#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:59:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179520 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341707.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341707
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Ca9 Mn4.5 Sb9'
_chemical_formula_weight         1703.70
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.4617(18)
_cell_length_b                   4.6169(7)
_cell_length_c                   44.051(6)
_cell_measurement_reflns_used    944
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      28.03
_cell_measurement_theta_min      2.83
_cell_volume                     2534.4(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.973
_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0499
_diffrn_reflns_av_sigmaI/netI    0.0318
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       55
_diffrn_reflns_limit_l_min       -57
_diffrn_reflns_number            25327
_diffrn_reflns_theta_full        28.07
_diffrn_reflns_theta_max         28.07
_diffrn_reflns_theta_min         0.92
_exptl_absorpt_coefficient_mu    13.380
_exptl_absorpt_correction_T_max  0.6896
_exptl_absorpt_correction_T_min  0.5007
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.465
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             3006
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.03
_refine_diff_density_max         3.008
_refine_diff_density_min         -3.464
_refine_diff_density_rms         0.343
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.146
_refine_ls_matrix_type           full
_refine_ls_number_parameters     155
_refine_ls_number_reflns         3367
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.146
_refine_ls_R_factor_all          0.0491
_refine_ls_R_factor_gt           0.0404
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0200P)²+54.9199P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0796
_refine_ls_wR_factor_ref         0.0840
_reflns_number_gt                2986
_reflns_number_total             3367
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_003.cif
_cod_data_source_block           II
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341707
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sb1 Sb 0.25160(6) 0.2500 0.449519(17) 0.01116(16) Uani 1 2 d S
Sb2 Sb 0.27558(6) 0.2500 0.298459(16) 0.00721(15) Uani 1 2 d S
Sb3 Sb 0.50553(6) 0.2500 0.620356(16) 0.00921(16) Uani 1 2 d S
Sb4 Sb 0.55166(7) 0.2500 0.779759(18) 0.01589(18) Uani 1 2 d S
Sb5 Sb 0.60544(6) 0.2500 0.468221(17) 0.01010(16) Uani 1 2 d S
Sb6 Sb 0.62119(6) 0.2500 0.295139(16) 0.00742(15) Uani 1 2 d S
Sb7 Sb 0.87464(7) 0.2500 0.629761(18) 0.01391(17) Uani 1 2 d S
Sb8 Sb 0.81276(6) 0.2500 0.375658(17) 0.01081(16) Uani 1 2 d S
Sb9A Sb 0.05575(13) 0.2500 0.54561(4) 0.0127(3) Uani 0.605(2) 2 d SP
Sb9B Sb 0.0867(2) 0.2500 0.53447(6) 0.0127(3) Uani 0.395(2) 2 d SP
Mn1 Mn 0.44173(14) 0.2500 0.25419(4) 0.0091(3) Uani 1 2 d S
Mn2 Mn 0.59265(13) 0.2500 0.35935(4) 0.0087(3) Uani 1 2 d S
Mn3 Mn 0.8215(3) 0.2500 0.68384(9) 0.0082(13) Uani 0.392(8) 2 d SP
Mn4 Mn 0.0674(3) 0.2500 0.60941(7) 0.0069(4) Uani 0.479(3) 2 d SP
Mn5 Mn 0.8503(2) 0.2500 0.57119(7) 0.0069(4) Uani 0.521(3) 2 d SP
Mn6A Mn 0.3024(5) 0.2500 0.50866(14) 0.0145(5) Uani 0.288(4) 2 d SP
Mn6B Mn 0.3997(2) 0.2500 0.49753(6) 0.0145(5) Uani 0.712(4) 2 d SP
Q1 Mn 0.0557(9) 0.2500 0.4693(2) 0.015 Uiso 0.171(5) 2 d SP
Ca1 Ca 0.0164(3) 0.1667(7) 0.41916(8) 0.0201(8) Uani 0.50 1 d P
Ca2 Ca 0.02592(19) 0.2500 0.32709(5) 0.0179(5) Uani 1 2 d S
Ca3 Ca 0.24152(19) 0.2500 0.67120(5) 0.0130(5) Uani 1 2 d S
Ca4 Ca 0.2894(2) 0.2500 0.57912(6) 0.0171(5) Uani 1 2 d S
Ca5 Ca 0.30206(18) 0.2500 0.37464(5) 0.0112(4) Uani 1 2 d S
Ca6 Ca 0.3050(2) 0.2500 0.75239(7) 0.0226(6) Uani 1 2 d S
Ca7 Ca 0.55254(18) 0.2500 0.69114(5) 0.0097(4) Uani 1 2 d S
Ca8 Ca 0.5751(2) 0.2500 0.55138(7) 0.0255(6) Uani 1 2 d S
Ca9 Ca 0.8451(3) 0.2500 0.50100(8) 0.0492(10) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Q1 Sb1 Mn6A 84.0(3) . .
Q1 Sb1 Mn5 71.40(13) . 5_656
Mn6A Sb1 Mn5 115.19(8) . 5_656
Q1 Sb1 Mn5 71.40(13) . 5_666
Mn6A Sb1 Mn5 115.19(8) . 5_666
Mn5 Sb1 Mn5 111.77(11) 5_656 5_666
Q1 Sb1 Mn6B 111.5(2) . .
Mn6A Sb1 Mn6B 27.45(15) . .
Mn5 Sb1 Mn6B 123.10(5) 5_656 .
Mn5 Sb1 Mn6B 123.10(5) 5_666 .
