#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:59:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179520 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341704.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341704
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Ca9 Mn4.41 Sb9'
_chemical_formula_weight         1698.48
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.490(2)
_cell_length_b                   4.6292(8)
_cell_length_c                   44.197(8)
_cell_measurement_reflns_used    1091
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      21.26
_cell_measurement_theta_min      4.93
_cell_volume                     2555.4(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1381
_diffrn_reflns_av_sigmaI/netI    0.0697
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       55
_diffrn_reflns_limit_l_min       -55
_diffrn_reflns_number            27444
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         0.92
_exptl_absorpt_coefficient_mu    13.226
_exptl_absorpt_correction_T_max  0.8791
_exptl_absorpt_correction_T_min  0.6694
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick,2003)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.415
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             2997
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_refine_diff_density_max         6.599
_refine_diff_density_min         -1.999
_refine_diff_density_rms         0.438
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.012
_refine_ls_matrix_type           full
_refine_ls_number_parameters     156
_refine_ls_number_reflns         2954
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.012
_refine_ls_R_factor_all          0.0920
_refine_ls_R_factor_gt           0.0465
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0346P)²+32.2479P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0868
_refine_ls_wR_factor_ref         0.1030
_reflns_number_gt                1914
_reflns_number_total             2954
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_002.cif
_cod_data_source_block           II
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341704
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ca1 Ca 0.0152(4) 0.1630(12) 0.41928(12) 0.0293(17) Uani 0.50 1 d P
Ca2 Ca 0.0251(3) 0.2500 0.32715(8) 0.0244(10) Uani 1 2 d S
Ca3 Ca 0.2419(3) 0.2500 0.67138(8) 0.0194(9) Uani 1 2 d S
Ca4 Ca 0.2897(3) 0.2500 0.57938(9) 0.0243(10) Uani 1 2 d S
Ca5 Ca 0.3015(3) 0.2500 0.37485(8) 0.0174(8) Uani 1 2 d S
Ca6 Ca 0.3057(3) 0.2500 0.75238(10) 0.0287(10) Uani 1 2 d S
Ca7 Ca 0.5528(3) 0.2500 0.69102(8) 0.0153(8) Uani 1 2 d S
Ca8 Ca 0.5748(3) 0.2500 0.55105(10) 0.0339(11) Uani 1 2 d S
Ca9 Ca 0.8480(4) 0.2500 0.50112(11) 0.0561(16) Uani 1 2 d S
Mn1 Mn 0.4410(2) 0.2500 0.25401(6) 0.0166(6) Uani 1 2 d S
Mn2 Mn 0.5918(2) 0.2500 0.35952(6) 0.0153(6) Uani 1 2 d S
Mn3 Mn 0.8201(6) 0.2500 0.68351(15) 0.016(2) Uani 0.407(10) 2 d SP
Mn4 Mn 1.0697(4) 0.2500 0.60959(11) 0.0134(16) Uani 0.484(7) 2 d SP
Mn5 Mn 0.8487(4) 0.2500 0.57131(10) 0.0093(14) Uani 0.516(7) 2 d SP
Mn6A Mn 0.3038(7) 0.2500 0.5084(2) 0.0219(9) Uani 0.337(5) 2 d SP
Mn6B Mn 0.3982(4) 0.2500 0.49742(10) 0.0219(9) Uani 0.663(5) 2 d SP
Sb1 Sb 0.25086(10) 0.2500 0.44955(3) 0.0165(3) Uani 1 2 d S
Sb2 Sb 0.27511(9) 0.2500 0.29841(3) 0.0131(3) Uani 1 2 d S
Sb3 Sb 0.50628(10) 0.2500 0.62035(3) 0.0148(3) Uani 1 2 d S
Sb4 Sb 0.55234(11) 0.2500 0.77965(3) 0.0209(3) Uani 1 2 d S
Sb5 Sb 0.60599(10) 0.2500 0.46826(3) 0.0165(3) Uani 1 2 d S
Sb6 Sb 0.62097(9) 0.2500 0.29517(2) 0.0124(3) Uani 1 2 d S
Sb7 Sb 0.87563(11) 0.2500 0.62970(3) 0.0203(3) Uani 1 2 d S
Sb8 Sb 0.81234(10) 0.2500 0.37545(3) 0.0161(3) Uani 1 2 d S
Sb9A Sb 0.0556(2) 0.2500 0.54591(7) 0.0155(5) Uani 0.579(4) 2 d SP
Sb9B Sb 0.0888(3) 0.2500 0.53476(9) 0.0155(5) Uani 0.421(4) 2 d SP
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ca1 Ca1 Mn4 139.05(15) 7_565 5_656
Ca1 Ca1 Mn5 137.54(15) 7_565 5_656
Mn4 Ca1 Mn5 78.4(2) 5_656 5_656
Ca1 Ca1 Sb9A 137.14(13) 7_565 5_556
Mn4 Ca1 Sb9A 66.53(18) 5_656 5_556
Mn5 Ca1 Sb9A 65.61(17) 5_656 5_556
Ca1 Ca1 Sb9B 128.41(11) 7_565 5_556
Mn4 Ca1 Sb9B 71.74(18) 5_656 5_556
Mn5 Ca1 Sb9B 73.31(18) 5_656 5_556
Sb9A Ca1 Sb9B 8.95(5) 5_556 5_556
Ca1 Ca1 Mn4 31.40(13) 7_565 5_666
Mn4 Ca1 Mn4 107.6(2) 5_656 5_666
Mn5 Ca1 Mn4 155.8(2) 5_656 5_666
Sb9A Ca1 Mn4 138.5(2) 5_556 5_666
Sb9B Ca1 Mn4 130.9(2) 5_556 5_666
Ca1 Ca1 Sb7 126.77(10) 7_565 5_656
Mn4 Ca1 Sb7 52.05(15) 5_656 5_656
Mn5 Ca1 Sb7 52.22(14) 5_656 5_656
Sb9A Ca1 Sb7 96.07(17) 5_556 5_656
Sb9B Ca1 Sb7 104.82(17) 5_556 5_656
Mn4 Ca1 Sb7 112.42(18) 5_666 5_656
Ca1 Ca1 Sb8 82.80(10) 7_565 1_455
Mn4 Ca1 Sb8 57.36(14) 5_656 1_455
Mn5 Ca1 Sb8 134.9(2) 5_656 1_455
Sb9A Ca1 Sb8 100.36(18) 5_556 1_455
Sb9B Ca1 Sb8 98.21(17) 5_556 1_455
Mn4 Ca1 Sb8 52.34(12) 5_666 1_455
Sb7 Ca1 Sb8 90.17(14) 5_656 1_455
Ca1 Ca1 Mn5 32.77(13) 7_565 5_666
Mn4 Ca1 Mn5 156.9(2) 5_656 5_666
Mn5 Ca1 Mn5 104.8(2) 5_656 5_666
Sb9A Ca1 Mn5 135.9(2) 5_556 5_666
Sb9B Ca1 Mn5 131.3(2) 5_556 5_666
Mn4 Ca1 Mn5 60.60(15) 5_666 5_666
Sb7 Ca1 Mn5 111.47(18) 5_656 5_666
Sb8 Ca1 Mn5 112.74(18) 1_455 5_666
Ca1 Ca1 Sb9A 33.14(11) 7_565 5_566
Mn4 Ca1 Sb9A 139.2(2) 5_656 5_566
Mn5 Ca1 Sb9A 136.1(2) 5_656 5_566
Sb9A Ca1 Sb9A 103.99(19) 5_556 5_566
Sb9B Ca1 Sb9A 95.29(16) 5_556 5_566
Mn4 Ca1 Sb9A 52.01(13) 5_666 5_566
Sb7 Ca1 Sb9A 159.85(19) 5_656 5_566
Sb8 Ca1 Sb9A 88.04(15) 1_455 5_566
Mn5 Ca1 Sb9A 51.56(13) 5_666 5_566
Ca1 Ca1 Sb1 82.90(10) 7_565 .
Mn4 Ca1 Sb1 132.8(2) 5_656 .
Mn5 Ca1 Sb1 55.45(13) 5_656 .
Sb9A Ca1 Sb1 98.90(18) 5_556 .
Sb9B Ca1 Sb1 100.79(17) 5_556 .
Mn4 Ca1 Sb1 111.09(18) 5_666 .
Sb7 Ca1 Sb1 88.10(14) 5_656 .
Sb8 Ca1 Sb1 160.73(19) 1_455 .
Mn5 Ca1 Sb1 50.82(11) 5_666 .
Sb9A Ca1 Sb1 87.02(14) 5_566 .
Ca1 Ca1 Sb9B 41.58(10) 7_565 5_566
Mn4 Ca1 Sb9B 134.2(2) 5_656 5_566
Mn5 Ca1 Sb9B 134.2(2) 5_656 5_566
Sb9A Ca1 Sb9B 95.58(17) 5_556 5_566
Sb9B Ca1 Sb9B 86.82(16) 5_556 5_566
Mn4 Ca1 Sb9B 57.76(14) 5_666 5_566
Sb7 Ca1 Sb9B 168.35(19) 5_656 5_566
Sb8 Ca1 Sb9B 87.78(15) 1_455 5_566
Mn5 Ca1 Sb9B 59.15(13) 5_666 5_566
Sb9A Ca1 Sb9B 8.60(4) 5_566 5_566
Sb1 Ca1 Sb9B 90.06(15) . 5_566
Mn3 Ca2 Mn3 98.6(2) 5_666 5_656
Mn3 Ca2 Sb7 46.20(13) 5_666 5_666
Mn3 Ca2 Sb7 112.92(17) 5_656 5_666
Mn3 Ca2 Sb7 112.92(17) 5_666 5_656
Mn3 Ca2 Sb7 46.20(13) 5_656 5_656
Sb7 Ca2 Sb7 91.00(10) 5_666 5_656
Mn3 Ca2 Sb4 128.67(17) 5_666 2_554
Mn3 Ca2 Sb4 63.36(13) 5_656 2_554
Sb7 Ca2 Sb4 174.15(14) 5_666 2_554
Sb7 Ca2 Sb4 89.16(3) 5_656 2_554
Mn3 Ca2 Sb4 63.36(13) 5_666 2_564
Mn3 Ca2 Sb4 128.67(17) 5_656 2_564
Sb7 Ca2 Sb4 89.16(3) 5_666 2_564
Sb7 Ca2 Sb4 174.15(14) 5_656 2_564
Sb4 Ca2 Sb4 90.08(10) 2_554 2_564
Mn3 Ca2 Sb2 49.84(11) 5_666 .
Mn3 Ca2 Sb2 49.84(11) 5_656 .
Sb7 Ca2 Sb2 82.38(8) 5_666 .
Sb7 Ca2 Sb2 82.38(8) 5_656 .
Sb4 Ca2 Sb2 91.84(9) 2_554 .
Sb4 Ca2 Sb2 91.84(9) 2_564 .
Mn3 Ca2 Sb8 126.19(12) 5_666 1_455
Mn3 Ca2 Sb8 126.19(12) 5_656 1_455
Sb7 Ca2 Sb8 85.98(8) 5_666 1_455
Sb7 Ca2 Sb8 85.98(8) 5_656 1_455
Sb4 Ca2 Sb8 99.87(9) 2_554 1_455
Sb4 Ca2 Sb8 99.87(9) 2_564 1_455
Sb2 Ca2 Sb8 163.36(13) . 1_455
Mn3 Ca2 Mn1 91.71(15) 5_666 6_556
Mn3 Ca2 Mn1 91.71(15) 5_656 6_556
Sb7 Ca2 Mn1 132.17(6) 5_666 6_556
Sb7 Ca2 Mn1 132.17(6) 5_656 6_556
Sb4 Ca2 Mn1 45.66(5) 2_554 6_556
Sb4 Ca2 Mn1 45.66(5) 2_564 6_556
Sb2 Ca2 Mn1 84.18(10) . 6_556
Sb8 Ca2 Mn1 112.47(11) 1_455 6_556
Mn3 Ca2 Mn4 81.35(13) 5_666 5_666
Mn3 Ca2 Mn4 140.27(18) 5_656 5_666
Sb7 Ca2 Mn4 41.90(8) 5_666 5_666
Sb7 Ca2 Mn4 96.92(11) 5_656 5_666
Sb4 Ca2 Mn4 143.84(14) 2_554 5_666
Sb4 Ca2 Mn4 87.10(7) 2_564 5_666
Sb2 Ca2 Mn4 124.27(11) . 5_666
Sb8 Ca2 Mn4 45.55(8) 1_455 5_666
Mn1 Ca2 Mn4 128.01(11) 6_556 5_666
Mn3 Ca2 Mn4 140.27(18) 5_666 5_656
Mn3 Ca2 Mn4 81.35(13) 5_656 5_656
Sb7 Ca2 Mn4 96.92(11) 5_666 5_656
Sb7 Ca2 Mn4 41.90(8) 5_656 5_656
Sb4 Ca2 Mn4 87.10(7) 2_554 5_656
Sb4 Ca2 Mn4 143.84(14) 2_564 5_656
Sb2 Ca2 Mn4 124.27(11) . 5_656
Sb8 Ca2 Mn4 45.55(8) 1_455 5_656
Mn1 Ca2 Mn4 128.01(11) 6_556 5_656
Mn4 Ca2 Mn4 74.64(11) 5_666 5_656
Mn3 Ca2 Ca5 62.60(14) 5_666 .
