#------------------------------------------------------------------------------
#$Date: 2025-01-26 11:50:00 +0200 (Sun, 26 Jan 2025) $
#$Revision: 297473 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/04/4340411.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4340411
loop_
_publ_author_name
'Akashi, Haruo'
'Isobe, Kiyoshi'
'Shibahara, Takashi'
_publ_section_title
;
 Synthesis and characterization of a twin Cubane-type
 molybdenum-rhodium-sulfur cluster, [{Mo3RhCp*S4(H2O)7(O)}2]8+.
 X-ray structure of [{Mo3RhCpS4(H2O7O}2](CH3C6H4SO3)(8).14H2O.
;
_journal_coden_ASTM              INOCAJ
_journal_issue                   10
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3494
_journal_page_last               3498
_journal_paper_doi               10.1021/ic048733y
_journal_volume                  44
_journal_year                    2005
_chemical_formula_moiety         'C76 H142 Mo6 O54 Rh2 S16'
_chemical_formula_sum            'C76 H142 Mo6 O54 Rh2 S16'
_chemical_formula_weight         3214.34
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                63.704(3)
_cell_angle_beta                 78.688(2)
_cell_angle_gamma                81.038(2)
_cell_formula_units_Z            1
_cell_length_a                   12.2631(8)
_cell_length_b                   15.911(1)
_cell_length_c                   17.389(3)
_cell_measurement_reflns_used    7019
_cell_measurement_temperature    93.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.1
_cell_volume                     2973.5(6)
_computing_cell_refinement       CRYSTALCLEAR
_computing_data_collection       CRYSTALCLEAR
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.6.0'
_computing_structure_refinement  CRYSTALS
_computing_structure_solution    SIR92
_diffrn_detector_area_resol_mean 7.32
_diffrn_measured_fraction_theta_full 0.9960
_diffrn_measured_fraction_theta_max 0.9861
_diffrn_measurement_device_type  'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method       ω
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.073
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            33644
_diffrn_reflns_theta_full        25.75
_diffrn_reflns_theta_max         27.48
_exptl_absorpt_coefficient_mu    1.249
_exptl_absorpt_correction_T_max  0.939
_exptl_absorpt_correction_T_min  0.695
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.795
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1628.00
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.61
_refine_diff_density_min         -3.49
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.992
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     737
_refine_ls_number_reflns         11328
_refine_ls_R_factor_gt           0.0610
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[0.0010Fo² + 1.0000σ(Fo²) + 0.5000]/(4Fo²)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1630
_reflns_number_gt                7661
_reflns_number_total             13440
_reflns_threshold_expression     F²>2.0σ(F²)
_cod_data_source_file            ic048733ysi20040923_125311.cif
_cod_data_source_block           010214B
_cod_depositor_comments
;

2025-01-22
Z value and formula fixed to values more according to usual
chemical conventions.                 miguel
;
_cod_original_formula_weight         1607.17
_cod_original_formula_moiety         'C38 H71 Mo3 O27 Rh1 S8'
_cod_original_formula_units_Z            2
_cod_original_cell_volume        2973.5(5)
_cod_original_formula_sum        'C38 H71 Mo3 O27 Rh1 S8'
_cod_database_code               4340411
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +X,+Y,+Z
2 -X,-Y,-Z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Rh(1) Rh 0.01465(5) 0.18656(4) 0.63249(4) 0.0137(2) Uani 1.00 1 d .
Mo(1) Mo 0.01154(5) 0.37297(5) 0.46407(4) 0.0129(2) Uani 1.00 1 d .
Mo(2) Mo 0.21417(5) 0.26746(5) 0.51156(4) 0.0129(2) Uani 1.00 1 d .
Mo(3) Mo 0.09712(5) 0.37460(5) 0.59911(4) 0.0128(2) Uani 1.00 1 d .
S(1) S 0.1802(1) 0.4324(1) 0.4544(1) 0.0145(5) Uani 1.00 1 d .
S(2) S 0.0679(1) 0.2145(1) 0.4839(1) 0.0152(5) Uani 1.00 1 d .
S(3) S 0.1808(1) 0.2175(1) 0.6613(1) 0.0146(5) Uani 1.00 1 d .
S(4) S -0.0809(1) 0.3395(1) 0.6034(1) 0.0140(5) Uani 1.00 1 d .
S(5) S 0.2638(2) 0.7438(1) -0.3246(1) 0.0183(5) Uani 1.00 1 d .
S(6) S 0.4775(2) 1.0366(1) -0.3047(1) 0.0173(5) Uani 1.00 1 d .
S(7) S 0.2726(2) 0.5643(1) 0.2151(1) 0.0201(5) Uani 1.00 1 d .
S(8) S 0.7893(2) 0.7544(1) 0.0996(1) 0.0207(5) Uani 1.00 1 d .
O(1) O -0.1446(4) 0.3397(4) 0.4441(4) 0.019(1) Uani 1.00 1 d .
O(2) O 0.0514(4) 0.4009(4) 0.3260(3) 0.017(1) Uani 1.00 1 d .
O(3) O 0.2997(4) 0.1306(4) 0.5357(4) 0.021(1) Uani 1.00 1 d .
O(4) O 0.3796(4) 0.2901(4) 0.5260(4) 0.017(1) Uani 1.00 1 d .
O(5) O 0.2991(4) 0.2966(4) 0.3842(3) 0.016(1) Uani 1.00 1 d .
O(6) O 0.0346(4) 0.3459(4) 0.7360(3) 0.018(1) Uani 1.00 1 d .
O(7) O 0.0538(4) 0.5014(4) 0.5785(3) 0.018(1) Uani 1.00 1 d .
O(8) O 0.2472(4) 0.4049(4) 0.6307(3) 0.014(1) Uani 1.00 1 d .
O(9) O 0.3114(5) 0.6475(4) -0.3049(4) 0.022(2) Uani 1.00 1 d .
O(10) O 0.1630(5) 0.7642(4) -0.3646(4) 0.022(2) Uani 1.00 1 d .
O(11) O 0.3454(5) 0.8121(4) -0.3755(4) 0.024(2) Uani 1.00 1 d .
O(12) O 0.4824(4) 1.1384(4) -0.3413(4) 0.020(1) Uani 1.00 1 d .
O(13) O 0.3790(5) 1.0129(4) -0.3231(4) 0.024(2) Uani 1.00 1 d .
O(14) O 0.5801(5) 0.9889(4) -0.3299(4) 0.023(2) Uani 1.00 1 d .
O(15) O 0.2910(5) 0.6422(4) 0.2315(4) 0.024(2) Uani 1.00 1 d .
O(16) O 0.1525(5) 0.5552(4) 0.2222(4) 0.026(2) Uani 1.00 1 d .
O(17) O 0.3288(5) 0.4764(4) 0.2689(4) 0.023(2) Uani 1.00 1 d .
O(18) O 0.8458(5) 0.6637(4) 0.1500(4) 0.026(2) Uani 1.00 1 d .
O(19) O 0.8394(5) 0.8318(5) 0.0957(4) 0.028(2) Uani 1.00 1 d .
O(20) O 0.6681(5) 0.7561(5) 0.1266(4) 0.031(2) Uani 1.00 1 d .
O(21) O 0.8788(5) 0.4644(4) 0.2362(4) 0.027(2) Uani 1.00 1 d .
O(22) O 0.5859(4) 0.7142(4) 0.2919(4) 0.020(1) Uani 1.00 1 d .
O(23) O 0.4229(5) 0.5895(4) 0.3567(4) 0.025(2) Uani 1.00 1 d .
O(24) O 0.5550(5) 0.8188(5) -0.3442(4) 0.029(2) Uani 1.00 1 d .
O(25) O 0.3088(5) 0.9945(5) -0.5088(4) 0.030(2) Uani 1.00 1 d .
O(26) O -0.3330(4) 0.4331(4) 0.4803(4) 0.022(2) Uani 1.00 1 d .
O(27) O 0.4871(4) 0.5930(4) -0.4008(4) 0.021(1) Uani 1.00 1 d .
C(1) C 0.0185(7) 0.0565(6) 0.7514(5) 0.019(2) Uani 1.00 1 d .
C(2) C 0.0155(6) 0.0343(5) 0.6817(5) 0.018(2) Uani 1.00 1 d .
C(3) C -0.0895(6) 0.0788(5) 0.6473(5) 0.017(2) Uani 1.00 1 d .
C(4) C -0.1475(7) 0.1273(6) 0.6969(5) 0.021(2) Uani 1.00 1 d .
C(5) C -0.0794(6) 0.1159(6) 0.7608(5) 0.018(2) Uani 1.00 1 d .
C(6) C 0.1037(7) 0.0168(6) 0.8122(6) 0.025(2) Uani 1.00 1 d .
C(7) C 0.0961(7) -0.0290(6) 0.6519(6) 0.023(2) Uani 1.00 1 d .
C(8) C -0.1360(7) 0.0679(7) 0.5794(6) 0.027(2) Uani 1.00 1 d .
C(9) C -0.2611(6) 0.1767(6) 0.6876(6) 0.022(2) Uani 1.00 1 d .
C(10) C -0.1072(7) 0.1517(7) 0.8292(6) 0.027(2) Uani 1.00 1 d .
C(11) C 0.2223(6) 0.7534(6) -0.2254(5) 0.016(2) Uani 1.00 1 d .
C(12) C 0.1269(7) 0.7107(6) -0.1708(6) 0.022(2) Uani 1.00 1 d .
C(13) C 0.0969(7) 0.7157(6) -0.0922(6) 0.025(2) Uani 1.00 1 d .
C(14) C 0.1572(7) 0.7636(7) -0.0663(6) 0.026(2) Uani 1.00 1 d .
C(15) C 0.2515(7) 0.8037(6) -0.1205(5) 0.018(2) Uani 1.00 1 d .
C(16) C 0.2839(6) 0.8010(6) -0.2009(5) 0.018(2) Uani 1.00 1 d .
C(17) C 0.1206(9) 0.7699(8) 0.0191(6) 0.035(3) Uani 1.00 1 d .
C(18) C 0.4632(6) 0.9937(6) -0.1913(5) 0.016(2) Uani 1.00 1 d .
C(19) C 0.3765(6) 1.0308(6) -0.1487(5) 0.018(2) Uani 1.00 1 d .
C(20) C 0.3582(7) 0.9938(5) -0.0590(5) 0.017(2) Uani 1.00 1 d .
C(21) C 0.4305(6) 0.9180(6) -0.0100(5) 0.019(2) Uani 1.00 1 d .
C(22) C 0.5175(6) 0.8830(6) -0.0542(6) 0.020(2) Uani 1.00 1 d .
C(23) C 0.5350(6) 0.9192(6) -0.1439(6) 0.020(2) Uani 1.00 1 d .
C(24) C 0.4092(7) 0.8770(7) 0.0874(6) 0.025(2) Uani 1.00 1 d .
C(25) C 0.8070(6) 0.7628(6) -0.0076(5) 0.021(2) Uani 1.00 1 d .
C(26) C 0.8315(7) 0.8485(6) -0.0788(6) 0.022(2) Uani 1.00 1 d .
C(27) C 0.8388(7) 0.8538(6) -0.1608(6) 0.024(2) Uani 1.00 1 d .
C(28) C 0.8221(7) 0.7783(6) -0.1758(6) 0.023(2) Uani 1.00 1 d .
C(29) C 0.7963(8) 0.6953(7) -0.1040(6) 0.029(3) Uani 1.00 1 d .
C(30) C 0.7886(7) 0.6865(7) -0.0207(6) 0.029(2) Uani 1.00 1 d .
C(31) C 0.8323(8) 0.7861(8) -0.2657(7) 0.035(3) Uani 1.00 1 d .
C(32) C 0.3305(7) 0.5883(6) 0.1083(6) 0.023(2) Uani 1.00 1 d .
C(33) C 0.4292(8) 0.6312(7) 0.0735(6) 0.029(2) Uani 1.00 1 d .
C(34) C 0.4798(9) 0.6428(7) -0.0104(7) 0.033(3) Uani 1.00 1 d .
C(35) C 0.4344(9) 0.6112(7) -0.0582(6) 0.035(3) Uani 1.00 1 d .
C(36) C 0.3336(8) 0.5684(7) -0.0216(6) 0.029(2) Uani 1.00 1 d .
C(37) C 0.2816(7) 0.5572(6) 0.0597(6) 0.025(2) Uani 1.00 1 d .
C(38) C 0.4899(9) 0.6230(9) -0.1460(7) 0.045(3) Uani 1.00 1 d .
