#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:26:17 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179377 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/74/4327477.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4327477
loop_
_publ_author_name
'Angel Ugrinov'
'Slavi C. Sevov'
_publ_contact_author
;
Slavi C. Sevov
Department of Chemistry and Biochemistry
251 Nieuwland Science Hall
University of Notre Dame
Notre Dame, IN 46556-5670
USA
;
_publ_contact_author_email       ssevov@nd.edu
_publ_contact_author_fax         'Intl. Code + (574)631-6652'
_publ_contact_author_phone       'Intl. Code + (574)631-5891'
_publ_section_title
;
 [Ge9Ge9Ge9Ge9]8-: A Linear Tetramer of Nine-Atom Germanium Clusters, a
 Nanorod
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5789
_journal_page_last               5791
_journal_paper_doi               10.1021/ic034677+
_journal_volume                  42
_journal_year                    2003
_chemical_formula_sum            'C108 H240 Ge36 N12 O48 Rb8'
_chemical_formula_weight         5772.12
_chemical_name_systematic
; 
(Rb-18C6)8(Ge9=Ge9=Ge9=Ge9).6en (2)
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.355(3)
_cell_angle_beta                 97.813(3)
_cell_angle_gamma                101.257(3)
_cell_formula_units_Z            1
_cell_length_a                   13.5706(19)
_cell_length_b                   15.885(2)
_cell_length_c                   22.645(3)
_cell_measurement_temperature    100(2)
_cell_volume                     4652.5(11)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL-V5.1'
_computing_molecular_graphics    'Bruker SHELXTL-V5.1'
_computing_publication_material  'Bruker SHELXTL-V5.1'
_computing_structure_refinement  'Bruker SHELXTL-V5.1'
_computing_structure_solution    'Bruker SHELXTL-V5.1'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.2613
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            16368
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.94
_exptl_absorpt_coefficient_mu    7.860
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.7275
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   xabs
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.060
_exptl_crystal_description       plate-like
_exptl_crystal_F_000             2804
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.03
_refine_diff_density_max         1.549
_refine_diff_density_min         -0.905
_refine_diff_density_rms         0.180
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.810
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     896
_refine_ls_number_reflns         16368
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.810
_refine_ls_R_factor_all          0.1635
_refine_ls_R_factor_gt           0.0649
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0228P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1201
_refine_ls_wR_factor_ref         0.1407
_reflns_number_gt                6622
_reflns_number_total             16368
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0346772Bsi20030609_044634_2.cif
_cod_data_source_block           compound-2
_cod_database_code               4327477
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ge1A Ge 0.10605(13) 0.06022(11) 0.27426(9) 0.0359(5) Uani 1 1 d .
Ge2A Ge -0.03229(12) 0.14312(10) 0.27086(8) 0.0287(4) Uani 1 1 d .
Ge3A Ge 0.16472(12) 0.22561(10) 0.27806(8) 0.0317(4) Uani 1 1 d .
Ge4A Ge 0.17797(12) 0.10085(10) 0.18201(8) 0.0320(4) Uani 1 1 d .
Ge5A Ge -0.01485(12) 0.01410(10) 0.16915(9) 0.0364(5) Uani 1 1 d .
Ge6A Ge 0.01137(12) 0.26796(10) 0.20896(8) 0.0311(4) Uani 1 1 d .
Ge7A Ge 0.17330(13) 0.25673(11) 0.17032(9) 0.0421(5) Uani 1 1 d .
Ge8A Ge 0.02796(13) 0.12891(12) 0.10662(9) 0.0393(5) Uani 1 1 d .
Ge9A Ge -0.12546(12) 0.13022(11) 0.16526(9) 0.0373(5) Uani 1 1 d .
Ge1B Ge -0.08737(12) 0.49803(10) 0.32541(8) 0.0312(4) Uani 1 1 d .
Ge2B Ge 0.01603(11) 0.37893(10) 0.30994(8) 0.0276(4) Uani 1 1 d .
Ge3B Ge -0.18606(11) 0.33846(10) 0.31013(8) 0.0285(4) Uani 1 1 d .
Ge4B Ge -0.17425(11) 0.45630(10) 0.41431(8) 0.0265(4) Uani 1 1 d .
Ge5B Ge 0.02887(11) 0.50779(9) 0.42471(8) 0.0246(4) Uani 1 1 d .
Ge6B Ge -0.05376(11) 0.25654(9) 0.36332(8) 0.0258(4) Uani 1 1 d .
Ge7B Ge -0.20647(11) 0.29206(10) 0.41323(8) 0.0310(4) Uani 1 1 d .
Ge8B Ge -0.04303(11) 0.38262(9) 0.47819(8) 0.0240(4) Uani 1 1 d .
Ge9B Ge 0.10362(11) 0.37233(10) 0.41924(8) 0.0301(4) Uani 1 1 d .
Rb1 Rb -0.32639(11) 0.09037(9) 0.31783(8) 0.0354(4) Uani 1 1 d .
O11 O -0.5068(7) 0.1632(6) 0.3340(6) 0.036(3) Uani 1 1 d .
O12 O -0.4433(7) 0.0808(6) 0.4271(5) 0.033(3) Uani 1 1 d .
O13 O -0.3533(9) -0.0175(7) 0.2022(5) 0.046(3) Uani 1 1 d .
O14 O -0.2838(7) -0.0047(6) 0.4140(5) 0.038(3) Uani 1 1 d .
O15 O -0.2743(7) -0.0866(6) 0.2960(5) 0.033(3) Uani 1 1 d .
O16 O -0.4908(9) 0.0831(8) 0.2173(6) 0.054(4) Uani 1 1 d .
C101 C -0.2031(12) -0.0807(10) 0.3464(9) 0.044(5) Uani 1 1 d .
H10A H -0.1529 -0.0260 0.3529 0.053 Uiso 1 1 calc R
H10B H -0.1682 -0.1283 0.3400 0.053 Uiso 1 1 calc R
C102 C -0.2316(12) -0.0882(10) 0.2426(8) 0.044(5) Uani 1 1 d .
H10C H -0.2014 -0.1387 0.2355 0.053 Uiso 1 1 calc R
H10D H -0.1787 -0.0358 0.2467 0.053 Uiso 1 1 calc R
C103 C -0.3393(11) -0.0065(10) 0.4621(8) 0.040(5) Uani 1 1 d .
H10E H -0.2970 -0.0162 0.4973 0.048 Uiso 1 1 calc R
H10F H -0.3985 -0.0549 0.4505 0.048 Uiso 1 1 calc R
C104 C -0.5702(12) 0.1682(10) 0.2820(8) 0.039(5) Uani 1 1 d .
H10G H -0.5933 0.2225 0.2886 0.047 Uiso 1 1 calc R
H10H H -0.6297 0.1202 0.2738 0.047 Uiso 1 1 calc R
C105 C -0.3140(12) -0.0929(10) 0.1912(7) 0.038(4) Uiso 1 1 d .
H10I H -0.2871 -0.0962 0.1535 0.045 Uiso 1 1 calc R
H10J H -0.3675 -0.1447 0.1876 0.045 Uiso 1 1 calc R
C106 C -0.5207(13) 0.1646(10) 0.2320(8) 0.044(5) Uani 1 1 d .
H10K H -0.4606 0.2121 0.2406 0.053 Uiso 1 1 calc R
H10L H -0.5656 0.1726 0.1973 0.053 Uiso 1 1 calc R
C107 C -0.3736(11) 0.0775(11) 0.4785(8) 0.041(5) Uani 1 1 d .
H10M H -0.4064 0.0773 0.5139 0.049 Uiso 1 1 calc R
H10N H -0.3162 0.1273 0.4869 0.049 Uiso 1 1 calc R
C108 C -0.4780(11) 0.1602(11) 0.4372(9) 0.052(6) Uani 1 1 d .
H10O H -0.4211 0.2100 0.4430 0.063 Uiso 1 1 calc R
H10P H -0.5091 0.1644 0.4734 0.063 Uiso 1 1 calc R
C109 C -0.2516(13) -0.0846(10) 0.3998(8) 0.046(5) Uani 1 1 d .
H10Q H -0.3096 -0.1339 0.3913 0.056 Uiso 1 1 calc R
H10R H -0.2036 -0.0913 0.4336 0.056 Uiso 1 1 calc R
C110 C -0.4429(13) 0.0778(13) 0.1673(9) 0.060(6) Uani 1 1 d .
H11A H -0.3803 0.1226 0.1757 0.072 Uiso 1 1 calc R
H11B H -0.4868 0.0878 0.1328 0.072 Uiso 1 1 calc R
C111 C -0.4191(13) -0.0110(11) 0.1525(9) 0.056(6) Uani 1 1 d .
H11C H -0.4808 -0.0567 0.1454 0.067 Uiso 1 1 calc R
H11D H -0.3875 -0.0161 0.1165 0.067 Uiso 1 1 calc R
C112 C -0.5519(12) 0.1601(10) 0.3848(9) 0.045(5) Uani 1 1 d .
H11E H -0.6057 0.1076 0.3774 0.054 Uiso 1 1 calc R
H11F H -0.5824 0.2102 0.3927 0.054 Uiso 1 1 calc R
Rb2 Rb 0.13718(11) 0.29844(9) 0.60142(8) 0.0317(4) Uani 1 1 d .
O21 O -0.0087(8) 0.1240(7) 0.5439(5) 0.038(3) Uani 1 1 d .
O22 O 0.1686(8) 0.2837(6) 0.7348(5) 0.034(3) Uani 1 1 d .
O23 O 0.1516(9) 0.1905(6) 0.4908(5) 0.040(3) Uani 1 1 d .
O24 O 0.3366(8) 0.2682(7) 0.5623(6) 0.050(4) Uani 1 1 d .
O25 O -0.0160(7) 0.2031(6) 0.6616(5) 0.033(3) Uani 1 1 d .
O26 O 0.3370(7) 0.3432(7) 0.6841(7) 0.049(4) Uani 1 1 d .
C201 C 0.0030(11) 0.2063(11) 0.7238(9) 0.044(5) Uani 1 1 d .
H20A H 0.0283 0.1554 0.7317 0.053 Uiso 1 1 calc R
H20B H -0.0601 0.2046 0.7396 0.053 Uiso 1 1 calc R
C202 C -0.0213(13) 0.1252(10) 0.4837(9) 0.048(5) Uani 1 1 d .
H20C H -0.0427 0.1780 0.4767 0.058 Uiso 1 1 calc R
H20D H -0.0742 0.0754 0.4618 0.058 Uiso 1 1 calc R
C203 C 0.3143(16) 0.2780(14) 0.5018(10) 0.066(7) Uani 1 1 d .
H20E H 0.3767 0.2873 0.4851 0.079 Uiso 1 1 calc R
H20F H 0.2850 0.3288 0.5004 0.079 Uiso 1 1 calc R
C204 C 0.2485(12) 0.3524(12) 0.7663(8) 0.053(5) Uani 1 1 d .
H20G H 0.2544 0.3545 0.8097 0.063 Uiso 1 1 calc R
H20H H 0.2363 0.4078 0.7579 0.063 Uiso 1 1 calc R
C205 C 0.0782(13) 0.1218(10) 0.4599(8) 0.045(5) Uani 1 1 d .
H20I H 0.0981 0.0677 0.4651 0.054 Uiso 1 1 calc R
H20J H 0.0687 0.1236 0.4169 0.054 Uiso 1 1 calc R
C206 C -0.0962(11) 0.1300(10) 0.5663(10) 0.049(6) Uani 1 1 d .
H20K H -0.1514 0.0817 0.5450 0.059 Uiso 1 1 calc R
H20L H -0.1152 0.1842 0.5603 0.059 Uiso 1 1 calc R
C207 C 0.2430(15) 0.2006(13) 0.4656(9) 0.057(6) Uani 1 1 d .
H20M H 0.2287 0.2074 0.4237 0.069 Uiso 1 1 calc R
H20N H 0.2717 0.1494 0.4666 0.069 Uiso 1 1 calc R
C208 C -0.0793(11) 0.1278(11) 0.6313(9) 0.042(5) Uani 1 1 d .
H20O H -0.1438 0.1208 0.6459 0.050 Uiso 1 1 calc R
H20P H -0.0496 0.0786 0.6380 0.050 Uiso 1 1 calc R
C209 C 0.4122(15) 0.3389(13) 0.5984(9) 0.065(6) Uiso 1 1 d .
H20Q H 0.3919 0.3934 0.5950 0.078 Uiso 1 1 calc R
H20R H 0.4760 0.3406 0.5832 0.078 Uiso 1 1 calc R
C210 C 0.3431(12) 0.3361(10) 0.7454(9) 0.042(5) Uani 1 1 d .
H21A H 0.4018 0.3783 0.7697 0.050 Uiso 1 1 calc R
H21B H 0.3511 0.2780 0.7499 0.050 Uiso 1 1 calc R
C211 C 0.0761(11) 0.2838(11) 0.7542(8) 0.038(4) Uani 1 1 d .
H21C H 0.0520 0.3349 0.7456 0.046 Uiso 1 1 calc R
H21D H 0.0849 0.2866 0.7978 0.046 Uiso 1 1 calc R
C212 C 0.4281(13) 0.3308(12) 0.6633(8) 0.050(5) Uiso 1 1 d .
H21E H 0.4396 0.2735 0.6672 0.060 Uiso 1 1 calc R
H21F H 0.4863 0.3750 0.6863 0.060 Uiso 1 1 calc R
Rb3 Rb 0.29444(11) 0.46799(10) 0.28705(8) 0.0386(5) Uani 1 1 d .
O31 O 0.4401(8) 0.4822(7) 0.1951(6) 0.046(3) Uani 1 1 d .
O32 O 0.3041(8) 0.5826(7) 0.4011(6) 0.043(3) Uani 1 1 d .
O33 O 0.2616(8) 0.6543(6) 0.3037(6) 0.042(3) Uani 1 1 d .
O34 O 0.2879(7) 0.5753(6) 0.1886(5) 0.037(3) Uani 1 1 d .
O35 O 0.4449(7) 0.4829(6) 0.4073(6) 0.044(3) Uani 1 1 d .
O36 O 0.4840(8) 0.4037(7) 0.2925(6) 0.046(3) Uani 1 1 d .
C301 C 0.4792(12) 0.4045(10) 0.1897(9) 0.049(5) Uani 1 1 d .
H30A H 0.5191 0.4015 0.1572 0.059 Uiso 1 1 calc R
H30B H 0.4238 0.3530 0.1808 0.059 Uiso 1 1 calc R
C302 C 0.5420(13) 0.4091(10) 0.2468(10) 0.053(6) Uani 1 1 d .
