.40(3) . .
Sn4 Sn3 Ge1 Sn5 49.07(2) . .
Sn1 Sn3 Ge1 Sn5 102.86(3) . .
Ni1 Sn3 Ge1 Sn3 0.0 . 2_556
Sn2 Sn3 Ge1 Sn3 41.709(13) . 2_556
Sn4 Sn3 Ge1 Sn3 -69.618(17) . 2_556
Sn1 Sn3 Ge1 Sn3 -15.821(12) . 2_556
Ni1 Sn3 Ge1 Sn4 69.621(17) . .
Sn2 Sn3 Ge1 Sn4 111.33(2) . .
Sn1 Sn3 Ge1 Sn4 53.80(2) . .
Ni1 Sn3 Ge1 Sn4 -52.696(18) . 2_556
Sn2 Sn3 Ge1 Sn4 -10.99(2) . 2_556
Sn4 Sn3 Ge1 Sn4 -122.32(3) . 2_556
Sn1 Sn3 Ge1 Sn4 -68.52(2) . 2_556
Sn3 Sn4 Ge1 Ni1 69.354(17) . .
Sn2 Sn4 Ge1 Ni1 -41.723(13) 2_556 .
Sn1 Sn4 Ge1 Ni1 15.467(12) . .
Ni1 Sn4 Ge1 Ni2 180.0 . .
Sn3 Sn4 Ge1 Ni2 -110.646(17) . .
Sn2 Sn4 Ge1 Ni2 138.277(13) 2_556 .
Sn1 Sn4 Ge1 Ni2 -164.533(12) . .
Ni1 Sn4 Ge1 Sn6 -117.11(2) . 2_556
Sn3 Sn4 Ge1 Sn6 -47.75(2) . 2_556
Sn2 Sn4 Ge1 Sn6 -158.83(3) 2_556 2_556
Sn1 Sn4 Ge1 Sn6 -101.64(3) . 2_556
Ni1 Sn4 Ge1 Sn6 117.89(2) . .
Sn3 Sn4 Ge1 Sn6 -172.76(3) . .
Sn2 Sn4 Ge1 Sn6 76.17(3) 2_556 .
Sn1 Sn4 Ge1 Sn6 133.36(3) . .
Ni1 Sn4 Ge1 Sn5 -95.33(14) . 2_556
Sn3 Sn4 Ge1 Sn5 -25.98(13) . 2_556
Sn2 Sn4 Ge1 Sn5 -137.05(14) 2_556 2_556
Sn1 Sn4 Ge1 Sn5 -79.86(14) . 2_556
Ni1 Sn4 Ge1 Sn5 162.915(16) . .
Sn3 Sn4 Ge1 Sn5 -127.73(2) . .
Sn2 Sn4 Ge1 Sn5 121.19(2) 2_556 .
Sn1 Sn4 Ge1 Sn5 178.38(2) . .
Ni1 Sn4 Ge1 Sn3 52.565(18) . 2_556
Sn3 Sn4 Ge1 Sn3 121.92(3) . 2_556
Sn2 Sn4 Ge1 Sn3 10.84(2) 2_556 2_556
Sn1 Sn4 Ge1 Sn3 68.03(2) . 2_556
Ni1 Sn4 Ge1 Sn3 -69.354(17) . .
Sn2 Sn4 Ge1 Sn3 -111.08(2) 2_556 .
Sn1 Sn4 Ge1 Sn3 -53.89(2) . .
Ni1 Sn4 Ge1 Sn4 0.0 . 2_556
Sn3 Sn4 Ge1 Sn4 69.354(17) . 2_556
Sn2 Sn4 Ge1 Sn4 -41.723(13) 2_556 2_556
Sn1 Sn4 Ge1 Sn4 15.467(12) . 2_556
Ni1 Ge1 Ni2 Sn5 -45(62) . 2_556
Sn6 Ge1 Ni2 Sn5 70.415(18) 2_556 2_556
Sn6 Ge1 Ni2 Sn5 -109.584(18) . 2_556
Sn5 Ge1 Ni2 Sn5 180.0 . 2_556
Sn3 Ge1 Ni2 Sn5 -88.632(18) 2_556 2_556
Sn3 Ge1 Ni2 Sn5 91.371(18) . 2_556
Sn4 Ge1 Ni2 Sn5 161.347(17) . 2_556
Sn4 Ge1 Ni2 Sn5 -18.653(17) 2_556 2_556
Ni1 Ge1 Ni2 Sn5 135(76) . .
Sn6 Ge1 Ni2 Sn5 -109.584(18) 2_556 .
Sn6 Ge1 Ni2 Sn5 70.416(18) . .
Sn5 Ge1 Ni2 Sn5 180.0 2_556 .
Sn3 Ge1 Ni2 Sn5 91.368(18) 2_556 .
Sn3 Ge1 Ni2 Sn5 -88.629(18) . .
Sn4 Ge1 Ni2 Sn5 -18.653(17) . .
Sn4 Ge1 Ni2 Sn5 161.347(17) 2_556 .
Ni1 Ge1 Ni2 Sn7 -79(58) . 2_556
Sn6 Ge1 Ni2 Sn7 35.87(2) 2_556 2_556
Sn6 Ge1 Ni2 Sn7 -144.13(2) . 2_556
Sn5 Ge1 Ni2 Sn7 -34.54(2) 2_556 2_556
Sn5 Ge1 Ni2 Sn7 145.46(2) . 2_556
Sn3 Ge1 Ni2 Sn7 -123.17(2) 2_556 2_556
Sn3 Ge1 Ni2 Sn7 56.83(2) . 2_556
Sn4 Ge1 Ni2 Sn7 126.80(2) . 2_556
Sn4 Ge1 Ni2 Sn7 -53.20(2) 2_556 2_556
Ni1 Ge1 Ni2 Sn7 101(71) . .
Sn6 Ge1 Ni2 Sn7 -144.12(2) 2_556 .
Sn6 Ge1 Ni2 Sn7 35.88(2) . .
Sn5 Ge1 Ni2 Sn7 145.46(2) 2_556 .
Sn5 Ge1 Ni2 Sn7 -34.54(2) . .