H(1) H 0.1589 -0.0223 0.7942 0.030 Uiso 1.00 1 c R
H(2) H 0.0684 -0.0191 0.8692 0.030 Uiso 1.00 1 c R
H(3) H 0.1376 0.0669 0.8117 0.030 Uiso 1.00 1 c R
H(4) H 0.0701 -0.0347 0.6065 0.030 Uiso 1.00 1 c R
H(5) H 0.1030 -0.0893 0.6989 0.030 Uiso 1.00 1 c R
H(6) H 0.1668 -0.0036 0.6312 0.030 Uiso 1.00 1 c R
H(7) H -0.2073 0.1014 0.5724 0.034 Uiso 1.00 1 c R
H(8) H -0.1428 0.0032 0.5964 0.034 Uiso 1.00 1 c R
H(9) H -0.0874 0.0921 0.5260 0.034 Uiso 1.00 1 c R
H(10) H -0.2823 0.2013 0.7296 0.024 Uiso 1.00 1 c R
H(11) H -0.3128 0.1336 0.6961 0.024 Uiso 1.00 1 c R
H(12) H -0.2607 0.2266 0.6312 0.024 Uiso 1.00 1 c R
H(13) H -0.0497 0.1303 0.8646 0.031 Uiso 1.00 1 c R
H(14) H -0.1757 0.1291 0.8640 0.031 Uiso 1.00 1 c R
H(15) H -0.1142 0.2185 0.8027 0.031 Uiso 1.00 1 c R
H(16) H 0.0836 0.6789 -0.1878 0.028 Uiso 1.00 1 c R
H(17) H 0.0334 0.6857 -0.0546 0.031 Uiso 1.00 1 c R
H(18) H 0.2955 0.8341 -0.1026 0.025 Uiso 1.00 1 c R
H(19) H 0.3474 0.8313 -0.2383 0.022 Uiso 1.00 1 c R
H(20) H 0.0709 0.8244 0.0107 0.045 Uiso 1.00 1 c R
H(21) H 0.1840 0.7738 0.0408 0.045 Uiso 1.00 1 c R
H(22) H 0.0838 0.7156 0.0594 0.045 Uiso 1.00 1 c R
H(23) H 0.3290 1.0823 -0.1813 0.023 Uiso 1.00 1 c R
H(24) H 0.2975 1.0190 -0.0304 0.022 Uiso 1.00 1 c R
H(25) H 0.5667 0.8326 -0.0222 0.024 Uiso 1.00 1 c R
H(26) H 0.5951 0.8938 -0.1728 0.025 Uiso 1.00 1 c R
H(27) H 0.4479 0.9094 0.1070 0.031 Uiso 1.00 1 c R
H(28) H 0.4348 0.8123 0.1106 0.031 Uiso 1.00 1 c R
H(29) H 0.3315 0.8831 0.1064 0.031 Uiso 1.00 1 c R
H(30) H 0.8427 0.9015 -0.0705 0.027 Uiso 1.00 1 c R
H(31) H 0.8560 0.9115 -0.2091 0.030 Uiso 1.00 1 c R
H(32) H 0.7835 0.6428 -0.1124 0.038 Uiso 1.00 1 c R
H(33) H 0.7709 0.6287 0.0274 0.032 Uiso 1.00 1 c R
H(34) H 0.7616 0.8066 -0.2853 0.043 Uiso 1.00 1 c R
H(35) H 0.8567 0.7264 -0.2657 0.043 Uiso 1.00 1 c R
H(36) H 0.8847 0.8304 -0.3029 0.043 Uiso 1.00 1 c R
H(37) H 0.4627 0.6528 0.1056 0.035 Uiso 1.00 1 c R
H(38) H 0.5472 0.6733 -0.0346 0.038 Uiso 1.00 1 c R
H(39) H 0.3004 0.5465 -0.0537 0.035 Uiso 1.00 1 c R
H(40) H 0.2129 0.5286 0.0830 0.032 Uiso 1.00 1 c R
H(41) H 0.4635 0.6812 -0.1884 0.046 Uiso 1.00 1 c R
H(42) H 0.4738 0.5730 -0.1569 0.046 Uiso 1.00 1 c R
H(43) H 0.5683 0.6218 -0.1492 0.046 Uiso 1.00 1 c R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.003 0.002
;
International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
H H 0.000 0.000
;
International Tables for Crystallography
(1992, Vol. C, Table 6.1.1.4)
;
O O 0.011 0.006
;
International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
Mo Mo -1.683 0.686
;
International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
S S 0.125 0.123
;
International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
Rh Rh -1.118 0.919
;
International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
Rh(1) Mo(2) Mo(1) 65.41(2)
Rh(1) Mo(2) Mo(3) 64.61(2)
Rh(1) Mo(2) S(2) 52.55(5)
S(2) Rh(1) Mo(2) 50.07(6)
Rh(1) Mo(2) S(3) 51.73(5)
S(3) Rh(1) Mo(2) 50.76(5)
S(4) Rh(1) Mo(2) 92.38(4)
C(1) Rh(1) Mo(2) 124.1(2)
C(2) Rh(1) Mo(2) 114.5(2)
C(3) Rh(1) Mo(2) 133.0(2)
C(4) Rh(1) Mo(2) 167.0(3)
C(5) Rh(1) Mo(2) 154.1(2)
Rh(1) Mo(2) S(1) 107.21(5)
Rh(1) Mo(2) O(3) 92.7(1)
Rh(1) Mo(2) O(4) 134.7(1)
Rh(1) Mo(2) O(5) 143.0(2)
Rh(1) S(2) Mo(1) 81.17(8)
Rh(1) S(2) Mo(2) 77.38(8)
S(3) Rh(1) S(2) 100.09(7)
S(4) Rh(1) S(2) 95.62(7)
C(1) Rh(1) S(2) 130.9(3)
C(2) Rh(1) S(2) 95.3(3)
C(3) Rh(1) S(2) 88.2(2)
C(4) Rh(1) S(2) 117.0(3)
C(5) Rh(1) S(2) 152.5(3)
Rh(1) S(3) Mo(2) 77.52(7)
Rh(1) S(3) Mo(3) 80.80(6)
S(4) Rh(1) S(3) 96.54(8)
C(1) Rh(1) S(3) 86.9(3)
C(2) Rh(1) S(3) 107.2(2)
C(3) Rh(1) S(3) 146.3(2)
C(4) Rh(1) S(3) 142.2(3)
C(5) Rh(1) S(3) 103.7(3)
Rh(1) S(4) Mo(1) 82.19(7)
Rh(1) S(4) Mo(3) 81.32(6)
C(1) Rh(1) S(4) 132.1(2)
C(2) Rh(1) S(4) 151.7(2)
C(3) Rh(1) S(4) 115.2(2)
C(4) Rh(1) S(4) 87.4(2)
C(5) Rh(1) S(4) 95.3(2)
Rh(1) C(1) C(2) 71.0(4)
C(2) Rh(1) C(1) 37.8(4)
C(3) Rh(1) C(1) 64.0(3)
C(4) Rh(1) C(1) 63.9(3)
Rh(1) C(1) C(5) 70.5(4)
C(5) Rh(1) C(1) 38.5(3)
Rh(1) C(1) C(6) 129.6(6)
Rh(1) C(2) C(1) 71.3(5)
Rh(1) C(2) C(3) 70.7(4)
C(3) Rh(1) C(2) 39.3(3)
C(4) Rh(1) C(2) 64.4(3)
C(5) Rh(1) C(2) 64.5(3)
Rh(1) C(2) C(7) 127.4(5)
Rh(1) C(3) C(2) 70.0(5)
Rh(1) C(3) C(4) 71.8(5)
C(4) Rh(1) C(3) 37.7(4)
C(5) Rh(1) C(3) 64.3(4)
Rh(1) C(3) C(8) 128.8(5)
Rh(1) C(4) C(3) 70.5(5)
Rh(1) C(4) C(5) 69.6(4)
C(5) Rh(1) C(4) 38.6(4)
Rh(1) C(4) C(9) 128.0(5)
Rh(1) C(5) C(1) 71.1(4)
Rh(1) C(5) C(4) 71.8(4)
Rh(1) C(5) C(10) 126.1(6)
Mo(1) Mo(2) Mo(3) 58.69(3)
Mo(3) Mo(1) Mo(2) 60.69(3)
Mo(1) Mo(2) S(2) 54.57(5)
S(2) Mo(1) Mo(2) 51.77(6)
Mo(1) Mo(2) S(3) 100.90(5)
S(4) Mo(1) Mo(2) 97.30(5)
Mo(1) Mo(2) S(1) 53.13(5)
S(1) Mo(1) Mo(2) 53.30(5)
O(1) Mo(1) Mo(2) 133.8(2)
O(2) Mo(1) Mo(2) 95.6(1)
Mo(1) Mo(2) O(3) 141.3(2)
Mo(1) Mo(2) O(4) 138.7(2)
Mo(1) Mo(2) O(5) 97.6(1)
Mo(1) Mo(3) Mo(2) 60.62(3)
S(2) Mo(1) Mo(3) 100.19(6)
Mo(1) Mo(3) S(3) 100.96(7)
Mo(1) Mo(3) S(4) 53.57(6)
S(4) Mo(1) Mo(3) 53.29(6)
Mo(1) Mo(3) S(1) 54.13(6)
S(1) Mo(1) Mo(3) 53.55(5)
O(1) Mo(1) Mo(3) 137.1(2)
O(2) Mo(1) Mo(3) 143.0(2)
Mo(1) Mo(3) O(7) 98.3(2)
Mo(1) Mo(3) O(6) 135.8(2)
Mo(1) Mo(3) O(8) 142.0(1)
Mo(1) S(1) Mo(2) 73.57(7)
Mo(1) S(1) Mo(3) 72.31(6)
S(2) Mo(1) S(1) 103.07(7)
S(4) Mo(1) S(1) 106.15(8)
O(1) Mo(1) S(1) 167.7(1)
O(2) Mo(1) S(1) 89.8(2)
Mo(1) S(2) Mo(2) 73.66(8)
S(4) Mo(1) S(2) 97.78(7)
O(1) Mo(1) S(2) 82.1(2)
O(2) Mo(1) S(2) 82.3(2)
Mo(1) S(4) Mo(3) 73.13(5)
O(1) Mo(1) S(4) 83.9(2)
O(2) Mo(1) S(4) 163.5(2)
O(2) Mo(1) O(1) 79.8(2)
S(2) Mo(2) Mo(3) 100.73(6)
Mo(2) Mo(3) S(3) 52.32(6)
S(3) Mo(2) Mo(3) 54.25(5)
Mo(2) Mo(3) S(4) 97.44(7)
Mo(2) Mo(3) S(1) 53.39(6)
S(1) Mo(2) Mo(3) 52.66(5)
Mo(2) Mo(3) O(7) 140.1(2)
O(3) Mo(2) Mo(3) 141.5(2)
O(4) Mo(2) Mo(3) 94.5(2)
O(5) Mo(2) Mo(3) 136.0(2)
Mo(2) Mo(3) O(6) 135.3(2)
Mo(2) Mo(3) O(8) 95.0(2)
Mo(2) S(1) Mo(3) 73.95(5)
S(2) Mo(2) S(1) 105.59(7)
S(3) Mo(2) S(1) 104.48(8)
O(3) Mo(2) S(1) 160.1(1)
O(4) Mo(2) S(1) 85.9(2)
O(5) Mo(2) S(1) 83.4(2)
S(3) Mo(2) S(2) 103.50(7)
O(3) Mo(2) S(2) 86.7(2)
O(4) Mo(2) S(2) 164.5(2)
O(5) Mo(2) S(2) 90.6(2)
Mo(2) S(3) Mo(3) 73.43(5)
O(3) Mo(2) S(3) 87.2(2)
O(4) Mo(2) S(3) 83.2(2)
O(5) Mo(2) S(3) 161.0(1)
O(4) Mo(2) O(3) 79.5(2)
O(5) Mo(2) O(3) 80.9(2)
O(5) Mo(2) O(4) 80.2(2)
S(3) Mo(3) S(1) 103.33(7)
S(4) Mo(3) S(1) 107.00(8)
O(7) Mo(3) S(1) 86.7(2)
O(6) Mo(3) S(1) 167.4(2)
O(8) Mo(3) S(1) 88.2(1)
S(4) Mo(3) S(3) 98.34(7)
O(7) Mo(3) S(3) 160.6(2)
O(6) Mo(3) S(3) 83.3(2)
O(8) Mo(3) S(3) 81.7(1)
O(7) Mo(3) S(4) 94.4(2)
O(6) Mo(3) S(4) 82.2(2)
O(8) Mo(3) S(4) 164.3(2)
O(7) Mo(3) O(6) 84.0(2)
O(8) Mo(3) O(6) 82.1(2)
O(8) Mo(3) O(7) 82.2(2)
O(10) S(5) O(9) 111.3(4)
O(11) S(5) O(9) 112.0(3)
C(11) S(5) O(9) 107.7(4)
O(11) S(5) O(10) 112.5(3)
C(11) S(5) O(10) 106.3(4)
C(11) S(5) O(11) 106.6(4)
S(5) C(11) C(12) 119.2(8)
S(5) C(11) C(16) 120.6(6)
O(13) S(6) O(12) 111.1(3)
O(14) S(6) O(12) 112.9(3)
C(18) S(6) O(12) 107.5(4)
O(14) S(6) O(13) 112.7(4)
C(18) S(6) O(13) 106.1(4)
C(18) S(6) O(14) 106.0(3)
S(6) C(18) C(19) 119.5(6)
