#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:57:32 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179401 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/98/4329839.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4329839
loop_
_publ_author_name
'Christian Hering'
'Mathias Lehmann'
'Axel Schulz'
'Alexander Villinger'
_publ_contact_author_address
;
Universität Rostock
Institut für Chemie
Abteilung für Anorganische Chemie
Albert-Einstein-Strasse 3a 
18059 Rostock
Bundesrepublik Deutschland
;
_publ_contact_author_email
;
axel.schulz@uni-rostock.de, alexander.villinger@uni-rostock.de'
;
_publ_contact_author_fax         '+49 (0)381/498-6382'
_publ_contact_author_name        'Axel Schulz'
_publ_contact_author_phone       '+49 (0)381/498-6400 or 6403'
_publ_section_title
;
 Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New
 Route To Stibinostibonium Cations
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8212
_journal_page_last               8224
_journal_paper_doi               10.1021/ic300770b
_journal_volume                  51
_journal_year                    2012
_chemical_formula_moiety         'C27 H34 Cl0.07 N6.79 Sb Si'
_chemical_formula_sum            'C27 H34 Cl0.07 N6.79 Sb Si'
_chemical_formula_weight         605.99
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_author_name               'Villinger, A.'
_audit_creation_method           SHELXL-97
_cell_angle_alpha                72.4500(10)
_cell_angle_beta                 71.9320(10)
_cell_angle_gamma                87.8540(10)
_cell_formula_units_Z            2
_cell_length_a                   10.7944(2)
_cell_length_b                   11.6711(2)
_cell_length_c                   12.4607(2)
_cell_measurement_reflns_used    8937
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      56.943
_cell_measurement_theta_min      5.241
_cell_volume                     1420.23(4)
_computing_cell_refinement       'Bruker Apex V7.51A'
_computing_data_collection       'Bruker Apex V7.51A'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'ORTEP-3v2.01 (Farrugia, 1997)'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Bruker Apex Kappa II-CCD-diffractometer'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0337
_diffrn_reflns_av_sigmaI/netI    0.0511
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            30855
_diffrn_reflns_theta_full        32.50
_diffrn_reflns_theta_max         32.50
_diffrn_reflns_theta_min         3.22
_exptl_absorpt_coefficient_mu    1.048
_exptl_absorpt_correction_T_max  0.8672
_exptl_absorpt_correction_T_min  0.8178
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2004)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.417
_exptl_crystal_description       block
_exptl_crystal_F_000             619
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.14
_refine_diff_density_max         0.528
_refine_diff_density_min         -0.430
_refine_diff_density_rms         0.088
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     338
_refine_ls_number_reflns         10109
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.029
_refine_ls_R_factor_all          0.0611
_refine_ls_R_factor_gt           0.0364
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0346P)²+0.1244P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0691
_refine_ls_wR_factor_ref         0.0772
_reflns_number_gt                7691
_reflns_number_total             10109
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ic300770b_si_001_11.cif
_cod_data_source_block           ch176
_cod_database_code               4329839
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 0.354162(13) 0.386635(11) 0.172291(12) 0.02654(5) Uani 1 1 d . . .
Si1 Si 0.08386(5) 0.27643(5) 0.14723(5) 0.02586(11) Uani 1 1 d . . .
N1 N 0.22280(14) 0.25497(13) 0.19775(13) 0.0212(3) Uani 1 1 d . A .
N2 N 0.34304(19) 0.48037(17) 0.00096(16) 0.0381(4) Uani 1 1 d . A .
N3 N 0.30051(19) 0.57615(18) -0.01973(17) 0.0412(5) Uani 1 1 d . . .
N4 N 0.2612(2) 0.6688(2) -0.0482(2) 0.0637(7) Uani 1 1 d . A .
