#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:25:09 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179376 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/73/4327370.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4327370
loop_
_publ_author_name
'Chong Lei'
'Jiang-Gao Mao'
'Yan-Qiong Sun'
'Jun-Ling Song'
_publ_section_title
;
 A Novel Organic-Inorganic Hybrid Based on an 8-Electron-Reduced Keggin
 Polymolybdate Capped by Tetrahedral, Trigonal Bipyramidal, and Octahedral
 Zinc: Synthesis and Crystal Structure of
 (CH3NH3)(H2bipy)[Zn4(bipy)3(H2O)2MoV8MoVI4O36(PO4)].4H2O
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1964
_journal_page_last               1968
_journal_paper_doi               10.1021/ic035290+
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'C41 H52 Mo12 N9 O46 P Zn4'
_chemical_formula_weight         2850.65
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.4100(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.3032(2)
_cell_length_b                   17.8113(3)
_cell_length_c                   23.4597(4)
_cell_measurement_temperature    293(2)
_cell_volume                     6935.58(19)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Siemens Smart CCD '
_diffrn_measurement_method       'narrow frame method '
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0431
_diffrn_reflns_av_sigmaI/netI    0.0483
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            22229
_diffrn_reflns_theta_full        25.05
_diffrn_reflns_theta_max         25.05
_diffrn_reflns_theta_min         1.46
_diffrn_standards_decay_%        <1.0%
_exptl_absorpt_coefficient_mu    3.577
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.534
_exptl_absorpt_correction_type   SADABS
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.730
_exptl_crystal_description       Prism
_exptl_crystal_F_000             5472
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.000
_refine_diff_density_min         -1.038
_refine_diff_density_rms         0.228
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.242
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1012
_refine_ls_number_reflns         12126
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.242
_refine_ls_R_factor_all          0.0821
_refine_ls_R_factor_gt           0.0586
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0000P)²+126.7583P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1113
_refine_ls_wR_factor_ref         0.1245
_reflns_number_gt                9682
_reflns_number_total             12126
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0352902Bsi20040109_033947.cif
_cod_data_source_block           lcznmo
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' tag value 'Monoclinc' was replaced with
'monoclinic' value as specified in the replacement file
'/home/robertas/cod-tools/perl-scripts/inputs/replacement_values.lst'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        6935.58(18)
_cod_database_code               4327370
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn1 Zn -0.27119(7) 0.93440(7) -0.03043(5) 0.0208(3) Uani 1 1 d . A .
Zn2 Zn -0.26405(7) 0.56729(7) -0.03030(5) 0.0196(3) Uani 1 1 d . . .
Zn3 Zn -0.01179(7) 0.73294(7) 0.14530(6) 0.0250(3) Uani 1 1 d . . .
Zn4 Zn -0.36389(7) 0.76355(7) 0.16844(6) 0.0272(3) Uani 1 1 d . A .
Mo1 Mo -0.09804(5) 0.91848(5) 0.09802(4) 0.0198(2) Uani 1 1 d . A .
Mo2 Mo -0.06340(5) 0.84257(5) 0.01306(4) 0.0189(2) Uani 1 1 d . A .
Mo3 Mo -0.31083(5) 0.58038(5) 0.10962(4) 0.0194(2) Uani 1 1 d . A .
Mo4 Mo -0.42029(5) 0.65589(5) 0.03056(4) 0.0192(2) Uani 1 1 d . A .
Mo5 Mo -0.21271(5) 0.74875(5) -0.08992(4) 0.01836(19) Uani 1 1 d . A .
Mo6 Mo -0.35936(5) 0.75448(5) -0.08297(4) 0.01909(19) Uani 1 1 d . A .
Mo7 Mo -0.15075(6) 0.81996(5) 0.21499(4) 0.0220(2) Uani 1 1 d . A .
Mo8 Mo -0.15784(6) 0.67285(5) 0.21442(4) 0.0213(2) Uani 1 1 d . A .
Mo9 Mo -0.11427(5) 0.56220(5) 0.10760(4) 0.0197(2) Uani 1 1 d . A .
Mo10 Mo -0.06299(5) 0.64989(5) 0.00631(4) 0.0199(2) Uani 1 1 d . A .
Mo11 Mo -0.28651(5) 0.93430(5) 0.11740(4) 0.0213(2) Uani 1 1 d . A .
Mo12 Mo -0.42421(5) 0.84793(5) 0.02350(4) 0.0211(2) Uani 1 1 d . A .
P1 P -0.22036(14) 0.74932(15) 0.06362(11) 0.0154(5) Uani 1 1 d . A .
N1 N -0.2547(5) 1.0514(5) -0.0173(4) 0.025(2) Uani 1 1 d . . .
N2 N -0.2513(6) 1.4489(5) -0.0166(4) 0.025(2) Uani 1 1 d . . .
N3 N -0.3625(5) 0.9627(5) -0.1111(4) 0.027(2) Uani 1 1 d . . .
N4 N -0.6545(6) 1.0337(5) -0.3864(4) 0.032(2) Uani 1 1 d . . .
N5 N -0.4840(6) 0.7598(6) 0.1704(5) 0.035(2) Uani 1 1 d . . .
N6 N -0.8905(5) 0.7388(6) 0.1723(4) 0.030(2) Uani 1 1 d . . .
N7 N 0.0077(6) 0.7218(6) 0.3800(5) 0.038(3) Uani 1 1 d . . .
H07A H -0.0377 0.7147 0.3874 0.045 Uiso 1 1 calc R . .
N8 N 0.4052(6) 0.7736(6) 0.3777(5) 0.046(3) Uani 1 1 d . . .
H08A H 0.4565 0.7806 0.3866 0.055 Uiso 1 1 calc R . .
C1 C -0.1888(7) 1.0887(6) -0.0191(6) 0.034(3) Uani 1 1 d . . .
H1A H -0.1437 1.0614 -0.0209 0.040 Uiso 1 1 calc R . .
C2 C -0.1847(7) 1.1666(6) -0.0186(6) 0.032(3) Uani 1 1 d . . .
H2A H -0.1374 1.1904 -0.0200 0.039 Uiso 1 1 calc R . .
C3 C -0.2512(7) 1.2092(6) -0.0158(5) 0.027(3) Uani 1 1 d . . .