S(6) C(18) C(23) 120.5(7)
O(17) S(7) O(15) 112.7(4)
O(16) S(7) O(15) 111.7(4)
C(32) S(7) O(15) 107.5(4)
O(17) S(7) O(16) 111.4(3)
C(32) S(7) O(16) 106.8(4)
C(32) S(7) O(17) 106.3(4)
S(7) C(32) C(33) 120.1(9)
S(7) C(32) C(37) 120.0(6)
O(19) S(8) O(18) 112.3(4)
O(20) S(8) O(18) 111.9(3)
C(25) S(8) O(18) 105.3(4)
O(20) S(8) O(19) 114.2(4)
C(25) S(8) O(19) 107.6(4)
C(25) S(8) O(20) 104.6(4)
S(8) C(25) C(26) 119.9(9)
S(8) C(25) C(30) 119.8(6)
C(1) C(2) C(3) 107.2(7)
C(5) C(1) C(2) 109.4(8)
C(6) C(1) C(2) 125.7(8)
C(1) C(2) C(7) 127.9(8)
C(1) C(5) C(4) 107.2(9)
C(6) C(1) C(5) 124.6(9)
C(1) C(5) C(10) 125.0(8)
C(2) C(3) C(4) 108.0(9)
C(7) C(2) C(3) 124.7(9)
C(2) C(3) C(8) 127.4(8)
C(3) C(4) C(5) 108.1(7)
C(8) C(3) C(4) 124.3(7)
C(3) C(4) C(9) 125.7(9)
C(9) C(4) C(5) 126.1(9)
C(4) C(5) C(10) 127.6(7)
C(16) C(11) C(12) 120.2(9)
C(11) C(12) C(13) 118(1)
C(11) C(16) C(15) 119.1(7)
C(12) C(13) C(14) 121.9(8)
C(13) C(14) C(15) 118(1)
C(13) C(14) C(17) 120.6(8)
C(14) C(15) C(16) 121(1)
C(17) C(14) C(15) 121(1)
C(23) C(18) C(19) 119.9(8)
C(18) C(19) C(20) 120.8(7)
C(18) C(23) C(22) 119.3(8)
C(19) C(20) C(21) 119.8(8)
C(20) C(21) C(22) 118.3(8)
C(20) C(21) C(24) 119.6(8)
C(21) C(22) C(23) 121.9(7)
C(24) C(21) C(22) 122.1(7)
C(30) C(25) C(26) 120.1(9)
C(25) C(26) C(27) 118(1)
C(25) C(30) C(29) 119.5(8)
C(26) C(27) C(28) 122.8(8)
C(27) C(28) C(29) 117(1)
C(27) C(28) C(31) 121.4(8)
C(28) C(29) C(30) 122(1)
C(31) C(28) C(29) 121(1)
C(37) C(32) C(33) 119.8(9)
C(32) C(33) C(34) 119(1)
C(32) C(37) C(36) 119.7(8)
C(33) C(34) C(35) 121.9(9)
C(34) C(35) C(38) 121(1)
C(34) C(35) C(36) 117.7(9)
C(35) C(36) C(37) 121(1)
C(38) C(35) C(36) 121(1)
C(1) C(6) H(3) 109.3308
C(1) C(6) H(1) 109.4681
C(1) C(6) H(2) 109.4691
C(2) C(7) H(6) 109.4484
C(2) C(7) H(4) 109.5468
C(2) C(7) H(5) 109.4630
C(3) C(8) H(9) 109.6008
C(3) C(8) H(7) 109.5284
C(3) C(8) H(8) 109.4718
C(4) C(9) H(12) 109.5946
C(4) C(9) H(10) 109.4789
C(4) C(9) H(11) 109.4704
C(5) C(10) H(15) 109.5474
C(5) C(10) H(13) 109.6461
C(5) C(10) H(14) 109.4681
H(3) C(6) H(1) 109.4748
H(2) C(6) H(1) 109.4735
H(3) C(6) H(2) 109.6109
H(6) C(7) H(4) 109.4713
H(5) C(7) H(4) 109.4396
H(6) C(7) H(5) 109.4581
H(9) C(8) H(7) 109.4742
H(8) C(8) H(7) 109.4425
H(9) C(8) H(8) 109.3093
H(12) C(9) H(10) 109.4732
H(11) C(9) H(10) 109.4659
H(12) C(9) H(11) 109.3441
H(15) C(10) H(13) 109.4703
H(14) C(10) H(13) 109.3851
H(15) C(10) H(14) 109.3097
C(11) C(12) H(16) 120.5205
C(11) C(16) H(19) 120.4508
H(16) C(12) C(13) 120.5191
C(12) C(13) H(17) 119.0730
H(17) C(13) C(14) 119.0723
C(14) C(15) H(18) 119.1172
C(14) C(17) H(21) 109.4744
C(14) C(17) H(22) 109.5352
C(14) C(17) H(20) 109.2602
C(15) C(16) H(19) 120.4563
H(18) C(15) C(16) 119.1146
H(21) C(17) H(20) 109.5748
H(22) C(17) H(20) 109.4723
H(22) C(17) H(21) 109.5101
C(18) C(19) H(23) 119.6079
C(18) C(23) H(26) 120.3594
H(23) C(19) C(20) 119.6098
C(19) C(20) H(24) 120.0867
H(24) C(20) C(21) 120.0870
C(21) C(22) H(25) 119.0566
C(21) C(24) H(28) 109.4717
C(21) C(24) H(29) 109.7778
C(21) C(24) H(27) 109.5595
C(22) C(23) H(26) 120.3648
H(25) C(22) C(23) 119.0579
H(28) C(24) H(27) 109.4276
H(29) C(24) H(27) 109.4691
H(29) C(24) H(28) 109.1204
C(25) C(26) H(30) 120.8306
C(25) C(30) H(33) 120.2704
H(30) C(26) C(27) 120.8376
C(26) C(27) H(31) 118.5967
H(31) C(27) C(28) 118.5935
C(28) C(29) H(32) 118.9516
C(28) C(31) H(34) 109.2295
C(28) C(31) H(35) 109.4685
C(28) C(31) H(36) 109.2748
C(29) C(30) H(33) 120.2696
H(32) C(29) C(30) 118.9498
H(35) C(31) H(34) 109.5916
H(36) C(31) H(34) 109.4766
H(36) C(31) H(35) 109.7845
C(32) C(33) H(37) 120.4022
C(32) C(37) H(40) 120.1498
H(37) C(33) C(34) 120.3973
C(33) C(34) H(38) 119.0358
H(38) C(34) C(35) 119.0479
C(35) C(36) H(39) 119.1743
C(35) C(38) H(41) 109.7109
C(35) C(38) H(42) 109.4658
C(35) C(38) H(43) 109.5984
C(36) C(37) H(40) 120.1361
H(39) C(36) C(37) 119.1788
H(42) C(38) H(41) 109.3538
H(43) C(38) H(41) 109.4660
H(43) C(38) H(42) 109.2310
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Rh(1) Mo(2) 2.9377(8)
Rh(1) S(2) 2.390(2)
Rh(1) S(3) 2.362(2)
Rh(1) S(4) 2.409(2)
Rh(1) C(1) 2.186(7)
Rh(1) C(2) 2.181(8)
Rh(1) C(3) 2.191(9)
Rh(1) C(4) 2.208(8)
Rh(1) C(5) 2.178(7)
Mo(1) Mo(2) 2.8199(8)
Mo(1) Mo(3) 2.765(1)
Mo(1) S(1) 2.352(2)
Mo(1) S(2) 2.394(2)
Mo(1) S(4) 2.325(2)
Mo(1) O(1) 2.192(6)
Mo(1) O(2) 2.205(6)
Mo(2) Mo(3) 2.822(1)
Mo(2) S(1) 2.357(2)
Mo(2) S(2) 2.309(2)
Mo(2) S(3) 2.330(2)
Mo(2) O(3) 2.162(6)
Mo(2) O(4) 2.194(6)
Mo(2) O(5) 2.130(5)
Mo(3) S(1) 2.335(2)
Mo(3) S(3) 2.389(2)
Mo(3) S(4) 2.316(2)
Mo(3) O(6) 2.213(6)
Mo(3) O(7) 1.892(6)
Mo(3) O(8) 2.198(6)
S(5) O(9) 1.463(6)
S(5) O(10) 1.460(7)
S(5) O(11) 1.450(6)
S(5) C(11) 1.77(1)
S(6) O(12) 1.461(6)
S(6) O(13) 1.451(7)
S(6) O(14) 1.461(6)
S(6) C(18) 1.758(9)
S(7) O(15) 1.448(8)
S(7) O(16) 1.477(6)
S(7) O(17) 1.449(5)
S(7) C(32) 1.743(9)
S(8) O(18) 1.462(6)
S(8) O(19) 1.432(8)
S(8) O(20) 1.468(6)
S(8) C(25) 1.78(1)
C(1) C(2) 1.41(2)
C(1) C(5) 1.44(1)
C(1) C(6) 1.50(1)
C(2) Rh(1) 2.181(8)
C(2) C(1) 1.41(2)
C(2) C(3) 1.47(1)
C(2) C(7) 1.49(1)
C(3) C(2) 1.47(1)
C(3) C(4) 1.42(1)
C(3) C(8) 1.49(2)
C(4) C(5) 1.45(1)
C(4) C(9) 1.49(1)
C(5) C(10) 1.50(2)
C(7) C(2) 1.49(1)
C(11) C(12) 1.40(1)
C(11) C(16) 1.38(1)
C(12) C(13) 1.38(2)
C(13) C(14) 1.39(2)
C(14) C(15) 1.38(1)
C(14) C(17) 1.51(2)
C(15) C(16) 1.40(1)
C(18) C(19) 1.38(1)
C(18) C(23) 1.40(1)
C(19) C(20) 1.39(1)
C(20) C(21) 1.42(1)
C(21) C(22) 1.38(1)
C(21) C(24) 1.50(1)
C(22) C(23) 1.39(1)
C(25) C(26) 1.40(1)
C(25) C(30) 1.39(2)
C(26) C(27) 1.38(2)
C(27) C(28) 1.39(2)
C(28) C(29) 1.38(1)
C(28) C(31) 1.49(2)
C(29) C(30) 1.38(2)
C(32) C(33) 1.38(1)
C(32) C(37) 1.41(2)
C(33) C(34) 1.41(1)
C(34) C(35) 1.38(2)
C(35) C(36) 1.40(1)
C(35) C(38) 1.49(2)
C(36) C(37) 1.38(1)
C(6) H(1) 0.9500
C(6) H(2) 0.9499
C(6) H(3) 0.9500
C(7) H(4) 0.9500
C(7) H(5) 0.9500
C(7) H(6) 0.9500
C(8) H(7) 0.9501
C(8) H(8) 0.9501
C(8) H(9) 0.9501
C(9) H(10) 0.9501
C(9) H(11) 0.9501
C(9) H(12) 0.9499
C(10) H(13) 0.9500
C(10) H(14) 0.9500
C(10) H(15) 0.9500
C(12) H(16) 0.9501
C(13) H(17) 0.9500
C(15) H(18) 0.9500
C(16) H(19) 0.9500
C(17) H(20) 0.9500
C(17) H(21) 0.9500
C(17) H(22) 0.9500
C(19) H(23) 0.9500
C(20) H(24) 0.9499
C(22) H(25) 0.9500
C(23) H(26) 0.9501
C(24) H(27) 0.9499
C(24) H(28) 0.9500
C(24) H(29) 0.9500
C(26) H(30) 0.9500
C(27) H(31) 0.9500
C(29) H(32) 0.9500
C(30) H(33) 0.9499
C(31) H(34) 0.9500
C(31) H(35) 0.9500
C(31) H(36) 0.9501
C(33) H(37) 0.9500
C(34) H(38) 0.9500
C(36) H(39) 0.9501
C(37) H(40) 0.9500
C(38) H(41) 0.9501
C(38) H(42) 0.9500
C(38) H(43) 0.9500
H(1) C(6) 0.9500
H(3) C(6) 0.9500
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_2
Rh(1) Mo(1) 3.1125(7) .
Rh(1) Mo(3) 3.080(1) .
Rh(1) C(6) 3.346(8) .
Rh(1) C(7) 3.30(1) .
Rh(1) C(8) 3.34(1) .
Rh(1) C(9) 3.337(7) .
Rh(1) C(10) 3.288(9) .
Mo(1) O(7) 3.569(8) .
S(1) O(2) 3.217(7) .
S(1) O(4) 3.102(5) .
S(1) O(5) 2.989(7) .
S(1) O(7) 2.919(7) .
S(1) O(8) 3.155(7) .
S(1) O(17) 3.211(6) .
S(2) S(4) 3.556(3) .
S(2) O(1) 3.017(5) .
S(2) O(2) 3.031(5) .
