#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:59:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179520 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341705.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341705
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'As9 Ca9 Zn4.46'
_chemical_formula_weight         1326.39
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.855(2)
_cell_length_b                   4.2747(8)
_cell_length_c                   41.440(8)
_cell_measurement_reflns_used    539
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      20.06
_cell_measurement_theta_min      5.72
_cell_volume                     2100.0(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1899
_diffrn_reflns_av_sigmaI/netI    0.0974
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       53
_diffrn_reflns_limit_l_min       -53
_diffrn_reflns_number            24023
_diffrn_reflns_theta_full        27.10
_diffrn_reflns_theta_max         27.10
_diffrn_reflns_theta_min         0.98
_exptl_absorpt_coefficient_mu    21.277
_exptl_absorpt_correction_T_max  0.7408
_exptl_absorpt_correction_T_min  0.5678
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick,2003)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.195
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             2443
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_refine_diff_density_max         3.466
_refine_diff_density_min         -1.486
_refine_diff_density_rms         0.349
_refine_ls_extinction_coef       0.00029(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.999
_refine_ls_matrix_type           full
_refine_ls_number_parameters     157
_refine_ls_number_reflns         2647
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.999
_refine_ls_R_factor_all          0.1118
_refine_ls_R_factor_gt           0.0494
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0280P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0792
_refine_ls_wR_factor_ref         0.0970
_reflns_number_gt                1559
_reflns_number_total             2647
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_002.cif
_cod_data_source_block           III
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_cell_volume        2100.1(7)
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341705
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ca1 Ca 0.0164(4) 0.1737(10) 0.41860(10) 0.0207(15) Uani 0.50 1 d P
Ca2 Ca 0.0304(3) 0.2500 0.32573(7) 0.0178(8) Uani 1 2 d S
Ca3 Ca 0.2400(3) 0.2500 0.67297(8) 0.0163(7) Uani 1 2 d S
Ca4 Ca 0.2840(3) 0.2500 0.57995(9) 0.0234(8) Uani 1 2 d S
Ca5 Ca 0.3045(3) 0.2500 0.37710(8) 0.0142(7) Uani 1 2 d S
Ca6 Ca 0.3081(3) 0.2500 0.75342(8) 0.0183(8) Uani 1 2 d S
Ca7 Ca 0.5453(3) 0.2500 0.69062(7) 0.0180(7) Uani 1 2 d S
Ca8 Ca 0.5684(3) 0.2500 0.54824(9) 0.0286(9) Uani 1 2 d S
Ca9 Ca 0.8592(3) 0.2500 0.50115(9) 0.0396(11) Uani 1 2 d S
Zn1 Zn 0.44134(16) 0.2500 0.25479(4) 0.0184(4) Uani 1 2 d S
Zn2 Zn 0.59389(15) 0.2500 0.36017(5) 0.0173(4) Uani 1 2 d S
Zn3 Zn 0.7828(3) 0.2500 0.67720(9) 0.0157(14) Uani 0.456(6) 2 d SP
Zn4 Zn 0.0748(3) 0.2500 0.61286(10) 0.0232(12) Uani 0.493(4) 2 d SP
Zn5 Zn 0.8348(3) 0.2500 0.57088(8) 0.0159(11) Uani 0.507(4) 2 d SP
Zn6A Zn 0.3004(4) 0.2500 0.50806(10) 0.0227(7) Uani 0.477(3) 2 d SP
Zn6B Zn 0.3799(4) 0.2500 0.49850(9) 0.0227(7) Uani 0.523(3) 2 d SP
As1 As 0.25167(14) 0.2500 0.44985(4) 0.0132(4) Uani 1 2 d S
As2 As 0.27886(13) 0.2500 0.29922(4) 0.0126(4) Uani 1 2 d S
As3 As 0.50110(13) 0.2500 0.61992(4) 0.0140(4) Uani 1 2 d S
As4 As 0.55705(14) 0.2500 0.77739(4) 0.0140(4) Uani 1 2 d S
As5 As 0.61120(15) 0.2500 0.46920(4) 0.0181(4) Uani 1 2 d S
As6 As 0.61988(13) 0.2500 0.29518(4) 0.0119(4) Uani 1 2 d S
As7 As 0.87822(13) 0.2500 0.62877(4) 0.0144(4) Uani 1 2 d S
As8 As 0.81308(14) 0.2500 0.37356(4) 0.0146(4) Uani 1 2 d S
As9A As 0.0520(4) 0.2500 0.54723(11) 0.0138(7) Uani 0.520(5) 2 d SP
As9B As 0.0890(4) 0.2500 0.53639(12) 0.0138(7) Uani 0.480(5) 2 d SP
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ca1 Ca1 As9A 137.98(13) 7_565 5_556
Ca1 Ca1 Zn4 136.92(12) 7_565 5_556
As9A Ca1 Zn4 67.52(17) 5_556 5_556
Ca1 Ca1 Zn5 134.91(11) 7_565 5_656
As9A Ca1 Zn5 66.77(17) 5_556 5_656
Zn4 Ca1 Zn5 82.73(16) 5_556 5_656
Ca1 Ca1 As9B 128.89(10) 7_565 5_556
As9A Ca1 As9B 9.54(7) 5_556 5_556
Zn4 Ca1 As9B 72.09(16) 5_556 5_556
Zn5 Ca1 As9B 75.21(16) 5_656 5_556
Ca1 Ca1 As7 127.90(9) 7_565 5_656
As9A Ca1 As7 94.09(16) 5_556 5_656
Zn4 Ca1 As7 52.13(12) 5_556 5_656
Zn5 Ca1 As7 52.27(11) 5_656 5_656
As9B Ca1 As7 103.20(15) 5_556 5_656
Ca1 Ca1 As9A 33.52(11) 7_565 5_566
As9A Ca1 As9A 104.5(2) 5_556 5_566
Zn4 Ca1 As9A 137.8(2) 5_556 5_566
Zn5 Ca1 As9A 134.1(2) 5_656 5_566
As9B Ca1 As9A 95.43(18) 5_556 5_566
As7 Ca1 As9A 161.33(18) 5_656 5_566
Ca1 Ca1 Zn4 34.50(10) 7_565 5_566
As9A Ca1 Zn4 138.2(2) 5_556 5_566
Zn4 Ca1 Zn4 102.42(19) 5_556 5_566
Zn5 Ca1 Zn4 154.8(2) 5_656 5_566
As9B Ca1 Zn4 129.99(19) 5_556 5_566
As7 Ca1 Zn4 111.67(15) 5_656 5_566
As9A Ca1 Zn4 54.74(14) 5_566 5_566
Ca1 Ca1 Zn5 36.41(10) 7_565 5_666
As9A Ca1 Zn5 135.0(2) 5_556 5_666
Zn4 Ca1 Zn5 156.1(2) 5_556 5_666
Zn5 Ca1 Zn5 98.50(17) 5_656 5_666
As9B Ca1 Zn5 131.52(19) 5_556 5_666
As7 Ca1 Zn5 110.18(14) 5_656 5_666
As9A Ca1 Zn5 54.48(13) 5_566 5_666
Zn4 Ca1 Zn5 66.88(12) 5_566 5_666
Ca1 Ca1 As8 83.89(9) 7_565 1_455
As9A Ca1 As8 99.85(18) 5_556 1_455
Zn4 Ca1 As8 54.19(11) 5_556 1_455
Zn5 Ca1 As8 135.98(17) 5_656 1_455
As9B Ca1 As8 96.88(16) 5_556 1_455
As7 Ca1 As8 89.62(12) 5_656 1_455
As9A Ca1 As8 89.27(15) 5_566 1_455
Zn4 Ca1 As8 50.40(10) 5_566 1_455
Zn5 Ca1 As8 117.01(15) 5_666 1_455
Ca1 Ca1 As1 83.94(8) 7_565 .
As9A Ca1 As1 97.77(18) 5_556 .
Zn4 Ca1 As1 133.66(18) 5_556 .
Zn5 Ca1 As1 51.91(10) 5_656 .
As9B Ca1 As1 100.73(17) 5_556 .
As7 Ca1 As1 87.78(12) 5_656 .
As9A Ca1 As1 87.65(15) 5_566 .
Zn4 Ca1 As1 114.95(15) 5_566 .
Zn5 Ca1 As1 48.37(8) 5_666 .
As8 Ca1 As1 162.33(16) 1_455 .
Ca1 Ca1 As9B 42.35(10) 7_565 5_566
As9A Ca1 As9B 95.70(19) 5_556 5_566
Zn4 Ca1 As9B 132.1(2) 5_556 5_566
Zn5 Ca1 As9B 133.19(19) 5_656 5_566
As9B Ca1 As9B 86.55(17) 5_556 5_566
As7 Ca1 As9B 170.19(17) 5_656 5_566
As9A Ca1 As9B 9.16(6) 5_566 5_566
Zn4 Ca1 As9B 59.96(13) 5_566 5_566
Zn5 Ca1 As9B 62.71(13) 5_666 5_566
As8 Ca1 As9B 88.12(14) 1_455 5_566
As1 Ca1 As9B 91.48(14) . 5_566
As7 Ca2 As7 89.01(9) 5_666 5_656
As7 Ca2 Zn3 44.16(8) 5_666 5_666
As7 Ca2 Zn3 104.80(12) 5_656 5_666
As7 Ca2 Zn3 104.80(12) 5_666 5_656
As7 Ca2 Zn3 44.16(8) 5_656 5_656
Zn3 Ca2 Zn3 87.88(13) 5_666 5_656
As7 Ca2 As4 177.91(12) 5_666 2_554
As7 Ca2 As4 92.01(3) 5_656 2_554
Zn3 Ca2 As4 133.77(13) 5_666 2_554
Zn3 Ca2 As4 74.77(8) 5_656 2_554
As7 Ca2 As4 92.01(3) 5_666 2_564
As7 Ca2 As4 177.91(12) 5_656 2_564
Zn3 Ca2 As4 74.77(8) 5_666 2_564
Zn3 Ca2 As4 133.77(13) 5_656 2_564
As4 Ca2 As4 86.91(9) 2_554 2_564
As7 Ca2 As2 83.30(8) 5_666 .
As7 Ca2 As2 83.30(8) 5_656 .
Zn3 Ca2 As2 46.57(7) 5_666 .
Zn3 Ca2 As2 46.57(7) 5_656 .
As4 Ca2 As2 95.01(8) 2_554 .
As4 Ca2 As2 95.01(8) 2_564 .
As7 Ca2 As8 84.52(8) 5_666 1_455
As7 Ca2 As8 84.52(8) 5_656 1_455
Zn3 Ca2 As8 126.43(9) 5_666 1_455
Zn3 Ca2 As8 126.43(9) 5_656 1_455
As4 Ca2 As8 97.39(8) 2_554 1_455
As4 Ca2 As8 97.39(8) 2_564 1_455
As2 Ca2 As8 162.89(12) . 1_455
As7 Ca2 Zn1 134.17(5) 5_666 6_556
As7 Ca2 Zn1 134.17(5) 5_656 6_556
Zn3 Ca2 Zn1 100.33(10) 5_666 6_556
Zn3 Ca2 Zn1 100.33(10) 5_656 6_556
As4 Ca2 Zn1 44.33(5) 2_554 6_556
As4 Ca2 Zn1 44.33(5) 2_564 6_556
As2 Ca2 Zn1 87.10(9) . 6_556
As8 Ca2 Zn1 110.01(10) 1_455 6_556
As7 Ca2 Zn4 42.22(7) 5_666 5_566
As7 Ca2 Zn4 95.95(10) 5_656 5_566
Zn3 Ca2 Zn4 82.13(9) 5_666 5_566
Zn3 Ca2 Zn4 134.33(13) 5_656 5_566
As4 Ca2 Zn4 139.38(12) 2_554 5_566
As4 Ca2 Zn4 86.03(7) 2_564 5_566
As2 Ca2 Zn4 125.44(9) . 5_566
As8 Ca2 Zn4 44.30(6) 1_455 5_566
Zn1 Ca2 Zn4 125.27(9) 6_556 5_566
As7 Ca2 Zn4 95.95(10) 5_666 5_556
As7 Ca2 Zn4 42.22(7) 5_656 5_556
Zn3 Ca2 Zn4 134.33(13) 5_666 5_556
Zn3 Ca2 Zn4 82.13(9) 5_656 5_556
As4 Ca2 Zn4 86.03(7) 2_554 5_556
As4 Ca2 Zn4 139.38(12) 2_564 5_556
As2 Ca2 Zn4 125.44(9) . 5_556
As8 Ca2 Zn4 44.30(6) 1_455 5_556
Zn1 Ca2 Zn4 125.27(9) 6_556 5_556
Zn4 Ca2 Zn4 74.05(10) 5_566 5_556
As7 Ca2 Ca3 132.51(11) 5_666 5_556
As7 Ca2 Ca3 84.15(6) 5_656 5_556
Zn3 Ca2 Ca3 169.61(9) 5_666 5_556
Zn3 Ca2 Ca3 102.35(6) 5_656 5_556
As4 Ca2 Ca3 49.45(6) 2_554 5_556
As4 Ca2 Ca3 96.48(9) 2_564 5_556
As2 Ca2 Ca3 141.66(6) . 5_556
As8 Ca2 Ca3 48.10(6) 1_455 5_556
Zn1 Ca2 Ca3 76.25(8) 6_556 5_556
Zn4 Ca2 Ca3 91.81(9) 5_566 5_556
Zn4 Ca2 Ca3 50.48(8) 5_556 5_556
As8 Ca3 As8 92.99(10) 5_656 5_666
As8 Ca3 As4 107.18(9) 5_656 6_557
As8 Ca3 As4 107.18(9) 5_666 6_557
As8 Ca3 As6 156.84(13) 5_656 5_666
As8 Ca3 As6 83.68(4) 5_666 5_666
As4 Ca3 As6 95.66(8) 6_557 5_666
As8 Ca3 As6 83.68(4) 5_656 5_656
As8 Ca3 As6 156.84(13) 5_666 5_656
As4 Ca3 As6 95.66(8) 6_557 5_656
As6 Ca3 As6 90.42(10) 5_666 5_656
As8 Ca3 Zn4 49.72(6) 5_656 .