C4 C -0.3180(7) 1.1693(7) -0.0145(7) 0.041(3) Uani 1 1 d . . .
H4A H -0.3645 1.1947 -0.0134 0.050 Uiso 1 1 calc R . .
C5 C -0.3175(7) 1.0918(6) -0.0149(7) 0.040(3) Uani 1 1 d . . .
H5A H -0.3641 1.0667 -0.0135 0.049 Uiso 1 1 calc R . .
C6 C -0.2505(6) 1.2919(6) -0.0170(5) 0.023(2) Uani 1 1 d . . .
C7 C -0.1867(7) 1.3321(7) -0.0260(6) 0.037(3) Uani 1 1 d . . .
H7A H -0.1428 1.3076 -0.0331 0.044 Uiso 1 1 calc R . .
C8 C -0.1897(7) 1.4104(6) -0.0244(6) 0.034(3) Uani 1 1 d . . .
H8A H -0.1457 1.4371 -0.0290 0.041 Uiso 1 1 calc R . .
C9 C -0.3118(8) 1.4111(6) -0.0053(6) 0.039(3) Uani 1 1 d . . .
H9A H -0.3538 1.4374 0.0030 0.047 Uiso 1 1 calc R . .
C10 C -0.3136(7) 1.3334(7) -0.0058(6) 0.036(3) Uani 1 1 d . . .
H10A H -0.3572 1.3085 0.0013 0.044 Uiso 1 1 calc R . .
C11 C -0.3427(8) 0.9638(10) -0.1620(6) 0.052(4) Uani 1 1 d . . .
H11A H -0.2891 0.9560 -0.1608 0.063 Uiso 1 1 calc R . .
C12 C -0.3979(8) 0.9758(10) -0.2164(6) 0.054(4) Uani 1 1 d . . .
H12A H -0.3808 0.9775 -0.2506 0.065 Uiso 1 1 calc R . .
C13 C -0.4796(8) 0.9856(7) -0.2206(5) 0.036(3) Uani 1 1 d . . .
C14 C -0.4976(8) 0.9851(7) -0.1667(5) 0.038(3) Uani 1 1 d . . .
H14A H -0.5507 0.9918 -0.1663 0.046 Uiso 1 1 calc R . .
C15 C -0.4398(7) 0.9751(6) -0.1146(5) 0.030(3) Uani 1 1 d . . .
H15A H -0.4548 0.9770 -0.0795 0.036 Uiso 1 1 calc R . .
C16 C -0.5401(7) 1.0009(7) -0.2777(5) 0.032(3) Uani 1 1 d . . .
C17 C -0.5192(7) 1.0104(8) -0.3300(6) 0.038(3) Uani 1 1 d . . .
H17A H -0.4657 1.0059 -0.3301 0.045 Uiso 1 1 calc R . .
C18 C -0.5776(7) 1.0265(7) -0.3816(5) 0.037(3) Uani 1 1 d . . .
H18A H -0.5613 1.0329 -0.4158 0.045 Uiso 1 1 calc R . .
C19 C -0.6766(8) 1.0212(9) -0.3363(6) 0.044(3) Uani 1 1 d . . .
H19A H -0.7309 1.0240 -0.3381 0.053 Uiso 1 1 calc R . .
C20 C -0.6211(8) 1.0044(9) -0.2822(6) 0.045(4) Uani 1 1 d . . .
H20A H -0.6388 0.9954 -0.2489 0.054 Uiso 1 1 calc R . .
C21A C -0.5179(14) 0.8143(13) 0.1973(11) 0.029(5) Uiso 0.50 1 d P A 1
C22A C -0.5940(14) 0.8124(13) 0.2023(11) 0.030(5) Uiso 0.50 1 d P A 1
C21B C -0.5284(16) 0.8187(16) 0.1624(13) 0.041(6) Uiso 0.50 1 d P A 2
C22B C -0.6083(16) 0.8182(15) 0.1643(13) 0.040(6) Uiso 0.50 1 d P A 2
C23 C -0.6413(7) 0.7519(7) 0.1813(5) 0.033(3) Uani 1 1 d . . .
C24 C -0.6057(10) 0.6910(9) 0.1635(10) 0.077(6) Uani 1 1 d . A .
H24A H -0.6337 0.6461 0.1541 0.093 Uiso 1 1 calc R . .
C25 C -0.5255(10) 0.6972(9) 0.1596(10) 0.081(7) Uani 1 1 d . A .
H25A H -0.5014 0.6549 0.1488 0.098 Uiso 1 1 calc R . .
C26 C -0.7262(7) 0.7467(7) 0.1818(5) 0.033(3) Uani 1 1 d . A .
C27 C -0.7653(8) 0.6796(8) 0.1838(8) 0.062(5) Uani 1 1 d . . .
H27A H -0.7364 0.6349 0.1885 0.074 Uiso 1 1 calc R A .
C28 C -0.8457(8) 0.6779(8) 0.1789(8) 0.060(5) Uani 1 1 d . A .
H28A H -0.8700 0.6316 0.1802 0.072 Uiso 1 1 calc R . .
C29 C -0.8533(8) 0.8028(8) 0.1732(8) 0.055(4) Uani 1 1 d . A .
H29A H -0.8841 0.8462 0.1697 0.066 Uiso 1 1 calc R . .
C30 C -0.7721(8) 0.8115(8) 0.1788(8) 0.061(5) Uani 1 1 d . . .
H30A H -0.7490 0.8589 0.1806 0.074 Uiso 1 1 calc R A .
C31 C 0.0376(8) 0.7915(9) 0.3829(6) 0.045(3) Uani 1 1 d . . .
H31A H 0.0087 0.8321 0.3913 0.053 Uiso 1 1 calc R . .
C32 C 0.1111(8) 0.8022(7) 0.3734(6) 0.039(3) Uani 1 1 d . . .
H32A H 0.1324 0.8504 0.3753 0.047 Uiso 1 1 calc R . .
C33 C 0.1549(6) 0.7417(7) 0.3608(5) 0.027(2) Uani 1 1 d . . .
C34 C 0.1180(8) 0.6730(7) 0.3549(7) 0.046(4) Uani 1 1 d . . .