Sn3 Ge1 Ni2 Sn7 56.83(2) 2_556 .
Sn3 Ge1 Ni2 Sn7 -123.17(2) . .
Sn4 Ge1 Ni2 Sn7 -53.19(2) . .
Sn4 Ge1 Ni2 Sn7 126.81(2) 2_556 .
Ni1 Ge1 Ni2 Sn6 -115(57) . 2_556
Sn6 Ge1 Ni2 Sn6 180.0 . 2_556
Sn5 Ge1 Ni2 Sn6 -70.415(18) 2_556 2_556
Sn5 Ge1 Ni2 Sn6 109.584(18) . 2_556
Sn3 Ge1 Ni2 Sn6 -159.048(16) 2_556 2_556
Sn3 Ge1 Ni2 Sn6 20.955(16) . 2_556
Sn4 Ge1 Ni2 Sn6 90.932(18) . 2_556
Sn4 Ge1 Ni2 Sn6 -89.068(18) 2_556 2_556
Ni1 Ge1 Ni2 Sn6 65(71) . .
Sn6 Ge1 Ni2 Sn6 180.0 2_556 .
Sn5 Ge1 Ni2 Sn6 109.584(18) 2_556 .
Sn5 Ge1 Ni2 Sn6 -70.416(18) . .
Sn3 Ge1 Ni2 Sn6 20.951(16) 2_556 .
Sn3 Ge1 Ni2 Sn6 -159.045(16) . .
Sn4 Ge1 Ni2 Sn6 -89.069(18) . .
Sn4 Ge1 Ni2 Sn6 90.931(18) 2_556 .
Ni1 Ge1 Ni2 Sn8 -169(100) . 2_556
Sn6 Ge1 Ni2 Sn8 -53.946(18) 2_556 2_556
Sn6 Ge1 Ni2 Sn8 126.055(18) . 2_556
Sn5 Ge1 Ni2 Sn8 -124.362(19) 2_556 2_556
Sn5 Ge1 Ni2 Sn8 55.638(19) . 2_556
Sn3 Ge1 Ni2 Sn8 147.006(18) 2_556 2_556
Sn3 Ge1 Ni2 Sn8 -32.991(18) . 2_556
Sn4 Ge1 Ni2 Sn8 36.985(18) . 2_556
Sn4 Ge1 Ni2 Sn8 -143.015(18) 2_556 2_556
Ni1 Ge1 Ni2 Sn8 11(59) . .
Sn6 Ge1 Ni2 Sn8 126.053(18) 2_556 .
Sn6 Ge1 Ni2 Sn8 -53.946(18) . .
Sn5 Ge1 Ni2 Sn8 55.637(19) 2_556 .
Sn5 Ge1 Ni2 Sn8 -124.363(19) . .
Sn3 Ge1 Ni2 Sn8 -32.995(18) 2_556 .
Sn3 Ge1 Ni2 Sn8 147.008(18) . .
Sn4 Ge1 Ni2 Sn8 -143.016(18) . .
Sn4 Ge1 Ni2 Sn8 36.984(18) 2_556 .
Ge1 Ni2 Sn5 Sn6 -79.97(2) . .
Sn5 Ni2 Sn5 Sn6 -79.97(2) 2_556 .
Sn7 Ni2 Sn5 Sn6 126.03(5) 2_556 .
Sn7 Ni2 Sn5 Sn6 79.78(2) . .
Sn6 Ni2 Sn5 Sn6 -151.28(6) 2_556 .
Sn8 Ni2 Sn5 Sn6 152.26(4) 2_556 .
Sn8 Ni2 Sn5 Sn6 34.97(4) . .
Ge1 Ni2 Sn5 Sn8 127.77(2) . 2_556
Sn5 Ni2 Sn5 Sn8 127.77(2) 2_556 2_556
Sn7 Ni2 Sn5 Sn8 -26.23(3) 2_556 2_556
Sn7 Ni2 Sn5 Sn8 -72.48(3) . 2_556
Sn6 Ni2 Sn5 Sn8 56.47(3) 2_556 2_556
Sn6 Ni2 Sn5 Sn8 -152.26(4) . 2_556
Sn8 Ni2 Sn5 Sn8 -117.29(7) . 2_556
Sn5 Ni2 Sn5 Ge1 -0.001(2) 2_556 .
Sn7 Ni2 Sn5 Ge1 -154.00(3) 2_556 .
Sn7 Ni2 Sn5 Ge1 159.743(16) . .
Sn6 Ni2 Sn5 Ge1 -71.31(4) 2_556 .
Sn6 Ni2 Sn5 Ge1 79.97(2) . .
Sn8 Ni2 Sn5 Ge1 -127.77(2) 2_556 .
Sn8 Ni2 Sn5 Ge1 114.93(5) . .
Ge1 Ni2 Sn5 Sn7 -159.743(16) . .
Sn5 Ni2 Sn5 Sn7 -159.743(17) 2_556 .
Sn7 Ni2 Sn5 Sn7 46.26(5) 2_556 .
Sn6 Ni2 Sn5 Sn7 128.95(4) 2_556 .
Sn6 Ni2 Sn5 Sn7 -79.78(2) . .
Sn8 Ni2 Sn5 Sn7 72.48(3) 2_556 .
Sn8 Ni2 Sn5 Sn7 -44.81(5) . .
Ni1 Ge1 Sn5 Ni2 180.0 . .
Sn6 Ge1 Sn5 Ni2 53.418(19) 2_556 .
Sn6 Ge1 Sn5 Ni2 -70.113(17) . .
Sn5 Ge1 Sn5 Ni2 0.0 2_556 .
Sn3 Ge1 Sn5 Ni2 -117.63(2) 2_556 .
Sn3 Ge1 Sn5 Ni2 118.77(2) . .
Sn4 Ge1 Sn5 Ni2 162.898(16) . .
Sn4 Ge1 Sn5 Ni2 -94.69(14) 2_556 .
Ni1 Ge1 Sn5 Sn6 -109.887(17) . .
Ni2 Ge1 Sn5 Sn6 70.113(17) . .
Sn6 Ge1 Sn5 Sn6 123.53(3) 2_556 .