Mn3 Ca2 Ca5 62.60(14) 5_656 .
Sb7 Ca2 Ca5 50.78(6) 5_666 .
Sb7 Ca2 Ca5 50.78(6) 5_656 .
Sb4 Ca2 Ca5 125.93(8) 2_554 .
Sb4 Ca2 Ca5 125.93(8) 2_564 .
Sb2 Ca2 Ca5 53.55(8) . .
Sb8 Ca2 Ca5 109.81(11) 1_455 .
Mn1 Ca2 Ca5 137.73(13) 6_556 .
Mn4 Ca2 Ca5 83.27(11) 5_666 .
Mn4 Ca2 Ca5 83.27(11) 5_656 .
Sb8 Ca3 Sb8 93.49(11) 5_656 5_666
Sb8 Ca3 Sb4 106.38(10) 5_656 6_557
Sb8 Ca3 Sb4 106.38(10) 5_666 6_557
Sb8 Ca3 Sb6 158.61(14) 5_656 5_666
Sb8 Ca3 Sb6 83.66(4) 5_666 5_666
Sb4 Ca3 Sb6 94.72(9) 6_557 5_666
Sb8 Ca3 Sb6 83.66(4) 5_656 5_656
Sb8 Ca3 Sb6 158.61(14) 5_666 5_656
Sb4 Ca3 Sb6 94.72(9) 6_557 5_656
Sb6 Ca3 Sb6 91.31(10) 5_666 5_656
Sb8 Ca3 Mn2 111.40(12) 5_656 5_666
Sb8 Ca3 Mn2 51.12(6) 5_666 5_666
Sb4 Ca3 Mn2 136.28(6) 6_557 5_666
Sb6 Ca3 Mn2 51.16(6) 5_666 5_666
Sb6 Ca3 Mn2 110.33(12) 5_656 5_666
Sb8 Ca3 Mn2 51.12(6) 5_656 5_656
Sb8 Ca3 Mn2 111.40(12) 5_666 5_656
Sb4 Ca3 Mn2 136.28(6) 6_557 5_656
Sb6 Ca3 Mn2 110.33(12) 5_666 5_656
Sb6 Ca3 Mn2 51.16(6) 5_656 5_656
Mn2 Ca3 Mn2 85.91(11) 5_666 5_656
Sb8 Ca3 Mn4 49.94(6) 5_656 1_455
Sb8 Ca3 Mn4 49.94(6) 5_666 1_455
Sb4 Ca3 Mn4 94.19(14) 6_557 1_455
Sb6 Ca3 Mn4 133.33(6) 5_666 1_455
Sb6 Ca3 Mn4 133.33(6) 5_656 1_455
Mn2 Ca3 Mn4 93.59(11) 5_666 1_455
Mn2 Ca3 Mn4 93.59(11) 5_656 1_455
Sb8 Ca3 Ca6 133.00(5) 5_656 .
Sb8 Ca3 Ca6 133.00(5) 5_666 .
Sb4 Ca3 Ca6 60.11(10) 6_557 .
Sb6 Ca3 Ca6 55.89(7) 5_666 .
Sb6 Ca3 Ca6 55.89(7) 5_656 .
Mn2 Ca3 Ca6 105.05(11) 5_666 .
Mn2 Ca3 Ca6 105.05(11) 5_656 .
Mn4 Ca3 Ca6 154.31(17) 1_455 .
Sb8 Ca3 Ca7 110.50(9) 5_656 .
Sb8 Ca3 Ca7 110.50(9) 5_666 .
Sb4 Ca3 Ca7 124.97(12) 6_557 .
Sb6 Ca3 Ca7 51.98(6) 5_666 .
Sb6 Ca3 Ca7 51.98(6) 5_656 .
Mn2 Ca3 Ca7 59.40(8) 5_666 .
Mn2 Ca3 Ca7 59.40(8) 5_656 .
Mn4 Ca3 Ca7 140.84(15) 1_455 .
Ca6 Ca3 Ca7 64.86(10) . .
Sb8 Ca3 Ca2 54.55(7) 5_656 5_556
Sb8 Ca3 Ca2 104.50(11) 5_666 5_556
Sb4 Ca3 Ca2 51.89(7) 6_557 5_556
Sb6 Ca3 Ca2 146.61(12) 5_666 5_556
Sb6 Ca3 Ca2 91.12(6) 5_656 5_556
Mn2 Ca3 Ca2 153.80(13) 5_666 5_556
Mn2 Ca3 Ca2 96.91(6) 5_656 5_556
Mn4 Ca3 Ca2 60.28(10) 1_455 5_556
Ca6 Ca3 Ca2 99.36(11) . 5_556
Ca7 Ca3 Ca2 142.95(6) . 5_556
Sb8 Ca3 Ca2 104.50(11) 5_656 5_566
Sb8 Ca3 Ca2 54.55(7) 5_666 5_566
Sb4 Ca3 Ca2 51.89(7) 6_557 5_566
Sb6 Ca3 Ca2 91.12(6) 5_666 5_566
Sb6 Ca3 Ca2 146.61(12) 5_656 5_566
Mn2 Ca3 Ca2 96.91(6) 5_666 5_566
Mn2 Ca3 Ca2 153.80(13) 5_656 5_566
Mn4 Ca3 Ca2 60.28(10) 1_455 5_566
Ca6 Ca3 Ca2 99.36(11) . 5_566
Ca7 Ca3 Ca2 142.95(6) . 5_566
Ca2 Ca3 Ca2 69.51(9) 5_556 5_566
Mn4 Ca4 Mn6A 119.1(2) 1_455 .
Mn4 Ca4 Sb9B 64.09(14) 1_455 .
Mn6A Ca4 Sb9B 55.06(19) . .
Mn4 Ca4 Sb3 120.30(16) 1_455 .
Mn6A Ca4 Sb3 120.6(2) . .
Sb9B Ca4 Sb3 175.61(17) . .
Mn4 Ca4 Sb9A 52.75(13) 1_455 .
Mn6A Ca4 Sb9A 66.40(19) . .
Sb9B Ca4 Sb9A 11.34(6) . .
Sb3 Ca4 Sb9A 173.05(16) . .
Mn4 Ca4 Sb8 52.45(8) 1_455 5_666
Mn6A Ca4 Sb8 128.58(11) . 5_666
Sb9B Ca4 Sb8 94.02(11) . 5_666
Sb3 Ca4 Sb8 89.11(9) . 5_666
Sb9A Ca4 Sb8 85.92(10) . 5_666
Mn4 Ca4 Sb8 52.45(8) 1_455 5_656
Mn6A Ca4 Sb8 128.58(11) . 5_656
Sb9B Ca4 Sb8 94.02(11) . 5_656
Sb3 Ca4 Sb8 89.11(9) . 5_656
Sb9A Ca4 Sb8 85.92(10) . 5_656
Sb8 Ca4 Sb8 88.69(11) 5_666 5_656
Mn4 Ca4 Sb5 128.12(9) 1_455 5_656
Mn6A Ca4 Sb5 50.07(10) . 5_656
Sb9B Ca4 Sb5 85.32(10) . 5_656
Sb3 Ca4 Sb5 91.49(9) . 5_656
Sb9A Ca4 Sb5 93.59(9) . 5_656
Sb8 Ca4 Sb5 178.60(11) 5_666 5_656
Sb8 Ca4 Sb5 92.59(2) 5_656 5_656
Mn4 Ca4 Sb5 128.12(9) 1_455 5_666
Mn6A Ca4 Sb5 50.07(10) . 5_666
Sb9B Ca4 Sb5 85.32(10) . 5_666
Sb3 Ca4 Sb5 91.49(9) . 5_666
Sb9A Ca4 Sb5 93.59(9) . 5_666
Sb8 Ca4 Sb5 92.59(2) 5_666 5_666
Sb8 Ca4 Sb5 178.60(11) 5_656 5_666
Sb5 Ca4 Sb5 86.13(10) 5_656 5_666
Mn4 Ca4 Ca8 173.46(17) 1_455 .
Mn6A Ca4 Ca8 67.4(2) . .
Sb9B Ca4 Ca8 122.45(16) . .
Sb3 Ca4 Ca8 53.16(9) . .
Sb9A Ca4 Ca8 133.79(15) . .
Sb8 Ca4 Ca8 124.26(9) 5_666 .
Sb8 Ca4 Ca8 124.26(9) 5_656 .
Sb5 Ca4 Ca8 55.33(7) 5_656 .
Sb5 Ca4 Ca8 55.33(7) 5_666 .
Mn4 Ca4 Ca3 55.75(13) 1_455 .
Mn6A Ca4 Ca3 174.9(2) . .
Sb9B Ca4 Ca3 119.83(15) . .
Sb3 Ca4 Ca3 64.55(9) . .
Sb9A Ca4 Ca3 108.50(13) . .
Sb8 Ca4 Ca3 49.29(6) 5_666 .
Sb8 Ca4 Ca3 49.29(6) 5_656 .
Sb5 Ca4 Ca3 132.10(7) 5_656 .
Sb5 Ca4 Ca3 132.10(7) 5_666 .
Ca8 Ca4 Ca3 117.71(13) . .
Mn4 Ca4 Ca1 35.92(10) 1_455 5_556
Mn6A Ca4 Ca1 93.68(18) . 5_556
Sb9B Ca4 Ca1 46.06(11) . 5_556
Sb3 Ca4 Ca1 137.31(12) . 5_556
Sb9A Ca4 Ca1 37.71(9) . 5_556
Sb8 Ca4 Ca1 87.79(12) 5_666 5_556
Sb8 Ca4 Ca1 48.27(9) 5_656 5_556
Sb5 Ca4 Ca1 92.63(9) 5_656 5_556
Sb5 Ca4 Ca1 131.19(13) 5_666 5_556
Ca8 Ca4 Ca1 147.95(10) . 5_556
Ca3 Ca4 Ca1 81.76(11) . 5_556
Sb7 Ca5 Sb7 92.36(10) 5_656 5_666
Sb7 Ca5 Sb3 177.65(9) 5_656 5_666
Sb7 Ca5 Sb3 89.98(3) 5_666 5_666
Sb7 Ca5 Sb3 89.98(3) 5_656 5_656
Sb7 Ca5 Sb3 177.65(9) 5_666 5_656
Sb3 Ca5 Sb3 87.67(9) 5_666 5_656
Sb7 Ca5 Sb1 86.10(8) 5_656 .
Sb7 Ca5 Sb1 86.10(8) 5_666 .
Sb3 Ca5 Sb1 94.17(8) 5_666 .
Sb3 Ca5 Sb1 94.17(8) 5_656 .
Sb7 Ca5 Sb2 82.57(8) 5_656 .
Sb7 Ca5 Sb2 82.57(8) 5_666 .
Sb3 Ca5 Sb2 97.64(8) 5_666 .
Sb3 Ca5 Sb2 97.64(8) 5_656 .
Sb1 Ca5 Sb2 163.60(13) . .
Sb7 Ca5 Mn2 131.78(6) 5_656 .
Sb7 Ca5 Mn2 131.78(6) 5_666 .
Sb3 Ca5 Mn2 46.00(5) 5_666 .
Sb3 Ca5 Mn2 46.00(5) 5_656 .
Sb1 Ca5 Mn2 111.42(11) . .
Sb2 Ca5 Mn2 84.98(9) . .
Sb7 Ca5 Mn3 40.46(10) 5_656 5_656
Sb7 Ca5 Mn3 97.01(12) 5_666 5_656
Sb3 Ca5 Mn3 139.05(14) 5_666 5_656
Sb3 Ca5 Mn3 84.72(9) 5_656 5_656
Sb1 Ca5 Mn3 126.45(12) . 5_656
Sb2 Ca5 Mn3 44.16(9) . 5_656
Mn2 Ca5 Mn3 105.62(13) . 5_656
Sb7 Ca5 Mn3 97.01(12) 5_656 5_666
Sb7 Ca5 Mn3 40.46(10) 5_666 5_666
Sb3 Ca5 Mn3 84.72(9) 5_666 5_666
Sb3 Ca5 Mn3 139.05(14) 5_656 5_666
Sb1 Ca5 Mn3 126.45(12) . 5_666
Sb2 Ca5 Mn3 44.16(9) . 5_666
Mn2 Ca5 Mn3 105.62(13) . 5_666
Mn3 Ca5 Mn3 75.43(14) 5_656 5_666
Sb7 Ca5 Mn5 97.93(11) 5_656 5_666
Sb7 Ca5 Mn5 42.43(7) 5_666 5_666
Sb3 Ca5 Mn5 83.88(7) 5_666 5_666
Sb3 Ca5 Mn5 137.24(13) 5_656 5_666
Sb1 Ca5 Mn5 45.13(7) . 5_666
Sb2 Ca5 Mn5 124.99(10) . 5_666
Mn2 Ca5 Mn5 126.74(10) . 5_666
Mn3 Ca5 Mn5 126.83(15) 5_656 5_666
Mn3 Ca5 Mn5 81.76(11) 5_666 5_666
Sb7 Ca5 Mn5 42.43(7) 5_656 5_656
Sb7 Ca5 Mn5 97.93(11) 5_666 5_656
Sb3 Ca5 Mn5 137.24(13) 5_666 5_656
Sb3 Ca5 Mn5 83.88(7) 5_656 5_656
Sb1 Ca5 Mn5 45.13(7) . 5_656
Sb2 Ca5 Mn5 124.99(10) . 5_656
Mn2 Ca5 Mn5 126.74(10) . 5_656
Mn3 Ca5 Mn5 81.76(11) 5_656 5_656
Mn3 Ca5 Mn5 126.83(15) 5_666 5_656
Mn5 Ca5 Mn5 74.76(11) 5_666 5_656
Sb7 Ca5 Ca2 51.60(6) 5_656 .
