#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:42:23 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179512 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/09/4340938.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4340938
loop_
_publ_author_name
'Baldoví, José J'
'Clemente-Juan, Juan M'
'Coronado, Eugenio'
'Duan, Yan'
'Gaita-Ariño, Alejandro'
'Giménez-Saiz, Carlos'
_publ_section_title
;
 Construction of a general library for the rational design of nanomagnets
 and spin qubits based on mononuclear f-block complexes. The
 polyoxometalate case.
;
_journal_issue                   18
_journal_name_full               'Inorganic chemistry'
_journal_page_first              9976
_journal_page_last               9980
_journal_paper_doi               10.1021/ic501867d
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'H64 Na9 Nd O68 W10'
_chemical_formula_weight         3342.16
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.1224(15)
_cell_angle_beta                 103.9474(16)
_cell_angle_gamma                90.3027(12)
_cell_formula_units_Z            2
_cell_length_a                   12.81263(19)
_cell_length_b                   13.0074(2)
_cell_length_c                   19.3992(4)
_cell_measurement_reflns_used    30415
_cell_measurement_temperature    120.00(10)
_cell_measurement_theta_max      32.3540
_cell_measurement_theta_min      3.2350
_cell_volume                     3128.76(10)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      120.00(10)
_diffrn_detector_area_resol_mean 16.0267
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.937
_diffrn_measurement_details
;
  1 omega  -76.00  -43.80   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -      -23.5000 -178.0000 -120.0000 46

  2 omega  -35.00   -2.80   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -      -23.5000  -57.0000  150.0000 46

  3 omega  -19.00    8.30   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -      -23.5000  -83.0000 -152.0000 39

  4 omega  -63.00  -33.60   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -      -23.5000  -38.0000 -150.0000 42

  5 omega   45.00   72.30   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590 -178.0000  150.0000 39

  6 omega  -10.00   63.50   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -99.0000  -60.0000 105

  7 omega  -11.00   98.20   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   19.0000  -60.0000 156

  8 omega    9.00   68.50   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -99.0000 -180.0000 85

  9 omega  -42.00   55.30   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -77.0000    0.0000 139

 10 omega   -3.00   96.40   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   77.0000  120.0000 142

 11 omega  -42.00   46.90   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -57.0000   90.0000 127

 12 omega  -46.00   52.00   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -38.0000 -150.0000 140

 13 omega    6.00   94.90   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   57.0000 -120.0000 127

 14 omega   35.00  101.50   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  178.0000  120.0000 95

 15 omega   -3.00   95.70   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   77.0000   90.0000 141

 16 omega   -3.00   95.70   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   77.0000  -30.0000 141

 17 omega  -42.00   29.40   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590  -57.0000  -30.0000 102

 18 omega    1.00   99.00   0.7000    4.0000
omega____ theta____ kappa____ phi______ frames
    -       26.7590   38.0000   30.0000 140

