#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:45:22 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179392 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/89/4328908.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4328908
loop_
_publ_author_name
'Hua Lin'
'Long-Hua Li'
'Ling Chen'
_publ_section_title
;
 Diverse Closed Cavities in Condensed Rare Earth Metal-Chalcogenide
 Matrixes: Cs[Lu7Q11] and (ClCs6)[RE21Q34] (RE = Dy, Ho; Q = S, Se, Te)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4588
_journal_page_last               4596
_journal_paper_doi               10.1021/ic202494w
_journal_volume                  51
_journal_year                    2012
_chemical_formula_moiety         'Cl Cs6 Dy21 S34'
_chemical_formula_sum            'Cl Cs6 Dy21 S34'
_chemical_formula_weight         5335.45
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 128.738(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   17.166(6)
_cell_length_b                   19.530(6)
_cell_length_c                   13.017(5)
_cell_measurement_reflns_used    5271
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.5010
_cell_measurement_theta_min      2.0058
_cell_volume                     3404(2)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2007)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  Saturn724
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0287
_diffrn_reflns_av_sigmaI/netI    0.0322
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            13510
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.01
_exptl_absorpt_coefficient_mu    26.972
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.8090
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Brown
_exptl_crystal_density_diffrn    5.206
_exptl_crystal_description       Block
_exptl_crystal_F_000             4554
_exptl_crystal_size_max          0.2000
_exptl_crystal_size_mid          0.1500
_exptl_crystal_size_min          0.1000
_refine_diff_density_max         1.793
_refine_diff_density_min         -2.189
_refine_diff_density_rms         0.285
_refine_ls_extinction_coef       0.000180(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.057
_refine_ls_matrix_type           full
_refine_ls_number_parameters     154
_refine_ls_number_reflns         4006
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.057
_refine_ls_R_factor_all          0.0230
_refine_ls_R_factor_gt           0.0196
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0157P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0423
_refine_ls_wR_factor_ref         0.0431
_reflns_number_gt                3647
_reflns_number_total             4006
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic202494w_si_001_3.cif
_cod_data_source_block           ClCs6Dy21S34
_cod_database_code               4328908
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cs1 Cs 0.42856(3) 0.377265(19) 0.27065(4) 0.02544(9) Uani 1 1 d .
Cs2 Cs 0.26875(4) 0.5000 0.41586(5) 0.02681(12) Uani 1 2 d S
Dy1 Dy 0.0000 0.301520(17) 0.0000 0.01011(7) Uani 1 2 d S
Dy2 Dy 0.254388(17) 0.208876(11) 0.24884(2) 0.00772(6) Uani 1 1 d .
Dy3 Dy 0.127683(16) 0.299549(11) 0.37606(2) 0.00782(6) Uani 1 1 d .
Dy4 Dy 0.0000 0.099905(15) 0.0000 0.00767(7) Uani 1 2 d S
Dy5 Dy 0.363386(18) 0.101941(11) 0.10703(2) 0.00845(6) Uani 1 1 d .
Dy6 Dy 0.5000 0.100259(16) 0.5000 0.01009(7) Uani 1 2 d S
Dy7 Dy 0.0000 0.5000 0.0000 0.00780(9) Uani 1 4 d S
Dy8 Dy 0.24329(2) 0.0000 0.25692(3) 0.00803(7) Uani 1 2 d S
S1 S 0.18356(13) 0.5000 0.05956(16) 0.0106(4) Uani 1 2 d S
S2 S 0.05895(13) 0.0000 0.18037(16) 0.0099(3) Uani 1 2 d S
S3 S 0.18975(9) 0.10042(6) 0.07652(11) 0.0083(2) Uani 1 1 d .
S4 S 0.18337(10) 0.30197(7) 0.06368(12) 0.0148(3) Uani 1 1 d .
S5 S 0.06953(9) 0.20305(6) 0.18546(11) 0.0079(2) Uani 1 1 d .
S6 S 0.43893(9) 0.19359(6) 0.31014(11) 0.0086(2) Uani 1 1 d .
S7 S 0.31117(9) 0.29815(6) 0.44223(11) 0.0097(3) Uani 1 1 d .
S8 S 0.31816(9) 0.10419(6) 0.43693(11) 0.0089(3) Uani 1 1 d .
S9 S 0.05112(9) 0.39956(6) 0.18145(11) 0.0080(2) Uani 1 1 d .
S10 S 0.42587(12) 0.0000 0.30767(15) 0.0077(3) Uani 1 2 d S
Cl1 Cl 0.5000 0.5000 0.5000 0.0238(6) Uani 1 4 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Cl1 Cs1 S5 129.48(3) . 8
Cl1 Cs1 S4 123.73(3) . .
S5 Cs1 S4 106.78(4) 8 .
Cl1 Cs1 S6 128.03(3) . .
S5 Cs1 S6 68.13(3) 8 .
S4 Cs1 S6 68.35(3) . .
Cl1 Cs1 S3 128.29(3) . 7
S5 Cs1 S3 68.24(3) 8 7
S4 Cs1 S3 68.71(3) . 7
S6 Cs1 S3 103.60(3) . 7
Cl1 Cs1 S7 82.61(3) . 2_656
S5 Cs1 S7 62.41(4) 8 2_656
S4 Cs1 S7 130.77(3) . 2_656
S6 Cs1 S7 63.15(3) . 2_656
S3 Cs1 S7 130.34(3) 7 2_656
Cl1 Cs1 S2 82.68(3) . 3
S5 Cs1 S2 63.52(3) 8 3
S4 Cs1 S2 130.09(4) . 3
S6 Cs1 S2 131.45(3) . 3
S3 Cs1 S2 62.30(3) 7 3
S7 Cs1 S2 90.17(4) 2_656 3
Cl1 Cs1 S1 80.22(3) . .
S5 Cs1 S1 131.36(4) 8 .
S4 Cs1 S1 60.27(3) . .
S6 Cs1 S1 128.30(3) . .
S3 Cs1 S1 63.43(3) 7 .
S7 Cs1 S1 162.79(3) 2_656 .
S2 Cs1 S1 88.86(4) 3 .
Cl1 Cs1 S7 79.58(3) . .
S5 Cs1 S7 130.86(3) 8 .
S4 Cs1 S7 60.93(4) . .
S6 Cs1 S7 63.19(3) . .
S3 Cs1 S7 129.34(3) 7 .
S7 Cs1 S7 89.29(4) 2_656 .
S2 Cs1 S7 162.17(3) 3 .
S1 Cs1 S7 86.42(4) . .
Cl1 Cs1 Dy5 117.21(2) . 7
S5 Cs1 Dy5 102.47(4) 8 7
S4 Cs1 Dy5 37.32(2) . 7
S6 Cs1 Dy5 100.04(2) . 7
S3 Cs1 Dy5 39.31(2) 7 7
S7 Cs1 Dy5 160.06(2) 2_656 7
S2 Cs1 Dy5 94.29(4) 3 7
S1 Cs1 Dy5 37.01(2) . 7
S7 Cs1 Dy5 92.26(4) . 7
Cl1 Cs1 Dy2 116.564(19) . .