Q1 Sb1 Ca8 130.35(8) . 5_656
Mn6A Sb1 Ca8 81.42(11) . 5_656
Mn5 Sb1 Ca8 72.69(7) 5_656 5_656
Mn5 Sb1 Ca8 155.73(8) 5_666 5_656
Mn6B Sb1 Ca8 63.91(6) . 5_656
Q1 Sb1 Ca8 130.35(8) . 5_666
Mn6A Sb1 Ca8 81.42(11) . 5_666
Mn5 Sb1 Ca8 155.73(8) 5_656 5_666
Mn5 Sb1 Ca8 72.69(7) 5_666 5_666
Mn6B Sb1 Ca8 63.91(6) . 5_666
Ca8 Sb1 Ca8 93.82(8) 5_656 5_666
Q1 Sb1 Ca1 44.6(2) . 7_565
Mn6A Sb1 Ca1 127.87(15) . 7_565
Mn5 Sb1 Ca1 63.37(8) 5_656 7_565
Mn5 Sb1 Ca1 49.87(8) 5_666 7_565
Mn6B Sb1 Ca1 154.76(9) . 7_565
Ca8 Sb1 Ca1 134.30(8) 5_656 7_565
Ca8 Sb1 Ca1 121.69(8) 5_666 7_565
Q1 Sb1 Ca1 44.6(2) . .
Mn6A Sb1 Ca1 127.87(15) . .
Mn5 Sb1 Ca1 49.87(8) 5_656 .
Mn5 Sb1 Ca1 63.37(8) 5_666 .
Mn6B Sb1 Ca1 154.76(9) . .
Ca8 Sb1 Ca1 121.69(8) 5_656 .
Ca8 Sb1 Ca1 134.30(8) 5_666 .
Ca1 Sb1 Ca1 13.61(12) 7_565 .
Q1 Sb1 Ca5 120.4(2) . .
Mn6A Sb1 Ca5 155.54(15) . .
Mn5 Sb1 Ca5 76.34(6) 5_656 .
Mn5 Sb1 Ca5 76.34(6) 5_666 .
Mn6B Sb1 Ca5 128.09(7) . .
Ca8 Sb1 Ca5 81.94(6) 5_656 .
Ca8 Sb1 Ca5 81.94(6) 5_666 .
Ca1 Sb1 Ca5 76.37(8) 7_565 .
Ca1 Sb1 Ca5 76.37(8) . .
Q1 Sb1 Ca9 56.63(15) . 5_656
Mn6A Sb1 Ca9 57.33(10) . 5_656
Mn5 Sb1 Ca9 59.04(8) 5_656 5_656
Mn5 Sb1 Ca9 127.67(8) 5_666 5_656
Mn6B Sb1 Ca9 75.51(7) . 5_656
Ca8 Sb1 Ca9 75.76(7) 5_656 5_656
Ca8 Sb1 Ca9 138.32(8) 5_666 5_656
Ca1 Sb1 Ca9 91.40(9) 7_565 5_656
Ca1 Sb1 Ca9 82.14(9) . 5_656
Ca5 Sb1 Ca9 134.18(5) . 5_656
Q1 Sb1 Ca9 56.63(15) . 5_666
Mn6A Sb1 Ca9 57.33(10) . 5_666
Mn5 Sb1 Ca9 127.67(8) 5_656 5_666
Mn5 Sb1 Ca9 59.04(8) 5_666 5_666
Mn6B Sb1 Ca9 75.51(7) . 5_666
Ca8 Sb1 Ca9 138.32(8) 5_656 5_666
Ca8 Sb1 Ca9 75.76(7) 5_666 5_666
Ca1 Sb1 Ca9 82.14(9) 7_565 5_666
Ca1 Sb1 Ca9 91.40(9) . 5_666
Ca5 Sb1 Ca9 134.18(5) . 5_666
Ca9 Sb1 Ca9 85.65(8) 5_656 5_666
Mn3 Sb2 Mn3 116.10(15) 5_656 5_666
Mn3 Sb2 Mn1 121.36(8) 5_656 .
Mn3 Sb2 Mn1 121.36(8) 5_666 .
Mn3 Sb2 Ca7 69.06(9) 5_656 5_656
Mn3 Sb2 Ca7 150.88(10) 5_666 5_656
Mn1 Sb2 Ca7 66.97(5) . 5_656
Mn3 Sb2 Ca7 150.88(10) 5_656 5_666
Mn3 Sb2 Ca7 69.06(9) 5_666 5_666
Mn1 Sb2 Ca7 66.97(5) . 5_666
Ca7 Sb2 Ca7 93.00(6) 5_656 5_666
Mn3 Sb2 Ca6 55.67(10) 5_656 2_554
Mn3 Sb2 Ca6 130.36(10) 5_666 2_554
Mn1 Sb2 Ca6 78.21(6) . 2_554
Ca7 Sb2 Ca6 77.38(5) 5_656 2_554
Ca7 Sb2 Ca6 144.81(7) 5_666 2_554
Mn3 Sb2 Ca6 130.36(10) 5_656 2_564
Mn3 Sb2 Ca6 55.66(10) 5_666 2_564
Mn1 Sb2 Ca6 78.22(6) . 2_564
Ca7 Sb2 Ca6 144.81(7) 5_656 2_564
Ca7 Sb2 Ca6 77.38(5) 5_666 2_564
Ca6 Sb2 Ca6 91.12(7) 2_554 2_564
Mn3 Sb2 Ca2 58.67(8) 5_656 .
Mn3 Sb2 Ca2 58.67(8) 5_666 .
Mn1 Sb2 Ca2 158.78(6) . .
Ca7 Sb2 Ca2 124.73(4) 5_656 .
Ca7 Sb2 Ca2 124.73(4) 5_666 .
Ca6 Sb2 Ca2 87.02(6) 2_554 .
Ca6 Sb2 Ca2 87.02(6) 2_564 .
Mn3 Sb2 Ca5 76.01(9) 5_656 .
Mn3 Sb2 Ca5 76.01(9) 5_666 .
Mn1 Sb2 Ca5 127.67(6) . .
Ca7 Sb2 Ca5 77.93(5) 5_656 .
Ca7 Sb2 Ca5 77.93(5) 5_666 .
Ca6 Sb2 Ca5 130.91(5) 2_554 .