;
_diffrn_measurement_device_type
'SuperNova, Single source at offset, Sapphire3'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      -0.0506643000
_diffrn_orient_matrix_UB_12      0.0206711000
_diffrn_orient_matrix_UB_13      0.0013046000
_diffrn_orient_matrix_UB_21      0.0033136000
_diffrn_orient_matrix_UB_22      -0.0216161000
_diffrn_orient_matrix_UB_23      0.0329810000
_diffrn_orient_matrix_UB_31      0.0260312000
_diffrn_orient_matrix_UB_32      0.0457831000
_diffrn_orient_matrix_UB_33      0.0183847000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0566
_diffrn_reflns_av_sigmaI/netI    0.0455
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            100504
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         32.51
_diffrn_reflns_theta_min         2.92
_exptl_absorpt_coefficient_mu    19.304
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.37284
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            grey
_exptl_crystal_density_diffrn    3.548
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3014
_exptl_crystal_size_max          0.4340
_exptl_crystal_size_mid          0.3013
_exptl_crystal_size_min          0.1312
_refine_diff_density_max         6.187
_refine_diff_density_min         -3.241
_refine_diff_density_rms         0.431
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.105
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     803
_refine_ls_number_reflns         21237
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.105
_refine_ls_R_factor_all          0.0541
_refine_ls_R_factor_gt           0.0381
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0365P)²+41.6254P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0863
_refine_ls_wR_factor_ref         0.0969
_reflns_number_gt                17458
_reflns_number_total             21237
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic501867d_si_002.cif
_cod_data_source_block           compound_11
_cod_depositor_comments          'Adding full bibliography for 4340938.cif.'
_cod_original_cell_volume        3128.77(10)
_cod_database_code               4340938
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
W1 W 0.96221(2) 0.01755(2) 0.684943(16) 0.00946(6) Uani 1 1 d .
W2 W 0.85858(2) -0.01290(2) 0.825217(15) 0.00886(5) Uani 1 1 d .
W3 W 0.98119(2) -0.20488(2) 0.761651(15) 0.00890(5) Uani 1 1 d .
W4 W 0.81993(2) -0.19074(2) 0.604101(15) 0.00962(6) Uani 1 1 d .
W5 W 0.69766(2) 0.00257(2) 0.668282(15) 0.00927(6) Uani 1 1 d .
W6 W 0.41708(2) -0.54345(2) 0.815925(16) 0.00957(6) Uani 1 1 d .
W7 W 0.65756(2) -0.43516(2) 0.895934(15) 0.00886(5) Uani 1 1 d .
W8 W 0.61771(2) -0.54689(2) 0.733499(16) 0.00913(6) Uani 1 1 d .
W9 W 0.41134(2) -0.39799(2) 0.679652(15) 0.00898(5) Uani 1 1 d .
W10 W 0.44842(2) -0.28844(2) 0.839384(15) 0.00867(5) Uani 1 1 d .
Nd1 Nd 0.68236(3) -0.25698(3) 0.75157(2) 0.00901(7) Uani 1 1 d .
O1 O 1.0481(4) 0.1074(4) 0.6614(3) 0.0163(11) Uani 1 1 d .
O2 O 0.8267(4) 0.0807(4) 0.6543(3) 0.0116(10) Uani 1 1 d .
O3 O 1.0560(4) -0.0863(4) 0.7270(3) 0.0118(10) Uani 1 1 d .
O4 O 0.9222(4) -0.0732(4) 0.6012(3) 0.0126(10) Uani 1 1 d .
O5 O 0.9567(4) 0.0677(4) 0.7791(3) 0.0106(10) Uani 1 1 d .
O6 O 0.8840(5) 0.0623(4) 0.9044(3) 0.0144(11) Uani 1 1 d .
O7 O 1.0990(4) -0.2705(4) 0.7937(3) 0.0145(11) Uani 1 1 d .
O8 O 0.8158(5) -0.2451(4) 0.5198(3) 0.0170(11) Uani 1 1 d .
O9 O 0.6037(4) 0.0909(4) 0.6277(3) 0.0135(10) Uani 1 1 d .