S5 Cs1 Dy2 102.64(3) 8 .
S4 Cs1 Dy2 37.32(2) . .
S6 Cs1 Dy2 39.30(2) . .
S3 Cs1 Dy2 100.57(2) 7 .
S7 Cs1 Dy2 95.23(3) 2_656 .
S2 Cs1 Dy2 160.50(2) 3 .
S1 Cs1 Dy2 91.36(3) . .
S7 Cs1 Dy2 37.016(19) . .
Dy5 Cs1 Dy2 74.63(2) 7 .
Cl1 Cs1 Dy4 120.06(2) . 7
S5 Cs1 Dy4 38.85(2) 8 7
S4 Cs1 Dy4 102.86(3) . 7
S6 Cs1 Dy4 101.544(19) . 7
S3 Cs1 Dy4 38.34(3) 7 7
S7 Cs1 Dy4 94.61(4) 2_656 7
S2 Cs1 Dy4 37.38(2) 3 7
S1 Cs1 Dy4 95.02(3) . 7
S7 Cs1 Dy4 160.29(2) . 7
Dy5 Cs1 Dy4 77.64(4) 7 7
Dy2 Cs1 Dy4 123.286(14) . 7
Cl1 Cs2 S9 131.32(3) . .
Cl1 Cs2 S9 131.32(3) . 6_565
S9 Cs2 S9 66.36(4) . 6_565
Cl1 Cs2 S8 127.14(3) . 4_556
S9 Cs2 S8 101.49(4) . 4_556
S9 Cs2 S8 66.15(4) 6_565 4_556
Cl1 Cs2 S8 127.14(3) . 7_556
S9 Cs2 S8 66.15(4) . 7_556
S9 Cs2 S8 101.49(4) 6_565 7_556
S8 Cs2 S8 66.93(4) 4_556 7_556
Cl1 Cs2 S1 82.88(3) . .
S9 Cs2 S1 64.63(3) . .
S9 Cs2 S1 64.63(3) 6_565 .
S8 Cs2 S1 130.24(3) 4_556 .
S8 Cs2 S1 130.24(3) 7_556 .
Cl1 Cs2 S7 81.859(19) . 6_565
S9 Cs2 S7 130.67(3) . 6_565
S9 Cs2 S7 64.46(3) 6_565 6_565
S8 Cs2 S7 61.39(3) 4_556 6_565
S8 Cs2 S7 127.76(3) 7_556 6_565
S1 Cs2 S7 90.848(18) . 6_565
Cl1 Cs2 S7 81.859(19) . .
S9 Cs2 S7 64.46(3) . .
S9 Cs2 S7 130.67(3) 6_565 .
S8 Cs2 S7 127.76(3) 4_556 .
S8 Cs2 S7 61.39(3) 7_556 .
S1 Cs2 S7 90.848(18) . .
S7 Cs2 S7 163.29(4) 6_565 .
Cl1 Cs2 S2 80.04(3) . 7_556
S9 Cs2 S2 128.38(3) . 7_556
S9 Cs2 S2 128.38(3) 6_565 7_556
S8 Cs2 S2 62.45(4) 4_556 7_556
S8 Cs2 S2 62.45(4) 7_556 7_556
S1 Cs2 S2 162.91(4) . 7_556
S7 Cs2 S2 86.755(18) 6_565 7_556
S7 Cs2 S2 86.755(18) . 7_556
Cl1 Cs2 Dy8 116.262(18) . 7_556
S9 Cs2 Dy8 99.74(3) . 7_556
S9 Cs2 Dy8 99.74(3) 6_565 7_556
S8 Cs2 Dy8 38.43(2) 4_556 7_556
S8 Cs2 Dy8 38.43(2) 7_556 7_556
S1 Cs2 Dy8 160.86(3) . 7_556
S7 Cs2 Dy8 91.915(18) 6_565 7_556
S7 Cs2 Dy8 91.915(18) . 7_556
S2 Cs2 Dy8 36.22(3) 7_556 7_556
Cl1 Cs2 Dy7 120.77(3) . .
S9 Cs2 Dy7 38.76(2) . .
S9 Cs2 Dy7 38.76(2) 6_565 .
S8 Cs2 Dy7 100.70(4) 4_556 .
S8 Cs2 Dy7 100.70(4) 7_556 .
S1 Cs2 Dy7 37.90(3) . .
S7 Cs2 Dy7 95.766(19) 6_565 .
S7 Cs2 Dy7 95.766(19) . .
S2 Cs2 Dy7 159.19(3) 7_556 .
Dy8 Cs2 Dy7 122.97(3) 7_556 .
Cl1 Cs2 Dy3 118.552(14) . .
S9 Cs2 Dy3 38.72(2) . .
S9 Cs2 Dy3 100.41(3) 6_565 .
S8 Cs2 Dy3 100.24(3) 4_556 .
S8 Cs2 Dy3 37.78(2) 7_556 .
S1 Cs2 Dy3 95.148(15) . .
S7 Cs2 Dy3 159.26(2) 6_565 .
S7 Cs2 Dy3 36.69(2) . .
S2 Cs2 Dy3 93.007(16) 7_556 .
Dy8 Cs2 Dy3 76.172(11) 7_556 .
Dy7 Cs2 Dy3 77.399(16) . .
S4 Dy1 S4 179.63(6) . 2
S4 Dy1 S5 93.13(4) . 2
S4 Dy1 S5 87.13(4) 2 2
S4 Dy1 S5 87.13(4) . .
S4 Dy1 S5 93.13(4) 2 .
S5 Dy1 S5 89.60(6) 2 .
S4 Dy1 S9 92.88(4) . .
S4 Dy1 S9 86.86(4) 2 .
S5 Dy1 S9 173.96(4) 2 .
S5 Dy1 S9 90.17(4) . .
S4 Dy1 S9 86.86(4) . 2
S4 Dy1 S9 92.88(4) 2 2
S5 Dy1 S9 90.17(4) 2 2
S5 Dy1 S9 173.96(4) . 2
S9 Dy1 S9 90.68(6) . 2
S4 Dy1 Dy7 89.81(3) . .
S4 Dy1 Dy7 89.81(3) 2 .
S5 Dy1 Dy7 135.20(3) 2 .
S5 Dy1 Dy7 135.20(3) . .
S9 Dy1 Dy7 45.34(3) . .
S9 Dy1 Dy7 45.34(3) 2 .