H30C H 0.5775 0.3616 0.2436 0.064 Uiso 1 1 calc R
H30D H 0.5927 0.4639 0.2570 0.064 Uiso 1 1 calc R
C303 C 0.3800(13) 0.4830(12) 0.1364(8) 0.056(6) Uani 1 1 d .
H30E H 0.3187 0.4366 0.1270 0.068 Uiso 1 1 calc R
H30F H 0.4196 0.4757 0.1041 0.068 Uiso 1 1 calc R
C304 C 0.3487(12) 0.5657(12) 0.4564(8) 0.046(5) Uani 1 1 d .
H30G H 0.4091 0.6114 0.4738 0.055 Uiso 1 1 calc R
H30H H 0.3010 0.5669 0.4846 0.055 Uiso 1 1 calc R
C305 C 0.2079(13) 0.6653(11) 0.3522(9) 0.052(5) Uani 1 1 d .
H30I H 0.1472 0.6186 0.3452 0.062 Uiso 1 1 calc R
H30J H 0.1869 0.7206 0.3553 0.062 Uiso 1 1 calc R
C306 C 0.2666(15) 0.6568(13) 0.2009(9) 0.067(7) Uani 1 1 d .
H30K H 0.2300 0.6687 0.1644 0.080 Uiso 1 1 calc R
H30L H 0.3299 0.7008 0.2135 0.080 Uiso 1 1 calc R
C307 C 0.2727(13) 0.6640(11) 0.4075(9) 0.052(5) Uani 1 1 d .
H30M H 0.3319 0.7122 0.4156 0.063 Uiso 1 1 calc R
H30N H 0.2360 0.6700 0.4413 0.063 Uiso 1 1 calc R
C308 C 0.2041(13) 0.6617(13) 0.2497(9) 0.067(7) Uani 1 1 d .
H30O H 0.1831 0.7171 0.2550 0.080 Uiso 1 1 calc R
H30P H 0.1432 0.6149 0.2387 0.080 Uiso 1 1 calc R
C309 C 0.4694(12) 0.3977(10) 0.3938(8) 0.044(5) Uani 1 1 d .
H30Q H 0.4073 0.3531 0.3783 0.053 Uiso 1 1 calc R
H30R H 0.5031 0.3841 0.4305 0.053 Uiso 1 1 calc R
C310 C 0.3755(12) 0.4847(11) 0.4488(9) 0.051(5) Uani 1 1 d .
H31A H 0.3150 0.4383 0.4334 0.061 Uiso 1 1 calc R
H31B H 0.4069 0.4754 0.4876 0.061 Uiso 1 1 calc R
C311 C 0.3540(12) 0.5692(11) 0.1439(9) 0.049(5) Uani 1 1 d .
H31C H 0.4158 0.6148 0.1570 0.059 Uiso 1 1 calc R
H31D H 0.3199 0.5772 0.1054 0.059 Uiso 1 1 calc R
C312 C 0.5378(14) 0.3990(10) 0.3475(10) 0.058(6) Uani 1 1 d .
H31E H 0.5950 0.4490 0.3604 0.070 Uiso 1 1 calc R
H31F H 0.5645 0.3463 0.3433 0.070 Uiso 1 1 calc R
Rb4 Rb -0.11591(12) 0.26757(11) 0.04649(9) 0.0439(5) Uani 1 1 d .
O41 O -0.1783(9) 0.3915(7) 0.1286(6) 0.054(3) Uani 1 1 d .
O42 O -0.3315(10) 0.2610(9) 0.0599(7) 0.063(4) Uani 1 1 d .
O43 O -0.0060(9) 0.4544(8) 0.0850(7) 0.065(4) Uani 1 1 d .
O44 O 0.0476(10) 0.3455(8) -0.0068(6) 0.058(4) Uani 1 1 d .
O45 O -0.2791(9) 0.1474(8) -0.0356(6) 0.062(4) Uani 1 1 d .
O46 O -0.1121(12) 0.2172(8) -0.0849(6) 0.076(4) Uani 1 1 d .
C401 C 0.0934(13) 0.4526(13) 0.0792(10) 0.061(6) Uani 1 1 d .
H40A H 0.1160 0.4106 0.1015 0.073 Uiso 1 1 calc R
H40B H 0.1371 0.5097 0.0966 0.073 Uiso 1 1 calc R
C402 C -0.0188(15) 0.4782(11) 0.1459(8) 0.049(5) Uani 1 1 d .
H40C H 0.0016 0.4365 0.1692 0.059 Uiso 1 1 calc R
H40D H 0.0239 0.5356 0.1638 0.059 Uiso 1 1 calc R
C403 C -0.3281(14) 0.2880(11) 0.1216(9) 0.052(5) Uani 1 1 d .
H40E H -0.2902 0.2543 0.1444 0.063 Uiso 1 1 calc R
H40F H -0.3966 0.2790 0.1309 0.063 Uiso 1 1 calc R
C404 C -0.1214(13) 0.4795(11) 0.1473(8) 0.047(5) Uani 1 1 d .
H40G H -0.1447 0.5155 0.1201 0.057 Uiso 1 1 calc R
H40H H -0.1299 0.5033 0.1881 0.057 Uiso 1 1 calc R
C405 C 0.1020(13) 0.4286(11) 0.0154(10) 0.058(6) Uani 1 1 d .
H40I H 0.0759 0.4684 -0.0076 0.069 Uiso 1 1 calc R
H40J H 0.1731 0.4325 0.0116 0.069 Uiso 1 1 calc R
C406 C -0.2781(13) 0.3810(11) 0.1386(9) 0.056(5) Uani 1 1 d .
H40K H -0.3143 0.4142 0.1144 0.067 Uiso 1 1 calc R
H40L H -0.2790 0.4025 0.1810 0.067 Uiso 1 1 calc R
C407 C -0.3801(13) 0.1710(12) 0.0408(9) 0.060(6) Uani 1 1 d .
H40M H -0.4494 0.1612 0.0490 0.072 Uiso 1 1 calc R
H40N H -0.3434 0.1358 0.0627 0.072 Uiso 1 1 calc R
C408 C 0.0450(19) 0.3148(15) -0.0691(10) 0.085(8) Uani 1 1 d .
H40O H 0.0119 0.3507 -0.0925 0.102 Uiso 1 1 calc R
H40P H 0.1144 0.3210 -0.0769 0.102 Uiso 1 1 calc R
C409 C -0.1670(16) 0.1299(12) -0.1011(10) 0.075(7) Uani 1 1 d .
H40Q H -0.1387 0.0957 -0.0742 0.090 Uiso 1 1 calc R
H40R H -0.1609 0.1057 -0.1423 0.090 Uiso 1 1 calc R
C410 C -0.0066(15) 0.2274(13) -0.0887(11) 0.070(7) Uani 1 1 d .
H41A H 0.0234 0.1916 -0.0637 0.084 Uiso 1 1 calc R
H41B H 0.0007 0.2076 -0.1303 0.084 Uiso 1 1 calc R
C411 C -0.2752(14) 0.1246(14) -0.0971(10) 0.075(7) Uani 1 1 d .
H41C H -0.3022 0.1646 -0.1195 0.091 Uiso 1 1 calc R
H41D H -0.3149 0.0657 -0.1137 0.091 Uiso 1 1 calc R
C412 C -0.3812(15) 0.1449(15) -0.0281(10) 0.081(7) Uani 1 1 d .
H41E H -0.4231 0.0866 -0.0439 0.098 Uiso 1 1 calc R
H41F H -0.4087 0.1856 -0.0496 0.098 Uiso 1 1 calc R
NC1 N 0.298(2) 0.8999(15) 0.2622(12) 0.157(11) Uani 1 1 d .
HC3A H 0.2439 0.9234 0.2619 0.236 Uiso 0.67 1 calc PR
HC3B H 0.2796 0.8450 0.2415 0.236 Uiso 0.67 1 calc PR
HC3C H 0.3442 0.9307 0.2448 0.236 Uiso 0.67 1 calc PR
CN1 C 0.435(2) 0.8702(18) 0.3246(16) 0.145(16) Uani 1 1 d .
HN3A H 0.4879 0.9067 0.3567 0.174 Uiso 1 1 calc R
HN3B H 0.4246 0.8102 0.3303 0.174 Uiso 1 1 calc R
NC2 N 0.461(3) 0.877(2) 0.2661(17) 0.26(2) Uani 1 1 d .
HC4A H 0.5170 0.8575 0.2624 0.383 Uiso 0.67 1 calc PR
HC4B H 0.4713 0.9329 0.2621 0.383 Uiso 0.67 1 calc PR
HC4C H 0.4097 0.8453 0.2373 0.383 Uiso 0.67 1 calc PR
CN2 C 0.3416(7) 0.9007(6) 0.3233(4) 0.21(3) Uani 1 1 d .
HN4A H 0.2937 0.8632 0.3412 0.257 Uiso 1 1 calc R
HN4B H 0.3553 0.9596 0.3470 0.257 Uiso 1 1 calc R
NC3 N 0.1756(7) 0.1161(6) -0.0209(4) 0.096(6) Uani 1 1 d R
HC3D H 0.1105 0.0905 -0.0356 0.144 Uiso 0.67 1 calc PR
HC3E H 0.2027 0.1431 -0.0483 0.144 Uiso 0.67 1 calc PR
HC3F H 0.1794 0.1550 0.0129 0.144 Uiso 0.67 1 calc PR
NC4 N -0.6466(7) 0.1574(6) 0.0703(4) 0.154(11) Uani 1 1 d R
HC4D H -0.5808 0.1833 0.0813 0.232 Uiso 0.67 1 calc PR
HC4E H -0.6673 0.1302 0.0994 0.232 Uiso 0.67 1 calc PR
HC4F H -0.6827 0.1975 0.0648 0.232 Uiso 0.67 1 calc PR
CN4 C -0.6606(7) 0.0978(6) 0.0174(4) 0.071(6) Uani 1 1 d R
HN4C H -0.6191 0.0557 0.0239 0.085 Uiso 1 1 calc R
HN4D H -0.6356 0.1282 -0.0133 0.085 Uiso 1 1 calc R
CN3 C 0.2325(7) 0.0490(6) -0.0068(4) 0.091(8) Uani 1 1 d R
HN3C H 0.2295 0.0061 -0.0431 0.110 Uiso 1 1 calc R
HN3D H 0.2042 0.0191 0.0233 0.110 Uiso 1 1 calc R
NC5 N 0.3673(7) 0.4245(6) -0.0499(4) 0.33(2) Uiso 1 1 d R
HC5A H 0.3420 0.4563 -0.0745 0.495 Uiso 0.67 1 calc PR
HC5B H 0.4123 0.4597 -0.0193 0.495 Uiso 0.67 1 calc PR
HC5C H 0.3169 0.3943 -0.0353 0.495 Uiso 0.67 1 calc PR
CN5 C 0.4101(7) 0.3731(6) -0.0786(4) 0.33(3) Uiso 1 1 d R
HN5A H 0.4608 0.4092 -0.0957 0.392 Uiso 1 1 calc R
HN5B H 0.3590 0.3393 -0.1127 0.392 Uiso 1 1 calc R
NC6 N 0.4695(7) 0.3461(6) 0.0100(4) 0.38(3) Uiso 1 1 d R
HC6A H 0.5003 0.3122 0.0304 0.570 Uiso 0.67 1 calc PR
HC6B H 0.4082 0.3453 0.0200 0.570 Uiso 0.67 1 calc PR
HC6C H 0.5068 0.4006 0.0195 0.570 Uiso 0.67 1 calc PR
CN6 C 0.4584(7) 0.3132(6) -0.0555(4) 0.76(9) Uiso 1 1 d R
HN6A H 0.5242 0.3145 -0.0681 0.909 Uiso 1 1 calc R
HN6B H 0.4167 0.2542 -0.0676 0.909 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge2A Ge1A Ge4A 98.19(8) . .
Ge2A Ge1A Ge3A 64.55(6) . .
Ge4A Ge1A Ge3A 64.82(7) . .
Ge2A Ge1A Ge5A 69.03(7) . .
Ge4A Ge1A Ge5A 62.20(7) . .
Ge3A Ge1A Ge5A 100.10(8) . .
Ge2A Ge1A C208 116.4(2) . 2_556
Ge4A Ge1A C208 140.8(3) . 2_556
Ge3A Ge1A C208 145.9(3) . 2_556
Ge5A Ge1A C208 112.1(3) . 2_556
Ge2A Ge1A NC1 171.6(4) . 1_545
Ge4A Ge1A NC1 81.1(4) . 1_545
Ge3A Ge1A NC1 121.9(4) . 1_545
Ge5A Ge1A NC1 103.6(4) . 1_545
C208 Ge1A NC1 61.9(4) 2_556 1_545
Ge2A Ge1A Ge9A 33.68(5) . .
Ge4A Ge1A Ge9A 73.21(6) . .
Ge3A Ge1A Ge9A 73.83(6) . .
Ge5A Ge1A Ge9A 36.83(5) . .
C208 Ge1A Ge9A 127.6(2) 2_556 .
NC1 Ge1A Ge9A 139.8(4) 1_545 .
Ge2A Ge1A Ge8A 66.00(6) . .
Ge4A Ge1A Ge8A 36.91(5) . .
Ge3A Ge1A Ge8A 67.59(6) . .
Ge5A Ge1A Ge8A 34.65(5) . .
C208 Ge1A Ge8A 146.1(3) 2_556 .
NC1 Ge1A Ge8A 110.4(4) 1_545 .
Ge9A Ge1A Ge8A 36.60(4) . .
Ge2A Ge1A Ge6A 36.50(5) . .
Ge4A Ge1A Ge6A 64.34(5) . .
Ge3A Ge1A Ge6A 38.46(5) . .
Ge5A Ge1A Ge6A 65.95(5) . .
C208 Ge1A Ge6A 152.9(2) 2_556 .
NC1 Ge1A Ge6A 145.0(4) 1_545 .
Ge9A Ge1A Ge6A 35.38(4) . .
Ge8A Ge1A Ge6A 42.03(4) . .
Ge2A Ge1A C201 112.6(2) . 2_556
Ge4A Ge1A C201 118.7(2) . 2_556
Ge3A Ge1A C201 176.2(2) . 2_556
Ge5A Ge1A C201 80.8(3) . 2_556
C208 Ge1A C201 32.2(3) 2_556 2_556
NC1 Ge1A C201 61.2(4) 1_545 2_556
Ge9A Ge1A C201 105.3(2) . 2_556
Ge8A Ge1A C201 114.0(3) . 2_556
Ge6A Ge1A C201 140.5(2) . 2_556
Ge1A Ge2A Ge9A 112.81(9) . .