Sn5 Ge1 Sn5 Sn6 70.113(17) 2_556 .
Sn3 Ge1 Sn5 Sn6 -47.52(2) 2_556 .
Sn3 Ge1 Sn5 Sn6 -171.12(3) . .
Sn4 Ge1 Sn5 Sn6 -126.99(2) . .
Sn4 Ge1 Sn5 Sn6 -24.58(13) 2_556 .
Ni1 Ge1 Sn5 Sn8 138.058(13) . 2_556
Ni2 Ge1 Sn5 Sn8 -41.942(13) . 2_556
Sn6 Ge1 Sn5 Sn8 11.48(2) 2_556 2_556
Sn6 Ge1 Sn5 Sn8 -112.05(2) . 2_556
Sn5 Ge1 Sn5 Sn8 -41.941(14) 2_556 2_556
Sn3 Ge1 Sn5 Sn8 -159.58(3) 2_556 2_556
Sn3 Ge1 Sn5 Sn8 76.83(3) . 2_556
Sn4 Ge1 Sn5 Sn8 120.96(2) . 2_556
Sn4 Ge1 Sn5 Sn8 -136.63(14) 2_556 2_556
Ni1 Ge1 Sn5 Sn7 -163.758(12) . .
Ni2 Ge1 Sn5 Sn7 16.242(12) . .
Sn6 Ge1 Sn5 Sn7 69.66(2) 2_556 .
Sn6 Ge1 Sn5 Sn7 -53.87(2) . .
Sn5 Ge1 Sn5 Sn7 16.242(12) 2_556 .
Sn3 Ge1 Sn5 Sn7 -101.39(3) 2_556 .
Sn3 Ge1 Sn5 Sn7 135.01(3) . .
Sn4 Ge1 Sn5 Sn7 179.14(2) . .
Sn4 Ge1 Sn5 Sn7 -78.45(14) 2_556 .
Ge1 Ni2 Sn6 Sn5 81.26(2) . .
Sn5 Ni2 Sn6 Sn5 153.21(6) 2_556 .
Sn7 Ni2 Sn6 Sn5 -125.78(5) 2_556 .
Sn7 Ni2 Sn6 Sn5 -77.91(2) . .
Sn6 Ni2 Sn6 Sn5 81.26(2) 2_556 .
Sn8 Ni2 Sn6 Sn5 -33.19(4) 2_556 .
Sn8 Ni2 Sn6 Sn5 -149.85(4) . .
Ge1 Ni2 Sn6 Sn8 -128.89(2) . .
Sn5 Ni2 Sn6 Sn8 -56.94(3) 2_556 .
Sn5 Ni2 Sn6 Sn8 149.85(4) . .
Sn7 Ni2 Sn6 Sn8 24.08(3) 2_556 .
Sn7 Ni2 Sn6 Sn8 71.94(3) . .
Sn6 Ni2 Sn6 Sn8 -128.89(2) 2_556 .
Sn8 Ni2 Sn6 Sn8 116.66(7) 2_556 .
Sn5 Ni2 Sn6 Ge1 71.95(4) 2_556 .
Sn5 Ni2 Sn6 Ge1 -81.26(2) . .
Sn7 Ni2 Sn6 Ge1 152.97(3) 2_556 .
Sn7 Ni2 Sn6 Ge1 -159.168(16) . .
Sn6 Ni2 Sn6 Ge1 0.001(1) 2_556 .
Sn8 Ni2 Sn6 Ge1 -114.45(5) 2_556 .
Sn8 Ni2 Sn6 Ge1 128.89(2) . .
Ge1 Ni2 Sn6 Sn7 159.168(16) . .
Sn5 Ni2 Sn6 Sn7 -128.88(4) 2_556 .
Sn5 Ni2 Sn6 Sn7 77.91(2) . .
Sn7 Ni2 Sn6 Sn7 -47.86(5) 2_556 .
Sn6 Ni2 Sn6 Sn7 159.170(16) 2_556 .
Sn8 Ni2 Sn6 Sn7 44.72(5) 2_556 .
Sn8 Ni2 Sn6 Sn7 -71.94(3) . .
Sn8 Sn5 Sn6 Ni2 24.58(4) 2_556 .
Ge1 Sn5 Sn6 Ni2 -53.80(4) . .
Sn7 Sn5 Sn6 Ni2 62.20(4) . .
Ni2 Sn5 Sn6 Sn8 -26.55(4) . .
Sn8 Sn5 Sn6 Sn8 -1.97(3) 2_556 .
Ge1 Sn5 Sn6 Sn8 -80.35(3) . .
Sn7 Sn5 Sn6 Sn8 35.65(2) . .
Ni2 Sn5 Sn6 Ge1 53.80(4) . .
Sn8 Sn5 Sn6 Ge1 78.38(3) 2_556 .
Sn7 Sn5 Sn6 Ge1 116.01(3) . .
Ni2 Sn5 Sn6 Sn7 -62.20(4) . .
Sn8 Sn5 Sn6 Sn7 -37.62(2) 2_556 .
Ge1 Sn5 Sn6 Sn7 -116.01(3) . .
Ni1 Ge1 Sn6 Ni2 180.0 . .
Sn6 Ge1 Sn6 Ni2 0.0 2_556 .
Sn5 Ge1 Sn6 Ni2 -52.822(18) 2_556 .
Sn5 Ge1 Sn6 Ni2 68.919(17) . .
Sn3 Ge1 Sn6 Ni2 -160.851(15) 2_556 .
Sn3 Ge1 Sn6 Ni2 98.10(12) . .
Sn4 Ge1 Sn6 Ni2 118.62(2) . .
Sn4 Ge1 Sn6 Ni2 -117.86(2) 2_556 .
Ni1 Ge1 Sn6 Sn5 111.081(17) . .
Ni2 Ge1 Sn6 Sn5 -68.919(17) . .
Sn6 Ge1 Sn6 Sn5 -68.919(17) 2_556 .
Sn5 Ge1 Sn6 Sn5 -121.74(3) 2_556 .
Sn3 Ge1 Sn6 Sn5 130.23(2) 2_556 .
Sn3 Ge1 Sn6 Sn5 29.18(12) . .