S4 Dy1 Dy5 42.35(3) . 7
S4 Dy1 Dy5 137.38(3) 2 7
S5 Dy1 Dy5 93.05(3) 2 7
S5 Dy1 Dy5 129.48(3) . 7
S9 Dy1 Dy5 91.75(3) . 7
S9 Dy1 Dy5 44.52(3) 2 7
Dy7 Dy1 Dy5 60.958(11) . 7
S4 Dy1 Dy5 137.38(3) . 8_455
S4 Dy1 Dy5 42.35(3) 2 8_455
S5 Dy1 Dy5 129.48(3) 2 8_455
S5 Dy1 Dy5 93.05(3) . 8_455
S9 Dy1 Dy5 44.52(3) . 8_455
S9 Dy1 Dy5 91.75(3) 2 8_455
Dy7 Dy1 Dy5 60.958(11) . 8_455
Dy5 Dy1 Dy5 121.92(2) 7 8_455
S4 Dy1 Dy2 137.79(3) . 2
S4 Dy1 Dy2 42.46(3) 2 2
S5 Dy1 Dy2 44.69(3) 2 2
S5 Dy1 Dy2 92.92(3) . 2
S9 Dy1 Dy2 129.32(3) . 2
S9 Dy1 Dy2 91.16(3) 2 2
Dy7 Dy1 Dy2 117.718(12) . 2
Dy5 Dy1 Dy2 122.84(3) 7 2
Dy5 Dy1 Dy2 84.80(3) 8_455 2
S4 Dy1 Dy2 42.46(3) . .
S4 Dy1 Dy2 137.79(3) 2 .
S5 Dy1 Dy2 92.92(3) 2 .
S5 Dy1 Dy2 44.69(3) . .
S9 Dy1 Dy2 91.16(3) . .
S9 Dy1 Dy2 129.32(3) 2 .
Dy7 Dy1 Dy2 117.718(12) . .
Dy5 Dy1 Dy2 84.80(3) 7 .
Dy5 Dy1 Dy2 122.84(3) 8_455 .
Dy2 Dy1 Dy2 124.56(2) 2 .
S4 Dy1 Dy3 90.96(3) . 2
S4 Dy1 Dy3 89.04(3) 2 2
S5 Dy1 Dy3 44.73(3) 2 2
S5 Dy1 Dy3 134.14(3) . 2
S9 Dy1 Dy3 135.67(3) . 2
S9 Dy1 Dy3 45.46(3) 2 2
Dy7 Dy1 Dy3 90.563(6) . 2
Dy5 Dy1 Dy3 63.111(19) 7 2
Dy5 Dy1 Dy3 117.504(19) 8_455 2
Dy2 Dy1 Dy3 59.739(10) 2 2
Dy2 Dy1 Dy3 119.656(11) . 2
S4 Dy2 S7 95.63(5) . .
S4 Dy2 S5 88.13(4) . .
S7 Dy2 S5 88.96(4) . .
S4 Dy2 S6 97.46(4) . .
S7 Dy2 S6 96.97(4) . .
S5 Dy2 S6 171.39(4) . .
S4 Dy2 S3 93.76(5) . .
S7 Dy2 S3 168.96(4) . .
S5 Dy2 S3 85.56(4) . .
S6 Dy2 S3 87.53(4) . .
S4 Dy2 S8 176.13(4) . .
S7 Dy2 S8 86.63(4) . .
S5 Dy2 S8 88.78(4) . .
S6 Dy2 S8 85.36(4) . .
S3 Dy2 S8 83.68(4) . .
S4 Dy2 Dy3 90.77(4) . .
S7 Dy2 Dy3 43.85(3) . .
S5 Dy2 Dy3 45.17(3) . .
S6 Dy2 Dy3 140.71(3) . .
S3 Dy2 Dy3 130.35(3) . .
S8 Dy2 Dy3 88.69(3) . .
S4 Dy2 Dy1 44.00(3) . .
S7 Dy2 Dy1 92.19(3) . .
S5 Dy2 Dy1 44.15(3) . .
S6 Dy2 Dy1 141.20(3) . .
S3 Dy2 Dy1 90.53(3) . .
S8 Dy2 Dy1 132.92(3) . .
Dy3 Dy2 Dy1 60.47(3) . .
S4 Dy2 Dy5 91.19(4) . .
S7 Dy2 Dy5 141.17(3) . .
S5 Dy2 Dy5 129.53(3) . .
S6 Dy2 Dy5 44.20(3) . .
S3 Dy2 Dy5 44.12(3) . .
S8 Dy2 Dy5 88.99(3) . .
Dy3 Dy2 Dy5 174.271(8) . .
Dy1 Dy2 Dy5 118.04(3) . .
S4 Dy2 Dy3 138.29(3) . 7_556
S7 Dy2 Dy3 42.76(3) . 7_556
S5 Dy2 Dy3 88.37(2) . 7_556
S6 Dy2 Dy3 91.75(3) . 7_556
S3 Dy2 Dy3 127.34(3) . 7_556
S8 Dy2 Dy3 43.88(3) . 7_556
Dy3 Dy2 Dy3 58.866(19) . 7_556
Dy1 Dy2 Dy3 119.257(12) . 7_556
Dy5 Dy2 Dy3 121.986(19) . 7_556
S4 Dy2 Dy6 140.28(3) . .
S7 Dy2 Dy6 89.97(3) . .
S5 Dy2 Dy6 131.36(3) . .
S6 Dy2 Dy6 42.84(3) . .
S3 Dy2 Dy6 86.49(3) . .
S8 Dy2 Dy6 42.64(3) . .
Dy3 Dy2 Dy6 118.83(3) . .
Dy1 Dy2 Dy6 174.921(8) . .
Dy5 Dy2 Dy6 62.09(3) . .
Dy3 Dy2 Dy6 60.015(11) 7_556 .
S4 Dy2 Cs1 55.99(3) . .
S7 Dy2 Cs1 67.43(3) . .
S5 Dy2 Cs1 132.36(3) . .
S6 Dy2 Cs1 56.10(3) . .
S3 Dy2 Cs1 123.03(3) . .
S8 Dy2 Cs1 127.87(3) . .
Dy3 Dy2 Cs1 99.99(2) . .
Dy1 Dy2 Cs1 94.05(3) . .
Dy5 Dy2 Cs1 85.56(2) . .
Dy3 Dy2 Cs1 98.731(10) 7_556 .
Dy6 Dy2 Cs1 91.03(3) . .
S7 Dy3 S7 88.67(4) 7_556 .
S7 Dy3 S8 88.66(5) 7_556 7_556
S7 Dy3 S8 92.53(4) . 7_556
S7 Dy3 S5 91.65(5) 7_556 .
S7 Dy3 S5 88.47(4) . .
S8 Dy3 S5 178.96(4) 7_556 .
S7 Dy3 S6 92.50(4) 7_556 8_455
S7 Dy3 S6 177.76(4) . 8_455
S8 Dy3 S6 85.60(4) 7_556 8_455
S5 Dy3 S6 93.40(4) . 8_455
S7 Dy3 S9 176.14(4) 7_556 .
S7 Dy3 S9 95.14(4) . .
S8 Dy3 S9 91.80(4) 7_556 .
S5 Dy3 S9 87.82(4) . .
S6 Dy3 S9 83.72(4) 8_455 .