Ge1A Ge2A Ge6B 123.43(9) . .
Ge9A Ge2A Ge6B 122.65(8) . .
Ge1A Ge2A Ge6A 109.17(8) . .
Ge9A Ge2A Ge6A 59.09(7) . .
Ge6B Ge2A Ge6A 90.99(7) . .
Ge1A Ge2A Ge3A 59.17(6) . .
Ge9A Ge2A Ge3A 108.89(9) . .
Ge6B Ge2A Ge3A 91.54(7) . .
Ge6A Ge2A Ge3A 60.49(6) . .
Ge1A Ge2A Ge5A 57.32(6) . .
Ge9A Ge2A Ge5A 57.06(6) . .
Ge6B Ge2A Ge5A 178.09(8) . .
Ge6A Ge2A Ge5A 90.33(8) . .
Ge3A Ge2A Ge5A 90.31(7) . .
Ge1A Ge2A Ge2B 123.15(7) . .
Ge9A Ge2A Ge2B 95.78(7) . .
Ge6B Ge2A Ge2B 44.85(5) . .
Ge6A Ge2A Ge2B 46.75(5) . .
Ge3A Ge2A Ge2B 65.49(5) . .
Ge5A Ge2A Ge2B 136.64(7) . .
Ge1A Ge2A Ge4A 41.41(6) . .
Ge9A Ge2A Ge4A 80.69(6) . .
Ge6B Ge2A Ge4A 137.62(7) . .
Ge6A Ge2A Ge4A 70.44(6) . .
Ge3A Ge2A Ge4A 46.09(5) . .
Ge5A Ge2A Ge4A 44.22(5) . .
Ge2B Ge2A Ge4A 103.73(5) . .
Ge1A Ge2A Ge8A 78.20(7) . .
Ge9A Ge2A Ge8A 41.60(5) . .
Ge6B Ge2A Ge8A 141.15(7) . .
Ge6A Ge2A Ge8A 50.18(6) . .
Ge3A Ge2A Ge8A 71.64(6) . .
Ge5A Ge2A Ge8A 40.15(5) . .
Ge2B Ge2A Ge8A 96.69(5) . .
Ge4A Ge2A Ge8A 39.89(4) . .
Ge1A Ge2A C102 87.3(2) . .
Ge9A Ge2A C102 77.1(3) . .
Ge6B Ge2A C102 113.8(2) . .
Ge6A Ge2A C102 136.2(3) . .
Ge3A Ge2A C102 146.0(2) . .
Ge5A Ge2A C102 64.3(2) . .
Ge2B Ge2A C102 148.4(2) . .
Ge4A Ge2A C102 105.3(2) . .
Ge8A Ge2A C102 97.6(3) . .
Ge1A Ge3A Ge7A 110.64(9) . .
Ge1A Ge3A Ge6A 104.98(8) . .
Ge7A Ge3A Ge6A 56.60(6) . .
Ge1A Ge3A Ge2A 56.27(6) . .
Ge7A Ge3A Ge2A 103.78(8) . .
Ge6A Ge3A Ge2A 58.32(6) . .
Ge1A Ge3A Ge4A 57.06(7) . .
Ge7A Ge3A Ge4A 56.99(7) . .
Ge6A Ge3A Ge4A 89.81(7) . .
Ge2A Ge3A Ge4A 88.62(7) . .
Ge1A Ge3A Ge2B 124.53(7) . .
Ge7A Ge3A Ge2B 92.70(6) . .
Ge6A Ge3A Ge2B 48.21(5) . .
Ge2A Ge3A Ge2B 69.79(5) . .
Ge4A Ge3A Ge2B 138.02(7) . .
Ge1A Ge3A Ge6B 87.29(6) . .
Ge7A Ge3A Ge6B 124.02(7) . .
Ge6A Ge3A Ge6B 67.70(6) . .
Ge2A Ge3A Ge6B 43.29(5) . .
Ge4A Ge3A Ge6B 131.90(7) . .
Ge2B Ge3A Ge6B 40.46(4) . .
Ge1A Ge3A Rb3 171.29(7) . .
Ge7A Ge3A Rb3 69.81(6) . .
Ge6A Ge3A Rb3 82.66(6) . .
Ge2A Ge3A Rb3 132.41(6) . .
Ge4A Ge3A Rb3 119.74(7) . .
Ge2B Ge3A Rb3 63.71(4) . .
Ge6B Ge3A Rb3 99.67(5) . .
Ge1A Ge3A C104 82.5(2) . 1_655
Ge7A Ge3A C104 88.6(3) . 1_655
Ge6A Ge3A C104 145.0(3) . 1_655
Ge2A Ge3A C104 138.7(2) . 1_655
Ge4A Ge3A C104 65.3(2) . 1_655
Ge2B Ge3A C104 149.9(2) . 1_655
Ge6B Ge3A C104 147.3(3) . 1_655
Rb3 Ge3A C104 88.8(2) . 1_655
Ge1A Ge3A Ge9B 113.73(7) . .
Ge7A Ge3A Ge9B 129.03(7) . .
Ge6A Ge3A Ge9B 88.27(6) . .
Ge2A Ge3A Ge9B 81.71(6) . .
Ge4A Ge3A Ge9B 169.63(7) . .
Ge2B Ge3A Ge9B 40.89(4) . .
Ge6B Ge3A Ge9B 38.49(4) . .
Rb3 Ge3A Ge9B 70.10(4) . .
C104 Ge3A Ge9B 120.5(3) 1_655 .
Ge7A Ge4A Ge1A 112.81(8) . .
Ge7A Ge4A Ge8A 60.52(7) . .
Ge1A Ge4A Ge8A 107.54(8) . .
Ge7A Ge4A Ge5A 106.82(7) . .
Ge1A Ge4A Ge5A 60.03(7) . .
Ge8A Ge4A Ge5A 56.72(7) . .
Ge7A Ge4A Ge3A 58.24(7) . .
Ge1A Ge4A Ge3A 58.12(7) . .
Ge8A Ge4A Ge3A 95.63(7) . .
Ge5A Ge4A Ge3A 94.57(7) . .
Ge7A Ge4A C104 93.2(2) . 1_655
Ge1A Ge4A C104 86.7(3) . 1_655
Ge8A Ge4A C104 153.2(2) . 1_655
Ge5A Ge4A C104 145.6(3) . 1_655
Ge3A Ge4A C104 72.3(3) . 1_655
Ge7A Ge4A C409 146.1(4) . 2
Ge1A Ge4A C409 97.0(4) . 2
Ge8A Ge4A C409 96.2(3) . 2
Ge5A Ge4A C409 73.8(3) . 2
Ge3A Ge4A C409 154.8(4) . 2
C104 Ge4A C409 104.7(4) 1_655 2
Ge7A Ge4A NC4 73.62(15) . 1_655
Ge1A Ge4A NC4 164.18(15) . 1_655
Ge8A Ge4A NC4 88.24(15) . 1_655
Ge5A Ge4A NC4 133.54(15) . 1_655
Ge3A Ge4A NC4 120.62(15) . 1_655
C104 Ge4A NC4 78.4(3) 1_655 1_655
C409 Ge4A NC4 81.9(4) 2 1_655
Ge7A Ge4A Ge2A 79.10(6) . .
Ge1A Ge4A Ge2A 40.41(5) . .
Ge8A Ge4A Ge2A 71.83(6) . .
Ge5A Ge4A Ge2A 49.27(5) . .
Ge3A Ge4A Ge2A 45.30(5) . .
C104 Ge4A Ge2A 110.7(3) 1_655 .
C409 Ge4A Ge2A 119.1(3) 2 .
NC4 Ge4A Ge2A 151.76(15) 1_655 .
Ge7A Ge4A Ge6A 40.06(5) . .
Ge1A Ge4A Ge6A 78.93(6) . .
Ge8A Ge4A Ge6A 51.13(5) . .
Ge5A Ge4A Ge6A 71.63(5) . .
Ge3A Ge4A Ge6A 44.51(5) . .
C104 Ge4A Ge6A 112.7(3) 1_655 .
C409 Ge4A Ge6A 142.0(3) 2 .
NC4 Ge4A Ge6A 111.55(15) 1_655 .
Ge2A Ge4A Ge6A 40.24(4) . .
Ge8A Ge5A Ge9A 61.58(7) . .
Ge8A Ge5A Ge1A 109.22(8) . .
Ge9A Ge5A Ge1A 106.24(8) . .
Ge8A Ge5A Ge4A 60.99(7) . .
Ge9A Ge5A Ge4A 106.17(8) . .
Ge1A Ge5A Ge4A 57.77(7) . .
Ge8A Ge5A Ge2A 91.96(7) . .
Ge9A Ge5A Ge2A 53.96(6) . .
Ge1A Ge5A Ge2A 53.65(6) . .
Ge4A Ge5A Ge2A 86.51(7) . .
Ge8A Ge5A NC3 83.40(15) . 2
Ge9A Ge5A NC3 88.83(15) . 2
Ge1A Ge5A NC3 163.61(15) . 2
Ge4A Ge5A NC3 124.91(15) . 2
Ge2A Ge5A NC3 138.66(15) . 2
Ge8A Ge5A C102 140.5(2) . .
Ge9A Ge5A C102 80.5(2) . .
Ge1A Ge5A C102 90.6(3) . .
Ge4A Ge5A C102 148.4(3) . .
Ge2A Ge5A C102 72.4(3) . .
NC3 Ge5A C102 85.5(3) 2 .
Ge8A Ge5A Ge6A 49.82(6) . .
Ge9A Ge5A Ge6A 39.61(5) . .
Ge1A Ge5A Ge6A 76.67(6) . .
Ge4A Ge5A Ge6A 68.25(5) . .
Ge2A Ge5A Ge6A 42.14(5) . .
NC3 Ge5A Ge6A 119.71(15) 2 .
C102 Ge5A Ge6A 106.6(2) . .
Ge8A Ge5A Ge3A 71.80(6) . .
Ge9A Ge5A Ge3A 77.31(6) . .
Ge1A Ge5A Ge3A 39.66(5) . .
Ge4A Ge5A Ge3A 43.53(5) . .
Ge2A Ge5A Ge3A 42.98(5) . .
NC3 Ge5A Ge3A 155.07(15) 2 .
C102 Ge5A Ge3A 112.0(3) . .
Ge6A Ge5A Ge3A 39.84(4) . .
Ge8A Ge5A C409 93.7(3) . 2
Ge9A Ge5A C409 153.0(3) . 2
Ge1A Ge5A C409 91.7(3) . 2
Ge4A Ge5A C409 66.2(3) . 2
Ge2A Ge5A C409 144.6(3) . 2
NC3 Ge5A C409 76.7(3) 2 2
C102 Ge5A C409 120.3(4) . 2
Ge6A Ge5A C409 131.9(3) . 2
Ge3A Ge5A C409 106.8(3) . 2
Ge7A Ge6A Ge9A 110.46(8) . .
Ge7A Ge6A Ge2A 108.39(8) . .
Ge9A Ge6A Ge2A 57.99(7) . .
Ge7A Ge6A Ge2B 119.94(9) . .
Ge9A Ge6A Ge2B 125.59(9) . .
Ge2A Ge6A Ge2B 86.62(8) . .
Ge7A Ge6A Ge3A 59.49(7) . .
Ge9A Ge6A Ge3A 108.58(8) . .
Ge2A Ge6A Ge3A 61.19(6) . .
Ge2B Ge6A Ge3A 82.24(7) . .
Ge7A Ge6A Ge8A 55.80(6) . .
Ge9A Ge6A Ge8A 55.78(6) . .
Ge2A Ge6A Ge8A 87.41(7) . .
Ge2B Ge6A Ge8A 170.82(8) . .
Ge3A Ge6A Ge8A 88.78(6) . .
Ge7A Ge6A Ge6B 129.82(8) . .
Ge9A Ge6A Ge6B 89.31(7) . .
Ge2A Ge6A Ge6B 44.38(5) . .
Ge2B Ge6A Ge6B 42.85(5) . .
Ge3A Ge6A Ge6B 70.64(6) . .
Ge8A Ge6A Ge6B 131.77(7) . .
Ge7A Ge6A Ge4A 40.92(5) . .
Ge9A Ge6A Ge4A 79.79(6) . .
Ge2A Ge6A Ge4A 69.31(5) . .
Ge2B Ge6A Ge4A 127.90(7) . .
Ge3A Ge6A Ge4A 45.68(5) . .
Ge8A Ge6A Ge4A 43.11(5) . .
Ge6B Ge6A Ge4A 104.86(5) . .
Ge7A Ge6A Rb4 89.09(7) . .
Ge9A Ge6A Rb4 68.00(6) . .
Ge2A Ge6A Rb4 125.99(7) . .
Ge2B Ge6A Rb4 128.54(7) . .
Ge3A Ge6A Rb4 145.91(7) . .
Ge8A Ge6A Rb4 60.61(5) . .
Ge6B Ge6A Rb4 140.59(5) . .
Ge4A Ge6A Rb4 102.28(5) . .
Ge7A Ge6A C402 95.2(3) . .
Ge9A Ge6A C402 116.9(3) . .
Ge2A Ge6A C402 156.2(3) . .
Ge2B Ge6A C402 78.8(3) . .
Ge3A Ge6A C402 133.6(3) . .
Ge8A Ge6A C402 109.0(3) . .
Ge6B Ge6A C402 116.8(3) . .
Ge4A Ge6A C402 134.3(3) . .
Rb4 Ge6A C402 55.5(3) . .
Ge6A Ge7A Ge4A 99.03(8) . .
Ge6A Ge7A Ge3A 63.92(7) . .
Ge4A Ge7A Ge3A 64.77(7) . .
Ge6A Ge7A Ge8A 71.76(7) . .
Ge4A Ge7A Ge8A 61.35(7) . .
Ge3A Ge7A Ge8A 100.29(8) . .
Ge6A Ge7A Rb3 85.69(7) . .
Ge4A Ge7A Rb3 127.27(8) . .
Ge3A Ge7A Rb3 71.08(6) . .
Ge8A Ge7A Rb3 157.28(7) . .
Ge6A Ge7A NC4 157.44(15) . 1_655
Ge4A Ge7A NC4 67.96(14) . 1_655
Ge3A Ge7A NC4 121.06(15) . 1_655
Ge8A Ge7A NC4 85.71(14) . 1_655
Rb3 Ge7A NC4 116.87(14) . 1_655
Ge6A Ge7A Ge9A 35.04(5) . .
Ge4A Ge7A Ge9A 73.77(6) . .
Ge3A Ge7A Ge9A 74.35(6) . .