Sn4 Ge1 Sn6 Sn5 49.70(2) . .
Sn4 Ge1 Sn6 Sn5 173.22(3) 2_556 .
Ni1 Ge1 Sn6 Sn8 -138.739(13) . .
Ni2 Ge1 Sn6 Sn8 41.261(13) . .
Sn6 Ge1 Sn6 Sn8 41.260(13) 2_556 .
Sn5 Ge1 Sn6 Sn8 -11.56(2) 2_556 .
Sn5 Ge1 Sn6 Sn8 110.18(2) . .
Sn3 Ge1 Sn6 Sn8 -119.59(2) 2_556 .
Sn3 Ge1 Sn6 Sn8 139.36(12) . .
Sn4 Ge1 Sn6 Sn8 159.88(3) . .
Sn4 Ge1 Sn6 Sn8 -76.60(3) 2_556 .
Ni1 Ge1 Sn6 Sn7 163.516(11) . .
Ni2 Ge1 Sn6 Sn7 -16.484(11) . .
Sn6 Ge1 Sn6 Sn7 -16.485(11) 2_556 .
Sn5 Ge1 Sn6 Sn7 -69.31(2) 2_556 .
Sn5 Ge1 Sn6 Sn7 52.43(2) . .
Sn3 Ge1 Sn6 Sn7 -177.34(2) 2_556 .
Sn3 Ge1 Sn6 Sn7 81.62(12) . .
Sn4 Ge1 Sn6 Sn7 102.13(3) . .
Sn4 Ge1 Sn6 Sn7 -134.34(3) 2_556 .
Ge1 Ni2 Sn7 Sn8 -106.96(2) . .
Sn5 Ni2 Sn7 Sn8 26.20(3) 2_556 .
Sn5 Ni2 Sn7 Sn8 -142.15(3) . .
Sn7 Ni2 Sn7 Sn8 73.04(2) 2_556 .
Sn6 Ni2 Sn7 Sn8 121.94(4) 2_556 .
Sn6 Ni2 Sn7 Sn8 -70.834(19) . .
Sn8 Ni2 Sn7 Sn8 145.81(3) 2_556 .
Ge1 Ni2 Sn7 Sn8 107.22(2) . 2_556
Sn5 Ni2 Sn7 Sn8 -119.62(4) 2_556 2_556
Sn5 Ni2 Sn7 Sn8 72.04(2) . 2_556
Sn7 Ni2 Sn7 Sn8 -72.77(2) 2_556 2_556
Sn6 Ni2 Sn7 Sn8 -23.87(3) 2_556 2_556
Sn6 Ni2 Sn7 Sn8 143.35(3) . 2_556
Sn8 Ni2 Sn7 Sn8 -145.81(3) . 2_556
Ge1 Ni2 Sn7 Sn7 180.0 . 2_556
Sn5 Ni2 Sn7 Sn7 -46.84(4) 2_556 2_556
Sn5 Ni2 Sn7 Sn7 144.81(3) . 2_556
Sn6 Ni2 Sn7 Sn7 48.90(4) 2_556 2_556
Sn6 Ni2 Sn7 Sn7 -143.87(2) . 2_556
Sn8 Ni2 Sn7 Sn7 72.77(2) 2_556 2_556
Sn8 Ni2 Sn7 Sn7 -73.04(2) . 2_556
Ge1 Ni2 Sn7 Sn5 35.18(3) . .
Sn5 Ni2 Sn7 Sn5 168.34(4) 2_556 .
Sn7 Ni2 Sn7 Sn5 -144.81(3) 2_556 .
Sn6 Ni2 Sn7 Sn5 -95.91(3) 2_556 .
Sn6 Ni2 Sn7 Sn5 71.31(2) . .
Sn8 Ni2 Sn7 Sn5 -72.04(2) 2_556 .
Sn8 Ni2 Sn7 Sn5 142.15(3) . .
Ge1 Ni2 Sn7 Sn6 -36.13(2) . .
Sn5 Ni2 Sn7 Sn6 97.03(3) 2_556 .
Sn5 Ni2 Sn7 Sn6 -71.31(2) . .
Sn7 Ni2 Sn7 Sn6 143.87(2) 2_556 .
Sn6 Ni2 Sn7 Sn6 -167.22(4) 2_556 .
Sn8 Ni2 Sn7 Sn6 -143.35(3) 2_556 .
Sn8 Ni2 Sn7 Sn6 70.834(19) . .
Sn6 Sn5 Sn7 Ni2 -66.258(19) . .
Sn8 Sn5 Sn7 Ni2 71.08(2) 2_556 .
Ge1 Sn5 Sn7 Ni2 -14.381(16) . .
Ni2 Sn5 Sn7 Sn8 32.03(2) . .
Sn6 Sn5 Sn7 Sn8 -34.23(2) . .
Sn8 Sn5 Sn7 Sn8 103.12(2) 2_556 .
Ge1 Sn5 Sn7 Sn8 17.65(2) . .
Ni2 Sn5 Sn7 Sn8 -71.08(2) . 2_556
Sn6 Sn5 Sn7 Sn8 -137.34(2) . 2_556
Ge1 Sn5 Sn7 Sn8 -85.46(2) . 2_556
Ni2 Sn5 Sn7 Sn7 -28.36(2) . 2_556
Sn6 Sn5 Sn7 Sn7 -94.62(2) . 2_556
Sn8 Sn5 Sn7 Sn7 42.72(2) 2_556 2_556
Ge1 Sn5 Sn7 Sn7 -42.74(3) . 2_556
Ni2 Sn5 Sn7 Sn6 66.258(19) . .
Sn8 Sn5 Sn7 Sn6 137.34(2) 2_556 .
Ge1 Sn5 Sn7 Sn6 51.877(16) . .
Sn5 Sn6 Sn7 Ni2 67.06(2) . .
Sn8 Sn6 Sn7 Ni2 -72.00(2) . .
Ge1 Sn6 Sn7 Ni2 14.802(17) . .
Ni2 Sn6 Sn7 Sn8 72.00(2) . .
Sn5 Sn6 Sn7 Sn8 139.06(2) . .
Ge1 Sn6 Sn7 Sn8 86.81(2) . .