Ca6 Sb2 Ca5 130.91(5) 2_564 .
Ca2 Sb2 Ca5 73.55(6) . .
Mn2 Sb3 Mn2 113.44(6) 5_656 5_666
Mn2 Sb3 Ca8 115.65(4) 5_656 .
Mn2 Sb3 Ca8 115.65(4) 5_666 .
Mn2 Sb3 Ca7 76.33(4) 5_656 .
Mn2 Sb3 Ca7 76.33(4) 5_666 .
Ca8 Sb3 Ca7 153.43(7) . .
Mn2 Sb3 Ca4 79.26(5) 5_656 .
Mn2 Sb3 Ca4 79.26(5) 5_666 .
Ca8 Sb3 Ca4 71.93(7) . .
Ca7 Sb3 Ca4 134.64(7) . .
Mn2 Sb3 Ca5 73.65(4) 5_656 5_656
Mn2 Sb3 Ca5 151.12(6) 5_666 5_656
Ca8 Sb3 Ca5 82.31(5) . 5_656
Ca7 Sb3 Ca5 78.60(5) . 5_656
Ca4 Sb3 Ca5 129.26(4) . 5_656
Mn2 Sb3 Ca5 151.12(6) 5_656 5_666
Mn2 Sb3 Ca5 73.65(4) 5_666 5_666
Ca8 Sb3 Ca5 82.31(6) . 5_666
Ca7 Sb3 Ca5 78.60(5) . 5_666
Ca4 Sb3 Ca5 129.26(4) . 5_666
Ca5 Sb3 Ca5 87.58(6) 5_656 5_666
Mn1 Sb4 Mn1 114.05(6) 5_656 5_666
Mn1 Sb4 Ca3 110.14(4) 5_656 6_657
Mn1 Sb4 Ca3 110.14(4) 5_666 6_657
Mn1 Sb4 Ca2 76.25(4) 5_656 2
Mn1 Sb4 Ca2 162.03(6) 5_666 2
Ca3 Sb4 Ca2 77.73(5) 6_657 2
Mn1 Sb4 Ca2 162.03(6) 5_656 2_565
Mn1 Sb4 Ca2 76.25(4) 5_666 2_565
Ca3 Sb4 Ca2 77.73(5) 6_657 2_565
Ca2 Sb4 Ca2 90.25(6) 2 2_565
Mn1 Sb4 Ca6 80.18(5) 5_656 .
Mn1 Sb4 Ca6 80.18(5) 5_666 .
Ca3 Sb4 Ca6 159.02(7) 6_657 .
Ca2 Sb4 Ca6 87.56(6) 2 .
Ca2 Sb4 Ca6 87.56(6) 2_565 .
Mn1 Sb4 Ca6 75.54(5) 5_656 6_657
Mn1 Sb4 Ca6 75.54(5) 5_666 6_657
Ca3 Sb4 Ca6 66.56(7) 6_657 6_657
Ca2 Sb4 Ca6 122.20(5) 2 6_657
Ca2 Sb4 Ca6 122.19(5) 2_565 6_657
Ca6 Sb4 Ca6 134.42(3) . 6_657
Mn6B Sb5 Mn6B 113.61(9) 5_656 5_666
Mn6B Sb5 Mn6A 27.36(14) 5_656 5_656
Mn6B Sb5 Mn6A 120.37(12) 5_666 5_656
Mn6B Sb5 Mn6A 120.37(12) 5_656 5_666
Mn6B Sb5 Mn6A 27.36(14) 5_666 5_666
Mn6A Sb5 Mn6A 112.8(2) 5_656 5_666
Mn6B Sb5 Mn6B 74.53(6) 5_656 .
Mn6B Sb5 Mn6B 74.53(6) 5_666 .
Mn6A Sb5 Mn6B 101.82(14) 5_656 .
Mn6A Sb5 Mn6B 101.82(13) 5_666 .
Mn6B Sb5 Ca9 77.46(6) 5_656 .
Mn6B Sb5 Ca9 77.46(6) 5_666 .
Mn6A Sb5 Ca9 57.80(12) 5_656 .
Mn6A Sb5 Ca9 57.80(11) 5_666 .
Mn6B Sb5 Ca9 127.48(8) . .
Mn6B Sb5 Ca8 63.06(7) 5_656 5_656
Mn6B Sb5 Ca8 134.80(7) 5_666 5_656
Mn6A Sb5 Ca8 78.36(12) 5_656 5_656
Mn6A Sb5 Ca8 161.87(13) 5_666 5_656
Mn6B Sb5 Ca8 60.93(5) . 5_656
Ca9 Sb5 Ca8 136.03(4) . 5_656
Mn6B Sb5 Ca8 134.80(7) 5_656 5_666
Mn6B Sb5 Ca8 63.06(7) 5_666 5_666
Mn6A Sb5 Ca8 161.87(13) 5_656 5_666
Mn6A Sb5 Ca8 78.36(12) 5_666 5_666
Mn6B Sb5 Ca8 60.93(5) . 5_666
Ca9 Sb5 Ca8 136.02(4) . 5_666
Ca8 Sb5 Ca8 87.53(7) 5_656 5_666
Mn6B Sb5 Ca4 76.97(6) 5_656 5_656
Mn6B Sb5 Ca4 156.81(7) 5_666 5_656
Mn6A Sb5 Ca4 59.77(13) 5_656 5_656
Mn6A Sb5 Ca4 129.46(14) 5_666 5_656
Mn6B Sb5 Ca4 128.65(5) . 5_656
Ca9 Sb5 Ca4 85.37(6) . 5_656
Ca8 Sb5 Ca4 68.22(6) 5_656 5_656
Ca8 Sb5 Ca4 125.10(6) 5_666 5_656
Mn6B Sb5 Ca4 156.81(7) 5_656 5_666
Mn6B Sb5 Ca4 76.97(6) 5_666 5_666
Mn6A Sb5 Ca4 129.46(14) 5_656 5_666
Mn6A Sb5 Ca4 59.77(13) 5_666 5_666
Mn6B Sb5 Ca4 128.65(5) . 5_666
Ca9 Sb5 Ca4 85.37(6) . 5_666
Ca8 Sb5 Ca4 125.10(6) 5_656 5_666
Ca8 Sb5 Ca4 68.22(6) 5_666 5_666
Ca4 Sb5 Ca4 86.29(7) 5_656 5_666
Mn6B Sb5 Ca8 56.87(5) 5_656 .