H34A H 0.1427 0.6318 0.3430 0.055 Uiso 1 1 calc R . .
C35 C 0.0456(7) 0.6646(7) 0.3662(7) 0.042(3) Uani 1 1 d . . .
H35A H 0.0228 0.6171 0.3641 0.051 Uiso 1 1 calc R . .
C36 C 0.2398(7) 0.7528(7) 0.3593(5) 0.034(3) Uani 1 1 d . . .
C37 C 0.2939(8) 0.6932(8) 0.3692(7) 0.053(4) Uani 1 1 d . . .
H37A H 0.2754 0.6443 0.3696 0.063 Uiso 1 1 calc R . .
C38 C 0.3752(8) 0.7069(8) 0.3784(7) 0.048(4) Uani 1 1 d . . .
H38A H 0.4102 0.6661 0.3856 0.058 Uiso 1 1 calc R . .
C39 C 0.3542(9) 0.8306(8) 0.3628(8) 0.064(5) Uani 1 1 d . . .
H39A H 0.3748 0.8777 0.3581 0.076 Uiso 1 1 calc R . .
C40 C 0.2731(8) 0.8241(8) 0.3539(8) 0.056(4) Uani 1 1 d . . .
H40A H 0.2400 0.8661 0.3444 0.067 Uiso 1 1 calc R . .
O1 O -0.0321(4) 0.9892(4) 0.1050(4) 0.0298(18) Uani 1 1 d . . .
O2 O 0.0088(4) 0.8977(4) 0.0023(4) 0.0279(18) Uani 1 1 d . . .
O3 O -0.3683(5) 0.5093(4) 0.1200(4) 0.0290(18) Uani 1 1 d . . .
O4 O -0.5005(5) 0.6010(5) 0.0245(4) 0.0329(19) Uani 1 1 d . . .
O5 O -0.2348(4) 0.7468(5) -0.1646(3) 0.0278(17) Uani 1 1 d . . .
O6 O -0.4073(4) 0.7557(5) -0.1558(3) 0.0305(18) Uani 1 1 d . . .
O7 O -0.1177(5) 0.8369(4) 0.2881(3) 0.034(2) Uani 1 1 d . . .
O8 O -0.1264(5) 0.6552(5) 0.2873(3) 0.0334(19) Uani 1 1 d . . .
O9 O -0.0551(5) 0.4852(4) 0.1128(4) 0.0311(19) Uani 1 1 d . . .
O10 O 0.0047(5) 0.5882(4) -0.0050(3) 0.0304(18) Uani 1 1 d . . .
O11 O -0.3384(5) 1.0106(4) 0.1291(4) 0.0321(19) Uani 1 1 d . . .
O12 O -0.5001(4) 0.9091(4) 0.0174(4) 0.0322(19) Uani 1 1 d . . .
O13 O -0.2470(4) 0.5999(4) 0.1913(3) 0.0261(17) Uani 1 1 d . . .
O14 O -0.3665(4) 0.8508(4) 0.1103(3) 0.0247(17) Uani 1 1 d . . .
O15 O -0.2374(4) 0.8995(4) 0.1928(3) 0.0234(16) Uani 1 1 d . . .
O16 O -0.0096(4) 0.7398(4) 0.0152(3) 0.0209(15) Uani 1 1 d . . .
O17 O -0.1181(4) 0.8171(4) -0.0703(3) 0.0205(15) Uani 1 1 d . . .
O18 O -0.2824(4) 0.6720(4) -0.0702(3) 0.0202(15) Uani 1 1 d . . .
O19 O -0.3718(4) 0.6710(4) 0.1159(3) 0.0229(16) Uani 1 1 d . . .
O20 O -0.2757(4) 0.8321(4) -0.0723(3) 0.0180(15) Uani 1 1 d . . .
O21 O -0.3310(4) 0.9175(4) 0.0304(3) 0.0266(17) Uani 1 1 d . . .
O22 O -0.2413(4) 0.7502(4) 0.2027(3) 0.0241(16) Uani 1 1 d . . .
O23 O -0.0339(4) 0.8281(4) 0.0997(3) 0.0222(16) Uani 1 1 d . . .
O24 O -0.1490(4) 0.5834(4) 0.0205(3) 0.0186(15) Uani 1 1 d . . .
O25 O -0.0407(4) 0.6454(4) 0.0947(3) 0.0226(16) Uani 1 1 d . . .
O26 O -0.0774(4) 0.7433(4) 0.1998(3) 0.0238(16) Uani 1 1 d . . .
O27 O -0.1527(4) 0.9105(4) 0.0130(3) 0.0202(15) Uani 1 1 d . . .
O28 O -0.3340(4) 0.5886(4) 0.0223(3) 0.0185(15) Uani 1 1 d . . .
O29 O -0.4691(4) 0.7580(4) 0.0346(3) 0.0228(16) Uani 1 1 d . . .
O30 O -0.0801(4) 0.8980(4) 0.1873(3) 0.0241(17) Uani 1 1 d . . .
O31 O -0.1277(4) 0.6663(4) -0.0690(3) 0.0226(16) Uani 1 1 d . . .
O32 O -0.1967(4) 0.9741(4) 0.1038(3) 0.0235(16) Uani 1 1 d . . .
O33 O -0.2128(4) 0.5228(4) 0.1026(3) 0.0223(16) Uani 1 1 d . . .
O34 O -0.0917(4) 0.5949(4) 0.1843(3) 0.0230(16) Uani 1 1 d . . .
O35 O -0.4366(4) 0.6797(4) -0.0583(3) 0.0234(16) Uani 1 1 d . . .
O36 O -0.4241(4) 0.8321(4) -0.0532(3) 0.0221(16) Uani 1 1 d . . .
O37 O -0.2063(4) 0.6782(4) 0.1032(3) 0.0214(16) Uani 1 1 d . . .
O38 O -0.1974(4) 0.8204(4) 0.1044(3) 0.0192(15) Uani 1 1 d . . .
O39 O -0.3106(4) 0.7510(4) 0.0267(3) 0.0184(14) Uani 1 1 d . . .
O40 O -0.1662(4) 0.7487(4) 0.0211(3) 0.0199(15) Uani 1 1 d . . .