S(2) O(3) 3.072(6) .
S(2) O(5) 3.158(5) .
S(2) C(2) 3.381(7) .
S(2) C(3) 3.190(7) .
S(2) C(8) 3.347(9) .
S(3) S(4) 3.561(2) .
S(3) O(3) 3.101(7) .
S(3) O(4) 3.005(5) .
S(3) O(6) 3.061(7) .
S(3) O(8) 3.003(7) .
S(3) C(1) 3.129(9) .
S(3) C(5) 3.571(8) .
S(3) C(6) 3.244(8) .
S(4) O(1) 3.020(8) .
S(4) O(6) 2.979(7) .
S(4) O(7) 3.100(7) .
S(4) C(4) 3.192(9) .
S(4) C(5) 3.394(7) .
S(4) C(9) 3.300(9) .
S(5) O(1) 3.530(8) 56502
S(5) O(21) 3.555(7) 66502
S(5) C(12) 2.742(9) .
S(5) C(16) 2.74(1) .
S(6) O(3) 3.519(6) 56401
S(6) C(19) 2.719(9) .
S(6) C(23) 2.745(8) .
S(7) O(23) 3.537(8) .
S(7) C(33) 2.710(9) .
S(7) C(37) 2.73(1) .
S(8) C(26) 2.761(8) .
S(8) C(30) 2.75(1) .
O(1) S(5) 3.530(8) 56502
O(1) O(2) 2.822(7) .
O(1) O(9) 3.39(1) 56502
O(1) O(10) 2.64(1) 56502
O(1) O(21) 3.240(8) 45501
O(1) O(26) 2.670(8) .
O(2) O(5) 3.339(7) .
O(2) O(16) 2.640(8) .
O(2) O(17) 3.591(8) .
O(2) O(21) 2.678(9) 45501
O(2) C(31) 3.58(1) 66502
O(3) O(4) 2.79(1) .
O(3) O(5) 2.784(7) .
O(3) O(24) 3.263(9) 66502
O(3) C(7) 3.49(1) .
O(4) O(5) 2.785(9) .
O(4) O(8) 3.187(9) .
O(4) O(27) 2.615(7) 66502
O(5) O(17) 2.701(7) .
O(5) O(24) 2.584(9) 66502
O(5) O(27) 3.495(9) 66502
O(5) C(31) 3.60(2) 66502
O(6) O(7) 2.757(6) .
O(6) O(8) 2.898(7) .
O(6) C(10) 3.37(1) .
O(7) O(8) 2.698(7) .
O(9) O(1) 3.39(1) 56502
O(9) O(10) 2.412(7) .
O(9) O(11) 2.415(8) .
O(9) O(21) 2.890(9) 66502
O(9) O(27) 2.733(8) .
O(9) C(11) 2.62(1) .
O(9) C(12) 3.30(1) .
O(9) C(16) 3.57(1) .
O(10) O(1) 2.64(1) 56502
O(10) O(11) 2.420(9) .
O(10) O(21) 3.379(8) 66502
O(10) C(7) 3.39(1) 56401
O(10) C(8) 3.54(1) 56502
O(10) C(11) 2.59(1) .
O(10) C(12) 3.04(1) .
O(11) O(24) 2.76(1) .
O(11) O(25) 2.835(7) .
O(11) C(11) 2.587(9) .
O(11) C(16) 2.91(1) .
O(12) O(3) 3.44(1) 56401
O(12) O(4) 2.828(7) 56401
O(12) O(13) 2.40(1) .
O(12) O(14) 2.434(9) .
O(12) C(9) 3.47(1) 66401
O(12) C(18) 2.601(8) .
O(12) C(19) 3.120(9) .
O(13) O(3) 2.604(8) 56401
O(13) O(14) 2.423(8) .
O(13) O(24) 3.60(1) .
O(13) C(16) 3.34(1) .
O(13) C(18) 2.57(1) .
O(13) C(19) 3.16(1) .
O(13) C(23) 3.59(1) .
O(14) O(24) 2.89(1) .
O(14) C(18) 2.58(1) .
O(14) C(23) 2.88(1) .
O(15) O(16) 2.42(1) .
O(15) O(17) 2.412(9) .
O(15) O(23) 2.72(1) .
O(15) C(32) 2.58(1) .
O(15) C(33) 2.99(1) .
O(16) O(17) 2.418(8) .
O(16) C(32) 2.590(9) .
O(16) C(37) 2.94(1) .
O(17) O(23) 3.27(1) .
O(17) O(27) 3.253(9) 66502
O(17) C(32) 2.56(1) .
O(17) C(33) 3.319(9) .
O(17) C(37) 3.42(1) .
O(17) C(38) 3.47(1) 66502
O(18) O(19) 2.404(9) .
O(18) O(20) 2.428(8) .
O(18) O(21) 2.846(8) .
O(18) C(25) 2.58(1) .
O(18) C(30) 3.04(1) .
O(19) O(20) 2.44(1) .
O(19) C(17) 3.60(1) 65501
O(19) C(25) 2.60(1) .
O(19) C(26) 2.95(1) .
O(20) O(22) 2.663(9) .
O(20) C(22) 3.59(1) .
O(20) C(24) 3.47(1) .
O(20) C(25) 2.58(1) .
O(20) C(26) 3.52(1) .
O(20) C(30) 3.24(1) .
O(21) S(5) 3.555(7) 66502
O(21) O(1) 3.240(8) 65501
O(21) O(2) 2.678(9) 65501
O(21) O(9) 2.890(9) 66502
O(21) O(10) 3.379(8) 66502
O(21) C(12) 3.46(1) 66502
O(22) O(23) 2.753(9) .
O(23) O(27) 2.756(9) 66502
O(24) O(3) 3.263(9) 66502
O(24) O(5) 2.584(9) 66502
O(24) C(38) 3.52(1) .
O(25) O(3) 2.58(1) 56401
O(25) C(7) 3.36(1) 56401
O(25) C(8) 3.12(1) 56502
O(26) O(27) 2.73(1) 56502
O(27) O(4) 2.615(7) 66502
O(27) O(5) 3.495(9) 66502
O(27) O(17) 3.253(9) 66502
O(27) O(23) 2.756(9) 66502
O(27) O(26) 2.73(1) 56502
C(1) C(3) 2.32(1) .
C(1) C(4) 2.33(1) .
C(1) C(7) 2.61(2) .
C(1) C(10) 2.60(1) .
C(2) S(2) 3.381(7) .
C(2) C(4) 2.34(1) .
C(2) C(5) 2.33(1) .
C(2) C(6) 2.59(1) .
C(2) C(8) 2.65(1) .
C(3) C(5) 2.33(1) .
C(3) C(7) 2.62(1) .
C(3) C(9) 2.59(1) .
C(4) C(2) 2.34(1) .
C(4) C(8) 2.58(2) .
C(4) C(10) 2.64(2) .
C(5) C(2) 2.33(1) .
C(5) C(6) 2.60(1) .
C(5) C(9) 2.62(1) .
C(6) C(2) 2.59(1) .
C(6) C(7) 3.20(2) .
C(6) C(10) 3.15(1) .
C(7) C(8) 3.22(1) .
C(8) O(10) 3.54(1) 56502
C(8) O(25) 3.12(1) 56502
C(8) C(2) 2.65(1) .
C(8) C(9) 3.13(2) .
C(9) C(10) 3.24(2) .
C(11) C(7) 3.47(1) 56401
C(11) C(13) 2.40(1) .
C(11) C(14) 2.79(1) .
C(11) C(15) 2.39(2) .
C(12) O(21) 3.46(1) 66502
C(12) C(14) 2.42(2) .
C(12) C(15) 2.77(2) .
C(12) C(16) 2.42(1) .
C(13) C(15) 2.38(1) .
C(13) C(16) 2.77(1) .
C(13) C(17) 2.52(2) .
C(13) C(36) 3.49(1) .
C(14) C(16) 2.42(1) .
C(14) C(36) 3.37(1) .
C(14) C(37) 3.36(1) .
C(15) C(6) 3.40(1) 56401
C(15) C(17) 2.52(1) .
C(15) C(35) 3.38(1) .
C(15) C(36) 3.43(1) .
C(16) C(35) 3.48(1) .
C(16) C(38) 3.41(1) .
C(17) O(19) 3.60(1) 45501
C(17) C(32) 3.56(1) .
C(17) C(37) 3.49(1) .
C(18) C(20) 2.41(1) .
C(18) C(21) 2.80(1) .
C(18) C(22) 2.40(1) .
C(19) C(21) 2.43(1) .
C(19) C(22) 2.76(1) .
C(19) C(23) 2.41(1) .
C(20) C(22) 2.41(1) .
C(20) C(23) 2.79(1) .
C(20) C(24) 2.53(1) .
C(21) C(23) 2.42(1) .
C(22) C(24) 2.53(1) .
C(25) C(27) 2.39(1) .
C(25) C(28) 2.80(1) .
C(25) C(29) 2.39(2) .
C(26) C(28) 2.43(2) .
C(26) C(29) 2.77(2) .
C(26) C(30) 2.42(1) .
C(27) C(29) 2.37(1) .
C(27) C(30) 2.75(1) .
C(27) C(31) 2.51(2) .
C(28) C(30) 2.42(1) .
C(29) C(31) 2.51(1) .
C(31) O(2) 3.58(1) 66502
C(31) O(5) 3.60(2) 66502
C(32) C(34) 2.41(1) .
C(32) C(35) 2.81(1) .
C(32) C(36) 2.41(2) .
C(32) C(38) 3.59(1) 66502
C(33) C(35) 2.44(2) .
C(33) C(36) 2.77(2) .
C(33) C(37) 2.41(2) .
C(34) C(36) 2.38(2) .
C(34) C(37) 2.77(1) .
C(34) C(38) 2.49(2) .
C(35) C(35) 3.52(1) 66502
C(35) C(37) 2.43(1) .
C(36) C(38) 2.52(1) .
C(38) O(17) 3.47(1) 66502
C(38) C(32) 3.59(1) 66502
Rh(1) H(3) 3.3615 .
Rh(1) H(6) 3.3042 .
Rh(1) H(9) 3.3486 .
Rh(1) H(12) 3.3400 .
Rh(1) H(15) 3.2803 .
S(2) H(4) 3.5734 .
S(2) H(6) 3.4795 .
S(2) H(9) 2.7013 .
S(2) H(35) 3.4455 66502
S(2) H(36) 3.4501 66502
S(3) H(1) 3.4980 .
S(3) H(3) 2.6763 .
S(4) H(10) 3.3228 .
S(4) H(12) 2.8926 .
S(4) H(15) 3.1083 .
S(5) H(5) 3.1816 56401
S(5) H(16) 2.8430 .
S(5) H(19) 2.8527 .
S(5) H(41) 3.4674 .
S(6) H(11) 3.2031 66401
S(6) H(19) 3.4809 .
S(6) H(23) 2.8082 .
S(6) H(26) 2.8566 .
S(7) H(21) 3.5617 .
S(7) H(37) 2.8195 .
S(7) H(40) 2.8418 .
S(8) H(22) 3.5516 65501
S(8) H(25) 3.5144 .
S(8) H(30) 2.8706 .
S(8) H(33) 2.8459 .
O(1) H(7) 3.5626 .
O(1) H(9) 3.5496 .
O(1) H(12) 3.1060 .
O(2) H(35) 2.6792 66502
O(3) H(6) 2.6173 .
O(5) H(34) 3.0985 66502
O(5) H(35) 3.2353 66502
O(6) H(13) 3.3530 .
O(6) H(15) 2.6507 .
O(9) H(16) 3.2291 .
O(9) H(41) 3.2600 .
O(9) H(42) 3.2503 .
O(10) H(4) 3.0741 56401
O(10) H(5) 2.9356 56401
O(10) H(7) 3.2655 56502
O(10) H(9) 2.9380 56502
O(10) H(16) 2.7898 .
O(10) H(36) 3.5153 45501
O(11) H(5) 3.4351 56401
O(11) H(6) 3.4074 56401
O(11) H(19) 2.5399 .
O(11) H(41) 3.4532 .
O(12) H(11) 2.6971 66401
O(12) H(12) 3.5088 66401
O(12) H(23) 2.8886 .
O(13) H(1) 3.0095 56401
O(13) H(6) 2.9469 56401
O(13) H(19) 2.6503 .
O(13) H(23) 3.0463 .
O(14) H(7) 3.1481 66401
O(14) H(8) 3.3931 66401
O(14) H(11) 3.0553 66401
O(14) H(26) 2.4969 .
O(14) H(34) 3.2621 .
O(15) H(21) 3.4343 .
O(15) H(28) 3.1374 .
O(15) H(29) 3.5288 .
O(15) H(37) 2.6888 .
O(16) H(21) 3.5236 .
O(16) H(22) 3.0176 .
O(16) H(40) 2.5877 .
O(17) H(37) 3.3435 .
O(17) H(40) 3.4954 .