As8 Ca3 Zn4 49.72(6) 5_666 .
As4 Ca3 Zn4 95.31(12) 6_557 .
As6 Ca3 Zn4 133.27(6) 5_666 .
As6 Ca3 Zn4 133.27(6) 5_656 .
As8 Ca3 Zn2 109.48(10) 5_656 5_666
As8 Ca3 Zn2 50.87(6) 5_666 5_666
As4 Ca3 Zn2 137.61(5) 6_557 5_666
As6 Ca3 Zn2 51.50(6) 5_666 5_666
As6 Ca3 Zn2 108.74(10) 5_656 5_666
Zn4 Ca3 Zn2 92.45(10) . 5_666
As8 Ca3 Zn2 50.87(6) 5_656 5_656
As8 Ca3 Zn2 109.48(10) 5_666 5_656
As4 Ca3 Zn2 137.61(5) 6_557 5_656
As6 Ca3 Zn2 108.74(10) 5_666 5_656
As6 Ca3 Zn2 51.50(5) 5_656 5_656
Zn4 Ca3 Zn2 92.45(10) . 5_656
Zn2 Ca3 Zn2 83.35(9) 5_666 5_656
As8 Ca3 Ca6 133.34(5) 5_656 .
As8 Ca3 Ca6 133.34(5) 5_666 .
As4 Ca3 Ca6 60.12(9) 6_557 .
As6 Ca3 Ca6 56.24(6) 5_666 .
As6 Ca3 Ca6 56.24(6) 5_656 .
Zn4 Ca3 Ca6 155.43(14) . .
Zn2 Ca3 Ca6 105.74(9) 5_666 .
Zn2 Ca3 Ca6 105.74(9) 5_656 .
As8 Ca3 Ca7 109.82(9) 5_656 .
As8 Ca3 Ca7 109.82(9) 5_666 .
As4 Ca3 Ca7 125.09(12) 6_557 .
As6 Ca3 Ca7 51.14(6) 5_666 .
As6 Ca3 Ca7 51.14(6) 5_656 .
Zn4 Ca3 Ca7 139.60(13) . .
Zn2 Ca3 Ca7 58.95(7) 5_666 .
Zn2 Ca3 Ca7 58.95(7) 5_656 .
Ca6 Ca3 Ca7 64.97(9) . .
As8 Ca3 Ca2 55.19(6) 5_656 5_556
As8 Ca3 Ca2 103.52(10) 5_666 5_556
As4 Ca3 Ca2 52.18(7) 6_557 5_556
As6 Ca3 Ca2 147.83(11) 5_666 5_556
As6 Ca3 Ca2 93.39(5) 5_656 5_556
Zn4 Ca3 Ca2 59.78(8) . 5_556
Zn2 Ca3 Ca2 152.18(11) 5_666 5_556
Zn2 Ca3 Ca2 98.44(5) 5_656 5_556
Ca6 Ca3 Ca2 100.50(9) . 5_556
Ca7 Ca3 Ca2 144.36(5) . 5_556
As8 Ca3 Ca2 103.52(10) 5_656 5_566
As8 Ca3 Ca2 55.19(6) 5_666 5_566
As4 Ca3 Ca2 52.18(7) 6_557 5_566
As6 Ca3 Ca2 93.39(5) 5_666 5_566
As6 Ca3 Ca2 147.83(11) 5_656 5_566
Zn4 Ca3 Ca2 59.78(8) . 5_566
Zn2 Ca3 Ca2 98.44(5) 5_666 5_566
Zn2 Ca3 Ca2 152.18(11) 5_656 5_566
Ca6 Ca3 Ca2 100.50(9) . 5_566
Ca7 Ca3 Ca2 144.36(5) . 5_566
Ca2 Ca3 Ca2 67.37(8) 5_556 5_566
Zn4 Ca4 As9B 66.80(15) . .
Zn4 Ca4 Zn6A 122.55(16) . .
As9B Ca4 Zn6A 55.75(15) . .
Zn4 Ca4 As3 118.44(14) . .
As9B Ca4 As3 174.76(17) . .
Zn6A Ca4 As3 119.01(15) . .
Zn4 Ca4 As9A 55.06(14) . .
As9B Ca4 As9A 11.75(8) . .
Zn6A Ca4 As9A 67.49(14) . .
As3 Ca4 As9A 173.50(16) . .
Zn4 Ca4 As8 51.33(7) . 5_666
As9B Ca4 As8 95.17(11) . 5_666
Zn6A Ca4 As8 130.13(8) . 5_666
As3 Ca4 As8 88.62(9) . 5_666
As9A Ca4 As8 86.67(11) . 5_666
Zn4 Ca4 As8 51.33(7) . 5_656
As9B Ca4 As8 95.17(11) . 5_656
Zn6A Ca4 As8 130.13(8) . 5_656
As3 Ca4 As8 88.62(9) . 5_656
As9A Ca4 As8 86.67(11) . 5_656
As8 Ca4 As8 87.22(10) 5_666 5_656
Zn4 Ca4 As5 130.27(8) . 5_656
As9B Ca4 As5 85.08(11) . 5_656
Zn6A Ca4 As5 48.71(7) . 5_656
As3 Ca4 As5 91.02(9) . 5_656
As9A Ca4 As5 93.82(11) . 5_656
As8 Ca4 As5 178.20(10) 5_666 5_656
As8 Ca4 As5 94.54(3) 5_656 5_656
Zn4 Ca4 As5 130.27(8) . 5_666
As9B Ca4 As5 85.08(11) . 5_666
Zn6A Ca4 As5 48.71(7) . 5_666
As3 Ca4 As5 91.02(9) . 5_666
As9A Ca4 As5 93.82(11) . 5_666
As8 Ca4 As5 94.54(3) 5_666 5_666
As8 Ca4 As5 178.20(10) 5_656 5_666
As5 Ca4 As5 83.70(10) 5_656 5_666
Zn4 Ca4 Zn6B 137.43(15) . .
As9B Ca4 Zn6B 70.63(14) . .
Zn6A Ca4 Zn6B 14.88(10) . .
As3 Ca4 Zn6B 104.13(12) . .
As9A Ca4 Zn6B 82.37(14) . .
As8 Ca4 Zn6B 135.04(6) 5_666 .
As8 Ca4 Zn6B 135.04(6) 5_656 .
As5 Ca4 Zn6B 43.41(5) 5_656 .
As5 Ca4 Zn6B 43.41(5) 5_666 .
Zn4 Ca4 Zn2 91.17(11) . 5_666
As9B Ca4 Zn2 138.18(8) . 5_666
Zn6A Ca4 Zn2 131.69(10) . 5_666
As3 Ca4 Zn2 44.36(5) . 5_666
As9A Ca4 Zn2 132.00(9) . 5_666
As8 Ca4 Zn2 46.19(6) 5_666 5_666
As8 Ca4 Zn2 97.53(10) 5_656 5_666
As5 Ca4 Zn2 133.00(11) 5_656 5_666
As5 Ca4 Zn2 83.43(6) 5_666 5_666
Zn6B Ca4 Zn2 121.84(9) . 5_666
Zn4 Ca4 Zn2 91.17(11) . 5_656
As9B Ca4 Zn2 138.18(8) . 5_656
Zn6A Ca4 Zn2 131.69(9) . 5_656
As3 Ca4 Zn2 44.36(5) . 5_656
As9A Ca4 Zn2 132.00(9) . 5_656
As8 Ca4 Zn2 97.53(10) 5_666 5_656
As8 Ca4 Zn2 46.19(6) 5_656 5_656
As5 Ca4 Zn2 83.43(6) 5_656 5_656
As5 Ca4 Zn2 133.00(11) 5_666 5_656
Zn6B Ca4 Zn2 121.84(9) . 5_656
Zn2 Ca4 Zn2 73.30(8) 5_666 5_656
As7 Ca5 As7 88.86(9) 5_656 5_666
As7 Ca5 As1 86.19(8) 5_656 .
As7 Ca5 As1 86.19(8) 5_666 .
As7 Ca5 As3 177.09(11) 5_656 5_666
As7 Ca5 As3 92.71(3) 5_666 5_666
As1 Ca5 As3 96.35(8) . 5_666
As7 Ca5 As3 92.71(3) 5_656 5_656
As7 Ca5 As3 177.09(11) 5_666 5_656
As1 Ca5 As3 96.35(8) . 5_656
As3 Ca5 As3 85.61(9) 5_666 5_656
As7 Ca5 As2 81.61(7) 5_656 .
As7 Ca5 As2 81.61(7) 5_666 .
As1 Ca5 As2 162.87(11) . .
As3 Ca5 As2 96.19(8) 5_666 .
As3 Ca5 As2 96.19(8) 5_656 .
As7 Ca5 Zn3 42.55(8) 5_656 5_656
As7 Ca5 Zn3 100.26(11) 5_666 5_656
As1 Ca5 Zn3 127.52(9) . 5_656
As3 Ca5 Zn3 134.65(12) 5_666 5_656
As3 Ca5 Zn3 79.33(7) 5_656 5_656
As2 Ca5 Zn3 44.40(6) . 5_656
As7 Ca5 Zn3 100.26(11) 5_656 5_666
As7 Ca5 Zn3 42.55(8) 5_666 5_666
As1 Ca5 Zn3 127.52(9) . 5_666
As3 Ca5 Zn3 79.33(7) 5_666 5_666
As3 Ca5 Zn3 134.65(12) 5_656 5_666
As2 Ca5 Zn3 44.40(6) . 5_666
Zn3 Ca5 Zn3 81.58(12) 5_656 5_666
As7 Ca5 Zn5 98.24(10) 5_656 5_666
As7 Ca5 Zn5 43.74(7) 5_666 5_666
As1 Ca5 Zn5 44.93(6) . 5_666
As3 Ca5 Zn5 84.58(7) 5_666 5_666
As3 Ca5 Zn5 138.24(12) 5_656 5_666
As2 Ca5 Zn5 125.18(9) . 5_666
Zn3 Ca5 Zn5 132.98(13) 5_656 5_666
Zn3 Ca5 Zn5 82.74(8) 5_666 5_666
As7 Ca5 Zn5 43.74(7) 5_656 5_656
As7 Ca5 Zn5 98.24(10) 5_666 5_656
As1 Ca5 Zn5 44.93(6) . 5_656
As3 Ca5 Zn5 138.24(12) 5_666 5_656
As3 Ca5 Zn5 84.58(7) 5_656 5_656
As2 Ca5 Zn5 125.18(9) . 5_656
Zn3 Ca5 Zn5 82.74(8) 5_656 5_656
Zn3 Ca5 Zn5 132.98(13) 5_666 5_656
Zn5 Ca5 Zn5 76.40(10) 5_666 5_656
As7 Ca5 Zn2 132.79(6) 5_656 .
As7 Ca5 Zn2 132.79(6) 5_666 .
As1 Ca5 Zn2 113.30(10) . .
As3 Ca5 Zn2 44.78(5) 5_666 .
As3 Ca5 Zn2 44.78(5) 5_656 .
As2 Ca5 Zn2 83.83(8) . .
Zn3 Ca5 Zn2 99.92(10) 5_656 .
Zn3 Ca5 Zn2 99.92(10) 5_666 .
Zn5 Ca5 Zn2 126.39(9) 5_666 .
Zn5 Ca5 Zn2 126.39(9) 5_656 .
As7 Ca5 Ca1 49.05(8) 5_656 .
As7 Ca5 Ca1 57.56(9) 5_666 .
As1 Ca5 Ca1 51.70(8) . .
As3 Ca5 Ca1 133.80(9) 5_666 .
As3 Ca5 Ca1 125.21(9) 5_656 .
As2 Ca5 Ca1 111.25(11) . .
Zn3 Ca5 Ca1 88.34(11) 5_656 .
Zn3 Ca5 Ca1 94.71(12) 5_666 .
Zn5 Ca5 Ca1 49.28(9) 5_666 .
Zn5 Ca5 Ca1 40.76(9) 5_656 .
Zn2 Ca5 Ca1 164.09(11) . .
Zn3 Ca6 As2 48.97(6) 6_557 2_565
Zn3 Ca6 As2 48.97(6) 6_557 2
As2 Ca6 As2 89.40(10) 2_565 2
Zn3 Ca6 As6 133.14(6) 6_557 5_656
As2 Ca6 As6 176.06(14) 2_565 5_656
As2 Ca6 As6 90.83(3) 2 5_656
Zn3 Ca6 As6 133.14(6) 6_557 5_666
As2 Ca6 As6 90.83(3) 2_565 5_666
As2 Ca6 As6 176.06(14) 2 5_666
As6 Ca6 As6 88.67(10) 5_656 5_666
Zn3 Ca6 As4 77.35(12) 6_557 .
As2 Ca6 As4 97.02(9) 2_565 .
As2 Ca6 As4 97.02(9) 2 .
