#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341706.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341706
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Ca9 Mn4.4 Sb9'
_chemical_formula_weight         1698.21
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.467(2)
_cell_length_b                   4.6227(9)
_cell_length_c                   44.067(8)
_cell_measurement_reflns_used    990
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      28.18
_cell_measurement_theta_min      2.83
_cell_volume                     2539.6(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.934
_diffrn_measured_fraction_theta_max 0.934
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0760
_diffrn_reflns_av_sigmaI/netI    0.0582
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       56
_diffrn_reflns_limit_l_min       -55
_diffrn_reflns_number            20241
_diffrn_reflns_theta_full        28.26
_diffrn_reflns_theta_max         28.26
_diffrn_reflns_theta_min         1.70
_exptl_absorpt_coefficient_mu    13.305
_exptl_absorpt_correction_T_max  0.7767
_exptl_absorpt_correction_T_min  0.5282
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.441
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             2996
_exptl_crystal_size_max          0.05
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_refine_diff_density_max         7.780
_refine_diff_density_min         -2.344
_refine_diff_density_rms         0.458
_refine_ls_extinction_coef       0.000133(19)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.113
_refine_ls_matrix_type           full
_refine_ls_number_parameters     153
_refine_ls_number_reflns         3291
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.113
_refine_ls_R_factor_all          0.0800
_refine_ls_R_factor_gt           0.0588
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0222P)²+124.7385P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1074
_refine_ls_wR_factor_ref         0.1167
_reflns_number_gt                2648
_reflns_number_total             3291
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_003.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_cell_volume        2539.7(8)
_cod_original_sg_symbol_H-M      Pnma
_cod_original_formula_sum        'Ca9 Mn4.40 Sb9'
_cod_database_code               4341706
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sb1 Sb 0.25121(10) 0.2500 0.44955(3) 0.0105(3) Uani 1 2 d S
Sb2 Sb 0.27528(9) 0.2500 0.29840(3) 0.0067(2) Uani 1 2 d S
Sb3 Sb 0.50585(10) 0.2500 0.62034(3) 0.0089(3) Uani 1 2 d S
Sb4 Sb 0.55170(11) 0.2500 0.77977(3) 0.0151(3) Uani 1 2 d S
Sb5 Sb 0.60561(10) 0.2500 0.46823(3) 0.0092(3) Uani 1 2 d S
Sb6 Sb 0.62101(9) 0.2500 0.29514(3) 0.0069(2) Uani 1 2 d S
Sb7 Sb 0.87493(11) 0.2500 0.62973(3) 0.0135(3) Uani 1 2 d S
Sb8 Sb 0.81251(10) 0.2500 0.37557(3) 0.0100(3) Uani 1 2 d S
Sb9A Sb 0.0556(2) 0.2500 0.54573(6) 0.0112(4) Uani 0.593(3) 2 d SP
Sb9B Sb 0.0880(3) 0.2500 0.53447(9) 0.0112(4) Uani 0.407(3) 2 d SP
Mn1 Mn 0.4417(2) 0.2500 0.25416(6) 0.0084(5) Uani 1 2 d S
Mn2 Mn 0.5925(2) 0.2500 0.35933(6) 0.0081(5) Uani 1 2 d S
Mn3 Mn 0.8215(5) 0.2500 0.68397(15) 0.008(2) Uani 0.404(12) 2 d SP
Mn4 Mn 0.0679(4) 0.2500 0.60944(12) 0.0070(7) Uani 0.477(5) 2 d SP
Mn5 Mn 0.8504(4) 0.2500 0.57119(11) 0.0070(7) Uani 0.523(5) 2 d SP
Mn6A Mn 0.3031(8) 0.2500 0.5085(2) 0.0137(8) Uani 0.310(6) 2 d SP
Mn6B Mn 0.3997(3) 0.2500 0.49737(10) 0.0137(8) Uani 0.690(6) 2 d SP
Ca1 Ca 0.0163(5) 0.1665(11) 0.41917(13) 0.0172(13) Uani 0.50 1 d P
Ca2 Ca 0.0250(3) 0.2500 0.32705(9) 0.0175(8) Uani 1 2 d S
Ca3 Ca 0.2412(3) 0.2500 0.67123(9) 0.0121(7) Uani 1 2 d S
Ca4 Ca 0.2889(3) 0.2500 0.57924(10) 0.0172(8) Uani 1 2 d S
Ca5 Ca 0.3018(3) 0.2500 0.37477(9) 0.0115(7) Uani 1 2 d S
Ca6 Ca 0.3055(3) 0.2500 0.75240(11) 0.0216(10) Uani 1 2 d S
Ca7 Ca 0.5525(3) 0.2500 0.69111(8) 0.0093(7) Uani 1 2 d S
Ca8 Ca 0.5748(3) 0.2500 0.55124(10) 0.0240(10) Uani 1 2 d S
Ca9 Ca 0.8464(4) 0.2500 0.50116(13) 0.0479(16) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Mn6A Sb1 Mn5 115.32(13) . 5_666
Mn6A Sb1 Mn5 115.32(13) . 5_656
Mn5 Sb1 Mn5 111.90(17) 5_666 5_656
Mn6A Sb1 Mn6B 27.3(2) . .
Mn5 Sb1 Mn6B 123.08(9) 5_666 .
Mn5 Sb1 Mn6B 123.08(9) 5_656 .
Mn6A Sb1 Ca8 81.10(17) . 5_666
Mn5 Sb1 Ca8 72.72(11) 5_666 5_666
Mn5 Sb1 Ca8 155.67(13) 5_656 5_666
Mn6B Sb1 Ca8 63.69(10) . 5_666
Mn6A Sb1 Ca8 81.10(16) . 5_656
Mn5 Sb1 Ca8 155.67(13) 5_666 5_656
Mn5 Sb1 Ca8 72.72(11) 5_656 5_656
Mn6B Sb1 Ca8 63.69(10) . 5_656
Ca8 Sb1 Ca8 93.63(12) 5_666 5_656
Mn6A Sb1 Ca1 128.2(2) . .
Mn5 Sb1 Ca1 63.47(13) 5_666 .
Mn5 Sb1 Ca1 49.92(13) 5_656 .
Mn6B Sb1 Ca1 154.96(14) . .
Ca8 Sb1 Ca1 134.44(12) 5_666 .
Ca8 Sb1 Ca1 121.78(12) 5_656 .
Mn6A Sb1 Ca1 128.2(2) . 7_565
Mn5 Sb1 Ca1 49.92(13) 5_666 7_565
Mn5 Sb1 Ca1 63.47(13) 5_656 7_565
Mn6B Sb1 Ca1 154.97(14) . 7_565
Ca8 Sb1 Ca1 121.78(11) 5_666 7_565
Ca8 Sb1 Ca1 134.43(12) 5_656 7_565
Ca1 Sb1 Ca1 13.66(18) . 7_565
Mn6A Sb1 Ca5 155.2(2) . .
Mn5 Sb1 Ca5 76.32(11) 5_666 .
Mn5 Sb1 Ca5 76.32(11) 5_656 .
Mn6B Sb1 Ca5 127.89(12) . .
Ca8 Sb1 Ca5 81.99(10) 5_666 .
Ca8 Sb1 Ca5 81.99(10) 5_656 .
Ca1 Sb1 Ca5 76.36(12) . .
Ca1 Sb1 Ca5 76.36(12) 7_565 .
Mn6A Sb1 Ca9 57.73(15) . 5_666
Mn5 Sb1 Ca9 58.88(13) 5_666 5_666
Mn5 Sb1 Ca9 127.63(13) 5_656 5_666
Mn6B Sb1 Ca9 75.87(12) . 5_666
Ca8 Sb1 Ca9 75.88(10) 5_666 5_666
Ca8 Sb1 Ca9 138.43(13) 5_656 5_666
Ca1 Sb1 Ca9 91.23(14) . 5_666
Ca1 Sb1 Ca9 81.93(14) 7_565 5_666
Ca5 Sb1 Ca9 134.05(8) . 5_666
Mn6A Sb1 Ca9 57.73(15) . 5_656
Mn5 Sb1 Ca9 127.63(13) 5_666 5_656
Mn5 Sb1 Ca9 58.88(13) 5_656 5_656
Mn6B Sb1 Ca9 75.87(12) . 5_656
Ca8 Sb1 Ca9 138.43(13) 5_666 5_656
Ca8 Sb1 Ca9 75.88(10) 5_656 5_656
Ca1 Sb1 Ca9 81.93(14) . 5_656
Ca1 Sb1 Ca9 91.23(14) 7_565 5_656
Ca5 Sb1 Ca9 134.05(8) . 5_656
Ca9 Sb1 Ca9 85.74(13) 5_666 5_656
Mn3 Sb2 Mn3 116.3(2) 5_666 5_656
Mn3 Sb2 Mn1 121.25(12) 5_666 .
Mn3 Sb2 Mn1 121.25(12) 5_656 .
Mn3 Sb2 Ca7 69.00(14) 5_666 5_666
Mn3 Sb2 Ca7 150.83(16) 5_656 5_666
Mn1 Sb2 Ca7 66.94(8) . 5_666
Mn3 Sb2 Ca7 150.83(16) 5_666 5_656
Mn3 Sb2 Ca7 68.99(14) 5_656 5_656
Mn1 Sb2 Ca7 66.95(8) . 5_656
Ca7 Sb2 Ca7 92.92(10) 5_666 5_656
Mn3 Sb2 Ca6 55.53(16) 5_666 2_564
Mn3 Sb2 Ca6 130.38(16) 5_656 2_564
Mn1 Sb2 Ca6 78.32(10) . 2_564
Ca7 Sb2 Ca6 77.43(8) 5_666 2_564
Ca7 Sb2 Ca6 144.91(12) 5_656 2_564
Mn3 Sb2 Ca6 130.38(16) 5_666 2_554
Mn3 Sb2 Ca6 55.53(16) 5_656 2_554
Mn1 Sb2 Ca6 78.32(10) . 2_554
Ca7 Sb2 Ca6 144.91(12) 5_666 2_554
Ca7 Sb2 Ca6 77.43(8) 5_656 2_554
Ca6 Sb2 Ca6 91.20(12) 2_564 2_554
Mn3 Sb2 Ca2 58.78(12) 5_666 .
Mn3 Sb2 Ca2 58.78(12) 5_656 .
Mn1 Sb2 Ca2 158.82(9) . .
Ca7 Sb2 Ca2 124.75(7) 5_666 .
Ca7 Sb2 Ca2 124.75(7) 5_656 .
Ca6 Sb2 Ca2 86.94(10) 2_564 .
Ca6 Sb2 Ca2 86.94(10) 2_554 .
Mn3 Sb2 Ca5 76.06(15) 5_666 .
Mn3 Sb2 Ca5 76.06(15) 5_656 .
Mn1 Sb2 Ca5 127.61(9) . .
Ca7 Sb2 Ca5 77.88(8) 5_666 .
Ca7 Sb2 Ca5 77.88(8) 5_656 .
Ca6 Sb2 Ca5 130.85(8) 2_564 .
Ca6 Sb2 Ca5 130.85(8) 2_554 .
Ca2 Sb2 Ca5 73.57(9) . .
Mn2 Sb3 Mn2 113.39(11) 5_666 5_656
Mn2 Sb3 Ca8 115.60(7) 5_666 .
Mn2 Sb3 Ca8 115.60(7) 5_656 .
Mn2 Sb3 Ca7 76.29(7) 5_666 .
Mn2 Sb3 Ca7 76.29(7) 5_656 .
Ca8 Sb3 Ca7 153.67(11) . .
Mn2 Sb3 Ca4 79.14(7) 5_666 .
Mn2 Sb3 Ca4 79.14(7) 5_656 .
Ca8 Sb3 Ca4 71.96(11) . .
Ca7 Sb3 Ca4 134.37(11) . .
Mn2 Sb3 Ca5 73.69(7) 5_666 5_666
Mn2 Sb3 Ca5 151.22(9) 5_656 5_666
Ca8 Sb3 Ca5 82.35(9) . 5_666
Ca7 Sb3 Ca5 78.75(8) . 5_666
Ca4 Sb3 Ca5 129.27(7) . 5_666
Mn2 Sb3 Ca5 151.22(9) 5_666 5_656
Mn2 Sb3 Ca5 73.69(7) 5_656 5_656
Ca8 Sb3 Ca5 82.35(9) . 5_656
Ca7 Sb3 Ca5 78.75(8) . 5_656
Ca4 Sb3 Ca5 129.27(7) . 5_656
Ca5 Sb3 Ca5 87.65(9) 5_666 5_656
Mn1 Sb4 Mn1 114.10(10) 5_666 5_656
Mn1 Sb4 Ca3 110.14(7) 5_666 6_657
Mn1 Sb4 Ca3 110.14(7) 5_656 6_657
Mn1 Sb4 Ca2 76.14(7) 5_666 2_565
Mn1 Sb4 Ca2 162.20(10) 5_656 2_565
Ca3 Sb4 Ca2 77.59(9) 6_657 2_565
Mn1 Sb4 Ca2 162.20(10) 5_666 2
Mn1 Sb4 Ca2 76.14(7) 5_656 2
Ca3 Sb4 Ca2 77.59(9) 6_657 2
Ca2 Sb4 Ca2 90.47(10) 2_565 2
Mn1 Sb4 Ca6 80.16(8) 5_666 .