N5 N 0.2340(5) 0.5092(4) 0.2394(5) 0.0490(8) Uani 0.930(4) 1 d P A 1
N6 N 0.2802(3) 0.57068(19) 0.2847(2) 0.0524(7) Uani 0.930(4) 1 d P A 1
N7 N 0.3154(4) 0.6302(2) 0.3271(3) 0.0859(11) Uani 0.930(4) 1 d P A 1
Cl1 Cl 0.234(3) 0.5403(17) 0.248(2) 0.0490(8) Uani 0.070(4) 1 d P A 2
C1 C 0.25210(16) 0.13899(15) 0.26412(15) 0.0192(3) Uani 1 1 d . A 3
C2 C 0.26628(17) 0.12247(16) 0.37672(16) 0.0222(4) Uani 1 1 d . A 3
C3 C 0.28710(19) 0.00785(17) 0.44427(16) 0.0266(4) Uani 1 1 d . A 3
H3 H 0.2942 -0.0028 0.5207 0.032 Uiso 1 1 calc R A 3
C4 C 0.29745(19) -0.08923(17) 0.40235(17) 0.0269(4) Uani 1 1 d . A 3
H4 H 0.3086 -0.1670 0.4501 0.032 Uiso 1 1 calc R A 3
C5 C 0.29137(18) -0.07206(16) 0.28930(16) 0.0228(4) Uani 1 1 d . A 3
H5 H 0.3013 -0.1387 0.2592 0.027 Uiso 1 1 calc R A 3
C6 C 0.27113(16) 0.04004(16) 0.21821(15) 0.0196(3) Uani 1 1 d . A 3
C7 C 0.26678(19) 0.22187(17) 0.43007(16) 0.0245(4) Uani 1 1 d . A 3
C8 C 0.38616(19) 0.26153(18) 0.43523(17) 0.0271(4) Uani 1 1 d . A 3
C9 C 0.3859(2) 0.3428(2) 0.49721(19) 0.0375(5) Uani 1 1 d . A 3
H9 H 0.4668 0.3711 0.4982 0.045 Uiso 1 1 calc R A 3
C10 C 0.2719(2) 0.3835(2) 0.5572(2) 0.0433(6) Uani 1 1 d . A 3
C11 C 0.1548(2) 0.3445(2) 0.5514(2) 0.0396(5) Uani 1 1 d . A 3
H11 H 0.0758 0.3735 0.5909 0.048 Uiso 1 1 calc R A 3
C12 C 0.1499(2) 0.26417(18) 0.48952(17) 0.0303(4) Uani 1 1 d . A 3
C13 C 0.5144(2) 0.2139(2) 0.37858(19) 0.0342(5) Uani 1 1 d . A 3
H13A H 0.5860 0.2734 0.3588 0.051 Uiso 1 1 calc R A 3
H13B H 0.5117 0.1986 0.3062 0.051 Uiso 1 1 calc R A 3
H13C H 0.5285 0.1387 0.4341 0.051 Uiso 1 1 calc R A 3
C14 C 0.2746(3) 0.4669(3) 0.6293(3) 0.0701(9) Uani 1 1 d . A 3
H14A H 0.3544 0.4572 0.6520 0.105 Uiso 1 1 calc R A 3
H14B H 0.1982 0.4469 0.7007 0.105 Uiso 1 1 calc R A 3
H14C H 0.2728 0.5505 0.5816 0.105 Uiso 1 1 calc R A 3
C15 C 0.0204(2) 0.2207(2) 0.4900(2) 0.0407(5) Uani 1 1 d . A 3
H15A H -0.0500 0.2549 0.5401 0.061 Uiso 1 1 calc R A 3
H15B H 0.0110 0.1326 0.5214 0.061 Uiso 1 1 calc R A 3
H15C H 0.0158 0.2461 0.4090 0.061 Uiso 1 1 calc R A 3
C16 C 0.27800(17) 0.04786(16) 0.09410(15) 0.0205(3) Uani 1 1 d . A 3
C17 C 0.19334(17) -0.02541(16) 0.07277(16) 0.0226(4) Uani 1 1 d . A 3