O10 O 0.9795(4) -0.1076(4) 0.8420(3) 0.0110(10) Uani 1 1 d .
O11 O 0.9455(4) -0.2520(4) 0.6614(3) 0.0104(9) Uani 1 1 d .
O12 O 0.7126(4) -0.0831(4) 0.5857(3) 0.0110(10) Uani 1 1 d .
O13 O 0.7457(4) 0.0615(4) 0.7652(3) 0.0101(9) Uani 1 1 d .
O14 O 0.8450(4) -0.0960(4) 0.7132(3) 0.0092(9) Uani 1 1 d .
O15 O 0.7674(4) -0.1125(4) 0.8358(3) 0.0106(10) Uani 1 1 d .
O16 O 0.8776(4) -0.2850(4) 0.7788(3) 0.0114(10) Uani 1 1 d .
O17 O 0.7289(4) -0.2698(4) 0.6364(3) 0.0114(10) Uani 1 1 d .
O18 O 0.6186(4) -0.0948(4) 0.6945(3) 0.0110(10) Uani 1 1 d .
O19 O 0.5425(4) -0.2053(4) 0.8126(3) 0.0118(10) Uani 1 1 d .
O20 O 0.7297(4) -0.3374(4) 0.8637(3) 0.0106(10) Uani 1 1 d .
O21 O 0.6966(4) -0.4400(4) 0.7192(3) 0.0115(10) Uani 1 1 d .
O22 O 0.5106(4) -0.3059(4) 0.6683(3) 0.0121(10) Uani 1 1 d .
O23 O 0.5272(4) -0.4216(4) 0.7869(3) 0.0099(9) Uani 1 1 d .
O24 O 0.5573(4) -0.3328(4) 0.9195(3) 0.0098(9) Uani 1 1 d .
O25 O 0.6963(4) -0.5440(4) 0.8331(3) 0.0101(9) Uani 1 1 d .
O26 O 0.4967(4) -0.5135(4) 0.6560(3) 0.0100(9) Uani 1 1 d .
O27 O 0.3570(4) -0.3017(4) 0.7428(3) 0.0116(10) Uani 1 1 d .
O28 O 0.7410(5) -0.4581(4) 0.9766(3) 0.0159(11) Uani 1 1 d .
O29 O 0.6693(5) -0.6528(4) 0.6939(3) 0.0150(11) Uani 1 1 d .
O30 O 0.3107(5) -0.3939(5) 0.6028(3) 0.0165(11) Uani 1 1 d .
O31 O 0.3748(4) -0.2047(4) 0.8817(3) 0.0135(10) Uani 1 1 d .
O32 O 0.3684(4) -0.4179(4) 0.8513(3) 0.0119(10) Uani 1 1 d .
O33 O 0.5355(4) -0.5341(4) 0.8960(3) 0.0126(10) Uani 1 1 d .
O34 O 0.5043(4) -0.6236(4) 0.7661(3) 0.0100(9) Uani 1 1 d .
O35 O 0.3381(4) -0.5068(4) 0.7226(3) 0.0115(10) Uani 1 1 d .
O36 O 0.3305(5) -0.6367(4) 0.8337(3) 0.0164(11) Uani 1 1 d .
O1W O 0.7747(5) -0.3517(5) 0.3761(4) 0.0289(15) Uani 1 1 d .
O2W O 0.6056(5) 0.5770(5) 0.5537(3) 0.0190(12) Uani 1 1 d .
O3W O 1.1213(5) -0.5206(5) 1.3315(3) 0.0209(12) Uani 1 1 d .
O4W O 0.8010(5) -0.6304(4) 1.0857(3) 0.0165(11) Uani 1 1 d .
O5W O 0.8838(5) -0.1606(5) 0.0991(3) 0.0205(12) Uani 1 1 d .
O6W O 0.9489(6) 0.2848(6) 0.4825(4) 0.0333(16) Uani 1 1 d .
O7W O 1.1218(5) -0.2822(5) 1.2308(4) 0.0226(13) Uani 1 1 d .
O8W O 0.7410(5) 0.0389(4) 0.1797(3) 0.0165(11) Uani 1 1 d .
O9W O 0.5999(5) 0.0612(5) -0.0097(3) 0.0215(12) Uani 1 1 d .
O10W O 0.6101(5) -0.0524(5) 0.4479(3) 0.0186(12) Uani 1 1 d .
O11W O 0.4381(5) -0.0092(4) 0.1585(3) 0.0166(11) Uani 1 1 d .
O12W O 0.4517(5) -0.3007(4) 1.0267(3) 0.0145(11) Uani 1 1 d .
O13W O 0.8706(5) -0.5385(4) 1.2734(3) 0.0184(12) Uani 1 1 d .
O14W O 0.7866(5) 0.1737(5) 0.5329(3) 0.0202(12) Uani 1 1 d .
O15W O 1.0680(5) -0.5267(5) 1.1576(3) 0.0181(12) Uani 1 1 d .
O16W O 0.8438(5) 0.0887(5) 0.0410(3) 0.0169(11) Uani 1 1 d .
O17W O 0.5333(5) -0.1768(5) 0.2883(3) 0.0204(12) Uani 1 1 d .
O18W O 0.9627(5) -0.6170(5) 0.9760(3) 0.0201(12) Uani 1 1 d .
O19W O 0.6125(5) -0.1675(4) 0.1083(3) 0.0173(11) Uani 1 1 d .
O20W O 0.5971(5) 0.0795(4) 0.3033(3) 0.0168(11) Uani 1 1 d .
O21W O 0.8753(5) -0.3634(5) 1.1435(3) 0.0175(11) Uani 1 1 d .
O22W O 0.0823(5) 0.2326(5) 0.0458(3) 0.0218(13) Uani 1 1 d .
O23W O 0.5536(5) -0.3046(5) 0.4316(3) 0.0191(12) Uani 1 1 d .
O24W O 0.2393(5) -0.2694(5) 1.0963(4) 0.0238(13) Uani 1 1 d .
O25W O 0.9740(5) -0.3205(5) 1.3465(4) 0.0240(14) Uani 1 1 d .
O26W O 0.7115(5) 0.3980(5) 0.5393(3) 0.0191(12) Uani 1 1 d .
O27W O 0.8368(6) -0.0466(6) 0.4422(4) 0.0288(15) Uani 1 1 d .
O28W O 0.6921(5) -0.1457(5) 0.9595(3) 0.0199(12) Uani 1 1 d .
O29W O 0.5424(6) 0.1899(5) 0.4480(3) 0.0233(13) Uani 1 1 d .