Mn6B Sb5 Ca8 56.88(5) 5_666 .
Mn6A Sb5 Ca8 71.16(13) 5_656 .
Mn6A Sb5 Ca8 71.16(13) 5_666 .
Mn6B Sb5 Ca8 57.39(7) . .
Ca9 Sb5 Ca8 70.09(7) . .
Ca8 Sb5 Ca8 100.84(6) 5_656 .
Ca8 Sb5 Ca8 100.84(6) 5_666 .
Ca4 Sb5 Ca8 130.87(4) 5_656 .
Ca4 Sb5 Ca8 130.87(4) 5_666 .
Mn2 Sb6 Mn1 121.72(5) . .
Mn2 Sb6 Ca7 74.34(5) . 5_656
Mn1 Sb6 Ca7 66.10(4) . 5_656
Mn2 Sb6 Ca7 74.34(5) . 5_666
Mn1 Sb6 Ca7 66.10(4) . 5_666
Ca7 Sb6 Ca7 91.53(6) 5_656 5_666
Mn2 Sb6 Ca3 67.11(5) . 5_656
Mn1 Sb6 Ca3 134.41(3) . 5_656
Ca7 Sb6 Ca3 75.99(5) 5_656 5_656
Ca7 Sb6 Ca3 141.35(6) 5_666 5_656
Mn2 Sb6 Ca3 67.11(5) . 5_666
Mn1 Sb6 Ca3 134.41(3) . 5_666
Ca7 Sb6 Ca3 141.35(6) 5_656 5_666
Ca7 Sb6 Ca3 75.99(5) 5_666 5_666
Ca3 Sb6 Ca3 91.12(6) 5_656 5_666
Mn2 Sb6 Ca6 132.43(4) . 5_656
Mn1 Sb6 Ca6 79.39(6) . 5_656
Ca7 Sb6 Ca6 78.59(5) 5_656 5_656
Ca7 Sb6 Ca6 145.09(7) 5_666 5_656
Ca3 Sb6 Ca6 68.81(6) 5_656 5_656
Ca3 Sb6 Ca6 130.76(6) 5_666 5_656
Mn2 Sb6 Ca6 132.43(4) . 5_666
Mn1 Sb6 Ca6 79.39(6) . 5_666
Ca7 Sb6 Ca6 145.09(7) 5_656 5_666
Ca7 Sb6 Ca6 78.59(5) 5_666 5_666
Ca3 Sb6 Ca6 130.76(6) 5_656 5_666
Ca3 Sb6 Ca6 68.81(6) 5_666 5_666
Ca6 Sb6 Ca6 90.53(7) 5_656 5_666
Mn3 Sb7 Mn4 125.99(13) . 1_655
Mn3 Sb7 Mn5 157.78(13) . .
Mn4 Sb7 Mn5 76.24(10) 1_655 .
Mn3 Sb7 Ca1 139.85(7) . 5_656
Mn4 Sb7 Ca1 50.61(8) 1_655 5_656
Mn5 Sb7 Ca1 51.62(8) . 5_656
Mn3 Sb7 Ca1 139.85(8) . 3_656
Mn4 Sb7 Ca1 50.61(8) 1_655 3_656
Mn5 Sb7 Ca1 51.62(8) . 3_656
Ca1 Sb7 Ca1 74.12(13) 5_656 3_656
Mn3 Sb7 Ca5 82.76(8) . 5_656
Mn4 Sb7 Ca5 128.63(5) 1_655 5_656
Mn5 Sb7 Ca5 81.92(6) . 5_656
Ca1 Sb7 Ca5 79.45(8) 5_656 5_656
Ca1 Sb7 Ca5 133.43(8) 3_656 5_656
Mn3 Sb7 Ca5 82.76(8) . 5_666
Mn4 Sb7 Ca5 128.63(5) 1_655 5_666
Mn5 Sb7 Ca5 81.92(6) . 5_666
Ca1 Sb7 Ca5 133.43(8) 5_656 5_666
Ca1 Sb7 Ca5 79.45(8) 3_656 5_666
Ca5 Sb7 Ca5 92.49(6) 5_656 5_666
Mn3 Sb7 Ca2 62.40(7) . 5_656
Mn4 Sb7 Ca2 81.17(7) 1_655 5_656
Mn5 Sb7 Ca2 128.89(5) . 5_656
Ca1 Sb7 Ca2 78.68(7) 5_656 5_656
Ca1 Sb7 Ca2 131.55(8) 3_656 5_656
Ca5 Sb7 Ca2 77.54(5) 5_656 5_656
Ca5 Sb7 Ca2 144.54(6) 5_666 5_656
Mn3 Sb7 Ca2 62.40(7) . 5_666
Mn4 Sb7 Ca2 81.17(7) 1_655 5_666
Mn5 Sb7 Ca2 128.89(5) . 5_666
Ca1 Sb7 Ca2 131.55(8) 5_656 5_666
Ca1 Sb7 Ca2 78.68(8) 3_656 5_666
Ca5 Sb7 Ca2 144.54(6) 5_656 5_666
Ca5 Sb7 Ca2 77.54(5) 5_666 5_666
Ca2 Sb7 Ca2 90.99(6) 5_656 5_666
Mn3 Sb7 Ca1 131.16(6) . 3_646
Mn4 Sb7 Ca1 56.87(7) 1_655 3_646
Mn5 Sb7 Ca1 57.68(7) . 3_646
Ca1 Sb7 Ca1 9.53(9) 5_656 3_646
Ca1 Sb7 Ca1 83.66(8) 3_656 3_646
Ca5 Sb7 Ca1 72.09(7) 5_656 3_646
Ca5 Sb7 Ca1 137.89(7) 5_666 3_646
Ca2 Sb7 Ca1 71.51(7) 5_656 3_646
Ca2 Sb7 Ca1 135.99(8) 5_666 3_646
Mn3 Sb7 Ca1 131.16(6) . 5_666
Mn4 Sb7 Ca1 56.87(7) 1_655 5_666
Mn5 Sb7 Ca1 57.68(7) . 5_666
Ca1 Sb7 Ca1 83.66(8) 5_656 5_666
Ca1 Sb7 Ca1 9.53(9) 3_656 5_666
Ca5 Sb7 Ca1 137.89(7) 5_656 5_666
Ca5 Sb7 Ca1 72.09(7) 5_666 5_666
Ca2 Sb7 Ca1 135.99(8) 5_656 5_666
Ca2 Sb7 Ca1 71.51(7) 5_666 5_666
Ca1 Sb7 Ca1 93.19(11) 3_646 5_666
Mn4 Sb8 Mn4 109.49(11) 5_656 5_666
Mn4 Sb8 Mn2 124.75(6) 5_656 .