Ge8A Ge7A Ge9A 37.79(5) . .
Rb3 Ge7A Ge9A 120.27(6) . .
NC4 Ge7A Ge9A 122.56(14) 1_655 .
Ge6A Ge7A Ge2A 36.85(5) . .
Ge4A Ge7A Ge2A 64.00(6) . .
Ge3A Ge7A Ge2A 39.20(5) . .
Ge8A Ge7A Ge2A 65.67(6) . .
Rb3 Ge7A Ge2A 97.88(6) . .
NC4 Ge7A Ge2A 131.42(14) 1_655 .
Ge9A Ge7A Ge2A 35.14(4) . .
Ge6A Ge7A Ge5A 66.43(6) . .
Ge4A Ge7A Ge5A 37.55(5) . .
Ge3A Ge7A Ge5A 67.22(6) . .
Ge8A Ge7A Ge5A 34.54(6) . .
Rb3 Ge7A Ge5A 136.80(7) . .
NC4 Ge7A Ge5A 94.36(14) 1_655 .
Ge9A Ge7A Ge5A 36.43(3) . .
Ge2A Ge7A Ge5A 40.56(4) . .
Ge6A Ge7A C401 81.1(3) . .
Ge4A Ge7A C401 155.4(3) . .
Ge3A Ge7A C401 133.8(3) . .
Ge8A Ge7A C401 96.0(3) . .
Rb3 Ge7A C401 77.4(3) . .
NC4 Ge7A C401 103.0(3) 1_655 .
Ge9A Ge7A C401 94.4(2) . .
Ge2A Ge7A C401 117.7(3) . .
Ge5A Ge7A C401 126.1(2) . .
Ge5A Ge8A Ge7A 109.41(9) . .
Ge5A Ge8A Ge9A 60.83(7) . .
Ge7A Ge8A Ge9A 104.60(8) . .
Ge5A Ge8A Ge4A 62.29(7) . .
Ge7A Ge8A Ge4A 58.13(6) . .
Ge9A Ge8A Ge4A 106.57(9) . .
Ge5A Ge8A Ge6A 90.30(8) . .
Ge7A Ge8A Ge6A 52.44(6) . .
Ge9A Ge8A Ge6A 53.16(6) . .
Ge4A Ge8A Ge6A 85.76(7) . .
Ge5A Ge8A Rb4 131.68(8) . .
Ge7A Ge8A Rb4 94.59(7) . .
Ge9A Ge8A Rb4 73.00(6) . .
Ge4A Ge8A Rb4 152.19(8) . .
Ge6A Ge8A Rb4 71.68(6) . .
Ge5A Ge8A NC3 126.75(16) . .
Ge7A Ge8A NC3 89.77(15) . .
Ge9A Ge8A NC3 160.71(16) . .
Ge4A Ge8A NC3 91.88(15) . .
Ge6A Ge8A NC3 136.21(16) . .
Rb4 Ge8A NC3 93.38(15) . .
Ge5A Ge8A Ge2A 47.89(6) . .
Ge7A Ge8A Ge2A 76.74(7) . .
Ge9A Ge8A Ge2A 39.43(5) . .
Ge4A Ge8A Ge2A 68.28(6) . .
Ge6A Ge8A Ge2A 42.41(5) . .
Rb4 Ge8A Ge2A 102.51(5) . .
NC3 Ge8A Ge2A 159.80(15) . .
Ge5A Ge8A Ge3A 71.36(6) . .
Ge7A Ge8A Ge3A 39.59(6) . .
Ge9A Ge8A Ge3A 76.93(6) . .
Ge4A Ge8A Ge3A 43.30(5) . .
Ge6A Ge8A Ge3A 42.47(5) . .
Rb4 Ge8A Ge3A 112.66(6) . .
NC3 Ge8A Ge3A 121.69(14) . .
Ge2A Ge8A Ge3A 40.19(4) . .
Ge5A Ge8A Ge1A 36.13(5) . .
Ge7A Ge8A Ge1A 73.31(7) . .
Ge9A Ge8A Ge1A 71.49(6) . .
Ge4A Ge8A Ge1A 35.55(5) . .
Ge6A Ge8A Ge1A 69.03(6) . .
Rb4 Ge8A Ge1A 137.78(6) . .
NC3 Ge8A Ge1A 125.96(14) . .
Ge2A Ge8A Ge1A 35.80(3) . .
Ge3A Ge8A Ge1A 36.71(4) . .
Ge2A Ge9A Ge6A 62.92(7) . .
Ge2A Ge9A Ge5A 68.98(7) . .
Ge6A Ge9A Ge5A 99.55(7) . .
Ge2A Ge9A Ge8A 98.96(8) . .
Ge6A Ge9A Ge8A 71.05(7) . .
Ge5A Ge9A Ge8A 57.58(7) . .
Ge2A Ge9A Rb4 135.85(8) . .
Ge6A Ge9A Rb4 72.93(7) . .
Ge5A Ge9A Rb4 120.70(8) . .
Ge8A Ge9A Rb4 64.81(6) . .
Ge2A Ge9A O13 89.65(19) . .
Ge6A Ge9A O13 142.45(19) . .
Ge5A Ge9A O13 93.00(15) . .
Ge8A Ge9A O13 142.56(16) . .
Rb4 Ge9A O13 128.97(18) . .
Ge2A Ge9A CN3 140.64(14) . 2
Ge6A Ge9A CN3 140.39(15) . 2
Ge5A Ge9A CN3 74.84(14) . 2
Ge8A Ge9A CN3 73.30(13) . 2
Rb4 Ge9A CN3 76.73(14) . 2
O13 Ge9A CN3 77.1(2) . 2
Ge2A Ge9A C111 108.3(3) . .
Ge6A Ge9A C111 149.6(2) . .
Ge5A Ge9A C111 104.0(2) . .
Ge8A Ge9A C111 138.6(3) . .
Rb4 Ge9A C111 109.8(3) . .
O13 Ge9A C111 19.3(3) . .
CN3 Ge9A C111 65.8(3) 2 .
Ge2A Ge9A C105 87.2(2) . .
Ge6A Ge9A C105 149.4(2) . .
Ge5A Ge9A C105 73.7(2) . .
Ge8A Ge9A C105 123.7(2) . .
Rb4 Ge9A C105 136.6(2) . .
O13 Ge9A C105 19.9(2) . .
CN3 Ge9A C105 67.9(3) 2 .
C111 Ge9A C105 32.3(3) . .
Ge2A Ge9A Ge7A 72.99(6) . .
Ge6A Ge9A Ge7A 34.50(5) . .
Ge5A Ge9A Ge7A 72.73(6) . .
Ge8A Ge9A Ge7A 37.61(5) . .
Rb4 Ge9A Ge7A 70.52(5) . .
O13 Ge9A Ge7A 160.48(18) . .
CN3 Ge9A Ge7A 110.66(13) 2 .
C111 Ge9A Ge7A 175.9(2) . .
C105 Ge9A Ge7A 145.4(2) . .
Ge5B Ge1B Ge3B 99.24(7) . .
Ge5B Ge1B Ge2B 71.93(6) . .
Ge3B Ge1B Ge2B 63.14(6) . .
Ge5B Ge1B Ge4B 63.37(7) . .
Ge3B Ge1B Ge4B 63.97(7) . .
Ge2B Ge1B Ge4B 100.57(7) . .
Ge5B Ge1B Rb2 84.89(6) . 2_566
Ge3B Ge1B Rb2 132.01(7) . 2_566
Ge2B Ge1B Rb2 155.01(8) . 2_566
Ge4B Ge1B Rb2 76.24(6) . 2_566
Ge5B Ge1B C404 148.5(3) . .
Ge3B Ge1B C404 89.9(2) . .
Ge2B Ge1B C404 85.9(3) . .
Ge4B Ge1B C404 145.1(3) . .
Rb2 Ge1B C404 111.1(2) 2_566 .
Ge5B Ge1B Ge9B 35.48(5) . .
Ge3B Ge1B Ge9B 74.24(5) . .
Ge2B Ge1B Ge9B 37.66(5) . .
Ge4B Ge1B Ge9B 74.05(5) . .
Rb2 Ge1B Ge9B 120.32(6) 2_566 .
C404 Ge1B Ge9B 122.8(3) . .
Ge5B Ge1B C204 140.9(2) . 2_566
Ge3B Ge1B C204 112.3(2) . 2_566
Ge2B Ge1B C204 143.0(3) . 2_566
Ge4B Ge1B C204 110.0(3) . 2_566
Rb2 Ge1B C204 56.9(2) 2_566 2_566
C404 Ge1B C204 57.0(3) . 2_566
Ge9B Ge1B C204 173.2(2) . 2_566
Ge5B Ge1B C211 119.9(2) . 2_566
Ge3B Ge1B C211 140.8(2) . 2_566
Ge2B Ge1B C211 128.3(2) . 2_566
Ge4B Ge1B C211 130.5(2) . 2_566
Rb2 Ge1B C211 56.4(2) 2_566 2_566
C404 Ge1B C211 58.1(3) . 2_566
Ge9B Ge1B C211 140.5(2) . 2_566
C204 Ge1B C211 32.8(3) 2_566 2_566
Ge5B Ge1B Ge6B 66.00(5) . .
Ge3B Ge1B Ge6B 38.60(4) . .
Ge2B Ge1B Ge6B 35.49(5) . .
Ge4B Ge1B Ge6B 66.56(5) . .
Rb2 Ge1B Ge6B 140.01(6) 2_566 .
C404 Ge1B Ge6B 107.8(2) . .
Ge9B Ge1B Ge6B 35.85(3) . .
C204 Ge1B Ge6B 150.5(2) 2_566 .
C211 Ge1B Ge6B 162.9(2) 2_566 .
Ge6B Ge2B Ge1B 108.62(8) . .
Ge6B Ge2B Ge9B 59.16(6) . .
Ge1B Ge2B Ge9B 105.52(8) . .
Ge6B Ge2B Ge6A 92.45(7) . .
Ge1B Ge2B Ge6A 127.56(9) . .
Ge9B Ge2B Ge6A 126.18(8) . .
Ge6B Ge2B Ge3B 61.53(6) . .
Ge1B Ge2B Ge3B 58.35(6) . .
Ge9B Ge2B Ge3B 105.67(8) . .
Ge6A Ge2B Ge3B 96.02(7) . .
Ge6B Ge2B Ge5B 88.75(7) . .
Ge1B Ge2B Ge5B 53.34(6) . .
Ge9B Ge2B Ge5B 53.33(6) . .
Ge6A Ge2B Ge5B 178.03(8) . .
Ge3B Ge2B Ge5B 85.92(6) . .
Ge6B Ge2B Ge3A 76.44(6) . .
Ge1B Ge2B Ge3A 174.73(8) . .
Ge9B Ge2B Ge3A 78.20(6) . .
Ge6A Ge2B Ge3A 49.55(5) . .
Ge3B Ge2B Ge3A 124.68(7) . .
Ge5B Ge2B Ge3A 129.38(7) . .
Ge6B Ge2B Ge2A 46.45(5) . .
Ge1B Ge2B Ge2A 138.02(7) . .
Ge9B Ge2B Ge2A 89.19(6) . .
Ge6A Ge2B Ge2A 46.63(5) . .
Ge3B Ge2B Ge2A 79.96(5) . .
Ge5B Ge2B Ge2A 134.31(7) . .
Ge3A Ge2B Ge2A 44.72(4) . .
Ge6B Ge2B Rb3 129.98(6) . .
Ge1B Ge2B Rb3 113.55(6) . .
Ge9B Ge2B Rb3 84.15(6) . .
Ge6A Ge2B Rb3 82.64(6) . .
Ge3B Ge2B Rb3 168.38(7) . .
Ge5B Ge2B Rb3 95.39(6) . .
Ge3A Ge2B Rb3 62.72(4) . .
Ge2A Ge2B Rb3 106.82(5) . .
Ge6B Ge2B Ge4B 70.37(5) . .
Ge1B Ge2B Ge4B 39.77(5) . .
Ge9B Ge2B Ge4B 76.96(6) . .
Ge6A Ge2B Ge4B 139.36(7) . .
Ge3B Ge2B Ge4B 43.34(5) . .
Ge5B Ge2B Ge4B 42.58(4) . .
Ge3A Ge2B Ge4B 145.50(6) . .
Ge2A Ge2B Ge4B 111.36(5) . .
Rb3 Ge2B Ge4B 136.76(5) . .
Ge1B Ge3B Ge7B 111.42(8) . .
Ge1B Ge3B Ge6B 104.72(7) . .
Ge7B Ge3B Ge6B 59.08(6) . .
Ge1B Ge3B Ge2B 58.52(6) . .
Ge7B Ge3B Ge2B 106.04(7) . .
Ge6B Ge3B Ge2B 56.59(6) . .
Ge1B Ge3B Ge4B 58.20(6) . .
Ge7B Ge3B Ge4B 57.33(6) . .
Ge6B Ge3B Ge4B 93.06(7) . .
Ge2B Ge3B Ge4B 94.01(7) . .
Ge1B Ge3B Ge5B 39.99(5) . .
Ge7B Ge3B Ge5B 76.83(6) . .
Ge6B Ge3B Ge5B 69.96(5) . .
Ge2B Ge3B Ge5B 50.33(5) . .
Ge4B Ge3B Ge5B 43.69(5) . .
Ge1B Ge3B Ge8B 77.61(6) . .
Ge7B Ge3B Ge8B 39.25(5) . .
Ge6B Ge3B Ge8B 49.50(5) . .
Ge2B Ge3B Ge8B 71.62(6) . .
Ge4B Ge3B Ge8B 43.57(5) . .
Ge5B Ge3B Ge8B 38.82(4) . .
Ge1B Ge3B Ge6A 88.75(6) . .
Ge7B Ge3B Ge6A 123.88(6) . .
Ge6B Ge3B Ge6A 65.33(5) . .
Ge2B Ge3B Ge6A 41.44(5) . .
Ge4B Ge3B Ge6A 135.45(7) . .
Ge5B Ge3B Ge6A 91.76(5) . .
Ge8B Ge3B Ge6A 105.23(5) . .
Ge1B Ge3B Rb1 169.95(8) . .
Ge7B Ge3B Rb1 58.73(5) . .
Ge6B Ge3B Rb1 69.11(5) . .
Ge2B Ge3B Rb1 120.09(6) . .
Ge4B Ge3B Rb1 113.27(7) . .
Ge5B Ge3B Rb1 130.51(5) . .
Ge8B Ge3B Rb1 92.47(5) . .
Ge6A Ge3B Rb1 95.47(5) . .
Ge1B Ge3B Ge2A 118.21(6) . .