O30W O 0.8178(5) 0.1914(5) 0.3586(3) 0.0214(13) Uani 1 1 d .
O31W O 0.7481(5) -0.1784(5) 0.2694(4) 0.0330(17) Uani 1 1 d .
O32W O 1.0489(7) 0.5191(8) 0.5797(5) 0.030(3) Uani 0.74(2) 1 d PU
O33W O 1.0051(19) 0.5740(18) 0.6078(13) 0.020(6) Uani 0.26(2) 1 d PU
Na1 Na 0.7058(3) 0.0898(3) 0.42068(18) 0.0180(7) Uani 1 1 d .
Na2 Na 0.9127(3) -0.4953(2) 1.05995(18) 0.0157(6) Uani 1 1 d .
Na3 Na 0.7284(3) -0.0498(3) 0.06519(18) 0.0163(6) Uani 1 1 d .
Na4 Na 0.2876(3) -0.2202(3) 0.98887(18) 0.0181(7) Uani 1 1 d .
Na5 Na 0.6886(3) -0.1947(3) 0.3936(2) 0.0270(8) Uani 1 1 d .
Na6 Na 0.6110(3) -0.0655(2) 0.21855(17) 0.0145(6) Uani 1 1 d .
Na7 Na 0.6299(3) 0.2513(3) 0.57102(18) 0.0180(7) Uani 1 1 d .
Na8 Na 1.0020(3) -0.4197(3) 1.24377(18) 0.0165(6) Uani 1 1 d .
Na9 Na 0.9014(4) 0.4125(4) 0.5734(2) 0.0367(10) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nd Nd -0.1943 3.0179 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 W1 O4 102.5(3) . .
O1 W1 O2 100.9(2) . .
O4 W1 O2 87.3(2) . .
O1 W1 O3 104.2(2) . .
O4 W1 O3 87.8(2) . .
O2 W1 O3 154.9(2) . .
O1 W1 O5 103.4(3) . .
O4 W1 O5 154.1(2) . .
O2 W1 O5 86.0(2) . .
O3 W1 O5 87.7(2) . .
O1 W1 O14 177.8(2) . .
O4 W1 O14 77.2(2) . .
O2 W1 O14 77.0(2) . .
O3 W1 O14 77.9(2) . .
O5 W1 O14 76.9(2) . .
O6 W2 O15 104.6(2) . .
O6 W2 O13 102.2(2) . .
O15 W2 O13 93.1(2) . .
O6 W2 O10 101.8(2) . .
O15 W2 O10 91.3(2) . .
O13 W2 O10 153.6(2) . .
O6 W2 O5 96.5(2) . .
O15 W2 O5 158.8(2) . .
O13 W2 O5 83.7(2) . .
O10 W2 O5 82.9(2) . .
O6 W2 O14 170.3(2) . .
O15 W2 O14 85.1(2) . .
O13 W2 O14 77.37(19) . .
O10 W2 O14 77.1(2) . .
O5 W2 O14 73.83(19) . .
O7 W3 O16 104.1(3) . .
O7 W3 O10 101.6(2) . .
O16 W3 O10 92.9(2) . .
O7 W3 O11 101.8(2) . .
O16 W3 O11 92.1(2) . .
O10 W3 O11 154.1(2) . .
O7 W3 O3 94.9(2) . .
O16 W3 O3 161.0(2) . .
O10 W3 O3 84.2(2) . .
O11 W3 O3 82.9(2) . .
O7 W3 O14 169.5(2) . .
O16 W3 O14 86.4(2) . .
O10 W3 O14 77.7(2) . .
O11 W3 O14 77.26(19) . .
O3 W3 O14 74.62(19) . .
O8 W4 O17 104.6(3) . .
O8 W4 O11 102.5(2) . .
O17 W4 O11 92.8(2) . .
O8 W4 O12 102.6(2) . .
O17 W4 O12 90.7(2) . .
O11 W4 O12 152.8(2) . .
O8 W4 O4 96.0(2) . .
O17 W4 O4 159.4(2) . .
O11 W4 O4 84.6(2) . .
O12 W4 O4 82.7(2) . .
O8 W4 O14 170.1(2) . .
O17 W4 O14 85.3(2) . .
O11 W4 O14 77.2(2) . .
O12 W4 O14 76.3(2) . .
O4 W4 O14 74.11(19) . .
O9 W5 O18 104.6(2) . .
O9 W5 O13 103.5(2) . .
O18 W5 O13 91.7(2) . .
O9 W5 O12 100.5(2) . .
O18 W5 O12 92.0(2) . .
O13 W5 O12 154.0(2) . .
O9 W5 O2 94.8(2) . .
O18 W5 O2 160.5(2) . .
O13 W5 O2 83.4(2) . .
O12 W5 O2 84.5(2) . .
O9 W5 O14 168.9(2) . .
O18 W5 O14 86.3(2) . .
O13 W5 O14 77.67(19) . .
O12 W5 O14 76.9(2) . .
O2 W5 O14 74.22(19) . .
O36 W6 O33 105.1(3) . .
O36 W6 O32 103.9(2) . .
O33 W6 O32 88.4(2) . .
O36 W6 O34 102.4(2) . .
O33 W6 O34 87.9(2) . .
O32 W6 O34 153.5(2) . .
O36 W6 O35 101.1(3) . .
O33 W6 O35 153.7(2) . .
O32 W6 O35 85.9(2) . .
O34 W6 O35 85.9(2) . .
O36 W6 O23 177.3(2) . .
O33 W6 O23 77.4(2) . .
O32 W6 O23 76.9(2) . .
O34 W6 O23 76.69(19) . .
O35 W6 O23 76.4(2) . .
O28 W7 O20 103.5(3) . .
O28 W7 O25 101.8(2) . .
O20 W7 O25 93.0(2) . .
O28 W7 O24 104.4(2) . .
O20 W7 O24 90.9(2) . .
O25 W7 O24 151.8(2) . .
O28 W7 O33 99.0(2) . .
O20 W7 O33 157.4(2) . .
O25 W7 O33 83.3(2) . .
O24 W7 O33 82.5(2) . .
O28 W7 O23 172.3(2) . .
O20 W7 O23 84.2(2) . .
O25 W7 O23 76.9(2) . .
O24 W7 O23 75.69(19) . .
O33 W7 O23 73.3(2) . .
O29 W8 O21 104.0(2) . .
O29 W8 O25 103.5(2) . .
O21 W8 O25 91.1(2) . .
O29 W8 O26 101.0(2) . .