Mn1 Sb4 Ca6 80.16(8) 5_656 .
Ca3 Sb4 Ca6 159.02(12) 6_657 .
Ca2 Sb4 Ca6 87.74(10) 2_565 .
Ca2 Sb4 Ca6 87.74(10) 2 .
Mn1 Sb4 Ca6 75.56(7) 5_666 6_657
Mn1 Sb4 Ca6 75.56(7) 5_656 6_657
Ca3 Sb4 Ca6 66.57(11) 6_657 6_657
Ca2 Sb4 Ca6 122.00(8) 2_565 6_657
Ca2 Sb4 Ca6 122.00(8) 2 6_657
Ca6 Sb4 Ca6 134.41(4) . 6_657
Mn6B Sb5 Mn6B 113.45(16) 5_666 5_656
Mn6B Sb5 Mn6A 27.2(2) 5_666 5_666
Mn6B Sb5 Mn6A 120.26(19) 5_656 5_666
Mn6B Sb5 Mn6A 120.26(19) 5_666 5_656
Mn6B Sb5 Mn6A 27.2(2) 5_656 5_656
Mn6A Sb5 Mn6A 112.9(3) 5_666 5_656
Mn6B Sb5 Mn6B 74.55(11) 5_666 .
Mn6B Sb5 Mn6B 74.55(11) 5_656 .
Mn6A Sb5 Mn6B 101.6(2) 5_666 .
Mn6A Sb5 Mn6B 101.6(2) 5_656 .
Mn6B Sb5 Ca9 77.46(10) 5_666 .
Mn6B Sb5 Ca9 77.46(10) 5_656 .
Mn6A Sb5 Ca9 57.96(17) 5_666 .
Mn6A Sb5 Ca9 57.96(17) 5_656 .
Mn6B Sb5 Ca9 127.63(13) . .
Mn6B Sb5 Ca8 63.00(11) 5_666 5_666
Mn6B Sb5 Ca8 134.74(12) 5_656 5_666
Mn6A Sb5 Ca8 78.15(18) 5_666 5_666
Mn6A Sb5 Ca8 161.6(2) 5_656 5_666
Mn6B Sb5 Ca8 60.81(9) . 5_666
Ca9 Sb5 Ca8 135.95(6) . 5_666
Mn6B Sb5 Ca8 134.74(12) 5_666 5_656
Mn6B Sb5 Ca8 62.99(11) 5_656 5_656
Mn6A Sb5 Ca8 161.6(2) 5_666 5_656
Mn6A Sb5 Ca8 78.14(18) 5_656 5_656
Mn6B Sb5 Ca8 60.81(9) . 5_656
Ca9 Sb5 Ca8 135.95(6) . 5_656
Ca8 Sb5 Ca8 87.66(11) 5_666 5_656
Mn6B Sb5 Ca4 77.12(9) 5_666 5_666
Mn6B Sb5 Ca4 156.81(12) 5_656 5_666
Mn6A Sb5 Ca4 60.0(2) 5_666 5_666
Mn6A Sb5 Ca4 129.7(2) 5_656 5_666
Mn6B Sb5 Ca4 128.63(8) . 5_666
Ca9 Sb5 Ca4 85.35(10) . 5_666
Ca8 Sb5 Ca4 68.29(9) 5_666 5_666
Ca8 Sb5 Ca4 125.18(10) 5_656 5_666
Mn6B Sb5 Ca4 156.81(12) 5_666 5_656
Mn6B Sb5 Ca4 77.12(9) 5_656 5_656
Mn6A Sb5 Ca4 129.7(2) 5_666 5_656
Mn6A Sb5 Ca4 60.0(2) 5_656 5_656
Mn6B Sb5 Ca4 128.63(8) . 5_656
Ca9 Sb5 Ca4 85.35(10) . 5_656
Ca8 Sb5 Ca4 125.18(10) 5_666 5_656
Ca8 Sb5 Ca4 68.29(9) 5_656 5_656
Ca4 Sb5 Ca4 86.17(11) 5_666 5_656
Mn6B Sb5 Ca8 56.80(8) 5_666 .
Mn6B Sb5 Ca8 56.80(8) 5_656 .
Mn6A Sb5 Ca8 71.04(19) 5_666 .
Mn6A Sb5 Ca8 71.04(19) 5_656 .
Mn6B Sb5 Ca8 57.44(11) . .
Ca9 Sb5 Ca8 70.20(12) . .
Ca8 Sb5 Ca8 100.68(9) 5_666 .
Ca8 Sb5 Ca8 100.68(9) 5_656 .
Ca4 Sb5 Ca8 130.95(7) 5_666 .
Ca4 Sb5 Ca8 130.95(7) 5_656 .
Mn2 Sb6 Mn1 121.78(9) . .
Mn2 Sb6 Ca7 74.34(8) . 5_666
Mn1 Sb6 Ca7 66.17(7) . 5_666
Mn2 Sb6 Ca7 74.34(8) . 5_656
Mn1 Sb6 Ca7 66.17(7) . 5_656
Ca7 Sb6 Ca7 91.64(10) 5_666 5_656
Mn2 Sb6 Ca3 67.18(8) . 5_666
Mn1 Sb6 Ca3 134.44(5) . 5_666
Ca7 Sb6 Ca3 76.02(8) 5_666 5_666
Ca7 Sb6 Ca3 141.43(10) 5_656 5_666
Mn2 Sb6 Ca3 67.18(8) . 5_656
Mn1 Sb6 Ca3 134.44(5) . 5_656
Ca7 Sb6 Ca3 141.43(10) 5_666 5_656
Ca7 Sb6 Ca3 76.02(8) 5_656 5_656
Ca3 Sb6 Ca3 91.06(10) 5_666 5_656
Mn2 Sb6 Ca6 132.41(7) . 5_666
Mn1 Sb6 Ca6 79.31(10) . 5_666
Ca7 Sb6 Ca6 78.49(8) 5_666 5_666
Ca7 Sb6 Ca6 145.09(11) 5_656 5_666
Ca3 Sb6 Ca6 68.77(10) 5_666 5_666
Ca3 Sb6 Ca6 130.73(10) 5_656 5_666
Mn2 Sb6 Ca6 132.41(7) . 5_656
Mn1 Sb6 Ca6 79.31(10) . 5_656
Ca7 Sb6 Ca6 145.09(11) 5_666 5_656
Ca7 Sb6 Ca6 78.49(8) 5_656 5_656
Ca3 Sb6 Ca6 130.73(10) 5_666 5_656
Ca3 Sb6 Ca6 68.77(10) 5_656 5_656
Ca6 Sb6 Ca6 90.61(12) 5_666 5_656
Mn3 Sb7 Mn4 126.0(2) . 1_655
Mn3 Sb7 Mn5 157.7(2) . .
Mn4 Sb7 Mn5 76.37(16) 1_655 .
Mn3 Sb7 Ca1 139.84(12) . 3_656
Mn4 Sb7 Ca1 50.70(13) 1_655 3_656
Mn5 Sb7 Ca1 51.66(12) . 3_656
Mn3 Sb7 Ca1 139.84(11) . 5_656
Mn4 Sb7 Ca1 50.70(13) 1_655 5_656
Mn5 Sb7 Ca1 51.66(12) . 5_656
Ca1 Sb7 Ca1 74.21(19) 3_656 5_656
Mn3 Sb7 Ca5 82.81(13) . 5_666
Mn4 Sb7 Ca5 128.60(8) 1_655 5_666
Mn5 Sb7 Ca5 81.80(10) . 5_666
Ca1 Sb7 Ca5 79.33(12) 3_656 5_666
Ca1 Sb7 Ca5 133.36(13) 5_656 5_666
Mn3 Sb7 Ca5 82.81(13) . 5_656
Mn4 Sb7 Ca5 128.60(8) 1_655 5_656
Mn5 Sb7 Ca5 81.80(10) . 5_656
Ca1 Sb7 Ca5 133.36(13) 3_656 5_656
Ca1 Sb7 Ca5 79.33(12) 5_656 5_656
Ca5 Sb7 Ca5 92.52(10) 5_666 5_656
Mn3 Sb7 Ca2 62.46(12) . 5_666
Mn4 Sb7 Ca2 81.04(11) 1_655 5_666
Mn5 Sb7 Ca2 128.92(8) . 5_666
Ca1 Sb7 Ca2 78.65(12) 3_656 5_666
Ca1 Sb7 Ca2 131.51(13) 5_656 5_666
Ca5 Sb7 Ca2 77.66(8) 5_666 5_666
Ca5 Sb7 Ca2 144.67(11) 5_656 5_666
Mn3 Sb7 Ca2 62.46(12) . 5_656
Mn4 Sb7 Ca2 81.04(11) 1_655 5_656
Mn5 Sb7 Ca2 128.92(8) . 5_656
Ca1 Sb7 Ca2 131.51(13) 3_656 5_656
Ca1 Sb7 Ca2 78.65(12) 5_656 5_656
Ca5 Sb7 Ca2 144.67(11) 5_666 5_656
Ca5 Sb7 Ca2 77.66(8) 5_656 5_656
Ca2 Sb7 Ca2 90.87(10) 5_666 5_656
Mn3 Sb7 Ca1 131.13(10) . 5_666
Mn4 Sb7 Ca1 56.97(11) 1_655 5_666
Mn5 Sb7 Ca1 57.74(11) . 5_666
Ca1 Sb7 Ca1 9.55(13) 3_656 5_666
Ca1 Sb7 Ca1 83.76(13) 5_656 5_666
Ca5 Sb7 Ca1 71.96(10) 5_666 5_666
Ca5 Sb7 Ca1 137.83(12) 5_656 5_666
Ca2 Sb7 Ca1 71.48(11) 5_666 5_666
Ca2 Sb7 Ca1 135.94(12) 5_656 5_666
Mn3 Sb7 Ca1 131.13(10) . 3_646
Mn4 Sb7 Ca1 56.97(11) 1_655 3_646
Mn5 Sb7 Ca1 57.74(10) . 3_646
Ca1 Sb7 Ca1 83.76(13) 3_656 3_646
Ca1 Sb7 Ca1 9.55(13) 5_656 3_646
Ca5 Sb7 Ca1 137.83(12) 5_666 3_646
Ca5 Sb7 Ca1 71.96(10) 5_656 3_646
Ca2 Sb7 Ca1 135.94(12) 5_666 3_646
Ca2 Sb7 Ca1 71.48(11) 5_656 3_646
Ca1 Sb7 Ca1 93.31(17) 5_666 3_646
Mn4 Sb8 Mn4 109.58(18) 5_666 5_656
Mn4 Sb8 Mn2 124.69(9) 5_666 .
Mn4 Sb8 Mn2 124.68(9) 5_656 .
Mn4 Sb8 Ca3 70.57(11) 5_666 5_666
Mn4 Sb8 Ca3 149.22(13) 5_656 5_666
Mn2 Sb8 Ca3 68.37(8) . 5_666
Mn4 Sb8 Ca3 149.22(13) 5_666 5_656
Mn4 Sb8 Ca3 70.57(11) 5_656 5_656
Mn2 Sb8 Ca3 68.37(8) . 5_656
Ca3 Sb8 Ca3 93.66(11) 5_666 5_656
Mn4 Sb8 Ca1 49.04(13) 5_666 7_665
Mn4 Sb8 Ca1 62.68(13) 5_656 7_665
Mn2 Sb8 Ca1 156.55(12) . 7_665
Ca3 Sb8 Ca1 117.98(11) 5_666 7_665
Ca3 Sb8 Ca1 130.13(11) 5_656 7_665
Mn4 Sb8 Ca1 62.68(13) 5_666 1_655
Mn4 Sb8 Ca1 49.04(13) 5_656 1_655
Mn2 Sb8 Ca1 156.55(12) . 1_655
Ca3 Sb8 Ca1 130.13(12) 5_666 1_655
Ca3 Sb8 Ca1 117.98(11) 5_656 1_655
Ca1 Sb8 Ca1 13.81(18) 7_665 1_655
Mn4 Sb8 Ca4 59.28(12) 5_666 5_666
Mn4 Sb8 Ca4 129.26(13) 5_656 5_666
Mn2 Sb8 Ca4 77.41(8) . 5_666
Ca3 Sb8 Ca4 78.53(8) 5_666 5_666
Ca3 Sb8 Ca4 145.30(11) 5_656 5_666
Ca1 Sb8 Ca4 81.83(12) 7_665 5_666
Ca1 Sb8 Ca4 91.50(12) 1_655 5_666
Mn4 Sb8 Ca4 129.26(13) 5_666 5_656
Mn4 Sb8 Ca4 59.28(12) 5_656 5_656
Mn2 Sb8 Ca4 77.41(8) . 5_656
Ca3 Sb8 Ca4 145.30(11) 5_666 5_656
Ca3 Sb8 Ca4 78.53(8) 5_656 5_656
Ca1 Sb8 Ca4 91.50(12) 7_665 5_656
Ca1 Sb8 Ca4 81.83(12) 1_655 5_656
Ca4 Sb8 Ca4 88.84(11) 5_666 5_656
Mn4 Sb8 Ca2 74.71(11) 5_666 1_655
Mn4 Sb8 Ca2 74.71(11) 5_656 1_655
Mn2 Sb8 Ca2 126.47(9) . 1_655
Ca3 Sb8 Ca2 75.86(8) 5_666 1_655
Ca3 Sb8 Ca2 75.86(8) 5_656 1_655
Ca1 Sb8 Ca2 76.10(12) 7_665 1_655
Ca1 Sb8 Ca2 76.10(12) 1_655 1_655
Ca4 Sb8 Ca2 132.57(6) 5_666 1_655
Ca4 Sb8 Ca2 132.57(6) 5_656 1_655
Sb9B Sb9A Ca1 132.22(15) . 3_556
Sb9B Sb9A Ca1 132.22(15) . 5_556
Ca1 Sb9A Ca1 94.2(2) 3_556 5_556
Sb9B Sb9A Mn5 152.8(5) . 1_455
Ca1 Sb9A Mn5 56.70(14) 3_556 1_455
Ca1 Sb9A Mn5 56.70(14) 5_556 1_455
Sb9B Sb9A Mn4 137.7(5) . .