Ni2 Sn6 Sn7 Sn8 -31.02(2) . 2_556
Sn5 Sn6 Sn7 Sn8 36.04(2) . 2_556
Sn8 Sn6 Sn7 Sn8 -103.03(2) . 2_556
Ge1 Sn6 Sn7 Sn8 -16.22(2) . 2_556
Ni2 Sn6 Sn7 Sn7 29.01(2) . 2_556
Sn5 Sn6 Sn7 Sn7 96.07(2) . 2_556
Sn8 Sn6 Sn7 Sn7 -43.00(2) . 2_556
Ge1 Sn6 Sn7 Sn7 43.81(2) . 2_556
Ni2 Sn6 Sn7 Sn5 -67.06(2) . .
Sn8 Sn6 Sn7 Sn5 -139.06(2) . .
Ge1 Sn6 Sn7 Sn5 -52.259(17) . .
Ge1 Ni2 Sn8 Sn6 58.56(2) . .
Sn5 Ni2 Sn8 Sn6 118.97(4) 2_556 .
Sn5 Ni2 Sn8 Sn6 -35.35(4) . .
Sn7 Ni2 Sn8 Sn6 -160.60(3) 2_556 .
Sn7 Ni2 Sn8 Sn6 -82.22(2) . .
Sn6 Ni2 Sn8 Sn6 152.32(7) 2_556 .
Sn8 Ni2 Sn8 Sn6 -121.45(2) 2_556 .
Ge1 Ni2 Sn8 Sn5 -60.42(2) . 2_556
Sn5 Ni2 Sn8 Sn5 -154.32(7) . 2_556
Sn7 Ni2 Sn8 Sn5 80.43(2) 2_556 2_556
Sn7 Ni2 Sn8 Sn5 158.81(3) . 2_556
Sn6 Ni2 Sn8 Sn5 33.34(4) 2_556 2_556
Sn6 Ni2 Sn8 Sn5 -118.97(4) . 2_556
Sn8 Ni2 Sn8 Sn5 119.58(2) 2_556 2_556
Ge1 Ni2 Sn8 Sn7 140.776(18) . .
Sn5 Ni2 Sn8 Sn7 -158.81(3) 2_556 .
Sn5 Ni2 Sn8 Sn7 46.87(4) . .
Sn7 Ni2 Sn8 Sn7 -78.38(4) 2_556 .
Sn6 Ni2 Sn8 Sn7 -125.47(6) 2_556 .
Sn6 Ni2 Sn8 Sn7 82.22(2) . .
Sn8 Ni2 Sn8 Sn7 -39.225(18) 2_556 .
Ge1 Ni2 Sn8 Sn7 -140.843(18) . 2_556
Sn5 Ni2 Sn8 Sn7 -80.43(2) 2_556 2_556
Sn5 Ni2 Sn8 Sn7 125.25(6) . 2_556
Sn7 Ni2 Sn8 Sn7 78.38(4) . 2_556
Sn6 Ni2 Sn8 Sn7 -47.08(5) 2_556 2_556
Sn6 Ni2 Sn8 Sn7 160.60(3) . 2_556
Sn8 Ni2 Sn8 Sn7 39.156(18) 2_556 2_556
Sn5 Sn6 Sn8 Ni2 25.84(3) . .
Ge1 Sn6 Sn8 Ni2 -33.79(3) . .
Sn7 Sn6 Sn8 Ni2 62.97(3) . .
Ni2 Sn6 Sn8 Sn5 45.54(3) . 2_556
Sn5 Sn6 Sn8 Sn5 71.38(2) . 2_556
Ge1 Sn6 Sn8 Sn5 11.75(2) . 2_556
Sn7 Sn6 Sn8 Sn5 108.51(2) . 2_556
Ni2 Sn6 Sn8 Sn7 -62.97(3) . .
Sn5 Sn6 Sn8 Sn7 -37.13(2) . .
Ge1 Sn6 Sn8 Sn7 -96.76(2) . .
Ni2 Sn6 Sn8 Sn7 -16.48(3) . 2_556
Sn5 Sn6 Sn8 Sn7 9.36(3) . 2_556
Ge1 Sn6 Sn8 Sn7 -50.27(3) . 2_556
Sn7 Sn6 Sn8 Sn7 46.49(2) . 2_556
Sn8 Sn7 Sn8 Ni2 29.80(3) 2_556 .
Sn7 Sn7 Sn8 Ni2 64.65(3) 2_556 .
Sn5 Sn7 Sn8 Ni2 -30.22(2) . .
Sn6 Sn7 Sn8 Ni2 -63.78(2) . .
Ni2 Sn7 Sn8 Sn6 63.78(2) . .
Sn8 Sn7 Sn8 Sn6 93.58(2) 2_556 .
Sn7 Sn7 Sn8 Sn6 128.43(2) 2_556 .
Sn5 Sn7 Sn8 Sn6 33.56(2) . .
Ni2 Sn7 Sn8 Sn5 -17.92(3) . 2_556
Sn8 Sn7 Sn8 Sn5 11.88(3) 2_556 2_556
Sn7 Sn7 Sn8 Sn5 46.726(17) 2_556 2_556
Sn5 Sn7 Sn8 Sn5 -48.14(3) . 2_556
Sn6 Sn7 Sn8 Sn5 -81.70(2) . 2_556
Ni2 Sn7 Sn8 Sn7 -64.65(3) . 2_556
Sn8 Sn7 Sn8 Sn7 -34.85(3) 2_556 2_556
Sn5 Sn7 Sn8 Sn7 -94.87(2) . 2_556
Sn6 Sn7 Sn8 Sn7 -128.43(2) . 2_556
O1 K1 N1 C7 107.6(7) . .
O3 K1 N1 C7 -20.1(6) . .
O5 K1 N1 C7 -134.8(7) . .
O6 K1 N1 C7 -146.1(6) . .
O2 K1 N1 C7 96.0(7) . .
O4 K1 N1 C7 -31.0(7) . .
N2 K1 N1 C7 -20(12) . .
O1 K1 N1 C13 -132.5(8) . .
O3 K1 N1 C13 99.7(7) . .