S7 Dy3 Dy3 44.41(3) 7_556 7_556
S7 Dy3 Dy3 44.26(3) . 7_556
S8 Dy3 Dy3 90.84(3) 7_556 7_556
S5 Dy3 Dy3 90.08(3) . 7_556
S6 Dy3 Dy3 136.88(3) 8_455 7_556
S9 Dy3 Dy3 139.39(3) . 7_556
S7 Dy3 Dy2 92.12(3) 7_556 .
S7 Dy3 Dy2 43.81(3) . .
S8 Dy3 Dy2 136.25(3) 7_556 .
S5 Dy3 Dy2 44.73(3) . .
S6 Dy3 Dy2 137.99(3) 8_455 .
S9 Dy3 Dy2 90.19(3) . .
Dy3 Dy3 Dy2 61.36(3) 7_556 .
S7 Dy3 Dy1 135.36(3) 7_556 .
S7 Dy3 Dy1 91.58(3) . .
S8 Dy3 Dy1 135.87(3) 7_556 .
S5 Dy3 Dy1 43.77(3) . .
S6 Dy3 Dy1 88.92(2) 8_455 .
S9 Dy3 Dy1 44.07(3) . .
Dy3 Dy3 Dy1 121.069(13) 7_556 .
Dy2 Dy3 Dy1 59.79(2) . .
S7 Dy3 Dy2 42.85(3) 7_556 7_556
S7 Dy3 Dy2 90.69(3) . 7_556
S8 Dy3 Dy2 45.81(3) 7_556 7_556
S5 Dy3 Dy2 134.49(3) . 7_556
S6 Dy3 Dy2 88.88(2) 8_455 7_556
S9 Dy3 Dy2 137.49(3) . 7_556
Dy3 Dy3 Dy2 59.776(12) 7_556 7_556
Dy2 Dy3 Dy2 121.134(19) . 7_556
Dy1 Dy3 Dy2 177.071(8) . 7_556
S7 Dy3 Dy6 90.18(3) 7_556 7_556
S7 Dy3 Dy6 135.17(3) . 7_556
S8 Dy3 Dy6 42.64(3) 7_556 7_556
S5 Dy3 Dy6 136.36(3) . 7_556
S6 Dy3 Dy6 42.96(3) 8_455 7_556
S9 Dy3 Dy6 87.57(3) . 7_556
Dy3 Dy3 Dy6 119.91(3) 7_556 7_556
Dy2 Dy3 Dy6 177.431(8) . 7_556
Dy1 Dy3 Dy6 119.02(2) . 7_556
Dy2 Dy3 Dy6 60.181(18) 7_556 7_556
S7 Dy3 Cs1 61.32(3) 7_556 8_455
S7 Dy3 Cs1 127.72(3) . 8_455
S8 Dy3 Cs1 125.29(3) 7_556 8_455
S5 Dy3 Cs1 54.11(3) . 8_455
S6 Dy3 Cs1 54.50(3) 8_455 8_455
S9 Dy3 Cs1 115.50(3) . 8_455
Dy3 Dy3 Cs1 95.35(3) 7_556 8_455
Dy2 Dy3 Cs1 92.40(2) . 8_455
Dy1 Dy3 Cs1 84.299(8) . 8_455
Dy2 Dy3 Cs1 92.848(8) 7_556 8_455
Dy6 Dy3 Cs1 89.70(2) 7_556 8_455
S2 Dy4 S2 88.10(6) 5 .
S2 Dy4 S3 88.47(4) 5 2
S2 Dy4 S3 91.83(4) . 2
S2 Dy4 S3 91.83(4) 5 .
S2 Dy4 S3 88.47(4) . .
S3 Dy4 S3 179.58(5) 2 .
S2 Dy4 S5 176.86(4) 5 .
S2 Dy4 S5 92.57(4) . .
S3 Dy4 S5 94.57(4) 2 .
S3 Dy4 S5 85.12(4) . .
S2 Dy4 S5 92.57(4) 5 2
S2 Dy4 S5 176.86(4) . 2
S3 Dy4 S5 85.12(4) 2 2
S3 Dy4 S5 94.57(4) . 2
S5 Dy4 S5 86.93(6) . 2
S2 Dy4 Dy8 43.37(4) 5 5
S2 Dy4 Dy8 90.10(4) . 5
S3 Dy4 Dy8 45.10(3) 2 5
S3 Dy4 Dy8 135.20(3) . 5
S5 Dy4 Dy8 139.67(3) . 5
S5 Dy4 Dy8 88.29(3) 2 5
S2 Dy4 Dy8 90.10(4) 5 .
S2 Dy4 Dy8 43.37(4) . .
S3 Dy4 Dy8 135.20(3) 2 .
S3 Dy4 Dy8 45.10(3) . .
S5 Dy4 Dy8 88.29(3) . .
S5 Dy4 Dy8 139.67(3) 2 .
Dy8 Dy4 Dy8 119.40(2) 5 .
S2 Dy4 Dy4 44.05(3) 5 5
S2 Dy4 Dy4 44.05(3) . 5
S3 Dy4 Dy4 90.21(2) 2 5
S3 Dy4 Dy4 90.21(2) . 5
S5 Dy4 Dy4 136.53(3) . 5
S5 Dy4 Dy4 136.53(3) 2 5
Dy8 Dy4 Dy4 59.698(12) 5 5
Dy8 Dy4 Dy4 59.698(12) . 5
S2 Dy4 Dy1 135.95(3) 5 .
S2 Dy4 Dy1 135.95(3) . .
S3 Dy4 Dy1 89.79(2) 2 .
S3 Dy4 Dy1 89.79(2) . .
S5 Dy4 Dy1 43.47(3) . .
S5 Dy4 Dy1 43.47(3) 2 .
Dy8 Dy4 Dy1 120.302(12) 5 .
Dy8 Dy4 Dy1 120.302(12) . .
Dy4 Dy4 Dy1 180.0 5 .
S2 Dy4 Cs1 61.46(4) 5 7
S2 Dy4 Cs1 128.52(4) . 7
S3 Dy4 Cs1 124.64(3) 2 7
S3 Dy4 Cs1 55.30(3) . 7
S5 Dy4 Cs1 115.94(3) . 7
S5 Dy4 Cs1 54.28(3) 2 7
Dy8 Dy4 Cs1 92.85(3) 5 7
Dy8 Dy4 Cs1 92.98(3) . 7
Dy4 Dy4 Cs1 95.792(7) 5 7
Dy1 Dy4 Cs1 84.208(7) . 7
S2 Dy4 Cs1 128.53(4) 5 8_455
S2 Dy4 Cs1 61.46(4) . 8_455
S3 Dy4 Cs1 55.30(3) 2 8_455
S3 Dy4 Cs1 124.64(3) . 8_455
S5 Dy4 Cs1 54.28(3) . 8_455
S5 Dy4 Cs1 115.94(3) 2 8_455
Dy8 Dy4 Cs1 92.98(3) 5 8_455
Dy8 Dy4 Cs1 92.85(3) . 8_455
Dy4 Dy4 Cs1 95.792(7) 5 8_455
Dy1 Dy4 Cs1 84.208(7) . 8_455
Cs1 Dy4 Cs1 168.416(13) 7 8_455
S4 Dy5 S1 93.94(5) 7 7
S4 Dy5 S9 88.61(4) 7 8
S1 Dy5 S9 88.25(4) 7 8
S4 Dy5 S3 98.98(4) 7 .