Ca1 Sb9A Mn4 55.30(14) 3_556 .
Ca1 Sb9A Mn4 55.30(14) 5_556 .
Mn5 Sb9A Mn4 69.43(16) 1_455 .
Sb9B Sb9A Ca1 123.07(12) . 5_566
Ca1 Sb9A Ca1 9.34(13) 3_556 5_566
Ca1 Sb9A Ca1 103.57(19) 5_556 5_566
Mn5 Sb9A Ca1 63.52(11) 1_455 5_566
Mn4 Sb9A Ca1 62.47(12) . 5_566
Sb9B Sb9A Ca1 123.07(12) . 3_546
Ca1 Sb9A Ca1 103.57(19) 3_556 3_546
Ca1 Sb9A Ca1 9.34(12) 5_556 3_546
Mn5 Sb9A Ca1 63.52(12) 1_455 3_546
Mn4 Sb9A Ca1 62.47(12) . 3_546
Ca1 Sb9A Ca1 112.9(2) 5_566 3_546
Sb9B Sb9A Ca4 77.8(5) . .
Ca1 Sb9A Ca4 92.17(15) 3_556 .
Ca1 Sb9A Ca4 92.17(15) 5_556 .
Mn5 Sb9A Ca4 129.40(16) 1_455 .
Mn4 Sb9A Ca4 59.97(14) . .
Ca1 Sb9A Ca4 91.76(12) 5_566 .
Ca1 Sb9A Ca4 91.76(12) 3_546 .
Sb9B Sb9A Ca9 92.2(5) . 1_455
Ca1 Sb9A Ca9 94.67(16) 3_556 1_455
Ca1 Sb9A Ca9 94.67(16) 5_556 1_455
Mn5 Sb9A Ca9 60.66(14) 1_455 1_455
Mn4 Sb9A Ca9 130.09(17) . 1_455
Ca1 Sb9A Ca9 93.79(13) 5_566 1_455
Ca1 Sb9A Ca9 93.79(13) 3_546 1_455
Ca4 Sb9A Ca9 169.94(16) . 1_455
Sb9B Sb9A Ca9 44.58(11) . 5_666
Ca1 Sb9A Ca9 88.96(13) 3_556 5_666
Ca1 Sb9A Ca9 176.78(16) 5_556 5_666
Mn5 Sb9A Ca9 125.79(11) 1_455 5_666
Mn4 Sb9A Ca9 126.82(11) . 5_666
Ca1 Sb9A Ca9 79.63(12) 5_566 5_666
Ca1 Sb9A Ca9 167.46(14) 3_546 5_666
Ca4 Sb9A Ca9 87.36(13) . 5_666
Ca9 Sb9A Ca9 85.40(13) 1_455 5_666
Sb9B Sb9A Ca9 44.58(11) . 5_656
Ca1 Sb9A Ca9 176.78(16) 3_556 5_656
Ca1 Sb9A Ca9 88.96(13) 5_556 5_656
Mn5 Sb9A Ca9 125.78(11) 1_455 5_656
Mn4 Sb9A Ca9 126.82(11) . 5_656
Ca1 Sb9A Ca9 167.46(14) 5_566 5_656
Ca1 Sb9A Ca9 79.62(11) 3_546 5_656
Ca4 Sb9A Ca9 87.36(13) . 5_656
Ca9 Sb9A Ca9 85.40(13) 1_455 5_656
Ca9 Sb9A Ca9 87.84(15) 5_666 5_656
Sb9A Sb9B Ca9 126.55(13) . 5_666
Sb9A Sb9B Ca9 126.55(13) . 5_656
Ca9 Sb9B Ca9 105.1(2) 5_666 5_656
Sb9A Sb9B Mn6A 152.3(6) . .
Ca9 Sb9B Mn6A 61.96(15) 5_666 .
Ca9 Sb9B Mn6A 61.96(15) 5_656 .
Sb9A Sb9B Ca1 38.97(13) . 3_556
Ca9 Sb9B Ca1 88.86(13) 5_666 3_556
Ca9 Sb9B Ca1 165.52(17) 5_656 3_556
Mn6A Sb9B Ca1 130.24(18) . 3_556
Sb9A Sb9B Ca1 38.97(13) . 5_556
Ca9 Sb9B Ca1 165.52(17) 5_666 5_556
Ca9 Sb9B Ca1 88.86(13) 5_656 5_556
Mn6A Sb9B Ca1 130.24(17) . 5_556
Ca1 Sb9B Ca1 77.0(2) 3_556 5_556
Sb9A Sb9B Ca4 90.9(5) . .
Ca9 Sb9B Ca4 96.50(15) 5_666 .
Ca9 Sb9B Ca4 96.50(15) 5_656 .
Mn6A Sb9B Ca4 61.4(2) . .
Ca1 Sb9B Ca4 85.50(16) 3_556 .
Ca1 Sb9B Ca4 85.50(16) 5_556 .
Sb9A Sb9B Ca9 76.8(5) . 1_455
Ca9 Sb9B Ca9 90.93(15) 5_666 1_455
Ca9 Sb9B Ca9 90.93(15) 5_656 1_455
Mn6A Sb9B Ca9 130.9(3) . 1_455
Ca1 Sb9B Ca9 84.92(16) 3_556 1_455
Ca1 Sb9B Ca9 84.92(16) 5_556 1_455
Ca4 Sb9B Ca9 167.75(19) . 1_455
Sb9A Sb9B Ca1 48.42(11) . 5_566
Ca9 Sb9B Ca1 79.28(12) 5_666 5_566
Ca9 Sb9B Ca1 174.52(18) 5_656 5_566
Mn6A Sb9B Ca1 123.46(14) . 5_566
Ca1 Sb9B Ca1 9.59(13) 3_556 5_566
Ca1 Sb9B Ca1 86.56(16) 5_556 5_566
Ca4 Sb9B Ca1 86.16(13) . 5_566
Ca9 Sb9B Ca1 85.66(13) 1_455 5_566
Sb9A Sb9B Ca1 48.42(12) . 3_546
Ca9 Sb9B Ca1 174.52(18) 5_666 3_546
Ca9 Sb9B Ca1 79.28(12) 5_656 3_546
Mn6A Sb9B Ca1 123.46(14) . 3_546
Ca1 Sb9B Ca1 86.56(16) 3_556 3_546
Ca1 Sb9B Ca1 9.59(13) 5_556 3_546
Ca4 Sb9B Ca1 86.16(13) . 3_546
Ca9 Sb9B Ca1 85.66(13) 1_455 3_546
Ca1 Sb9B Ca1 96.2(2) 5_566 3_546
Sb4 Mn1 Sb4 114.10(10) 5_666 5_656
Sb4 Mn1 Sb2 113.18(7) 5_666 .
Sb4 Mn1 Sb2 113.18(7) 5_656 .
Sb4 Mn1 Sb6 108.54(7) 5_666 .
Sb4 Mn1 Sb6 108.54(7) 5_656 .
Sb2 Mn1 Sb6 97.85(9) . .
Sb4 Mn1 Ca7 79.09(5) 5_666 5_666
Sb4 Mn1 Ca7 166.37(9) 5_656 5_666
Sb2 Mn1 Ca7 61.42(8) . 5_666
Sb6 Mn1 Ca7 61.94(7) . 5_666
Sb4 Mn1 Ca7 166.37(9) 5_666 5_656
Sb4 Mn1 Ca7 79.09(5) 5_656 5_656
Sb2 Mn1 Ca7 61.42(8) . 5_656
Sb6 Mn1 Ca7 61.94(7) . 5_656
Ca7 Mn1 Ca7 87.55(11) 5_666 5_656
Sb4 Mn1 Ca2 58.00(5) 5_666 6_656
Sb4 Mn1 Ca2 58.00(5) 5_656 6_656
Sb2 Mn1 Ca2 149.40(12) . 6_656
Sb6 Mn1 Ca2 112.75(11) . 6_656
Ca7 Mn1 Ca2 133.40(7) 5_666 6_656
Ca7 Mn1 Ca2 133.40(7) 5_656 6_656
Sb3 Mn2 Sb3 113.39(10) 5_666 5_656
Sb3 Mn2 Sb8 110.33(7) 5_666 .
Sb3 Mn2 Sb8 110.33(7) 5_656 .
Sb3 Mn2 Sb6 112.12(7) 5_666 .
Sb3 Mn2 Sb6 112.12(7) 5_656 .
Sb8 Mn2 Sb6 97.47(9) . .
Sb3 Mn2 Ca3 80.20(5) 5_666 5_666
Sb3 Mn2 Ca3 166.23(9) 5_656 5_666
Sb8 Mn2 Ca3 60.51(8) . 5_666
Sb6 Mn2 Ca3 61.89(8) . 5_666
Sb3 Mn2 Ca3 166.23(9) 5_666 5_656
Sb3 Mn2 Ca3 80.20(5) 5_656 5_656
Sb8 Mn2 Ca3 60.51(8) . 5_656
Sb6 Mn2 Ca3 61.89(8) . 5_656
Ca3 Mn2 Ca3 86.14(11) 5_666 5_656
Sb3 Mn2 Ca7 56.84(6) 5_666 5_666
Sb3 Mn2 Ca7 120.16(10) 5_656 5_666
Sb8 Mn2 Ca7 128.87(8) . 5_666
Sb6 Mn2 Ca7 57.45(7) . 5_666
Ca3 Mn2 Ca7 68.39(8) 5_666 5_666
Ca3 Mn2 Ca7 119.29(11) 5_656 5_666
Sb3 Mn2 Ca7 120.16(10) 5_666 5_656
Sb3 Mn2 Ca7 56.84(6) 5_656 5_656
Sb8 Mn2 Ca7 128.87(8) . 5_656
Sb6 Mn2 Ca7 57.45(7) . 5_656
Ca3 Mn2 Ca7 119.29(11) 5_666 5_656
Ca3 Mn2 Ca7 68.39(8) 5_656 5_656
Ca7 Mn2 Ca7 77.78(9) 5_666 5_656
Sb3 Mn2 Ca5 60.29(6) 5_666 .
Sb3 Mn2 Ca5 60.29(6) 5_656 .
Sb8 Mn2 Ca5 154.75(11) . .
Sb6 Mn2 Ca5 107.78(10) . .
Ca3 Mn2 Ca5 132.49(7) 5_666 .
Ca3 Mn2 Ca5 132.49(7) 5_656 .
Ca7 Mn2 Ca5 68.20(8) 5_666 .
Ca7 Mn2 Ca5 68.20(8) 5_656 .
Sb7 Mn3 Sb2 113.21(16) . 5_666
Sb7 Mn3 Sb2 113.21(16) . 5_656
Sb2 Mn3 Sb2 116.3(2) 5_666 5_656
Sb7 Mn3 Ca6 168.5(3) . 6_657
Sb2 Mn3 Ca6 71.56(15) 5_666 6_657
Sb2 Mn3 Ca6 71.56(15) 5_656 6_657
Sb7 Mn3 Ca2 71.16(15) . 5_666
Sb2 Mn3 Ca2 71.27(7) 5_666 5_666
Sb2 Mn3 Ca2 166.1(3) 5_656 5_666
Ca6 Mn3 Ca2 101.79(19) 6_657 5_666
Sb7 Mn3 Ca2 71.16(15) . 5_656
Sb2 Mn3 Ca2 166.1(3) 5_666 5_656
Sb2 Mn3 Ca2 71.27(7) 5_656 5_656
Ca6 Mn3 Ca2 101.79(19) 6_657 5_656
Ca2 Mn3 Ca2 99.0(2) 5_666 5_656
Sb7 Mn3 Ca7 110.9(2) . .
Sb2 Mn3 Ca7 62.07(12) 5_666 .
Sb2 Mn3 Ca7 62.07(12) 5_656 .
Ca6 Mn3 Ca7 80.55(19) 6_657 .
Ca2 Mn3 Ca7 129.91(11) 5_666 .
Ca2 Mn3 Ca7 129.91(12) 5_656 .