Sb7 Ca5 Ca2 51.60(6) 5_666 .
Sb3 Ca5 Ca2 130.26(7) 5_666 .
Sb3 Ca5 Ca2 130.26(7) 5_656 .
Sb1 Ca5 Ca2 110.58(11) . .
Sb2 Ca5 Ca2 53.02(8) . .
Mn2 Ca5 Ca2 138.00(12) . .
Mn3 Ca5 Ca2 45.75(10) 5_656 .
Mn3 Ca5 Ca2 45.75(10) 5_666 .
Mn5 Ca5 Ca2 84.58(10) 5_666 .
Mn5 Ca5 Ca2 84.58(10) 5_656 .
Mn3 Ca6 Sb2 52.67(9) 6_557 2_565
Mn3 Ca6 Sb2 52.67(9) 6_557 2
Sb2 Ca6 Sb2 91.09(11) 2_565 2
Mn3 Ca6 Sb6 128.75(11) 6_557 5_656
Sb2 Ca6 Sb6 178.00(17) 2_565 5_656
Sb2 Ca6 Sb6 89.15(2) 2 5_656
Mn3 Ca6 Sb6 128.75(11) 6_557 5_666
Sb2 Ca6 Sb6 89.15(2) 2_565 5_666
Sb2 Ca6 Sb6 178.00(17) 2 5_666
Sb6 Ca6 Sb6 90.55(11) 5_656 5_666
Mn3 Ca6 Sb4 64.99(17) 6_557 .
Sb2 Ca6 Sb4 93.51(11) 2_565 .
Sb2 Ca6 Sb4 93.51(11) 2 .
Sb6 Ca6 Sb4 88.46(9) 5_656 .
Sb6 Ca6 Sb4 88.46(9) 5_666 .
Mn3 Ca6 Sb4 117.74(19) 6_557 6_557
Sb2 Ca6 Sb4 88.41(9) 2_565 6_557
Sb2 Ca6 Sb4 88.41(9) 2 6_557
Sb6 Ca6 Sb4 89.61(10) 5_656 6_557
Sb6 Ca6 Sb4 89.61(10) 5_666 6_557
Sb4 Ca6 Sb4 177.27(14) . 6_557
Mn3 Ca6 Ca3 171.1(2) 6_557 .
Sb2 Ca6 Ca3 123.02(10) 2_565 .
Sb2 Ca6 Ca3 123.02(10) 2 .
Sb6 Ca6 Ca3 55.35(8) 5_656 .
Sb6 Ca6 Ca3 55.35(8) 5_666 .
Sb4 Ca6 Ca3 123.91(14) . .
Sb4 Ca6 Ca3 53.36(10) 6_557 .
Mn3 Ca6 Ca7 55.26(17) 6_557 6_557
Sb2 Ca6 Ca7 50.69(6) 2_565 6_557
Sb2 Ca6 Ca7 50.69(6) 2 6_557
Sb6 Ca6 Ca7 128.38(8) 5_656 6_557
Sb6 Ca6 Ca7 128.38(8) 5_666 6_557
Sb4 Ca6 Ca7 120.25(14) . 6_557
Sb4 Ca6 Ca7 62.48(9) 6_557 6_557
Ca3 Ca6 Ca7 115.84(14) . 6_557
Mn3 Ca6 Ca7 127.7(2) 6_557 .
Sb2 Ca6 Ca7 130.38(7) 2_565 .
Sb2 Ca6 Ca7 130.38(7) 2 .
Sb6 Ca6 Ca7 50.43(6) 5_656 .
Sb6 Ca6 Ca7 50.43(6) 5_666 .
Sb4 Ca6 Ca7 62.67(9) . .
Sb4 Ca6 Ca7 114.59(13) 6_557 .
Ca3 Ca6 Ca7 61.24(10) . .
Ca7 Ca6 Ca7 177.07(15) 6_557 .
Sb3 Ca7 Sb2 105.47(9) . 5_666
Sb3 Ca7 Sb2 105.47(9) . 5_656
Sb2 Ca7 Sb2 92.91(10) 5_666 5_656
Sb3 Ca7 Sb6 93.61(8) . 5_656
Sb2 Ca7 Sb6 160.70(12) 5_666 5_656
Sb2 Ca7 Sb6 84.57(3) 5_656 5_656
Sb3 Ca7 Sb6 93.61(8) . 5_666
Sb2 Ca7 Sb6 84.57(3) 5_666 5_666
Sb2 Ca7 Sb6 160.70(12) 5_656 5_666
Sb6 Ca7 Sb6 91.51(10) 5_656 5_666
Sb3 Ca7 Mn3 94.85(15) . .
Sb2 Ca7 Mn3 49.05(6) 5_666 .
Sb2 Ca7 Mn3 49.05(6) 5_656 .
Sb6 Ca7 Mn3 133.40(6) 5_656 .
Sb6 Ca7 Mn3 133.40(6) 5_666 .
Sb3 Ca7 Mn1 135.71(6) . 5_666
Sb2 Ca7 Mn1 51.60(6) 5_666 5_666
Sb2 Ca7 Mn1 112.25(11) 5_656 5_666
Sb6 Ca7 Mn1 111.88(11) 5_656 5_666
Sb6 Ca7 Mn1 52.03(6) 5_666 5_666
Mn3 Ca7 Mn1 92.79(12) . 5_666
Sb3 Ca7 Mn1 135.71(6) . 5_656
Sb2 Ca7 Mn1 112.25(11) 5_666 5_656
Sb2 Ca7 Mn1 51.60(6) 5_656 5_656
Sb6 Ca7 Mn1 52.03(6) 5_656 5_656
Sb6 Ca7 Mn1 111.88(11) 5_666 5_656
Mn3 Ca7 Mn1 92.79(12) . 5_656
Mn1 Ca7 Mn1 87.20(10) 5_666 5_656
Sb3 Ca7 Mn2 46.78(6) . 5_656
Sb2 Ca7 Mn2 150.79(12) 5_666 5_656
Sb2 Ca7 Mn2 87.89(5) 5_656 5_656
Sb6 Ca7 Mn2 48.41(6) 5_656 5_656
Sb6 Ca7 Mn2 103.60(10) 5_666 5_656
Mn3 Ca7 Mn2 115.28(12) . 5_656
Mn1 Ca7 Mn2 151.92(13) 5_666 5_656
Mn1 Ca7 Mn2 90.97(6) 5_656 5_656
Sb3 Ca7 Mn2 46.78(6) . 5_666
Sb2 Ca7 Mn2 87.89(5) 5_666 5_666
Sb2 Ca7 Mn2 150.79(12) 5_656 5_666
Sb6 Ca7 Mn2 103.60(10) 5_656 5_666
Sb6 Ca7 Mn2 48.41(6) 5_666 5_666
Mn3 Ca7 Mn2 115.28(12) . 5_666
Mn1 Ca7 Mn2 90.97(6) 5_666 5_666
Mn1 Ca7 Mn2 151.92(13) 5_656 5_666
Mn2 Ca7 Mn2 77.73(9) 5_656 5_666
Sb3 Ca7 Ca3 66.86(9) . .
Sb2 Ca7 Ca3 133.54(5) 5_666 .
Sb2 Ca7 Ca3 133.54(5) 5_656 .
Sb6 Ca7 Ca3 52.10(6) 5_656 .
Sb6 Ca7 Ca3 52.10(6) 5_666 .
Mn3 Ca7 Ca3 161.72(17) . .
Mn1 Ca7 Ca3 100.39(10) 5_666 .
Mn1 Ca7 Ca3 100.39(10) 5_656 .
Mn2 Ca7 Ca3 52.43(7) 5_656 .
Mn2 Ca7 Ca3 52.43(7) 5_666 .
Sb3 Ca7 Ca6 138.91(14) . 6_657
Sb2 Ca7 Ca6 51.79(6) 5_666 6_657
Sb2 Ca7 Ca6 51.79(6) 5_656 6_657
Sb6 Ca7 Ca6 114.16(9) 5_656 6_657
Sb6 Ca7 Ca6 114.16(9) 5_666 6_657
Mn3 Ca7 Ca6 44.06(14) . 6_657
Mn1 Ca7 Ca6 62.14(8) 5_666 6_657
Mn1 Ca7 Ca6 62.14(8) 5_656 6_657
Mn2 Ca7 Ca6 139.43(6) 5_656 6_657
Mn2 Ca7 Ca6 139.43(6) 5_666 6_657
Ca3 Ca7 Ca6 154.23(13) . 6_657
Mn6B Ca8 Mn6B 93.72(16) 5_656 5_666
Mn6B Ca8 Sb1 116.92(15) 5_656 5_666
Mn6B Ca8 Sb1 52.40(9) 5_666 5_666
Mn6B Ca8 Sb1 52.40(9) 5_656 5_656
Mn6B Ca8 Sb1 116.92(15) 5_666 5_656
Sb1 Ca8 Sb1 93.48(12) 5_666 5_656
Mn6B Ca8 Sb3 132.78(8) 5_656 .
Mn6B Ca8 Sb3 132.78(8) 5_666 .
Sb1 Ca8 Sb3 101.09(11) 5_666 .
Sb1 Ca8 Sb3 101.09(11) 5_656 .
Mn6B Ca8 Mn6B 65.05(13) 5_656 .
Mn6B Ca8 Mn6B 65.05(13) 5_666 .
Sb1 Ca8 Mn6B 117.43(11) 5_666 .
Sb1 Ca8 Mn6B 117.43(11) 5_656 .
Sb3 Ca8 Mn6B 121.45(16) . .
Mn6B Ca8 Sb5 52.73(9) 5_656 5_656
Mn6B Ca8 Sb5 113.86(15) 5_666 5_656
Sb1 Ca8 Sb5 164.69(16) 5_666 5_656
Sb1 Ca8 Sb5 87.50(3) 5_656 5_656
Sb3 Ca8 Sb5 93.68(9) . 5_656
Mn6B Ca8 Sb5 49.70(7) . 5_656
Mn6B Ca8 Sb5 113.86(15) 5_656 5_666
Mn6B Ca8 Sb5 52.73(9) 5_666 5_666
Sb1 Ca8 Sb5 87.50(3) 5_666 5_666
Sb1 Ca8 Sb5 164.69(16) 5_656 5_666
Sb3 Ca8 Sb5 93.68(9) . 5_666
Mn6B Ca8 Sb5 49.70(7) . 5_666
Sb5 Ca8 Sb5 87.60(11) 5_656 5_666
Mn6B Ca8 Mn5 93.90(13) 5_656 .
Mn6B Ca8 Mn5 93.90(13) 5_666 .
Sb1 Ca8 Mn5 48.64(6) 5_666 .
Sb1 Ca8 Mn5 48.64(6) 5_656 .
Sb3 Ca8 Mn5 90.94(14) . .
Mn6B Ca8 Mn5 147.61(18) . .
Sb5 Ca8 Mn5 135.87(6) 5_656 .
Sb5 Ca8 Mn5 135.87(6) 5_666 .
Mn6B Ca8 Sb5 46.93(8) 5_656 .
Mn6B Ca8 Sb5 46.93(8) 5_666 .
Sb1 Ca8 Sb5 85.36(9) 5_666 .
Sb1 Ca8 Sb5 85.36(9) 5_656 .
Sb3 Ca8 Sb5 170.48(15) . .
Mn6B Ca8 Sb5 49.03(10) . .
Sb5 Ca8 Sb5 79.50(9) 5_656 .
Sb5 Ca8 Sb5 79.50(9) 5_666 .
Mn5 Ca8 Sb5 98.58(13) . .
Mn6B Ca8 Ca4 108.94(13) 5_656 .
Mn6B Ca8 Ca4 108.94(13) 5_666 .
Sb1 Ca8 Ca4 130.48(7) 5_666 .
Sb1 Ca8 Ca4 130.48(7) 5_656 .
Sb3 Ca8 Ca4 55.02(9) . .
Mn6B Ca8 Ca4 66.43(13) . .
Sb5 Ca8 Ca4 56.48(7) 5_656 .
Sb5 Ca8 Ca4 56.48(7) 5_666 .
Mn5 Ca8 Ca4 145.96(17) . .
Sb5 Ca8 Ca4 115.46(13) . .