As6 Ca6 As4 86.86(8) 5_656 .
As6 Ca6 As4 86.86(8) 5_666 .
Zn3 Ca6 As4 107.27(13) 6_557 6_557
As2 Ca6 As4 86.25(8) 2_565 6_557
As2 Ca6 As4 86.25(8) 2 6_557
As6 Ca6 As4 89.84(8) 5_656 6_557
As6 Ca6 As4 89.84(8) 5_666 6_557
As4 Ca6 As4 175.38(12) . 6_557
Zn3 Ca6 Ca3 160.45(15) 6_557 .
As2 Ca6 Ca3 121.83(8) 2_565 .
As2 Ca6 Ca3 121.83(8) 2 .
As6 Ca6 Ca3 54.95(6) 5_656 .
As6 Ca6 Ca3 54.95(6) 5_666 .
As4 Ca6 Ca3 122.20(12) . .
As4 Ca6 Ca3 53.18(8) 6_557 .
Zn3 Ca6 Zn1 84.29(10) 6_557 2
As2 Ca6 Zn1 97.32(9) 2_565 2
As2 Ca6 Zn1 45.84(5) 2 2
As6 Ca6 Zn1 80.05(6) 5_656 2
As6 Ca6 Zn1 130.24(11) 5_666 2
As4 Ca6 Zn1 139.73(6) . 2
As4 Ca6 Zn1 42.39(5) 6_557 2
Ca3 Ca6 Zn1 79.90(8) . 2
Zn3 Ca6 Zn1 84.29(10) 6_557 2_565
As2 Ca6 Zn1 45.84(5) 2_565 2_565
As2 Ca6 Zn1 97.32(9) 2 2_565
As6 Ca6 Zn1 130.24(11) 5_656 2_565
As6 Ca6 Zn1 80.05(6) 5_666 2_565
As4 Ca6 Zn1 139.73(6) . 2_565
As4 Ca6 Zn1 42.39(4) 6_557 2_565
Ca3 Ca6 Zn1 79.90(8) . 2_565
Zn1 Ca6 Zn1 71.72(7) 2 2_565
Zn3 Ca6 Zn1 100.13(11) 6_557 5_666
As2 Ca6 Zn1 85.58(6) 2_565 5_666
As2 Ca6 Zn1 137.81(12) 2 5_666
As6 Ca6 Zn1 96.87(9) 5_656 5_666
As6 Ca6 Zn1 46.12(5) 5_666 5_666
As4 Ca6 Zn1 42.56(5) . 5_666
As4 Ca6 Zn1 134.94(7) 6_557 5_666
Ca3 Ca6 Zn1 95.75(9) . 5_666
Zn1 Ca6 Zn1 175.58(10) 2 5_666
Zn1 Ca6 Zn1 108.408(15) 2_565 5_666
Zn3 Ca6 Zn1 100.13(11) 6_557 5_656
As2 Ca6 Zn1 137.81(12) 2_565 5_656
As2 Ca6 Zn1 85.58(5) 2 5_656
As6 Ca6 Zn1 46.12(5) 5_656 5_656
As6 Ca6 Zn1 96.87(9) 5_666 5_656
As4 Ca6 Zn1 42.56(5) . 5_656
As4 Ca6 Zn1 134.94(7) 6_557 5_656
Ca3 Ca6 Zn1 95.75(9) . 5_656
Zn1 Ca6 Zn1 108.408(16) 2 5_656
Zn1 Ca6 Zn1 175.58(10) 2_565 5_656
Zn1 Ca6 Zn1 71.11(7) 5_666 5_656
Zn3 Ca7 As6 133.47(5) . 5_656
Zn3 Ca7 As6 133.47(5) . 5_666
As6 Ca7 As6 92.54(10) 5_656 5_666
Zn3 Ca7 As3 88.96(13) . .
As6 Ca7 As3 94.55(8) 5_656 .
As6 Ca7 As3 94.55(8) 5_666 .
Zn3 Ca7 As2 49.36(6) . 5_666
As6 Ca7 As2 160.42(12) 5_656 5_666
As6 Ca7 As2 85.28(4) 5_666 5_666
As3 Ca7 As2 105.01(9) . 5_666
Zn3 Ca7 As2 49.36(6) . 5_656
As6 Ca7 As2 85.28(4) 5_656 5_656
As6 Ca7 As2 160.42(12) 5_666 5_656
As3 Ca7 As2 105.01(9) . 5_656
As2 Ca7 As2 90.28(10) 5_666 5_656
Zn3 Ca7 Zn1 95.21(11) . 5_666
As6 Ca7 Zn1 112.64(11) 5_656 5_666
As6 Ca7 Zn1 52.67(5) 5_666 5_666
As3 Ca7 Zn1 136.35(5) . 5_666
As2 Ca7 Zn1 51.48(5) 5_666 5_666
As2 Ca7 Zn1 110.47(10) 5_656 5_666
Zn3 Ca7 Zn1 95.21(11) . 5_656
As6 Ca7 Zn1 52.67(5) 5_656 5_656
As6 Ca7 Zn1 112.64(11) 5_666 5_656
As3 Ca7 Zn1 136.35(5) . 5_656
As2 Ca7 Zn1 110.47(10) 5_666 5_656
As2 Ca7 Zn1 51.48(5) 5_656 5_656
Zn1 Ca7 Zn1 86.62(9) 5_666 5_656
Zn3 Ca7 Zn2 110.71(11) . 5_656
As6 Ca7 Zn2 49.62(5) 5_656 5_656
As6 Ca7 Zn2 104.74(10) 5_666 5_656
As3 Ca7 Zn2 46.37(5) . 5_656
As2 Ca7 Zn2 149.49(12) 5_666 5_656
As2 Ca7 Zn2 88.65(5) 5_656 5_656
Zn1 Ca7 Zn2 154.04(12) 5_666 5_656
Zn1 Ca7 Zn2 92.44(5) 5_656 5_656
Zn3 Ca7 Zn2 110.71(11) . 5_666
As6 Ca7 Zn2 104.74(10) 5_656 5_666
As6 Ca7 Zn2 49.62(5) 5_666 5_666
As3 Ca7 Zn2 46.37(5) . 5_666
As2 Ca7 Zn2 88.65(5) 5_666 5_666
As2 Ca7 Zn2 149.49(12) 5_656 5_666
Zn1 Ca7 Zn2 92.44(5) 5_666 5_666
Zn1 Ca7 Zn2 154.04(12) 5_656 5_666
Zn2 Ca7 Zn2 77.26(8) 5_656 5_666
Zn3 Ca7 As4 98.95(12) . .
As6 Ca7 As4 80.03(8) 5_656 .
As6 Ca7 As4 80.03(8) 5_666 .
As3 Ca7 As4 172.09(13) . .
As2 Ca7 As4 80.43(7) 5_666 .
As2 Ca7 As4 80.43(7) 5_656 .
Zn1 Ca7 As4 43.34(5) 5_666 .
Zn1 Ca7 As4 43.34(5) 5_656 .
Zn2 Ca7 As4 129.28(7) 5_656 .
Zn2 Ca7 As4 129.28(7) 5_666 .
Zn3 Ca7 Ca3 157.40(15) . .
As6 Ca7 Ca3 52.45(6) 5_656 .
As6 Ca7 Ca3 52.45(6) 5_666 .
As3 Ca7 Ca3 68.44(9) . .
As2 Ca7 Ca3 134.86(5) 5_666 .
As2 Ca7 Ca3 134.86(5) 5_656 .
Zn1 Ca7 Ca3 101.17(9) 5_666 .
Zn1 Ca7 Ca3 101.17(9) 5_656 .
Zn2 Ca7 Ca3 53.55(6) 5_656 .
Zn2 Ca7 Ca3 53.55(6) 5_666 .
As4 Ca7 Ca3 103.65(10) . .
Zn6B Ca8 Zn6B 92.91(15) 5_656 5_666
Zn6B Ca8 As1 112.53(13) 5_656 5_666
Zn6B Ca8 As1 50.03(9) 5_666 5_666
Zn6B Ca8 As1 50.03(8) 5_656 5_656
Zn6B Ca8 As1 112.53(13) 5_666 5_656
As1 Ca8 As1 90.06(10) 5_666 5_656
Zn6B Ca8 Zn6B 72.99(13) 5_656 .
Zn6B Ca8 Zn6B 72.99(13) 5_666 .
As1 Ca8 Zn6B 122.47(10) 5_666 .
As1 Ca8 Zn6B 122.47(10) 5_656 .
Zn6B Ca8 As3 133.49(7) 5_656 .
Zn6B Ca8 As3 133.49(7) 5_666 .
As1 Ca8 As3 99.08(10) 5_666 .
As1 Ca8 As3 99.08(10) 5_656 .
Zn6B Ca8 As3 117.67(14) . .
Zn6B Ca8 As5 59.35(9) 5_656 5_656
Zn6B Ca8 As5 119.27(14) 5_666 5_656
As1 Ca8 As5 168.02(14) 5_666 5_656
As1 Ca8 As5 90.19(4) 5_656 5_656
Zn6B Ca8 As5 48.52(7) . 5_656
As3 Ca8 As5 92.70(9) . 5_656
Zn6B Ca8 As5 119.27(14) 5_656 5_666
Zn6B Ca8 As5 59.35(9) 5_666 5_666
As1 Ca8 As5 90.19(4) 5_666 5_666
As1 Ca8 As5 168.02(14) 5_656 5_666
Zn6B Ca8 As5 48.52(7) . 5_666
As3 Ca8 As5 92.70(9) . 5_666
As5 Ca8 As5 87.10(10) 5_656 5_666
Zn6B Ca8 Zn5 89.29(12) 5_656 .
Zn6B Ca8 Zn5 89.29(12) 5_666 .
As1 Ca8 Zn5 46.81(6) 5_666 .
As1 Ca8 Zn5 46.81(6) 5_656 .
Zn6B Ca8 Zn5 153.84(16) . .
As3 Ca8 Zn5 88.49(12) . .
As5 Ca8 Zn5 136.40(5) 5_656 .
As5 Ca8 Zn5 136.40(5) 5_666 .
Zn6B Ca8 As5 47.08(7) 5_656 .
Zn6B Ca8 As5 47.08(7) 5_666 .
As1 Ca8 As5 85.28(9) 5_666 .
As1 Ca8 As5 85.28(8) 5_656 .
Zn6B Ca8 As5 56.11(11) . .
As3 Ca8 As5 173.78(14) . .
As5 Ca8 As5 82.81(9) 5_656 .
As5 Ca8 As5 82.81(9) 5_666 .
Zn5 Ca8 As5 97.73(12) . .
Zn6B Ca8 Zn6A 15.04(9) 5_656 5_656
Zn6B Ca8 Zn6A 85.01(12) 5_666 5_656
As1 Ca8 Zn6A 97.74(11) 5_666 5_656
As1 Ca8 Zn6A 43.69(8) 5_656 5_656
Zn6B Ca8 Zn6A 82.85(13) . 5_656
As3 Ca8 Zn6A 138.90(8) . 5_656
As5 Ca8 Zn6A 74.39(8) 5_656 5_656
As5 Ca8 Zn6A 124.48(13) 5_666 5_656
Zn5 Ca8 Zn6A 76.43(11) . 5_656
As5 Ca8 Zn6A 43.82(7) . 5_656
Zn6B Ca8 Zn6A 85.01(12) 5_656 5_666
Zn6B Ca8 Zn6A 15.04(8) 5_666 5_666
As1 Ca8 Zn6A 43.69(8) 5_666 5_666
As1 Ca8 Zn6A 97.74(11) 5_656 5_666
Zn6B Ca8 Zn6A 82.85(13) . 5_666
As3 Ca8 Zn6A 138.90(8) . 5_666
As5 Ca8 Zn6A 124.48(13) 5_656 5_666
As5 Ca8 Zn6A 74.39(8) 5_666 5_666
Zn5 Ca8 Zn6A 76.43(11) . 5_666
As5 Ca8 Zn6A 43.82(7) . 5_666
Zn6A Ca8 Zn6A 74.63(11) 5_656 5_666
As9B Ca9 As9B 103.9(2) 5_656 5_666
As9B Ca9 Zn6A 59.21(13) 5_656 5_656
As9B Ca9 Zn6A 131.09(19) 5_666 5_656
As9B Ca9 Zn6A 131.09(19) 5_656 5_666
As9B Ca9 Zn6A 59.21(13) 5_666 5_666
Zn6A Ca9 Zn6A 95.84(17) 5_656 5_666
As9B Ca9 Zn5 126.36(11) 5_656 .
As9B Ca9 Zn5 126.36(11) 5_666 .
Zn6A Ca9 Zn5 93.81(13) 5_656 .
Zn6A Ca9 Zn5 93.81(13) 5_666 .