Mn4 Sb8 Mn2 124.75(6) 5_666 .
Mn4 Sb8 Ca3 70.70(7) 5_656 5_656
Mn4 Sb8 Ca3 149.20(8) 5_666 5_656
Mn2 Sb8 Ca3 68.19(5) . 5_656
Mn4 Sb8 Ca3 149.20(8) 5_656 5_666
Mn4 Sb8 Ca3 70.70(7) 5_666 5_666
Mn2 Sb8 Ca3 68.19(5) . 5_666
Ca3 Sb8 Ca3 93.48(7) 5_656 5_666
Mn4 Sb8 Ca1 49.03(8) 5_656 1_655
Mn4 Sb8 Ca1 62.64(8) 5_666 1_655
Mn2 Sb8 Ca1 156.63(8) . 1_655
Ca3 Sb8 Ca1 118.12(7) 5_656 1_655
Ca3 Sb8 Ca1 130.25(8) 5_666 1_655
Mn4 Sb8 Ca1 62.64(8) 5_656 7_665
Mn4 Sb8 Ca1 49.03(8) 5_666 7_665
Mn2 Sb8 Ca1 156.63(8) . 7_665
Ca3 Sb8 Ca1 130.25(8) 5_656 7_665
Ca3 Sb8 Ca1 118.12(7) 5_666 7_665
Ca1 Sb8 Ca1 13.79(12) 1_655 7_665
Mn4 Sb8 Ca4 59.52(7) 5_656 5_656
Mn4 Sb8 Ca4 129.32(8) 5_666 5_656
Mn2 Sb8 Ca4 77.29(5) . 5_656
Ca3 Sb8 Ca4 78.56(5) 5_656 5_656
Ca3 Sb8 Ca4 145.00(7) 5_666 5_656
Ca1 Sb8 Ca4 81.99(8) 1_655 5_656
Ca1 Sb8 Ca4 91.62(8) 7_665 5_656
Mn4 Sb8 Ca4 129.33(8) 5_656 5_666
Mn4 Sb8 Ca4 59.52(7) 5_666 5_666
Mn2 Sb8 Ca4 77.29(5) . 5_666
Ca3 Sb8 Ca4 145.00(7) 5_656 5_666
Ca3 Sb8 Ca4 78.56(5) 5_666 5_666
Ca1 Sb8 Ca4 91.62(8) 1_655 5_666
Ca1 Sb8 Ca4 81.99(8) 7_665 5_666
Ca4 Sb8 Ca4 88.63(7) 5_656 5_666
Mn4 Sb8 Ca2 74.61(7) 5_656 1_655
Mn4 Sb8 Ca2 74.61(7) 5_666 1_655
Mn2 Sb8 Ca2 126.48(6) . 1_655
Ca3 Sb8 Ca2 75.98(5) 5_656 1_655
Ca3 Sb8 Ca2 75.98(5) 5_666 1_655
Ca1 Sb8 Ca2 76.01(8) 1_655 1_655
Ca1 Sb8 Ca2 76.01(8) 7_665 1_655
Ca4 Sb8 Ca2 132.71(4) 5_656 1_655
Ca4 Sb8 Ca2 132.71(4) 5_666 1_655
Sb9B Sb9A Ca1 132.46(10) . 5_556
Sb9B Sb9A Ca1 132.46(10) . 3_556
Ca1 Sb9A Ca1 94.02(16) 5_556 3_556
Sb9B Sb9A Q1 97.1(3) . 5_556
Ca1 Sb9A Q1 50.2(2) 5_556 5_556
Ca1 Sb9A Q1 125.3(2) 3_556 5_556
Sb9B Sb9A Q1 97.1(3) . 5_566
Ca1 Sb9A Q1 125.3(2) 5_556 5_566
Ca1 Sb9A Q1 50.2(2) 3_556 5_566
Q1 Sb9A Q1 112.7(4) 5_556 5_566
Sb9B Sb9A Mn5 151.9(3) . 1_455
Ca1 Sb9A Mn5 56.60(9) 5_556 1_455
Ca1 Sb9A Mn5 56.60(9) 3_556 1_455
Q1 Sb9A Mn5 68.7(2) 5_556 1_455
Q1 Sb9A Mn5 68.7(2) 5_566 1_455
Sb9B Sb9A Mn4 138.9(3) . .
Ca1 Sb9A Mn4 55.13(9) 5_556 .