O21 W8 O26 91.9(2) . .
O25 W8 O26 153.8(2) . .
O29 W8 O34 97.3(2) . .
O21 W8 O34 158.8(2) . .
O25 W8 O34 84.3(2) . .
O26 W8 O34 83.5(2) . .
O29 W8 O23 171.4(2) . .
O21 W8 O23 84.4(2) . .
O25 W8 O23 77.99(19) . .
O26 W8 O23 76.4(2) . .
O34 W8 O23 74.35(19) . .
O30 W9 O22 103.4(3) . .
O30 W9 O27 100.2(2) . .
O22 W9 O27 92.6(2) . .
O30 W9 O26 102.4(2) . .
O22 W9 O26 91.5(2) . .
O27 W9 O26 155.4(2) . .
O30 W9 O35 95.7(3) . .
O22 W9 O35 160.8(2) . .
O27 W9 O35 84.6(2) . .
O26 W9 O35 83.6(2) . .
O30 W9 O23 170.9(2) . .
O22 W9 O23 85.7(2) . .
O27 W9 O23 78.6(2) . .
O26 W9 O23 77.5(2) . .
O35 W9 O23 75.2(2) . .
O31 W10 O19 104.1(2) . .
O31 W10 O24 101.8(2) . .
O19 W10 O24 92.8(2) . .
O31 W10 O27 101.1(2) . .
O19 W10 O27 91.3(2) . .
O24 W10 O27 154.9(2) . .
O31 W10 O32 95.6(2) . .
O19 W10 O32 160.2(2) . .
O24 W10 O32 84.0(2) . .
O27 W10 O32 83.8(2) . .
O31 W10 O23 170.2(2) . .
O19 W10 O23 85.7(2) . .
O24 W10 O23 77.7(2) . .
O27 W10 O23 77.98(19) . .
O32 W10 O23 74.54(19) . .
O20 Nd1 O21 74.68(18) . .
O20 Nd1 O17 138.62(17) . .
O21 Nd1 O17 73.26(18) . .
O20 Nd1 O22 118.43(18) . .
O21 Nd1 O22 75.09(18) . .
O17 Nd1 O22 77.15(18) . .
O20 Nd1 O19 75.13(18) . .
O21 Nd1 O19 117.84(17) . .
O17 Nd1 O19 144.14(18) . .
O22 Nd1 O19 73.83(18) . .
O20 Nd1 O15 77.73(17) . .
O21 Nd1 O15 143.59(18) . .
O17 Nd1 O15 116.10(17) . .
O22 Nd1 O15 140.14(18) . .
O19 Nd1 O15 76.41(17) . .
O20 Nd1 O16 72.78(18) . .
O21 Nd1 O16 75.99(17) . .
O17 Nd1 O16 74.62(18) . .
O22 Nd1 O16 144.18(18) . .
O19 Nd1 O16 139.67(18) . .
O15 Nd1 O16 73.46(17) . .
O20 Nd1 O18 144.49(17) . .
O21 Nd1 O18 139.78(18) . .
O17 Nd1 O18 74.12(17) . .
O22 Nd1 O18 75.28(17) . .
O19 Nd1 O18 78.47(17) . .
O15 Nd1 O18 73.28(17) . .
O16 Nd1 O18 116.65(17) . .
W1 O2 W5 116.1(3) . .
W1 O3 W3 114.7(3) . .
W1 O4 W4 116.2(3) . .
W1 O5 W2 116.0(3) . .
W4 O8 Na5 128.2(3) . .
W5 O9 Na7 130.4(3) . .
W3 O10 W2 114.3(3) . .
W4 O11 W3 115.1(2) . .
W5 O12 W4 115.7(3) . .
W5 O13 W2 114.9(2) . .
W1 O14 W3 92.77(18) . .
W1 O14 W5 92.69(18) . .
W3 O14 W5 174.5(2) . .
W1 O14 W4 92.49(18) . .
W3 O14 W4 89.64(17) . .
W5 O14 W4 90.54(18) . .
W1 O14 W2 93.18(18) . .
W3 O14 W2 90.00(18) . .
W5 O14 W2 89.28(17) . .
W4 O14 W2 174.3(2) . .
W2 O15 Nd1 129.6(3) . .
W3 O16 Nd1 128.3(3) . .
W4 O17 Nd1 129.5(3) . .
W5 O18 Nd1 127.8(2) . .
W10 O19 Nd1 127.3(3) . .
W7 O20 Nd1 129.3(3) . .
W8 O21 Nd1 129.2(3) . .
W9 O22 Nd1 127.4(3) . .
W9 O23 W6 93.58(19) . .
W9 O23 W10 89.78(17) . .
W6 O23 W10 92.33(18) . .
W9 O23 W8 90.96(19) . .
W6 O23 W8 92.12(18) . .
W10 O23 W8 175.4(2) . .
W9 O23 W7 175.0(2) . .
W6 O23 W7 91.39(18) . .
W10 O23 W7 90.02(18) . .
W8 O23 W7 88.86(16) . .
W10 O24 W7 115.8(2) . .
W7 O25 W8 115.5(3) . .
W9 O26 W8 114.6(3) . .
W9 O27 W10 113.0(3) . .
W7 O28 Na2 156.1(3) . .
W8 O29 Na7 136.2(3) . 1_545
W10 O31 Na4 133.1(3) . .
W6 O32 W10 116.2(2) . .
W6 O33 W7 117.9(3) . .
W6 O34 W8 116.8(2) . .
W6 O35 W9 114.9(3) . .
Na9 O3W Na8 92.8(3) 2_757 .
Na2 O4W Na4 130.4(3) . 2_647
Na3 O8W Na6 98.6(2) . .
Na3 O9W Na4 98.2(3) . 2_656
Na1 O10W Na5 101.3(3) . .
Na1 O14W Na7 102.7(3) . .
Na8 O15W Na2 93.4(2) . .
Na4 O16W Na3 99.8(2) 2_656 .
Na6 O17W Na5 101.5(3) . .
Na2 O18W Na2 96.8(2) . 2_747
Na6 O19W Na3 96.9(2) . .
Na1 O20W Na6 120.8(3) . .
Na8 O21W Na2 95.4(2) . .
Na7 O23W Na5 123.4(3) 2_656 .
Na9 O25W Na8 93.7(2) 2_757 .
Na7 O26W Na9 117.5(3) . .
Na1 O27W Na5 93.1(3) . .
Na7 O29W Na1 96.9(3) . .
Na6 O31W Na5 96.9(3) . .
O33W O32W Na9 83.3(13) . .