O(17) H(42) 3.0307 66502
O(17) H(43) 3.0987 66502
O(18) H(22) 3.0787 65501
O(18) H(33) 2.7725 .
O(19) H(20) 2.9430 65501
O(19) H(22) 3.3719 65501
O(19) H(30) 2.5920 .
O(20) H(25) 2.7787 .
O(20) H(27) 3.3058 .
O(20) H(28) 2.8913 .
O(20) H(33) 3.1820 .
O(20) H(37) 3.3704 .
O(21) H(16) 2.7092 66502
O(22) H(28) 3.5838 .
O(24) H(19) 2.8706 .
O(24) H(34) 2.8631 .
O(24) H(41) 2.7765 .
O(24) H(43) 3.4630 .
O(25) H(4) 3.1788 56401
O(25) H(6) 2.7110 56401
O(25) H(7) 2.7787 56502
O(25) H(8) 2.7577 56502
O(25) H(9) 3.3484 56502
O(26) H(12) 3.2915 .
C(1) H(1) 2.0232 .
C(1) H(2) 2.0231 .
C(1) H(3) 2.0215 .
C(1) H(4) 3.3438 .
C(1) H(5) 2.8369 .
C(1) H(6) 2.8856 .
C(1) H(13) 2.6549 .
C(1) H(14) 3.1872 .
C(1) H(15) 3.2010 .
C(2) H(1) 2.6511 .
C(2) H(2) 3.1576 .
C(2) H(3) 3.1976 .
C(2) H(4) 2.0157 .
C(2) H(5) 2.0148 .
C(2) H(6) 2.0146 .
C(2) H(7) 3.3987 .
C(2) H(8) 2.8807 .
C(2) H(9) 2.9227 .
C(3) H(4) 2.6613 .
C(3) H(5) 3.2043 .
C(3) H(6) 3.2200 .
C(3) H(7) 2.0199 .
C(3) H(8) 2.0192 .
C(3) H(9) 2.0207 .
C(3) H(10) 3.3390 .
C(3) H(11) 2.8247 .
C(3) H(12) 2.8508 .
C(4) H(7) 2.6273 .
C(4) H(8) 3.1522 .
C(4) H(9) 3.1893 .
C(4) H(10) 2.0158 .
C(4) H(11) 2.0157 .
C(4) H(12) 2.0170 .
C(4) H(13) 3.3862 .
C(4) H(14) 2.8713 .
C(4) H(15) 2.9160 .
C(5) H(1) 3.3531 .
C(5) H(2) 2.8267 .
C(5) H(3) 2.8526 .
C(5) H(10) 2.6755 .
C(5) H(11) 3.2047 .
C(5) H(12) 3.2179 .
C(5) H(13) 2.0235 .
C(5) H(14) 2.0214 .
C(5) H(15) 2.0224 .
C(6) H(5) 3.1136 .
C(6) H(6) 3.2377 .
C(6) H(13) 2.7114 .
C(7) H(1) 2.7821 .
C(7) H(8) 3.1599 .
C(7) H(9) 3.2274 .
C(8) H(4) 2.7884 .
C(8) H(11) 3.0597 .
C(8) H(12) 3.1300 .
C(9) H(7) 2.6923 .
C(9) H(14) 3.1676 .
C(9) H(15) 3.2641 .
C(10) H(2) 3.0979 .
C(10) H(3) 3.1100 .
C(10) H(10) 2.8205 .
C(11) H(5) 2.6137 56401
C(11) H(6) 3.5965 56401
C(11) H(16) 2.0573 .
C(11) H(17) 3.2548 .
C(11) H(18) 3.2484 .
C(11) H(19) 2.0363 .
C(11) H(39) 3.4788 .
C(11) H(41) 3.0841 .
C(12) H(5) 2.9875 56401
C(12) H(17) 2.0187 .
C(12) H(19) 3.2781 .
C(12) H(39) 3.2798 .
C(13) H(5) 3.5785 56401
C(13) H(16) 2.0330 .
C(13) H(18) 3.2351 .
C(13) H(20) 2.9389 .
C(13) H(21) 3.2429 .
C(13) H(22) 2.6076 .
C(13) H(39) 3.2997 .
C(13) H(40) 3.5366 .
C(14) H(1) 3.1888 56401
C(14) H(2) 3.2034 56401
C(14) H(16) 3.2778 .
C(14) H(17) 2.0317 .
C(14) H(18) 2.0197 .
C(14) H(19) 3.2768 .
C(14) H(20) 2.0299 .
C(14) H(21) 2.0324 .
C(14) H(22) 2.0331 .
C(14) H(39) 3.5570 .
C(14) H(40) 3.5334 .
C(15) H(1) 2.6823 56401
C(15) H(2) 3.2794 56401
C(15) H(5) 3.5517 56401
C(15) H(17) 3.2330 .
C(15) H(19) 2.0475 .
C(15) H(20) 2.9452 .
C(15) H(21) 2.6099 .
C(15) H(22) 3.2355 .
C(15) H(41) 3.3479 .
C(16) H(1) 2.9605 56401
C(16) H(5) 2.9357 56401
C(16) H(6) 3.5309 56401
C(16) H(16) 3.2755 .
C(16) H(18) 2.0343 .
C(16) H(41) 2.6531 .
C(17) H(2) 3.2723 56401
C(17) H(17) 2.6627 .
C(17) H(18) 2.6667 .
C(17) H(40) 3.5509 .
C(18) H(11) 3.5029 66401
C(18) H(18) 3.1566 .
C(18) H(19) 3.5820 .
C(18) H(23) 2.0274 .
C(18) H(24) 3.2613 .
C(18) H(25) 3.2564 .
C(18) H(26) 2.0486 .
C(19) H(1) 3.3620 56401
C(19) H(3) 3.0504 56401
C(19) H(18) 3.1397 .
C(19) H(24) 2.0348 .
C(19) H(26) 3.2652 .
C(20) H(3) 3.5797 56401
C(20) H(18) 3.1880 .
C(20) H(23) 2.0302 .
C(20) H(25) 3.2665 .
C(20) H(27) 2.9500 .
C(20) H(28) 3.2576 .
C(20) H(29) 2.6091 .
C(21) H(18) 3.2789 .
C(21) H(23) 3.2862 .
C(21) H(24) 2.0678 .
C(21) H(25) 2.0222 .
C(21) H(26) 3.2736 .
C(21) H(27) 2.0303 .
C(21) H(28) 2.0293 .
C(21) H(29) 2.0329 .
C(22) H(18) 3.2953 .
C(22) H(24) 3.2669 .
C(22) H(26) 2.0385 .
C(22) H(27) 2.9600 .
C(22) H(28) 2.6199 .
C(22) H(29) 3.2418 .
C(22) H(37) 3.5502 .
C(22) H(38) 3.1693 .
C(23) H(18) 3.2438 .
C(23) H(23) 3.2626 .
C(23) H(25) 2.0255 .
C(23) H(38) 3.5060 .
C(24) H(24) 2.6851 .
C(24) H(25) 2.6805 .
C(24) H(37) 3.4079 .
C(25) H(17) 2.9692 65501
C(25) H(25) 3.0010 .
C(25) H(30) 2.0576 .
C(25) H(31) 3.2417 .
C(25) H(32) 3.2414 .
C(25) H(33) 2.0391 .
C(26) H(2) 3.5893 66401
C(26) H(17) 3.2347 65501
C(26) H(20) 3.4788 65501
C(26) H(25) 3.2179 .
C(26) H(26) 3.4293 .
C(26) H(31) 2.0119 .
C(26) H(33) 3.2773 .
C(27) H(17) 3.4089 65501
C(27) H(26) 2.9856 .
C(27) H(30) 2.0338 .
C(27) H(32) 3.2285 .
C(27) H(34) 2.9349 .
C(27) H(35) 3.2351 .
C(27) H(36) 2.6009 .
C(28) H(16) 3.3589 65501
C(28) H(17) 3.3957 65501
C(28) H(26) 3.0922 .
C(28) H(30) 3.2834 .
C(28) H(31) 2.0245 .
C(28) H(32) 2.0234 .
C(28) H(33) 3.2696 .
C(28) H(34) 2.0156 .
C(28) H(35) 2.0184 .
C(28) H(36) 2.0162 .
C(29) H(16) 3.5559 65501
C(29) H(17) 3.1520 65501
C(29) H(26) 3.5885 .
C(29) H(31) 3.2257 .
C(29) H(33) 2.0288 .
C(29) H(34) 2.9329 .
C(29) H(35) 2.6007 .
C(29) H(36) 3.2287 .
C(29) H(38) 3.0702 .
C(29) H(40) 3.4347 66502
C(29) H(43) 3.5348 .
C(30) H(17) 2.9424 65501
C(30) H(25) 3.2882 .
C(30) H(30) 3.2787 .
C(30) H(32) 2.0159 .
C(30) H(38) 3.0644 .
C(31) H(8) 3.2379 66401
C(31) H(16) 3.4923 65501
C(31) H(31) 2.6590 .
C(31) H(32) 2.6599 .
C(32) H(21) 3.0691 .
C(32) H(22) 3.3988 .
C(32) H(37) 2.0316 .
C(32) H(38) 3.2571 .
C(32) H(39) 3.2631 .
C(32) H(40) 2.0550 .
C(32) H(42) 3.1657 66502
C(32) H(43) 3.1892 66502
C(33) H(21) 3.4511 .
C(33) H(25) 3.4254 .
C(33) H(28) 3.2320 .
C(33) H(38) 2.0478 .
C(33) H(40) 3.2660 .
C(33) H(42) 3.0628 66502
C(34) H(18) 3.4488 .
C(34) H(25) 3.2660 .
C(34) H(37) 2.0612 .
C(34) H(39) 3.2351 .
C(34) H(41) 2.9187 .
C(34) H(42) 3.2136 .
C(34) H(42) 3.4311 66502
C(34) H(43) 2.5853 .
C(35) H(18) 3.5039 .
C(35) H(37) 3.2869 .
C(35) H(38) 2.0157 .
C(35) H(39) 2.0413 .
C(35) H(40) 3.2816 .
C(35) H(41) 2.0161 .
C(35) H(42) 2.0132 .
C(35) H(43) 2.0147 .
C(36) H(32) 3.4692 66502
C(36) H(38) 3.2382 .
C(36) H(40) 2.0283 .
C(36) H(41) 2.9391 .
C(36) H(42) 2.6066 .
C(36) H(43) 3.2428 .
C(36) H(43) 3.4245 66502
C(37) H(21) 3.3582 .
C(37) H(22) 3.2118 .
C(37) H(32) 3.0863 66502
C(37) H(37) 3.2716 .
C(37) H(39) 2.0190 .
C(37) H(43) 3.0800 66502
C(38) H(19) 3.3465 .
C(38) H(38) 2.6399 .
C(38) H(39) 2.6733 .
H(1) S(3) 3.4980 .
H(1) C(1) 2.0232 .
H(1) C(2) 2.6511 .
H(1) C(5) 3.3531 .
H(1) C(7) 2.7821 .
H(2) C(2) 3.1576 .
H(3) Rh(1) 3.3615 .
H(3) S(3) 2.6763 .
H(3) C(1) 2.0215 .
H(3) C(2) 3.1976 .
H(3) C(5) 2.8526 .
H(3) C(10) 3.1100 .
H(4) C(2) 2.0157 .
H(5) C(2) 2.0148 .
H(6) C(2) 2.0146 .
H(7) O(10) 3.2655 56502
H(7) O(25) 2.7787 56502
H(7) C(2) 3.3987 .
H(8) O(25) 2.7577 56502
H(8) C(2) 2.8807 .
H(9) O(10) 2.9380 56502
H(9) O(25) 3.3484 56502
H(9) C(2) 2.9227 .
H(16) O(21) 2.7092 66502
H(16) C(28) 3.3589 45501
H(16) C(29) 3.5559 45501
H(16) C(31) 3.4923 45501
H(17) C(25) 2.9692 45501
H(17) C(26) 3.2347 45501
H(17) C(27) 3.4089 45501
H(17) C(28) 3.3957 45501
H(17) C(29) 3.1520 45501
H(17) C(30) 2.9424 45501
H(18) C(6) 3.4066 56401
H(20) O(19) 2.9430 45501
H(20) C(6) 3.4540 56401
H(20) C(26) 3.4788 45501
H(22) S(8) 3.5516 45501
H(22) O(18) 3.0787 45501
H(22) O(19) 3.3719 45501
H(23) S(3) 3.3068 56401
H(23) C(6) 3.1394 56401
H(30) C(1) 3.5485 66401
H(30) C(5) 3.4939 66401
H(31) C(1) 3.0424 66401
H(31) C(2) 2.7739 66401
H(31) C(3) 2.7877 66401
H(31) C(4) 3.0764 66401
H(31) C(5) 3.2573 66401
H(31) C(7) 3.3849 66401
H(31) C(8) 3.3994 66401
H(32) C(36) 3.4692 66502
H(32) C(37) 3.0863 66502
H(34) O(5) 3.0985 66502
H(35) S(2) 3.4455 66502
H(35) O(2) 2.6792 66502
H(35) O(5) 3.2353 66502
H(36) S(2) 3.4501 66502
H(36) O(10) 3.5153 65501
H(36) C(7) 3.4344 66401
H(36) C(8) 3.4045 66401
H(40) C(29) 3.4347 66502
H(42) O(17) 3.0307 66502
H(42) C(32) 3.1657 66502
H(42) C(33) 3.0628 66502
H(42) C(34) 3.4311 66502
H(43) O(17) 3.0987 66502
H(43) C(32) 3.1892 66502
H(43) C(36) 3.4245 66502
H(43) C(37) 3.0800 66502
Rh(1) Mo(1) 3.1125(7) .