Mn6B Ca8 Mn6A 18.19(14) 5_656 5_656
Mn6B Ca8 Mn6A 86.28(14) 5_666 5_656
Sb1 Ca8 Mn6A 99.42(15) 5_666 5_656
Sb1 Ca8 Mn6A 43.97(13) 5_656 5_656
Sb3 Ca8 Mn6A 140.37(11) . 5_656
Mn6B Ca8 Mn6A 76.50(17) . 5_656
Sb5 Ca8 Mn6A 70.89(13) 5_656 5_656
Sb5 Ca8 Mn6A 120.81(17) 5_666 5_656
Mn5 Ca8 Mn6A 77.88(17) . 5_656
Sb5 Ca8 Mn6A 43.37(11) . 5_656
Ca4 Ca8 Mn6A 127.10(16) . 5_656
Sb9B Ca9 Sb9B 105.2(2) 5_656 5_666
Sb9B Ca9 Mn6A 59.06(17) 5_656 5_656
Sb9B Ca9 Mn6A 134.6(3) 5_666 5_656
Sb9B Ca9 Mn6A 134.6(3) 5_656 5_666
Sb9B Ca9 Mn6A 59.06(17) 5_666 5_666
Mn6A Ca9 Mn6A 100.0(3) 5_656 5_666
Sb9B Ca9 Mn5 122.91(13) 5_656 .
Sb9B Ca9 Mn5 122.91(13) 5_666 .
Mn6A Ca9 Mn5 98.1(2) 5_656 .
Mn6A Ca9 Mn5 98.1(2) 5_666 .
Sb9B Ca9 Sb9A 96.60(15) 5_656 1_655
Sb9B Ca9 Sb9A 96.60(15) 5_666 1_655
Mn6A Ca9 Sb9A 125.69(17) 5_656 1_655
Mn6A Ca9 Sb9A 125.69(17) 5_666 1_655
Mn5 Ca9 Sb9A 52.48(13) . 1_655
Sb9B Ca9 Sb9A 8.97(5) 5_656 5_656
Sb9B Ca9 Sb9A 96.56(16) 5_666 5_656
Mn6A Ca9 Sb9A 66.94(17) 5_656 5_656
Mn6A Ca9 Sb9A 132.1(2) 5_666 5_656
Mn5 Ca9 Sb9A 128.47(12) . 5_656
Sb9A Ca9 Sb9A 95.24(13) 1_655 5_656
Sb9B Ca9 Sb9A 96.56(16) 5_656 5_666
Sb9B Ca9 Sb9A 8.97(5) 5_666 5_666
Mn6A Ca9 Sb9A 132.1(2) 5_656 5_666
Mn6A Ca9 Sb9A 66.94(17) 5_666 5_666
Mn5 Ca9 Sb9A 128.47(12) . 5_666
Sb9A Ca9 Sb9A 95.24(13) 1_655 5_666
Sb9A Ca9 Sb9A 87.87(14) 5_656 5_666
Sb9B Ca9 Sb5 90.49(14) 5_656 .
Sb9B Ca9 Sb5 90.49(14) 5_666 .
Mn6A Ca9 Sb5 51.24(15) 5_656 .
Mn6A Ca9 Sb5 51.24(15) 5_666 .
Mn5 Ca9 Sb5 115.82(18) . .
Sb9A Ca9 Sb5 168.29(17) 1_655 .
Sb9A Ca9 Sb5 93.18(12) 5_656 .
Sb9A Ca9 Sb5 93.18(12) 5_666 .
Sb9B Ca9 Sb9B 89.91(15) 5_656 1_655
Sb9B Ca9 Sb9B 89.91(15) 5_666 1_655
Mn6A Ca9 Sb9B 128.64(16) 5_656 1_655
Mn6A Ca9 Sb9B 128.64(16) 5_666 1_655
Mn5 Ca9 Sb9B 63.54(15) . 1_655
Sb9A Ca9 Sb9B 11.07(5) 1_655 1_655
Sb9A Ca9 Sb9B 87.28(12) 5_656 1_655
Sb9A Ca9 Sb9B 87.28(12) 5_666 1_655
Sb5 Ca9 Sb9B 179.36(18) . 1_655
Sb9B Ca9 Sb1 169.94(15) 5_656 5_666
Sb9B Ca9 Sb1 84.66(7) 5_666 5_666
Mn6A Ca9 Sb1 112.4(2) 5_656 5_666
Mn6A Ca9 Sb1 48.86(17) 5_666 5_666
Mn5 Ca9 Sb1 50.35(8) . 5_666
Sb9A Ca9 Sb1 84.25(11) 1_655 5_666
Sb9A Ca9 Sb1 178.73(13) 5_656 5_666
Sb9A Ca9 Sb1 93.33(4) 5_666 5_666
Sb5 Ca9 Sb1 87.16(11) . 5_666
Sb9B Ca9 Sb1 92.37(12) 1_655 5_666
Sb9B Ca9 Sb1 84.66(7) 5_656 5_656
Sb9B Ca9 Sb1 169.94(15) 5_666 5_656
Mn6A Ca9 Sb1 48.86(17) 5_656 5_656
Mn6A Ca9 Sb1 112.4(2) 5_666 5_656
Mn5 Ca9 Sb1 50.35(8) . 5_656
Sb9A Ca9 Sb1 84.25(11) 1_655 5_656
Sb9A Ca9 Sb1 93.33(4) 5_656 5_656
Sb9A Ca9 Sb1 178.73(13) 5_666 5_656
Sb5 Ca9 Sb1 87.16(11) . 5_656
Sb9B Ca9 Sb1 92.37(12) 1_655 5_656
Sb1 Ca9 Sb1 85.46(11) 5_666 5_656
Sb4 Mn1 Sb4 114.45(10) 5_656 5_666
Sb4 Mn1 Sb2 113.17(7) 5_656 .
Sb4 Mn1 Sb2 113.17(7) 5_666 .
Sb4 Mn1 Sb6 108.47(7) 5_656 .
Sb4 Mn1 Sb6 108.47(7) 5_666 .
Sb2 Mn1 Sb6 97.58(9) . .
Sb4 Mn1 Ca7 166.02(9) 5_656 5_666
Sb4 Mn1 Ca7 79.09(5) 5_666 5_666
Sb2 Mn1 Ca7 61.25(7) . 5_666
Sb6 Mn1 Ca7 61.75(7) . 5_666
Sb4 Mn1 Ca7 79.09(5) 5_656 5_656
Sb4 Mn1 Ca7 166.02(9) 5_666 5_656
Sb2 Mn1 Ca7 61.25(8) . 5_656
Sb6 Mn1 Ca7 61.75(7) . 5_656
Ca7 Mn1 Ca7 87.20(10) 5_666 5_656
Sb4 Mn1 Ca2 58.19(5) 5_656 6_656
Sb4 Mn1 Ca2 58.19(5) 5_666 6_656
Sb2 Mn1 Ca2 149.75(12) . 6_656
Sb6 Mn1 Ca2 112.68(11) . 6_656
Ca7 Mn1 Ca2 133.49(7) 5_666 6_656
Ca7 Mn1 Ca2 133.49(7) 5_656 6_656
Sb3 Mn2 Sb3 113.63(10) 5_656 5_666
Sb3 Mn2 Sb8 110.45(7) 5_656 .
Sb3 Mn2 Sb8 110.45(7) 5_666 .
Sb3 Mn2 Sb6 112.05(7) 5_656 .
Sb3 Mn2 Sb6 112.05(7) 5_666 .
Sb8 Mn2 Sb6 97.02(9) . .
Sb3 Mn2 Ca3 166.03(9) 5_656 5_666
Sb3 Mn2 Ca3 80.20(5) 5_666 5_666
Sb8 Mn2 Ca3 60.46(8) . 5_666
Sb6 Mn2 Ca3 61.54(8) . 5_666
Sb3 Mn2 Ca3 80.20(5) 5_656 5_656
Sb3 Mn2 Ca3 166.03(9) 5_666 5_656
Sb8 Mn2 Ca3 60.46(8) . 5_656
Sb6 Mn2 Ca3 61.53(8) . 5_656
Ca3 Mn2 Ca3 85.91(11) 5_666 5_656
Sb3 Mn2 Ca7 56.84(6) 5_656 5_656
Sb3 Mn2 Ca7 120.22(10) 5_666 5_656
Sb8 Mn2 Ca7 128.62(8) . 5_656
Sb6 Mn2 Ca7 57.42(7) . 5_656
Ca3 Mn2 Ca7 118.91(11) 5_666 5_656
Ca3 Mn2 Ca7 68.17(9) 5_656 5_656
Sb3 Mn2 Ca7 120.22(10) 5_656 5_666
Sb3 Mn2 Ca7 56.84(6) 5_666 5_666
Sb8 Mn2 Ca7 128.62(8) . 5_666
Sb6 Mn2 Ca7 57.42(7) . 5_666
Ca3 Mn2 Ca7 68.17(8) 5_666 5_666
Ca3 Mn2 Ca7 118.91(11) 5_656 5_666
Ca7 Mn2 Ca7 77.73(9) 5_656 5_666
Sb3 Mn2 Ca5 60.37(6) 5_656 .
Sb3 Mn2 Ca5 60.37(6) 5_666 .
Sb8 Mn2 Ca5 155.08(11) . .
Sb6 Mn2 Ca5 107.89(10) . .
Ca3 Mn2 Ca5 132.45(7) 5_666 .
Ca3 Mn2 Ca5 132.45(7) 5_656 .
Ca7 Mn2 Ca5 68.29(8) 5_656 .
Ca7 Mn2 Ca5 68.29(8) 5_666 .
Sb7 Mn3 Sb2 113.83(16) . 5_656
Sb7 Mn3 Sb2 113.83(16) . 5_666
Sb2 Mn3 Sb2 116.5(2) 5_656 5_666
Sb7 Mn3 Ca6 167.4(3) . 6_657
Sb2 Mn3 Ca6 71.30(14) 5_656 6_657
Sb2 Mn3 Ca6 71.30(14) 5_666 6_657
Sb7 Mn3 Ca2 71.00(15) . 5_666
Sb2 Mn3 Ca2 165.2(3) 5_656 5_666
Sb2 Mn3 Ca2 71.17(7) 5_666 5_666
Ca6 Mn3 Ca2 101.20(19) 6_657 5_666
Sb7 Mn3 Ca2 71.00(15) . 5_656
Sb2 Mn3 Ca2 71.17(7) 5_656 5_656
Sb2 Mn3 Ca2 165.2(3) 5_666 5_656
Ca6 Mn3 Ca2 101.20(19) 6_657 5_656
Ca2 Mn3 Ca2 98.6(2) 5_666 5_656
Sb7 Mn3 Ca7 111.9(2) . .
Sb2 Mn3 Ca7 62.37(13) 5_656 .
Sb2 Mn3 Ca7 62.37(13) 5_666 .
Ca6 Mn3 Ca7 80.68(19) 6_657 .
Ca2 Mn3 Ca7 130.21(12) 5_666 .
Ca2 Mn3 Ca7 130.21(12) 5_656 .
Sb7 Mn3 Ca5 57.17(12) . 5_656
Sb2 Mn3 Ca5 60.30(10) 5_656 5_656
Sb2 Mn3 Ca5 123.0(2) 5_666 5_656
Ca6 Mn3 Ca5 130.91(16) 6_657 5_656
Ca2 Mn3 Ca5 127.8(2) 5_666 5_656
Ca2 Mn3 Ca5 71.64(11) 5_656 5_656
Ca7 Mn3 Ca5 70.62(14) . 5_656
Sb7 Mn3 Ca5 57.17(12) . 5_666
Sb2 Mn3 Ca5 123.0(2) 5_656 5_666
Sb2 Mn3 Ca5 60.30(10) 5_666 5_666
Ca6 Mn3 Ca5 130.91(16) 6_657 5_666
Ca2 Mn3 Ca5 71.64(11) 5_666 5_666
Ca2 Mn3 Ca5 127.8(2) 5_656 5_666
Ca7 Mn3 Ca5 70.62(14) . 5_666
Ca5 Mn3 Ca5 75.43(14) 5_656 5_666
Ca1 Mn4 Ca1 98.1(3) 5_656 3_656
Ca1 Mn4 Sb7 77.31(18) 5_656 .
Ca1 Mn4 Sb7 77.31(18) 3_656 .
Ca1 Mn4 Sb9A 58.04(16) 5_656 1_655
Ca1 Mn4 Sb9A 58.04(16) 3_656 1_655
Sb7 Mn4 Sb9A 106.57(19) . 1_655
Ca1 Mn4 Sb8 163.0(2) 5_656 5_766
Ca1 Mn4 Sb8 73.59(13) 3_656 5_766
Sb7 Mn4 Sb8 114.18(12) . 5_766
Sb9A Mn4 Sb8 105.45(12) 1_655 5_766
Ca1 Mn4 Sb8 73.59(13) 5_656 5_756
Ca1 Mn4 Sb8 163.0(2) 3_656 5_756
Sb7 Mn4 Sb8 114.18(12) . 5_756
Sb9A Mn4 Sb8 105.45(12) 1_655 5_756
Sb8 Mn4 Sb8 110.17(18) 5_766 5_756
Ca1 Mn4 Ca4 99.00(19) 5_656 1_655
Ca1 Mn4 Ca4 99.00(19) 3_656 1_655
Sb7 Mn4 Ca4 174.2(2) . 1_655
Sb9A Mn4 Ca4 67.67(14) 1_655 1_655
Sb8 Mn4 Ca4 68.45(11) 5_766 1_655
Sb8 Mn4 Ca4 68.45(11) 5_756 1_655
Ca1 Mn4 Ca1 9.55(14) 5_656 3_646
Ca1 Mn4 Ca1 107.6(2) 3_656 3_646
Sb7 Mn4 Ca1 79.94(15) . 3_646
Sb9A Mn4 Ca1 65.12(13) 1_655 3_646
Sb8 Mn4 Ca1 165.4(2) 5_766 3_646
Sb8 Mn4 Ca1 64.40(11) 5_756 3_646
Ca4 Mn4 Ca1 97.15(15) 1_655 3_646
Ca1 Mn4 Ca1 107.6(2) 5_656 5_666
Ca1 Mn4 Ca1 9.55(14) 3_656 5_666
Sb7 Mn4 Ca1 79.94(14) . 5_666
Sb9A Mn4 Ca1 65.12(13) 1_655 5_666
Sb8 Mn4 Ca1 64.40(11) 5_766 5_666
Sb8 Mn4 Ca1 165.4(2) 5_756 5_666
Ca4 Mn4 Ca1 97.15(15) 1_655 5_666
Ca1 Mn4 Ca1 117.2(3) 3_646 5_666
Ca1 Mn4 Mn5 51.64(16) 5_656 .