O32W O33W Na9 70.1(12) . .
O14W Na1 O20W 154.8(3) . .
O14W Na1 O10W 104.1(2) . .
O20W Na1 O10W 90.6(2) . .
O14W Na1 O27W 90.3(3) . .
O20W Na1 O27W 113.4(3) . .
O10W Na1 O27W 75.2(2) . .
O14W Na1 O30W 92.6(2) . .
O20W Na1 O30W 78.7(2) . .
O10W Na1 O30W 159.1(3) . .
O27W Na1 O30W 92.7(2) . .
O14W Na1 O29W 79.4(2) . .
O20W Na1 O29W 82.7(2) . .
O10W Na1 O29W 81.9(2) . .
O27W Na1 O29W 151.8(3) . .
O30W Na1 O29W 113.8(2) . .
O14W Na1 Na5 121.3(2) . .
O20W Na1 Na5 83.00(18) . .
O10W Na1 Na5 39.68(17) . .
O27W Na1 Na5 45.8(2) . .
O30W Na1 Na5 120.39(19) . .
O29W Na1 Na5 119.27(19) . .
O14W Na1 Na7 39.96(17) . .
O20W Na1 Na7 121.96(18) . .
O10W Na1 Na7 89.10(18) . .
O27W Na1 Na7 122.3(2) . .
O30W Na1 Na7 111.75(18) . .
O29W Na1 Na7 39.95(16) . .
Na5 Na1 Na7 125.93(12) . .
O14W Na1 Na6 171.1(2) . .
O20W Na1 Na6 30.21(15) . .
O10W Na1 Na6 80.22(18) . .
O27W Na1 Na6 83.3(2) . .
O30W Na1 Na6 81.59(18) . .
O29W Na1 Na6 109.04(18) . .
Na5 Na1 Na6 57.53(9) . .
Na7 Na1 Na6 148.74(12) . .
O18W Na2 O21W 175.0(3) . .
O18W Na2 O18W 83.2(2) . 2_747
O21W Na2 O18W 91.9(2) . 2_747
O18W Na2 O4W 87.5(2) . .
O21W Na2 O4W 97.4(2) . .
O18W Na2 O4W 170.5(2) 2_747 .
O18W Na2 O15W 94.8(2) . .
O21W Na2 O15W 83.6(2) . .
O18W Na2 O15W 83.9(2) 2_747 .
O4W Na2 O15W 94.8(2) . .
O18W Na2 O28 92.9(2) . .
O21W Na2 O28 89.0(2) . .
O18W Na2 O28 101.8(2) 2_747 .
O4W Na2 O28 80.7(2) . .
O15W Na2 O28 170.9(2) . .
O18W Na2 Na8 137.2(2) . .
O21W Na2 Na8 42.01(16) . .
O18W Na2 Na8 95.00(19) 2_747 .
O4W Na2 Na8 90.37(18) . .
O15W Na2 Na8 42.83(15) . .
O28 Na2 Na8 128.79(18) . .
O18W Na2 Na2 41.86(16) . 2_747
O21W Na2 Na2 133.2(2) . 2_747
O18W Na2 Na2 41.37(16) 2_747 2_747
O4W Na2 Na2 129.3(2) . 2_747
O15W Na2 Na2 89.09(18) . 2_747
O28 Na2 Na2 99.88(19) . 2_747
Na8 Na2 Na2 123.18(15) . 2_747
O28W Na3 O8W 170.8(3) 1_554 .
O28W Na3 O19W 89.1(2) 1_554 .
O8W Na3 O19W 82.2(2) . .
O28W Na3 O5W 85.5(2) 1_554 .
O8W Na3 O5W 97.9(2) . .
O19W Na3 O5W 91.9(2) . .
O28W Na3 O9W 79.3(2) 1_554 .
O8W Na3 O9W 99.7(2) . .
O19W Na3 O9W 103.6(2) . .
O5W Na3 O9W 157.9(3) . .
O28W Na3 O16W 100.9(2) 1_554 .
O8W Na3 O16W 87.7(2) . .
O19W Na3 O16W 169.7(2) . .
O5W Na3 O16W 91.0(2) . .
O9W Na3 O16W 76.5(2) . .
O28W Na3 Na6 129.9(2) 1_554 .
O8W Na3 Na6 41.08(15) . .
O19W Na3 Na6 41.42(15) . .
O5W Na3 Na6 100.41(19) . .
O9W Na3 Na6 101.59(18) . .
O16W Na3 Na6 128.33(18) . .
O28W Na3 Na4 103.15(19) 1_554 2_656
O8W Na3 Na4 81.24(17) . 2_656
O19W Na3 Na4 136.10(19) . 2_656
O5W Na3 Na4 130.48(19) . 2_656
O9W Na3 Na4 40.90(17) . 2_656
O16W Na3 Na4 39.51(15) . 2_656
Na6 Na3 Na4 109.27(11) . 2_656
O12W Na4 O16W 161.5(3) . 2_656
O12W Na4 O4W 94.8(2) . 2_647
O16W Na4 O4W 102.1(2) 2_656 2_647
O12W Na4 O24W 88.5(2) . .
O16W Na4 O24W 97.7(2) 2_656 .
O4W Na4 O24W 94.8(2) 2_647 .
O12W Na4 O9W 83.9(2) . 2_656
O16W Na4 O9W 77.5(2) 2_656 2_656
O4W Na4 O9W 152.4(2) 2_647 2_656
O24W Na4 O9W 112.6(3) . 2_656
O12W Na4 O31 77.6(2) . .
O16W Na4 O31 97.0(2) 2_656 .
O4W Na4 O31 81.7(2) 2_647 .
O24W Na4 O31 165.3(2) . .
O9W Na4 O31 71.0(2) 2_656 .
O12W Na4 Na3 122.03(19) . 2_656
O16W Na4 Na3 40.68(16) 2_656 2_656
O4W Na4 Na3 124.85(19) 2_647 2_656
O24W Na4 Na3 122.78(19) . 2_656
O9W Na4 Na3 40.87(16) 2_656 2_656
O31 Na4 Na3 69.77(15) . 2_656
O1W Na5 O10W 162.3(3) . .
O1W Na5 O17W 108.8(3) . .
O10W Na5 O17W 84.6(2) . .
O1W Na5 O23W 85.3(2) . .
O10W Na5 O23W 85.2(2) . .
O17W Na5 O23W 82.0(2) . .
O1W Na5 O27W 109.2(3) . .
O10W Na5 O27W 70.7(2) . .
O17W Na5 O27W 122.6(3) . .