S1 Dy5 S3 97.22(5) 7 .
S9 Dy5 S3 170.28(3) 8 .
S4 Dy5 S6 93.38(5) 7 .
S1 Dy5 S6 170.35(4) 7 .
S9 Dy5 S6 85.64(3) 8 .
S3 Dy5 S6 87.84(4) . .
S4 Dy5 S10 176.61(4) 7 .
S1 Dy5 S10 88.46(4) 7 .
S9 Dy5 S10 89.07(4) 8 .
S3 Dy5 S10 83.07(4) . .
S6 Dy5 S10 83.98(4) . .
S4 Dy5 Dy1 44.09(3) 7 7
S1 Dy5 Dy1 90.79(4) 7 7
S9 Dy5 Dy1 44.53(3) 8 7
S3 Dy5 Dy1 142.82(3) . 7
S6 Dy5 Dy1 90.09(3) . 7
S10 Dy5 Dy1 133.59(4) . 7
S4 Dy5 Dy7 89.79(4) 7 3_545
S1 Dy5 Dy7 43.88(4) 7 3_545
S9 Dy5 Dy7 44.44(3) 8 3_545
S3 Dy5 Dy7 140.85(3) . 3_545
S6 Dy5 Dy7 129.91(3) . 3_545
S10 Dy5 Dy7 90.29(4) . 3_545
Dy1 Dy5 Dy7 59.43(2) 7 3_545
S4 Dy5 Dy2 91.97(4) 7 .
S1 Dy5 Dy2 141.59(4) 7 .
S9 Dy5 Dy2 129.85(3) 8 .
S3 Dy5 Dy2 44.39(3) . .
S6 Dy5 Dy2 44.25(3) . .
S10 Dy5 Dy2 87.62(4) . .
Dy1 Dy5 Dy2 118.69(2) 7 .
Dy7 Dy5 Dy2 173.997(8) 3_545 .
S4 Dy5 Dy5 135.72(3) 7 6
S1 Dy5 Dy5 41.78(3) 7 6
S9 Dy5 Dy5 89.38(2) 8 6
S3 Dy5 Dy5 89.38(2) . 6
S6 Dy5 Dy5 130.53(3) . 6
S10 Dy5 Dy5 46.71(3) . 6
Dy1 Dy5 Dy5 119.042(11) 7 6
Dy7 Dy5 Dy5 59.615(11) 3_545 6
Dy2 Dy5 Dy5 121.930(11) . 6
S4 Dy5 Cs1 56.33(3) 7 7
S1 Dy5 Cs1 66.40(4) 7 7
S9 Dy5 Cs1 132.73(3) 8 7
S3 Dy5 Cs1 56.99(4) . 7
S6 Dy5 Cs1 123.10(3) . 7
S10 Dy5 Cs1 126.97(4) . 7
Dy1 Dy5 Cs1 94.42(3) 7 7
Dy7 Dy5 Cs1 99.72(3) 3_545 7
Dy2 Dy5 Cs1 86.02(3) . 7
Dy5 Dy5 Cs1 95.401(6) 6 7
S8 Dy6 S8 176.73(5) 2_656 .
S8 Dy6 S6 89.41(4) 2_656 2_656
S8 Dy6 S6 88.38(3) . 2_656
S8 Dy6 S6 88.38(3) 2_656 .
S8 Dy6 S6 89.41(4) . .
S6 Dy6 S6 95.06(6) 2_656 .
S8 Dy6 S10 94.87(4) 2_656 .
S8 Dy6 S10 87.44(4) . .
S6 Dy6 S10 175.14(4) 2_656 .
S6 Dy6 S10 87.39(4) . .
S8 Dy6 S10 87.44(4) 2_656 5_656
S8 Dy6 S10 94.87(4) . 5_656
S6 Dy6 S10 87.39(4) 2_656 5_656
S6 Dy6 S10 175.14(4) . 5_656
S10 Dy6 S10 90.49(5) . 5_656
S8 Dy6 Dy6 91.64(3) 2_656 5_656
S8 Dy6 Dy6 91.64(3) . 5_656
S6 Dy6 Dy6 132.47(3) 2_656 5_656
S6 Dy6 Dy6 132.47(3) . 5_656
S10 Dy6 Dy6 45.24(3) . 5_656
S10 Dy6 Dy6 45.24(3) 5_656 5_656
S8 Dy6 Dy3 43.65(3) 2_656 8
S8 Dy6 Dy3 134.06(3) . 8
S6 Dy6 Dy3 92.44(3) 2_656 8
S6 Dy6 Dy3 44.74(3) . 8
S10 Dy6 Dy3 92.25(4) . 8
S10 Dy6 Dy3 131.07(4) 5_656 8
Dy6 Dy6 Dy3 119.634(11) 5_656 8
S8 Dy6 Dy3 134.06(3) 2_656 7_556
S8 Dy6 Dy3 43.65(3) . 7_556
S6 Dy6 Dy3 44.74(3) 2_656 7_556
S6 Dy6 Dy3 92.44(3) . 7_556
S10 Dy6 Dy3 131.07(4) . 7_556
S10 Dy6 Dy3 92.25(4) 5_656 7_556
Dy6 Dy6 Dy3 119.634(11) 5_656 7_556
Dy3 Dy6 Dy3 120.73(2) 8 7_556
S8 Dy6 Dy2 45.56(3) 2_656 2_656
S8 Dy6 Dy2 132.03(3) . 2_656
S6 Dy6 Dy2 43.97(3) 2_656 2_656
S6 Dy6 Dy2 89.83(3) . 2_656
S10 Dy6 Dy2 140.41(4) . 2_656
S10 Dy6 Dy2 89.02(3) 5_656 2_656
Dy6 Dy6 Dy2 122.353(12) 5_656 2_656
Dy3 Dy6 Dy2 59.80(3) 8 2_656
Dy3 Dy6 Dy2 88.50(3) 7_556 2_656
S8 Dy6 Dy2 132.03(3) 2_656 .
S8 Dy6 Dy2 45.56(3) . .
S6 Dy6 Dy2 89.83(3) 2_656 .
S6 Dy6 Dy2 43.97(3) . .
S10 Dy6 Dy2 89.02(3) . .
S10 Dy6 Dy2 140.41(4) 5_656 .
Dy6 Dy6 Dy2 122.353(12) 5_656 .
Dy3 Dy6 Dy2 88.50(3) 8 .
Dy3 Dy6 Dy2 59.80(3) 7_556 .
Dy2 Dy6 Dy2 115.29(2) 2_656 .
S8 Dy6 Dy8 138.97(3) 2_656 .
S8 Dy6 Dy8 43.43(3) . .