As9B Ca9 As9A 101.18(15) 5_656 1_655
As9B Ca9 As9A 101.18(15) 5_666 1_655
Zn6A Ca9 As9A 126.09(11) 5_656 1_655
Zn6A Ca9 As9A 126.09(11) 5_666 1_655
Zn5 Ca9 As9A 55.83(14) . 1_655
As9B Ca9 As9B 94.09(15) 5_656 1_655
As9B Ca9 As9B 94.09(15) 5_666 1_655
Zn6A Ca9 As9B 129.91(10) 5_656 1_655
Zn6A Ca9 As9B 129.91(10) 5_666 1_655
Zn5 Ca9 As9B 67.51(14) . 1_655
As9A Ca9 As9B 11.68(8) 1_655 1_655
As9B Ca9 As9A 9.55(8) 5_656 5_656
As9B Ca9 As9A 95.45(17) 5_666 5_656
Zn6A Ca9 As9A 68.12(12) 5_656 5_656
Zn6A Ca9 As9A 130.26(18) 5_666 5_656
Zn5 Ca9 As9A 132.40(10) . 5_656
As9A Ca9 As9A 98.82(14) 1_655 5_656
As9B Ca9 As9A 90.35(12) 1_655 5_656
As9B Ca9 As9A 95.45(17) 5_656 5_666
As9B Ca9 As9A 9.55(8) 5_666 5_666
Zn6A Ca9 As9A 130.26(18) 5_656 5_666
Zn6A Ca9 As9A 68.12(12) 5_666 5_666
Zn5 Ca9 As9A 132.40(10) . 5_666
As9A Ca9 As9A 98.82(14) 1_655 5_666
As9B Ca9 As9A 90.35(12) 1_655 5_666
As9A Ca9 As9A 86.69(15) 5_656 5_666
As9B Ca9 As5 88.34(14) 5_656 .
As9B Ca9 As5 88.34(14) 5_666 .
Zn6A Ca9 As5 49.20(9) 5_656 .
Zn6A Ca9 As5 49.20(9) 5_666 .
Zn5 Ca9 As5 108.54(14) . .
As9A Ca9 As5 164.36(17) 1_655 .
As9B Ca9 As5 176.05(16) 1_655 .
As9A Ca9 As5 92.52(13) 5_656 .
As9A Ca9 As5 92.52(13) 5_666 .
As9B Ca9 As1 166.96(16) 5_656 5_666
As9B Ca9 As1 86.06(9) 5_666 5_666
Zn6A Ca9 As1 107.90(14) 5_656 5_666
Zn6A Ca9 As1 47.50(9) 5_666 5_666
Zn5 Ca9 As1 48.20(7) . 5_666
As9A Ca9 As1 84.78(11) 1_655 5_666
As9B Ca9 As1 93.53(12) 1_655 5_666
As9A Ca9 As1 175.73(16) 5_656 5_666
As9A Ca9 As1 95.06(6) 5_666 5_666
As5 Ca9 As1 83.52(9) . 5_666
As9B Ca9 As1 86.06(9) 5_656 5_656
As9B Ca9 As1 166.96(16) 5_666 5_656
Zn6A Ca9 As1 47.50(9) 5_656 5_656
Zn6A Ca9 As1 107.90(14) 5_666 5_656
Zn5 Ca9 As1 48.20(7) . 5_656
As9A Ca9 As1 84.78(11) 1_655 5_656
As9B Ca9 As1 93.53(12) 1_655 5_656
As9A Ca9 As1 95.06(6) 5_656 5_656
As9A Ca9 As1 175.73(16) 5_666 5_656
As5 Ca9 As1 83.52(9) . 5_656
As1 Ca9 As1 82.93(10) 5_666 5_656
As4 Zn1 As4 116.07(9) 5_656 5_666
As4 Zn1 As2 111.79(6) 5_656 .
As4 Zn1 As2 111.79(6) 5_666 .
As4 Zn1 As6 108.81(6) 5_656 .
As4 Zn1 As6 108.81(6) 5_666 .
As2 Zn1 As6 97.97(8) . .
As4 Zn1 Ca7 164.97(8) 5_656 5_666
As4 Zn1 Ca7 78.58(5) 5_666 5_666
As2 Zn1 Ca7 62.31(7) . 5_666
As6 Zn1 Ca7 60.65(7) . 5_666
As4 Zn1 Ca7 78.58(5) 5_656 5_656
As4 Zn1 Ca7 164.97(8) 5_666 5_656
As2 Zn1 Ca7 62.31(7) . 5_656
As6 Zn1 Ca7 60.65(7) . 5_656
Ca7 Zn1 Ca7 86.62(9) 5_666 5_656
As4 Zn1 Ca2 59.54(5) 5_656 6_656
As4 Zn1 Ca2 59.54(5) 5_666 6_656
As2 Zn1 Ca2 151.26(9) . 6_656
As6 Zn1 Ca2 110.77(9) . 6_656
Ca7 Zn1 Ca2 132.59(6) 5_666 6_656
Ca7 Zn1 Ca2 132.59(6) 5_656 6_656
As4 Zn1 Ca6 60.06(6) 5_656 2_554
As4 Zn1 Ca6 119.66(8) 5_666 2_554
As2 Zn1 Ca6 54.90(6) . 2_554
As6 Zn1 Ca6 130.19(6) . 2_554
Ca7 Zn1 Ca6 117.03(9) 5_666 2_554
Ca7 Zn1 Ca6 69.56(7) 5_656 2_554
Ca2 Zn1 Ca6 103.27(8) 6_656 2_554
As4 Zn1 Ca6 119.66(8) 5_656 2_564
As4 Zn1 Ca6 60.06(6) 5_666 2_564
As2 Zn1 Ca6 54.90(6) . 2_564
As6 Zn1 Ca6 130.19(6) . 2_564
Ca7 Zn1 Ca6 69.56(7) 5_666 2_564
Ca7 Zn1 Ca6 117.03(9) 5_656 2_564
Ca2 Zn1 Ca6 103.27(8) 6_656 2_564
Ca6 Zn1 Ca6 71.72(7) 2_554 2_564
As4 Zn1 Ca6 115.99(8) 5_656 5_666
As4 Zn1 Ca6 56.74(6) 5_666 5_666
As2 Zn1 Ca6 130.41(7) . 5_666
As6 Zn1 Ca6 54.79(6) . 5_666
Ca7 Zn1 Ca6 68.11(8) 5_666 5_666
Ca7 Zn1 Ca6 115.14(9) 5_656 5_666
Ca2 Zn1 Ca6 70.60(7) 6_656 5_666
Ca6 Zn1 Ca6 173.79(6) 2_554 5_666
Ca6 Zn1 Ca6 108.234(15) 2_564 5_666
As4 Zn1 Ca6 56.74(6) 5_656 5_656
As4 Zn1 Ca6 115.99(8) 5_666 5_656
As2 Zn1 Ca6 130.41(7) . 5_656
As6 Zn1 Ca6 54.79(6) . 5_656
Ca7 Zn1 Ca6 115.14(9) 5_666 5_656
Ca7 Zn1 Ca6 68.11(8) 5_656 5_656
Ca2 Zn1 Ca6 70.60(7) 6_656 5_656
Ca6 Zn1 Ca6 108.234(15) 2_554 5_656
Ca6 Zn1 Ca6 173.79(6) 2_564 5_656
Ca6 Zn1 Ca6 71.11(7) 5_666 5_656
As3 Zn2 As3 113.70(9) 5_656 5_666
As3 Zn2 As8 111.34(6) 5_656 .
As3 Zn2 As8 111.34(6) 5_666 .
As3 Zn2 As6 111.79(6) 5_656 .
As3 Zn2 As6 111.79(6) 5_666 .
As8 Zn2 As6 95.53(8) . .
As3 Zn2 Ca3 164.80(7) 5_656 5_666
As3 Zn2 Ca3 81.47(5) 5_666 5_666
As8 Zn2 Ca3 59.35(7) . 5_666
As6 Zn2 Ca3 60.38(7) . 5_666
As3 Zn2 Ca3 81.47(5) 5_656 5_656
As3 Zn2 Ca3 164.80(7) 5_666 5_656
As8 Zn2 Ca3 59.35(7) . 5_656
As6 Zn2 Ca3 60.38(7) . 5_656
Ca3 Zn2 Ca3 83.35(9) 5_666 5_656
As3 Zn2 Ca7 57.55(6) 5_656 5_656
As3 Zn2 Ca7 120.59(8) 5_666 5_656
As8 Zn2 Ca7 126.85(7) . 5_656
As6 Zn2 Ca7 56.21(6) . 5_656
Ca3 Zn2 Ca7 116.59(9) 5_666 5_656
Ca3 Zn2 Ca7 67.50(8) 5_656 5_656
As3 Zn2 Ca7 120.59(8) 5_656 5_666
As3 Zn2 Ca7 57.55(6) 5_666 5_666
As8 Zn2 Ca7 126.85(7) . 5_666
As6 Zn2 Ca7 56.21(6) . 5_666
Ca3 Zn2 Ca7 67.50(8) 5_666 5_666
Ca3 Zn2 Ca7 116.59(9) 5_656 5_666
Ca7 Zn2 Ca7 77.26(8) 5_656 5_666
As3 Zn2 Ca5 60.20(5) 5_656 .
As3 Zn2 Ca5 60.20(5) 5_666 .
As8 Zn2 Ca5 156.39(9) . .
As6 Zn2 Ca5 108.09(8) . .
Ca3 Zn2 Ca5 133.30(6) 5_666 .
Ca3 Zn2 Ca5 133.30(6) 5_656 .
Ca7 Zn2 Ca5 69.58(7) 5_656 .
Ca7 Zn2 Ca5 69.58(7) 5_666 .
As3 Zn2 Ca4 117.01(9) 5_656 5_666
As3 Zn2 Ca4 56.95(6) 5_666 5_666
As8 Zn2 Ca4 57.30(6) . 5_666
As6 Zn2 Ca4 129.98(7) . 5_666
Ca3 Zn2 Ca4 69.60(7) 5_666 5_666
Ca3 Zn2 Ca4 116.44(9) 5_656 5_666
Ca7 Zn2 Ca4 173.50(10) 5_656 5_666
Ca7 Zn2 Ca4 104.38(5) 5_666 5_666
Ca5 Zn2 Ca4 104.91(8) . 5_666
As3 Zn2 Ca4 56.95(6) 5_656 5_656
As3 Zn2 Ca4 117.01(9) 5_666 5_656
As8 Zn2 Ca4 57.30(6) . 5_656
As6 Zn2 Ca4 129.98(7) . 5_656
Ca3 Zn2 Ca4 116.44(9) 5_666 5_656
Ca3 Zn2 Ca4 69.60(7) 5_656 5_656
Ca7 Zn2 Ca4 104.38(5) 5_656 5_656
Ca7 Zn2 Ca4 173.50(10) 5_666 5_656
Ca5 Zn2 Ca4 104.91(8) . 5_656
Ca4 Zn2 Ca4 73.30(8) 5_666 5_656
As7 Zn3 As2 119.45(9) . 5_656
As7 Zn3 As2 119.45(9) . 5_666
As2 Zn3 As2 120.55(17) 5_656 5_666
As7 Zn3 Ca7 130.59(18) . .
As2 Zn3 Ca7 68.39(9) 5_656 .
As2 Zn3 Ca7 68.39(9) 5_666 .
As7 Zn3 Ca6 144.64(19) . 6_657
As2 Zn3 Ca6 68.64(10) 5_656 6_657
As2 Zn3 Ca6 68.64(10) 5_666 6_657
Ca7 Zn3 Ca6 84.77(14) . 6_657
As7 Zn3 Ca2 67.21(10) . 5_666
As2 Zn3 Ca2 146.28(17) 5_656 5_666
As2 Zn3 Ca2 68.07(7) 5_666 5_666
Ca7 Zn3 Ca2 135.48(7) . 5_666
Ca6 Zn3 Ca2 87.98(12) 6_657 5_666
As7 Zn3 Ca2 67.21(10) . 5_656
As2 Zn3 Ca2 68.07(7) 5_656 5_656
As2 Zn3 Ca2 146.28(17) 5_666 5_656
Ca7 Zn3 Ca2 135.48(7) . 5_656
Ca6 Zn3 Ca2 87.98(12) 6_657 5_656
Ca2 Zn3 Ca2 87.88(13) 5_666 5_656
As7 Zn3 Ca5 63.66(9) . 5_656
As2 Zn3 Ca5 67.16(7) 5_656 5_656
As2 Zn3 Ca5 138.29(16) 5_666 5_656
Ca7 Zn3 Ca5 79.80(11) . 5_656
Ca6 Zn3 Ca5 135.80(8) 6_657 5_656
Ca2 Zn3 Ca5 130.82(14) 5_666 5_656
Ca2 Zn3 Ca5 75.35(8) 5_656 5_656
As7 Zn3 Ca5 63.66(9) . 5_666
As2 Zn3 Ca5 138.29(16) 5_656 5_666
As2 Zn3 Ca5 67.16(7) 5_666 5_666
Ca7 Zn3 Ca5 79.80(11) . 5_666
Ca6 Zn3 Ca5 135.80(8) 6_657 5_666
Ca2 Zn3 Ca5 75.35(8) 5_666 5_666
Ca2 Zn3 Ca5 130.82(14) 5_656 5_666
Ca5 Zn3 Ca5 81.58(12) 5_656 5_666
As7 Zn4 Ca1 73.95(14) 1_455 5_556
As7 Zn4 Ca1 73.95(14) 1_455 3_556
Ca1 Zn4 Ca1 93.8(2) 5_556 3_556
As7 Zn4 As8 115.88(10) 1_455 5_666
Ca1 Zn4 As8 160.9(2) 5_556 5_666
Ca1 Zn4 As8 74.58(11) 3_556 5_666
As7 Zn4 As8 115.88(10) 1_455 5_656
Ca1 Zn4 As8 74.58(11) 5_556 5_656
Ca1 Zn4 As8 160.86(19) 3_556 5_656
As8 Zn4 As8 111.94(16) 5_666 5_656
As7 Zn4 As9A 100.12(18) 1_455 .
Ca1 Zn4 As9A 55.51(13) 5_556 .
Ca1 Zn4 As9A 55.51(13) 3_556 .