Rh(1) Mo(3) 3.080(1) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
S(2) Rh(1) Mo(2) Mo(1) 63.08(3)
S(2) Rh(1) Mo(2) Mo(3) 128.54(3)
S(2) Rh(1) Mo(2) S(1) 96.73(7)
S(2) Rh(1) Mo(2) S(3) -168.15(7)
S(2) Rh(1) Mo(2) O(3) -83.8(2)
S(2) Rh(1) Mo(2) O(4) -161.8(2)
S(2) Rh(1) Mo(2) O(5) -5.4(2)
S(3) Rh(1) Mo(2) Mo(1) -128.77(4)
S(3) Rh(1) Mo(2) Mo(3) -63.31(3)
S(3) Rh(1) Mo(2) S(1) -95.12(7)
S(3) Rh(1) Mo(2) S(2) 168.15(7)
S(3) Rh(1) Mo(2) O(3) 84.3(2)
S(3) Rh(1) Mo(2) O(4) 6.4(2)
S(3) Rh(1) Mo(2) O(5) 162.8(2)
S(4) Rh(1) Mo(2) Mo(1) -32.24(3)
S(4) Rh(1) Mo(2) Mo(3) 33.22(3)
S(4) Rh(1) Mo(2) S(1) 1.42(7)
S(4) Rh(1) Mo(2) S(2) -95.32(6)
S(4) Rh(1) Mo(2) S(3) 96.53(7)
S(4) Rh(1) Mo(2) O(3) -179.2(2)
S(4) Rh(1) Mo(2) O(4) 102.9(2)
S(4) Rh(1) Mo(2) O(5) -100.7(2)
C(1) Rh(1) Mo(2) Mo(1) -179.18(5)
C(1) Rh(1) Mo(2) Mo(3) -113.72(5)
C(1) Rh(1) Mo(2) S(1) -145.52(7)
C(1) Rh(1) Mo(2) S(2) 117.75(8)
C(1) Rh(1) Mo(2) S(3) -50.40(8)
C(1) Rh(1) Mo(2) O(3) 33.9(2)
C(1) Rh(1) Mo(2) O(4) -44.0(2)
C(1) Rh(1) Mo(2) O(5) 112.3(2)
C(2) Rh(1) Mo(2) Mo(1) 138.49(5)
C(2) Rh(1) Mo(2) Mo(3) -156.05(4)
C(2) Rh(1) Mo(2) S(1) 172.15(7)
C(2) Rh(1) Mo(2) S(2) 75.42(7)
C(2) Rh(1) Mo(2) S(3) -92.73(7)
C(2) Rh(1) Mo(2) O(3) -8.4(2)
C(2) Rh(1) Mo(2) O(4) -86.3(2)
C(2) Rh(1) Mo(2) O(5) 70.0(2)
C(3) Rh(1) Mo(2) Mo(1) 96.36(4)
C(3) Rh(1) Mo(2) Mo(3) 161.82(4)
C(3) Rh(1) Mo(2) S(1) 130.01(7)
C(3) Rh(1) Mo(2) S(2) 33.28(7)
C(3) Rh(1) Mo(2) S(3) -134.87(8)
C(3) Rh(1) Mo(2) O(3) -50.6(2)
C(3) Rh(1) Mo(2) O(4) -128.5(2)
C(3) Rh(1) Mo(2) O(5) 27.9(2)
C(4) Rh(1) Mo(2) Mo(1) 56.6(2)
C(4) Rh(1) Mo(2) Mo(3) 122.1(2)
C(4) Rh(1) Mo(2) S(1) 90.3(2)
C(4) Rh(1) Mo(2) S(2) -6.5(2)
C(4) Rh(1) Mo(2) S(3) -174.6(2)
C(4) Rh(1) Mo(2) O(3) -90.3(2)
C(4) Rh(1) Mo(2) O(4) -168.2(3)
C(4) Rh(1) Mo(2) O(5) -11.9(3)
C(5) Rh(1) Mo(2) Mo(1) -139.66(9)
C(5) Rh(1) Mo(2) Mo(3) -74.20(9)
C(5) Rh(1) Mo(2) S(1) -106.0(1)
C(5) Rh(1) Mo(2) S(2) 157.3(1)
C(5) Rh(1) Mo(2) S(3) -10.9(1)
C(5) Rh(1) Mo(2) O(3) 73.4(2)
C(5) Rh(1) Mo(2) O(4) -4.5(3)
C(5) Rh(1) Mo(2) O(5) 151.9(2)
Mo(2) Rh(1) S(2) Mo(1) -75.13(6)
S(3) Rh(1) S(2) Mo(1) -84.42(5)
S(3) Rh(1) S(2) Mo(2) -9.29(5)
S(4) Rh(1) S(2) Mo(1) 13.30(5)
S(4) Rh(1) S(2) Mo(2) 88.42(5)
C(1) Rh(1) S(2) Mo(1) -179.09(5)
C(1) Rh(1) S(2) Mo(2) -103.96(7)
C(2) Rh(1) S(2) Mo(1) 166.94(5)
C(2) Rh(1) S(2) Mo(2) -117.93(5)
C(3) Rh(1) S(2) Mo(1) 128.59(5)
C(3) Rh(1) S(2) Mo(2) -156.28(5)
C(4) Rh(1) S(2) Mo(1) 103.24(6)
C(4) Rh(1) S(2) Mo(2) 178.37(4)
C(5) Rh(1) S(2) Mo(1) 126.3(1)
C(5) Rh(1) S(2) Mo(2) -158.53(8)
Mo(2) Rh(1) S(3) Mo(3) 74.94(5)
S(2) Rh(1) S(3) Mo(2) 9.20(6)
S(2) Rh(1) S(3) Mo(3) 84.14(5)
S(4) Rh(1) S(3) Mo(2) -87.72(5)
S(4) Rh(1) S(3) Mo(3) -12.78(5)
C(1) Rh(1) S(3) Mo(2) 140.28(5)
C(1) Rh(1) S(3) Mo(3) -144.79(5)
C(2) Rh(1) S(3) Mo(2) 108.01(5)
C(2) Rh(1) S(3) Mo(3) -177.05(4)
C(3) Rh(1) S(3) Mo(2) 111.06(9)
C(3) Rh(1) S(3) Mo(3) -174.00(8)
C(4) Rh(1) S(3) Mo(2) 178.03(7)
C(4) Rh(1) S(3) Mo(3) -107.04(8)
C(5) Rh(1) S(3) Mo(2) 175.12(5)
C(5) Rh(1) S(3) Mo(3) -109.94(5)
Mo(2) Rh(1) S(4) Mo(1) 36.43(6)
Mo(2) Rh(1) S(4) Mo(3) -37.58(5)
S(2) Rh(1) S(4) Mo(1) -13.66(6)
S(2) Rh(1) S(4) Mo(3) -87.67(5)
S(3) Rh(1) S(4) Mo(1) 87.18(6)
S(3) Rh(1) S(4) Mo(3) 13.17(6)
C(1) Rh(1) S(4) Mo(1) 178.94(5)
C(1) Rh(1) S(4) Mo(3) 104.93(7)
C(2) Rh(1) S(4) Mo(1) -125.7(1)
C(2) Rh(1) S(4) Mo(3) 160.3(1)
C(3) Rh(1) S(4) Mo(1) -104.25(6)
C(3) Rh(1) S(4) Mo(3) -178.26(4)
C(4) Rh(1) S(4) Mo(1) -130.55(6)
C(4) Rh(1) S(4) Mo(3) 155.44(6)
C(5) Rh(1) S(4) Mo(1) -168.37(6)
C(5) Rh(1) S(4) Mo(3) 117.62(5)
Mo(2) Rh(1) C(1) C(2) -87.1(5)
Mo(2) Rh(1) C(1) C(5) 153.4(5)
Mo(2) Rh(1) C(1) C(6) 33(1)
S(2) Rh(1) C(1) C(2) -23.1(6)
S(2) Rh(1) C(1) C(5) -142.7(5)
S(2) Rh(1) C(1) C(6) 97.9(9)
S(3) Rh(1) C(1) C(2) -123.7(4)
S(3) Rh(1) C(1) C(5) 116.7(6)
S(3) Rh(1) C(1) C(6) -2.7(9)
S(4) Rh(1) C(1) C(2) 140.2(4)
S(4) Rh(1) C(1) C(5) 20.6(7)
S(4) Rh(1) C(1) C(6) -98.8(8)
C(2) Rh(1) C(1) C(5) -119.6(7)
C(2) Rh(1) C(1) C(6) 121(1)
C(3) Rh(1) C(1) C(2) 38.7(4)
C(3) Rh(1) C(1) C(5) -80.9(5)
C(3) Rh(1) C(1) C(6) 159.7(9)
C(4) Rh(1) C(1) C(2) 81.0(4)
C(4) Rh(1) C(1) C(5) -38.6(5)
C(4) Rh(1) C(1) C(6) -157(1)
C(5) Rh(1) C(1) C(2) 119.6(6)
C(5) Rh(1) C(1) C(6) -119(1)
Mo(2) Rh(1) C(2) C(1) 114.5(4)
Mo(2) Rh(1) C(2) C(3) -128.6(4)
Mo(2) Rh(1) C(2) C(7) -9.3(9)
S(2) Rh(1) C(2) C(1) 162.7(4)
S(2) Rh(1) C(2) C(3) -80.4(5)
S(2) Rh(1) C(2) C(7) 38.9(8)
S(3) Rh(1) C(2) C(1) 60.4(4)
S(3) Rh(1) C(2) C(3) 177.3(4)
S(3) Rh(1) C(2) C(7) -63.4(9)
S(4) Rh(1) C(2) C(1) -85.2(7)
S(4) Rh(1) C(2) C(3) 31.7(8)
S(4) Rh(1) C(2) C(7) 151.0(6)
C(1) Rh(1) C(2) C(3) 116.9(6)
C(1) Rh(1) C(2) C(7) -123(1)
C(3) Rh(1) C(2) C(1) -116.9(5)
C(3) Rh(1) C(2) C(7) 119(1)
C(4) Rh(1) C(2) C(1) -79.8(4)
C(4) Rh(1) C(2) C(3) 37.1(4)
C(4) Rh(1) C(2) C(7) 156.4(9)
C(5) Rh(1) C(2) C(1) -36.8(4)
C(5) Rh(1) C(2) C(3) 80.1(4)
C(5) Rh(1) C(2) C(7) -160.6(9)
Mo(2) Rh(1) C(3) C(2) 75.9(5)
Mo(2) Rh(1) C(3) C(4) -166.4(3)
Mo(2) Rh(1) C(3) C(8) -46.7(8)
S(2) Rh(1) C(3) C(2) 100.8(5)
S(2) Rh(1) C(3) C(4) -141.5(4)
S(2) Rh(1) C(3) C(8) -21.8(7)
S(3) Rh(1) C(3) C(2) -4.6(7)
S(3) Rh(1) C(3) C(4) 113.1(5)
S(3) Rh(1) C(3) C(8) -127.2(6)
S(4) Rh(1) C(3) C(2) -163.9(4)
S(4) Rh(1) C(3) C(4) -46.2(5)
S(4) Rh(1) C(3) C(8) 73.5(7)
C(1) Rh(1) C(3) C(2) -37.5(4)
C(1) Rh(1) C(3) C(4) 80.2(4)
C(1) Rh(1) C(3) C(8) -160.1(8)
C(2) Rh(1) C(3) C(4) 117.7(6)
C(2) Rh(1) C(3) C(8) -122.6(9)
C(4) Rh(1) C(3) C(2) -117.7(6)
C(4) Rh(1) C(3) C(8) 119.7(8)
C(5) Rh(1) C(3) C(2) -80.4(5)
C(5) Rh(1) C(3) C(4) 37.3(4)
C(5) Rh(1) C(3) C(8) 157.0(7)
Mo(2) Rh(1) C(4) C(3) 49(1)
Mo(2) Rh(1) C(4) C(5) 168.7(8)
Mo(2) Rh(1) C(4) C(9) -70(1)
S(2) Rh(1) C(4) C(3) 44.3(4)
S(2) Rh(1) C(4) C(5) 163.1(4)
S(2) Rh(1) C(4) C(9) -76(1)
S(3) Rh(1) C(4) C(3) -123.4(5)
S(3) Rh(1) C(4) C(5) -4.5(7)
S(3) Rh(1) C(4) C(9) 116.0(8)
S(4) Rh(1) C(4) C(3) 139.2(4)
S(4) Rh(1) C(4) C(5) -101.9(5)
S(4) Rh(1) C(4) C(9) 18.7(9)
C(1) Rh(1) C(4) C(3) -80.4(4)
C(1) Rh(1) C(4) C(5) 38.4(4)
C(1) Rh(1) C(4) C(9) 158(1)
C(2) Rh(1) C(4) C(3) -38.2(4)