C18 C 0.20668(19) -0.02045(17) -0.04328(17) 0.0263(4) Uani 1 1 d . A 3
H18 H 0.1479 -0.0689 -0.0569 0.032 Uiso 1 1 calc R A 3
C19 C 0.30260(19) 0.05264(18) -0.13958(16) 0.0265(4) Uani 1 1 d . A 3
C20 C 0.38869(18) 0.12061(17) -0.11720(16) 0.0247(4) Uani 1 1 d . A 3
H20 H 0.4562 0.1702 -0.1820 0.030 Uiso 1 1 calc R A 3
C21 C 0.37935(17) 0.11854(16) -0.00246(16) 0.0224(4) Uani 1 1 d . A 3
C22 C 0.0894(2) -0.11526(19) 0.17012(18) 0.0312(4) Uani 1 1 d . A 3
H22A H 0.0107 -0.1141 0.1465 0.047 Uiso 1 1 calc R A 3
H22B H 0.0684 -0.0935 0.2435 0.047 Uiso 1 1 calc R A 3
H22C H 0.1221 -0.1962 0.1831 0.047 Uiso 1 1 calc R A 3
C23 C 0.3161(2) 0.0562(2) -0.26486(18) 0.0385(5) Uani 1 1 d . A 3
H23A H 0.3017 -0.0254 -0.2669 0.058 Uiso 1 1 calc R A 3
H23B H 0.4040 0.0885 -0.3168 0.058 Uiso 1 1 calc R A 3
H23C H 0.2513 0.1079 -0.2922 0.058 Uiso 1 1 calc R A 3
C24 C 0.48495(18) 0.18835(18) 0.01204(17) 0.0270(4) Uani 1 1 d . A 3
H24A H 0.5708 0.1667 -0.0303 0.040 Uiso 1 1 calc R A 3
H24B H 0.4760 0.1688 0.0964 0.040 Uiso 1 1 calc R A 3
H24C H 0.4766 0.2748 -0.0205 0.040 Uiso 1 1 calc R A 3
C25 C -0.0393(2) 0.1495(2) 0.2397(2) 0.0378(5) Uani 1 1 d . A 3
H25A H -0.0197 0.0814 0.2078 0.057 Uiso 1 1 calc R A 3
H25B H -0.1265 0.1753 0.2387 0.057 Uiso 1 1 calc R A 3
H25C H -0.0366 0.1250 0.3214 0.057 Uiso 1 1 calc R A 3
C26 C 0.1170(2) 0.2901(2) -0.01166(18) 0.0362(5) Uani 1 1 d . A 3
H26A H 0.1859 0.3535 -0.0604 0.054 Uiso 1 1 calc R A 3
H26B H 0.0373 0.3105 -0.0334 0.054 Uiso 1 1 calc R A 3
H26C H 0.1454 0.2134 -0.0250 0.054 Uiso 1 1 calc R A 3
C27 C 0.0087(2) 0.4167(2) 0.1709(2) 0.0396(5) Uani 1 1 d . A 3
H27A H -0.0054 0.4146 0.2531 0.059 Uiso 1 1 calc R A 3
H27B H -0.0752 0.4227 0.1551 0.059 Uiso 1 1 calc R A 3
H27C H 0.0671 0.4867 0.1170 0.059 Uiso 1 1 calc R A 3
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N1 Sb1 N5 101.55(14)
N1 Sb1 N2 92.93(7)
N5 Sb1 N2 89.24(16)
N1 Sb1 Cl1 107.2(6)
N5 Sb1 Cl1 5.7(7)
N2 Sb1 Cl1 89.7(7)
N1 Si1 C26 115.33(9)
N1 Si1 C25 108.67(8)
C26 Si1 C25 109.23(11)
N1 Si1 C27 108.89(9)
C26 Si1 C27 107.31(10)
C25 Si1 C27 107.09(11)
C1 N1 Si1 122.63(12)
C1 N1 Sb1 112.34(11)
Si1 N1 Sb1 125.03(8)
N3 N2 Sb1 121.67(17)
N4 N3 N2 175.0(3)
N6 N5 Sb1 117.0(3)