As8 Zn4 As9A 105.55(12) 5_666 .
As8 Zn4 As9A 105.55(12) 5_656 .
As7 Zn4 Ca4 166.99(19) 1_455 .
Ca1 Zn4 Ca4 97.40(15) 5_556 .
Ca1 Zn4 Ca4 97.40(15) 3_556 .
As8 Zn4 Ca4 69.73(9) 5_666 .
As8 Zn4 Ca4 69.73(9) 5_656 .
As9A Zn4 Ca4 66.86(15) . .
As7 Zn4 Ca1 76.75(12) 1_455 3_546
Ca1 Zn4 Ca1 8.57(12) 5_556 3_546
Ca1 Zn4 Ca1 102.42(19) 3_556 3_546
As8 Zn4 Ca1 164.67(18) 5_666 3_546
As8 Zn4 Ca1 66.33(9) 5_656 3_546
As9A Zn4 Ca1 61.99(11) . 3_546
Ca4 Zn4 Ca1 96.13(13) . 3_546
As7 Zn4 Ca1 76.75(12) 1_455 5_566
Ca1 Zn4 Ca1 102.42(19) 5_556 5_566
Ca1 Zn4 Ca1 8.57(12) 3_556 5_566
As8 Zn4 Ca1 66.33(9) 5_666 5_566
As8 Zn4 Ca1 164.67(18) 5_656 5_566
As9A Zn4 Ca1 61.99(11) . 5_566
Ca4 Zn4 Ca1 96.13(13) . 5_566
Ca1 Zn4 Ca1 111.0(2) 3_546 5_566
As7 Zn4 Ca3 112.38(15) 1_455 .
Ca1 Zn4 Ca3 133.06(12) 5_556 .
Ca1 Zn4 Ca3 133.06(12) 3_556 .
As8 Zn4 Ca3 60.66(9) 5_666 .
As8 Zn4 Ca3 60.66(9) 5_656 .
As9A Zn4 Ca3 147.50(19) . .
Ca4 Zn4 Ca3 80.63(13) . .
Ca1 Zn4 Ca3 124.49(10) 3_546 .
Ca1 Zn4 Ca3 124.49(10) 5_566 .
As7 Zn4 Ca2 57.77(9) 1_455 5_566
Ca1 Zn4 Ca2 131.57(18) 5_556 5_566
Ca1 Zn4 Ca2 77.52(12) 3_556 5_566
As8 Zn4 Ca2 61.69(8) 5_666 5_566
As8 Zn4 Ca2 121.58(14) 5_656 5_566
As9A Zn4 Ca2 132.74(11) . 5_566
Ca4 Zn4 Ca2 130.79(11) . 5_566
Ca1 Zn4 Ca2 132.98(15) 3_546 5_566
Ca1 Zn4 Ca2 71.90(10) 5_566 5_566
Ca3 Zn4 Ca2 69.73(10) . 5_566
As7 Zn4 Ca2 57.77(9) 1_455 5_556
Ca1 Zn4 Ca2 77.52(12) 5_556 5_556
Ca1 Zn4 Ca2 131.57(18) 3_556 5_556
As8 Zn4 Ca2 121.58(14) 5_666 5_556
As8 Zn4 Ca2 61.69(8) 5_656 5_556
As9A Zn4 Ca2 132.74(11) . 5_556
Ca4 Zn4 Ca2 130.79(10) . 5_556
Ca1 Zn4 Ca2 71.90(10) 3_546 5_556
Ca1 Zn4 Ca2 132.98(15) 5_566 5_556
Ca3 Zn4 Ca2 69.73(10) . 5_556
Ca2 Zn4 Ca2 74.05(10) 5_566 5_556
As7 Zn5 As1 114.73(9) . 5_656
As7 Zn5 As1 114.73(9) . 5_666
As1 Zn5 As1 115.92(15) 5_656 5_666
As7 Zn5 Ca1 71.92(13) . 3_656
As1 Zn5 Ca1 159.38(18) 5_656 3_656
As1 Zn5 Ca1 74.88(11) 5_666 3_656
As7 Zn5 Ca1 71.92(13) . 5_656
As1 Zn5 Ca1 74.88(11) 5_656 5_656
As1 Zn5 Ca1 159.38(18) 5_666 5_656
Ca1 Zn5 Ca1 89.8(2) 3_656 5_656
As7 Zn5 As9A 98.73(16) . 1_655
As1 Zn5 As9A 105.00(11) 5_656 1_655
As1 Zn5 As9A 105.00(11) 5_666 1_655
Ca1 Zn5 As9A 54.40(13) 3_656 1_655
Ca1 Zn5 As9A 54.40(13) 5_656 1_655
As7 Zn5 Ca9 162.19(18) . .
As1 Zn5 Ca9 72.63(9) 5_656 .
As1 Zn5 Ca9 72.63(9) 5_666 .
Ca1 Zn5 Ca9 95.78(15) 3_656 .
Ca1 Zn5 Ca9 95.78(15) 5_656 .
As9A Zn5 Ca9 63.46(14) 1_655 .
As7 Zn5 Ca1 74.92(11) . 5_666
As1 Zn5 Ca1 164.81(17) 5_656 5_666
As1 Zn5 Ca1 66.46(9) 5_666 5_666
Ca1 Zn5 Ca1 8.68(12) 3_656 5_666
Ca1 Zn5 Ca1 98.50(17) 5_656 5_666
As9A Zn5 Ca1 60.80(11) 1_655 5_666
Ca9 Zn5 Ca1 94.85(12) . 5_666
As7 Zn5 Ca1 74.92(11) . 3_646
As1 Zn5 Ca1 66.46(9) 5_656 3_646
As1 Zn5 Ca1 164.81(18) 5_666 3_646
Ca1 Zn5 Ca1 98.50(17) 3_656 3_646
Ca1 Zn5 Ca1 8.68(12) 5_656 3_646
As9A Zn5 Ca1 60.80(11) 1_655 3_646
Ca9 Zn5 Ca1 94.85(12) . 3_646
Ca1 Zn5 Ca1 107.2(2) 5_666 3_646
As7 Zn5 Ca8 118.64(15) . .
As1 Zn5 Ca8 60.87(8) 5_656 .
As1 Zn5 Ca8 60.87(8) 5_666 .
Ca1 Zn5 Ca8 135.03(11) 3_656 .
Ca1 Zn5 Ca8 135.03(11) 5_656 .
As9A Zn5 Ca8 142.62(17) 1_655 .
Ca9 Zn5 Ca8 79.16(13) . .
Ca1 Zn5 Ca8 126.37(10) 5_666 .
Ca1 Zn5 Ca8 126.37(10) 3_646 .
As7 Zn5 Ca5 59.36(9) . 5_666
As1 Zn5 Ca5 122.84(14) 5_656 5_666
As1 Zn5 Ca5 59.59(8) 5_666 5_666
Ca1 Zn5 Ca5 77.65(11) 3_656 5_666
Ca1 Zn5 Ca5 131.24(16) 5_656 5_666
As9A Zn5 Ca5 131.96(10) 1_655 5_666
Ca9 Zn5 Ca5 131.92(10) . 5_666
Ca1 Zn5 Ca5 71.88(9) 5_666 5_666
Ca1 Zn5 Ca5 133.18(14) 3_646 5_666
Ca8 Zn5 Ca5 73.70(10) . 5_666
As7 Zn5 Ca5 59.36(9) . 5_656
As1 Zn5 Ca5 59.59(8) 5_656 5_656
As1 Zn5 Ca5 122.84(14) 5_666 5_656
Ca1 Zn5 Ca5 131.24(16) 3_656 5_656
Ca1 Zn5 Ca5 77.65(11) 5_656 5_656
As9A Zn5 Ca5 131.96(10) 1_655 5_656
Ca9 Zn5 Ca5 131.92(10) . 5_656
Ca1 Zn5 Ca5 133.18(14) 5_666 5_656
Ca1 Zn5 Ca5 71.88(9) 3_646 5_656
Ca8 Zn5 Ca5 73.70(10) . 5_656
Ca5 Zn5 Ca5 76.40(10) 5_666 5_656
Zn6B Zn6A As1 80.7(3) . .
Zn6B Zn6A As5 76.43(19) . 5_666
As1 Zn6A As5 116.95(11) . 5_666
Zn6B Zn6A As5 76.43(19) . 5_656
As1 Zn6A As5 116.95(11) . 5_656
As5 Zn6A As5 113.21(17) 5_666 5_656
Zn6B Zn6A As9B 177.7(4) . .
As1 Zn6A As9B 101.63(19) . .
As5 Zn6A As9B 102.39(14) 5_666 .
As5 Zn6A As9B 102.39(14) 5_656 .
Zn6B Zn6A Ca9 123.7(2) . 5_656
As1 Zn6A Ca9 73.63(12) . 5_656
As5 Zn6A Ca9 159.6(2) 5_666 5_656
As5 Zn6A Ca9 72.42(8) 5_656 5_656
As9B Zn6A Ca9 57.40(11) . 5_656
Zn6B Zn6A Ca9 123.7(2) . 5_666
As1 Zn6A Ca9 73.63(12) . 5_666
As5 Zn6A Ca9 72.42(8) 5_666 5_666
As5 Zn6A Ca9 159.6(2) 5_656 5_666
As9B Zn6A Ca9 57.40(11) . 5_666
Ca9 Zn6A Ca9 95.84(17) 5_656 5_666
Zn6B Zn6A Ca4 116.6(4) . .
As1 Zn6A Ca4 162.8(2) . .
As5 Zn6A Ca4 70.09(10) 5_666 .
As5 Zn6A Ca4 70.09(10) 5_656 .
As9B Zn6A Ca4 61.15(15) . .
Ca9 Zn6A Ca4 95.12(14) 5_656 .
Ca9 Zn6A Ca4 95.12(14) 5_666 .
Zn6B Zn6A Ca8 48.45(19) . 5_656
As1 Zn6A Ca8 57.27(10) . 5_656
As5 Zn6A Ca8 124.68(17) 5_666 5_656
As5 Zn6A Ca8 63.69(9) 5_656 5_656
As9B Zn6A Ca8 132.87(12) . 5_656
Ca9 Zn6A Ca8 75.66(10) 5_656 5_656
Ca9 Zn6A Ca8 130.70(16) 5_666 5_656
Ca4 Zn6A Ca8 133.56(10) . 5_656
Zn6B Zn6A Ca8 48.45(19) . 5_666
As1 Zn6A Ca8 57.27(10) . 5_666
As5 Zn6A Ca8 63.69(9) 5_666 5_666
As5 Zn6A Ca8 124.68(17) 5_656 5_666
As9B Zn6A Ca8 132.87(12) . 5_666
Ca9 Zn6A Ca8 130.70(16) 5_656 5_666
Ca9 Zn6A Ca8 75.66(10) 5_666 5_666
Ca4 Zn6A Ca8 133.56(10) . 5_666
Ca8 Zn6A Ca8 74.63(11) 5_656 5_666
Zn6B Zn6A Ca8 50.5(3) . .
As1 Zn6A Ca8 131.13(18) . .
As5 Zn6A Ca8 57.76(9) 5_666 .
As5 Zn6A Ca8 57.76(9) 5_656 .
As9B Zn6A Ca8 127.23(18) . .
Ca9 Zn6A Ca8 130.04(9) 5_656 .
Ca9 Zn6A Ca8 130.04(9) 5_666 .
Ca4 Zn6A Ca8 66.08(11) . .
Ca8 Zn6A Ca8 85.21(12) 5_656 .
Ca8 Zn6A Ca8 85.21(12) 5_666 .
Zn6A Zn6B As5 80.38(19) . 5_666
Zn6A Zn6B As5 80.38(19) . 5_656
As5 Zn6B As5 115.73(16) 5_666 5_656
Zn6A Zn6B As1 75.8(3) . .
As5 Zn6B As1 116.65(10) 5_666 .
As5 Zn6B As1 116.65(10) 5_656 .
Zn6A Zn6B Ca8 116.5(2) . 5_656
As5 Zn6B Ca8 162.44(18) 5_666 5_656
As5 Zn6B Ca8 74.09(7) 5_656 5_656
As1 Zn6B Ca8 66.47(10) . 5_656
Zn6A Zn6B Ca8 116.5(2) . 5_666
As5 Zn6B Ca8 74.09(7) 5_666 5_666
As5 Zn6B Ca8 162.44(18) 5_656 5_666
As1 Zn6B Ca8 66.47(10) . 5_666
Ca8 Zn6B Ca8 92.91(15) 5_656 5_666
Zn6A Zn6B As5 178.9(4) . .
As5 Zn6B As5 100.16(11) 5_666 .
As5 Zn6B As5 100.16(11) 5_656 .
As1 Zn6B As5 103.14(14) . .
Ca8 Zn6B As5 62.87(10) 5_656 .
Ca8 Zn6B As5 62.87(10) 5_666 .
Zn6A Zn6B Ca8 114.5(4) . .
As5 Zn6B Ca8 67.03(9) 5_666 .
As5 Zn6B Ca8 67.03(9) 5_656 .
As1 Zn6B Ca8 169.72(19) . .
Ca8 Zn6B Ca8 107.01(13) 5_656 .
Ca8 Zn6B Ca8 107.01(13) 5_666 .
As5 Zn6B Ca8 66.58(11) . .