S6 Dy6 Dy8 131.54(3) 2_656 .
S6 Dy6 Dy8 90.11(3) . .
S10 Dy6 Dy8 44.11(4) . .
S10 Dy6 Dy8 91.41(4) 5_656 .
Dy6 Dy6 Dy8 60.502(12) 5_656 .
Dy3 Dy6 Dy8 122.67(3) 8 .
Dy3 Dy6 Dy8 86.97(3) 7_556 .
Dy2 Dy6 Dy8 175.461(7) 2_656 .
Dy2 Dy6 Dy8 61.97(2) . .
S1 Dy7 S1 180.0 5_565 .
S1 Dy7 S9 86.30(4) 5_565 6_565
S1 Dy7 S9 93.70(4) . 6_565
S1 Dy7 S9 93.70(4) 5_565 2
S1 Dy7 S9 86.30(4) . 2
S9 Dy7 S9 180.0 6_565 2
S1 Dy7 S9 86.30(4) 5_565 .
S1 Dy7 S9 93.70(4) . .
S9 Dy7 S9 90.71(5) 6_565 .
S9 Dy7 S9 89.29(5) 2 .
S1 Dy7 S9 93.70(4) 5_565 5_565
S1 Dy7 S9 86.30(4) . 5_565
S9 Dy7 S9 89.29(5) 6_565 5_565
S9 Dy7 S9 90.71(5) 2 5_565
S9 Dy7 S9 180.00(3) . 5_565
S1 Dy7 Dy1 90.0 5_565 .
S1 Dy7 Dy1 90.0 . .
S9 Dy7 Dy1 135.35(3) 6_565 .
S9 Dy7 Dy1 44.65(3) 2 .
S9 Dy7 Dy1 44.65(3) . .
S9 Dy7 Dy1 135.35(3) 5_565 .
S1 Dy7 Dy1 90.0 5_565 5_565
S1 Dy7 Dy1 90.0 . 5_565
S9 Dy7 Dy1 44.65(3) 6_565 5_565
S9 Dy7 Dy1 135.35(3) 2 5_565
S9 Dy7 Dy1 135.35(3) . 5_565
S9 Dy7 Dy1 44.65(3) 5_565 5_565
Dy1 Dy7 Dy1 180.0 . 5_565
S1 Dy7 Dy5 137.39(3) 5_565 4
S1 Dy7 Dy5 42.61(3) . 4
S9 Dy7 Dy5 90.15(3) 6_565 4
S9 Dy7 Dy5 89.85(3) 2 4
S9 Dy7 Dy5 136.24(3) . 4
S9 Dy7 Dy5 43.76(3) 5_565 4
Dy1 Dy7 Dy5 120.385(10) . 4
Dy1 Dy7 Dy5 59.615(10) 5_565 4
S1 Dy7 Dy5 42.61(3) 5_565 3_455
S1 Dy7 Dy5 137.39(3) . 3_455
S9 Dy7 Dy5 43.76(3) 6_565 3_455
S9 Dy7 Dy5 136.24(3) 2 3_455
S9 Dy7 Dy5 89.85(3) . 3_455
S9 Dy7 Dy5 90.15(3) 5_565 3_455
Dy1 Dy7 Dy5 120.385(11) . 3_455
Dy1 Dy7 Dy5 59.615(11) 5_565 3_455
Dy5 Dy7 Dy5 119.23(2) 4 3_455
S1 Dy7 Dy5 137.39(3) 5_565 7
S1 Dy7 Dy5 42.61(3) . 7
S9 Dy7 Dy5 136.24(3) 6_565 7
S9 Dy7 Dy5 43.76(3) 2 7
S9 Dy7 Dy5 90.15(3) . 7
S9 Dy7 Dy5 89.85(3) 5_565 7
Dy1 Dy7 Dy5 59.615(11) . 7
Dy1 Dy7 Dy5 120.385(11) 5_565 7
Dy5 Dy7 Dy5 60.77(2) 4 7
Dy5 Dy7 Dy5 180.0 3_455 7
S1 Dy7 Dy5 42.61(3) 5_565 8_455
S1 Dy7 Dy5 137.39(3) . 8_455
S9 Dy7 Dy5 89.85(3) 6_565 8_455
S9 Dy7 Dy5 90.15(3) 2 8_455
S9 Dy7 Dy5 43.76(3) . 8_455
S9 Dy7 Dy5 136.24(3) 5_565 8_455
Dy1 Dy7 Dy5 59.615(11) . 8_455
Dy1 Dy7 Dy5 120.385(11) 5_565 8_455
Dy5 Dy7 Dy5 180.0 4 8_455
Dy5 Dy7 Dy5 60.77(2) 3_455 8_455
Dy5 Dy7 Dy5 119.23(2) 7 8_455
S2 Dy8 S3 89.80(4) . 6
S2 Dy8 S3 89.80(4) . .
S3 Dy8 S3 91.44(6) 6 .
S2 Dy8 S8 97.58(4) . .
S3 Dy8 S8 172.12(4) 6 .
S3 Dy8 S8 85.85(4) . .
S2 Dy8 S8 97.58(4) . 6
S3 Dy8 S8 85.85(4) 6 6
S3 Dy8 S8 172.12(4) . 6
S8 Dy8 S8 95.86(6) . 6
S2 Dy8 S10 173.71(5) . .
S3 Dy8 S10 85.82(3) 6 .
S3 Dy8 S10 85.82(3) . .
S8 Dy8 S10 86.61(4) . .
S8 Dy8 S10 86.61(4) 6 .
S2 Dy8 Dy4 44.55(3) . 5
S3 Dy8 Dy4 45.25(3) 6 5
S3 Dy8 Dy4 91.06(3) . 5
S8 Dy8 Dy4 142.07(3) . 5
S8 Dy8 Dy4 92.27(3) 6 5
S10 Dy8 Dy4 130.92(3) . 5
S2 Dy8 Dy4 44.55(3) . .
S3 Dy8 Dy4 91.06(3) 6 .
S3 Dy8 Dy4 45.25(3) . .
S8 Dy8 Dy4 92.27(3) . .
S8 Dy8 Dy4 142.07(3) 6 .
S10 Dy8 Dy4 130.92(3) . .
Dy4 Dy8 Dy4 60.60(2) 5 .
S2 Dy8 Dy6 139.92(3) . .
S3 Dy8 Dy6 130.16(3) 6 .
S3 Dy8 Dy6 86.55(3) . .
S8 Dy8 Dy6 42.35(3) . .
S8 Dy8 Dy6 89.54(3) 6 .
S10 Dy8 Dy6 44.35(3) . .
Dy4 Dy8 Dy6 174.824(9) 5 .
Dy4 Dy8 Dy6 119.94(2) . .