Ca1 Mn4 Mn5 51.64(16) 3_656 .
Sb7 Mn4 Mn5 51.65(13) . .
Sb9A Mn4 Mn5 54.91(14) 1_655 .
Sb8 Mn4 Mn5 124.59(9) 5_766 .
Sb8 Mn4 Mn5 124.59(9) 5_756 .
Ca4 Mn4 Mn5 122.58(19) 1_655 .
Ca1 Mn4 Mn5 60.44(13) 3_646 .
Ca1 Mn4 Mn5 60.44(13) 5_666 .
Ca1 Mn4 Ca3 130.94(15) 5_656 1_655
Ca1 Mn4 Ca3 130.94(15) 3_656 1_655
Sb7 Mn4 Ca3 108.09(17) . 1_655
Sb9A Mn4 Ca3 145.3(2) 1_655 1_655
Sb8 Mn4 Ca3 59.52(9) 5_766 1_655
Sb8 Mn4 Ca3 59.52(9) 5_756 1_655
Ca4 Mn4 Ca3 77.68(15) 1_655 1_655
Ca1 Mn4 Ca3 121.39(13) 3_646 1_655
Ca1 Mn4 Ca3 121.39(13) 5_666 1_655
Mn5 Mn4 Ca3 159.7(2) . 1_655
Ca1 Mn4 Ca2 134.2(2) 5_656 5_666
Ca1 Mn4 Ca2 77.38(14) 3_656 5_666
Sb7 Mn4 Ca2 57.10(10) . 5_666
Sb9A Mn4 Ca2 135.36(11) 1_655 5_666
Sb8 Mn4 Ca2 59.55(8) 5_766 5_666
Sb8 Mn4 Ca2 119.17(16) 5_756 5_666
Ca4 Mn4 Ca2 126.79(13) 1_655 5_666
Ca1 Mn4 Ca2 135.05(18) 3_646 5_666
Ca1 Mn4 Ca2 70.90(11) 5_666 5_666
Mn5 Mn4 Ca2 96.80(14) . 5_666
Ca3 Mn4 Ca2 67.45(11) 1_655 5_666
Ca1 Mn5 Ca1 95.1(3) 3_656 5_656
Ca1 Mn5 Sb7 75.89(16) 3_656 .
Ca1 Mn5 Sb7 75.89(16) 5_656 .
Ca1 Mn5 Sb1 163.6(2) 3_656 5_656
Ca1 Mn5 Sb1 74.50(13) 5_656 5_656
Sb7 Mn5 Sb1 112.71(11) . 5_656
Ca1 Mn5 Sb1 74.50(13) 3_656 5_666
Ca1 Mn5 Sb1 163.6(2) 5_656 5_666
Sb7 Mn5 Sb1 112.71(11) . 5_666
Sb1 Mn5 Sb1 112.45(16) 5_656 5_666
Ca1 Mn5 Sb9A 57.48(15) 3_656 1_655
Ca1 Mn5 Sb9A 57.48(15) 5_656 1_655
Sb7 Mn5 Sb9A 106.05(17) . 1_655
Sb1 Mn5 Sb9A 106.12(12) 5_656 1_655
Sb1 Mn5 Sb9A 106.12(12) 5_666 1_655
Ca1 Mn5 Ca9 99.34(18) 3_656 .
Ca1 Mn5 Ca9 99.34(18) 5_656 .
Sb7 Mn5 Ca9 172.7(2) . .
Sb1 Mn5 Ca9 70.59(10) 5_656 .
Sb1 Mn5 Ca9 70.59(10) 5_666 .
Sb9A Mn5 Ca9 66.68(15) 1_655 .
Ca1 Mn5 Ca1 9.69(14) 3_656 5_666
Ca1 Mn5 Ca1 104.8(2) 5_656 5_666
Sb7 Mn5 Ca1 78.72(13) . 5_666
Sb1 Mn5 Ca1 167.5(2) 5_656 5_666
Sb1 Mn5 Ca1 65.07(11) 5_666 5_666
Sb9A Mn5 Ca1 64.47(13) 1_655 5_666
Ca9 Mn5 Ca1 97.47(15) . 5_666
Ca1 Mn5 Ca1 104.8(2) 3_656 3_646
Ca1 Mn5 Ca1 9.69(14) 5_656 3_646
Sb7 Mn5 Ca1 78.72(13) . 3_646
Sb1 Mn5 Ca1 65.07(11) 5_656 3_646
Sb1 Mn5 Ca1 167.5(2) 5_666 3_646
Sb9A Mn5 Ca1 64.47(13) 1_655 3_646
Ca9 Mn5 Ca1 97.47(14) . 3_646
Ca1 Mn5 Ca1 114.5(2) 5_666 3_646
Ca1 Mn5 Mn4 49.99(15) 3_656 .
Ca1 Mn5 Mn4 49.99(15) 5_656 .
Sb7 Mn5 Mn4 51.06(12) . .
Sb1 Mn5 Mn4 123.63(8) 5_656 .
Sb1 Mn5 Mn4 123.63(8) 5_666 .
Sb9A Mn5 Mn4 54.99(14) 1_655 .
Ca9 Mn5 Mn4 121.7(2) . .
Ca1 Mn5 Mn4 58.97(12) 5_666 .
Ca1 Mn5 Mn4 58.97(12) 3_646 .
Ca1 Mn5 Ca8 132.46(14) 3_656 .
Ca1 Mn5 Ca8 132.46(15) 5_656 .
Sb7 Mn5 Ca8 112.09(17) . .
Sb1 Mn5 Ca8 58.95(9) 5_656 .
Sb1 Mn5 Ca8 58.95(9) 5_666 .
Sb9A Mn5 Ca8 141.85(18) 1_655 .
Ca9 Mn5 Ca8 75.18(16) . .
Ca1 Mn5 Ca8 122.77(12) 5_666 .
Ca1 Mn5 Ca8 122.77(12) 3_646 .
Mn4 Mn5 Ca8 163.2(2) . .
Ca1 Mn5 Ca5 76.97(14) 3_656 5_666
Ca1 Mn5 Ca5 132.1(2) 5_656 5_666
Sb7 Mn5 Ca5 56.27(9) . 5_666
Sb1 Mn5 Ca5 119.45(16) 5_656 5_666
Sb1 Mn5 Ca5 58.83(8) 5_666 5_666
Sb9A Mn5 Ca5 134.41(10) 1_655 5_666
Ca9 Mn5 Ca5 128.52(13) . 5_666
Ca1 Mn5 Ca5 70.61(11) 5_666 5_666
Ca1 Mn5 Ca5 133.53(17) 3_646 5_666
Mn4 Mn5 Ca5 95.35(13) . 5_666
Ca8 Mn5 Ca5 71.47(11) . 5_666
Mn6B Mn6A Sb1 81.9(5) . .
Mn6B Mn6A Sb5 76.5(3) . 5_666
Sb1 Mn6A Sb5 117.41(19) . 5_666
Mn6B Mn6A Sb5 76.5(3) . 5_656
Sb1 Mn6A Sb5 117.41(19) . 5_656
Sb5 Mn6A Sb5 113.2(3) 5_666 5_656
Mn6B Mn6A Sb9B 179.0(6) . .
Sb1 Mn6A Sb9B 99.2(3) . .
Sb5 Mn6A Sb9B 103.0(2) 5_666 .
Sb5 Mn6A Sb9B 103.0(2) 5_656 .
Mn6B Mn6A Ca9 121.8(3) . 5_656
Sb1 Mn6A Ca9 73.2(2) . 5_656
Sb5 Mn6A Ca9 161.1(4) 5_666 5_656
Sb5 Mn6A Ca9 70.57(10) 5_656 5_656
Sb9B Mn6A Ca9 58.64(17) . 5_656
Mn6B Mn6A Ca9 121.8(3) . 5_666
Sb1 Mn6A Ca9 73.2(2) . 5_666
Sb5 Mn6A Ca9 70.57(10) 5_666 5_666
Sb5 Mn6A Ca9 161.1(4) 5_656 5_666
Sb9B Mn6A Ca9 58.64(17) . 5_666
Ca9 Mn6A Ca9 100.0(3) 5_656 5_666
Mn6B Mn6A Ca4 115.6(5) . .
Sb1 Mn6A Ca4 162.5(4) . .
Sb5 Mn6A Ca4 69.62(18) 5_666 .
Sb5 Mn6A Ca4 69.62(18) 5_656 .
Sb9B Mn6A Ca4 63.3(2) . .
Ca9 Mn6A Ca4 96.0(2) 5_656 .
Ca9 Mn6A Ca4 96.0(2) 5_666 .
Mn6B Mn6A Ca8 51.0(3) . 5_656
Sb1 Mn6A Ca8 55.29(15) . 5_656
Sb5 Mn6A Ca8 126.9(3) 5_666 5_656
Sb5 Mn6A Ca8 65.69(13) 5_656 5_656
Sb9B Mn6A Ca8 129.7(2) . 5_656
Ca9 Mn6A Ca8 71.87(14) 5_656 5_656
Ca9 Mn6A Ca8 128.2(3) 5_666 5_656
Ca4 Mn6A Ca8 135.23(17) . 5_656
Mn6B Mn6A Ca8 51.0(3) . 5_666
Sb1 Mn6A Ca8 55.29(15) . 5_666
Sb5 Mn6A Ca8 65.69(13) 5_666 5_666
Sb5 Mn6A Ca8 126.9(3) 5_656 5_666
Sb9B Mn6A Ca8 129.7(2) . 5_666
Ca9 Mn6A Ca8 128.2(3) 5_656 5_666
Ca9 Mn6A Ca8 71.87(14) 5_666 5_666
Ca4 Mn6A Ca8 135.23(17) . 5_666
Ca8 Mn6A Ca8 74.68(18) 5_656 5_666
Mn6A Mn6B Sb5 76.9(2) . 5_666
Mn6A Mn6B Sb5 76.9(2) . 5_656
Sb5 Mn6B Sb5 113.51(16) 5_666 5_656
Mn6A Mn6B Sb1 71.4(4) . .
Sb5 Mn6B Sb1 113.65(11) 5_666 .
Sb5 Mn6B Sb1 113.65(11) 5_656 .
Mn6A Mn6B Sb5 176.0(5) . .
Sb5 Mn6B Sb5 105.10(11) 5_666 .
Sb5 Mn6B Sb5 105.10(11) 5_656 .
Sb1 Mn6B Sb5 104.61(14) . .
Mn6A Mn6B Ca8 110.8(3) . 5_656
Sb5 Mn6B Ca8 169.22(16) 5_666 5_656
Sb5 Mn6B Ca8 76.22(7) 5_656 5_656
Sb1 Mn6B Ca8 63.91(11) . 5_656
Sb5 Mn6B Ca8 66.69(11) . 5_656
Mn6A Mn6B Ca8 110.8(3) . 5_666
Sb5 Mn6B Ca8 76.22(7) 5_666 5_666
Sb5 Mn6B Ca8 169.22(16) 5_656 5_666
Sb1 Mn6B Ca8 63.91(11) . 5_666
Sb5 Mn6B Ca8 66.69(11) . 5_666
Ca8 Mn6B Ca8 93.72(16) 5_656 5_666
Mn6A Mn6B Ca8 110.5(5) . .
Sb5 Mn6B Ca8 67.15(10) 5_666 .
Sb5 Mn6B Ca8 67.15(10) 5_656 .
Sb1 Mn6B Ca8 178.07(19) . .
Sb5 Mn6B Ca8 73.46(13) . .
Ca8 Mn6B Ca8 114.95(13) 5_656 .
Ca8 Mn6B Ca8 114.95(13) 5_666 .
Mn6A Sb1 Mn5 115.53(12) . 5_656
Mn6A Sb1 Mn5 115.53(12) . 5_666
Mn5 Sb1 Mn5 112.45(17) 5_656 5_666
Mn6A Sb1 Mn6B 26.7(2) . .
Mn5 Sb1 Mn6B 122.88(8) 5_656 .
Mn5 Sb1 Mn6B 122.88(8) 5_666 .
Mn6A Sb1 Ca8 80.75(16) . 5_666
Mn5 Sb1 Ca8 155.31(13) 5_656 5_666
Mn5 Sb1 Ca8 72.41(11) 5_666 5_666
Mn6B Sb1 Ca8 63.68(10) . 5_666
Mn6A Sb1 Ca8 80.75(16) . 5_656
Mn5 Sb1 Ca8 72.41(11) 5_656 5_656
Mn5 Sb1 Ca8 155.31(13) 5_666 5_656
Mn6B Sb1 Ca8 63.68(10) . 5_656
Ca8 Sb1 Ca8 93.48(12) 5_666 5_656
Mn6A Sb1 Ca1 128.4(2) . .