Zn6A Zn6B Ca9 42.47(15) . 5_656
As5 Zn6B Ca9 122.75(15) 5_666 5_656
As5 Zn6B Ca9 61.40(9) 5_656 5_656
As1 Zn6B Ca9 61.48(10) . 5_656
Ca8 Zn6B Ca9 74.48(9) 5_656 5_656
Ca8 Zn6B Ca9 127.24(15) 5_666 5_656
As5 Zn6B Ca9 137.04(8) . 5_656
Ca8 Zn6B Ca9 125.73(11) . 5_656
Zn6A Zn6B Ca9 42.47(15) . 5_666
As5 Zn6B Ca9 61.40(9) 5_666 5_666
As5 Zn6B Ca9 122.75(15) 5_656 5_666
As1 Zn6B Ca9 61.48(10) . 5_666
Ca8 Zn6B Ca9 127.24(15) 5_656 5_666
Ca8 Zn6B Ca9 74.48(9) 5_666 5_666
As5 Zn6B Ca9 137.04(8) . 5_666
Ca8 Zn6B Ca9 125.73(11) . 5_666
Ca9 Zn6B Ca9 74.04(11) 5_656 5_666
Zn6A Zn6B Ca4 48.6(3) . .
As5 Zn6B Ca4 60.71(9) 5_666 .
As5 Zn6B Ca4 60.71(9) 5_656 .
As1 Zn6B Ca4 124.36(17) . .
Ca8 Zn6B Ca4 133.54(7) 5_656 .
Ca8 Zn6B Ca4 133.54(7) 5_666 .
As5 Zn6B Ca4 132.50(14) . .
Ca8 Zn6B Ca4 65.92(11) . .
Ca9 Zn6B Ca4 74.99(11) 5_656 .
Ca9 Zn6B Ca4 74.99(10) 5_666 .
Zn6A As1 Zn5 115.22(9) . 5_656
Zn6A As1 Zn5 115.22(9) . 5_666
Zn5 As1 Zn5 115.92(15) 5_656 5_666
Zn6A As1 Zn6B 23.55(12) . .
Zn5 As1 Zn6B 121.12(8) 5_656 .
Zn5 As1 Zn6B 121.12(8) 5_666 .
Zn6A As1 Ca8 79.05(11) . 5_666
Zn5 As1 Ca8 153.62(12) 5_656 5_666
Zn5 As1 Ca8 72.33(10) 5_666 5_666
Zn6B As1 Ca8 63.50(10) . 5_666
Zn6A As1 Ca8 79.05(11) . 5_656
Zn5 As1 Ca8 72.33(10) 5_656 5_656
Zn5 As1 Ca8 153.62(12) 5_666 5_656
Zn6B As1 Ca8 63.50(10) . 5_656
Ca8 As1 Ca8 90.06(11) 5_666 5_656
Zn6A As1 Ca5 154.78(14) . .
Zn5 As1 Ca5 75.48(9) 5_656 .
Zn5 As1 Ca5 75.48(9) 5_666 .
Zn6B As1 Ca5 131.23(13) . .
Ca8 As1 Ca5 83.22(9) 5_666 .
Ca8 As1 Ca5 83.22(9) 5_656 .
Zn6A As1 Ca1 128.12(14) . 7_565
Zn5 As1 Ca1 65.16(12) 5_656 7_565
Zn5 As1 Ca1 53.21(11) 5_666 7_565
Zn6B As1 Ca1 151.33(14) . 7_565
Ca8 As1 Ca1 124.98(10) 5_666 7_565
Ca8 As1 Ca1 136.27(11) 5_656 7_565
Ca5 As1 Ca1 76.91(10) . 7_565
Zn6A As1 Ca1 128.12(14) . .
Zn5 As1 Ca1 53.21(11) 5_656 .
Zn5 As1 Ca1 65.16(12) 5_666 .
Zn6B As1 Ca1 151.33(14) . .
Ca8 As1 Ca1 136.27(11) 5_666 .
Ca8 As1 Ca1 124.98(10) 5_656 .
Ca5 As1 Ca1 76.91(10) . .
Ca1 As1 Ca1 12.11(16) 7_565 .
Zn6A As1 Ca9 58.87(10) . 5_666
Zn5 As1 Ca9 127.60(12) 5_656 5_666
Zn5 As1 Ca9 59.17(10) 5_666 5_666
Zn6B As1 Ca9 75.09(10) . 5_666
Ca8 As1 Ca9 78.61(8) 5_666 5_666
Ca8 As1 Ca9 137.69(11) 5_656 5_666
Ca5 As1 Ca9 134.34(6) . 5_666
Ca1 As1 Ca9 80.01(11) 7_565 5_666
Ca1 As1 Ca9 88.06(11) . 5_666
Zn6A As1 Ca9 58.87(10) . 5_656
Zn5 As1 Ca9 59.17(10) 5_656 5_656
Zn5 As1 Ca9 127.60(12) 5_666 5_656
Zn6B As1 Ca9 75.09(10) . 5_656
Ca8 As1 Ca9 137.69(11) 5_666 5_656
Ca8 As1 Ca9 78.61(8) 5_656 5_656
Ca5 As1 Ca9 134.34(6) . 5_656
Ca1 As1 Ca9 88.06(11) 7_565 5_656
Ca1 As1 Ca9 80.01(11) . 5_656
Ca9 As1 Ca9 82.93(10) 5_666 5_656
Zn3 As2 Zn3 120.55(17) 5_656 5_666
Zn3 As2 Zn1 119.28(8) 5_656 .
Zn3 As2 Zn1 119.28(8) 5_666 .
Zn3 As2 Ca7 139.95(12) 5_656 5_666
Zn3 As2 Ca7 62.25(10) 5_666 5_666
Zn1 As2 Ca7 66.21(7) . 5_666
Zn3 As2 Ca7 62.25(10) 5_656 5_656
Zn3 As2 Ca7 139.95(12) 5_666 5_656
Zn1 As2 Ca7 66.21(7) . 5_656
Ca7 As2 Ca7 90.28(10) 5_666 5_656
Zn3 As2 Ca6 62.39(10) 5_656 2_554
Zn3 As2 Ca6 139.31(12) 5_666 2_554
Zn1 As2 Ca6 79.25(8) . 2_554
Ca7 As2 Ca6 145.11(10) 5_666 2_554
Ca7 As2 Ca6 79.81(7) 5_656 2_554
Zn3 As2 Ca6 139.31(12) 5_656 2_564
Zn3 As2 Ca6 62.39(10) 5_666 2_564
Zn1 As2 Ca6 79.25(8) . 2_564
Ca7 As2 Ca6 79.81(7) 5_666 2_564
Ca7 As2 Ca6 145.11(10) 5_656 2_564
Ca6 As2 Ca6 89.40(10) 2_554 2_564
Zn3 As2 Ca2 65.35(9) 5_656 .
Zn3 As2 Ca2 65.35(9) 5_666 .
Zn1 As2 Ca2 156.75(9) . .
Ca7 As2 Ca2 126.80(7) 5_666 .
Ca7 As2 Ca2 126.80(7) 5_656 .
Ca6 As2 Ca2 84.30(9) 2_554 .
Ca6 As2 Ca2 84.30(9) 2_564 .
Zn3 As2 Ca5 68.44(10) 5_656 .
Zn3 As2 Ca5 68.44(10) 5_666 .
Zn1 As2 Ca5 128.32(9) . .
Ca7 As2 Ca5 78.24(8) 5_666 .
Ca7 As2 Ca5 78.24(8) 5_656 .
Ca6 As2 Ca5 130.82(6) 2_554 .
Ca6 As2 Ca5 130.82(6) 2_564 .
Ca2 As2 Ca5 74.93(8) . .
Zn2 As3 Zn2 113.70(9) 5_656 5_666
Zn2 As3 Ca7 76.08(7) 5_656 .
Zn2 As3 Ca7 76.08(7) 5_666 .
Zn2 As3 Ca4 78.69(7) 5_656 .
Zn2 As3 Ca4 78.69(7) 5_666 .
Ca7 As3 Ca4 132.89(11) . .
Zn2 As3 Ca8 115.25(6) 5_656 .
Zn2 As3 Ca8 115.25(6) 5_666 .
Ca7 As3 Ca8 154.84(11) . .
Ca4 As3 Ca8 72.28(10) . .
Zn2 As3 Ca5 151.57(9) 5_656 5_666
Zn2 As3 Ca5 75.02(6) 5_666 5_666
Ca7 As3 Ca5 80.35(8) . 5_666
Ca4 As3 Ca5 129.60(7) . 5_666
Ca8 As3 Ca5 81.26(8) . 5_666
Zn2 As3 Ca5 75.02(6) 5_656 5_656
Zn2 As3 Ca5 151.57(9) 5_666 5_656
Ca7 As3 Ca5 80.35(8) . 5_656
Ca4 As3 Ca5 129.60(7) . 5_656
Ca8 As3 Ca5 81.26(8) . 5_656
Ca5 As3 Ca5 85.61(9) 5_666 5_656
Zn1 As4 Zn1 116.07(9) 5_656 5_666
Zn1 As4 Ca3 111.03(6) 5_656 6_657
Zn1 As4 Ca3 111.03(6) 5_666 6_657
Zn1 As4 Ca2 158.01(9) 5_656 2_565
Zn1 As4 Ca2 76.13(6) 5_666 2_565
Ca3 As4 Ca2 78.37(8) 6_657 2_565
Zn1 As4 Ca2 76.13(6) 5_656 2
Zn1 As4 Ca2 158.01(9) 5_666 2
Ca3 As4 Ca2 78.37(8) 6_657 2
Ca2 As4 Ca2 86.91(9) 2_565 2
Zn1 As4 Ca6 80.70(7) 5_656 .
Zn1 As4 Ca6 80.70(7) 5_666 .
Ca3 As4 Ca6 155.11(10) 6_657 .
Ca2 As4 Ca6 83.65(8) 2_565 .
Ca2 As4 Ca6 83.65(8) 2 .
Zn1 As4 Ca6 77.55(6) 5_656 6_657
Zn1 As4 Ca6 77.55(6) 5_666 6_657
Ca3 As4 Ca6 66.70(9) 6_657 6_657
Ca2 As4 Ca6 124.11(7) 2_565 6_657
Ca2 As4 Ca6 124.11(7) 2 6_657
Ca6 As4 Ca6 138.18(5) . 6_657
Zn1 As4 Ca7 58.09(5) 5_656 .
Zn1 As4 Ca7 58.09(5) 5_666 .
Ca3 As4 Ca7 135.71(10) 6_657 .
Ca2 As4 Ca7 129.14(6) 2_565 .
Ca2 As4 Ca7 129.14(6) 2 .
Ca6 As4 Ca7 69.18(9) . .
Ca6 As4 Ca7 69.01(8) 6_657 .
Zn6B As5 Zn6B 115.73(16) 5_666 5_656
Zn6B As5 Zn6A 23.19(11) 5_666 5_666
Zn6B As5 Zn6A 119.65(12) 5_656 5_666
Zn6B As5 Zn6A 119.65(12) 5_666 5_656
Zn6B As5 Zn6A 23.19(11) 5_656 5_656
Zn6A As5 Zn6A 113.21(17) 5_666 5_656
Zn6B As5 Zn6B 79.84(11) 5_666 .
Zn6B As5 Zn6B 79.84(11) 5_656 .
Zn6A As5 Zn6B 103.02(12) 5_666 .
Zn6A As5 Zn6B 103.02(12) 5_656 .
Zn6B As5 Ca8 137.37(13) 5_666 5_656
Zn6B As5 Ca8 64.46(10) 5_656 5_656
Zn6A As5 Ca8 160.38(13) 5_666 5_656
Zn6A As5 Ca8 77.96(10) 5_656 5_656
Zn6B As5 Ca8 57.78(8) . 5_656
Zn6B As5 Ca8 64.46(10) 5_666 5_666
Zn6B As5 Ca8 137.37(13) 5_656 5_666
Zn6A As5 Ca8 77.96(10) 5_666 5_666
Zn6A As5 Ca8 160.38(13) 5_656 5_666
Zn6B As5 Ca8 57.78(8) . 5_666
Ca8 As5 Ca8 87.10(10) 5_656 5_666
Zn6B As5 Ca4 152.37(13) 5_666 5_656
Zn6B As5 Ca4 75.88(9) 5_656 5_656
Zn6A As5 Ca4 129.21(14) 5_666 5_656
Zn6A As5 Ca4 61.20(11) 5_656 5_656
Zn6B As5 Ca4 127.75(7) . 5_656
Ca8 As5 Ca4 70.02(8) 5_656 5_656
Ca8 As5 Ca4 125.29(10) 5_666 5_656
Zn6B As5 Ca4 75.88(9) 5_666 5_666
Zn6B As5 Ca4 152.37(13) 5_656 5_666
Zn6A As5 Ca4 61.20(11) 5_666 5_666
Zn6A As5 Ca4 129.21(14) 5_656 5_666
Zn6B As5 Ca4 127.75(7) . 5_666
Ca8 As5 Ca4 125.29(10) 5_656 5_666
Ca8 As5 Ca4 70.02(8) 5_666 5_666
Ca4 As5 Ca4 83.70(10) 5_656 5_666
Zn6B As5 Ca9 75.18(10) 5_666 .
Zn6B As5 Ca9 75.18(10) 5_656 .
Zn6A As5 Ca9 58.38(9) 5_666 .
Zn6A As5 Ca9 58.38(9) 5_656 .
Zn6B As5 Ca9 131.88(11) . .
Ca8 As5 Ca9 136.17(5) 5_656 .
Ca8 As5 Ca9 136.17(5) 5_666 .
Ca4 As5 Ca9 84.68(9) 5_656 .
Ca4 As5 Ca9 84.68(9) 5_666 .