C(2) Rh(1) C(4) C(5) 80.7(5)
C(2) Rh(1) C(4) C(9) -158(1)
C(3) Rh(1) C(4) C(5) 118.9(6)
C(3) Rh(1) C(4) C(9) -120(1)
C(5) Rh(1) C(4) C(3) -118.9(5)
C(5) Rh(1) C(4) C(9) 120(1)
Mo(2) Rh(1) C(5) C(1) -58.0(9)
Mo(2) Rh(1) C(5) C(4) -174.2(4)
Mo(2) Rh(1) C(5) C(10) 62.5(9)
S(2) Rh(1) C(5) C(1) 82.1(7)
S(2) Rh(1) C(5) C(4) -34.1(7)
S(2) Rh(1) C(5) C(10) -157.4(5)
S(3) Rh(1) C(5) C(1) -66.7(6)
S(3) Rh(1) C(5) C(4) 177.1(5)
S(3) Rh(1) C(5) C(10) 53.8(6)
S(4) Rh(1) C(5) C(1) -164.8(6)
S(4) Rh(1) C(5) C(4) 79.0(5)
S(4) Rh(1) C(5) C(10) -44.3(6)
C(1) Rh(1) C(5) C(4) -116.2(7)
C(1) Rh(1) C(5) C(10) 120.5(8)
C(2) Rh(1) C(5) C(1) 36.2(5)
C(2) Rh(1) C(5) C(4) -80.0(5)
C(2) Rh(1) C(5) C(10) 156.7(7)
C(3) Rh(1) C(5) C(1) 79.6(6)
C(3) Rh(1) C(5) C(4) -36.6(5)
C(3) Rh(1) C(5) C(10) -159.9(7)
C(4) Rh(1) C(5) C(1) 116.2(7)
C(4) Rh(1) C(5) C(10) -123.3(7)
Mo(3) Mo(1) Mo(2) Rh(1) 74.14(3)
Mo(3) Mo(1) Mo(2) S(1) -64.43(7)
Mo(3) Mo(1) Mo(2) S(2) 134.48(6)
Mo(3) Mo(1) Mo(2) S(3) 35.59(6)
Mo(3) Mo(1) Mo(2) O(3) 134.9(2)
Mo(3) Mo(1) Mo(2) O(4) -56.5(2)
Mo(3) Mo(1) Mo(2) O(5) -140.2(2)
S(1) Mo(1) Mo(2) Rh(1) 138.57(4)
S(1) Mo(1) Mo(2) Mo(3) 64.43(3)
S(1) Mo(1) Mo(2) S(2) -161.09(7)
S(1) Mo(1) Mo(2) S(3) 100.02(7)
S(1) Mo(1) Mo(2) O(3) -160.7(2)
S(1) Mo(1) Mo(2) O(4) 7.9(2)
S(1) Mo(1) Mo(2) O(5) -75.8(2)
S(2) Mo(1) Mo(2) Rh(1) -60.34(3)
S(2) Mo(1) Mo(2) Mo(3) -134.48(3)
S(2) Mo(1) Mo(2) S(1) 161.09(7)
S(2) Mo(1) Mo(2) S(3) -98.89(7)
S(2) Mo(1) Mo(2) O(3) 0.4(2)
S(2) Mo(1) Mo(2) O(4) 169.0(2)
S(2) Mo(1) Mo(2) O(5) 85.3(2)
S(4) Mo(1) Mo(2) Rh(1) 33.84(3)
S(4) Mo(1) Mo(2) Mo(3) -40.29(3)
S(4) Mo(1) Mo(2) S(1) -104.72(8)
S(4) Mo(1) Mo(2) S(2) 94.19(6)
S(4) Mo(1) Mo(2) S(3) -4.70(7)
S(4) Mo(1) Mo(2) O(3) 94.6(2)
S(4) Mo(1) Mo(2) O(4) -96.8(2)
S(4) Mo(1) Mo(2) O(5) 179.5(2)
O(1) Mo(1) Mo(2) Rh(1) -54.60(5)
O(1) Mo(1) Mo(2) Mo(3) -128.74(5)
O(1) Mo(1) Mo(2) S(1) 166.83(8)
O(1) Mo(1) Mo(2) S(2) 5.74(7)
O(1) Mo(1) Mo(2) S(3) -93.15(8)
O(1) Mo(1) Mo(2) O(3) 6.2(3)
O(1) Mo(1) Mo(2) O(4) 174.7(2)
O(1) Mo(1) Mo(2) O(5) 91.1(2)
O(2) Mo(1) Mo(2) Rh(1) -135.95(4)
O(2) Mo(1) Mo(2) Mo(3) 149.91(4)
O(2) Mo(1) Mo(2) S(1) 85.48(7)
O(2) Mo(1) Mo(2) S(2) -75.61(7)
O(2) Mo(1) Mo(2) S(3) -174.50(7)
O(2) Mo(1) Mo(2) O(3) -75.2(2)
O(2) Mo(1) Mo(2) O(4) 93.4(2)
O(2) Mo(1) Mo(2) O(5) 9.7(2)
Mo(2) Mo(1) Mo(3) S(1) 64.11(6)
Mo(2) Mo(1) Mo(3) S(3) -34.56(5)
Mo(2) Mo(1) Mo(3) S(4) -126.89(7)
Mo(2) Mo(1) Mo(3) O(6) -126.1(2)
Mo(2) Mo(1) Mo(3) O(7) 143.8(1)
Mo(2) Mo(1) Mo(3) O(8) 55.9(2)
S(1) Mo(1) Mo(3) Mo(2) -64.11(3)
S(1) Mo(1) Mo(3) S(3) -98.67(5)
S(1) Mo(1) Mo(3) S(4) 169.00(7)
S(1) Mo(1) Mo(3) O(6) 169.8(2)
S(1) Mo(1) Mo(3) O(7) 79.7(1)
S(1) Mo(1) Mo(3) O(8) -8.2(2)
S(2) Mo(1) Mo(3) Mo(2) 34.71(2)
S(2) Mo(1) Mo(3) S(1) 98.82(6)
S(2) Mo(1) Mo(3) S(3) 0.15(5)
S(2) Mo(1) Mo(3) S(4) -92.18(7)
S(2) Mo(1) Mo(3) O(6) -91.4(2)
S(2) Mo(1) Mo(3) O(7) 178.5(1)
S(2) Mo(1) Mo(3) O(8) 90.6(2)
S(4) Mo(1) Mo(3) Mo(2) 126.89(3)
S(4) Mo(1) Mo(3) S(1) -169.00(7)
S(4) Mo(1) Mo(3) S(3) 92.33(5)
S(4) Mo(1) Mo(3) O(6) 0.8(2)
S(4) Mo(1) Mo(3) O(7) -89.3(1)
S(4) Mo(1) Mo(3) O(8) -177.2(2)
O(1) Mo(1) Mo(3) Mo(2) 124.13(5)
O(1) Mo(1) Mo(3) S(1) -171.76(8)
O(1) Mo(1) Mo(3) S(3) 89.57(7)
O(1) Mo(1) Mo(3) S(4) -2.76(8)
O(1) Mo(1) Mo(3) O(6) -2.0(2)
O(1) Mo(1) Mo(3) O(7) -92.1(2)
O(1) Mo(1) Mo(3) O(8) 180.0(2)
O(2) Mo(1) Mo(3) Mo(2) -56.10(6)
O(2) Mo(1) Mo(3) S(1) 8.01(8)
O(2) Mo(1) Mo(3) S(3) -90.66(7)
O(2) Mo(1) Mo(3) S(4) 177.01(9)
O(2) Mo(1) Mo(3) O(6) 177.8(2)
O(2) Mo(1) Mo(3) O(7) 87.7(2)
O(2) Mo(1) Mo(3) O(8) -0.2(2)
Mo(2) Mo(1) S(1) Mo(3) -77.95(5)
Mo(3) Mo(1) S(1) Mo(2) 77.95(5)
S(2) Mo(1) S(1) Mo(2) -15.15(6)
S(2) Mo(1) S(1) Mo(3) -93.10(5)
S(4) Mo(1) S(1) Mo(2) 87.12(6)
S(4) Mo(1) S(1) Mo(3) 9.17(6)
O(1) Mo(1) S(1) Mo(2) -129.3(3)
O(1) Mo(1) S(1) Mo(3) 152.7(3)
O(2) Mo(1) S(1) Mo(2) -97.25(5)
O(2) Mo(1) S(1) Mo(3) -175.20(5)
Mo(2) Mo(1) S(2) Rh(1) 79.35(6)
Mo(3) Mo(1) S(2) Rh(1) 40.13(5)
Mo(3) Mo(1) S(2) Mo(2) -39.21(5)
S(1) Mo(1) S(2) Rh(1) 94.83(5)
S(1) Mo(1) S(2) Mo(2) 15.48(5)
S(4) Mo(1) S(2) Rh(1) -13.85(6)
S(4) Mo(1) S(2) Mo(2) -93.20(5)
O(1) Mo(1) S(2) Rh(1) -96.47(5)
O(1) Mo(1) S(2) Mo(2) -175.82(5)
O(2) Mo(1) S(2) Rh(1) -177.19(6)
O(2) Mo(1) S(2) Mo(2) 103.46(5)
Mo(2) Mo(1) S(4) Rh(1) -38.55(6)
Mo(2) Mo(1) S(4) Mo(3) 44.68(5)
Mo(3) Mo(1) S(4) Rh(1) -83.23(5)
S(1) Mo(1) S(4) Rh(1) -92.43(6)
S(1) Mo(1) S(4) Mo(3) -9.20(6)
S(2) Mo(1) S(4) Rh(1) 13.70(6)
S(2) Mo(1) S(4) Mo(3) 96.94(5)
O(1) Mo(1) S(4) Rh(1) 94.88(6)
O(1) Mo(1) S(4) Mo(3) 178.11(5)
O(2) Mo(1) S(4) Rh(1) 103.1(2)
O(2) Mo(1) S(4) Mo(3) -173.7(2)
Rh(1) Mo(2) Mo(3) Mo(1) -75.48(2)
Rh(1) Mo(2) Mo(3) S(1) -140.70(7)
Rh(1) Mo(2) Mo(3) S(3) 59.76(7)
Rh(1) Mo(2) Mo(3) S(4) -35.02(4)
Rh(1) Mo(2) Mo(3) O(6) 51.4(2)
Rh(1) Mo(2) Mo(3) O(7) -141.0(3)
Rh(1) Mo(2) Mo(3) O(8) 135.3(1)
Mo(1) Mo(2) Mo(3) S(1) -65.22(7)
Mo(1) Mo(2) Mo(3) S(3) 135.24(7)
Mo(1) Mo(2) Mo(3) S(4) 40.46(5)
Mo(1) Mo(2) Mo(3) O(6) 126.9(2)
Mo(1) Mo(2) Mo(3) O(7) -65.5(3)
Mo(1) Mo(2) Mo(3) O(8) -149.2(1)
S(1) Mo(2) Mo(3) Mo(1) 65.22(3)
S(1) Mo(2) Mo(3) S(3) -159.54(7)
S(1) Mo(2) Mo(3) S(4) 105.68(5)
S(1) Mo(2) Mo(3) O(6) -167.9(2)
S(1) Mo(2) Mo(3) O(7) -0.3(3)
S(1) Mo(2) Mo(3) O(8) -84.0(1)
S(2) Mo(2) Mo(3) Mo(1) -36.27(2)
S(2) Mo(2) Mo(3) S(1) -101.49(7)
S(2) Mo(2) Mo(3) S(3) 98.97(7)
S(2) Mo(2) Mo(3) S(4) 4.18(5)
S(2) Mo(2) Mo(3) O(6) 90.6(2)
S(2) Mo(2) Mo(3) O(7) -101.8(3)
S(2) Mo(2) Mo(3) O(8) 174.5(1)
S(3) Mo(2) Mo(3) Mo(1) -135.24(3)
S(3) Mo(2) Mo(3) S(1) 159.54(7)
S(3) Mo(2) Mo(3) S(4) -94.79(5)
S(3) Mo(2) Mo(3) O(6) -8.4(2)
S(3) Mo(2) Mo(3) O(7) 159.2(3)
S(3) Mo(2) Mo(3) O(8) 75.5(1)
O(3) Mo(2) Mo(3) Mo(1) -134.68(6)
O(3) Mo(2) Mo(3) S(1) 160.10(9)
O(3) Mo(2) Mo(3) S(3) 0.57(8)
O(3) Mo(2) Mo(3) S(4) -94.22(7)
O(3) Mo(2) Mo(3) O(6) -7.8(2)
O(3) Mo(2) Mo(3) O(7) 159.8(3)
O(3) Mo(2) Mo(3) O(8) 76.1(1)
O(4) Mo(2) Mo(3) Mo(1) 146.46(3)
O(4) Mo(2) Mo(3) S(1) 81.24(7)
O(4) Mo(2) Mo(3) S(3) -78.30(7)
O(4) Mo(2) Mo(3) S(4) -173.08(5)
O(4) Mo(2) Mo(3) O(6) -86.7(2)
O(4) Mo(2) Mo(3) O(7) 80.9(3)