S2 Dy8 Dy6 139.92(3) . 5_656
S3 Dy8 Dy6 86.55(3) 6 5_656
S3 Dy8 Dy6 130.16(3) . 5_656
S8 Dy8 Dy6 89.54(3) . 5_656
S8 Dy8 Dy6 42.35(3) 6 5_656
S10 Dy8 Dy6 44.35(3) . 5_656
Dy4 Dy8 Dy6 119.94(2) 5 5_656
Dy4 Dy8 Dy6 174.824(9) . 5_656
Dy6 Dy8 Dy6 59.00(2) . 5_656
S2 Dy8 Cs2 66.17(4) . 7_556
S3 Dy8 Cs2 129.59(3) 6 7_556
S3 Dy8 Cs2 129.59(3) . 7_556
S8 Dy8 Cs2 56.79(3) . 7_556
S8 Dy8 Cs2 56.79(3) 6 7_556
S10 Dy8 Cs2 120.12(3) . 7_556
Dy4 Dy8 Cs2 99.09(3) 5 7_556
Dy4 Dy8 Cs2 99.09(3) . 7_556
Dy6 Dy8 Cs2 85.96(3) . 7_556
Dy6 Dy8 Cs2 85.96(3) 5_656 7_556
Dy5 S1 Dy5 96.44(6) 7 4
Dy5 S1 Dy7 93.50(5) 7 .
Dy5 S1 Dy7 93.50(5) 4 .
Dy5 S1 Cs2 131.68(3) 7 .
Dy5 S1 Cs2 131.68(3) 4 .
Dy7 S1 Cs2 81.08(4) . .
Dy5 S1 Cs1 130.36(6) 7 6_565
Dy5 S1 Cs1 76.59(3) 4 6_565
Dy7 S1 Cs1 135.49(3) . 6_565
Cs2 S1 Cs1 74.71(3) . 6_565
Dy5 S1 Cs1 76.59(3) 7 .
Dy5 S1 Cs1 130.36(6) 4 .
Dy7 S1 Cs1 135.49(3) . .
Cs2 S1 Cs1 74.71(3) . .
Cs1 S1 Cs1 72.28(4) 6_565 .
Dy8 S2 Dy4 92.08(4) . 5
Dy8 S2 Dy4 92.08(4) . .
Dy4 S2 Dy4 91.90(6) 5 .
Dy8 S2 Cs1 130.97(4) . 3_445
Dy4 S2 Cs1 81.16(3) 5 3_445
Dy4 S2 Cs1 136.35(6) . 3_445
Dy8 S2 Cs1 130.97(4) . 8_455
Dy4 S2 Cs1 136.35(6) 5 8_455
Dy4 S2 Cs1 81.16(3) . 8_455
Cs1 S2 Cs1 75.21(4) 3_445 8_455
Dy8 S2 Cs2 77.61(4) . 7_556
Dy4 S2 Cs2 133.31(3) 5 7_556
Dy4 S2 Cs2 133.31(3) . 7_556
Cs1 S2 Cs2 72.93(3) 3_445 7_556
Cs1 S2 Cs2 72.93(3) 8_455 7_556
Dy8 S3 Dy4 89.65(3) . .
Dy8 S3 Dy5 97.59(4) . .
Dy4 S3 Dy5 170.03(5) . .
Dy8 S3 Dy2 95.97(5) . .
Dy4 S3 Dy2 94.58(4) . .
Dy5 S3 Dy2 91.50(4) . .
Dy8 S3 Cs1 141.00(4) . 7
Dy4 S3 Cs1 86.36(3) . 7
Dy5 S3 Cs1 83.70(3) . 7
Dy2 S3 Cs1 123.01(4) . 7
Dy5 S4 Dy2 172.63(6) 7 .
Dy5 S4 Dy1 93.57(4) 7 .
Dy2 S4 Dy1 93.54(4) . .
Dy5 S4 Cs1 86.35(4) 7 .
Dy2 S4 Cs1 86.68(4) . .
Dy1 S4 Cs1 145.27(5) . .
Dy1 S5 Dy2 91.17(4) . .
Dy1 S5 Dy3 91.50(5) . .
Dy2 S5 Dy3 90.10(4) . .
Dy1 S5 Dy4 91.73(4) . .
Dy2 S5 Dy4 94.52(4) . .
Dy3 S5 Dy4 174.30(5) . .
Dy1 S5 Cs1 125.35(4) . 8_455
Dy2 S5 Cs1 143.44(4) . 8_455
Dy3 S5 Cs1 87.43(4) . 8_455
Dy4 S5 Cs1 86.87(4) . 8_455
Dy6 S6 Dy5 96.89(5) . .
Dy6 S6 Dy2 93.20(3) . .
Dy5 S6 Dy2 91.55(4) . .
Dy6 S6 Dy3 92.29(4) . 8
Dy5 S6 Dy3 94.88(4) . 8
Dy2 S6 Dy3 170.99(5) . 8
Dy6 S6 Cs1 139.21(4) . .
Dy5 S6 Cs1 123.85(4) . .
Dy2 S6 Cs1 84.60(3) . .
Dy3 S6 Cs1 86.58(3) 8 .
Dy3 S7 Dy2 94.39(5) 7_556 .
Dy3 S7 Dy3 91.33(4) 7_556 .
Dy2 S7 Dy3 92.34(4) . .
Dy3 S7 Cs1 81.76(3) 7_556 2_656
Dy2 S7 Cs1 132.45(4) . 2_656
Dy3 S7 Cs1 134.92(4) . 2_656
Dy3 S7 Cs2 136.68(4) 7_556 .
Dy2 S7 Cs2 128.32(4) . .
Dy3 S7 Cs2 81.28(3) . .
Cs1 S7 Cs2 74.36(3) 2_656 .
Dy3 S7 Cs1 133.39(4) 7_556 .
Dy2 S7 Cs1 75.55(3) . .
Dy3 S7 Cs1 133.71(4) . .
Cs1 S7 Cs1 73.62(4) 2_656 .
Cs2 S7 Cs1 73.03(2) . .
Dy6 S8 Dy3 93.71(4) . 7_556
Dy6 S8 Dy8 94.22(4) . .
Dy3 S8 Dy8 170.66(5) 7_556 .
Dy6 S8 Dy2 91.80(4) . .
Dy3 S8 Dy2 90.31(4) 7_556 .
Dy8 S8 Dy2 94.36(4) . .
Dy6 S8 Cs2 126.56(4) . 7_556
Dy3 S8 Cs2 86.54(4) 7_556 7_556
Dy8 S8 Cs2 84.77(4) . 7_556
Dy2 S8 Cs2 141.63(5) . 7_556
Dy5 S9 Dy1 90.95(4) 8_455 .
Dy5 S9 Dy7 91.80(4) 8_455 .
Dy1 S9 Dy7 90.01(4) . .
Dy5 S9 Dy3 95.49(4) 8_455 .
Dy1 S9 Dy3 90.48(5) . .
Dy7 S9 Dy3 172.68(5) . .
Dy5 S9 Cs2 132.81(4) 8_455 .
Dy1 S9 Cs2 136.17(4) . .
Dy7 S9 Cs2 86.75(4) . .
Dy3 S9 Cs2 87.84(4) . .