Zn6B As5 Ca8 58.83(8) 5_666 .
Zn6B As5 Ca8 58.83(8) 5_656 .
Zn6A As5 Ca8 72.48(11) 5_666 .
Zn6A As5 Ca8 72.48(11) 5_656 .
Zn6B As5 Ca8 57.31(10) . .
Ca8 As5 Ca8 97.19(9) 5_656 .
Ca8 As5 Ca8 97.19(9) 5_666 .
Ca4 As5 Ca8 133.46(6) 5_656 .
Ca4 As5 Ca8 133.46(6) 5_666 .
Ca9 As5 Ca8 74.57(10) . .
Zn1 As6 Zn2 121.80(8) . .
Zn1 As6 Ca7 66.68(7) . 5_656
Zn2 As6 Ca7 74.16(7) . 5_656
Zn1 As6 Ca7 66.68(7) . 5_666
Zn2 As6 Ca7 74.16(7) . 5_666
Ca7 As6 Ca7 92.54(10) 5_656 5_666
Zn1 As6 Ca3 134.79(5) . 5_666
Zn2 As6 Ca3 68.12(7) . 5_666
Ca7 As6 Ca3 142.26(10) 5_656 5_666
Ca7 As6 Ca3 76.41(7) 5_666 5_666
Zn1 As6 Ca3 134.79(5) . 5_656
Zn2 As6 Ca3 68.12(7) . 5_656
Ca7 As6 Ca3 76.41(7) 5_656 5_656
Ca7 As6 Ca3 142.26(10) 5_666 5_656
Ca3 As6 Ca3 90.42(10) 5_666 5_656
Zn1 As6 Ca6 79.09(8) . 5_656
Zn2 As6 Ca6 133.31(5) . 5_656
Ca7 As6 Ca6 79.10(7) 5_656 5_656
Ca7 As6 Ca6 145.18(10) 5_666 5_656
Ca3 As6 Ca6 129.09(10) 5_666 5_656
Ca3 As6 Ca6 68.81(8) 5_656 5_656
Zn1 As6 Ca6 79.09(8) . 5_666
Zn2 As6 Ca6 133.31(5) . 5_666
Ca7 As6 Ca6 145.18(10) 5_656 5_666
Ca7 As6 Ca6 79.10(7) 5_666 5_666
Ca3 As6 Ca6 68.81(8) 5_666 5_666
Ca3 As6 Ca6 129.09(10) 5_656 5_666
Ca6 As6 Ca6 88.67(10) 5_656 5_666
Zn3 As7 Zn4 135.20(15) . 1_655
Zn3 As7 Zn5 138.49(15) . .
Zn4 As7 Zn5 86.31(14) 1_655 .
Zn3 As7 Ca1 142.00(9) . 5_656
Zn4 As7 Ca1 53.92(11) 1_655 5_656
Zn5 As7 Ca1 55.81(11) . 5_656
Zn3 As7 Ca1 142.00(9) . 3_656
Zn4 As7 Ca1 53.92(11) 1_655 3_656
Zn5 As7 Ca1 55.81(11) . 3_656
Ca1 As7 Ca1 75.80(17) 5_656 3_656
Zn3 As7 Ca2 68.64(10) . 5_666
Zn4 As7 Ca2 80.01(10) 1_655 5_666
Zn5 As7 Ca2 132.78(6) . 5_666
Ca1 As7 Ca2 133.76(12) 5_656 5_666
Ca1 As7 Ca2 80.24(10) 3_656 5_666
Zn3 As7 Ca2 68.64(9) . 5_656
Zn4 As7 Ca2 80.01(10) 1_655 5_656
Zn5 As7 Ca2 132.78(6) . 5_656
Ca1 As7 Ca2 80.24(10) 5_656 5_656
Ca1 As7 Ca2 133.76(12) 3_656 5_656
Ca2 As7 Ca2 89.01(9) 5_666 5_656
Zn3 As7 Ca5 73.79(10) . 5_656
Zn4 As7 Ca5 131.39(7) 1_655 5_656
Zn5 As7 Ca5 76.90(9) . 5_656
Ca1 As7 Ca5 79.50(10) 5_656 5_656
Ca1 As7 Ca5 132.67(12) 3_656 5_656
Ca2 As7 Ca5 142.38(10) 5_666 5_656
Ca2 As7 Ca5 79.08(7) 5_656 5_656
Zn3 As7 Ca5 73.79(9) . 5_666
Zn4 As7 Ca5 131.39(7) 1_655 5_666
Zn5 As7 Ca5 76.90(9) . 5_666
Ca1 As7 Ca5 132.67(12) 5_656 5_666
Ca1 As7 Ca5 79.50(10) 3_656 5_666
Ca2 As7 Ca5 79.08(7) 5_666 5_666
Ca2 As7 Ca5 142.38(10) 5_656 5_666
Ca5 As7 Ca5 88.86(9) 5_656 5_666
Zn3 As7 Ca1 133.29(8) . 3_646
Zn4 As7 Ca1 59.17(9) 1_655 3_646
Zn5 As7 Ca1 60.72(9) . 3_646
Ca1 As7 Ca1 8.74(12) 5_656 3_646
Ca1 As7 Ca1 84.54(11) 3_656 3_646
Ca2 As7 Ca1 137.46(11) 5_666 3_646
Ca2 As7 Ca1 73.59(9) 5_656 3_646
Ca5 As7 Ca1 72.94(9) 5_656 3_646
Ca5 As7 Ca1 136.43(11) 5_666 3_646
Zn3 As7 Ca1 133.29(8) . 5_666
Zn4 As7 Ca1 59.17(9) 1_655 5_666
Zn5 As7 Ca1 60.72(9) . 5_666
Ca1 As7 Ca1 84.54(11) 5_656 5_666
Ca1 As7 Ca1 8.74(12) 3_656 5_666
Ca2 As7 Ca1 73.59(9) 5_666 5_666
Ca2 As7 Ca1 137.46(11) 5_656 5_666
Ca5 As7 Ca1 136.43(11) 5_656 5_666
Ca5 As7 Ca1 72.94(9) 5_666 5_666
Ca1 As7 Ca1 93.27(15) 3_646 5_666
Zn4 As8 Zn4 111.94(16) 5_666 5_656
Zn4 As8 Zn2 123.34(8) 5_666 .
Zn4 As8 Zn2 123.34(8) 5_656 .
Zn4 As8 Ca3 148.64(12) 5_666 5_656
Zn4 As8 Ca3 69.62(10) 5_656 5_656
Zn2 As8 Ca3 69.78(7) . 5_656
Zn4 As8 Ca3 69.62(10) 5_666 5_666
Zn4 As8 Ca3 148.64(12) 5_656 5_666
Zn2 As8 Ca3 69.78(7) . 5_666
Ca3 As8 Ca3 92.99(10) 5_656 5_666
Zn4 As8 Ca1 51.23(11) 5_666 7_665
Zn4 As8 Ca1 63.27(12) 5_656 7_665
Zn2 As8 Ca1 153.64(11) . 7_665
Ca3 As8 Ca1 130.05(11) 5_656 7_665
Ca3 As8 Ca1 119.28(10) 5_666 7_665
Zn4 As8 Ca1 63.27(12) 5_666 1_655
Zn4 As8 Ca1 51.23(11) 5_656 1_655
Zn2 As8 Ca1 153.64(11) . 1_655
Ca3 As8 Ca1 119.28(10) 5_656 1_655
Ca3 As8 Ca1 130.05(11) 5_666 1_655
Ca1 As8 Ca1 12.22(16) 7_665 1_655
Zn4 As8 Ca4 58.94(10) 5_666 5_666
Zn4 As8 Ca4 128.85(12) 5_656 5_666
Zn2 As8 Ca4 76.51(8) . 5_666
Ca3 As8 Ca4 145.87(11) 5_656 5_666
Ca3 As8 Ca4 80.05(7) 5_666 5_666
Ca1 As8 Ca4 80.80(11) 7_665 5_666
Ca1 As8 Ca4 89.25(11) 1_655 5_666
Zn4 As8 Ca4 128.85(12) 5_666 5_656
Zn4 As8 Ca4 58.94(10) 5_656 5_656
Zn2 As8 Ca4 76.51(8) . 5_656
Ca3 As8 Ca4 80.05(7) 5_656 5_656
Ca3 As8 Ca4 145.87(11) 5_666 5_656
Ca1 As8 Ca4 89.25(11) 7_665 5_656
Ca1 As8 Ca4 80.80(11) 1_655 5_656
Ca4 As8 Ca4 87.22(10) 5_666 5_656
Zn4 As8 Ca2 74.01(9) 5_666 1_655
Zn4 As8 Ca2 74.01(9) 5_656 1_655
Zn2 As8 Ca2 130.38(9) . 1_655
Ca3 As8 Ca2 76.72(8) 5_656 1_655
Ca3 As8 Ca2 76.72(8) 5_666 1_655
Ca1 As8 Ca2 75.41(10) 7_665 1_655
Ca1 As8 Ca2 75.41(10) 1_655 1_655
Ca4 As8 Ca2 132.32(6) 5_666 1_655
Ca4 As8 Ca2 132.32(6) 5_656 1_655
As9B As9A Ca1 130.4(2) . 3_556
As9B As9A Ca1 130.4(2) . 5_556
Ca1 As9A Ca1 96.0(3) 3_556 5_556
As9B As9A Zn4 130.0(9) . .
Ca1 As9A Zn4 56.97(14) 3_556 .
Ca1 As9A Zn4 56.97(14) 5_556 .
As9B As9A Zn5 155.2(9) . 1_455
Ca1 As9A Zn5 58.83(15) 3_556 1_455
Ca1 As9A Zn5 58.83(15) 5_556 1_455
Zn4 As9A Zn5 74.83(16) . 1_455
As9B As9A Ca1 122.32(19) . 5_566
Ca1 As9A Ca1 8.50(12) 3_556 5_566
Ca1 As9A Ca1 104.5(2) 5_556 5_566
Zn4 As9A Ca1 63.27(12) . 5_566
Zn5 As9A Ca1 64.73(12) 1_455 5_566
As9B As9A Ca1 122.32(19) . 3_546
Ca1 As9A Ca1 104.5(2) 3_556 3_546
Ca1 As9A Ca1 8.50(12) 5_556 3_546
Zn4 As9A Ca1 63.27(12) . 3_546
Zn5 As9A Ca1 64.73(12) 1_455 3_546
Ca1 As9A Ca1 113.0(2) 5_566 3_546
As9B As9A Ca9 94.4(8) . 1_455
Ca1 As9A Ca9 96.72(17) 3_556 1_455
Ca1 As9A Ca9 96.72(17) 5_556 1_455
Zn4 As9A Ca9 135.5(2) . 1_455
Zn5 As9A Ca9 60.71(14) 1_455 1_455
Ca1 As9A Ca9 95.54(14) 5_566 1_455
Ca1 As9A Ca9 95.54(14) 3_546 1_455
As9B As9A Ca4 71.9(8) . .
Ca1 As9A Ca4 92.38(17) 3_556 .
Ca1 As9A Ca4 92.38(17) 5_556 .
Zn4 As9A Ca4 58.08(14) . .
Zn5 As9A Ca4 132.9(2) 1_455 .
Ca1 As9A Ca4 91.96(14) 5_566 .
Ca1 As9A Ca4 91.96(14) 3_546 .
Ca9 As9A Ca4 166.4(2) 1_455 .
As9B As9A Ca9 45.8(2) . 5_656
Ca1 As9A Ca9 175.14(19) 3_556 5_656
Ca1 As9A Ca9 88.65(11) 5_556 5_656
Zn4 As9A Ca9 127.39(13) . 5_656
Zn5 As9A Ca9 123.03(13) 1_455 5_656
Ca1 As9A Ca9 166.80(17) 5_566 5_656
Ca1 As9A Ca9 80.16(10) 3_546 5_656
Ca9 As9A Ca9 81.18(14) 1_455 5_656
Ca4 As9A Ca9 88.94(14) . 5_656
As9B As9A Ca9 45.8(2) . 5_666
Ca1 As9A Ca9 88.65(11) 3_556 5_666
Ca1 As9A Ca9 175.14(19) 5_556 5_666
Zn4 As9A Ca9 127.39(13) . 5_666
Zn5 As9A Ca9 123.03(13) 1_455 5_666
Ca1 As9A Ca9 80.16(10) 5_566 5_666
Ca1 As9A Ca9 166.80(17) 3_546 5_666
Ca9 As9A Ca9 81.18(14) 1_455 5_666
Ca4 As9A Ca9 88.94(14) . 5_666
Ca9 As9A Ca9 86.69(15) 5_656 5_666
As9A As9B Ca9 124.6(3) . 5_656
As9A As9B Ca9 124.6(3) . 5_666
Ca9 As9B Ca9 103.9(2) 5_656 5_666
As9A As9B Zn6A 159.4(9) . .
Ca9 As9B Zn6A 63.38(13) 5_656 .
Ca9 As9B Zn6A 63.38(13) 5_666 .
As9A As9B Ca1 40.1(2) . 3_556
Ca9 As9B Ca1 164.4(2) 5_656 3_556
Ca9 As9B Ca1 88.52(11) 5_666 3_556
Zn6A As9B Ca1 131.81(16) . 3_556
As9A As9B Ca1 40.1(2) . 5_556
Ca9 As9B Ca1 88.52(11) 5_656 5_556
Ca9 As9B Ca1 164.4(2) 5_666 5_556
Zn6A As9B Ca1 131.81(16) . 5_556
Ca1 As9B Ca1 77.8(2) 3_556 5_556
As9A As9B Ca4 96.3(8) . .