Ca1 Sb9A Mn4 55.13(9) 3_556 .
Q1 Sb9A Mn4 105.2(2) 5_556 .
Q1 Sb9A Mn4 105.2(2) 5_566 .
Mn5 Sb9A Mn4 69.20(10) 1_455 .
Sb9B Sb9A Ca1 123.28(8) . 3_546
Ca1 Sb9A Ca1 9.33(8) 5_556 3_546
Ca1 Sb9A Ca1 103.35(12) 3_556 3_546
Q1 Sb9A Ca1 44.1(2) 5_556 3_546
Q1 Sb9A Ca1 131.9(2) 5_566 3_546
Mn5 Sb9A Ca1 63.42(8) 1_455 3_546
Mn4 Sb9A Ca1 62.31(7) . 3_546
Sb9B Sb9A Ca1 123.28(8) . 5_566
Ca1 Sb9A Ca1 103.35(12) 5_556 5_566
Ca1 Sb9A Ca1 9.33(9) 3_556 5_566
Q1 Sb9A Ca1 131.9(2) 5_556 5_566
Q1 Sb9A Ca1 44.1(2) 5_566 5_566
Mn5 Sb9A Ca1 63.42(7) 1_455 5_566
Mn4 Sb9A Ca1 62.31(7) . 5_566
Ca1 Sb9A Ca1 112.68(14) 3_546 5_566
Sb9B Sb9A Ca4 78.7(3) . .
Ca1 Sb9A Ca4 92.18(9) 5_556 .
Ca1 Sb9A Ca4 92.18(9) 3_556 .
Q1 Sb9A Ca4 123.64(19) 5_556 .
Q1 Sb9A Ca4 123.63(19) 5_566 .
Mn5 Sb9A Ca4 129.35(9) 1_455 .
Mn4 Sb9A Ca4 60.16(8) . .
Ca1 Sb9A Ca4 91.77(8) 3_546 .
Ca1 Sb9A Ca4 91.77(8) 5_566 .
Sb9B Sb9A Ca9 91.3(3) . 1_455
Ca1 Sb9A Ca9 94.60(10) 5_556 1_455
Ca1 Sb9A Ca9 94.60(10) 3_556 1_455
Q1 Sb9A Ca9 57.12(19) 5_556 1_455
Q1 Sb9A Ca9 57.12(19) 5_566 1_455
Mn5 Sb9A Ca9 60.59(9) 1_455 1_455
Mn4 Sb9A Ca9 129.78(10) . 1_455
Ca1 Sb9A Ca9 93.74(8) 3_546 1_455
Ca1 Sb9A Ca9 93.73(8) 5_566 1_455
Ca4 Sb9A Ca9 170.06(9) . 1_455
Sb9B Sb9A Ca9 44.39(6) . 5_656
Ca1 Sb9A Ca9 89.05(9) 5_556 5_656
Ca1 Sb9A Ca9 176.85(10) 3_556 5_656
Q1 Sb9A Ca9 57.5(2) 5_556 5_656
Q1 Sb9A Ca9 128.1(2) 5_566 5_656
Mn5 Sb9A Ca9 126.04(7) 1_455 5_656
Mn4 Sb9A Ca9 126.66(7) . 5_656
Ca1 Sb9A Ca9 79.72(7) 3_546 5_656
Ca1 Sb9A Ca9 167.58(9) 5_566 5_656
Ca4 Sb9A Ca9 87.01(8) . 5_656
Ca9 Sb9A Ca9 85.83(8) 1_455 5_656
Sb9A Sb9B Q1 134.2(4) . .
Sb9A Sb9B Ca9 126.99(8) . 5_656
Q1 Sb9B Ca9 60.49(12) . 5_656
Sb9A Sb9B Ca9 126.99(8) . 5_666
Q1 Sb9B Ca9 60.49(12) . 5_666
Ca9 Sb9B Ca9 104.78(13) 5_656 5_666
Sb9A Sb9B Q1 70.7(3) . 5_556
Q1 Sb9B Q1 82.1(3) . 5_556
Ca9 Sb9B Q1 61.3(2) 5_656 5_556
Ca9 Sb9B Q1 140.7(2) 5_666 5_556
Sb9A Sb9B Q1 70.7(3) . 5_566
Q1 Sb9B Q1 82.1(3) . 5_566
Ca9 Sb9B Q1 140.7(2) 5_656 5_566
Ca9 Sb9B Q1 61.3(2) 5_666 5_566
Q1 Sb9B Q1 104.7(3) 5_556 5_566
Sb9A Sb9B Mn6A 151.1(4) . .
Q1 Sb9B Mn6A 74.7(3) . .
Ca9 Sb9B Mn6A 61.49(9) 5_656 .
Ca9 Sb9B Mn6A 61.49(9) 5_666 .
Q1 Sb9B Mn6A 122.57(19) 5_556 .
Q1 Sb9B Mn6A 122.6(2) 5_566 .
Sb9A Sb9B Ca1 38.96(8) . 5_556
Q1 Sb9B Ca1 126.91(16) . 5_556
Ca9 Sb9B Ca1 88.99(8) 5_656 5_556
Ca9 Sb9B Ca1 165.95(11) 5_666 5_556
Q1 Sb9B Ca1 44.8(2) 5_556 5_556
Q1 Sb9B Ca1 106.1(2) 5_566 5_556
Mn6A Sb9B Ca1 129.87(11) . 5_556
Sb9A Sb9B Ca1 38.96(8) . 3_556
Q1 Sb9B Ca1 126.91(16) . 3_556
Ca9 Sb9B Ca1 165.95(11) 5_656 3_556
Ca9 Sb9B Ca1 88.99(8) 5_666 3_556
Q1 Sb9B Ca1 106.1(2) 5_556 3_556
Q1 Sb9B Ca1 44.8(2) 5_566 3_556
Mn6A Sb9B Ca1 129.87(11) . 3_556
Ca1 Sb9B Ca1 77.13(14) 5_556 3_556
Sb9A Sb9B Ca4 90.2(3) . .