O1W O -0.3546(10) 0.6685(9) 0.2392(7) 0.105(5) Uani 1 1 d . . .
O2W O -0.3470(6) 0.8359(7) 0.2456(4) 0.061(3) Uani 1 1 d . . .
O3W O -0.1216(6) -0.0176(6) 0.3702(6) 0.072(3) Uani 1 1 d . . .
O4W O 0.1955(6) -0.0223(5) 0.2330(5) 0.057(3) Uani 1 1 d . . .
O5W O 0.1391(6) 0.4675(5) 0.6148(4) 0.047(2) Uani 1 1 d . . .
O6W O -0.0641(8) 0.4230(10) 0.2392(6) 0.109(5) Uani 1 1 d . . .
N9 N -0.0810(17) 0.0332(13) 0.2528(10) 0.149(10) Uani 1 1 d D . .
C41 C -0.168(3) 0.031(3) 0.256(2) 0.25(2) Uiso 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O21 Zn1 O27 104.9(3) . .
O21 Zn1 O20 104.4(3) . .
O27 Zn1 O20 87.2(3) . .
O21 Zn1 N1 96.9(3) . .
O27 Zn1 N1 93.3(3) . .
O20 Zn1 N1 157.8(3) . .
O21 Zn1 N3 105.2(3) . .
O27 Zn1 N3 149.7(3) . .
O20 Zn1 N3 82.4(3) . .
N1 Zn1 N3 86.1(4) . .
O21 Zn1 Zn2 82.2(2) . .
O27 Zn1 Zn2 77.1(2) . .
O20 Zn1 Zn2 27.71(19) . .
N1 Zn1 Zn2 169.7(3) . .
N3 Zn1 Zn2 104.1(2) . .
O28 Zn2 O24 106.0(3) . .
O28 Zn2 O18 93.8(3) . .
O24 Zn2 O18 97.9(3) . .
O28 Zn2 N2 98.6(3) . 1_545
O24 Zn2 N2 90.5(3) . 1_545
O18 Zn2 N2 162.5(3) . 1_545
O28 Zn2 N4 105.0(3) . 2_444
O24 Zn2 N4 148.9(3) . 2_444
O18 Zn2 N4 82.1(3) . 2_444
N2 Zn2 N4 82.9(4) 1_545 2_444
O28 Zn2 Zn1 78.18(19) . .
O24 Zn2 Zn1 82.76(19) . .
O18 Zn2 Zn1 25.70(19) . .
N2 Zn2 Zn1 171.3(2) 1_545 .
N4 Zn2 Zn1 105.7(3) 2_444 .
O25 Zn3 O26 112.4(3) . .
O25 Zn3 O23 112.4(3) . .
O26 Zn3 O23 102.3(3) . .
O25 Zn3 N6 107.5(3) . 1_655
O26 Zn3 N6 122.5(3) . 1_655
O23 Zn3 N6 98.7(4) . 1_655
O19 Zn4 O22 91.6(3) . .
O19 Zn4 O14 102.9(3) . .
O22 Zn4 O14 100.0(3) . .
O19 Zn4 N5 95.2(4) . .
O22 Zn4 N5 155.2(4) . .
O14 Zn4 N5 101.7(3) . .
O19 Zn4 O2W 162.3(4) . .
O22 Zn4 O2W 82.1(3) . .
O14 Zn4 O2W 94.4(4) . .
N5 Zn4 O2W 84.3(4) . .
O19 Zn4 O1W 79.9(4) . .
O22 Zn4 O1W 77.5(4) . .
O14 Zn4 O1W 176.3(4) . .
N5 Zn4 O1W 80.3(5) . .
O2W Zn4 O1W 82.6(5) . .
O1 Mo1 O23 104.5(3) . .
O1 Mo1 O27 106.0(3) . .
O23 Mo1 O27 94.0(3) . .
O1 Mo1 O32 101.0(3) . .
O23 Mo1 O32 153.4(3) . .
O27 Mo1 O32 85.9(3) . .
O1 Mo1 O30 97.5(3) . .
O23 Mo1 O30 84.9(3) . .
O27 Mo1 O30 156.0(3) . .
O32 Mo1 O30 84.6(3) . .
O1 Mo1 O38 170.3(3) . .
O23 Mo1 O38 79.5(3) . .
O27 Mo1 O38 82.3(3) . .
O32 Mo1 O38 74.1(3) . .
O30 Mo1 O38 73.9(2) . .
O1 Mo1 Mo2 99.6(3) . .
O23 Mo1 Mo2 48.5(2) . .
O27 Mo1 Mo2 48.3(2) . .
O32 Mo1 Mo2 133.4(2) . .
O30 Mo1 Mo2 133.0(2) . .
O38 Mo1 Mo2 89.67(16) . .
O2 Mo2 O27 105.2(3) . .
O2 Mo2 O23 104.3(3) . .
O27 Mo2 O23 93.2(3) . .
O2 Mo2 O17 99.0(3) . .
O27 Mo2 O17 89.1(3) . .
O23 Mo2 O17 155.1(3) . .
O2 Mo2 O16 100.1(3) . .
O27 Mo2 O16 154.6(3) . .
O23 Mo2 O16 82.8(3) . .
O17 Mo2 O16 84.6(3) . .
O2 Mo2 O40 172.9(3) . .
O27 Mo2 O40 80.5(3) . .
O23 Mo2 O40 79.4(3) . .
O17 Mo2 O40 76.5(3) . .
O16 Mo2 O40 74.2(2) . .
O2 Mo2 Mo1 98.9(3) . .
O27 Mo2 Mo1 48.0(2) . .
O23 Mo2 Mo1 47.8(2) . .
O17 Mo2 Mo1 136.6(2) . .
O16 Mo2 Mo1 130.1(2) . .
O40 Mo2 Mo1 88.12(16) . .
O3 Mo3 O13 100.8(4) . .
O3 Mo3 O19 105.0(3) . .
O13 Mo3 O19 86.9(3) . .
O3 Mo3 O28 104.6(3) . .
O13 Mo3 O28 153.5(3) . .
O19 Mo3 O28 93.5(3) . .
O3 Mo3 O33 100.1(3) . .
O13 Mo3 O33 85.2(3) . .
O19 Mo3 O33 154.7(3) . .