Mn5 Sb1 Ca1 50.04(13) 5_656 .
Mn5 Sb1 Ca1 64.11(13) 5_666 .
Mn6B Sb1 Ca1 154.51(14) . .
Ca8 Sb1 Ca1 134.88(12) 5_666 .
Ca8 Sb1 Ca1 121.70(12) 5_656 .
Mn6A Sb1 Ca1 128.4(2) . 7_565
Mn5 Sb1 Ca1 64.11(13) 5_656 7_565
Mn5 Sb1 Ca1 50.04(13) 5_666 7_565
Mn6B Sb1 Ca1 154.51(14) . 7_565
Ca8 Sb1 Ca1 121.70(12) 5_666 7_565
Ca8 Sb1 Ca1 134.88(12) 5_656 7_565
Ca1 Sb1 Ca1 14.2(2) . 7_565
Mn6A Sb1 Ca5 154.9(2) . .
Mn5 Sb1 Ca5 76.04(10) 5_656 .
Mn5 Sb1 Ca5 76.04(10) 5_666 .
Mn6B Sb1 Ca5 128.15(12) . .
Ca8 Sb1 Ca5 82.12(9) 5_666 .
Ca8 Sb1 Ca5 82.12(9) 5_656 .
Ca1 Sb1 Ca5 76.50(11) . .
Ca1 Sb1 Ca5 76.50(11) 7_565 .
Mn6A Sb1 Ca9 57.99(14) . 5_666
Mn5 Sb1 Ca9 127.88(13) 5_656 5_666
Mn5 Sb1 Ca9 59.06(12) 5_666 5_666
Mn6B Sb1 Ca9 75.84(12) . 5_666
Ca8 Sb1 Ca9 76.07(10) 5_666 5_666
Ca8 Sb1 Ca9 138.39(13) 5_656 5_666
Ca1 Sb1 Ca9 91.11(13) . 5_666
Ca1 Sb1 Ca9 81.46(13) 7_565 5_666
Ca5 Sb1 Ca9 134.09(7) . 5_666
Mn6A Sb1 Ca9 57.99(14) . 5_656
Mn5 Sb1 Ca9 59.06(12) 5_656 5_656
Mn5 Sb1 Ca9 127.88(13) 5_666 5_656
Mn6B Sb1 Ca9 75.84(12) . 5_656
Ca8 Sb1 Ca9 138.39(13) 5_666 5_656
Ca8 Sb1 Ca9 76.07(10) 5_656 5_656
Ca1 Sb1 Ca9 81.46(13) . 5_656
Ca1 Sb1 Ca9 91.11(13) 7_565 5_656
Ca5 Sb1 Ca9 134.09(7) . 5_656
Ca9 Sb1 Ca9 85.46(11) 5_666 5_656
Mn3 Sb2 Mn3 116.5(2) 5_656 5_666
Mn3 Sb2 Mn1 121.27(12) 5_656 .
Mn3 Sb2 Mn1 121.27(12) 5_666 .
Mn3 Sb2 Ca7 150.17(16) 5_656 5_666
Mn3 Sb2 Ca7 68.58(14) 5_666 5_666
Mn1 Sb2 Ca7 67.15(8) . 5_666
Mn3 Sb2 Ca7 68.58(14) 5_656 5_656
Mn3 Sb2 Ca7 150.17(16) 5_666 5_656
Mn1 Sb2 Ca7 67.15(7) . 5_656
Ca7 Sb2 Ca7 92.91(10) 5_666 5_656
Mn3 Sb2 Ca6 56.03(15) 5_656 2_554
Mn3 Sb2 Ca6 130.93(17) 5_666 2_554
Mn1 Sb2 Ca6 78.14(9) . 2_554
Ca7 Sb2 Ca6 144.95(11) 5_666 2_554
Ca7 Sb2 Ca6 77.52(8) 5_656 2_554
Mn3 Sb2 Ca6 130.93(17) 5_656 2_564
Mn3 Sb2 Ca6 56.03(16) 5_666 2_564
Mn1 Sb2 Ca6 78.14(9) . 2_564
Ca7 Sb2 Ca6 77.52(8) 5_666 2_564
Ca7 Sb2 Ca6 144.95(11) 5_656 2_564
Ca6 Sb2 Ca6 91.09(11) 2_554 2_564
Mn3 Sb2 Ca2 58.99(13) 5_656 .
Mn3 Sb2 Ca2 58.99(13) 5_666 .
Mn1 Sb2 Ca2 158.70(9) . .
Ca7 Sb2 Ca2 124.65(7) 5_666 .
Ca7 Sb2 Ca2 124.65(7) 5_656 .
Ca6 Sb2 Ca2 87.03(10) 2_554 .
Ca6 Sb2 Ca2 87.03(10) 2_564 .
Mn3 Sb2 Ca5 75.54(15) 5_656 .
Mn3 Sb2 Ca5 75.54(15) 5_666 .
Mn1 Sb2 Ca5 127.87(9) . .
Ca7 Sb2 Ca5 77.83(8) 5_666 .
Ca7 Sb2 Ca5 77.83(8) 5_656 .
Ca6 Sb2 Ca5 130.89(7) 2_554 .
Ca6 Sb2 Ca5 130.89(7) 2_564 .
Ca2 Sb2 Ca5 73.43(9) . .
Mn2 Sb3 Mn2 113.63(11) 5_656 5_666
Mn2 Sb3 Ca7 76.39(7) 5_656 .
Mn2 Sb3 Ca7 76.39(7) 5_666 .
Mn2 Sb3 Ca8 115.40(7) 5_656 .
Mn2 Sb3 Ca8 115.40(7) 5_666 .
Ca7 Sb3 Ca8 153.86(11) . .
Mn2 Sb3 Ca4 79.10(7) 5_656 .
Mn2 Sb3 Ca4 79.10(7) 5_666 .
Ca7 Sb3 Ca4 134.32(11) . .
Ca8 Sb3 Ca4 71.82(11) . .
Mn2 Sb3 Ca5 151.33(9) 5_656 5_666
Mn2 Sb3 Ca5 73.63(7) 5_666 5_666
Ca7 Sb3 Ca5 78.83(8) . 5_666
Ca8 Sb3 Ca5 82.41(9) . 5_666
Ca4 Sb3 Ca5 129.23(7) . 5_666
Mn2 Sb3 Ca5 73.63(7) 5_656 5_656
Mn2 Sb3 Ca5 151.33(9) 5_666 5_656
Ca7 Sb3 Ca5 78.83(8) . 5_656
Ca8 Sb3 Ca5 82.41(9) . 5_656
Ca4 Sb3 Ca5 129.23(7) . 5_656
Ca5 Sb3 Ca5 87.67(9) 5_666 5_656
Mn1 Sb4 Mn1 114.45(10) 5_656 5_666
Mn1 Sb4 Ca3 110.03(7) 5_656 6_657
Mn1 Sb4 Ca3 110.03(7) 5_666 6_657
Mn1 Sb4 Ca2 161.93(10) 5_656 2_565
Mn1 Sb4 Ca2 76.16(7) 5_666 2_565
Ca3 Sb4 Ca2 77.60(9) 6_657 2_565
Mn1 Sb4 Ca2 76.16(7) 5_656 2
Mn1 Sb4 Ca2 161.93(10) 5_666 2
Ca3 Sb4 Ca2 77.60(9) 6_657 2
Ca2 Sb4 Ca2 90.08(10) 2_565 2
Mn1 Sb4 Ca6 80.27(8) 5_656 .
Mn1 Sb4 Ca6 80.27(8) 5_666 .
Ca3 Sb4 Ca6 158.94(11) 6_657 .
Ca2 Sb4 Ca6 87.62(9) 2_565 .
Ca2 Sb4 Ca6 87.62(9) 2 .
Mn1 Sb4 Ca6 75.63(8) 5_656 6_657
Mn1 Sb4 Ca6 75.63(8) 5_666 6_657
Ca3 Sb4 Ca6 66.53(10) 6_657 6_657
Ca2 Sb4 Ca6 122.14(8) 2_565 6_657
Ca2 Sb4 Ca6 122.14(8) 2 6_657
Ca6 Sb4 Ca6 134.52(4) . 6_657
Mn6B Sb5 Mn6B 113.51(16) 5_666 5_656
Mn6B Sb5 Mn6A 26.6(2) 5_666 5_666
Mn6B Sb5 Mn6A 120.14(18) 5_656 5_666
Mn6B Sb5 Mn6A 120.14(18) 5_666 5_656
Mn6B Sb5 Mn6A 26.6(2) 5_656 5_656
Mn6A Sb5 Mn6A 113.2(3) 5_666 5_656
Mn6B Sb5 Mn6B 74.90(11) 5_666 .
Mn6B Sb5 Mn6B 74.90(11) 5_656 .
Mn6A Sb5 Mn6B 101.45(19) 5_666 .
Mn6A Sb5 Mn6B 101.45(19) 5_656 .
Mn6B Sb5 Ca8 134.91(12) 5_666 5_656
Mn6B Sb5 Ca8 63.15(11) 5_656 5_656
Mn6A Sb5 Ca8 161.24(19) 5_666 5_656
Mn6A Sb5 Ca8 77.96(17) 5_656 5_656
Mn6B Sb5 Ca8 60.58(9) . 5_656
Mn6B Sb5 Ca8 63.15(11) 5_666 5_666
Mn6B Sb5 Ca8 134.91(12) 5_656 5_666
Mn6A Sb5 Ca8 77.96(17) 5_666 5_666
Mn6A Sb5 Ca8 161.24(19) 5_656 5_666
Mn6B Sb5 Ca8 60.58(9) . 5_666
Ca8 Sb5 Ca8 87.60(11) 5_656 5_666
Mn6B Sb5 Ca9 77.27(11) 5_666 .
Mn6B Sb5 Ca9 77.27(11) 5_656 .
Mn6A Sb5 Ca9 58.19(16) 5_666 .
Mn6A Sb5 Ca9 58.19(16) 5_656 .
Mn6B Sb5 Ca9 127.94(12) . .
Ca8 Sb5 Ca9 135.98(6) 5_656 .
Ca8 Sb5 Ca9 135.98(6) 5_666 .
Mn6B Sb5 Ca4 156.73(12) 5_666 5_656
Mn6B Sb5 Ca4 77.09(9) 5_656 5_656
Mn6A Sb5 Ca4 130.1(2) 5_666 5_656
Mn6A Sb5 Ca4 60.32(18) 5_656 5_656
Mn6B Sb5 Ca4 128.36(8) . 5_656
Ca8 Sb5 Ca4 68.19(9) 5_656 5_656
Ca8 Sb5 Ca4 125.00(10) 5_666 5_656
Ca9 Sb5 Ca4 85.55(9) . 5_656
Mn6B Sb5 Ca4 77.09(9) 5_666 5_666
Mn6B Sb5 Ca4 156.73(12) 5_656 5_666
Mn6A Sb5 Ca4 60.32(18) 5_666 5_666
Mn6A Sb5 Ca4 130.1(2) 5_656 5_666
Mn6B Sb5 Ca4 128.36(8) . 5_666
Ca8 Sb5 Ca4 125.00(10) 5_656 5_666
Ca8 Sb5 Ca4 68.19(9) 5_666 5_666
Ca9 Sb5 Ca4 85.55(9) . 5_666
Ca4 Sb5 Ca4 86.13(10) 5_656 5_666
Mn6B Sb5 Ca8 56.85(8) 5_666 .
Mn6B Sb5 Ca8 56.85(8) 5_656 .
Mn6A Sb5 Ca8 70.94(18) 5_666 .
Mn6A Sb5 Ca8 70.94(18) 5_656 .
Mn6B Sb5 Ca8 57.51(11) . .
Ca8 Sb5 Ca8 100.50(9) 5_656 .
Ca8 Sb5 Ca8 100.50(9) 5_666 .
Ca9 Sb5 Ca8 70.42(11) . .
Ca4 Sb5 Ca8 131.18(6) 5_656 .
Ca4 Sb5 Ca8 131.18(6) 5_666 .
Mn2 Sb6 Mn1 121.68(9) . .
Mn2 Sb6 Ca7 74.17(7) . 5_656
Mn1 Sb6 Ca7 66.22(7) . 5_656
Mn2 Sb6 Ca7 74.17(7) . 5_666
Mn1 Sb6 Ca7 66.22(7) . 5_666
Ca7 Sb6 Ca7 91.51(10) 5_656 5_666
Mn2 Sb6 Ca3 67.31(8) . 5_666
Mn1 Sb6 Ca3 134.32(5) . 5_666
Ca7 Sb6 Ca3 141.38(9) 5_656 5_666
Ca7 Sb6 Ca3 75.92(8) 5_666 5_666
Mn2 Sb6 Ca3 67.31(8) . 5_656
Mn1 Sb6 Ca3 134.32(5) . 5_656
Ca7 Sb6 Ca3 75.92(8) 5_656 5_656
Ca7 Sb6 Ca3 141.38(9) 5_666 5_656
Ca3 Sb6 Ca3 91.31(10) 5_666 5_656
Mn2 Sb6 Ca6 132.50(7) . 5_656
Mn1 Sb6 Ca6 79.21(9) . 5_656
Ca7 Sb6 Ca6 78.57(8) 5_656 5_656
Ca7 Sb6 Ca6 145.06(11) 5_666 5_656
Ca3 Sb6 Ca6 130.84(11) 5_666 5_656
Ca3 Sb6 Ca6 68.76(9) 5_656 5_656
Mn2 Sb6 Ca6 132.50(7) . 5_666
Mn1 Sb6 Ca6 79.21(9) . 5_666
Ca7 Sb6 Ca6 145.06(11) 5_656 5_666
Ca7 Sb6 Ca6 78.57(8) 5_666 5_666
Ca3 Sb6 Ca6 68.76(9) 5_666 5_666
Ca3 Sb6 Ca6 130.84(11) 5_656 5_666
Ca6 Sb6 Ca6 90.55(11) 5_656 5_666
Mn3 Sb7 Mn4 126.4(2) . .