O5 K1 N1 C13 -14.9(7) . .
O6 K1 N1 C13 -26.2(8) . .
O2 K1 N1 C13 -144.1(7) . .
O4 K1 N1 C13 88.9(7) . .
N2 K1 N1 C13 100(12) . .
O1 K1 N1 C1 -12.1(6) . .
O3 K1 N1 C1 -139.9(7) . .
O5 K1 N1 C1 105.5(6) . .
O6 K1 N1 C1 94.1(6) . .
O2 K1 N1 C1 -23.7(7) . .
O4 K1 N1 C1 -150.8(6) . .
N2 K1 N1 C1 -140(12) . .
O1 K1 N2 C6 -26.3(7) . .
O3 K1 N2 C6 100.9(7) . .
O5 K1 N2 C6 -145.1(6) . .
O6 K1 N2 C6 -132.5(7) . .
O2 K1 N2 C6 -15.8(6) . .
O4 K1 N2 C6 112.0(7) . .
N1 K1 N2 C6 101(12) . .
O1 K1 N2 C18 95.2(7) . .
O3 K1 N2 C18 -137.5(7) . .
O5 K1 N2 C18 -23.5(8) . .
O6 K1 N2 C18 -11.0(6) . .
O2 K1 N2 C18 105.7(7) . .
O4 K1 N2 C18 -126.5(7) . .
N1 K1 N2 C18 -138(12) . .
O1 K1 N2 C12 -145.6(7) . .
O3 K1 N2 C12 -18.4(8) . .
O5 K1 N2 C12 95.6(7) . .
O6 K1 N2 C12 108.1(7) . .
O2 K1 N2 C12 -135.2(8) . .
O4 K1 N2 C12 -7.4(7) . .
N1 K1 N2 C12 -19(12) . .
O3 K1 O1 C3 -114.8(8) . .
O5 K1 O1 C3 150.0(8) . .
O6 K1 O1 C3 89.2(8) . .
O2 K1 O1 C3 9.3(7) . .
O4 K1 O1 C3 -59.0(9) . .
N1 K1 O1 C3 -159.2(8) . .
N2 K1 O1 C3 19.7(8) . .
O3 K1 O1 C2 25.5(7) . .
O5 K1 O1 C2 -69.7(7) . .
O6 K1 O1 C2 -130.6(7) . .
O2 K1 O1 C2 149.6(7) . .
O4 K1 O1 C2 81.2(8) . .
N1 K1 O1 C2 -19.0(7) . .
N2 K1 O1 C2 159.9(7) . .
O1 K1 O2 C4 23.3(6) . .
O3 K1 O2 C4 107.8(7) . .
O5 K1 O2 C4 -42.6(7) . .
O6 K1 O2 C4 -95.3(6) . .
O4 K1 O2 C4 169.4(6) . .
N1 K1 O2 C4 34.9(7) . .
N2 K1 O2 C4 -146.3(7) . .
O1 K1 O2 C5 152.9(8) . .
O3 K1 O2 C5 -122.7(7) . .
O5 K1 O2 C5 86.9(8) . .
O6 K1 O2 C5 34.2(7) . .
O4 K1 O2 C5 -61.0(7) . .
N1 K1 O2 C5 164.5(7) . .
N2 K1 O2 C5 -16.8(7) . .
O1 K1 O3 C9 167.7(7) . .
O5 K1 O3 C9 -95.0(7) . .
O6 K1 O3 C9 -42.3(8) . .
O2 K1 O3 C9 104.9(7) . .
O4 K1 O3 C9 21.7(7) . .
N1 K1 O3 C9 -147.3(7) . .
N2 K1 O3 C9 32.7(7) . .
O1 K1 O3 C8 -54.6(7) . .
O5 K1 O3 C8 42.7(7) . .
O6 K1 O3 C8 95.4(7) . .
O2 K1 O3 C8 -117.3(7) . .
O4 K1 O3 C8 159.4(7) . .
N1 K1 O3 C8 -9.6(7) . .
N2 K1 O3 C8 170.4(7) . .
O1 K1 O4 C10 -57.0(8) . .
O3 K1 O4 C10 11.5(6) . .
O5 K1 O4 C10 90.9(7) . .
O6 K1 O4 C10 151.0(7) . .
O2 K1 O4 C10 -112.9(7) . .
N1 K1 O4 C10 22.4(7) . .
N2 K1 O4 C10 -157.3(7) . .
O1 K1 O4 C11 73.5(8) . .
O3 K1 O4 C11 142.0(7) . .
O5 K1 O4 C11 -138.7(7) . .
O6 K1 O4 C11 -78.5(7) . .
O2 K1 O4 C11 17.6(7) . .
N1 K1 O4 C11 152.9(7) . .
N2 K1 O4 C11 -26.9(7) . .
O1 K1 O5 C14 33.8(7) . .
O3 K1 O5 C14 -69.3(7) . .
O6 K1 O5 C14 151.6(8) . .
O2 K1 O5 C14 87.0(8) . .
O4 K1 O5 C14 -127.9(7) . .
N1 K1 O5 C14 -17.3(7) . .
N2 K1 O5 C14 164.0(7) . .
O1 K1 O5 C15 -100.6(6) . .
O3 K1 O5 C15 156.3(6) . .
O6 K1 O5 C15 17.2(6) . .
O2 K1 O5 C15 -47.4(7) . .
O4 K1 O5 C15 97.7(6) . .
N1 K1 O5 C15 -151.7(7) . .
N2 K1 O5 C15 29.6(7) . .
O1 K1 O6 C16 97.5(6) . .
O3 K1 O6 C16 -49.2(7) . .
O5 K1 O6 C16 15.7(6) . .
O2 K1 O6 C16 157.0(6) . .
O4 K1 O6 C16 -100.6(6) . .
N1 K1 O6 C16 26.9(7) . .
N2 K1 O6 C16 -152.0(7) . .
O1 K1 O6 C17 -132.2(6) . .
O3 K1 O6 C17 81.1(7) . .
O5 K1 O6 C17 146.0(7) . .
O2 K1 O6 C17 -72.7(7) . .
O4 K1 O6 C17 29.7(7) . .