Ge7B Ge3B Ge2A 89.24(6) . .
Ge6B Ge3B Ge2A 38.59(5) . .
Ge2B Ge3B Ge2A 59.89(5) . .
Ge4B Ge3B Ge2A 131.46(7) . .
Ge5B Ge3B Ge2A 99.30(4) . .
Ge8B Ge3B Ge2A 88.02(4) . .
Ge6A Ge3B Ge2A 37.98(4) . .
Rb1 Ge3B Ge2A 62.27(4) . .
Ge7B Ge4B Ge1B 112.33(8) . .
Ge7B Ge4B Ge5B 104.74(6) . .
Ge1B Ge4B Ge5B 57.39(6) . .
Ge7B Ge4B Ge8B 57.12(6) . .
Ge1B Ge4B Ge8B 105.25(7) . .
Ge5B Ge4B Ge8B 57.54(5) . .
Ge7B Ge4B Ge3B 58.69(6) . .
Ge1B Ge4B Ge3B 57.83(6) . .
Ge5B Ge4B Ge3B 91.73(7) . .
Ge8B Ge4B Ge3B 92.32(6) . .
Ge7B Ge4B Ge8B 121.97(7) . 2_566
Ge1B Ge4B Ge8B 88.28(6) . 2_566
Ge5B Ge4B Ge8B 42.08(5) . 2_566
Ge8B Ge4B Ge8B 65.34(5) . 2_566
Ge3B Ge4B Ge8B 133.81(6) . 2_566
Ge7B Ge4B Ge5B 87.73(6) . 2_566
Ge1B Ge4B Ge5B 122.53(6) . 2_566
Ge5B Ge4B Ge5B 65.64(6) . 2_566
Ge8B Ge4B Ge5B 41.72(5) . 2_566
Ge3B Ge4B Ge5B 134.05(6) . 2_566
Ge8B Ge4B Ge5B 40.02(4) 2_566 2_566
Ge7B Ge4B C312 82.4(2) . 1_455
Ge1B Ge4B C312 104.0(3) . 1_455
Ge5B Ge4B C312 161.3(3) . 1_455
Ge8B Ge4B C312 136.7(3) . 1_455
Ge3B Ge4B C312 77.1(3) . 1_455
Ge8B Ge4B C312 146.5(3) 2_566 1_455
Ge5B Ge4B C312 132.6(3) 2_566 1_455
Ge7B Ge4B Rb2 174.22(8) . 2_566
Ge1B Ge4B Rb2 63.90(5) . 2_566
Ge5B Ge4B Rb2 77.19(5) . 2_566
Ge8B Ge4B Rb2 127.39(6) . 2_566
Ge3B Ge4B Rb2 116.08(7) . 2_566
Ge8B Ge4B Rb2 63.12(4) 2_566 2_566
Ge5B Ge4B Rb2 98.01(5) 2_566 2_566
C312 Ge4B Rb2 94.2(2) 1_455 2_566
Ge7B Ge4B Ge6B 40.87(5) . .
Ge1B Ge4B Ge6B 76.38(5) . .
Ge5B Ge4B Ge6B 69.21(5) . .
Ge8B Ge4B Ge6B 49.31(5) . .
Ge3B Ge4B Ge6B 43.03(5) . .
Ge8B Ge4B Ge6B 103.42(5) 2_566 .
Ge5B Ge4B Ge6B 91.02(4) 2_566 .
C312 Ge4B Ge6B 109.7(2) 1_455 .
Rb2 Ge4B Ge6B 137.68(5) 2_566 .
Ge1B Ge5B Ge8B 125.89(7) . 2_566
Ge1B Ge5B Ge9B 109.29(8) . .
Ge8B Ge5B Ge9B 123.78(9) 2_566 .
Ge1B Ge5B Ge8B 110.10(7) . .
Ge8B Ge5B Ge8B 89.58(7) 2_566 .
Ge9B Ge5B Ge8B 59.75(6) . .
Ge1B Ge5B Ge4B 59.24(6) . .
Ge8B Ge5B Ge4B 92.66(7) 2_566 .
Ge9B Ge5B Ge4B 108.05(7) . .
Ge8B Ge5B Ge4B 61.57(6) . .
Ge1B Ge5B Ge2B 54.73(6) . .
Ge8B Ge5B Ge2B 179.01(8) 2_566 .
Ge9B Ge5B Ge2B 55.79(6) . .
Ge8B Ge5B Ge2B 90.87(7) . .
Ge4B Ge5B Ge2B 88.34(6) . .
Ge1B Ge5B Ge5B 130.77(8) . 2_566
Ge8B Ge5B Ge5B 45.45(5) 2_566 2_566
Ge9B Ge5B Ge5B 91.61(7) . 2_566
Ge8B Ge5B Ge5B 44.13(5) . 2_566
Ge4B Ge5B Ge5B 72.12(6) . 2_566
Ge2B Ge5B Ge5B 134.99(8) . 2_566
Ge1B Ge5B Ge4B 170.52(7) . 2_566
Ge8B Ge5B Ge4B 45.23(5) 2_566 2_566
Ge9B Ge5B Ge4B 78.93(6) . 2_566
Ge8B Ge5B Ge4B 69.46(6) . 2_566
Ge4B Ge5B Ge4B 114.36(6) . 2_566
Ge2B Ge5B Ge4B 134.21(6) . 2_566
Ge5B Ge5B Ge4B 42.24(4) 2_566 2_566
Ge1B Ge5B O32 107.70(19) . .
Ge8B Ge5B O32 96.39(19) 2_566 .
Ge9B Ge5B O32 74.49(16) . .
Ge8B Ge5B O32 127.71(17) . .
Ge4B Ge5B O32 166.93(19) . .
Ge2B Ge5B O32 82.63(18) . .
Ge5B Ge5B O32 120.90(19) 2_566 .
Ge4B Ge5B O32 78.67(18) 2_566 .
Ge1B Ge5B C307 102.1(3) . .
Ge8B Ge5B C307 83.3(3) 2_566 .
Ge9B Ge5B C307 95.9(2) . .
Ge8B Ge5B C307 144.4(3) . .
Ge4B Ge5B C307 153.2(3) . .
Ge2B Ge5B C307 95.8(3) . .
Ge5B Ge5B C307 119.9(3) 2_566 .
Ge4B Ge5B C307 81.2(3) 2_566 .
O32 Ge5B C307 21.5(3) . .
Ge2B Ge6B Ge9B 61.88(7) . .
Ge2B Ge6B Ge7B 110.12(7) . .
Ge9B Ge6B Ge7B 106.37(8) . .
Ge2B Ge6B Ge2A 88.69(8) . .
Ge9B Ge6B Ge2A 118.01(8) . .
Ge7B Ge6B Ge2A 135.46(8) . .
Ge2B Ge6B Ge3B 61.88(6) . .
Ge9B Ge6B Ge3B 107.96(7) . .
Ge7B Ge6B Ge3B 58.73(6) . .
Ge2A Ge6B Ge3B 101.69(8) . .
Ge2B Ge6B Ge8B 92.09(7) . .
Ge9B Ge6B Ge8B 54.41(6) . .
Ge7B Ge6B Ge8B 53.04(6) . .
Ge2A Ge6B Ge8B 170.16(8) . .
Ge3B Ge6B Ge8B 87.30(6) . .
Ge2B Ge6B C202 150.6(3) . .
Ge9B Ge6B C202 89.9(3) . .
Ge7B Ge6B C202 84.5(3) . .
Ge2A Ge6B C202 98.5(3) . .
Ge3B Ge6B C202 142.1(3) . .
Ge8B Ge6B C202 76.2(3) . .
Ge2B Ge6B Ge6A 44.70(5) . .
Ge9B Ge6B Ge6A 94.36(7) . .
Ge7B Ge6B Ge6A 132.12(7) . .
Ge2A Ge6B Ge6A 44.63(5) . .
Ge3B Ge6B Ge6A 74.02(6) . .
Ge8B Ge6B Ge6A 136.77(6) . .
C202 Ge6B Ge6A 139.2(3) . .
Ge2B Ge6B C205 131.9(3) . .
Ge9B Ge6B C205 79.6(3) . .
Ge7B Ge6B C205 107.5(3) . .
Ge2A Ge6B C205 84.9(2) . .
Ge3B Ge6B C205 165.3(3) . .
Ge8B Ge6B C205 87.3(2) . .
C202 Ge6B C205 23.3(4) . .
Ge6A Ge6B C205 118.6(3) . .
Ge2B Ge6B Ge3A 63.10(5) . .
Ge9B Ge6B Ge3A 72.99(6) . .
Ge7B Ge6B Ge3A 172.84(7) . .
Ge2A Ge6B Ge3A 45.17(5) . .
Ge3B Ge6B Ge3A 114.42(7) . .
Ge8B Ge6B Ge3A 127.27(6) . .
C202 Ge6B Ge3A 102.6(3) . .
Ge6A Ge6B Ge3A 41.66(4) . .
C205 Ge6B Ge3A 79.5(3) . .
Ge8B Ge7B Ge4B 64.36(6) . .
Ge8B Ge7B Ge3B 100.05(7) . .
Ge4B Ge7B Ge3B 63.97(7) . .
Ge8B Ge7B Ge6B 71.21(6) . .
Ge4B Ge7B Ge6B 99.16(7) . .
Ge3B Ge7B Ge6B 62.18(6) . .
Ge8B Ge7B Rb1 145.72(7) . .
Ge4B Ge7B Rb1 140.83(8) . .
Ge3B Ge7B Rb1 82.13(7) . .
Ge6B Ge7B Rb1 80.14(6) . .
Ge8B Ge7B C108 137.8(3) . .
Ge4B Ge7B C108 120.7(2) . .
Ge3B Ge7B C108 120.2(3) . .
Ge6B Ge7B C108 137.2(3) . .
Rb1 Ge7B C108 59.6(3) . .
Ge8B Ge7B Ge9B 35.91(5) . .
Ge4B Ge7B Ge9B 74.42(5) . .
Ge3B Ge7B Ge9B 74.22(5) . .
Ge6B Ge7B Ge9B 36.40(5) . .
Rb1 Ge7B Ge9B 116.21(5) . .
C108 Ge7B Ge9B 161.9(2) . .
Ge8B Ge7B Ge5B 36.28(5) . .
Ge4B Ge7B Ge5B 38.71(4) . .
Ge3B Ge7B Ge5B 65.68(5) . .
Ge6B Ge7B Ge5B 65.81(5) . .
Rb1 Ge7B Ge5B 140.93(6) . .
C108 Ge7B Ge5B 157.0(2) . .
Ge9B Ge7B Ge5B 35.80(3) . .
Ge8B Ge7B Ge2B 67.22(6) . .
Ge4B Ge7B Ge2B 66.38(5) . .
Ge3B Ge7B Ge2B 37.79(4) . .
Ge6B Ge7B Ge2B 34.52(4) . .
Rb1 Ge7B Ge2B 98.99(5) . .
C108 Ge7B Ge2B 154.9(3) . .
Ge9B Ge7B Ge2B 36.59(4) . .
Ge5B Ge7B Ge2B 41.94(4) . .
Ge8B Ge7B C307 75.0(2) . 2_566
Ge4B Ge7B C307 90.2(2) . 2_566
Ge3B Ge7B C307 152.4(2) . 2_566
Ge6B Ge7B C307 136.3(2) . 2_566
Rb1 Ge7B C307 117.5(2) . 2_566
C108 Ge7B C307 63.6(4) . 2_566
Ge9B Ge7B C307 109.5(2) . 2_566
Ge5B Ge7B C307 100.7(2) . 2_566
Ge2B Ge7B C307 141.3(2) . 2_566
Ge7B Ge8B Ge5B 125.78(8) . 2_566
Ge7B Ge8B Ge9B 108.88(8) . .
Ge5B Ge8B Ge9B 124.08(8) 2_566 .
Ge7B Ge8B Ge5B 108.65(8) . .
Ge5B Ge8B Ge5B 90.42(7) 2_566 .
Ge9B Ge8B Ge5B 59.20(6) . .
Ge7B Ge8B Ge4B 58.52(6) . .
Ge5B Ge8B Ge4B 93.05(7) 2_566 .
Ge9B Ge8B Ge4B 107.09(8) . .
Ge5B Ge8B Ge4B 60.89(6) . .
Ge7B Ge8B Ge6B 55.75(6) . .
Ge5B Ge8B Ge6B 178.30(8) 2_566 .
Ge9B Ge8B Ge6B 54.25(6) . .
Ge5B Ge8B Ge6B 88.29(7) . .
Ge4B Ge8B Ge6B 87.29(7) . .
Ge7B Ge8B Ge8B 129.77(8) . 2_566
Ge5B Ge8B Ge8B 45.88(5) 2_566 2_566
Ge9B Ge8B Ge8B 91.46(7) . 2_566
Ge5B Ge8B Ge8B 44.54(5) . 2_566
Ge4B Ge8B Ge8B 71.82(6) . 2_566
Ge6B Ge8B Ge8B 132.82(9) . 2_566
Ge7B Ge8B Ge4B 170.28(7) . 2_566
Ge5B Ge8B Ge4B 45.26(5) 2_566 2_566
Ge9B Ge8B Ge4B 79.28(6) . 2_566
Ge5B Ge8B Ge4B 70.51(6) . 2_566
Ge4B Ge8B Ge4B 114.66(5) . 2_566
Ge6B Ge8B Ge4B 133.15(6) . 2_566
Ge8B Ge8B Ge4B 42.84(4) 2_566 2_566
Ge7B Ge8B Ge3B 40.70(5) . .
Ge5B Ge8B Ge3B 137.15(6) 2_566 .
Ge9B Ge8B Ge3B 78.68(6) . .
Ge5B Ge8B Ge3B 69.92(6) . .
Ge4B Ge8B Ge3B 44.10(5) . .
Ge6B Ge8B Ge3B 43.20(4) . .
Ge8B Ge8B Ge3B 105.53(7) 2_566 .
Ge4B Ge8B Ge3B 140.36(6) 2_566 .
Ge7B Ge8B Ge2B 77.25(6) . .
Ge5B Ge8B Ge2B 139.06(7) 2_566 .
Ge9B Ge8B Ge2B 40.21(5) . .
Ge5B Ge8B Ge2B 48.65(5) . .
Ge4B Ge8B Ge2B 69.61(5) . .
Ge6B Ge8B Ge2B 39.64(4) . .
Ge8B Ge8B Ge2B 93.18(6) 2_566 .
Ge4B Ge8B Ge2B 107.61(5) 2_566 .
Ge3B Ge8B Ge2B 39.80(4) . .
Ge5B Ge9B Ge6B 99.51(7) . .