O28 Mo3 O33 83.3(3) . .
O3 Mo3 O37 171.8(3) . .
O13 Mo3 O37 73.9(3) . .
O19 Mo3 O37 81.2(3) . .
O28 Mo3 O37 80.0(2) . .
O33 Mo3 O37 73.5(3) . .
O3 Mo3 Mo4 98.7(3) . .
O13 Mo3 Mo4 134.3(2) . .
O19 Mo3 Mo4 48.1(2) . .
O28 Mo3 Mo4 48.2(2) . .
O33 Mo3 Mo4 131.0(2) . .
O37 Mo3 Mo4 89.43(16) . .
O4 Mo4 O19 105.9(4) . .
O4 Mo4 O28 105.7(3) . .
O19 Mo4 O28 93.8(3) . .
O4 Mo4 O29 100.5(3) . .
O19 Mo4 O29 83.8(3) . .
O28 Mo4 O29 153.3(3) . .
O4 Mo4 O35 99.2(3) . .
O19 Mo4 O35 154.1(3) . .
O28 Mo4 O35 85.2(3) . .
O29 Mo4 O35 85.6(3) . .
O4 Mo4 O39 171.4(3) . .
O19 Mo4 O39 80.6(3) . .
O28 Mo4 O39 79.0(2) . .
O29 Mo4 O39 74.3(2) . .
O35 Mo4 O39 73.8(2) . .
O4 Mo4 Mo3 100.2(3) . .
O19 Mo4 Mo3 48.0(2) . .
O28 Mo4 Mo3 48.6(2) . .
O29 Mo4 Mo3 131.1(2) . .
O35 Mo4 Mo3 133.3(2) . .
O39 Mo4 Mo3 88.26(15) . .
O5 Mo5 O20 105.0(3) . .
O5 Mo5 O18 104.9(3) . .
O20 Mo5 O18 93.7(3) . .
O5 Mo5 O17 100.5(3) . .
O20 Mo5 O17 87.6(3) . .
O18 Mo5 O17 153.3(3) . .
O5 Mo5 O31 99.9(3) . .
O20 Mo5 O31 154.7(3) . .
O18 Mo5 O31 83.7(3) . .
O17 Mo5 O31 84.0(3) . .
O5 Mo5 O40 174.4(3) . .
O20 Mo5 O40 79.3(3) . .
O18 Mo5 O40 78.0(3) . .
O17 Mo5 O40 76.0(2) . .
O31 Mo5 O40 75.5(3) . .
O5 Mo5 Mo6 97.4(3) . .
O20 Mo5 Mo6 48.9(2) . .
O18 Mo5 Mo6 48.3(2) . .
O17 Mo5 Mo6 136.0(2) . .
O31 Mo5 Mo6 131.8(2) . .
O40 Mo5 Mo6 88.12(15) . .
O6 Mo6 O18 106.7(3) . .
O6 Mo6 O20 104.8(3) . .
O18 Mo6 O20 93.6(3) . .
O6 Mo6 O36 100.3(3) . .
O18 Mo6 O36 152.0(3) . .
O20 Mo6 O36 86.3(3) . .
O6 Mo6 O35 96.9(3) . .
O18 Mo6 O35 86.6(3) . .
O20 Mo6 O35 157.3(3) . .
O36 Mo6 O35 83.1(3) . .
O6 Mo6 O39 170.7(3) . .
O18 Mo6 O39 78.7(3) . .
O20 Mo6 O39 82.1(2) . .
O36 Mo6 O39 73.6(2) . .
O35 Mo6 O39 75.6(2) . .
O6 Mo6 Mo5 98.5(3) . .
O18 Mo6 Mo5 48.7(2) . .
O20 Mo6 Mo5 48.41(19) . .
O36 Mo6 Mo5 134.1(2) . .
O35 Mo6 Mo5 135.2(2) . .
O39 Mo6 Mo5 90.69(15) . .
O7 Mo7 O22 107.0(3) . .
O7 Mo7 O26 105.0(4) . .
O22 Mo7 O26 93.6(3) . .
O7 Mo7 O15 98.7(4) . .
O22 Mo7 O15 84.4(3) . .
O26 Mo7 O15 155.6(3) . .
O7 Mo7 O30 98.0(3) . .
O22 Mo7 O30 154.0(3) . .
O26 Mo7 O30 86.6(3) . .
O15 Mo7 O30 84.8(3) . .
O7 Mo7 O38 169.4(3) . .
O22 Mo7 O38 80.7(3) . .
O26 Mo7 O38 81.4(2) . .
O15 Mo7 O38 74.4(3) . .
O30 Mo7 O38 73.6(2) . .
O7 Mo7 Mo8 100.8(3) . .
O22 Mo7 Mo8 47.9(2) . .
O26 Mo7 Mo8 48.4(2) . .
O15 Mo7 Mo8 132.0(2) . .
O30 Mo7 Mo8 134.4(2) . .
O38 Mo7 Mo8 89.84(16) . .
O8 Mo8 O22 106.8(4) . .
O8 Mo8 O13 99.3(4) . .
O22 Mo8 O13 86.3(3) . .
O8 Mo8 O26 104.8(3) . .
O22 Mo8 O26 93.2(3) . .
O13 Mo8 O26 154.9(3) . .
O8 Mo8 O34 100.0(4) . .
O22 Mo8 O34 152.9(3) . .
O13 Mo8 O34 85.9(3) . .
O26 Mo8 O34 83.2(3) . .
O8 Mo8 O37 171.3(3) . .
O22 Mo8 O37 79.1(3) . .
O13 Mo8 O37 74.5(3) . .
O26 Mo8 O37 80.8(2) . .
O34 Mo8 O37 73.8(3) . .
O8 Mo8 Mo7 100.5(3) . .
O22 Mo8 Mo7 47.9(2) . .
O13 Mo8 Mo7 133.7(2) . .
O26 Mo8 Mo7 48.1(2) . .
O34 Mo8 Mo7 130.5(2) . .
O37 Mo8 Mo7 88.21(16) . .
O9 Mo9 O33 103.2(3) . .
O9 Mo9 O34 103.4(4) . .
O33 Mo9 O34 97.0(3) . .
O9 Mo9 O24 103.1(3) . .