N1 K1 O6 C17 157.2(6) . .
N2 K1 O6 C17 -21.7(6) . .
C7 N1 C1 C2 -75.5(12) . .
C13 N1 C1 C2 161.7(10) . .
K1 N1 C1 C2 42.2(11) . .
C3 O1 C2 C1 -169.1(9) . .
K1 O1 C2 C1 48.7(11) . .
N1 C1 C2 O1 -61.9(13) . .
C2 O1 C3 C4 176.7(9) . .
K1 O1 C3 C4 -40.4(12) . .
C5 O2 C4 C3 173.3(9) . .
K1 O2 C4 C3 -54.1(9) . .
O1 C3 C4 O2 64.1(12) . .
C4 O2 C5 C6 176.6(9) . .
K1 O2 C5 C6 47.6(11) . .
C18 N2 C6 C5 -71.5(11) . .
C12 N2 C6 C5 167.2(9) . .
K1 N2 C6 C5 48.1(10) . .
O2 C5 C6 N2 -66.3(12) . .
C13 N1 C7 C8 -68.6(11) . .
C1 N1 C7 C8 168.6(9) . .
K1 N1 C7 C8 50.3(10) . .
C9 O3 C8 C7 176.5(9) . .
K1 O3 C8 C7 37.6(11) . .
N1 C7 C8 O3 -60.3(12) . .
C8 O3 C9 C10 164.5(9) . .
K1 O3 C9 C10 -52.9(10) . .
C11 O4 C10 C9 -175.0(9) . .
K1 O4 C10 C9 -42.4(9) . .
O3 C9 C10 O4 64.2(11) . .
C10 O4 C11 C12 -169.2(9) . .
K1 O4 C11 C12 58.6(11) . .
C6 N2 C12 C11 -78.6(12) . .
C18 N2 C12 C11 158.7(11) . .
K1 N2 C12 C11 39.9(12) . .
O4 C11 C12 N2 -67.3(14) . .
C7 N1 C13 C14 163.2(9) . .
C1 N1 C13 C14 -73.9(11) . .
K1 N1 C13 C14 45.2(11) . .
C15 O5 C14 C13 -177.6(9) . .
K1 O5 C14 C13 47.6(11) . .
N1 C13 C14 O5 -63.4(13) . .
C14 O5 C15 C16 174.7(8) . .
K1 O5 C15 C16 -47.8(9) . .
C17 O6 C16 C15 179.9(8) . .
K1 O6 C16 C15 -46.9(9) . .
O5 C15 C16 O6 65.3(10) . .
C16 O6 C17 C18 -176.1(8) . .
K1 O6 C17 C18 52.7(10) . .
C6 N2 C18 C17 162.1(9) . .
C12 N2 C18 C17 -76.5(11) . .
K1 N2 C18 C17 42.6(10) . .
O6 C17 C18 N2 -65.6(12) . .
O8 K2 N3 C25 148.3(5) . .
O7 K2 N3 C25 136.4(6) . .
O12 K2 N3 C25 -92.1(6) . .
O9 K2 N3 C25 16.3(5) . .
O11 K2 N3 C25 -104.5(6) . .
O10 K2 N3 C25 27.3(6) . .
N4 K2 N3 C25 -11(10) . .
O8 K2 N3 C19 27.2(7) . .
O7 K2 N3 C19 15.3(6) . .
O12 K2 N3 C19 146.8(6) . .
O9 K2 N3 C19 -104.8(6) . .
O11 K2 N3 C19 134.4(7) . .
O10 K2 N3 C19 -93.8(6) . .
N4 K2 N3 C19 -132(10) . .
O8 K2 N3 C31 -92.7(6) . .
O7 K2 N3 C31 -104.6(6) . .
O12 K2 N3 C31 26.9(6) . .
O9 K2 N3 C31 135.3(6) . .
O11 K2 N3 C31 14.5(5) . .
O10 K2 N3 C31 146.3(6) . .
N4 K2 N3 C31 108(10) . .
O8 K2 N4 C24 10.7(5) . .
O7 K2 N4 C24 23.1(6) . .
O12 K2 N4 C24 -108.0(6) . .
O9 K2 N4 C24 143.2(5) . .
O11 K2 N4 C24 -97.1(5) . .
O10 K2 N4 C24 131.5(6) . .
N3 K2 N4 C24 171(10) . .
O8 K2 N4 C30 -109.2(5) . .
O7 K2 N4 C30 -96.7(5) . .
O12 K2 N4 C30 132.1(6) . .
O9 K2 N4 C30 23.4(6) . .
O11 K2 N4 C30 143.1(5) . .
O10 K2 N4 C30 11.6(5) . .
N3 K2 N4 C30 51(10) . .
O8 K2 N4 C36 130.4(6) . .
O7 K2 N4 C36 142.9(5) . .
O12 K2 N4 C36 11.7(5) . .
O9 K2 N4 C36 -97.0(6) . .
O11 K2 N4 C36 22.7(6) . .
O10 K2 N4 C36 -108.8(6) . .
N3 K2 N4 C36 -70(10) . .
O8 K2 O7 C20 -151.8(7) . .
O12 K2 O7 C20 -84.9(7) . .
O9 K2 O7 C20 66.1(7) . .
O11 K2 O7 C20 -33.1(7) . .
O10 K2 O7 C20 125.7(7) . .
N3 K2 O7 C20 16.6(6) . .
N4 K2 O7 C20 -164.2(6) . .
O8 K2 O7 C21 -21.0(5) . .
O12 K2 O7 C21 45.9(6) . .
O9 K2 O7 C21 -163.1(5) . .
O11 K2 O7 C21 97.7(5) . .
O10 K2 O7 C21 -103.5(5) . .
N3 K2 O7 C21 147.4(6) . .
N4 K2 O7 C21 -33.4(6) . .
O7 K2 O8 C23 -146.7(6) . .
O12 K2 O8 C23 71.7(5) . .
O9 K2 O8 C23 -79.5(6) . .
O11 K2 O8 C23 131.4(5) . .
O10 K2 O8 C23 -27.4(5) . .
N3 K2 O8 C23 -158.4(5) . .
N4 K2 O8 C23 21.1(5) . .