Ge5B Ge9B Ge8B 61.05(6) . .
Ge6B Ge9B Ge8B 71.34(6) . .
Ge5B Ge9B Ge2B 70.88(6) . .
Ge6B Ge9B Ge2B 58.96(6) . .
Ge8B Ge9B Ge2B 100.76(7) . .
Ge5B Ge9B O23 147.19(19) . .
Ge6B Ge9B O23 81.54(19) . .
Ge8B Ge9B O23 89.05(18) . .
Ge2B Ge9B O23 132.50(19) . .
Ge5B Ge9B C310 97.7(3) . .
Ge6B Ge9B C310 155.1(3) . .
Ge8B Ge9B C310 133.3(3) . .
Ge2B Ge9B C310 111.0(3) . .
O23 Ge9B C310 93.6(3) . .
Ge5B Ge9B C207 161.4(3) . .
Ge6B Ge9B C207 92.5(4) . .
Ge8B Ge9B C207 110.5(3) . .
Ge2B Ge9B C207 127.7(3) . .
O23 Ge9B C207 21.9(3) . .
C310 Ge9B C207 76.0(4) . .
Ge5B Ge9B C203 142.3(4) . .
Ge6B Ge9B C203 114.0(3) . .
Ge8B Ge9B C203 112.8(3) . .
Ge2B Ge9B C203 141.5(3) . .
O23 Ge9B C203 35.8(4) . .
C310 Ge9B C203 57.8(4) . .
C207 Ge9B C203 21.8(4) . .
Ge5B Ge9B Ge3A 129.52(8) . .
Ge6B Ge9B Ge3A 68.52(6) . .
Ge8B Ge9B Ge3A 139.69(7) . .
Ge2B Ge9B Ge3A 60.91(5) . .
O23 Ge9B Ge3A 81.70(17) . .
C310 Ge9B Ge3A 86.6(3) . .
C207 Ge9B Ge3A 68.2(3) . .
C203 Ge9B Ge3A 81.0(3) . .
Ge5B Ge9B C304 77.0(3) . .
Ge6B Ge9B C304 162.8(3) . .
Ge8B Ge9B C304 119.5(3) . .
Ge2B Ge9B C304 104.5(3) . .
O23 Ge9B C304 110.6(3) . .
C310 Ge9B C304 20.7(3) . .
C207 Ge9B C304 95.4(4) . .
C203 Ge9B C304 75.5(4) . .
Ge3A Ge9B C304 100.4(3) . .
O13 Rb1 O14 111.2(3) . .
O13 Rb1 O16 56.0(3) . .
O14 Rb1 O16 138.7(3) . .
O13 Rb1 O11 111.5(3) . .
O14 Rb1 O11 109.4(3) . .
O16 Rb1 O11 56.8(3) . .
O13 Rb1 O15 55.7(3) . .
O14 Rb1 O15 56.7(3) . .
O16 Rb1 O15 105.2(3) . .
O11 Rb1 O15 138.2(3) . .
O13 Rb1 O12 132.9(3) . .
O14 Rb1 O12 55.1(3) . .
O16 Rb1 O12 102.2(3) . .
O11 Rb1 O12 54.5(3) . .
O15 Rb1 O12 102.2(3) . .
O13 Rb1 Ge7B 147.0(3) . .
O14 Rb1 Ge7B 91.9(2) . .
O16 Rb1 Ge7B 119.7(2) . .
O11 Rb1 Ge7B 80.4(2) . .
O15 Rb1 Ge7B 133.9(2) . .
O12 Rb1 Ge7B 79.50(18) . .
O13 Rb1 C101 76.3(4) . .
O14 Rb1 C101 40.5(4) . .
O16 Rb1 C101 127.2(4) . .
O11 Rb1 C101 144.3(4) . .
O15 Rb1 C101 22.1(3) . .
O12 Rb1 C101 93.9(3) . .
Ge7B Rb1 C101 112.5(3) . .
O13 Rb1 C106 77.6(3) . .
O14 Rb1 C106 144.4(4) . .
O16 Rb1 C106 23.0(3) . .
O11 Rb1 C106 39.9(4) . .
O15 Rb1 C106 128.1(3) . .
O12 Rb1 C106 92.9(4) . .
Ge7B Rb1 C106 97.5(3) . .
C101 Rb1 C106 149.9(4) . .
O13 Rb1 Ge6B 112.8(2) . .
O14 Rb1 Ge6B 93.3(2) . .
O16 Rb1 Ge6B 128.0(3) . .
O11 Rb1 Ge6B 117.2(2) . .
O15 Rb1 Ge6B 103.52(19) . .
O12 Rb1 Ge6B 112.87(19) . .
Ge7B Rb1 Ge6B 39.90(4) . .
C101 Rb1 Ge6B 88.4(3) . .
C106 Rb1 Ge6B 115.6(3) . .
O13 Rb1 Ge3B 109.2(2) . .
O14 Rb1 Ge3B 126.9(2) . .
O16 Rb1 Ge3B 92.7(2) . .
O11 Rb1 Ge3B 85.5(2) . .
O15 Rb1 Ge3B 135.6(2) . .
O12 Rb1 Ge3B 113.36(18) . .
Ge7B Rb1 Ge3B 39.13(4) . .
C101 Rb1 Ge3B 126.1(3) . .
C106 Rb1 Ge3B 77.0(3) . .
Ge6B Rb1 Ge3B 38.84(3) . .
O13 Rb1 Ge2A 76.8(2) . .
O14 Rb1 Ge2A 98.66(19) . .
O16 Rb1 Ge2A 113.4(3) . .
O11 Rb1 Ge2A 144.1(2) . .
O15 Rb1 Ge2A 76.28(19) . .
O12 Rb1 Ge2A 143.68(19) . .
Ge7B Rb1 Ge2A 76.60(4) . .
C101 Rb1 Ge2A 71.0(3) . .
C106 Rb1 Ge2A 116.9(3) . .
Ge6B Rb1 Ge2A 36.98(4) . .
Ge3B Rb1 Ge2A 59.34(4) . .
C112 O11 C104 115.3(12) . .
C112 O11 Rb1 122.5(8) . .
C104 O11 Rb1 117.3(10) . .
C107 O12 C108 109.6(12) . .
C107 O12 Rb1 108.2(8) . .
C108 O12 Rb1 105.7(9) . .
C111 O13 C105 111.4(12) . .
C111 O13 Rb1 124.0(9) . .
C105 O13 Rb1 123.8(9) . .
C111 O13 Ge9A 94.6(10) . .
C105 O13 Ge9A 94.1(9) . .
Rb1 O13 Ge9A 90.4(3) . .
C103 O14 C109 110.5(12) . .
C103 O14 Rb1 122.2(7) . .
C109 O14 Rb1 119.0(10) . .
C101 O15 C102 112.5(12) . .
C101 O15 Rb1 101.9(8) . .
C102 O15 Rb1 103.7(8) . .
C110 O16 C106 113.0(14) . .
C110 O16 Rb1 103.2(9) . .
C106 O16 Rb1 103.9(9) . .
O15 C101 C109 110.6(13) . .
O15 C101 Rb1 55.9(6) . .
C109 C101 Rb1 88.3(8) . .
O15 C102 C105 108.3(12) . .
O15 C102 Ge5A 146.0(10) . .
C105 C102 Ge5A 95.8(10) . .
O15 C102 Ge2A 104.5(9) . .
C105 C102 Ge2A 109.3(10) . .
Ge5A C102 Ge2A 43.36(18) . .
O15 C102 Ge9A 126.3(9) . .
C105 C102 Ge9A 75.7(9) . .
Ge5A C102 Ge9A 37.31(15) . .
Ge2A C102 Ge9A 35.26(14) . .
O14 C103 C107 111.7(13) . .
O11 C104 C106 111.5(14) . .
O11 C104 Ge4A 149.7(10) . 1_455
C106 C104 Ge4A 91.2(10) . 1_455
O11 C104 Ge3A 125.0(10) . 1_455
C106 C104 Ge3A 122.6(11) . 1_455
Ge4A C104 Ge3A 42.47(17) 1_455 1_455
O13 C105 C102 108.3(13) . .
O13 C105 Ge9A 66.1(8) . .
C102 C105 Ge9A 83.9(9) . .
O13 C105 Ge5A 101.4(9) . .
C102 C105 Ge5A 63.7(9) . .
Ge9A C105 Ge5A 36.33(14) . .
C104 C106 O16 112.1(15) . .
C104 C106 Rb1 88.3(10) . .
O16 C106 Rb1 53.1(7) . .
C104 C106 Ge4A 68.3(9) . 1_455
O16 C106 Ge4A 103.6(9) . 1_455
Rb1 C106 Ge4A 138.7(5) . 1_455
O12 C107 C103 105.1(13) . .
O12 C108 C112 108.2(15) . .
O12 C108 Ge7B 89.5(8) . .
C112 C108 Ge7B 107.2(11) . .
O14 C109 C101 107.1(14) . .
O16 C110 C111 110.0(17) . .
O16 C110 Ge9A 127.7(10) . .
C111 C110 Ge9A 75.4(9) . .
O13 C111 C110 105.6(14) . .
O13 C111 Ge9A 66.0(9) . .
C110 C111 Ge9A 83.9(10) . .
O11 C112 C108 111.0(13) . .
O23 Rb2 O25 109.8(3) . .
O23 Rb2 O26 109.5(3) . .
O25 Rb2 O26 108.3(3) . .
O23 Rb2 O22 134.8(3) . .
O25 Rb2 O22 54.7(3) . .
O26 Rb2 O22 54.8(3) . .
O23 Rb2 O21 55.3(3) . .
O25 Rb2 O21 55.2(3) . .
O26 Rb2 O21 132.1(3) . .
O22 Rb2 O21 101.1(3) . .
O23 Rb2 O24 55.0(3) . .
O25 Rb2 O24 134.9(3) . .
O26 Rb2 O24 55.8(4) . .
O22 Rb2 O24 103.0(3) . .
O21 Rb2 O24 101.5(3) . .
O23 Rb2 C203 41.0(4) . .
O25 Rb2 C203 145.3(4) . .
O26 Rb2 C203 76.3(5) . .
O22 Rb2 C203 126.2(4) . .
O21 Rb2 C203 95.4(4) . .
O24 Rb2 C203 23.1(4) . .
O23 Rb2 C202 40.4(4) . .
O25 Rb2 C202 74.5(4) . .
O26 Rb2 C202 141.2(3) . .
O22 Rb2 C202 122.5(4) . .
O21 Rb2 C202 21.4(3) . .
O24 Rb2 C202 94.0(4) . .
C203 Rb2 C202 81.2(5) . .
O23 Rb2 Ge1B 147.3(2) . 2_566
O25 Rb2 Ge1B 89.12(19) . 2_566
O26 Rb2 Ge1B 88.2(2) . 2_566
O22 Rb2 Ge1B 77.86(18) . 2_566
O21 Rb2 Ge1B 130.4(2) . 2_566
O24 Rb2 Ge1B 127.4(2) . 2_566
C203 Rb2 Ge1B 125.6(3) . 2_566
C202 Rb2 Ge1B 130.5(2) . 2_566
O23 Rb2 C206 75.2(4) . .
O25 Rb2 C206 39.1(4) . .
O26 Rb2 C206 139.0(4) . .
O22 Rb2 C206 92.2(4) . .
O21 Rb2 C206 21.5(3) . .
O24 Rb2 C206 122.8(3) . .
C203 Rb2 C206 116.1(5) . .
C202 Rb2 C206 36.2(4) . .
Ge1B Rb2 C206 109.6(3) 2_566 .
O23 Rb2 C211 141.1(3) . .
O25 Rb2 C211 38.9(3) . .
O26 Rb2 C211 74.6(3) . .
O22 Rb2 C211 21.0(3) . .
O21 Rb2 C211 92.4(4) . .
O24 Rb2 C211 123.7(3) . .
C203 Rb2 C211 146.8(4) . .
C202 Rb2 C211 112.9(4) . .
Ge1B Rb2 C211 69.0(2) 2_566 .
C206 Rb2 C211 78.0(4) . .
O23 Rb2 C204 141.0(3) . .
O25 Rb2 C204 74.4(4) . .
O26 Rb2 C204 39.0(3) . .
O22 Rb2 C204 20.9(3) . .
O21 Rb2 C204 121.6(4) . .
O24 Rb2 C204 93.6(4) . .
C203 Rb2 C204 115.2(5) . .
C202 Rb2 C204 142.7(4) . .
Ge1B Rb2 C204 68.6(3) 2_566 .
C206 Rb2 C204 112.7(4) . .
C211 Rb2 C204 36.7(4) . .
C202 O21 C206 111.2(13) . .
C202 O21 Rb2 103.6(9) . .
C206 O21 Rb2 103.8(9) . .
C211 O22 C204 114.4(12) . .
C211 O22 Rb2 107.1(9) . .
C204 O22 Rb2 108.2(10) . .
C205 O23 C207 113.3(14) . .
C205 O23 Rb2 124.6(10) . .
C207 O23 Rb2 121.9(11) . .
C205 O23 Ge9B 104.0(9) . .
C207 O23 Ge9B 85.3(7) . .
Rb2 O23 Ge9B 85.6(2) . .
C205 O23 Ge6B 66.6(8) . .
C207 O23 Ge6B 103.4(9) . .
Rb2 O23 Ge6B 103.1(3) . .
Ge9B O23 Ge6B 37.61(10) . .
C203 O24 C209 112.6(15) . .
C203 O24 Rb2 97.9(10) . .
C209 O24 Rb2 104.3(10) . .
C208 O25 C201 112.3(13) . .
C208 O25 Rb2 120.1(10) . .
C201 O25 Rb2 120.8(9) . .
C210 O26 C212 110.3(12) . .
C210 O26 Rb2 120.8(9) . .
C212 O26 Rb2 122.0(11) . .
O25 C201 C211 111.1(14) . .
O25 C201 Ge1A 99.3(9) . 2_556
C211 C201 Ge1A 144.3(12) . 2_556
O21 C202 C205 110.4(14) . .
O21 C202 Rb2 55.0(8) . .
C205 C202 Rb2 84.3(9) . .
O21 C202 Ge6B 147.0(10) . .
C205 C202 Ge6B 81.6(9) . .
Rb2 C202 Ge6B 97.9(4) . .
O21 C202 Ge8B 103.1(9) . .
C205 C202 Ge8B 101.5(9) . .
Rb2 C202 Ge8B 61.7(2) . .
Ge6B C202 Ge8B 43.87(18) . .
O24 C203 C207 110.6(17) . .
O24 C203 Rb2 59.0(8) . .