Sb7 Mn3 Ca5 56.75(13) . 5_666
Sb2 Mn3 Ca5 59.85(10) 5_666 5_666
Sb2 Mn3 Ca5 122.2(2) 5_656 5_666
Ca6 Mn3 Ca5 130.65(15) 6_657 5_666
Ca2 Mn3 Ca5 71.50(11) 5_666 5_666
Ca2 Mn3 Ca5 127.5(2) 5_656 5_666
Ca7 Mn3 Ca5 70.16(14) . 5_666
Sb7 Mn3 Ca5 56.75(13) . 5_656
Sb2 Mn3 Ca5 122.2(2) 5_666 5_656
Sb2 Mn3 Ca5 59.85(10) 5_656 5_656
Ca6 Mn3 Ca5 130.65(15) 6_657 5_656
Ca2 Mn3 Ca5 127.5(2) 5_666 5_656
Ca2 Mn3 Ca5 71.50(11) 5_656 5_656
Ca7 Mn3 Ca5 70.16(14) . 5_656
Ca5 Mn3 Ca5 75.03(14) 5_666 5_656
Ca1 Mn4 Ca1 99.1(3) 3_556 5_556
Ca1 Mn4 Sb7 77.56(18) 3_556 1_455
Ca1 Mn4 Sb7 77.56(18) 5_556 1_455
Ca1 Mn4 Sb9A 58.66(17) 3_556 .
Ca1 Mn4 Sb9A 58.66(17) 5_556 .
Sb7 Mn4 Sb9A 107.27(19) 1_455 .
Ca1 Mn4 Sb8 73.33(13) 3_556 5_666
Ca1 Mn4 Sb8 163.1(3) 5_556 5_666
Sb7 Mn4 Sb8 114.39(12) 1_455 5_666
Sb9A Mn4 Sb8 105.17(13) . 5_666
Ca1 Mn4 Sb8 163.1(3) 3_556 5_656
Ca1 Mn4 Sb8 73.33(13) 5_556 5_656
Sb7 Mn4 Sb8 114.39(12) 1_455 5_656
Sb9A Mn4 Sb8 105.17(13) . 5_656
Sb8 Mn4 Sb8 109.58(18) 5_666 5_656
Ca1 Mn4 Ca4 99.0(2) 3_556 .
Ca1 Mn4 Ca4 99.02(19) 5_556 .
Sb7 Mn4 Ca4 174.6(2) 1_455 .
Sb9A Mn4 Ca4 67.32(15) . .
Sb8 Mn4 Ca4 68.09(11) 5_666 .
Sb8 Mn4 Ca4 68.09(11) 5_656 .
Ca1 Mn4 Ca1 9.12(12) 3_556 5_566
Ca1 Mn4 Ca1 108.3(3) 5_556 5_566
Sb7 Mn4 Ca1 80.06(15) 1_455 5_566
Sb9A Mn4 Ca1 65.37(14) . 5_566
Sb8 Mn4 Ca1 64.56(11) 5_666 5_566
Sb8 Mn4 Ca1 165.1(2) 5_656 5_566
Ca4 Mn4 Ca1 97.22(16) . 5_566
Ca1 Mn4 Ca1 108.3(3) 3_556 3_546
Ca1 Mn4 Ca1 9.12(12) 5_556 3_546
Sb7 Mn4 Ca1 80.06(15) 1_455 3_546
Sb9A Mn4 Ca1 65.37(14) . 3_546
Sb8 Mn4 Ca1 165.1(2) 5_666 3_546
Sb8 Mn4 Ca1 64.56(11) 5_656 3_546
Ca4 Mn4 Ca1 97.22(15) . 3_546
Ca1 Mn4 Ca1 117.4(3) 5_566 3_546
Ca1 Mn4 Mn5 52.01(16) 3_556 1_455
Ca1 Mn4 Mn5 52.01(16) 5_556 1_455
Sb7 Mn4 Mn5 52.25(13) 1_455 1_455
Sb9A Mn4 Mn5 55.02(14) . 1_455
Sb8 Mn4 Mn5 124.82(9) 5_666 1_455
Sb8 Mn4 Mn5 124.82(9) 5_656 1_455
Ca4 Mn4 Mn5 122.3(2) . 1_455
Ca1 Mn4 Mn5 60.45(14) 5_566 1_455
Ca1 Mn4 Mn5 60.45(13) 3_546 1_455
Ca1 Mn4 Ca3 130.41(16) 3_556 .
Ca1 Mn4 Ca3 130.41(16) 5_556 .
Sb7 Mn4 Ca3 108.05(18) 1_455 .
Sb9A Mn4 Ca3 144.7(2) . .
Sb8 Mn4 Ca3 59.30(10) 5_666 .
Sb8 Mn4 Ca3 59.30(10) 5_656 .
Ca4 Mn4 Ca3 77.35(15) . .
Ca1 Mn4 Ca3 121.30(13) 5_566 .
Ca1 Mn4 Ca3 121.30(13) 3_546 .
Mn5 Mn4 Ca3 160.3(2) 1_455 .
Ca1 Mn4 Ca2 77.18(15) 3_556 5_566
Ca1 Mn4 Ca2 134.6(2) 5_556 5_566
Sb7 Mn4 Ca2 57.26(10) 1_455 5_566
Sb9A Mn4 Ca2 135.80(11) . 5_566
Sb8 Mn4 Ca2 59.54(9) 5_666 5_566
Sb8 Mn4 Ca2 118.98(17) 5_656 5_566
Ca4 Mn4 Ca2 126.39(14) . 5_566
Ca1 Mn4 Ca2 70.97(12) 5_566 5_566
Ca1 Mn4 Ca2 135.28(19) 3_546 5_566
Mn5 Mn4 Ca2 97.45(15) 1_455 5_566
Ca3 Mn4 Ca2 67.27(11) . 5_566
Ca1 Mn5 Ca1 96.6(3) 3_656 5_656
Ca1 Mn5 Sb7 76.14(17) 3_656 .
Ca1 Mn5 Sb7 76.14(17) 5_656 .
Ca1 Mn5 Sb1 74.21(13) 3_656 5_666
Ca1 Mn5 Sb1 164.9(2) 5_656 5_666
Sb7 Mn5 Sb1 112.26(12) . 5_666
Ca1 Mn5 Sb1 164.9(2) 3_656 5_656
Ca1 Mn5 Sb1 74.21(13) 5_656 5_656
Sb7 Mn5 Sb1 112.26(12) . 5_656
Sb1 Mn5 Sb1 111.90(17) 5_666 5_656
Ca1 Mn5 Sb9A 58.40(15) 3_656 1_655
Ca1 Mn5 Sb9A 58.40(16) 5_656 1_655
Sb7 Mn5 Sb9A 106.91(18) . 1_655
Sb1 Mn5 Sb9A 106.51(12) 5_666 1_655
Sb1 Mn5 Sb9A 106.51(12) 5_656 1_655
Ca1 Mn5 Ca9 100.09(19) 3_656 .
Ca1 Mn5 Ca9 100.09(19) 5_656 .
Sb7 Mn5 Ca9 174.2(2) . .
Sb1 Mn5 Ca9 70.43(11) 5_666 .
Sb1 Mn5 Ca9 70.43(11) 5_656 .
Sb9A Mn5 Ca9 67.24(16) 1_655 .
Ca1 Mn5 Mn4 50.63(15) 3_656 1_655
Ca1 Mn5 Mn4 50.63(15) 5_656 1_655
Sb7 Mn5 Mn4 51.37(13) . 1_655
Sb1 Mn5 Mn4 123.96(9) 5_666 1_655
Sb1 Mn5 Mn4 123.96(9) 5_656 1_655
Sb9A Mn5 Mn4 55.54(14) 1_655 1_655
Ca9 Mn5 Mn4 122.8(2) . 1_655
Ca1 Mn5 Ca1 9.24(12) 3_656 5_666
Ca1 Mn5 Ca1 105.9(2) 5_656 5_666
Sb7 Mn5 Ca1 78.86(14) . 5_666
Sb1 Mn5 Ca1 65.20(11) 5_666 5_666
Sb1 Mn5 Ca1 168.2(2) 5_656 5_666
Sb9A Mn5 Ca1 64.99(13) 1_655 5_666
Ca9 Mn5 Ca1 98.12(15) . 5_666
Mn4 Mn5 Ca1 59.22(13) 1_655 5_666
Ca1 Mn5 Ca1 105.8(2) 3_656 3_646
Ca1 Mn5 Ca1 9.24(13) 5_656 3_646
Sb7 Mn5 Ca1 78.86(14) . 3_646
Sb1 Mn5 Ca1 168.2(2) 5_666 3_646
Sb1 Mn5 Ca1 65.19(11) 5_656 3_646
Sb9A Mn5 Ca1 64.99(13) 1_655 3_646
Ca9 Mn5 Ca1 98.12(15) . 3_646
Mn4 Mn5 Ca1 59.22(13) 1_655 3_646
Ca1 Mn5 Ca1 115.1(2) 5_666 3_646
Ca1 Mn5 Ca8 131.70(14) 3_656 .
Ca1 Mn5 Ca8 131.69(15) 5_656 .
Sb7 Mn5 Ca8 111.12(17) . .
Sb1 Mn5 Ca8 58.59(9) 5_666 .
Sb1 Mn5 Ca8 58.59(9) 5_656 .
Sb9A Mn5 Ca8 141.97(19) 1_655 .
Ca9 Mn5 Ca8 74.72(17) . .
Mn4 Mn5 Ca8 162.5(2) 1_655 .
Ca1 Mn5 Ca8 122.46(12) 5_666 .
Ca1 Mn5 Ca8 122.45(13) 3_646 .
Ca1 Mn5 Ca5 76.45(15) 3_656 5_666
Ca1 Mn5 Ca5 132.0(2) 5_656 5_666
Sb7 Mn5 Ca5 55.93(10) . 5_666
Sb1 Mn5 Ca5 58.52(8) 5_666 5_666
Sb1 Mn5 Ca5 118.67(16) 5_656 5_666
Sb9A Mn5 Ca5 134.80(11) 1_655 5_666
Ca9 Mn5 Ca5 127.94(14) . 5_666
Mn4 Mn5 Ca5 95.31(14) 1_655 5_666
Ca1 Mn5 Ca5 70.42(12) 5_666 5_666
Ca1 Mn5 Ca5 133.27(18) 3_646 5_666
Ca8 Mn5 Ca5 70.96(11) . 5_666
Mn6B Mn6A Sb1 81.8(5) . .
Mn6B Mn6A Sb5 76.1(3) . 5_666
Sb1 Mn6A Sb5 117.3(2) . 5_666
Mn6B Mn6A Sb5 76.1(3) . 5_656
Sb1 Mn6A Sb5 117.3(2) . 5_656
Sb5 Mn6A Sb5 112.9(3) 5_666 5_656
Mn6B Mn6A Sb9B 179.0(6) . .
Sb1 Mn6A Sb9B 99.1(3) . .
Sb5 Mn6A Sb9B 103.4(2) 5_666 .
Sb5 Mn6A Sb9B 103.4(2) 5_656 .
Mn6B Mn6A Ca9 121.5(3) . 5_666
Sb1 Mn6A Ca9 73.3(2) . 5_666
Sb5 Mn6A Ca9 70.44(10) 5_666 5_666
Sb5 Mn6A Ca9 161.8(4) 5_656 5_666
Sb9B Mn6A Ca9 58.96(19) . 5_666
Mn6B Mn6A Ca9 121.5(3) . 5_656
Sb1 Mn6A Ca9 73.3(2) . 5_656
Sb5 Mn6A Ca9 161.8(4) 5_666 5_656
Sb5 Mn6A Ca9 70.44(10) 5_656 5_656
Sb9B Mn6A Ca9 58.96(19) . 5_656
Ca9 Mn6A Ca9 100.8(3) 5_666 5_656
Mn6B Mn6A Ca4 115.4(6) . .
Sb1 Mn6A Ca4 162.8(4) . .
Sb5 Mn6A Ca4 69.8(2) 5_666 .
Sb5 Mn6A Ca4 69.8(2) 5_656 .
Sb9B Mn6A Ca4 63.6(2) . .
Ca9 Mn6A Ca4 96.1(2) 5_666 .
Ca9 Mn6A Ca4 96.1(2) 5_656 .
Mn6B Mn6A Ca8 51.0(3) . 5_666
Sb1 Mn6A Ca8 55.08(16) . 5_666
Sb5 Mn6A Ca8 65.60(14) 5_666 5_666
Sb5 Mn6A Ca8 126.6(3) 5_656 5_666
Sb9B Mn6A Ca8 129.6(2) . 5_666
Ca9 Mn6A Ca8 71.55(16) 5_666 5_666
Ca9 Mn6A Ca8 128.0(3) 5_656 5_666
Ca4 Mn6A Ca8 135.29(19) . 5_666
Mn6B Mn6A Ca8 51.0(3) . 5_656
Sb1 Mn6A Ca8 55.08(16) . 5_656
Sb5 Mn6A Ca8 126.6(3) 5_666 5_656
Sb5 Mn6A Ca8 65.60(14) 5_656 5_656
Sb9B Mn6A Ca8 129.6(2) . 5_656
Ca9 Mn6A Ca8 128.0(3) 5_666 5_656
Ca9 Mn6A Ca8 71.55(16) 5_656 5_656
Ca4 Mn6A Ca8 135.29(19) . 5_656
Ca8 Mn6A Ca8 74.48(19) 5_666 5_656
Mn6A Mn6B Sb5 76.8(3) . 5_666
Mn6A Mn6B Sb5 76.8(3) . 5_656
Sb5 Mn6B Sb5 113.45(16) 5_666 5_656
Mn6A Mn6B Sb1 70.9(5) . .
Sb5 Mn6B Sb1 113.34(10) 5_666 .
Sb5 Mn6B Sb1 113.34(10) 5_656 .
Mn6A Mn6B Sb5 175.6(5) . .