Q1 Sb9B Ca4 135.6(2) . .
Ca9 Sb9B Ca4 95.70(10) 5_656 .
Ca9 Sb9B Ca4 95.70(10) 5_666 .
Q1 Sb9B Ca4 121.00(19) 5_556 .
Q1 Sb9B Ca4 121.00(19) 5_566 .
Mn6A Sb9B Ca4 60.82(14) . .
Ca1 Sb9B Ca4 85.51(10) 5_556 .
Ca1 Sb9B Ca4 85.51(10) 3_556 .
Sb9A Sb9B Ca9 77.9(3) . 1_455
Q1 Sb9B Ca9 56.2(2) . 1_455
Ca9 Sb9B Ca9 91.49(10) 5_656 1_455
Ca9 Sb9B Ca9 91.49(10) 5_666 1_455
Q1 Sb9B Ca9 55.14(18) 5_556 1_455
Q1 Sb9B Ca9 55.14(18) 5_566 1_455
Mn6A Sb9B Ca9 130.99(16) . 1_455
Ca1 Sb9B Ca9 85.26(10) 5_556 1_455
Ca1 Sb9B Ca9 85.26(10) 3_556 1_455
Ca4 Sb9B Ca9 168.19(12) . 1_455
Sb9A Sb9B Ca1 48.42(7) . 3_546
Q1 Sb9B Ca1 120.84(13) . 3_546
Ca9 Sb9B Ca1 79.42(8) 5_656 3_546
Ca9 Sb9B Ca1 175.16(11) 5_666 3_546
Q1 Sb9B Ca1 39.3(2) 5_556 3_546
Q1 Sb9B Ca1 113.9(2) 5_566 3_546
Mn6A Sb9B Ca1 123.17(9) . 3_546
Ca1 Sb9B Ca1 9.57(9) 5_556 3_546
Ca1 Sb9B Ca1 86.70(11) 3_556 3_546
Ca4 Sb9B Ca1 86.17(8) . 3_546
Ca9 Sb9B Ca1 85.96(9) 1_455 3_546
Sb4 Mn1 Sb4 114.04(6) 5_656 5_666
Sb4 Mn1 Sb2 113.23(4) 5_656 .
Sb4 Mn1 Sb2 113.23(4) 5_666 .
Sb4 Mn1 Sb6 108.54(4) 5_656 .
Sb4 Mn1 Sb6 108.54(4) 5_666 .
Sb2 Mn1 Sb6 97.83(5) . .
Sb4 Mn1 Ca7 79.12(3) 5_656 5_656
Sb4 Mn1 Ca7 166.40(6) 5_666 5_656
Sb2 Mn1 Ca7 61.36(5) . 5_656
Sb6 Mn1 Ca7 61.98(5) . 5_656
Sb4 Mn1 Ca7 166.40(6) 5_656 5_666
Sb4 Mn1 Ca7 79.12(3) 5_666 5_666
Sb2 Mn1 Ca7 61.36(5) . 5_666
Sb6 Mn1 Ca7 61.98(5) . 5_666
Ca7 Mn1 Ca7 87.55(7) 5_656 5_666
Sb4 Mn1 Ca2 58.00(3) 5_656 6_656
Sb4 Mn1 Ca2 58.00(3) 5_666 6_656
Sb2 Mn1 Ca2 149.61(7) . 6_656
Sb6 Mn1 Ca2 112.56(7) . 6_656
Ca7 Mn1 Ca2 133.36(4) 5_656 6_656
Ca7 Mn1 Ca2 133.36(4) 5_666 6_656
Sb3 Mn2 Sb3 113.43(6) 5_656 5_666
Sb3 Mn2 Sb8 110.28(4) 5_656 .
Sb3 Mn2 Sb8 110.28(4) 5_666 .
Sb3 Mn2 Sb6 112.12(4) 5_656 .
Sb3 Mn2 Sb6 112.12(4) 5_666 .
Sb8 Mn2 Sb6 97.51(5) . .
Sb3 Mn2 Ca3 80.14(3) 5_656 5_656
Sb3 Mn2 Ca3 166.25(6) 5_666 5_656
Sb8 Mn2 Ca3 60.60(5) . 5_656
Sb6 Mn2 Ca3 61.86(5) . 5_656
Sb3 Mn2 Ca3 166.25(6) 5_656 5_666
Sb3 Mn2 Ca3 80.14(3) 5_666 5_666
Sb8 Mn2 Ca3 60.60(5) . 5_666
Sb6 Mn2 Ca3 61.86(5) . 5_666
Ca3 Mn2 Ca3 86.22(7) 5_656 5_666
Sb3 Mn2 Ca7 56.88(4) 5_656 5_656
Sb3 Mn2 Ca7 120.14(6) 5_666 5_656
Sb8 Mn2 Ca7 128.94(5) . 5_656
Sb6 Mn2 Ca7 57.44(4) . 5_656
Ca3 Mn2 Ca7 68.37(5) 5_656 5_656
Ca3 Mn2 Ca7 119.25(7) 5_666 5_656
Sb3 Mn2 Ca7 120.14(6) 5_656 5_666
Sb3 Mn2 Ca7 56.88(4) 5_666 5_666
Sb8 Mn2 Ca7 128.94(5) . 5_666
Sb6 Mn2 Ca7 57.44(4) . 5_666
Ca3 Mn2 Ca7 119.25(7) 5_656 5_666
Ca3 Mn2 Ca7 68.37(5) 5_666 5_666
Ca7 Mn2 Ca7 77.68(5) 5_656 5_666
Sb3 Mn2 Ca5 60.34(3) 5_656 .
Sb3 Mn2 Ca5 60.34(3) 5_666 .
Sb8 Mn2 Ca5 154.78(7) . .