O23W Na5 O27W 142.0(3) . .
O1W Na5 O31W 75.7(3) . .
O10W Na5 O31W 121.2(3) . .
O17W Na5 O31W 66.3(2) . .
O23W Na5 O31W 134.5(3) . .
O27W Na5 O31W 83.5(2) . .
O1W Na5 O8 70.5(2) . .
O10W Na5 O8 93.4(2) . .
O17W Na5 O8 164.1(2) . .
O23W Na5 O8 82.0(2) . .
O27W Na5 O8 71.0(2) . .
O31W Na5 O8 127.0(2) . .
O1W Na5 Na1 148.5(2) . .
O10W Na5 Na1 38.99(16) . .
O17W Na5 Na1 88.25(18) . .
O23W Na5 Na1 124.08(19) . .
O27W Na5 Na1 41.16(16) . .
O31W Na5 Na1 88.10(19) . .
O8 Na5 Na1 100.16(18) . .
O1W Na5 Na6 109.6(2) . .
O10W Na5 Na6 88.09(19) . .
O17W Na5 Na6 38.36(16) . .
O23W Na5 Na6 120.4(2) . .
O27W Na5 Na6 88.45(19) . .
O31W Na5 Na6 38.07(16) . .
O8 Na5 Na6 157.54(19) . .
Na1 Na5 Na6 67.60(10) . .
O31W Na6 O11W 159.4(3) . .
O31W Na6 O17W 73.5(3) . .
O11W Na6 O17W 91.9(2) . .
O31W Na6 O8W 90.6(3) . .
O11W Na6 O8W 105.9(2) . .
O17W Na6 O8W 161.2(3) . .
O31W Na6 O19W 83.5(3) . .
O11W Na6 O19W 86.8(2) . .
O17W Na6 O19W 105.9(2) . .
O8W Na6 O19W 81.7(2) . .
O31W Na6 O20W 111.2(3) . .
O11W Na6 O20W 82.3(2) . .
O17W Na6 O20W 88.8(2) . .
O8W Na6 O20W 87.5(2) . .
O19W Na6 O20W 162.0(2) . .
O31W Na6 Na3 90.1(2) . .
O11W Na6 Na3 94.66(18) . .
O17W Na6 Na3 146.15(19) . .
O8W Na6 Na3 40.37(15) . .
O19W Na6 Na3 41.66(16) . .
O20W Na6 Na3 124.95(19) . .
O31W Na6 Na5 45.0(2) . .
O11W Na6 Na5 128.28(19) . .
O17W Na6 Na5 40.16(17) . .
O8W Na6 Na5 121.04(19) . .
O19W Na6 Na5 118.55(18) . .
O20W Na6 Na5 79.42(17) . .
Na3 Na6 Na5 134.97(12) . .
O31W Na6 Na1 82.2(2) . .
O11W Na6 Na1 109.69(17) . .
O17W Na6 Na1 78.87(17) . .
O8W Na6 Na1 89.12(17) . .
O19W Na6 Na1 162.92(19) . .
O20W Na6 Na1 29.00(15) . .
Na3 Na6 Na1 128.97(11) . .
Na5 Na6 Na1 54.87(8) . .
O26W Na7 O23W 103.9(2) . 2_656
O26W Na7 O29W 94.8(2) . .
O23W Na7 O29W 80.9(2) 2_656 .
O26W Na7 O9 161.5(3) . .
O23W Na7 O9 91.7(2) 2_656 .
O29W Na7 O9 97.4(2) . .
O26W Na7 O14W 78.7(2) . .
O23W Na7 O14W 160.9(3) 2_656 .
O29W Na7 O14W 80.0(2) . .
O9 Na7 O14W 89.8(2) . .
O26W Na7 O29 84.0(2) . 1_565
O23W Na7 O29 82.5(2) 2_656 1_565
O29W Na7 O29 162.6(2) . 1_565
O9 Na7 O29 88.4(2) . 1_565
O14W Na7 O29 116.6(2) . 1_565
O26W Na7 Na1 90.06(18) . .
O23W Na7 Na1 123.6(2) 2_656 .
O29W Na7 Na1 43.16(17) . .
O9 Na7 Na1 89.41(17) . .
O14W Na7 Na1 37.36(16) . .
O29 Na7 Na1 153.88(18) 1_565 .
O26W Na7 Na9 31.26(17) . .
O23W Na7 Na9 132.24(19) 2_656 .
O29W Na7 Na9 109.4(2) . .
O9 Na7 Na9 130.51(19) . .
O14W Na7 Na9 56.65(17) . .
O29 Na7 Na9 78.31(16) 1_565 .
Na1 Na7 Na9 83.43(10) . .
O21W Na8 O25W 106.8(2) . .
O21W Na8 O15W 85.2(2) . .
O25W Na8 O15W 167.4(3) . .
O21W Na8 O7W 88.0(2) . .
O25W Na8 O7W 87.5(2) . .
O15W Na8 O7W 89.1(2) . .
O21W Na8 O3W 165.6(3) . .
O25W Na8 O3W 84.4(2) . .
O15W Na8 O3W 84.5(2) . .
O7W Na8 O3W 101.8(2) . .
O21W Na8 O13W 93.2(2) . .
O25W Na8 O13W 82.3(2) . .
O15W Na8 O13W 101.2(2) . .
O7W Na8 O13W 169.6(3) . .
O3W Na8 O13W 79.0(2) . .
O21W Na8 Na9 149.0(2) . 2_757
O25W Na8 Na9 42.54(19) . 2_757
O15W Na8 Na9 125.7(2) . 2_757
O7W Na8 Na9 93.6(2) . 2_757
O3W Na8 Na9 41.96(17) . 2_757
O13W Na8 Na9 80.05(19) . 2_757
O21W Na8 Na2 42.64(16) . .
O25W Na8 Na2 148.7(2) . .
O15W Na8 Na2 43.82(16) . .
O7W Na8 Na2 96.09(19) . .
O3W Na8 Na2 124.79(19) . .
O13W Na8 Na2 91.74(19) . .
Na9 Na8 Na2 165.38(14) 2_757 .
O32W Na9 O3W 83.7(3) . 2_757
O32W Na9 O25W 83.1(3) . 2_757
O3W Na9 O25W 88.8(3) 2_757 2_757
O32W Na9 O26W 145.0(4) . .
O3W Na9 O26W 86.2(3) 2_757 .
O25W Na9 O26W 130.1(3) 2_757 .
O32W Na9 O33W 26.7(6) . .
O3W Na9 O33W 59.1(6) 2_757 .