Sb5 Mn6B Sb5 105.45(11) 5_666 .
Sb5 Mn6B Sb5 105.45(11) 5_656 .
Sb1 Mn6B Sb5 104.72(14) . .
Mn6A Mn6B Ca8 110.4(3) . 5_666
Sb5 Mn6B Ca8 76.30(7) 5_666 5_666
Sb5 Mn6B Ca8 169.48(15) 5_656 5_666
Sb1 Mn6B Ca8 63.77(11) . 5_666
Sb5 Mn6B Ca8 66.90(11) . 5_666
Mn6A Mn6B Ca8 110.4(3) . 5_656
Sb5 Mn6B Ca8 169.48(15) 5_666 5_656
Sb5 Mn6B Ca8 76.30(7) 5_656 5_656
Sb1 Mn6B Ca8 63.77(11) . 5_656
Sb5 Mn6B Ca8 66.90(11) . 5_656
Ca8 Mn6B Ca8 93.72(16) 5_666 5_656
Mn6A Mn6B Ca8 110.5(5) . .
Sb5 Mn6B Ca8 67.21(9) 5_666 .
Sb5 Mn6B Ca8 67.21(9) 5_656 .
Sb1 Mn6B Ca8 178.67(19) . .
Sb5 Mn6B Ca8 73.96(13) . .
Ca8 Mn6B Ca8 115.45(13) 5_666 .
Ca8 Mn6B Ca8 115.45(12) 5_656 .
Ca1 Ca1 Mn4 139.56(16) 7_565 5_556
Ca1 Ca1 Mn5 138.31(15) 7_565 5_656
Mn4 Ca1 Mn5 77.35(19) 5_556 5_656
Ca1 Ca1 Sb9A 137.13(13) 7_565 5_556
Mn4 Ca1 Sb9A 66.04(17) 5_556 5_556
Mn5 Ca1 Sb9A 64.91(16) 5_656 5_556
Ca1 Ca1 Sb9B 128.50(11) 7_565 5_556
Mn4 Ca1 Sb9B 71.39(18) 5_556 5_556
Mn5 Ca1 Sb9B 72.39(17) 5_656 5_556
Sb9A Ca1 Sb9B 8.81(5) 5_556 5_556
Ca1 Ca1 Mn4 31.29(13) 7_565 5_566
Mn4 Ca1 Mn4 108.3(3) 5_556 5_566
Mn5 Ca1 Mn4 156.6(3) 5_656 5_566
Sb9A Ca1 Mn4 138.4(2) 5_556 5_566
Sb9B Ca1 Mn4 131.0(2) 5_556 5_566
Ca1 Ca1 Sb7 127.09(9) 7_565 5_656
Mn4 Ca1 Sb7 51.73(15) 5_556 5_656
Mn5 Ca1 Sb7 52.19(15) 5_656 5_656
Sb9A Ca1 Sb7 95.76(16) 5_556 5_656
Sb9B Ca1 Sb7 104.41(15) 5_556 5_656
Mn4 Ca1 Sb7 112.77(19) 5_566 5_656
Ca1 Ca1 Mn5 32.46(13) 7_565 5_666
Mn4 Ca1 Mn5 157.6(3) 5_556 5_666
Mn5 Ca1 Mn5 105.8(2) 5_656 5_666
Sb9A Ca1 Mn5 135.9(2) 5_556 5_666
Sb9B Ca1 Mn5 131.0(2) 5_556 5_666
Mn4 Ca1 Mn5 60.33(15) 5_566 5_666
Sb7 Ca1 Mn5 112.20(18) 5_656 5_666
Ca1 Ca1 Sb8 83.09(9) 7_565 1_455
Mn4 Ca1 Sb8 57.63(15) 5_556 1_455
Mn5 Ca1 Sb8 134.3(2) 5_656 1_455
Sb9A Ca1 Sb8 99.80(18) 5_556 1_455
Sb9B Ca1 Sb8 97.89(17) 5_556 1_455
Mn4 Ca1 Sb8 52.77(12) 5_566 1_455
Sb7 Ca1 Sb8 90.27(15) 5_656 1_455
Mn5 Ca1 Sb8 112.94(17) 5_666 1_455
Ca1 Ca1 Sb9A 33.55(10) 7_565 5_566
Mn4 Ca1 Sb9A 139.3(2) 5_556 5_566
Mn5 Ca1 Sb9A 136.2(2) 5_656 5_566
Sb9A Ca1 Sb9A 103.58(19) 5_556 5_566
Sb9B Ca1 Sb9A 94.96(17) 5_556 5_566
Mn4 Ca1 Sb9A 52.17(13) 5_566 5_566
Sb7 Ca1 Sb9A 160.60(19) 5_656 5_566
Mn5 Ca1 Sb9A 51.49(12) 5_666 5_566
Sb8 Ca1 Sb9A 88.08(14) 1_455 5_566
Ca1 Ca1 Sb1 83.17(9) 7_565 .
Mn4 Ca1 Sb1 132.1(2) 5_556 .
Mn5 Ca1 Sb1 55.87(14) 5_656 .
Sb9A Ca1 Sb1 98.77(18) 5_556 .
Sb9B Ca1 Sb1 100.43(17) 5_556 .
Mn4 Ca1 Sb1 111.31(18) 5_566 .
Sb7 Ca1 Sb1 88.10(14) 5_656 .
Mn5 Ca1 Sb1 51.34(11) 5_666 .
Sb8 Ca1 Sb1 161.43(18) 1_455 .
Sb9A Ca1 Sb1 87.35(14) 5_566 .
Ca1 Ca1 Sb9B 41.94(10) 7_565 5_566
Mn4 Ca1 Sb9B 134.3(2) 5_556 5_566
Mn5 Ca1 Sb9B 133.9(2) 5_656 5_566
Sb9A Ca1 Sb9B 95.22(18) 5_556 5_566
Sb9B Ca1 Sb9B 86.56(16) 5_556 5_566
Mn4 Ca1 Sb9B 58.00(14) 5_566 5_566
Sb7 Ca1 Sb9B 169.03(18) 5_656 5_566
Mn5 Ca1 Sb9B 58.93(13) 5_666 5_566
Sb8 Ca1 Sb9B 87.93(14) 1_455 5_566
Sb9A Ca1 Sb9B 8.50(4) 5_566 5_566
Sb1 Ca1 Sb9B 90.16(14) . 5_566
Mn3 Ca2 Mn3 99.0(2) 5_666 5_656
Mn3 Ca2 Sb7 46.38(13) 5_666 5_666
Mn3 Ca2 Sb7 113.18(17) 5_656 5_666
Mn3 Ca2 Sb7 113.18(17) 5_666 5_656
Mn3 Ca2 Sb7 46.38(13) 5_656 5_656
Sb7 Ca2 Sb7 90.87(10) 5_666 5_656
Mn3 Ca2 Sb4 62.79(13) 5_666 2_564
Mn3 Ca2 Sb4 128.51(18) 5_656 2_564
Sb7 Ca2 Sb4 89.02(3) 5_666 2_564
Sb7 Ca2 Sb4 173.99(15) 5_656 2_564
Mn3 Ca2 Sb4 128.51(18) 5_666 2_554
Mn3 Ca2 Sb4 62.79(13) 5_656 2_554
Sb7 Ca2 Sb4 173.99(15) 5_666 2_554
Sb7 Ca2 Sb4 89.02(3) 5_656 2_554
Sb4 Ca2 Sb4 90.47(10) 2_564 2_554
Mn3 Ca2 Sb2 49.95(11) 5_666 .
Mn3 Ca2 Sb2 49.95(11) 5_656 .
Sb7 Ca2 Sb2 82.18(9) 5_666 .
Sb7 Ca2 Sb2 82.18(8) 5_656 .
Sb4 Ca2 Sb2 91.85(9) 2_564 .
Sb4 Ca2 Sb2 91.85(9) 2_554 .
Mn3 Ca2 Sb8 126.17(12) 5_666 1_455
Mn3 Ca2 Sb8 126.17(12) 5_656 1_455
Sb7 Ca2 Sb8 86.01(9) 5_666 1_455
Sb7 Ca2 Sb8 86.01(9) 5_656 1_455
Sb4 Ca2 Sb8 99.97(9) 2_564 1_455
Sb4 Ca2 Sb8 99.97(9) 2_554 1_455
Sb2 Ca2 Sb8 163.13(13) . 1_455
Mn3 Ca2 Mn1 91.26(16) 5_666 6_556
Mn3 Ca2 Mn1 91.26(16) 5_656 6_556
Sb7 Ca2 Mn1 132.14(6) 5_666 6_556
Sb7 Ca2 Mn1 132.14(6) 5_656 6_556
Sb4 Ca2 Mn1 45.85(5) 2_564 6_556
Sb4 Ca2 Mn1 45.85(5) 2_554 6_556
Sb2 Ca2 Mn1 84.16(10) . 6_556
Sb8 Ca2 Mn1 112.72(12) 1_455 6_556
Mn3 Ca2 Mn4 81.22(13) 5_666 5_566
Mn3 Ca2 Mn4 140.36(19) 5_656 5_566
Sb7 Ca2 Mn4 41.70(9) 5_666 5_566
Sb7 Ca2 Mn4 96.76(12) 5_656 5_566
Sb4 Ca2 Mn4 87.14(8) 2_564 5_566
Sb4 Ca2 Mn4 144.24(15) 2_554 5_566
Sb2 Ca2 Mn4 123.87(11) . 5_566
Sb8 Ca2 Mn4 45.75(8) 1_455 5_566
Mn1 Ca2 Mn4 128.37(11) 6_556 5_566
Mn3 Ca2 Mn4 140.36(19) 5_666 5_556
Mn3 Ca2 Mn4 81.22(13) 5_656 5_556
Sb7 Ca2 Mn4 96.76(12) 5_666 5_556
Sb7 Ca2 Mn4 41.70(9) 5_656 5_556
Sb4 Ca2 Mn4 144.24(15) 2_564 5_556
Sb4 Ca2 Mn4 87.14(8) 2_554 5_556
Sb2 Ca2 Mn4 123.87(11) . 5_556
Sb8 Ca2 Mn4 45.75(8) 1_455 5_556
Mn1 Ca2 Mn4 128.37(11) 6_556 5_556
Mn4 Ca2 Mn4 74.70(12) 5_566 5_556
Mn3 Ca2 Ca5 62.98(14) 5_666 .
Mn3 Ca2 Ca5 62.98(14) 5_656 .
Sb7 Ca2 Ca5 50.67(6) 5_666 .
Sb7 Ca2 Ca5 50.67(6) 5_656 .
Sb4 Ca2 Ca5 125.73(8) 2_564 .
Sb4 Ca2 Ca5 125.73(8) 2_554 .
Sb2 Ca2 Ca5 53.39(8) . .
Sb8 Ca2 Ca5 109.74(12) 1_455 .
Mn1 Ca2 Ca5 137.55(13) 6_556 .
Mn4 Ca2 Ca5 82.95(11) 5_566 .
Mn4 Ca2 Ca5 82.95(11) 5_556 .
Sb8 Ca3 Sb8 93.66(11) 5_666 5_656
Sb8 Ca3 Sb4 106.45(9) 5_666 6_557
Sb8 Ca3 Sb4 106.45(9) 5_656 6_557
Sb8 Ca3 Sb6 83.65(4) 5_666 5_666
Sb8 Ca3 Sb6 158.47(14) 5_656 5_666
Sb4 Ca3 Sb6 94.76(9) 6_557 5_666
Sb8 Ca3 Sb6 158.47(14) 5_666 5_656
Sb8 Ca3 Sb6 83.65(4) 5_656 5_656
Sb4 Ca3 Sb6 94.76(9) 6_557 5_656
Sb6 Ca3 Sb6 91.06(10) 5_666 5_656
Sb8 Ca3 Mn2 51.12(6) 5_666 5_666
Sb8 Ca3 Mn2 111.62(12) 5_656 5_666
Sb4 Ca3 Mn2 136.11(6) 6_557 5_666
Sb6 Ca3 Mn2 50.93(6) 5_666 5_666
Sb6 Ca3 Mn2 110.14(12) 5_656 5_666
Sb8 Ca3 Mn2 111.62(12) 5_666 5_656
Sb8 Ca3 Mn2 51.12(6) 5_656 5_656
Sb4 Ca3 Mn2 136.11(6) 6_557 5_656
Sb6 Ca3 Mn2 110.14(12) 5_666 5_656
Sb6 Ca3 Mn2 50.93(6) 5_656 5_656
Mn2 Ca3 Mn2 86.14(11) 5_666 5_656
Sb8 Ca3 Mn4 50.13(6) 5_666 .
Sb8 Ca3 Mn4 50.13(6) 5_656 .
Sb4 Ca3 Mn4 94.00(14) 6_557 .
Sb6 Ca3 Mn4 133.48(6) 5_666 .
Sb6 Ca3 Mn4 133.48(6) 5_656 .
Mn2 Ca3 Mn4 93.96(11) 5_666 .
Mn2 Ca3 Mn4 93.96(11) 5_656 .
Sb8 Ca3 Ca6 132.94(6) 5_666 .
Sb8 Ca3 Ca6 132.94(6) 5_656 .
Sb4 Ca3 Ca6 60.20(10) 6_557 .
Sb6 Ca3 Ca6 55.77(7) 5_666 .