N7 N6 N5 175.8(4)
C2 C1 C6 118.29(15)
C2 C1 N1 119.96(16)
C6 C1 N1 121.72(15)
C3 C2 C1 119.88(17)
C3 C2 C7 115.54(15)
C1 C2 C7 124.52(16)
C4 C3 C2 121.42(17)
C4 C3 H3 119.3
C2 C3 H3 119.3
C3 C4 C5 118.89(17)
C3 C4 H4 120.6
C5 C4 H4 120.6
C4 C5 C6 122.04(17)
C4 C5 H5 119.0
C6 C5 H5 119.0
C5 C6 C1 119.20(16)
C5 C6 C16 116.28(16)
C1 C6 C16 124.45(15)
C12 C7 C8 119.04(18)
C12 C7 C2 121.46(17)
C8 C7 C2 118.88(17)
C9 C8 C7 119.43(18)
C9 C8 C13 119.14(18)
C7 C8 C13 121.39(18)
C10 C9 C8 122.0(2)
C10 C9 H9 119.0
C8 C9 H9 119.0
C9 C10 C11 118.2(2)
C9 C10 C14 120.7(2)
C11 C10 C14 121.1(2)
C10 C11 C12 122.0(2)
C10 C11 H11 119.0
C12 C11 H11 119.0
C11 C12 C7 119.24(19)
C11 C12 C15 119.99(19)
C7 C12 C15 120.73(19)
C21 C16 C17 118.79(16)
C21 C16 C6 119.95(15)
C17 C16 C6 120.85(16)
C18 C17 C16 119.43(17)
C18 C17 C22 116.67(16)
C16 C17 C22 123.85(16)
C19 C18 C17 122.30(17)
C19 C18 H18 118.9
C17 C18 H18 118.9
C18 C19 C20 117.74(17)
C18 C19 C23 121.54(18)
C20 C19 C23 120.70(18)
C19 C20 C21 122.05(17)
C19 C20 H20 119.0
C21 C20 H20 119.0
C20 C21 C16 119.56(16)
C20 C21 C24 117.39(16)
C16 C21 C24 122.96(16)
Si1 C25 H25A 109.5
Si1 C25 H25B 109.5
Si1 C25 H25C 109.5
Si1 C26 H26A 109.5
Si1 C26 H26B 109.5
Si1 C26 H26C 109.5
Si1 C27 H27A 109.5
Si1 C27 H27B 109.5
Si1 C27 H27C 109.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Sb1 N1 2.0156(15)
Sb1 N5 2.082(4)
Sb1 N2 2.1236(18)
Sb1 Cl1 2.421(18)
Si1 N1 1.7806(15)
Si1 C26 1.857(2)
Si1 C25 1.859(2)
Si1 C27 1.863(2)
N1 C1 1.439(2)
N2 N3 1.178(3)
N3 N4 1.141(3)
N5 N6 1.237(6)
N6 N7 1.128(4)
C1 C2 1.413(2)
C1 C6 1.418(2)
C2 C3 1.402(2)
C2 C7 1.502(3)
C3 C4 1.371(3)
C3 H3 0.9500
C4 C5 1.384(3)
C4 H4 0.9500
C5 C6 1.394(2)
C5 H5 0.9500
C6 C16 1.500(2)
C7 C12 1.407(3)
C7 C8 1.412(3)
C8 C9 1.392(3)
C8 C13 1.516(3)
C9 C10 1.377(3)
C9 H9 0.9500
C10 C11 1.389(3)
C10 C14 1.517(3)
C11 C12 1.394(3)
C11 H11 0.9500
C12 C15 1.502(3)
C13 H13A 0.9800
C13 H13B 0.9800
C13 H13C 0.9800
C14 H14A 0.9800
C14 H14B 0.9800
C14 H14C 0.9800
C15 H15A 0.9800
C15 H15B 0.9800
C15 H15C 0.9800
C16 C21 1.406(2)
C16 C17 1.408(2)
C17 C18 1.392(3)
C17 C22 1.519(3)
C18 C19 1.385(3)
C18 H18 0.9500
C19 C20 1.386(3)
C19 C23 1.510(3)
C20 C21 1.395(3)
C20 H20 0.9500