Mn3 Sb7 Mn5 156.3(2) . .
Mn4 Sb7 Mn5 77.28(16) . .
Mn3 Sb7 Ca1 140.38(12) . 5_656
Mn4 Sb7 Ca1 50.64(13) . 5_656
Mn5 Sb7 Ca1 51.90(12) . 5_656
Mn3 Sb7 Ca1 140.38(12) . 3_656
Mn4 Sb7 Ca1 50.64(13) . 3_656
Mn5 Sb7 Ca1 51.90(12) . 3_656
Ca1 Sb7 Ca1 73.5(2) 5_656 3_656
Mn3 Sb7 Ca5 82.36(13) . 5_656
Mn4 Sb7 Ca5 128.74(7) . 5_656
Mn5 Sb7 Ca5 81.30(10) . 5_656
Ca1 Sb7 Ca5 79.62(12) 5_656 5_656
Ca1 Sb7 Ca5 133.13(13) 3_656 5_656
Mn3 Sb7 Ca5 82.36(13) . 5_666
Mn4 Sb7 Ca5 128.74(7) . 5_666
Mn5 Sb7 Ca5 81.30(10) . 5_666
Ca1 Sb7 Ca5 133.13(12) 5_656 5_666
Ca1 Sb7 Ca5 79.62(12) 3_656 5_666
Ca5 Sb7 Ca5 92.36(10) 5_656 5_666
Mn3 Sb7 Ca2 62.80(12) . 5_666
Mn4 Sb7 Ca2 81.01(11) . 5_666
Mn5 Sb7 Ca2 129.21(7) . 5_666
Ca1 Sb7 Ca2 131.47(13) 5_656 5_666
Ca1 Sb7 Ca2 78.95(12) 3_656 5_666
Ca5 Sb7 Ca2 144.58(10) 5_656 5_666
Ca5 Sb7 Ca2 77.62(8) 5_666 5_666
Mn3 Sb7 Ca2 62.80(12) . 5_656
Mn4 Sb7 Ca2 81.01(11) . 5_656
Mn5 Sb7 Ca2 129.21(7) . 5_656
Ca1 Sb7 Ca2 78.95(11) 5_656 5_656
Ca1 Sb7 Ca2 131.47(13) 3_656 5_656
Ca5 Sb7 Ca2 77.62(8) 5_656 5_656
Ca5 Sb7 Ca2 144.58(10) 5_666 5_656
Ca2 Sb7 Ca2 91.00(10) 5_666 5_656
Mn3 Sb7 Ca1 131.23(10) . 3_646
Mn4 Sb7 Ca1 57.14(10) . 3_646
Mn5 Sb7 Ca1 58.13(10) . 3_646
Ca1 Sb7 Ca1 9.96(14) 5_656 3_646
Ca1 Sb7 Ca1 83.50(12) 3_656 3_646
Ca5 Sb7 Ca1 71.94(11) 5_656 3_646
Ca5 Sb7 Ca1 137.80(11) 5_666 3_646
Ca2 Sb7 Ca1 136.11(12) 5_666 3_646
Ca2 Sb7 Ca1 71.46(10) 5_656 3_646
Mn3 Sb7 Ca1 131.23(10) . 5_666
Mn4 Sb7 Ca1 57.14(11) . 5_666
Mn5 Sb7 Ca1 58.13(10) . 5_666
Ca1 Sb7 Ca1 83.50(12) 5_656 5_666
Ca1 Sb7 Ca1 9.96(14) 3_656 5_666
Ca5 Sb7 Ca1 137.80(11) 5_656 5_666
Ca5 Sb7 Ca1 71.94(11) 5_666 5_666
Ca2 Sb7 Ca1 71.46(10) 5_666 5_666
Ca2 Sb7 Ca1 136.11(12) 5_656 5_666
Ca1 Sb7 Ca1 93.46(17) 3_646 5_666
Mn4 Sb8 Mn4 110.17(18) 5_766 5_756
Mn4 Sb8 Mn2 124.33(9) 5_766 .
Mn4 Sb8 Mn2 124.33(9) 5_756 .
Mn4 Sb8 Ca3 149.44(13) 5_766 5_656
Mn4 Sb8 Ca3 70.53(11) 5_756 5_656
Mn2 Sb8 Ca3 68.42(8) . 5_656
Mn4 Sb8 Ca3 70.53(11) 5_766 5_666
Mn4 Sb8 Ca3 149.44(13) 5_756 5_666
Mn2 Sb8 Ca3 68.42(8) . 5_666
Ca3 Sb8 Ca3 93.49(11) 5_656 5_666
Mn4 Sb8 Ca1 49.04(13) 5_766 7_665
Mn4 Sb8 Ca1 63.26(13) 5_756 7_665
Mn2 Sb8 Ca1 155.90(12) . 7_665
Ca3 Sb8 Ca1 130.67(12) 5_656 7_665
Ca3 Sb8 Ca1 117.98(12) 5_666 7_665
Mn4 Sb8 Ca1 63.26(13) 5_766 1_655
Mn4 Sb8 Ca1 49.04(13) 5_756 1_655
Mn2 Sb8 Ca1 155.90(12) . 1_655
Ca3 Sb8 Ca1 117.98(12) 5_656 1_655
Ca3 Sb8 Ca1 130.67(12) 5_666 1_655
Ca1 Sb8 Ca1 14.4(2) 7_665 1_655
Mn4 Sb8 Ca4 59.10(11) 5_766 5_666
Mn4 Sb8 Ca4 129.26(13) 5_756 5_666
Mn2 Sb8 Ca4 77.09(8) . 5_666
Ca3 Sb8 Ca4 145.05(11) 5_656 5_666
Ca3 Sb8 Ca4 78.55(8) 5_666 5_666
Ca1 Sb8 Ca4 81.51(12) 7_665 5_666
Ca1 Sb8 Ca4 91.58(12) 1_655 5_666
Mn4 Sb8 Ca4 129.26(13) 5_766 5_656
Mn4 Sb8 Ca4 59.10(11) 5_756 5_656
Mn2 Sb8 Ca4 77.09(8) . 5_656
Ca3 Sb8 Ca4 78.55(8) 5_656 5_656
Ca3 Sb8 Ca4 145.05(11) 5_666 5_656
Ca1 Sb8 Ca4 91.58(12) 7_665 5_656
Ca1 Sb8 Ca4 81.51(12) 1_655 5_656
Ca4 Sb8 Ca4 88.69(11) 5_666 5_656
Mn4 Sb8 Ca2 74.91(11) 5_766 1_655
Mn4 Sb8 Ca2 74.91(11) 5_756 1_655
Mn2 Sb8 Ca2 126.89(9) . 1_655
Ca3 Sb8 Ca2 76.02(9) 5_656 1_655
Ca3 Sb8 Ca2 76.02(9) 5_666 1_655
Ca1 Sb8 Ca2 76.28(12) 7_665 1_655
Ca1 Sb8 Ca2 76.28(12) 1_655 1_655
Ca4 Sb8 Ca2 132.65(6) 5_666 1_655
Ca4 Sb8 Ca2 132.65(6) 5_656 1_655
Sb9B Sb9A Ca1 132.03(17) . 3_556
Sb9B Sb9A Ca1 132.03(17) . 5_556
Ca1 Sb9A Ca1 94.3(3) 3_556 5_556
Sb9B Sb9A Mn5 153.6(6) . 1_455
Ca1 Sb9A Mn5 56.91(15) 3_556 1_455
Ca1 Sb9A Mn5 56.91(14) 5_556 1_455
Sb9B Sb9A Mn4 136.3(6) . 1_455
Ca1 Sb9A Mn4 55.43(14) 3_556 1_455
Ca1 Sb9A Mn4 55.43(14) 5_556 1_455
Mn5 Sb9A Mn4 70.10(15) 1_455 1_455
Sb9B Sb9A Ca1 122.55(13) . 5_566
Ca1 Sb9A Ca1 9.72(14) 3_556 5_566
Ca1 Sb9A Ca1 103.99(19) 5_556 5_566
Mn5 Sb9A Ca1 63.97(12) 1_455 5_566
Mn4 Sb9A Ca1 62.87(11) 1_455 5_566
Sb9B Sb9A Ca1 122.55(13) . 3_546
Ca1 Sb9A Ca1 103.99(19) 3_556 3_546
Ca1 Sb9A Ca1 9.72(14) 5_556 3_546
Mn5 Sb9A Ca1 63.97(12) 1_455 3_546
Mn4 Sb9A Ca1 62.87(11) 1_455 3_546
Ca1 Sb9A Ca1 113.7(2) 5_566 3_546
Sb9B Sb9A Ca9 92.7(6) . 1_455
Ca1 Sb9A Ca9 95.07(16) 3_556 1_455
Ca1 Sb9A Ca9 95.07(16) 5_556 1_455
Mn5 Sb9A Ca9 60.85(14) 1_455 1_455
Mn4 Sb9A Ca9 130.95(17) 1_455 1_455
Ca1 Sb9A Ca9 94.08(12) 5_566 1_455
Ca1 Sb9A Ca9 94.08(12) 3_546 1_455
Sb9B Sb9A Ca4 76.7(6) . .
Ca1 Sb9A Ca4 92.08(15) 3_556 .
Ca1 Sb9A Ca4 92.08(15) 5_556 .
Mn5 Sb9A Ca4 129.68(15) 1_455 .
Mn4 Sb9A Ca4 59.59(14) 1_455 .
Ca1 Sb9A Ca4 91.67(12) 5_566 .
Ca1 Sb9A Ca4 91.67(12) 3_546 .
Ca9 Sb9A Ca4 169.47(15) 1_455 .
Sb9B Sb9A Ca9 44.83(12) . 5_656
Ca1 Sb9A Ca9 176.79(16) 3_556 5_656
Ca1 Sb9A Ca9 88.93(13) 5_556 5_656
Mn5 Sb9A Ca9 125.41(11) 1_455 5_656
Mn4 Sb9A Ca9 126.83(11) 1_455 5_656
Ca1 Sb9A Ca9 167.07(14) 5_566 5_656
Ca1 Sb9A Ca9 79.21(11) 3_546 5_656
Ca9 Sb9A Ca9 84.76(13) 1_455 5_656
Ca4 Sb9A Ca9 87.66(12) . 5_656
Sb9B Sb9A Ca9 44.83(12) . 5_666
Ca1 Sb9A Ca9 88.93(14) 3_556 5_666
Ca1 Sb9A Ca9 176.79(16) 5_556 5_666
Mn5 Sb9A Ca9 125.41(11) 1_455 5_666
Mn4 Sb9A Ca9 126.83(11) 1_455 5_666
Ca1 Sb9A Ca9 79.21(11) 5_566 5_666
Ca1 Sb9A Ca9 167.07(14) 3_546 5_666
Ca9 Sb9A Ca9 84.76(13) 1_455 5_666
Ca4 Sb9A Ca9 87.66(12) . 5_666
Ca9 Sb9A Ca9 87.87(14) 5_656 5_666
Sb9A Sb9B Ca9 126.20(15) . 5_656
Sb9A Sb9B Ca9 126.20(15) . 5_666
Ca9 Sb9B Ca9 105.2(2) 5_656 5_666
Sb9A Sb9B Mn6A 153.5(6) . .
Ca9 Sb9B Mn6A 62.30(14) 5_656 .
Ca9 Sb9B Mn6A 62.30(14) 5_666 .
Sb9A Sb9B Ca1 39.02(15) . 3_556
Ca9 Sb9B Ca1 165.20(18) 5_656 3_556
Ca9 Sb9B Ca1 88.86(13) 5_666 3_556
Mn6A Sb9B Ca1 130.54(18) . 3_556
Sb9A Sb9B Ca1 39.02(15) . 5_556
Ca9 Sb9B Ca1 88.86(13) 5_656 5_556
Ca9 Sb9B Ca1 165.20(17) 5_666 5_556
Mn6A Sb9B Ca1 130.54(17) . 5_556
Ca1 Sb9B Ca1 76.8(2) 3_556 5_556
Sb9A Sb9B Ca4 91.9(6) . .
Ca9 Sb9B Ca4 97.09(15) 5_656 .
Ca9 Sb9B Ca4 97.09(15) 5_666 .
Mn6A Sb9B Ca4 61.6(2) . .
Ca1 Sb9B Ca4 85.64(15) 3_556 .
Ca1 Sb9B Ca4 85.64(15) 5_556 .