O(4) Mo(2) Mo(3) O(8) -2.8(1)
O(5) Mo(2) Mo(3) Mo(1) 65.98(5)
O(5) Mo(2) Mo(3) S(1) 0.76(8)
O(5) Mo(2) Mo(3) S(3) -158.78(9)
O(5) Mo(2) Mo(3) S(4) 106.44(7)
O(5) Mo(2) Mo(3) O(6) -167.2(2)
O(5) Mo(2) Mo(3) O(7) 0.5(3)
O(5) Mo(2) Mo(3) O(8) -83.3(1)
Rh(1) Mo(2) S(1) Mo(1) -39.04(6)
Rh(1) Mo(2) S(1) Mo(3) 36.80(6)
Mo(1) Mo(2) S(1) Mo(3) 75.84(5)
Mo(3) Mo(2) S(1) Mo(1) -75.84(5)
S(2) Mo(2) S(1) Mo(1) 15.91(6)
S(2) Mo(2) S(1) Mo(3) 91.75(6)
S(3) Mo(2) S(1) Mo(1) -92.88(5)
S(3) Mo(2) S(1) Mo(3) -17.04(6)
O(3) Mo(2) S(1) Mo(1) 142.6(2)
O(3) Mo(2) S(1) Mo(3) -141.5(2)
O(4) Mo(2) S(1) Mo(1) -174.78(6)
O(4) Mo(2) S(1) Mo(3) -98.94(5)
O(5) Mo(2) S(1) Mo(1) 104.70(5)
O(5) Mo(2) S(1) Mo(3) -179.47(6)
Rh(1) Mo(2) S(2) Mo(1) 84.35(6)
Mo(1) Mo(2) S(2) Rh(1) -84.35(6)
Mo(3) Mo(2) S(2) Rh(1) -46.00(5)
Mo(3) Mo(2) S(2) Mo(1) 38.35(4)
S(1) Mo(2) S(2) Rh(1) -99.96(5)
S(1) Mo(2) S(2) Mo(1) -15.62(5)
S(3) Mo(2) S(2) Rh(1) 9.54(5)
S(3) Mo(2) S(2) Mo(1) 93.89(4)
O(3) Mo(2) S(2) Rh(1) 95.91(4)
O(3) Mo(2) S(2) Mo(1) -179.74(5)
O(4) Mo(2) S(2) Rh(1) 123.8(2)
O(4) Mo(2) S(2) Mo(1) -151.9(2)
O(5) Mo(2) S(2) Rh(1) 176.76(5)
O(5) Mo(2) S(2) Mo(1) -98.90(4)
Rh(1) Mo(2) S(3) Mo(3) -83.99(5)
Mo(1) Mo(2) S(3) Rh(1) 46.21(6)
Mo(1) Mo(2) S(3) Mo(3) -37.78(5)
Mo(3) Mo(2) S(3) Rh(1) 83.99(5)
S(1) Mo(2) S(3) Rh(1) 100.67(5)
S(1) Mo(2) S(3) Mo(3) 16.68(6)
S(2) Mo(2) S(3) Rh(1) -9.65(6)
S(2) Mo(2) S(3) Mo(3) -93.64(5)
O(3) Mo(2) S(3) Rh(1) -95.66(5)
O(3) Mo(2) S(3) Mo(3) -179.65(5)
O(4) Mo(2) S(3) Rh(1) -175.43(6)
O(4) Mo(2) S(3) Mo(3) 100.58(5)
O(5) Mo(2) S(3) Rh(1) -146.7(2)
O(5) Mo(2) S(3) Mo(3) 129.3(2)
Mo(1) Mo(3) S(1) Mo(2) -77.42(6)
Mo(2) Mo(3) S(1) Mo(1) 77.42(6)
S(3) Mo(3) S(1) Mo(1) 93.93(5)
S(3) Mo(3) S(1) Mo(2) 16.51(6)
S(4) Mo(3) S(1) Mo(1) -9.24(6)
S(4) Mo(3) S(1) Mo(2) -86.66(5)
O(6) Mo(3) S(1) Mo(1) -145.2(2)
O(6) Mo(3) S(1) Mo(2) 137.4(2)
O(7) Mo(3) S(1) Mo(1) -102.78(5)
O(7) Mo(3) S(1) Mo(2) 179.81(6)
O(8) Mo(3) S(1) Mo(1) 174.94(5)
O(8) Mo(3) S(1) Mo(2) 97.52(5)
Mo(1) Mo(3) S(3) Rh(1) -40.98(5)
Mo(1) Mo(3) S(3) Mo(2) 38.66(5)
Mo(2) Mo(3) S(3) Rh(1) -79.64(7)
S(1) Mo(3) S(3) Rh(1) -96.42(5)
S(1) Mo(3) S(3) Mo(2) -16.77(6)
S(4) Mo(3) S(3) Rh(1) 13.35(6)
S(4) Mo(3) S(3) Mo(2) 92.99(5)
O(6) Mo(3) S(3) Rh(1) 94.42(5)
O(6) Mo(3) S(3) Mo(2) 174.06(6)
O(7) Mo(3) S(3) Rh(1) 143.9(1)
O(7) Mo(3) S(3) Mo(2) -136.5(1)
O(8) Mo(3) S(3) Rh(1) 177.49(6)
O(8) Mo(3) S(3) Mo(2) -102.87(5)
Mo(1) Mo(3) S(4) Rh(1) 84.41(7)
Mo(2) Mo(3) S(4) Rh(1) 39.76(5)
Mo(2) Mo(3) S(4) Mo(1) -44.65(5)
S(1) Mo(3) S(4) Rh(1) 93.71(5)
S(1) Mo(3) S(4) Mo(1) 9.31(6)
S(3) Mo(3) S(4) Rh(1) -13.06(6)
S(3) Mo(3) S(4) Mo(1) -97.47(5)
O(6) Mo(3) S(4) Rh(1) -95.07(5)
O(6) Mo(3) S(4) Mo(1) -179.47(5)
O(7) Mo(3) S(4) Rh(1) -178.48(5)
O(7) Mo(3) S(4) Mo(1) 97.12(5)
O(8) Mo(3) S(4) Rh(1) -101.9(2)
O(8) Mo(3) S(4) Mo(1) 173.7(2)
O(9) S(5) C(11) C(12) -73.3(6)
O(9) S(5) C(11) C(16) 105.7(6)
O(10) S(5) C(11) C(12) 46.0(6)
O(10) S(5) C(11) C(16) -135.0(6)
O(11) S(5) C(11) C(12) 166.2(5)
O(11) S(5) C(11) C(16) -14.8(6)
O(12) S(6) C(18) C(19) 54.9(8)
O(12) S(6) C(18) C(23) -128.5(7)
O(13) S(6) C(18) C(19) -64.1(8)
O(13) S(6) C(18) C(23) 112.5(7)
O(14) S(6) C(18) C(19) 176.0(7)
O(14) S(6) C(18) C(23) -7.4(9)
O(15) S(7) C(32) C(33) 37.6(7)
O(15) S(7) C(32) C(37) -146.8(6)
O(16) S(7) C(32) C(33) 157.7(6)
O(16) S(7) C(32) C(37) -26.7(7)
O(17) S(7) C(32) C(33) -83.2(7)
O(17) S(7) C(32) C(37) 92.4(7)
O(18) S(8) C(25) C(26) -138.8(6)
O(18) S(8) C(25) C(30) 46.0(7)
O(19) S(8) C(25) C(26) -18.8(7)
O(19) S(8) C(25) C(30) 166.0(6)
O(20) S(8) C(25) C(26) 103.0(6)
O(20) S(8) C(25) C(30) -72.2(7)
Rh(1) C(1) C(2) C(3) -61.9(5)
Rh(1) C(1) C(2) C(7) 123.3(8)
C(5) C(1) C(2) Rh(1) 60.4(5)
C(5) C(1) C(2) C(3) -1.5(8)
C(5) C(1) C(2) C(7) -176.3(7)
C(6) C(1) C(2) Rh(1) -125.5(7)
C(6) C(1) C(2) C(3) 172.6(7)
C(6) C(1) C(2) C(7) -2(1)
Rh(1) C(1) C(5) C(4) 63.1(6)
Rh(1) C(1) C(5) C(10) -121.4(8)
C(2) C(1) C(5) Rh(1) -60.7(5)
C(2) C(1) C(5) C(4) 2.5(8)
C(2) C(1) C(5) C(10) 177.9(7)
C(6) C(1) C(5) Rh(1) 125.1(8)
C(6) C(1) C(5) C(4) -171.7(7)
C(6) C(1) C(5) C(10) 3(1)
Rh(1) C(2) C(3) C(4) -62.3(6)
Rh(1) C(2) C(3) C(8) 124.7(7)
C(1) C(2) C(3) Rh(1) 62.2(5)
C(1) C(2) C(3) C(4) -0.1(6)
C(1) C(2) C(3) C(8) -173.1(7)
C(7) C(2) C(3) Rh(1) -122.8(7)
C(7) C(2) C(3) C(4) 175.0(6)
C(7) C(2) C(3) C(8) 1(1)
Rh(1) C(3) C(4) C(5) -59.7(6)
Rh(1) C(3) C(4) C(9) 123.1(7)
C(2) C(3) C(4) Rh(1) 61.3(5)
C(2) C(3) C(4) C(5) 1.6(8)
C(2) C(3) C(4) C(9) -175.7(7)
C(8) C(3) C(4) Rh(1) -125.4(6)
C(8) C(3) C(4) C(5) 174.9(6)
C(8) C(3) C(4) C(9) -2(1)
Rh(1) C(4) C(5) C(1) -62.7(5)
Rh(1) C(4) C(5) C(10) 122.0(8)
C(3) C(4) C(5) Rh(1) 60.1(5)
C(3) C(4) C(5) C(1) -2.5(8)
C(3) C(4) C(5) C(10) -177.9(7)
C(9) C(4) C(5) Rh(1) -122.6(8)
C(9) C(4) C(5) C(1) 174.7(7)
C(9) C(4) C(5) C(10) 0(1)
S(5) C(11) C(12) C(13) 177.8(6)
C(16) C(11) C(12) C(13) -1(1)
S(5) C(11) C(16) C(15) -177.3(6)
C(12) C(11) C(16) C(15) 1(1)
C(11) C(12) C(13) C(14) 1(1)
C(12) C(13) C(14) C(15) -2(1)
C(12) C(13) C(14) C(17) 177.8(8)
C(13) C(14) C(15) C(16) 3(1)
C(17) C(14) C(15) C(16) -177.3(7)
C(14) C(15) C(16) C(11) -2(1)
S(6) C(18) C(19) C(20) 175.3(8)
C(23) C(18) C(19) C(20) -1(1)
S(6) C(18) C(23) C(22) -176.3(8)
C(19) C(18) C(23) C(22) 0(1)
C(18) C(19) C(20) C(21) 1(1)
C(19) C(20) C(21) C(22) 0(1)
C(19) C(20) C(21) C(24) -178.7(9)
C(20) C(21) C(22) C(23) 0(1)
C(24) C(21) C(22) C(23) 177.7(9)
C(21) C(22) C(23) C(18) 0(1)
S(8) C(25) C(26) C(27) -176.5(7)
C(30) C(25) C(26) C(27) -1(1)
S(8) C(25) C(30) C(29) 176.3(7)
C(26) C(25) C(30) C(29) 1(1)
C(25) C(26) C(27) C(28) 0(1)
C(26) C(27) C(28) C(29) 0(1)
C(26) C(27) C(28) C(31) -179.1(8)
C(27) C(28) C(29) C(30) -1(1)
C(31) C(28) C(29) C(30) 178.8(8)
C(28) C(29) C(30) C(25) 0(1)
S(7) C(32) C(33) C(34) 174.8(7)
C(37) C(32) C(33) C(34) 0(1)
S(7) C(32) C(37) C(36) -173.6(7)
C(33) C(32) C(37) C(36) 2(1)
C(32) C(33) C(34) C(35) 0(1)
C(33) C(34) C(35) C(36) 1(1)
C(33) C(34) C(35) C(38) -178.6(9)
C(34) C(35) C(36) C(37) 0(1)
C(38) C(35) C(36) C(37) 179.9(6)
C(35) C(36) C(37) C(32) -1(1)