C21 C24 1.511(3)
C22 H22A 0.9800
C22 H22B 0.9800
C22 H22C 0.9800
C23 H23A 0.9800
C23 H23B 0.9800
C23 H23C 0.9800
C24 H24A 0.9800
C24 H24B 0.9800
C24 H24C 0.9800
C25 H25A 0.9800
C25 H25B 0.9800
C25 H25C 0.9800
C26 H26A 0.9800
C26 H26B 0.9800
C26 H26C 0.9800
C27 H27A 0.9800
C27 H27B 0.9800
C27 H27C 0.9800
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C26 Si1 N1 C1 -101.16(16)
C25 Si1 N1 C1 21.84(17)
C27 Si1 N1 C1 138.17(15)
C26 Si1 N1 Sb1 79.81(13)
C25 Si1 N1 Sb1 -157.19(11)
C27 Si1 N1 Sb1 -40.86(13)
N5 Sb1 N1 C1 -125.56(19)
N2 Sb1 N1 C1 144.62(12)
Cl1 Sb1 N1 C1 -124.8(7)
N5 Sb1 N1 Si1 53.56(18)
N2 Sb1 N1 Si1 -36.26(11)
Cl1 Sb1 N1 Si1 54.3(7)
N1 Sb1 N2 N3 114.07(18)
N5 Sb1 N2 N3 12.5(2)
Cl1 Sb1 N2 N3 6.8(6)
Sb1 N2 N3 N4 179(100)
N1 Sb1 N5 N6 148.9(3)
N2 Sb1 N5 N6 -118.2(4)
Cl1 Sb1 N5 N6 -24(8)
Sb1 N5 N6 N7 177(100)
Si1 N1 C1 C2 -123.41(16)
Sb1 N1 C1 C2 55.73(19)
Si1 N1 C1 C6 58.4(2)
Sb1 N1 C1 C6 -122.45(15)
C6 C1 C2 C3 -5.5(3)
N1 C1 C2 C3 176.21(16)
C6 C1 C2 C7 171.56(17)
N1 C1 C2 C7 -6.7(3)
C1 C2 C3 C4 1.7(3)
C7 C2 C3 C4 -175.70(18)
C2 C3 C4 C5 2.1(3)
C3 C4 C5 C6 -2.0(3)
C4 C5 C6 C1 -2.0(3)
C4 C5 C6 C16 175.01(17)
C2 C1 C6 C5 5.7(2)
N1 C1 C6 C5 -176.11(16)
C2 C1 C6 C16 -171.06(16)
N1 C1 C6 C16 7.1(3)
C3 C2 C7 C12 -99.9(2)
C1 C2 C7 C12 82.9(2)
C3 C2 C7 C8 71.0(2)
C1 C2 C7 C8 -106.2(2)
C12 C7 C8 C9 -1.0(3)
C2 C7 C8 C9 -172.15(18)
C12 C7 C8 C13 176.64(18)
C2 C7 C8 C13 5.5(3)
C7 C8 C9 C10 2.0(3)
C13 C8 C9 C10 -175.7(2)
C8 C9 C10 C11 -2.2(4)
C8 C9 C10 C14 176.7(2)
C9 C10 C11 C12 1.5(4)
C14 C10 C11 C12 -177.4(2)
C10 C11 C12 C7 -0.6(3)
C10 C11 C12 C15 177.5(2)
C8 C7 C12 C11 0.3(3)
C2 C7 C12 C11 171.23(18)
C8 C7 C12 C15 -177.71(18)
C2 C7 C12 C15 -6.8(3)
C5 C6 C16 C21 -113.42(19)
C1 C6 C16 C21 63.4(2)
C5 C6 C16 C17 59.2(2)
C1 C6 C16 C17 -124.01(19)
C21 C16 C17 C18 -4.0(3)
C6 C16 C17 C18 -176.70(16)
C21 C16 C17 C22 173.41(17)
C6 C16 C17 C22 0.7(3)
C16 C17 C18 C19 1.4(3)
C22 C17 C18 C19 -176.27(18)
C17 C18 C19 C20 1.3(3)
C17 C18 C19 C23 179.60(19)
C18 C19 C20 C21 -1.2(3)
C23 C19 C20 C21 -179.52(18)
C19 C20 C21 C16 -1.5(3)
C19 C20 C21 C24 175.14(17)
C17 C16 C21 C20 4.1(3)
C6 C16 C21 C20 176.86(16)
C17 C16 C21 C24 -172.37(16)
C6 C16 C21 C24 0.4(3)