Ca9 As9B Ca4 100.05(16) 5_656 .
Ca9 As9B Ca4 100.05(16) 5_666 .
Zn6A As9B Ca4 63.10(16) . .
Ca1 As9B Ca4 86.75(16) 3_556 .
Ca1 As9B Ca4 86.75(16) 5_556 .
As9A As9B Ca9 73.9(8) . 1_455
Ca9 As9B Ca9 85.91(15) 5_656 1_455
Ca9 As9B Ca9 85.91(15) 5_666 1_455
Zn6A As9B Ca9 126.7(2) . 1_455
Ca1 As9B Ca9 85.62(16) 3_556 1_455
Ca1 As9B Ca9 85.62(16) 5_556 1_455
Ca4 As9B Ca9 170.2(2) . 1_455
As9A As9B Ca1 48.52(16) . 5_566
Ca9 As9B Ca1 171.0(2) 5_656 5_566
Ca9 As9B Ca1 79.83(10) 5_666 5_566
Zn6A As9B Ca1 125.24(13) . 5_566
Ca1 As9B Ca1 8.76(12) 3_556 5_566
Ca1 As9B Ca1 86.55(17) 5_556 5_566
Ca4 As9B Ca1 87.19(14) . 5_566
Ca9 As9B Ca1 86.21(14) 1_455 5_566
As9A As9B Ca1 48.52(16) . 3_546
Ca9 As9B Ca1 79.83(10) 5_656 3_546
Ca9 As9B Ca1 171.0(2) 5_666 3_546
Zn6A As9B Ca1 125.24(13) . 3_546
Ca1 As9B Ca1 86.55(17) 3_556 3_546
Ca1 As9B Ca1 8.76(12) 5_556 3_546
Ca4 As9B Ca1 87.19(14) . 3_546
Ca9 As9B Ca1 86.21(14) 1_455 3_546
Ca1 As9B Ca1 95.3(2) 5_566 3_546
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ca1 Ca1 0.652(9) 7_565
Ca1 As9A 2.438(5) 5_556
Ca1 Zn4 2.480(5) 5_556
Ca1 Zn5 2.565(5) 5_656
Ca1 As9B 2.885(6) 5_556
Ca1 As7 2.948(4) 5_656
Ca1 As9A 2.955(5) 5_566
Ca1 Zn4 2.989(5) 5_566
Ca1 Zn5 3.061(5) 5_666
Ca1 As8 3.066(5) 1_455
Ca1 As1 3.093(5) .
Ca1 As9B 3.333(5) 5_566
Ca2 As7 3.049(3) 5_666
Ca2 As7 3.049(3) 5_656
Ca2 Zn3 3.080(4) 5_666
Ca2 Zn3 3.080(4) 5_656
Ca2 As4 3.108(3) 2_554
Ca2 As4 3.108(3) 2_564
Ca2 As2 3.144(4) .
Ca2 As8 3.251(4) 1_455
Ca2 Zn1 3.500(4) 6_556
Ca2 Zn4 3.550(4) 5_566
Ca2 Zn4 3.550(4) 5_556
Ca2 Ca3 3.853(4) 5_556
Ca3 As8 2.947(3) 5_656
Ca3 As8 2.947(3) 5_666
Ca3 As4 2.989(4) 6_557
Ca3 As6 3.012(3) 5_666
Ca3 As6 3.012(3) 5_656
Ca3 Zn4 3.169(5) .
Ca3 Zn2 3.214(3) 5_666
Ca3 Zn2 3.214(3) 5_656
Ca3 Ca6 3.430(4) .
Ca3 Ca7 3.692(5) .
Ca3 Ca2 3.853(4) 5_556
Ca3 Ca2 3.853(4) 5_566
Ca4 Zn4 2.830(5) .
Ca4 As9B 2.932(6) .
Ca4 Zn6A 2.986(6) .
Ca4 As3 3.061(4) .
Ca4 As9A 3.066(6) .
Ca4 As8 3.099(3) 5_666
Ca4 As8 3.099(3) 5_656
Ca4 As5 3.204(3) 5_656
Ca4 As5 3.204(3) 5_666
Ca4 Zn6B 3.562(5) .
Ca4 Zn2 3.581(3) 5_666
Ca4 Zn2 3.581(3) 5_656
Ca5 As7 3.053(3) 5_656
Ca5 As7 3.053(3) 5_666
Ca5 As1 3.079(4) .
Ca5 As3 3.145(3) 5_666
Ca5 As3 3.145(3) 5_656
Ca5 As2 3.242(4) .
Ca5 Zn3 3.272(4) 5_656
Ca5 Zn3 3.272(4) 5_666
Ca5 Zn5 3.456(4) 5_666
Ca5 Zn5 3.456(4) 5_656
Ca5 Zn2 3.501(4) .
Ca6 Zn3 2.891(5) 6_557
Ca6 As2 3.039(3) 2_565
Ca6 As2 3.039(3) 2
Ca6 As6 3.058(3) 5_656
Ca6 As6 3.058(3) 5_666
Ca6 As4 3.115(4) .
Ca6 As4 3.238(4) 6_557
Ca6 Zn1 3.649(3) 2
Ca6 Zn1 3.649(3) 2_565
Ca6 Zn1 3.676(3) 5_666
Ca6 Zn1 3.676(3) 5_656
Ca7 Zn3 2.870(5) .
Ca7 As6 2.958(3) 5_656
Ca7 As6 2.958(3) 5_666
Ca7 As3 2.977(4) .
Ca7 As2 3.015(3) 5_666
Ca7 As2 3.015(3) 5_656
Ca7 Zn1 3.116(3) 5_666
Ca7 Zn1 3.116(3) 5_656
Ca7 Zn2 3.424(3) 5_656
Ca7 Zn2 3.424(3) 5_666
Ca7 As4 3.598(4) .
Ca8 Zn6B 2.949(4) 5_656
Ca8 Zn6B 2.949(4) 5_666
Ca8 As1 3.021(3) 5_666
Ca8 As1 3.021(3) 5_656
Ca8 Zn6B 3.040(5) .
Ca8 As3 3.075(4) .
Ca8 As5 3.102(3) 5_656
Ca8 As5 3.102(3) 5_666
Ca8 Zn5 3.295(5) .
Ca8 As5 3.315(4) .
Ca8 Zn6A 3.526(5) 5_656
Ca8 Zn6A 3.526(5) 5_666
Ca9 As9B 2.714(4) 5_656
Ca9 As9B 2.714(4) 5_666
Ca9 Zn6A 2.880(4) 5_656
Ca9 Zn6A 2.880(4) 5_666
Ca9 Zn5 2.904(5) .
Ca9 As9A 2.979(6) 1_655
Ca9 As9B 3.092(6) 1_655
Ca9 As9A 3.114(4) 5_656
Ca9 As9A 3.114(4) 5_666
Ca9 As5 3.224(4) .
Ca9 As1 3.228(3) 5_666
Ca9 As1 3.228(3) 5_656
Zn1 As4 2.5193(13) 5_656
Zn1 As4 2.5193(13) 5_666
Zn1 As2 2.665(2) .
Zn1 As6 2.698(2) .
Zn1 Ca7 3.116(3) 5_666
Zn1 Ca7 3.116(3) 5_656
Zn1 Ca2 3.500(4) 6_656
Zn1 Ca6 3.649(3) 2_554
Zn1 Ca6 3.649(3) 2_564
Zn1 Ca6 3.676(3) 5_666
Zn1 Ca6 3.676(3) 5_656
Zn2 As3 2.5529(14) 5_656
Zn2 As3 2.5529(14) 5_666
Zn2 As8 2.657(3) .
Zn2 As6 2.711(3) .
Zn2 Ca3 3.214(3) 5_666
Zn2 Ca3 3.214(3) 5_656
Zn2 Ca7 3.424(3) 5_656
Zn2 Ca7 3.424(3) 5_666
Zn2 Ca4 3.581(3) 5_666
Zn2 Ca4 3.581(3) 5_656
Zn3 As7 2.304(4) .
Zn3 As2 2.461(2) 5_656
Zn3 As2 2.461(2) 5_666
Zn3 Ca6 2.891(5) 6_657
Zn3 Ca2 3.080(4) 5_666
Zn3 Ca2 3.080(4) 5_656
Zn3 Ca5 3.272(4) 5_656
Zn3 Ca5 3.272(4) 5_666
Zn4 As7 2.422(4) 1_455
Zn4 Ca1 2.480(5) 5_556
Zn4 Ca1 2.480(5) 3_556
Zn4 As8 2.579(2) 5_666
Zn4 As8 2.579(2) 5_656
Zn4 As9A 2.733(6) .
Zn4 Ca1 2.989(5) 3_546
Zn4 Ca1 2.989(5) 5_566
Zn4 Ca2 3.550(4) 5_566
Zn4 Ca2 3.550(4) 5_556
Zn5 As7 2.453(4) .
Zn5 As1 2.521(2) 5_656
Zn5 As1 2.521(2) 5_666
Zn5 Ca1 2.565(5) 3_656
Zn5 Ca1 2.565(5) 5_656
Zn5 As9A 2.755(6) 1_655
Zn5 Ca1 3.061(5) 5_666
Zn5 Ca1 3.061(5) 3_646
Zn5 Ca5 3.456(4) 5_666
Zn5 Ca5 3.456(4) 5_656
Zn6A Zn6B 1.022(5) .
Zn6A As1 2.481(4) .
Zn6A As5 2.560(3) 5_666
Zn6A As5 2.560(3) 5_656
Zn6A As9B 2.767(7) .
Zn6A Ca9 2.880(4) 5_656
Zn6A Ca9 2.880(4) 5_666
Zn6A Ca8 3.526(5) 5_656
Zn6A Ca8 3.526(5) 5_666
Zn6B As5 2.524(2) 5_666
Zn6B As5 2.524(2) 5_656
Zn6B As1 2.525(4) .
Zn6B Ca8 2.949(4) 5_656
Zn6B Ca8 2.949(4) 5_666
Zn6B As5 2.999(5) .
Zn6B Ca9 3.550(4) 5_656
Zn6B Ca9 3.550(4) 5_666
As1 Zn5 2.521(2) 5_656
As1 Zn5 2.521(2) 5_666
As1 Ca8 3.021(3) 5_666
As1 Ca8 3.021(3) 5_656
As1 Ca1 3.093(5) 7_565
As1 Ca9 3.228(3) 5_666
As1 Ca9 3.228(3) 5_656
As2 Zn3 2.461(2) 5_656
As2 Zn3 2.461(2) 5_666
As2 Ca7 3.015(3) 5_666
As2 Ca7 3.015(3) 5_656
As2 Ca6 3.039(3) 2_554
As2 Ca6 3.039(3) 2_564
As3 Zn2 2.5529(14) 5_656
As3 Zn2 2.5529(14) 5_666
As3 Ca5 3.145(3) 5_666
As3 Ca5 3.145(3) 5_656
As4 Zn1 2.5193(13) 5_656
As4 Zn1 2.5193(13) 5_666
As4 Ca3 2.989(4) 6_657
As4 Ca2 3.108(3) 2_565
As4 Ca2 3.108(3) 2
As4 Ca6 3.238(4) 6_657
As5 Zn6B 2.524(2) 5_666
As5 Zn6B 2.524(2) 5_656
As5 Zn6A 2.560(3) 5_666
As5 Zn6A 2.560(3) 5_656
As5 Ca8 3.102(3) 5_656
As5 Ca8 3.102(3) 5_666
As5 Ca4 3.204(3) 5_656
As5 Ca4 3.204(3) 5_666
As6 Ca7 2.958(3) 5_656
As6 Ca7 2.958(3) 5_666
As6 Ca3 3.012(3) 5_666
As6 Ca3 3.012(3) 5_656
As6 Ca6 3.058(3) 5_656
As6 Ca6 3.058(3) 5_666
As7 Zn4 2.422(4) 1_655
As7 Ca1 2.948(4) 5_656
As7 Ca1 2.948(4) 3_656
As7 Ca2 3.049(3) 5_666
As7 Ca2 3.049(3) 5_656
As7 Ca5 3.053(3) 5_656
As7 Ca5 3.053(3) 5_666
As7 Ca1 3.389(4) 3_646
As7 Ca1 3.389(5) 5_666
As8 Zn4 2.579(2) 5_666
As8 Zn4 2.579(2) 5_656
As8 Ca3 2.947(2) 5_656
As8 Ca3 2.947(3) 5_666
As8 Ca1 3.066(5) 7_665
As8 Ca1 3.066(5) 1_655
As8 Ca4 3.099(3) 5_666
As8 Ca4 3.099(3) 5_656
As8 Ca2 3.251(4) 1_655
As9A As9B 0.628(4) .
As9A Ca1 2.438(5) 3_556
As9A Ca1 2.438(5) 5_556
As9A Zn5 2.755(6) 1_455
As9A Ca1 2.955(5) 5_566
As9A Ca1 2.955(5) 3_546
As9A Ca9 2.979(6) 1_455
As9A Ca9 3.114(4) 5_656
As9A Ca9 3.114(4) 5_666
As9B Ca9 2.714(4) 5_656
As9B Ca9 2.714(4) 5_666
As9B Ca1 2.885(6) 3_556
As9B Ca1 2.885(6) 5_556
As9B Ca9 3.092(6) 1_455
As9B Ca1 3.333(5) 5_566
As9B Ca1 3.333(6) 3_546