O7 K2 O8 C22 -12.5(5) . .
O12 K2 O8 C22 -154.1(5) . .
O9 K2 O8 C22 54.7(6) . .
O11 K2 O8 C22 -94.4(5) . .
O10 K2 O8 C22 106.8(5) . .
N3 K2 O8 C22 -24.3(6) . .
N4 K2 O8 C22 155.2(6) . .
O8 K2 O9 C26 -88.4(6) . .
O7 K2 O9 C26 -33.7(6) . .
O12 K2 O9 C26 124.5(6) . .
O11 K2 O9 C26 64.5(6) . .
O10 K2 O9 C26 -153.2(6) . .
N3 K2 O9 C26 15.7(6) . .
N4 K2 O9 C26 -165.0(6) . .
O8 K2 O9 C27 45.4(6) . .
O7 K2 O9 C27 100.1(5) . .
O12 K2 O9 C27 -101.6(5) . .
O11 K2 O9 C27 -161.7(5) . .
O10 K2 O9 C27 -19.4(5) . .
N3 K2 O9 C27 149.5(6) . .
N4 K2 O9 C27 -31.1(6) . .
O8 K2 O10 C29 69.9(5) . .
O7 K2 O10 C29 131.2(5) . .
O12 K2 O10 C29 -28.6(6) . .
O9 K2 O10 C29 -147.1(6) . .
O11 K2 O10 C29 -81.5(6) . .
N3 K2 O10 C29 -158.2(5) . .
N4 K2 O10 C29 20.9(5) . .
O8 K2 O10 C28 -158.6(5) . .
O7 K2 O10 C28 -97.3(5) . .
O12 K2 O10 C28 102.8(5) . .
O9 K2 O10 C28 -15.6(5) . .
O11 K2 O10 C28 50.0(6) . .
N3 K2 O10 C28 -26.7(6) . .
N4 K2 O10 C28 152.4(6) . .
O8 K2 O11 C33 -98.1(6) . .
O7 K2 O11 C33 -159.1(5) . .
O12 K2 O11 C33 -16.5(5) . .
O9 K2 O11 C33 101.8(6) . .
O10 K2 O11 C33 49.3(6) . .
N3 K2 O11 C33 151.0(6) . .
N4 K2 O11 C33 -27.6(6) . .
O8 K2 O11 C32 128.4(6) . .
O7 K2 O11 C32 67.5(6) . .
O12 K2 O11 C32 -150.0(6) . .
O9 K2 O11 C32 -31.6(6) . .
O10 K2 O11 C32 -84.2(6) . .
N3 K2 O11 C32 17.5(5) . .
N4 K2 O11 C32 -161.1(5) . .
O8 K2 O12 C34 100.4(6) . .
O7 K2 O12 C34 46.1(7) . .
O9 K2 O12 C34 -100.8(6) . .
O11 K2 O12 C34 -18.2(6) . .
O10 K2 O12 C34 -160.5(6) . .
N3 K2 O12 C34 -30.6(6) . .
N4 K2 O12 C34 150.8(6) . .
O8 K2 O12 C35 -30.0(6) . .
O7 K2 O12 C35 -84.3(7) . .
O9 K2 O12 C35 128.8(6) . .
O11 K2 O12 C35 -148.7(6) . .
O10 K2 O12 C35 69.0(6) . .
N3 K2 O12 C35 -161.0(6) . .
N4 K2 O12 C35 20.3(6) . .
C25 N3 C19 C20 -164.9(8) . .
C31 N3 C19 C20 74.2(10) . .
K2 N3 C19 C20 -46.0(10) . .
C21 O7 C20 C19 -178.1(8) . .
K2 O7 C20 C19 -46.6(10) . .
N3 C19 C20 O7 63.6(12) . .
C20 O7 C21 C22 -172.7(8) . .
K2 O7 C21 C22 52.6(8) . .
C23 O8 C22 C21 -179.6(7) . .
K2 O8 C22 C21 43.6(8) . .
O7 C21 C22 O8 -65.2(9) . .
C22 O8 C23 C24 173.3(7) . .
K2 O8 C23 C24 -50.9(8) . .
C30 N4 C24 C23 78.7(9) . .
C36 N4 C24 C23 -159.8(8) . .
K2 N4 C24 C23 -41.8(9) . .
O8 C23 C24 N4 63.6(10) . .
C19 N3 C25 C26 71.7(10) . .
C31 N3 C25 C26 -167.1(8) . .
K2 N3 C25 C26 -47.7(9) . .
C27 O9 C26 C25 179.9(7) . .
K2 O9 C26 C25 -45.2(9) . .
N3 C25 C26 O9 64.4(10) . .
C26 O9 C27 C28 -170.5(7) . .
K2 O9 C27 C28 52.4(7) . .
C29 O10 C28 C27 -177.4(7) . .
K2 O10 C28 C27 48.2(8) . .
O9 C27 C28 O10 -68.2(9) . .
C28 O10 C29 C30 176.9(7) . .
K2 O10 C29 C30 -50.6(9) . .
C24 N4 C30 C29 -162.2(7) . .
C36 N4 C30 C29 76.1(9) . .
K2 N4 C30 C29 -42.8(8) . .
O10 C29 C30 N4 63.8(10) . .
C25 N3 C31 C32 72.5(10) . .
C19 N3 C31 C32 -165.2(8) . .
K2 N3 C31 C32 -45.8(9) . .
C33 O11 C32 C31 178.5(8) . .
K2 O11 C32 C31 -47.4(9) . .
N3 C31 C32 O11 63.9(11) . .
C32 O11 C33 C34 -175.5(7) . .
K2 O11 C33 C34 48.4(8) . .
C35 O12 C34 C33 -176.0(7) . .
K2 O12 C34 C33 50.9(8) . .
O11 C33 C34 O12 -67.2(9) . .
C34 O12 C35 C36 176.9(7) . .
K2 O12 C35 C36 -51.1(9) . .
C24 N4 C36 C35 75.1(10) . .
C30 N4 C36 C35 -163.9(8) . .
K2 N4 C36 C35 -43.5(9) . .
O12 C35 C36 N4 65.9(10) . .