O33 Mo9 O24 90.1(3) . .
O34 Mo9 O24 150.1(3) . .
O9 Mo9 O25 102.1(3) . .
O33 Mo9 O25 152.7(3) . .
O34 Mo9 O25 86.9(3) . .
O24 Mo9 O25 74.3(3) . .
O9 Mo9 O37 177.8(3) . .
O33 Mo9 O37 75.6(3) . .
O34 Mo9 O37 75.1(3) . .
O24 Mo9 O37 78.7(2) . .
O25 Mo9 O37 79.4(2) . .
O9 Mo9 Mo10 99.3(3) . .
O33 Mo9 Mo10 126.7(2) . .
O34 Mo9 Mo10 123.7(2) . .
O24 Mo9 Mo10 37.54(19) . .
O25 Mo9 Mo10 37.8(2) . .
O37 Mo9 Mo10 82.89(16) . .
O10 Mo10 O31 102.4(3) . .
O10 Mo10 O16 103.7(4) . .
O31 Mo10 O16 97.0(3) . .
O10 Mo10 O25 101.5(3) . .
O31 Mo10 O25 153.3(3) . .
O16 Mo10 O25 88.5(3) . .
O10 Mo10 O24 102.9(3) . .
O31 Mo10 O24 88.5(3) . .
O16 Mo10 O24 150.9(3) . .
O25 Mo10 O24 74.9(3) . .
O10 Mo10 O40 177.9(3) . .
O31 Mo10 O40 76.4(3) . .
O16 Mo10 O40 74.7(3) . .
O25 Mo10 O40 80.0(2) . .
O24 Mo10 O40 78.9(2) . .
O10 Mo10 Mo9 98.7(3) . .
O31 Mo10 Mo9 125.3(2) . .
O16 Mo10 Mo9 125.8(2) . .
O25 Mo10 Mo9 38.4(2) . .
O24 Mo10 Mo9 37.45(19) . .
O40 Mo10 Mo9 83.41(15) . .
O11 Mo11 O32 103.6(3) . .
O11 Mo11 O15 103.7(4) . .
O32 Mo11 O15 96.6(3) . .
O11 Mo11 O21 102.6(4) . .
O32 Mo11 O21 88.9(3) . .
O15 Mo11 O21 151.1(3) . .
O11 Mo11 O14 102.9(3) . .
O32 Mo11 O14 151.5(3) . .
O15 Mo11 O14 87.2(3) . .
O21 Mo11 O14 75.2(3) . .
O11 Mo11 O38 176.0(3) . .
O32 Mo11 O38 73.7(3) . .
O15 Mo11 O38 74.0(3) . .
O21 Mo11 O38 80.5(3) . .
O14 Mo11 O38 80.3(3) . .
O11 Mo11 Mo12 100.0(3) . .
O32 Mo11 Mo12 125.6(2) . .
O15 Mo11 Mo12 124.1(2) . .
O21 Mo11 Mo12 38.1(2) . .
O14 Mo11 Mo12 38.0(2) . .
O38 Mo11 Mo12 83.93(15) . .
O12 Mo12 O36 103.6(4) . .
O12 Mo12 O29 103.1(3) . .
O36 Mo12 O29 97.1(3) . .
O12 Mo12 O14 102.9(4) . .
O36 Mo12 O14 150.5(3) . .
O29 Mo12 O14 89.3(3) . .
O12 Mo12 O21 101.4(3) . .
O36 Mo12 O21 87.1(3) . .
O29 Mo12 O21 153.3(3) . .
O14 Mo12 O21 75.1(3) . .
O12 Mo12 O39 176.7(3) . .
O36 Mo12 O39 73.4(3) . .
O29 Mo12 O39 76.3(3) . .
O14 Mo12 O39 80.3(3) . .
O21 Mo12 O39 79.8(3) . .
O12 Mo12 Mo11 99.3(3) . .
O36 Mo12 Mo11 123.7(2) . .
O29 Mo12 Mo11 126.5(2) . .
O14 Mo12 Mo11 38.2(2) . .
O21 Mo12 Mo11 37.8(2) . .
O39 Mo12 Mo11 83.54(15) . .
O37 P1 O40 111.0(4) . .
O37 P1 O39 108.2(4) . .
O40 P1 O39 109.6(4) . .
O37 P1 O38 109.0(4) . .
O40 P1 O38 107.7(4) . .
O39 P1 O38 111.4(4) . .
C5 N1 C1 117.0(10) . .
C5 N1 Zn1 117.7(7) . .
C1 N1 Zn1 124.7(8) . .
C8 N2 C9 118.2(10) . .
C8 N2 Zn2 123.0(8) . 1_565
C9 N2 Zn2 118.4(8) . 1_565
C11 N3 C15 116.7(10) . .
C11 N3 Zn1 118.7(8) . .
C15 N3 Zn1 124.5(8) . .
C18 N4 C19 116.0(10) . .
C18 N4 Zn2 119.7(8) . 2_454
C19 N4 Zn2 124.2(8) . 2_454
C21B N5 C25 113.2(16) . .
C21B N5 C21A 34.4(14) . .
C25 N5 C21A 114.0(14) . .
C21B N5 Zn4 121.9(14) . .
C25 N5 Zn4 121.0(9) . .
C21A N5 Zn4 122.8(12) . .
C29 N6 C28 116.5(10) . .
C29 N6 Zn3 120.9(9) . 1_455
C28 N6 Zn3 121.3(9) . 1_455
C35 N7 C31 121.6(11) . .
C38 N8 C39 117.7(11) . .
N1 C1 C2 122.7(11) . .
C1 C2 C3 120.2(10) . .
C4 C3 C2 115.6(11) . .
C4 C3 C6 122.2(11) . .
C2 C3 C6 122.1(10) . .
C3 C4 C5 121.0(11) . .
N1 C5 C4 123.5(10) . .
C7 C6 C10 116.9(10) . .
C7 C6 C3 122.1(10) . .
C10 C6 C3 120.9(11) . .
C6 C7 C8 118.4(11) . .
N2 C8 C7 124.1(10) . .
N2 C9 C10 121.4(11) . .
C9 C10 C6 120.8(11) . .
N3 C11 C12 123.0(11) . .
C11 C12 C13 120.5(12) . .