Sb6 Ca3 Ca6 55.77(7) 5_656 .
Mn2 Ca3 Ca6 104.73(11) 5_666 .
Mn2 Ca3 Ca6 104.73(11) 5_656 .
Mn4 Ca3 Ca6 154.20(16) . .
Sb8 Ca3 Ca7 110.45(9) 5_666 .
Sb8 Ca3 Ca7 110.45(9) 5_656 .
Sb4 Ca3 Ca7 124.85(13) 6_557 .
Sb6 Ca3 Ca7 51.81(6) 5_666 .
Sb6 Ca3 Ca7 51.81(6) 5_656 .
Mn2 Ca3 Ca7 59.34(8) 5_666 .
Mn2 Ca3 Ca7 59.34(8) 5_656 .
Mn4 Ca3 Ca7 141.16(15) . .
Ca6 Ca3 Ca7 64.65(10) . .
Sb8 Ca3 Ca2 54.70(7) 5_666 5_566
Sb8 Ca3 Ca2 104.81(11) 5_656 5_566
Sb4 Ca3 Ca2 51.82(7) 6_557 5_566
Sb6 Ca3 Ca2 91.09(6) 5_666 5_566
Sb6 Ca3 Ca2 146.56(12) 5_656 5_566
Mn2 Ca3 Ca2 96.88(6) 5_666 5_566
Mn2 Ca3 Ca2 154.20(13) 5_656 5_566
Mn4 Ca3 Ca2 60.31(10) . 5_566
Ca6 Ca3 Ca2 99.27(11) . 5_566
Ca7 Ca3 Ca2 142.77(6) . 5_566
Sb8 Ca3 Ca2 104.81(11) 5_666 5_556
Sb8 Ca3 Ca2 54.70(7) 5_656 5_556
Sb4 Ca3 Ca2 51.81(7) 6_557 5_556
Sb6 Ca3 Ca2 146.56(12) 5_666 5_556
Sb6 Ca3 Ca2 91.09(6) 5_656 5_556
Mn2 Ca3 Ca2 154.20(13) 5_666 5_556
Mn2 Ca3 Ca2 96.88(6) 5_656 5_556
Mn4 Ca3 Ca2 60.31(10) . 5_556
Ca6 Ca3 Ca2 99.27(11) . 5_556
Ca7 Ca3 Ca2 142.77(6) . 5_556
Ca2 Ca3 Ca2 69.70(9) 5_566 5_556
Mn4 Ca4 Mn6A 119.0(2) . .
Mn4 Ca4 Sb9B 64.02(15) . .
Mn6A Ca4 Sb9B 55.0(2) . .
Mn4 Ca4 Sb3 120.41(17) . .
Mn6A Ca4 Sb3 120.6(2) . .
Sb9B Ca4 Sb3 175.57(18) . .
Mn4 Ca4 Sb9A 52.71(13) . .
Mn6A Ca4 Sb9A 66.3(2) . .
Sb9B Ca4 Sb9A 11.31(6) . .
Sb3 Ca4 Sb9A 173.12(16) . .
Mn4 Ca4 Sb8 52.63(8) . 5_666
Mn6A Ca4 Sb8 128.59(11) . 5_666
Sb9B Ca4 Sb8 94.16(11) . 5_666
Sb3 Ca4 Sb8 89.00(9) . 5_666
Sb9A Ca4 Sb8 86.09(10) . 5_666
Mn4 Ca4 Sb8 52.63(8) . 5_656
Mn6A Ca4 Sb8 128.59(11) . 5_656
Sb9B Ca4 Sb8 94.16(11) . 5_656
Sb3 Ca4 Sb8 89.00(9) . 5_656
Sb9A Ca4 Sb8 86.09(10) . 5_656
Sb8 Ca4 Sb8 88.84(11) 5_666 5_656
Mn4 Ca4 Sb5 128.25(9) . 5_666
Mn6A Ca4 Sb5 50.26(10) . 5_666
Sb9B Ca4 Sb5 85.58(10) . 5_666
Sb3 Ca4 Sb5 91.19(9) . 5_666
Sb9A Ca4 Sb5 93.83(10) . 5_666
Sb8 Ca4 Sb5 92.49(2) 5_666 5_666
Sb8 Ca4 Sb5 178.65(11) 5_656 5_666
Mn4 Ca4 Sb5 128.25(9) . 5_656
Mn6A Ca4 Sb5 50.26(10) . 5_656
Sb9B Ca4 Sb5 85.58(10) . 5_656
Sb3 Ca4 Sb5 91.19(9) . 5_656
Sb9A Ca4 Sb5 93.83(10) . 5_656
Sb8 Ca4 Sb5 178.65(11) 5_666 5_656
Sb8 Ca4 Sb5 92.49(3) 5_656 5_656
Sb5 Ca4 Sb5 86.17(11) 5_666 5_656
Mn4 Ca4 Ca8 173.30(18) . .
Mn6A Ca4 Ca8 67.7(2) . .
Sb9B Ca4 Ca8 122.68(16) . .
Sb3 Ca4 Ca8 52.89(10) . .
Sb9A Ca4 Ca8 133.99(16) . .
Sb8 Ca4 Ca8 123.98(9) 5_666 .
Sb8 Ca4 Ca8 123.98(9) 5_656 .
Sb5 Ca4 Ca8 55.27(8) 5_666 .
Sb5 Ca4 Ca8 55.27(8) 5_656 .
Mn4 Ca4 Ca3 55.87(13) . .
Mn6A Ca4 Ca3 174.9(2) . .
Sb9B Ca4 Ca3 119.89(15) . .
Sb3 Ca4 Ca3 64.54(9) . .
Sb9A Ca4 Ca3 108.58(13) . .
Sb8 Ca4 Ca3 49.29(6) 5_666 .
Sb8 Ca4 Ca3 49.29(6) 5_656 .
Sb5 Ca4 Ca3 131.92(7) 5_666 .
Sb5 Ca4 Ca3 131.92(7) 5_656 .
Ca8 Ca4 Ca3 117.43(13) . .
Mn4 Ca4 Ca1 35.86(10) . 3_556
Mn6A Ca4 Ca1 93.85(19) . 3_556
Sb9B Ca4 Ca1 46.33(11) . 3_556
Sb3 Ca4 Ca1 137.06(12) . 3_556
Sb9A Ca4 Ca1 38.00(9) . 3_556
Sb8 Ca4 Ca1 48.13(9) 5_666 3_556
Sb8 Ca4 Ca1 87.97(12) 5_656 3_556
Sb5 Ca4 Ca1 92.79(9) 5_666 3_556
Sb5 Ca4 Ca1 131.72(13) 5_656 3_556
Ca8 Ca4 Ca1 148.05(11) . 3_556
Ca3 Ca4 Ca1 81.62(12) . 3_556
Sb7 Ca5 Sb7 92.52(10) 5_666 5_656
Sb7 Ca5 Sb3 89.92(3) 5_666 5_666
Sb7 Ca5 Sb3 177.56(10) 5_656 5_666
Sb7 Ca5 Sb3 177.56(10) 5_666 5_656
Sb7 Ca5 Sb3 89.92(3) 5_656 5_656
Sb3 Ca5 Sb3 87.65(9) 5_666 5_656
Sb7 Ca5 Sb1 86.07(8) 5_666 .
Sb7 Ca5 Sb1 86.07(8) 5_656 .
Sb3 Ca5 Sb1 94.11(8) 5_666 .
Sb3 Ca5 Sb1 94.11(8) 5_656 .
Sb7 Ca5 Sb2 82.60(8) 5_666 .
Sb7 Ca5 Sb2 82.60(8) 5_656 .
Sb3 Ca5 Sb2 97.72(9) 5_666 .
Sb3 Ca5 Sb2 97.72(9) 5_656 .
Sb1 Ca5 Sb2 163.57(13) . .
Sb7 Ca5 Mn2 131.71(6) 5_666 .
Sb7 Ca5 Mn2 131.71(6) 5_656 .
Sb3 Ca5 Mn2 46.02(5) 5_666 .
Sb3 Ca5 Mn2 46.02(5) 5_656 .
Sb1 Ca5 Mn2 111.45(11) . .
Sb2 Ca5 Mn2 84.98(9) . .
Sb7 Ca5 Mn3 40.44(10) 5_666 5_666
Sb7 Ca5 Mn3 96.83(12) 5_656 5_666
Sb3 Ca5 Mn3 85.03(9) 5_666 5_666
Sb3 Ca5 Mn3 139.17(15) 5_656 5_666
Sb1 Ca5 Mn3 126.43(12) . 5_666
Sb2 Ca5 Mn3 44.09(9) . 5_666
Mn2 Ca5 Mn3 105.80(13) . 5_666
Sb7 Ca5 Mn3 96.83(12) 5_666 5_656
Sb7 Ca5 Mn3 40.44(10) 5_656 5_656
Sb3 Ca5 Mn3 139.17(15) 5_666 5_656
Sb3 Ca5 Mn3 85.03(9) 5_656 5_656
Sb1 Ca5 Mn3 126.43(12) . 5_656
Sb2 Ca5 Mn3 44.09(9) . 5_656
Mn2 Ca5 Mn3 105.80(13) . 5_656
Mn3 Ca5 Mn3 75.03(15) 5_666 5_656
Sb7 Ca5 Mn5 42.26(8) 5_666 5_666
Sb7 Ca5 Mn5 97.69(11) 5_656 5_666
Sb3 Ca5 Mn5 84.13(7) 5_666 5_666
Sb3 Ca5 Mn5 137.32(13) 5_656 5_666
Sb1 Ca5 Mn5 45.16(7) . 5_666
Sb2 Ca5 Mn5 124.86(10) . 5_666
Mn2 Ca5 Mn5 127.06(10) . 5_666
Mn3 Ca5 Mn5 81.70(11) 5_666 5_666
Mn3 Ca5 Mn5 126.31(15) 5_656 5_666
Sb7 Ca5 Mn5 97.69(11) 5_666 5_656
Sb7 Ca5 Mn5 42.26(8) 5_656 5_656
Sb3 Ca5 Mn5 137.32(13) 5_666 5_656
Sb3 Ca5 Mn5 84.13(7) 5_656 5_656
Sb1 Ca5 Mn5 45.16(7) . 5_656
Sb2 Ca5 Mn5 124.86(10) . 5_656
Mn2 Ca5 Mn5 127.06(10) . 5_656
Mn3 Ca5 Mn5 126.31(15) 5_666 5_656
Mn3 Ca5 Mn5 81.70(12) 5_656 5_656
Mn5 Ca5 Mn5 74.41(11) 5_666 5_656
Sb7 Ca5 Ca2 51.67(6) 5_666 .
Sb7 Ca5 Ca2 51.67(6) 5_656 .
Sb3 Ca5 Ca2 130.33(7) 5_666 .
Sb3 Ca5 Ca2 130.33(7) 5_656 .
Sb1 Ca5 Ca2 110.53(11) . .
Sb2 Ca5 Ca2 53.04(8) . .
Mn2 Ca5 Ca2 138.01(13) . .
Mn3 Ca5 Ca2 45.52(9) 5_666 .
Mn3 Ca5 Ca2 45.52(9) 5_656 .
Mn5 Ca5 Ca2 84.29(11) 5_666 .
Mn5 Ca5 Ca2 84.29(11) 5_656 .
Mn3 Ca6 Sb2 52.92(9) 6_557 2_565
Mn3 Ca6 Sb2 52.92(9) 6_557 2
Sb2 Ca6 Sb2 91.20(12) 2_565 2
Mn3 Ca6 Sb6 128.51(11) 6_557 5_666
Sb2 Ca6 Sb6 89.06(3) 2_565 5_666
Sb2 Ca6 Sb6 178.03(18) 2 5_666
Mn3 Ca6 Sb6 128.51(11) 6_557 5_656
Sb2 Ca6 Sb6 178.03(18) 2_565 5_656
Sb2 Ca6 Sb6 89.06(3) 2 5_656
Sb6 Ca6 Sb6 90.61(12) 5_666 5_656
Mn3 Ca6 Sb4 64.46(17) 6_557 .
Sb2 Ca6 Sb4 93.46(11) 2_565 .
Sb2 Ca6 Sb4 93.46(11) 2 .
Sb6 Ca6 Sb4 88.47(9) 5_666 .
Sb6 Ca6 Sb4 88.47(9) 5_656 .
Mn3 Ca6 Sb4 118.23(19) 6_557 6_557
Sb2 Ca6 Sb4 88.42(9) 2_565 6_557
Sb2 Ca6 Sb4 88.42(9) 2 6_557
Sb6 Ca6 Sb4 89.64(11) 5_666 6_557
Sb6 Ca6 Sb4 89.64(11) 5_656 6_557
Sb4 Ca6 Sb4 177.31(15) . 6_557
Mn3 Ca6 Ca3 171.5(2) 6_557 .
Sb2 Ca6 Ca3 122.92(11) 2_565 .
Sb2 Ca6 Ca3 122.92(11) 2 .
Sb6 Ca6 Ca3 55.45(8) 5_666 .
Sb6 Ca6 Ca3 55.45(8) 5_656 .
Sb4 Ca6 Ca3 124.08(14) . .
Sb4 Ca6 Ca3 53.23(10) 6_557 .