O25W Na9 O33W 93.0(6) 2_757 .
O26W Na9 O33W 125.2(6) . .
O32W Na9 O6W 93.7(3) . .
O3W Na9 O6W 171.7(3) 2_757 .
O25W Na9 O6W 83.0(3) 2_757 .
O26W Na9 O6W 100.3(3) . .
O33W Na9 O6W 119.6(6) . .
O32W Na9 Na8 83.6(3) . 2_757
O3W Na9 Na8 45.24(18) 2_757 2_757
O25W Na9 Na8 43.76(18) 2_757 2_757
O26W Na9 Na8 111.8(2) . 2_757
O33W Na9 Na8 74.0(6) . 2_757
O6W Na9 Na8 126.7(3) . 2_757
O32W Na9 Na7 174.1(3) . .
O3W Na9 Na7 91.1(2) 2_757 .
O25W Na9 Na7 99.6(2) 2_757 .
O26W Na9 Na7 31.19(17) . .
O33W Na9 Na7 147.5(6) . .
O6W Na9 Na7 91.8(2) . .
Na8 Na9 Na7 94.64(13) 2_757 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O1 1.758(5) .
W1 O4 1.900(5) .
W1 O2 1.905(5) .
W1 O3 1.907(5) .
W1 O5 1.912(5) .
W1 O14 2.286(5) .
W2 O6 1.721(6) .
W2 O15 1.795(5) .
W2 O13 1.936(5) .
W2 O10 1.964(5) .
W2 O5 2.035(5) .
W2 O14 2.324(5) .
W3 O7 1.741(5) .
W3 O16 1.790(5) .
W3 O10 1.940(5) .
W3 O11 1.940(5) .
W3 O3 2.048(5) .
W3 O14 2.315(5) .
W4 O8 1.723(6) .
W4 O17 1.800(5) .
W4 O11 1.933(5) .
W4 O12 1.958(5) .
W4 O4 2.021(5) .
W4 O14 2.322(5) .
W5 O9 1.754(5) .
W5 O18 1.793(5) .
W5 O13 1.931(5) .
W5 O12 1.934(5) .
W5 O2 2.019(5) .
W5 O14 2.316(5) .
W6 O36 1.747(5) .
W6 O33 1.888(6) .
W6 O32 1.893(5) .
W6 O34 1.912(5) .
W6 O35 1.943(5) .
W6 O23 2.304(5) .
W7 O28 1.716(6) .
W7 O20 1.801(5) .
W7 O25 1.947(5) .
W7 O24 1.962(5) .
W7 O33 2.021(5) .
W7 O23 2.377(5) .
W8 O29 1.740(5) .
W8 O21 1.791(5) .
W8 O25 1.949(5) .
W8 O26 1.958(5) .
W8 O34 2.006(5) .
W8 O23 2.331(5) .
W9 O30 1.725(6) .
W9 O22 1.805(5) .
W9 O27 1.938(5) .
W9 O26 1.956(5) .
W9 O35 2.027(5) .
W9 O23 2.288(5) .
W10 O31 1.734(5) .
W10 O19 1.806(5) .
W10 O24 1.946(5) .
W10 O27 1.950(6) .
W10 O32 2.023(5) .
W10 O23 2.305(5) .
Nd1 O20 2.427(5) .
Nd1 O21 2.437(5) .
Nd1 O17 2.443(5) .
Nd1 O22 2.446(5) .
Nd1 O19 2.447(5) .
Nd1 O15 2.464(5) .
Nd1 O16 2.464(5) .
Nd1 O18 2.503(5) .
O8 Na5 2.721(7) .
O9 Na7 2.486(6) .
O28 Na2 2.469(7) .
O29 Na7 2.544(7) 1_545
O31 Na4 2.606(6) .
O1W Na5 2.367(8) .
O3W Na9 2.314(8) 2_757
O3W Na8 2.458(7) .
O4W Na2 2.415(6) .
O4W Na4 2.437(7) 2_647
O5W Na3 2.451(7) .
O6W Na9 2.519(8) .
O7W Na8 2.416(7) .
O8W Na3 2.397(7) .
O8W Na6 2.432(6) .
O9W Na3 2.466(7) .
O9W Na4 2.467(7) 2_656
O10W Na1 2.373(7) .
O10W Na5 2.408(7) .
O11W Na6 2.388(6) .
O12W Na4 2.334(7) .
O13W Na8 2.474(7) .
O14W Na1 2.358(7) .
O14W Na7 2.496(7) .
O15W Na8 2.409(7) .
O15W Na2 2.453(7) .
O16W Na4 2.408(7) 2_656
O16W Na3 2.467(7) .
O17W Na6 2.415(7) .
O17W Na5 2.510(8) .
O18W Na2 2.390(7) .
O18W Na2 2.413(7) 2_747
O19W Na6 2.439(7) .
O19W Na3 2.451(7) .
O20W Na1 2.359(7) .
O20W Na6 2.448(6) .
O21W Na8 2.377(7) .
O21W Na2 2.406(7) .
O23W Na7 2.444(7) 2_656
O23W Na5 2.515(7) .
O24W Na4 2.438(7) .
O25W Na9 2.342(8) 2_757
O25W Na8 2.396(7) .
O26W Na7 2.360(7) .
O26W Na9 2.365(8) .
O27W Na1 2.437(8) .
O27W Na5 2.654(8) .
O28W Na3 2.269(7) 1_556
O29W Na7 2.452(7) .
O29W Na1 2.613(7) .
O30W Na1 2.510(7) .
O31W Na6 2.369(7) .
O31W Na5 2.718(10) .
O32W O33W 1.10(3) .
O32W Na9 2.313(10) .
O33W Na9 2.44(2) .
Na1 Na5 3.698(5) .
Na1 Na7 3.792(5) .
Na1 Na6 4.180(5) .
Na2 O18W 2.413(7) 2_747
Na2 Na8 3.537(5) .
Na2 Na2 3.591(6) 2_747
Na3 O28W 2.269(7) 1_554
Na3 Na6 3.660(5) .
Na3 Na4 3.729(5) 2_656
Na4 O16W 2.408(7) 2_656
Na4 O4W 2.437(7) 2_647
Na4 O9W 2.467(7) 2_656
Na4 Na3 3.729(5) 2_656
Na5 Na6 3.814(5) .
Na7 O23W 2.444(7) 2_656
Na7 O29 2.544(7) 1_565
Na7 Na9 4.041(6) .
Na8 Na9 3.458(6) 2_757
Na9 O3W 2.314(7) 2_757
Na9 O25W 2.342(8) 2_757
Na9 Na8 3.458(6) 2_757