Dy8 S10 Dy6 91.53(4) . .
Dy8 S10 Dy6 91.53(4) . 5_656
Dy6 S10 Dy6 89.51(5) . 5_656
Dy8 S10 Dy5 93.41(4) . 6
Dy6 S10 Dy5 174.86(6) . 6
Dy6 S10 Dy5 91.74(3) 5_656 6
Dy8 S10 Dy5 93.41(4) . .
Dy6 S10 Dy5 91.74(3) . .
Dy6 S10 Dy5 174.86(6) 5_656 .
Dy5 S10 Dy5 86.59(5) 6 .
Cs2 Cl1 Cs2 180.000(18) . 5_666
Cs2 Cl1 Cs1 90.588(11) . .
Cs2 Cl1 Cs1 89.412(11) 5_666 .
Cs2 Cl1 Cs1 89.412(11) . 5_666
Cs2 Cl1 Cs1 90.588(11) 5_666 5_666
Cs1 Cl1 Cs1 180.0 . 5_666
Cs2 Cl1 Cs1 90.588(11) . 6_565
Cs2 Cl1 Cs1 89.412(11) 5_666 6_565
Cs1 Cl1 Cs1 89.56(3) . 6_565
Cs1 Cl1 Cs1 90.44(3) 5_666 6_565
Cs2 Cl1 Cs1 89.412(11) . 2_656
Cs2 Cl1 Cs1 90.588(11) 5_666 2_656
Cs1 Cl1 Cs1 90.44(3) . 2_656
Cs1 Cl1 Cs1 89.56(3) 5_666 2_656
Cs1 Cl1 Cs1 180.000(9) 6_565 2_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cs1 Cl1 3.4030(9) .
Cs1 S5 3.5924(15) 8
Cs1 S4 3.5978(18) .
Cs1 S6 3.6125(17) .
Cs1 S3 3.6400(19) 7
Cs1 S7 3.9267(16) 2_656
Cs1 S2 3.9280(16) 3
Cs2 Cl1 3.3936(15) .
Cs2 S9 3.5844(15) .
Cs2 S9 3.5844(15) 6_565
Cs2 S8 3.6898(14) 4_556
Cs2 S8 3.6898(14) 7_556
Cs2 S1 3.894(2) .
Cs2 S7 3.9845(17) 6_565
Cs2 S7 3.9845(17) .
Dy1 S4 2.7074(17) .
Dy1 S4 2.7074(17) 2
Dy1 S5 2.7100(14) 2
Dy1 S5 2.7100(13) .
Dy1 S9 2.7240(13) .
Dy1 S9 2.7240(13) 2
Dy1 Dy7 3.8763(12) .
Dy1 Dy5 3.8838(9) 7
Dy1 Dy5 3.8838(9) 8_455
Dy1 Dy2 3.8901(10) 2
Dy1 Dy2 3.8900(10) .
Dy1 Dy3 3.9165(16) 2
Dy2 S4 2.6313(14) .
Dy2 S7 2.6936(14) .
Dy2 S5 2.7361(17) .
Dy2 S6 2.7564(16) .
Dy2 S3 2.7630(13) .
Dy2 S8 2.8317(14) .
Dy2 Dy3 3.8879(9) .
Dy2 Dy5 3.9487(9) .
Dy2 Dy3 3.9490(17) 7_556
Dy2 Dy6 3.9640(10) .
Dy3 S7 2.6887(14) 7_556
Dy3 S7 2.6959(17) .
Dy3 S8 2.7371(13) 7_556
Dy3 S5 2.7575(13) .
Dy3 S6 2.7881(16) 8_455
Dy3 S9 2.7915(13) .
Dy3 Dy3 3.8515(10) 7_556
Dy3 Dy2 3.9490(17) 7_556
Dy3 Dy6 3.9574(9) 7_556
Dy4 S2 2.7147(13) 5
Dy4 S2 2.7147(13) .
Dy4 S3 2.7462(16) 2
Dy4 S3 2.7462(16) .
Dy4 S5 2.7757(13) .
Dy4 S5 2.7757(13) 2
Dy4 Dy8 3.8670(10) 5
Dy4 Dy8 3.8670(10) .
Dy4 Dy4 3.9023(13) 5
Dy5 S4 2.6213(14) 7
Dy5 S1 2.6699(13) 7
Dy5 S9 2.7236(17) 8
Dy5 S3 2.7497(16) .
Dy5 S6 2.7539(14) .
Dy5 S10 2.9033(13) .
Dy5 Dy1 3.8838(9) 7
Dy5 Dy7 3.9361(9) 3_545
Dy5 Dy5 3.9818(13) 6
Dy6 S8 2.6864(17) 2_656
Dy6 S8 2.6864(17) .
Dy6 S6 2.6993(14) 2_656
Dy6 S6 2.6993(14) .
Dy6 S10 2.7809(13) .
Dy6 S10 2.7809(13) 5_656
Dy6 Dy6 3.9161(13) 5_656
Dy6 Dy3 3.9574(9) 8
Dy6 Dy3 3.9574(9) 7_556
Dy6 Dy2 3.9640(10) 2_656
Dy6 Dy8 3.9766(11) .
Dy7 S1 2.734(2) 5_565
Dy7 S1 2.734(2) .
Dy7 S9 2.7573(13) 6_565
Dy7 S9 2.7573(13) 2
Dy7 S9 2.7573(13) .
Dy7 S9 2.7573(13) 5_565
Dy7 Dy1 3.8763(12) 5_565
Dy7 Dy5 3.9361(9) 4
Dy7 Dy5 3.9361(9) 3_455
Dy7 Dy5 3.9361(9) 7
Dy7 Dy5 3.9361(9) 8_455
Dy8 S2 2.657(2) .
Dy8 S3 2.7394(13) 6
Dy8 S3 2.7394(13) .
Dy8 S8 2.7411(13) .
Dy8 S8 2.7411(13) 6
Dy8 S10 2.769(2) .
Dy8 Dy4 3.8670(10) 5
Dy8 Dy6 3.9766(11) 5_656
S1 Dy5 2.6699(13) 7
S1 Dy5 2.6699(13) 4
S2 Dy4 2.7147(13) 5
S2 Cs1 3.9280(15) 3_445
S2 Cs1 3.9280(15) 8_455
S3 Cs1 3.6400(19) 7
S4 Dy5 2.6213(14) 7
S5 Cs1 3.5923(15) 8_455
S6 Dy3 2.7881(16) 8
S7 Dy3 2.6887(14) 7_556
S7 Cs1 3.9267(16) 2_656
S8 Dy3 2.7371(13) 7_556
S8 Cs2 3.6898(14) 7_556
S9 Dy5 2.7236(17) 8_455
S10 Dy6 2.7809(13) 5_656
S10 Dy5 2.9033(13) 6
Cl1 Cs2 3.3936(15) 5_666
Cl1 Cs1 3.4030(9) 5_666
Cl1 Cs1 3.4030(9) 6_565
Cl1 Cs1 3.4030(9) 2_656