C207 C203 Rb2 89.1(11) . .
O24 C203 Ge9B 131.5(11) . .
C207 C203 Ge9B 76.5(10) . .
Rb2 C203 Ge9B 73.7(3) . .
O22 C204 C210 107.2(14) . .
O22 C204 Rb2 51.0(8) . .
C210 C204 Rb2 84.6(11) . .
O22 C204 Ge1B 83.2(8) . 2_566
C210 C204 Ge1B 117.5(12) . 2_566
Rb2 C204 Ge1B 54.4(2) . 2_566
O23 C205 C202 109.3(13) . .
O23 C205 Ge6B 94.5(9) . .
C202 C205 Ge6B 75.1(8) . .
O23 C205 Ge9B 57.9(8) . .
C202 C205 Ge9B 92.1(8) . .
Ge6B C205 Ge9B 36.85(15) . .
O23 C205 Ge1A 111.9(11) . .
C202 C205 Ge1A 125.5(11) . .
Ge6B C205 Ge1A 67.7(3) . .
Ge9B C205 Ge1A 81.3(3) . .
O21 C206 C208 109.3(13) . .
O21 C206 Rb2 54.7(7) . .
C208 C206 Rb2 85.6(9) . .
O23 C207 C203 107.7(15) . .
O23 C207 Ge9B 72.9(7) . .
C203 C207 Ge9B 81.7(10) . .
O25 C208 C206 108.9(14) . .
O25 C208 Ge1A 113.7(11) . 2_556
C206 C208 Ge1A 134.4(11) . 2_556
O24 C209 C212 111.6(17) . .
O26 C210 C204 109.0(14) . .
O22 C211 C201 109.7(13) . .
O22 C211 Rb2 51.9(7) . .
C201 C211 Rb2 85.0(10) . .
O22 C211 Ge1B 83.1(8) . 2_566
C201 C211 Ge1B 116.9(11) . 2_566
Rb2 C211 Ge1B 54.5(2) . 2_566
O26 C212 C209 105.4(14) . .
O32 Rb3 O36 107.9(3) . .
O32 Rb3 O34 107.8(3) . .
O36 Rb3 O34 108.0(3) . .
O32 Rb3 O33 53.8(3) . .
O36 Rb3 O33 130.4(3) . .
O34 Rb3 O33 55.0(3) . .
O32 Rb3 O31 129.0(3) . .
O36 Rb3 O31 54.6(3) . .
O34 Rb3 O31 54.1(3) . .
O33 Rb3 O31 98.4(3) . .
O32 Rb3 O35 53.6(3) . .
O36 Rb3 O35 56.3(3) . .
O34 Rb3 O35 134.0(3) . .
O33 Rb3 O35 99.7(3) . .
O31 Rb3 O35 101.7(3) . .
O32 Rb3 C309 75.6(4) . .
O36 Rb3 C309 40.3(4) . .
O34 Rb3 C309 142.3(3) . .
O33 Rb3 C309 122.9(3) . .
O31 Rb3 C309 93.7(4) . .
O35 Rb3 C309 23.4(3) . .
O32 Rb3 C310 39.7(3) . .
O36 Rb3 C310 77.0(4) . .
O34 Rb3 C310 142.6(3) . .
O33 Rb3 C310 92.8(4) . .
O31 Rb3 C310 124.3(3) . .
O35 Rb3 C310 22.7(3) . .
C309 Rb3 C310 38.3(4) . .
O32 Rb3 C308 73.6(4) . .
O36 Rb3 C308 137.8(4) . .
O34 Rb3 C308 39.2(4) . .
O33 Rb3 C308 21.1(3) . .
O31 Rb3 C308 90.7(4) . .
O35 Rb3 C308 120.6(3) . .
C309 Rb3 C308 143.5(4) . .
C310 Rb3 C308 113.2(4) . .
O32 Rb3 C305 38.8(4) . .
O36 Rb3 C305 138.3(4) . .
O34 Rb3 C305 74.5(4) . .
O33 Rb3 C305 21.2(3) . .
O31 Rb3 C305 119.3(3) . .
O35 Rb3 C305 91.3(4) . .
C309 Rb3 C305 114.1(4) . .
C310 Rb3 C305 78.2(4) . .
C308 Rb3 C305 36.2(4) . .
O32 Rb3 C301 136.8(3) . .
O36 Rb3 C301 38.5(4) . .
O34 Rb3 C301 74.0(3) . .
O33 Rb3 C301 119.5(3) . .
O31 Rb3 C301 21.5(3) . .
O35 Rb3 C301 93.1(4) . .
C309 Rb3 C301 78.7(4) . .
C310 Rb3 C301 115.0(4) . .
C308 Rb3 C301 112.0(4) . .
C305 Rb3 C301 140.0(4) . .
O32 Rb3 Ge7A 151.0(2) . .
O36 Rb3 Ge7A 85.9(2) . .
O34 Rb3 Ge7A 91.0(2) . .
O33 Rb3 Ge7A 134.1(2) . .
O31 Rb3 Ge7A 79.9(2) . .
O35 Rb3 Ge7A 125.81(19) . .
C309 Rb3 Ge7A 103.0(3) . .
C310 Rb3 Ge7A 126.3(3) . .
C308 Rb3 Ge7A 113.5(3) . .
C305 Rb3 Ge7A 135.7(3) . .
C301 Rb3 Ge7A 68.8(3) . .
C301 O31 C303 108.6(13) . .
C301 O31 Rb3 106.6(9) . .
C303 O31 Rb3 107.7(9) . .
C304 O32 C307 113.2(14) . .
C304 O32 Rb3 121.7(10) . .
C307 O32 Rb3 124.9(10) . .
C304 O32 Ge5B 95.0(8) . .
C307 O32 Ge5B 79.5(8) . .
Rb3 O32 Ge5B 99.0(3) . .
C304 O32 Ge9B 78.2(8) . .
C307 O32 Ge9B 117.3(9) . .
Rb3 O32 Ge9B 79.5(2) . .
Ge5B O32 Ge9B 37.89(10) . .
C308 O33 C305 110.9(13) . .
C308 O33 Rb3 107.1(9) . .
C305 O33 Rb3 107.1(9) . .
C306 O34 C311 112.3(14) . .
C306 O34 Rb3 119.5(11) . .
C311 O34 Rb3 120.5(8) . .
C310 O35 C309 111.8(12) . .
C310 O35 Rb3 99.3(8) . .
C309 O35 Rb3 97.9(8) . .
C312 O36 C302 114.2(14) . .
C312 O36 Rb3 120.5(10) . .
C302 O36 Rb3 120.9(10) . .
O31 C301 C302 106.5(14) . .
O31 C301 Rb3 51.9(8) . .
C302 C301 Rb3 83.5(10) . .
O36 C302 C301 111.1(14) . .
O36 C302 Ge3B 105.8(10) . 1_655
C301 C302 Ge3B 137.8(11) . 1_655
O31 C303 C311 104.8(14) . .
C310 C304 O32 111.8(16) . .
C310 C304 Ge9B 69.0(9) . .
O32 C304 Ge9B 81.4(8) . .
C310 C304 Ge4B 101.1(11) . 2_566
O32 C304 Ge4B 117.5(9) . 2_566
Ge9B C304 Ge4B 62.7(2) . 2_566
C310 C304 Ge5B 105.3(10) . .
O32 C304 Ge5B 65.5(7) . .
Ge9B C304 Ge5B 36.26(14) . .
Ge4B C304 Ge5B 55.0(2) 2_566 .
O33 C305 C307 109.1(14) . .
O33 C305 Rb3 51.7(7) . .
C307 C305 Rb3 85.7(10) . .
O33 C305 Ge5B 134.3(10) . .
C307 C305 Ge5B 78.3(10) . .
Rb3 C305 Ge5B 85.4(4) . .
O33 C305 Ge1B 115.5(10) . .
C307 C305 Ge1B 114.1(11) . .
Rb3 C305 Ge1B 86.3(4) . .
Ge5B C305 Ge1B 35.87(16) . .
O34 C306 C308 110.4(17) . .
O32 C307 C305 108.5(15) . .
O32 C307 Ge5B 79.0(8) . .
C305 C307 Ge5B 80.2(10) . .
O32 C307 Ge7B 104.8(10) . 2_566
C305 C307 Ge7B 127.3(11) . 2_566
Ge5B C307 Ge7B 67.3(3) . 2_566
O33 C308 C306 109.1(13) . .
O33 C308 Rb3 51.9(7) . .
C306 C308 Rb3 85.6(9) . .
O35 C309 C312 109.0(13) . .
O35 C309 Rb3 58.7(7) . .
C312 C309 Rb3 86.6(10) . .
C304 C310 O35 109.2(13) . .
C304 C310 Rb3 86.5(11) . .
O35 C310 Rb3 58.0(8) . .
C304 C310 Ge9B 90.3(9) . .
O35 C310 Ge9B 126.9(10) . .
Rb3 C310 Ge9B 75.4(3) . .
O34 C311 C303 109.5(14) . .
O36 C312 C309 109.5(14) . .
O36 C312 Ge4B 132.9(12) . 1_655
C309 C312 Ge4B 114.5(12) . 1_655
O36 C312 Ge3B 105.9(11) . 1_655
C309 C312 Ge3B 142.6(11) . 1_655
Ge4B C312 Ge3B 39.23(17) 1_655 1_655
O41 Rb4 O44 112.2(4) . .
O41 Rb4 O45 114.2(4) . .
O44 Rb4 O45 115.5(4) . .
O41 Rb4 O46 140.7(3) . .
O44 Rb4 O46 58.5(4) . .
O45 Rb4 O46 57.1(4) . .
O41 Rb4 O42 56.2(4) . .
O44 Rb4 O42 144.9(3) . .
O45 Rb4 O42 58.6(4) . .
O46 Rb4 O42 107.4(4) . .
O41 Rb4 O43 56.2(4) . .
O44 Rb4 O43 56.4(4) . .
O45 Rb4 O43 145.1(3) . .
O46 Rb4 O43 106.7(4) . .
O42 Rb4 O43 106.7(3) . .
O41 Rb4 Ge8A 118.1(2) . .
O44 Rb4 Ge8A 92.0(2) . .
O45 Rb4 Ge8A 102.8(3) . .
O46 Rb4 Ge8A 100.9(2) . .
O42 Rb4 Ge8A 123.0(3) . .
O43 Rb4 Ge8A 111.1(2) . .
O41 Rb4 C401 76.2(4) . .
O44 Rb4 C401 40.0(4) . .
O45 Rb4 C401 151.3(4) . .
O46 Rb4 C401 97.3(5) . .
O42 Rb4 C401 128.7(4) . .
O43 Rb4 C401 22.0(4) . .
Ge8A Rb4 C401 94.2(3) . .
O41 Rb4 C403 40.4(4) . .
O44 Rb4 C403 149.5(4) . .
O45 Rb4 C403 78.2(4) . .
O46 Rb4 C403 129.3(4) . .
O42 Rb4 C403 22.0(4) . .
O43 Rb4 C403 96.2(4) . .
Ge8A Rb4 C403 112.2(3) . .
C401 Rb4 C403 116.6(4) . .
O41 Rb4 C409 147.4(4) . .
O44 Rb4 C409 78.4(5) . .
O45 Rb4 C409 39.7(4) . .
O46 Rb4 C409 22.3(4) . .
O42 Rb4 C409 96.9(4) . .
O43 Rb4 C409 129.0(5) . .
Ge8A Rb4 C409 91.1(3) . .
C401 Rb4 C409 118.2(5) . .
C403 Rb4 C409 117.7(5) . .
O41 Rb4 C407 76.9(4) . .
O44 Rb4 C407 151.9(4) . .
O45 Rb4 C407 41.3(4) . .
O46 Rb4 C407 97.1(5) . .
O42 Rb4 C407 22.6(4) . .
O43 Rb4 C407 129.2(4) . .
Ge8A Rb4 C407 107.3(3) . .
C401 Rb4 C407 151.3(4) . .
C403 Rb4 C407 37.6(4) . .
C409 Rb4 C407 81.0(5) . .
O41 Rb4 C410 146.3(4) . .
O44 Rb4 C410 40.4(4) . .
O45 Rb4 C410 77.5(5) . .
O46 Rb4 C410 22.6(4) . .
O42 Rb4 C410 129.8(4) . .
O43 Rb4 C410 95.4(4) . .
Ge8A Rb4 C410 87.3(3) . .
C401 Rb4 C410 80.4(5) . .
C403 Rb4 C410 151.8(5) . .
C409 Rb4 C410 38.5(5) . .
C407 Rb4 C410 118.6(5) . .
C406 O41 C404 113.1(13) . .
C406 O41 Rb4 122.1(10) . .
C404 O41 Rb4 121.9(10) . .
C406 O41 Ge6A 120.8(10) . .
C404 O41 Ge6A 100.4(9) . .
Rb4 O41 Ge6A 66.7(2) . .
C403 O42 C407 110.8(14) . .
C403 O42 Rb4 104.7(10) . .
C407 O42 Rb4 104.2(9) . .
C401 O43 C402 113.3(16) . .
C401 O43 Rb4 103.7(10) . .
C402 O43 Rb4 104.8(10) . .
C405 O44 C408 115.2(16) . .
C405 O44 Rb4 122.0(11) . .
C408 O44 Rb4 117.5(13) . .
C411 O45 C412 109.5(15) . .
C411 O45 Rb4 121.7(11) . .
C412 O45 Rb4 120.4(11) . .
C409 O46 C410 113.4(15) . .
C409 O46 Rb4 104.5(12) . .
C410 O46 Rb4 104.6(12) . .
O43 C401 C405 110.7(17) . .
O43 C401 Rb4 54.2(9) . .
C405 C401 Rb4 85.3(10) . .
O43 C401 Ge7A 106.9(10) . .
C405 C401 Ge7A 108.3(12) . .
Rb4 C401 Ge7A 70.9(3) . .
C404 C402 O43 109.3(15) . .
C404 C402 Rb4 85.5(11) . .
O43 C402 Rb4 52.9(8) . .
C404 C402 Ge6A 102.8(11) . .
O43 C402 Ge6A 101.6(9) . .
Rb4 C402 Ge6A 61.3(3) . .
C404 C402 Ge1B 67.5(11) . .
O43 C402 Ge1B 168.8(11) . .
Rb4 C402 Ge1B 115.9(5) . .
Ge6A C402 Ge1B 69.5(3) . .
C404 C402 Ge2B 92.9(11) . .
O43 C402 Ge2B 138.0(10) . .
Rb4 C402 Ge2B 95.8(4) . .
Ge6A C402 Ge2B 37.27(16) . .