Mn3 Ca6 Ca7 55.80(16) 6_557 6_557
Sb2 Ca6 Ca7 50.77(6) 2_565 6_557
Sb2 Ca6 Ca7 50.77(6) 2 6_557
Sb6 Ca6 Ca7 128.35(8) 5_666 6_557
Sb6 Ca6 Ca7 128.35(8) 5_656 6_557
Sb4 Ca6 Ca7 120.27(15) . 6_557
Sb4 Ca6 Ca7 62.42(9) 6_557 6_557
Ca3 Ca6 Ca7 115.65(14) . 6_557
Mn3 Ca6 Ca7 127.2(2) 6_557 .
Sb2 Ca6 Ca7 130.32(7) 2_565 .
Sb2 Ca6 Ca7 130.32(7) 2 .
Sb6 Ca6 Ca7 50.44(6) 5_666 .
Sb6 Ca6 Ca7 50.44(6) 5_656 .
Sb4 Ca6 Ca7 62.70(9) . .
Sb4 Ca6 Ca7 114.61(14) 6_557 .
Ca3 Ca6 Ca7 61.38(10) . .
Ca7 Ca6 Ca7 177.03(16) 6_557 .
Sb3 Ca7 Sb2 105.42(9) . 5_666
Sb3 Ca7 Sb2 105.42(9) . 5_656
Sb2 Ca7 Sb2 92.92(10) 5_666 5_656
Sb3 Ca7 Sb6 93.54(8) . 5_666
Sb2 Ca7 Sb6 84.54(3) 5_666 5_666
Sb2 Ca7 Sb6 160.84(13) 5_656 5_666
Sb3 Ca7 Sb6 93.54(8) . 5_656
Sb2 Ca7 Sb6 160.84(13) 5_666 5_656
Sb2 Ca7 Sb6 84.54(3) 5_656 5_656
Sb6 Ca7 Sb6 91.64(10) 5_666 5_656
Sb3 Ca7 Mn1 135.52(6) . 5_666
Sb2 Ca7 Mn1 51.63(6) 5_666 5_666
Sb2 Ca7 Mn1 112.48(11) 5_656 5_666
Sb6 Ca7 Mn1 51.89(6) 5_666 5_666
Sb6 Ca7 Mn1 112.03(12) 5_656 5_666
Sb3 Ca7 Mn1 135.52(6) . 5_656
Sb2 Ca7 Mn1 112.48(11) 5_666 5_656
Sb2 Ca7 Mn1 51.63(6) 5_656 5_656
Sb6 Ca7 Mn1 112.03(12) 5_666 5_656
Sb6 Ca7 Mn1 51.89(6) 5_656 5_656
Mn1 Ca7 Mn1 87.55(11) 5_666 5_656
Sb3 Ca7 Mn3 95.20(15) . .
Sb2 Ca7 Mn3 48.93(6) 5_666 .
Sb2 Ca7 Mn3 48.93(6) 5_656 .
Sb6 Ca7 Mn3 133.29(6) 5_666 .
Sb6 Ca7 Mn3 133.29(6) 5_656 .
Mn1 Ca7 Mn3 92.62(12) 5_666 .
Mn1 Ca7 Mn3 92.62(12) 5_656 .
Sb3 Ca7 Mn2 46.87(6) . 5_666
Sb2 Ca7 Mn2 87.89(5) 5_666 5_666
Sb2 Ca7 Mn2 150.85(13) 5_656 5_666
Sb6 Ca7 Mn2 48.21(6) 5_666 5_666
Sb6 Ca7 Mn2 103.54(10) 5_656 5_666
Mn1 Ca7 Mn2 90.70(6) 5_666 5_666
Mn1 Ca7 Mn2 151.75(13) 5_656 5_666
Mn3 Ca7 Mn2 115.63(12) . 5_666
Sb3 Ca7 Mn2 46.87(6) . 5_656
Sb2 Ca7 Mn2 150.85(13) 5_666 5_656
Sb2 Ca7 Mn2 87.88(5) 5_656 5_656
Sb6 Ca7 Mn2 103.54(10) 5_666 5_656
Sb6 Ca7 Mn2 48.21(6) 5_656 5_656
Mn1 Ca7 Mn2 151.75(13) 5_666 5_656
Mn1 Ca7 Mn2 90.70(6) 5_656 5_656
Mn3 Ca7 Mn2 115.63(12) . 5_656
Mn2 Ca7 Mn2 77.78(9) 5_666 5_656
Sb3 Ca7 Ca3 66.72(9) . .
Sb2 Ca7 Ca3 133.54(5) 5_666 .
Sb2 Ca7 Ca3 133.54(5) 5_656 .
Sb6 Ca7 Ca3 52.17(6) 5_666 .
Sb6 Ca7 Ca3 52.18(6) 5_656 .
Mn1 Ca7 Ca3 100.38(10) 5_666 .
Mn1 Ca7 Ca3 100.38(10) 5_656 .
Mn3 Ca7 Ca3 161.92(17) . .
Mn2 Ca7 Ca3 52.26(7) 5_666 .
Mn2 Ca7 Ca3 52.26(7) 5_656 .
Sb3 Ca7 Ca6 138.84(14) . 6_657
Sb2 Ca7 Ca6 51.80(6) 5_666 6_657
Sb2 Ca7 Ca6 51.80(6) 5_656 6_657
Sb6 Ca7 Ca6 114.23(9) 5_666 6_657
Sb6 Ca7 Ca6 114.23(9) 5_656 6_657
Mn1 Ca7 Ca6 62.34(8) 5_666 6_657
Mn1 Ca7 Ca6 62.34(8) 5_656 6_657
Mn3 Ca7 Ca6 43.64(15) . 6_657
Mn2 Ca7 Ca6 139.43(6) 5_666 6_657
Mn2 Ca7 Ca6 139.43(6) 5_656 6_657
Ca3 Ca7 Ca6 154.44(14) . 6_657
Sb3 Ca8 Mn6B 132.71(8) . 5_666
Sb3 Ca8 Mn6B 132.71(8) . 5_656
Mn6B Ca8 Mn6B 93.72(16) 5_666 5_656
Sb3 Ca8 Sb1 101.33(11) . 5_666
Mn6B Ca8 Sb1 52.54(9) 5_666 5_666
Mn6B Ca8 Sb1 117.12(15) 5_656 5_666
Sb3 Ca8 Sb1 101.33(11) . 5_656
Mn6B Ca8 Sb1 117.12(15) 5_666 5_656
Mn6B Ca8 Sb1 52.54(9) 5_656 5_656
Sb1 Ca8 Sb1 93.63(12) 5_666 5_656
Sb3 Ca8 Mn6B 121.62(16) . .
Mn6B Ca8 Mn6B 64.55(13) 5_666 .
Mn6B Ca8 Mn6B 64.55(13) 5_656 .
Sb1 Ca8 Mn6B 117.08(11) 5_666 .
Sb1 Ca8 Mn6B 117.08(11) 5_656 .
Sb3 Ca8 Sb5 93.69(10) . 5_666
Mn6B Ca8 Sb5 52.30(9) 5_666 5_666
Mn6B Ca8 Sb5 113.52(15) 5_656 5_666
Sb1 Ca8 Sb5 87.33(4) 5_666 5_666
Sb1 Ca8 Sb5 164.44(16) 5_656 5_666
Mn6B Ca8 Sb5 49.79(7) . 5_666
Sb3 Ca8 Sb5 93.69(10) . 5_656
Mn6B Ca8 Sb5 113.52(15) 5_666 5_656
Mn6B Ca8 Sb5 52.30(9) 5_656 5_656
Sb1 Ca8 Sb5 164.44(16) 5_666 5_656
Sb1 Ca8 Sb5 87.33(4) 5_656 5_656
Mn6B Ca8 Sb5 49.79(7) . 5_656
Sb5 Ca8 Sb5 87.66(11) 5_666 5_656
Sb3 Ca8 Mn5 91.41(14) . .
Mn6B Ca8 Mn5 94.03(13) 5_666 .
Mn6B Ca8 Mn5 94.03(13) 5_656 .
Sb1 Ca8 Mn5 48.69(6) 5_666 .
Sb1 Ca8 Mn5 48.69(6) 5_656 .
Mn6B Ca8 Mn5 146.97(18) . .
Sb5 Ca8 Mn5 135.78(6) 5_666 .
Sb5 Ca8 Mn5 135.78(6) 5_656 .
Sb3 Ca8 Sb5 170.22(15) . .
Mn6B Ca8 Sb5 46.91(8) 5_666 .
Mn6B Ca8 Sb5 46.91(8) 5_656 .
Sb1 Ca8 Sb5 85.28(9) 5_666 .
Sb1 Ca8 Sb5 85.28(9) 5_656 .
Mn6B Ca8 Sb5 48.60(10) . .
Sb5 Ca8 Sb5 79.32(9) 5_666 .
Sb5 Ca8 Sb5 79.32(9) 5_656 .
Mn5 Ca8 Sb5 98.36(13) . .
Sb3 Ca8 Ca4 55.15(9) . .
Mn6B Ca8 Ca4 108.43(13) 5_666 .
Mn6B Ca8 Ca4 108.43(13) 5_656 .
Sb1 Ca8 Ca4 130.56(7) 5_666 .
Sb1 Ca8 Ca4 130.56(7) 5_656 .
Mn6B Ca8 Ca4 66.47(13) . .
Sb5 Ca8 Ca4 56.44(7) 5_666 .
Sb5 Ca8 Ca4 56.44(7) 5_656 .
Mn5 Ca8 Ca4 146.56(17) . .
Sb5 Ca8 Ca4 115.08(13) . .
Sb3 Ca8 Mn6A 140.49(12) . 5_666
Mn6B Ca8 Mn6A 18.61(15) 5_666 5_666
Mn6B Ca8 Mn6A 86.29(15) 5_656 5_666
Sb1 Ca8 Mn6A 43.82(14) 5_666 5_666
Sb1 Ca8 Mn6A 99.26(16) 5_656 5_666
Mn6B Ca8 Mn6A 76.27(18) . 5_666
Sb5 Ca8 Mn6A 70.87(14) 5_666 5_666
Sb5 Ca8 Mn6A 120.70(18) 5_656 5_666
Mn5 Ca8 Mn6A 77.57(18) . 5_666
Sb5 Ca8 Mn6A 43.36(12) . 5_666
Ca4 Ca8 Mn6A 127.02(16) . 5_666
Sb9B Ca9 Sb9B 105.1(2) 5_666 5_656
Sb9B Ca9 Mn6A 59.08(18) 5_666 5_666
Sb9B Ca9 Mn6A 135.2(3) 5_656 5_666
Sb9B Ca9 Mn6A 135.2(3) 5_666 5_656
Sb9B Ca9 Mn6A 59.08(18) 5_656 5_656
Mn6A Ca9 Mn6A 100.8(3) 5_666 5_656
Sb9B Ca9 Mn5 122.32(14) 5_666 .
Sb9B Ca9 Mn5 122.32(14) 5_656 .
Mn6A Ca9 Mn5 98.7(2) 5_666 .
Mn6A Ca9 Mn5 98.7(2) 5_656 .
Sb9B Ca9 Sb9A 95.74(15) 5_666 1_655
Sb9B Ca9 Sb9A 95.74(15) 5_656 1_655
Mn6A Ca9 Sb9A 125.57(19) 5_666 1_655
Mn6A Ca9 Sb9A 125.57(18) 5_656 1_655
Mn5 Ca9 Sb9A 52.10(14) . 1_655
Sb9B Ca9 Sb9A 8.87(5) 5_666 5_666
Sb9B Ca9 Sb9A 96.50(17) 5_656 5_666
Mn6A Ca9 Sb9A 66.75(18) 5_666 5_666
Mn6A Ca9 Sb9A 132.4(3) 5_656 5_666
Mn5 Ca9 Sb9A 127.89(13) . 5_666
Sb9A Ca9 Sb9A 94.60(13) 1_655 5_666
Sb9B Ca9 Sb9A 96.50(17) 5_666 5_656
Sb9B Ca9 Sb9A 8.87(5) 5_656 5_656
Mn6A Ca9 Sb9A 132.4(3) 5_666 5_656
Mn6A Ca9 Sb9A 66.75(18) 5_656 5_656
Mn5 Ca9 Sb9A 127.89(13) . 5_656
Sb9A Ca9 Sb9A 94.60(13) 1_655 5_656
Sb9A Ca9 Sb9A 87.83(15) 5_666 5_656
Sb9B Ca9 Sb5 91.04(15) 5_666 .
Sb9B Ca9 Sb5 91.04(15) 5_656 .
Mn6A Ca9 Sb5 51.60(17) 5_666 .
Mn6A Ca9 Sb5 51.60(17) 5_656 .
Mn5 Ca9 Sb5 116.72(19) . .
Sb9A Ca9 Sb5 168.82(19) 1_655 .
Sb9A Ca9 Sb5 93.45(13) 5_666 .
Sb9A Ca9 Sb5 93.45(13) 5_656 .