C14 C13 C12 114.7(11) . .
C14 C13 C16 123.0(11) . .
C12 C13 C16 122.1(11) . .
C15 C14 C13 121.7(12) . .
N3 C15 C14 123.2(12) . .
C20 C16 C17 116.2(11) . .
C20 C16 C13 121.7(11) . .
C17 C16 C13 122.1(11) . .
C18 C17 C16 119.8(12) . .
N4 C18 C17 125.1(12) . .
N4 C19 C20 122.4(12) . .
C16 C20 C19 120.4(12) . .
C22A C21A N5 125(2) . .
C21A C22A C23 119(2) . .
N5 C21B C22B 123(2) . .
C21B C22B C23 120(2) . .
C22A C23 C24 117.5(15) . .
C22A C23 C22B 36.1(13) . .
C24 C23 C22B 108.8(14) . .
C22A C23 C26 123.1(14) . .
C24 C23 C26 119.2(12) . .
C22B C23 C26 122.4(15) . .
C23 C24 C25 119.4(14) . .
N5 C25 C24 123.0(14) . .
C27 C26 C30 116.1(11) . .
C27 C26 C23 123.6(11) . .
C30 C26 C23 120.3(12) . .
C28 C27 C26 121.0(12) . .
N6 C28 C27 123.0(12) . .
N6 C29 C30 125.6(13) . .
C29 C30 C26 117.6(13) . .
N7 C31 C32 119.0(13) . .
C31 C32 C33 120.9(13) . .
C34 C33 C32 116.5(11) . .
C34 C33 C36 123.3(11) . .
C32 C33 C36 119.9(11) . .
C35 C34 C33 120.4(13) . .
N7 C35 C34 121.3(12) . .
C37 C36 C40 115.4(12) . .
C37 C36 C33 121.0(11) . .
C40 C36 C33 123.3(11) . .
C38 C37 C36 119.9(13) . .
N8 C38 C37 123.5(12) . .
N8 C39 C40 123.7(13) . .
C39 C40 C36 119.3(13) . .
Mo3 O13 Mo8 124.7(4) . .
Mo12 O14 Mo11 103.8(3) . .
Mo12 O14 Zn4 124.5(4) . .
Mo11 O14 Zn4 128.2(4) . .
Mo11 O15 Mo7 126.2(4) . .
Mo10 O16 Mo2 124.6(3) . .
Mo2 O17 Mo5 120.3(3) . .
Mo6 O18 Mo5 83.0(3) . .
Mo6 O18 Zn2 139.4(4) . .
Mo5 O18 Zn2 135.1(3) . .
Mo3 O19 Mo4 84.0(3) . .
Mo3 O19 Zn4 140.1(4) . .
Mo4 O19 Zn4 131.7(4) . .
Mo5 O20 Mo6 82.7(3) . .
Mo5 O20 Zn1 145.5(4) . .
Mo6 O20 Zn1 127.5(3) . .
Mo11 O21 Mo12 104.2(3) . .
Mo11 O21 Zn1 125.3(4) . .
Mo12 O21 Zn1 126.9(4) . .
Mo7 O22 Mo8 84.2(3) . .
Mo7 O22 Zn4 132.7(4) . .
Mo8 O22 Zn4 140.7(4) . .
Mo1 O23 Mo2 83.7(3) . .
Mo1 O23 Zn3 137.7(4) . .
Mo2 O23 Zn3 128.5(4) . .
Mo9 O24 Mo10 105.0(3) . .
Mo9 O24 Zn2 122.3(3) . .
Mo10 O24 Zn2 129.7(3) . .
Zn3 O25 Mo10 122.9(4) . .
Zn3 O25 Mo9 124.1(4) . .
Mo10 O25 Mo9 103.8(3) . .
Zn3 O26 Mo7 135.5(4) . .
Zn3 O26 Mo8 128.7(4) . .
Mo7 O26 Mo8 83.5(3) . .
Mo1 O27 Mo2 83.7(3) . .
Mo1 O27 Zn1 128.1(3) . .
Mo2 O27 Zn1 143.3(4) . .
Mo4 O28 Mo3 83.1(3) . .
Mo4 O28 Zn2 142.0(4) . .
Mo3 O28 Zn2 130.2(4) . .
Mo12 O29 Mo4 125.6(3) . .
Mo1 O30 Mo7 120.3(3) . .
Mo10 O31 Mo5 123.5(4) . .
Mo11 O32 Mo1 127.2(4) . .
Mo9 O33 Mo3 126.2(4) . .
Mo9 O34 Mo8 124.9(4) . .
Mo4 O35 Mo6 119.8(3) . .
Mo12 O36 Mo6 127.0(4) . .
P1 O37 Mo8 127.2(4) . .
P1 O37 Mo3 127.0(4) . .
Mo8 O37 Mo3 86.9(2) . .
P1 O37 Mo9 131.8(4) . .
Mo8 O37 Mo9 84.7(2) . .
Mo3 O37 Mo9 83.7(2) . .
P1 O38 Mo1 126.2(4) . .
P1 O38 Mo7 125.8(4) . .
Mo1 O38 Mo7 92.2(2) . .
P1 O38 Mo11 129.8(4) . .
Mo1 O38 Mo11 84.4(2) . .
Mo7 O38 Mo11 84.8(2) . .
P1 O39 Mo6 125.0(4) . .
P1 O39 Mo4 127.1(4) . .
Mo6 O39 Mo4 90.8(2) . .
P1 O39 Mo12 131.3(4) . .
Mo6 O39 Mo12 85.4(2) . .
Mo4 O39 Mo12 83.02(19) . .
P1 O40 Mo2 128.3(4) . .
P1 O40 Mo5 126.5(4) . .
Mo2 O40 Mo5 87.0(2) . .
P1 O40 Mo10 130.9(4) . .
Mo2 O40 Mo10 84.96(19) . .
Mo5 O40 Mo10 83.8(2) . .
O6W O4W O5W 106.1(5) 2_545 4_565
C41 N9 O3W 59(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Zn1 O21 2.008(7) .
Zn1 O27 2.059(7) .
Zn1 O20 2.062(7) .
Zn1 N1 2.114(9) .
Zn1 N3 2.154(9) .