Sb9A Sb9B Ca9 76.2(6) . 1_455
Ca9 Sb9B Ca9 90.09(15) 5_656 1_455
Ca9 Sb9B Ca9 90.09(15) 5_666 1_455
Mn6A Sb9B Ca9 130.3(2) . 1_455
Ca1 Sb9B Ca9 85.06(15) 3_556 1_455
Ca1 Sb9B Ca9 85.06(15) 5_556 1_455
Ca4 Sb9B Ca9 168.13(18) . 1_455
Sb9A Sb9B Ca1 48.85(12) . 5_566
Ca9 Sb9B Ca1 174.29(18) 5_656 5_566
Ca9 Sb9B Ca1 78.87(12) 5_666 5_566
Mn6A Sb9B Ca1 123.40(14) . 5_566
Ca1 Sb9B Ca1 10.01(14) 3_556 5_566
Ca1 Sb9B Ca1 86.82(16) 5_556 5_566
Ca4 Sb9B Ca1 86.31(13) . 5_566
Ca9 Sb9B Ca1 85.82(13) 1_455 5_566
Sb9A Sb9B Ca1 48.85(12) . 3_546
Ca9 Sb9B Ca1 78.87(12) 5_656 3_546
Ca9 Sb9B Ca1 174.29(18) 5_666 3_546
Mn6A Sb9B Ca1 123.40(14) . 3_546
Ca1 Sb9B Ca1 86.82(16) 3_556 3_546
Ca1 Sb9B Ca1 10.01(14) 5_556 3_546
Ca4 Sb9B Ca1 86.31(13) . 3_546
Ca9 Sb9B Ca1 85.82(13) 1_455 3_546
Ca1 Sb9B Ca1 96.8(2) 5_566 3_546
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ca1 Ca1 0.806(11) 7_565
Ca1 Mn4 2.531(6) 5_656
Ca1 Mn5 2.591(6) 5_656
Ca1 Sb9A 2.608(6) 5_556
Ca1 Sb9B 3.077(6) 5_556
Ca1 Mn4 3.184(6) 5_666
Ca1 Sb7 3.194(5) 5_656
Ca1 Sb8 3.215(6) 1_455
Ca1 Mn5 3.232(6) 5_666
Ca1 Sb9A 3.245(6) 5_566
Ca1 Sb1 3.258(6) .
Ca1 Sb9B 3.633(6) 5_566
Ca2 Mn3 3.053(5) 5_666
Ca2 Mn3 3.053(5) 5_656
Ca2 Sb7 3.245(3) 5_666
Ca2 Sb7 3.245(3) 5_656
Ca2 Sb4 3.271(3) 2_554
Ca2 Sb4 3.271(3) 2_564
Ca2 Sb2 3.371(4) .
Ca2 Sb8 3.409(4) 1_455
Ca2 Mn1 3.738(4) 6_556
Ca2 Mn4 3.818(5) 5_666
Ca2 Mn4 3.818(5) 5_656
Ca2 Ca5 4.045(5) .
Ca3 Sb8 3.178(3) 5_656
Ca3 Sb8 3.178(3) 5_666
Ca3 Sb4 3.208(4) 6_557
Ca3 Sb6 3.237(3) 5_666
Ca3 Sb6 3.237(3) 5_656
Ca3 Mn2 3.397(3) 5_666
Ca3 Mn2 3.397(3) 5_656
Ca3 Mn4 3.477(6) 1_455
Ca3 Ca6 3.667(6) .
Ca3 Ca7 3.978(5) .
Ca3 Ca2 4.060(5) 5_556
Ca3 Ca2 4.060(5) 5_566
Ca4 Mn4 3.055(7) 1_455
Ca4 Mn6A 3.142(10) .
Ca4 Sb9B 3.191(6) .
Ca4 Sb3 3.256(4) .
Ca4 Sb9A 3.277(5) .
Ca4 Sb8 3.311(3) 5_666
Ca4 Sb8 3.311(3) 5_656
Ca4 Sb5 3.390(3) 5_656
Ca4 Sb5 3.390(3) 5_666
Ca4 Ca8 3.775(6) .
Ca4 Ca1 4.261(7) 5_556
Ca5 Sb7 3.208(3) 5_656
Ca5 Sb7 3.208(3) 5_666
Ca5 Sb3 3.342(3) 5_666
Ca5 Sb3 3.342(3) 5_656
Ca5 Sb1 3.362(4) .
Ca5 Sb2 3.394(4) .
Ca5 Mn2 3.689(5) .
Ca5 Mn3 3.784(6) 5_656
Ca5 Mn3 3.784(6) 5_666
Ca5 Mn5 3.813(5) 5_666
Ca5 Mn5 3.813(5) 5_656
Ca6 Mn3 2.839(8) 6_557
Ca6 Sb2 3.243(3) 2_565
Ca6 Sb2 3.243(3) 2
Ca6 Sb6 3.258(3) 5_656
Ca6 Sb6 3.258(3) 5_666
Ca6 Sb4 3.308(5) .
Ca6 Sb4 3.466(5) 6_557
Ca6 Ca7 4.029(5) 6_557
Ca6 Ca7 4.108(5) .
Ca7 Sb3 3.177(4) .
Ca7 Sb2 3.193(3) 5_666
Ca7 Sb2 3.193(3) 5_656
Ca7 Sb6 3.231(3) 5_656
Ca7 Sb6 3.231(3) 5_666
Ca7 Mn3 3.355(8) .
Ca7 Mn1 3.356(3) 5_666
Ca7 Mn1 3.356(3) 5_656
Ca7 Mn2 3.689(3) 5_656
Ca7 Mn2 3.689(3) 5_666
Ca7 Ca6 4.029(5) 6_657
Ca8 Mn6B 3.172(4) 5_656
Ca8 Mn6B 3.172(4) 5_666
Ca8 Sb1 3.178(3) 5_666
Ca8 Sb1 3.178(3) 5_656
Ca8 Sb3 3.180(5) .
Ca8 Mn6B 3.238(6) .
Ca8 Sb5 3.344(3) 5_656
Ca8 Sb5 3.344(3) 5_666
Ca8 Mn5 3.537(7) .
Ca8 Sb5 3.680(5) .
Ca8 Mn6A 3.816(8) 5_656
Ca9 Sb9B 2.915(4) 5_656
Ca9 Sb9B 2.915(4) 5_666
Ca9 Mn6A 3.022(7) 5_656
Ca9 Mn6A 3.022(7) 5_666
Ca9 Mn5 3.102(7) .
Ca9 Sb9A 3.262(6) 1_655
Ca9 Sb9A 3.336(4) 5_656
Ca9 Sb9A 3.336(4) 5_666
Ca9 Sb5 3.354(6) .
Ca9 Sb9B 3.355(7) 1_655
Ca9 Sb1 3.411(4) 5_666
Ca9 Sb1 3.411(4) 5_656
Mn1 Sb4 2.7528(16) 5_656
Mn1 Sb4 2.7528(16) 5_666
Mn1 Sb2 2.854(3) .
Mn1 Sb6 2.891(3) .
Mn1 Ca7 3.356(3) 5_666
Mn1 Ca7 3.356(3) 5_656
Mn1 Ca2 3.738(4) 6_656
Mn2 Sb3 2.7656(17) 5_656
Mn2 Sb3 2.7656(17) 5_666
Mn2 Sb8 2.844(3) .
Mn2 Sb6 2.868(3) .
Mn2 Ca3 3.397(3) 5_666
Mn2 Ca3 3.397(3) 5_656
Mn2 Ca7 3.689(3) 5_656
Mn2 Ca7 3.689(3) 5_666
Mn3 Sb7 2.477(7) .
Mn3 Sb2 2.722(4) 5_656
Mn3 Sb2 2.722(4) 5_666
Mn3 Ca6 2.839(8) 6_657
Mn3 Ca2 3.053(5) 5_666
Mn3 Ca2 3.053(5) 5_656
Mn3 Ca5 3.784(6) 5_656
Mn3 Ca5 3.784(6) 5_666
Mn4 Ca1 2.531(7) 5_656
Mn4 Ca1 2.531(6) 3_656
Mn4 Sb7 2.581(5) .
Mn4 Sb9A 2.820(6) 1_655
Mn4 Sb8 2.823(3) 5_766
Mn4 Sb8 2.823(3) 5_756
Mn4 Ca4 3.055(7) 1_655
Mn4 Ca1 3.184(6) 3_646
Mn4 Ca1 3.184(6) 5_666
Mn4 Mn5 3.237(7) .
Mn4 Ca3 3.477(6) 1_655
Mn4 Ca2 3.818(5) 5_666
Mn5 Ca1 2.591(7) 3_656
Mn5 Ca1 2.591(6) 5_656
Mn5 Sb7 2.603(5) .
Mn5 Sb1 2.785(3) 5_656
Mn5 Sb1 2.785(3) 5_666
Mn5 Sb9A 2.817(6) 1_655
Mn5 Ca1 3.232(6) 5_666
Mn5 Ca1 3.232(6) 3_646
Mn5 Ca5 3.813(5) 5_666
Mn6A Mn6B 1.274(10) .
Mn6A Sb1 2.684(9) .
Mn6A Sb5 2.773(5) 5_666
Mn6A Sb5 2.773(5) 5_656
Mn6A Sb9B 2.927(10) .
Mn6A Ca9 3.022(7) 5_656
Mn6A Ca9 3.022(7) 5_666
Mn6A Ca8 3.816(8) 5_656
Mn6A Ca8 3.816(8) 5_666
Mn6B Sb5 2.768(3) 5_666
Mn6B Sb5 2.768(3) 5_656
Mn6B Sb1 2.804(5) .
Mn6B Sb5 2.898(5) .
Mn6B Ca8 3.172(4) 5_656
Mn6B Ca8 3.172(4) 5_666
Sb1 Mn5 2.785(3) 5_656
Sb1 Mn5 2.785(3) 5_666
Sb1 Ca8 3.178(3) 5_666
Sb1 Ca8 3.178(3) 5_656
Sb1 Ca1 3.258(6) 7_565
Sb1 Ca9 3.411(4) 5_666
Sb1 Ca9 3.411(4) 5_656
Sb2 Mn3 2.722(4) 5_656
Sb2 Mn3 2.722(4) 5_666
Sb2 Ca7 3.193(3) 5_666
Sb2 Ca7 3.193(3) 5_656
Sb2 Ca6 3.243(3) 2_554
Sb2 Ca6 3.243(3) 2_564
Sb3 Mn2 2.7656(17) 5_656
Sb3 Mn2 2.7656(17) 5_666
Sb3 Ca5 3.342(3) 5_666
Sb3 Ca5 3.342(3) 5_656
Sb4 Mn1 2.7528(16) 5_656
Sb4 Mn1 2.7528(16) 5_666
Sb4 Ca3 3.208(4) 6_657
Sb4 Ca2 3.271(3) 2_565
Sb4 Ca2 3.271(3) 2
Sb4 Ca6 3.466(5) 6_657
Sb5 Mn6B 2.768(3) 5_666
Sb5 Mn6B 2.768(3) 5_656
Sb5 Mn6A 2.773(5) 5_666
Sb5 Mn6A 2.773(5) 5_656
Sb5 Ca8 3.344(3) 5_656
Sb5 Ca8 3.344(3) 5_666
Sb5 Ca4 3.390(3) 5_656
Sb5 Ca4 3.390(3) 5_666
Sb6 Ca7 3.231(3) 5_656
Sb6 Ca7 3.231(3) 5_666
Sb6 Ca3 3.237(3) 5_666
Sb6 Ca3 3.237(3) 5_656
Sb6 Ca6 3.258(3) 5_656
Sb6 Ca6 3.258(3) 5_666
Sb7 Ca1 3.194(5) 5_656
Sb7 Ca1 3.194(6) 3_656
Sb7 Ca5 3.208(3) 5_656
Sb7 Ca5 3.208(3) 5_666
Sb7 Ca2 3.245(3) 5_666
Sb7 Ca2 3.245(3) 5_656
Sb7 Ca1 3.732(6) 3_646
Sb7 Ca1 3.732(6) 5_666
Sb8 Mn4 2.823(3) 5_766
Sb8 Mn4 2.823(3) 5_756
Sb8 Ca3 3.178(3) 5_656
Sb8 Ca3 3.178(3) 5_666
Sb8 Ca1 3.215(6) 7_665
Sb8 Ca1 3.215(6) 1_655
Sb8 Ca4 3.311(3) 5_666
Sb8 Ca4 3.311(3) 5_656
Sb8 Ca2 3.409(4) 1_655
Sb9A Sb9B 0.645(3) .
Sb9A Ca1 2.608(6) 3_556
Sb9A Ca1 2.608(6) 5_556
Sb9A Mn5 2.817(6) 1_455
Sb9A Mn4 2.820(6) 1_455
Sb9A Ca1 3.245(6) 5_566
Sb9A Ca1 3.245(6) 3_546
Sb9A Ca9 3.262(6) 1_455
Sb9A Ca9 3.336(4) 5_656
Sb9A Ca9 3.336(4) 5_666
Sb9B Ca9 2.915(4) 5_656
Sb9B Ca9 2.915(4) 5_666
Sb9B Ca1 3.077(6) 3_556
Sb9B Ca1 3.077(6) 5_556
Sb9B Ca9 3.355(7) 1_455
Sb9B Ca1 3.633(6) 5_566
Sb9B Ca1 3.633(6) 3_546