Sb9B Ca9 Sb9B 89.07(15) 5_666 1_655
Sb9B Ca9 Sb9B 89.07(15) 5_656 1_655
Mn6A Ca9 Sb9B 128.36(17) 5_666 1_655
Mn6A Ca9 Sb9B 128.36(17) 5_656 1_655
Mn5 Ca9 Sb9B 63.10(16) . 1_655
Sb9A Ca9 Sb9B 11.00(6) 1_655 1_655
Sb9A Ca9 Sb9B 86.68(13) 5_666 1_655
Sb9A Ca9 Sb9B 86.68(13) 5_656 1_655
Sb5 Ca9 Sb9B 179.8(2) . 1_655
Sb9B Ca9 Sb1 84.57(7) 5_666 5_666
Sb9B Ca9 Sb1 170.25(16) 5_656 5_666
Mn6A Ca9 Sb1 48.99(19) 5_666 5_666
Mn6A Ca9 Sb1 113.1(2) 5_656 5_666
Mn5 Ca9 Sb1 50.69(9) . 5_666
Sb9A Ca9 Sb1 84.35(12) 1_655 5_666
Sb9A Ca9 Sb1 93.20(4) 5_666 5_666
Sb9A Ca9 Sb1 178.57(17) 5_656 5_666
Sb5 Ca9 Sb1 87.46(12) . 5_666
Sb9B Ca9 Sb1 92.40(14) 1_655 5_666
Sb9B Ca9 Sb1 170.25(16) 5_666 5_656
Sb9B Ca9 Sb1 84.57(7) 5_656 5_656
Mn6A Ca9 Sb1 113.1(2) 5_666 5_656
Mn6A Ca9 Sb1 48.99(19) 5_656 5_656
Mn5 Ca9 Sb1 50.69(9) . 5_656
Sb9A Ca9 Sb1 84.35(12) 1_655 5_656
Sb9A Ca9 Sb1 178.57(17) 5_666 5_656
Sb9A Ca9 Sb1 93.20(4) 5_656 5_656
Sb5 Ca9 Sb1 87.46(12) . 5_656
Sb9B Ca9 Sb1 92.40(14) 1_655 5_656
Sb1 Ca9 Sb1 85.74(13) 5_666 5_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 Mn6A 2.677(10) .
Sb1 Mn5 2.790(3) 5_666
Sb1 Mn5 2.790(3) 5_656
Sb1 Mn6B 2.805(4) .
Sb1 Ca8 3.170(3) 5_666
Sb1 Ca8 3.170(3) 5_656
Sb1 Ca1 3.243(6) .
Sb1 Ca1 3.243(6) 7_565
Sb1 Ca5 3.355(4) .
Sb1 Ca9 3.397(4) 5_666
Sb1 Ca9 3.397(4) 5_656
Sb2 Mn3 2.721(3) 5_666
Sb2 Mn3 2.721(4) 5_656
Sb2 Mn1 2.847(3) .
Sb2 Ca7 3.189(3) 5_666
Sb2 Ca7 3.189(3) 5_656
Sb2 Ca6 3.235(3) 2_564
Sb2 Ca6 3.235(3) 2_554
Sb2 Ca2 3.366(4) .
Sb2 Ca5 3.381(4) .
Sb3 Mn2 2.7656(17) 5_666
Sb3 Mn2 2.7656(17) 5_656
Sb3 Ca8 3.164(5) .
Sb3 Ca7 3.172(4) .
Sb3 Ca4 3.256(4) .
Sb3 Ca5 3.338(3) 5_666
Sb3 Ca5 3.338(3) 5_656
Sb4 Mn1 2.7544(17) 5_666
Sb4 Mn1 2.7544(17) 5_656
Sb4 Ca3 3.200(4) 6_657
Sb4 Ca2 3.255(3) 2_565
Sb4 Ca2 3.255(3) 2
Sb4 Ca6 3.299(5) .
Sb4 Ca6 3.467(5) 6_657
Sb5 Mn6B 2.765(3) 5_666
Sb5 Mn6B 2.765(3) 5_656
Sb5 Mn6A 2.773(5) 5_666
Sb5 Mn6A 2.773(5) 5_656
Sb5 Mn6B 2.871(4) .
Sb5 Ca9 3.334(6) .
Sb5 Ca8 3.337(3) 5_666
Sb5 Ca8 3.338(3) 5_656
Sb5 Ca4 3.384(3) 5_666
Sb5 Ca4 3.384(3) 5_656
Sb5 Ca8 3.678(5) .
Sb6 Mn2 2.851(3) .
Sb6 Mn1 2.874(3) .
Sb6 Ca7 3.223(3) 5_666
Sb6 Ca7 3.223(3) 5_656
Sb6 Ca3 3.239(3) 5_666
Sb6 Ca3 3.239(3) 5_656
Sb6 Ca6 3.251(3) 5_666
Sb6 Ca6 3.251(3) 5_656
Sb7 Mn3 2.482(7) .
Sb7 Mn4 2.566(5) 1_655
Sb7 Mn5 2.598(5) .
Sb7 Ca1 3.192(5) 3_656
Sb7 Ca1 3.192(5) 5_656
Sb7 Ca5 3.199(3) 5_666
Sb7 Ca5 3.199(3) 5_656
Sb7 Ca2 3.244(3) 5_666
Sb7 Ca2 3.244(3) 5_656
Sb7 Ca1 3.709(5) 5_666
Sb7 Ca1 3.709(5) 3_646
Sb8 Mn4 2.829(3) 5_666
Sb8 Mn4 2.829(3) 5_656
Sb8 Mn2 2.834(3) .
Sb8 Ca3 3.169(3) 5_666
Sb8 Ca3 3.169(3) 5_656
Sb8 Ca1 3.209(6) 7_665
Sb8 Ca1 3.209(6) 1_655
Sb8 Ca4 3.302(3) 5_666
Sb8 Ca4 3.302(3) 5_656
Sb8 Ca2 3.405(4) 1_655
Sb9A Sb9B 0.640(3) .
Sb9A Ca1 2.628(6) 3_556
Sb9A Ca1 2.628(6) 5_556
Sb9A Mn5 2.794(6) 1_455
Sb9A Mn4 2.812(6) .
Sb9A Ca1 3.236(5) 5_566
Sb9A Ca1 3.236(5) 3_546
Sb9A Ca4 3.261(5) .
Sb9A Ca9 3.266(6) 1_455
Sb9A Ca9 3.332(4) 5_666
Sb9A Ca9 3.332(4) 5_656
Sb9B Ca9 2.911(4) 5_666
Sb9B Ca9 2.911(4) 5_656
Sb9B Mn6A 2.915(10) .
Sb9B Ca1 3.094(6) 3_556
Sb9B Ca1 3.094(6) 5_556
Sb9B Ca4 3.188(6) .
Sb9B Ca9 3.351(7) 1_455
Sb9B Ca1 3.625(6) 5_566
Sb9B Ca1 3.625(6) 3_546
Mn1 Sb4 2.7544(17) 5_666
Mn1 Sb4 2.7544(17) 5_656
Mn1 Ca7 3.341(3) 5_666
Mn1 Ca7 3.341(3) 5_656
Mn1 Ca2 3.727(5) 6_656
Mn2 Sb3 2.7656(17) 5_666
Mn2 Sb3 2.7656(17) 5_656
Mn2 Ca3 3.385(3) 5_666
Mn2 Ca3 3.385(3) 5_656
Mn2 Ca7 3.682(3) 5_666
Mn2 Ca7 3.682(3) 5_656
Mn2 Ca5 3.688(5) .
Mn3 Sb2 2.721(3) 5_666
Mn3 Sb2 2.721(3) 5_656
Mn3 Ca6 2.811(8) 6_657
Mn3 Ca2 3.040(5) 5_666
Mn3 Ca2 3.040(5) 5_656
Mn3 Ca7 3.369(8) .
Mn3 Ca5 3.795(6) 5_666
Mn3 Ca5 3.795(6) 5_656
Mn4 Ca1 2.530(6) 3_556
Mn4 Ca1 2.530(6) 5_556
Mn4 Sb7 2.566(5) 1_455
Mn4 Sb8 2.829(3) 5_666
Mn4 Sb8 2.829(3) 5_656
Mn4 Ca4 3.060(7) .
Mn4 Ca1 3.157(6) 5_566
Mn4 Ca1 3.157(6) 3_546
Mn4 Mn5 3.193(7) 1_455
Mn4 Ca3 3.476(7) .
Mn4 Ca2 3.810(5) 5_566
Mn5 Ca1 2.579(6) 3_656
Mn5 Ca1 2.579(6) 5_656
Mn5 Sb1 2.790(3) 5_666
Mn5 Sb1 2.790(3) 5_656
Mn5 Sb9A 2.794(6) 1_655
Mn5 Ca9 3.087(7) .
Mn5 Mn4 3.192(7) 1_655
Mn5 Ca1 3.196(6) 5_666
Mn5 Ca1 3.196(6) 3_646
Mn5 Ca8 3.546(7) .
Mn5 Ca5 3.822(5) 5_666
Mn6A Mn6B 1.300(10) .
Mn6A Sb5 2.773(5) 5_666
Mn6A Sb5 2.773(5) 5_656
Mn6A Ca9 2.999(7) 5_666
Mn6A Ca9 2.999(7) 5_656
Mn6A Ca4 3.123(10) .
Mn6A Ca8 3.820(8) 5_666
Mn6A Ca8 3.820(8) 5_656
Mn6B Sb5 2.765(3) 5_666
Mn6B Sb5 2.765(3) 5_656
Mn6B Ca8 3.168(4) 5_666
Mn6B Ca8 3.168(4) 5_656
Mn6B Ca8 3.225(6) .
Ca1 Ca1 0.772(10) 7_565
Ca1 Mn4 2.529(6) 5_556
Ca1 Mn5 2.579(6) 5_656
Ca1 Sb9A 2.628(6) 5_556
Ca1 Sb9B 3.094(6) 5_556
Ca1 Mn4 3.157(6) 5_566
Ca1 Sb7 3.192(5) 5_656
Ca1 Mn5 3.196(6) 5_666
Ca1 Sb8 3.209(6) 1_455
Ca1 Sb9A 3.236(5) 5_566
Ca1 Sb9B 3.625(6) 5_566
Ca2 Mn3 3.039(5) 5_666
Ca2 Mn3 3.040(5) 5_656
Ca2 Sb7 3.244(3) 5_666
Ca2 Sb7 3.244(3) 5_656
Ca2 Sb4 3.255(3) 2_564
Ca2 Sb4 3.255(3) 2_554
Ca2 Sb8 3.405(4) 1_455
Ca2 Mn1 3.727(5) 6_556
Ca2 Mn4 3.810(5) 5_566
Ca2 Mn4 3.810(5) 5_556
Ca2 Ca5 4.040(5) .
Ca3 Sb8 3.169(3) 5_666
Ca3 Sb8 3.169(3) 5_656
Ca3 Sb4 3.200(4) 6_557
Ca3 Sb6 3.239(3) 5_666
Ca3 Sb6 3.239(3) 5_656
Ca3 Mn2 3.385(3) 5_666
Ca3 Mn2 3.385(3) 5_656
Ca3 Ca6 3.666(6) .
Ca3 Ca7 3.979(5) .
Ca3 Ca2 4.045(4) 5_566
Ca3 Ca2 4.045(5) 5_556
Ca4 Sb8 3.302(3) 5_666
Ca4 Sb8 3.302(3) 5_656
Ca4 Sb5 3.384(3) 5_666
Ca4 Sb5 3.384(3) 5_656
Ca4 Ca8 3.773(6) .
Ca4 Ca1 4.265(7) 3_556
Ca5 Sb7 3.199(3) 5_666
Ca5 Sb7 3.199(3) 5_656
Ca5 Sb3 3.338(3) 5_666
Ca5 Sb3 3.338(3) 5_656
Ca5 Mn3 3.795(6) 5_666
Ca5 Mn3 3.795(6) 5_656
Ca5 Mn5 3.822(5) 5_666
Ca5 Mn5 3.822(5) 5_656
Ca6 Mn3 2.811(8) 6_557
Ca6 Sb2 3.235(3) 2_565
Ca6 Sb2 3.235(3) 2
Ca6 Sb6 3.251(3) 5_666
Ca6 Sb6 3.252(3) 5_656
Ca6 Sb4 3.467(5) 6_557
Ca6 Ca7 4.018(5) 6_557
Ca6 Ca7 4.096(6) .
Ca7 Sb2 3.189(3) 5_666
Ca7 Sb2 3.189(3) 5_656
Ca7 Sb6 3.223(3) 5_666
Ca7 Sb6 3.223(3) 5_656
Ca7 Mn1 3.341(3) 5_666
Ca7 Mn1 3.341(3) 5_656
Ca7 Mn2 3.681(3) 5_666
Ca7 Mn2 3.681(3) 5_656
Ca7 Ca6 4.018(5) 6_657
Ca8 Mn6B 3.168(4) 5_666
Ca8 Mn6B 3.168(4) 5_656
Ca8 Sb1 3.170(3) 5_666
Ca8 Sb1 3.170(3) 5_656
Ca8 Sb5 3.337(3) 5_666
Ca8 Sb5 3.337(3) 5_656
Ca8 Mn6A 3.820(8) 5_666
Ca9 Sb9B 2.911(4) 5_666
Ca9 Sb9B 2.911(4) 5_656
Ca9 Mn6A 2.999(7) 5_666
Ca9 Mn6A 2.999(7) 5_656
Ca9 Sb9A 3.265(6) 1_655
Ca9 Sb9A 3.332(4) 5_666
Ca9 Sb9A 3.332(4) 5_656
Ca9 Sb9B 3.351(7) 1_655
Ca9 Sb1 3.397(4) 5_666
Ca9 Sb1 3.397(4) 5_656