Ge1B C402 Ge2B 35.09(15) . .
O42 C403 C406 108.3(16) . .
O42 C403 Rb4 53.3(8) . .
C406 C403 Rb4 84.9(10) . .
O42 C403 Ge9A 92.0(9) . .
C406 C403 Ge9A 111.4(11) . .
Rb4 C403 Ge9A 56.7(3) . .
C402 C404 O41 107.1(14) . .
C402 C404 Ge1B 93.3(11) . .
O41 C404 Ge1B 99.4(10) . .
O44 C405 C401 108.8(15) . .
O44 C405 Rb4 40.1(8) . .
C401 C405 Rb4 71.8(10) . .
O41 C406 C403 109.0(14) . .
O41 C406 Rb4 39.6(8) . .
C403 C406 Rb4 72.2(10) . .
O41 C406 Ge3B 89.6(10) . .
C403 C406 Ge3B 87.7(12) . .
Rb4 C406 Ge3B 102.4(4) . .
O42 C407 C412 108.3(16) . .
O42 C407 Rb4 53.2(8) . .
C412 C407 Rb4 84.2(10) . .
C410 C408 O44 113(2) . .
C410 C408 Rb4 74.7(14) . .
O44 C408 Rb4 42.8(10) . .
O46 C409 C411 110.4(15) . .
O46 C409 Rb4 53.2(10) . .
C411 C409 Rb4 85.5(12) . .
O46 C409 Ge4A 147.2(13) . 2
C411 C409 Ge4A 100.6(12) . 2
Rb4 C409 Ge4A 142.7(7) . 2
O46 C409 Ge5A 107.9(12) . 2
C411 C409 Ge5A 140.5(13) . 2
Rb4 C409 Ge5A 126.0(6) . 2
Ge4A C409 Ge5A 40.02(17) 2 2
C408 C410 O46 110.9(17) . .
C408 C410 Rb4 83.4(14) . .
O46 C410 Rb4 52.9(10) . .
C408 C410 Ge5A 145.1(14) . 2
O46 C410 Ge5A 103.7(11) . 2
Rb4 C410 Ge5A 123.2(5) . 2
O45 C411 C409 106.2(18) . .
O45 C412 C407 106.9(16) . .
CN2 NC1 Ge1A 105.4(12) . 1_565
NC2 CN1 CN2 103(3) . .
NC1 CN2 CN1 109.9(18) . .
CN3 NC3 Ge8A 100.60(14) . .
CN3 NC3 Ge5A 97.38(14) . 2
Ge8A NC3 Ge5A 112.7(2) . 2
CN4 NC4 Ge4A 116.46(14) . 1_455
CN4 NC4 Ge7A 135.37(13) . 1_455
Ge4A NC4 Ge7A 38.42(9) 1_455 1_455
NC4 CN4 CN3 115.7 . 1_455
NC3 CN3 CN4 105.5 . 1_655
NC3 CN3 Ge9A 98.17(13) . 2
CN4 CN3 Ge9A 127.80(12) 1_655 2
NC3 CN3 Ge8A 84.43(13) . 2
CN4 CN3 Ge8A 164.13(13) 1_655 2
Ge9A CN3 Ge8A 36.92(9) 2 2
NC3 CN3 Ge5A 62.32(13) . 2
CN4 CN3 Ge5A 140.30(12) 1_655 2
Ge9A CN3 Ge5A 36.34(8) 2 2
Ge8A CN3 Ge5A 34.77(8) 2 2
NC3 CN3 Ge8A 59.41(12) . .
CN4 CN3 Ge8A 111.41(12) 1_655 .
Ge9A CN3 Ge8A 120.7(2) 2 .
Ge8A CN3 Ge8A 84.24(16) 2 .
Ge5A CN3 Ge8A 94.80(17) 2 .
NC5 CN5 CN6 126.2 . .
CN5 CN6 NC6 100.8 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ge1A Ge2A 2.495(2) .
Ge1A Ge4A 2.545(3) .
Ge1A Ge3A 2.576(2) .
Ge1A Ge5A 2.607(3) .
Ge1A C208 3.936(17) 2_556
Ge1A NC1 3.99(2) 1_545
Ge1A Ge9A 4.165(2) .
Ge1A Ge8A 4.175(3) .
Ge1A Ge6A 4.178(2) .
Ge1A C201 4.212(17) 2_556
Ge2A Ge9A 2.505(3) .
Ge2A Ge6B 2.619(2) .
Ge2A Ge6A 2.631(2) .
Ge2A Ge3A 2.708(2) .
Ge2A Ge5A 2.892(2) .
Ge2A Ge2B 3.612(2) .
Ge2A Ge4A 3.809(2) .
Ge2A Ge8A 3.896(3) .
Ge2A C102 4.014(16) .
Ge3A Ge7A 2.580(3) .
Ge3A Ge6A 2.690(2) .
Ge3A Ge4A 2.745(2) .
Ge3A Ge2B 3.502(2) .
Ge3A Ge6B 3.818(2) .
Ge3A Rb3 3.869(2) .
Ge3A C104 3.873(16) 1_655
Ge3A Ge9B 3.923(2) .
Ge4A Ge7A 2.545(2) .
Ge4A Ge8A 2.630(2) .
Ge4A Ge5A 2.662(2) .
Ge4A C104 3.692(15) 1_655
Ge4A C409 3.788(17) 2
Ge4A NC4 3.796(9) 1_655
Ge4A Ge6A 3.837(2) .
Ge5A Ge8A 2.514(3) .
Ge5A Ge9A 2.600(2) .
Ge5A NC3 3.782(9) 2
Ge5A C102 3.795(16) .
Ge5A Ge6A 3.921(2) .
Ge5A C409 3.974(18) 2
Ge6A Ge7A 2.500(2) .
Ge6A Ge9A 2.535(2) .
Ge6A Ge2B 2.636(2) .
Ge6A Ge8A 2.995(3) .
Ge6A Ge6B 3.744(3) .
Ge6A Rb4 3.844(3) .
Ge6A C402 3.910(17) .
Ge7A Ge8A 2.609(3) .
Ge7A Rb3 3.838(2) .
Ge7A NC4 3.929(9) 1_655
Ge7A Ge9A 4.136(2) .
Ge7A C401 4.232(18) .
Ge8A Ge9A 2.619(3) .
Ge8A Rb4 3.528(2) .
Ge8A NC3 3.732(9) .
Ge9A Rb4 3.729(3) .
Ge9A O13 3.777(12) .
Ge9A CN3 4.092(9) 2
Ge9A C111 4.121(18) .
Ge9A C105 4.122(16) .
Ge1B Ge5B 2.529(2) .
Ge1B Ge3B 2.569(2) .
Ge1B Ge2B 2.574(2) .
Ge1B Ge4B 2.580(2) .
Ge1B Rb2 3.616(2) 2_566
Ge1B C404 3.951(18) .
Ge1B Ge9B 4.138(2) .
Ge1B C204 4.140(17) 2_566
Ge1B C211 4.145(16) 2_566
Ge1B Ge6B 4.160(2) .
Ge2B Ge6B 2.548(2) .
Ge2B Ge9B 2.623(3) .
Ge2B Ge3B 2.693(2) .
Ge2B Ge5B 2.997(2) .
Ge2B Rb3 3.902(2) .
Ge2B Ge4B 3.965(2) .
Ge3B Ge7B 2.594(3) .
Ge3B Ge6B 2.684(2) .
Ge3B Ge4B 2.728(2) .
Ge3B Ge5B 3.884(2) .
Ge3B Ge8B 3.916(2) .
Ge3B Rb1 4.071(2) .
Ge4B Ge7B 2.555(2) .
Ge4B Ge5B 2.684(2) .
Ge4B Ge8B 2.701(2) .
Ge4B Ge8B 3.774(2) 2_566
Ge4B Ge5B 3.800(2) 2_566
Ge4B C312 3.865(18) 1_455
Ge4B Rb2 3.911(2) 2_566
Ge4B Ge6B 3.927(2) .
Ge5B Ge8B 2.532(2) 2_566
Ge5B Ge9B 2.544(2) .
Ge5B Ge8B 2.592(2) .
Ge5B Ge5B 3.637(3) 2_566
Ge5B Ge4B 3.800(2) 2_566
Ge5B O32 3.830(10) .
Ge5B C307 3.835(18) .
Ge6B Ge9B 2.554(2) .
Ge6B Ge7B 2.603(2) .
Ge6B Ge8B 2.981(2) .
Ge6B C202 3.722(18) .
Ge6B C205 3.811(15) .
Ge7B Ge8B 2.516(2) .
Ge7B Rb1 3.513(2) .
Ge7B C108 4.020(16) .
Ge7B Ge9B 4.129(2) .
Ge7B C307 4.25(2) 2_566
Ge8B Ge5B 2.532(2) 2_566
Ge8B Ge9B 2.559(2) .
Ge8B Ge8B 3.610(3) 2_566
Ge8B Ge4B 3.774(2) 2_566
Ge9B O23 3.655(10) .
Ge9B C310 3.690(16) .
Ge9B C207 3.812(15) .
Ge9B C203 3.879(19) .
Ge9B C304 3.952(17) .
Rb1 O13 2.822(11) .
Rb1 O14 2.903(10) .
Rb1 O16 2.934(11) .
Rb1 O11 2.946(9) .
Rb1 O15 3.011(9) .
Rb1 O12 3.124(10) .
Rb1 C101 3.556(14) .
Rb1 C106 3.561(14) .
O11 C112 1.377(18) .
O11 C104 1.384(17) .
O12 C107 1.411(16) .
O12 C108 1.426(17) .
O13 C111 1.369(19) .
O13 C105 1.404(16) .
O14 C103 1.405(18) .
O14 C109 1.424(16) .
O15 C101 1.369(18) .
O15 C102 1.407(18) .
O16 C110 1.38(2) .
O16 C106 1.433(17) .
C101 C109 1.46(2) .
C102 C105 1.48(2) .
C103 C107 1.505(19) .
C104 C106 1.39(2) .
C104 Ge4A 3.692(15) 1_455
C104 Ge3A 3.873(16) 1_455
C106 Ge4A 3.973(16) 1_455
C108 C112 1.45(2) .
C110 C111 1.50(2) .
Rb2 O23 2.850(11) .
Rb2 O25 2.946(11) .
Rb2 O26 2.966(11) .
Rb2 O22 3.046(11) .
Rb2 O21 3.046(11) .
Rb2 O24 3.059(10) .
Rb2 C203 3.54(2) .
Rb2 C202 3.613(18) .
Rb2 Ge1B 3.615(2) 2_566
Rb2 C206 3.624(15) .
Rb2 C211 3.699(17) .
Rb2 C204 3.726(18) .
O21 C202 1.354(19) .
O21 C206 1.369(18) .
O22 C211 1.386(17) .
O22 C204 1.397(18) .
O23 C205 1.345(18) .
O23 C207 1.426(19) .
O24 C203 1.40(2) .
O24 C209 1.42(2) .
O25 C208 1.347(18) .
O25 C201 1.389(19) .
O26 C210 1.403(19) .
O26 C212 1.419(18) .
C201 C211 1.43(2) .
C201 Ge1A 4.212(17) 2_556
C202 C205 1.53(2) .
C203 C207 1.45(3) .
C204 C210 1.48(2) .
C204 Ge1B 4.140(17) 2_566
C206 C208 1.46(2) .
C208 Ge1A 3.936(17) 2_556
C209 C212 1.49(2) .
C211 Ge1B 4.145(16) 2_566
Rb3 O32 2.878(12) .
Rb3 O36 2.942(10) .
Rb3 O34 3.020(11) .
Rb3 O33 3.049(9) .
Rb3 O31 3.064(12) .
Rb3 O35 3.120(11) .
Rb3 C309 3.616(15) .
Rb3 C310 3.630(19) .
Rb3 C308 3.706(18) .
Rb3 C305 3.713(17) .
Rb3 C301 3.733(17) .
O31 C301 1.430(17) .
O31 C303 1.465(19) .
O32 C304 1.404(18) .
O32 C307 1.430(18) .
O33 C308 1.394(19) .
O33 C305 1.405(18) .
O34 C306 1.373(18) .
O34 C311 1.446(19) .
O35 C310 1.419(19) .
O35 C309 1.450(17) .
O36 C312 1.38(2) .
O36 C302 1.386(19) .
C301 C302 1.43(2) .
C302 Ge3B 4.200(16) 1_655
C303 C311 1.47(2) .
C304 C310 1.40(2) .
C304 Ge4B 4.025(16) 2_566
C305 C307 1.44(2) .
C306 C308 1.48(3) .
C307 Ge7B 4.25(2) 2_566
C309 C312 1.49(2) .
C312 Ge4B 3.865(18) 1_655
C312 Ge3B 4.205(18) 1_655
Rb4 O41 2.818(12) .
Rb4 O44 2.839(13) .
Rb4 O45 2.844(12) .
Rb4 O46 2.964(14) .
Rb4 O42 2.966(12) .
Rb4 O43 2.979(13) .
Rb4 C401 3.566(18) .
Rb4 C403 3.579(19) .
Rb4 C409 3.58(2) .
Rb4 C407 3.590(17) .
Rb4 C410 3.60(2) .
O41 C406 1.386(19) .
O41 C404 1.423(19) .
O42 C403 1.39(2) .
O42 C407 1.42(2) .
O43 C401 1.38(2) .
O43 C402 1.41(2) .
O44 C405 1.358(19) .
O44 C408 1.41(2) .
O45 C411 1.39(2) .
O45 C412 1.41(2) .
O46 C409 1.40(2) .
O46 C410 1.43(2) .
C401 C405 1.46(2) .
C402 C404 1.40(2) .
C403 C406 1.46(2) .
C407 C412 1.54(3) .
C408 C410 1.40(3) .
C409 C411 1.47(2) .
C409 Ge4A 3.788(17) 2
C409 Ge5A 3.974(18) 2
C410 Ge5A 4.05(2) 2
NC1 CN2 1.43(3) .
NC1 Ge1A 3.99(2) 1_565
CN1 NC2 1.43(4) .
CN1 CN2 1.44(3) .
NC3 CN3 1.4820 .
NC3 Ge5A 3.782(9) 2
NC4 CN4 1.3671 .
NC4 Ge4A 3.796(9) 1_455
NC4 Ge7A 3.929(9) 1_455
CN4 CN3 1.4879 1_455
CN3 CN4 1.4878 1_655
CN3 Ge9A 4.092(9) 2
CN3 Ge8A 4.176(9) 2
CN3 Ge5A 4.235(9) 2
NC5 CN5 1.2421 .
CN5 CN6 1.3852 .
NC6 CN6 1.4682 .