Zn1 Zn2 6.5399(16) .
Zn2 O28 1.994(7) .
Zn2 O24 2.031(7) .
Zn2 O18 2.071(7) .
Zn2 N2 2.134(9) 1_545
Zn2 N4 2.147(9) 2_444
Zn3 O25 1.938(7) .
Zn3 O26 1.944(7) .
Zn3 O23 1.983(7) .
Zn3 N6 2.017(9) 1_655
Zn4 O19 2.041(7) .
Zn4 O22 2.060(7) .
Zn4 O14 2.060(7) .
Zn4 N5 2.093(9) .
Zn4 O2W 2.174(10) .
Zn4 O1W 2.345(15) .
Mo1 O1 1.677(8) .
Mo1 O23 1.949(7) .
Mo1 O27 1.956(7) .
Mo1 O32 2.011(7) .
Mo1 O30 2.062(7) .
Mo1 O38 2.485(7) .
Mo1 Mo2 2.6144(13) .
Mo2 O2 1.664(7) .
Mo2 O27 1.963(7) .
Mo2 O23 1.969(7) .
Mo2 O17 1.971(7) .
Mo2 O16 2.048(7) .
Mo2 O40 2.487(7) .
Mo3 O3 1.669(7) .
Mo3 O13 1.953(7) .
Mo3 O19 1.956(7) .
Mo3 O28 1.979(7) .
Mo3 O33 2.029(7) .
Mo3 O37 2.547(7) .
Mo3 Mo4 2.6175(13) .
Mo4 O4 1.670(8) .
Mo4 O19 1.958(7) .
Mo4 O28 1.967(7) .
Mo4 O29 2.018(7) .
Mo4 O35 2.067(7) .
Mo4 O39 2.565(7) .
Mo5 O5 1.685(7) .
Mo5 O20 1.953(7) .
Mo5 O18 1.962(7) .
Mo5 O17 1.986(7) .
Mo5 O31 2.038(7) .
Mo5 O40 2.499(6) .
Mo5 Mo6 2.5903(12) .
Mo6 O6 1.675(7) .
Mo6 O18 1.949(7) .
Mo6 O20 1.966(7) .
Mo6 O36 2.023(7) .
Mo6 O35 2.080(7) .
Mo6 O39 2.472(6) .
Mo7 O7 1.675(8) .
Mo7 O22 1.956(7) .
Mo7 O26 1.964(7) .
Mo7 O15 2.021(7) .
Mo7 O30 2.073(7) .
Mo7 O38 2.489(7) .
Mo7 Mo8 2.6231(13) .
Mo8 O8 1.671(8) .
Mo8 O22 1.958(7) .
Mo8 O13 1.972(7) .
Mo8 O26 1.975(7) .
Mo8 O34 2.048(7) .
Mo8 O37 2.508(7) .
Mo9 O9 1.696(7) .
Mo9 O33 1.816(7) .
Mo9 O34 1.825(7) .
Mo9 O24 1.997(7) .
Mo9 O25 2.031(7) .
Mo9 O37 2.593(7) .
Mo9 Mo10 3.1724(13) .
Mo10 O10 1.681(8) .
Mo10 O31 1.827(7) .
Mo10 O16 1.831(7) .
Mo10 O25 2.001(7) .
Mo10 O24 2.001(7) .
Mo10 O40 2.599(7) .
Mo11 O11 1.694(8) .
Mo11 O32 1.816(7) .
Mo11 O15 1.840(7) .
Mo11 O21 1.990(7) .
Mo11 O14 2.006(7) .
Mo11 O38 2.617(7) .
Mo11 Mo12 3.1513(13) .
Mo12 O12 1.681(7) .
Mo12 O36 1.823(7) .
Mo12 O29 1.831(7) .
Mo12 O14 1.999(7) .
Mo12 O21 2.004(7) .
Mo12 O39 2.601(7) .
P1 O37 1.548(7) .
P1 O40 1.550(7) .
P1 O39 1.557(7) .
P1 O38 1.570(7) .
N1 C5 1.318(14) .
N1 C1 1.330(14) .
N2 C8 1.323(14) .
N2 C9 1.333(15) .
N2 Zn2 2.134(9) 1_565
N3 C11 1.333(15) .
N3 C15 1.336(14) .
N4 C18 1.310(15) .
N4 C19 1.354(16) .
N4 Zn2 2.147(9) 2_454
N5 C21B 1.28(3) .
N5 C25 1.312(18) .
N5 C21A 1.38(3) .
N6 C29 1.307(16) .
N6 C28 1.316(17) .
N6 Zn3 2.017(9) 1_455
N7 C35 1.300(16) .
N7 C31 1.339(18) .
N8 C38 1.300(17) .
N8 C39 1.326(17) .
C1 C2 1.390(15) .
C2 C3 1.396(16) .
C3 C4 1.363(16) .
C3 C6 1.472(14) .
C4 C5 1.382(16) .
C6 C7 1.383(15) .
C6 C10 1.403(15) .
C7 C8 1.397(16) .
C9 C10 1.383(16) .
C11 C12 1.378(17) .
C12 C13 1.399(17) .
C13 C14 1.384(17) .
C13 C16 1.474(15) .
C14 C15 1.355(16) .
C16 C20 1.377(17) .
C16 C17 1.385(17) .
C17 C18 1.370(16) .
C19 C20 1.390(17) .
C21A C22A 1.35(3) .
C22A C23 1.36(3) .
C21B C22B 1.40(4) .
C22B C23 1.41(3) .
C23 C24 1.369(19) .
C23 C26 1.475(15) .
C24 C25 1.42(2) .
C26 C27 1.381(18) .
C26 C30 1.391(18) .
C27 C28 1.365(18) .
C29 C30 1.382(18) .
C31 C32 1.366(18) .
C32 C33 1.395(16) .
C33 C34 1.368(17) .
C33 C36 1.494(16) .
C34 C35 1.361(17) .
C36 C37 1.390(18) .
C36 C40 1.414(18) .
C37 C38 1.383(18) .
C39 C40 1.364(19) .
O3W N9 3.16(3) .
O4W O6W 2.717(17) 2_545
O4W O5W 2.839(14) 4_565
O6W N9 3.15(3) 2
N9 C41 1.53(4) .