Sb6 Mn2 Ca5 107.71(6) . .
Ca3 Mn2 Ca5 132.40(4) 5_656 .
Ca3 Mn2 Ca5 132.40(4) 5_666 .
Ca7 Mn2 Ca5 68.12(5) 5_656 .
Ca7 Mn2 Ca5 68.12(5) 5_666 .
Sb7 Mn3 Sb2 113.28(10) . 5_656
Sb7 Mn3 Sb2 113.28(10) . 5_666
Sb2 Mn3 Sb2 116.10(15) 5_656 5_666
Sb7 Mn3 Ca6 168.7(2) . 6_657
Sb2 Mn3 Ca6 71.43(9) 5_656 6_657
Sb2 Mn3 Ca6 71.43(9) 5_666 6_657
Sb7 Mn3 Ca2 71.26(10) . 5_656
Sb2 Mn3 Ca2 71.22(4) 5_656 5_656
Sb2 Mn3 Ca2 166.27(17) 5_666 5_656
Ca6 Mn3 Ca2 101.80(12) 6_657 5_656
Sb7 Mn3 Ca2 71.26(10) . 5_666
Sb2 Mn3 Ca2 166.27(17) 5_656 5_666
Sb2 Mn3 Ca2 71.22(4) 5_666 5_666
Ca6 Mn3 Ca2 101.80(12) 6_657 5_666
Ca2 Mn3 Ca2 99.30(14) 5_656 5_666
Sb7 Mn3 Ca7 111.00(15) . .
Sb2 Mn3 Ca7 61.95(8) 5_656 .
Sb2 Mn3 Ca7 61.96(8) 5_666 .
Ca6 Mn3 Ca7 80.32(12) 6_657 .
Ca2 Mn3 Ca7 129.79(7) 5_656 .
Ca2 Mn3 Ca7 129.79(7) 5_666 .
Sb7 Mn3 Ca5 56.86(8) . 5_656
Sb2 Mn3 Ca5 59.78(6) 5_656 5_656
Sb2 Mn3 Ca5 122.10(14) 5_666 5_656
Ca6 Mn3 Ca5 130.45(10) 6_657 5_656
Ca2 Mn3 Ca5 71.49(7) 5_656 5_656
Ca2 Mn3 Ca5 127.71(14) 5_666 5_656
Ca7 Mn3 Ca5 70.13(9) . 5_656
Sb7 Mn3 Ca5 56.86(8) . 5_666
Sb2 Mn3 Ca5 122.10(14) 5_656 5_666
Sb2 Mn3 Ca5 59.78(6) 5_666 5_666
Ca6 Mn3 Ca5 130.45(10) 6_657 5_666
Ca2 Mn3 Ca5 127.71(14) 5_656 5_666
Ca2 Mn3 Ca5 71.49(7) 5_666 5_666
Ca7 Mn3 Ca5 70.13(9) . 5_666
Ca5 Mn3 Ca5 75.13(9) 5_656 5_666
Ca1 Mn4 Ca1 99.27(19) 5_556 3_556
Ca1 Mn4 Sb7 77.69(11) 5_556 1_455
Ca1 Mn4 Sb7 77.69(12) 3_556 1_455
Ca1 Mn4 Sb9A 58.72(10) 5_556 .
Ca1 Mn4 Sb9A 58.72(10) 3_556 .
Sb7 Mn4 Sb9A 107.50(12) 1_455 .
Ca1 Mn4 Sb8 73.27(8) 5_556 5_656
Ca1 Mn4 Sb8 163.06(15) 3_556 5_656
Sb7 Mn4 Sb8 114.43(7) 1_455 5_656
Sb9A Mn4 Sb8 105.05(8) . 5_656
Ca1 Mn4 Sb8 163.06(15) 5_556 5_666
Ca1 Mn4 Sb8 73.27(8) 3_556 5_666
Sb7 Mn4 Sb8 114.43(7) 1_455 5_666
Sb9A Mn4 Sb8 105.05(8) . 5_666
Sb8 Mn4 Sb8 109.50(11) 5_656 5_666
Ca1 Mn4 Ca4 98.96(12) 5_556 .
Ca1 Mn4 Ca4 98.96(12) 3_556 .
Sb7 Mn4 Ca4 174.71(14) 1_455 .
Sb9A Mn4 Ca4 67.20(9) . .
Sb8 Mn4 Ca4 68.00(7) 5_656 .
Sb8 Mn4 Ca4 68.00(7) 5_666 .
Ca1 Mn4 Ca1 9.10(8) 5_556 3_546
Ca1 Mn4 Ca1 108.37(16) 3_556 3_546
Sb7 Mn4 Ca1 80.17(9) 1_455 3_546
Sb9A Mn4 Ca1 65.41(8) . 3_546
Sb8 Mn4 Ca1 64.53(7) 5_656 3_546
Sb8 Mn4 Ca1 165.01(14) 5_666 3_546
Ca4 Mn4 Ca1 97.17(10) . 3_546
Ca1 Mn4 Ca1 108.37(16) 5_556 5_566
Ca1 Mn4 Ca1 9.10(8) 3_556 5_566
Sb7 Mn4 Ca1 80.16(9) 1_455 5_566
Sb9A Mn4 Ca1 65.41(8) . 5_566
Sb8 Mn4 Ca1 165.01(14) 5_656 5_566
Sb8 Mn4 Ca1 64.53(7) 5_666 5_566
Ca4 Mn4 Ca1 97.17(10) . 5_566
Ca1 Mn4 Ca1 117.46(17) 3_546 5_566
Ca1 Mn4 Mn5 52.09(10) 5_556 1_455
Ca1 Mn4 Mn5 52.09(10) 3_556 1_455
Sb7 Mn4 Mn5 52.35(8) 1_455 1_455
Sb9A Mn4 Mn5 55.15(8) . 1_455
Sb8 Mn4 Mn5 124.85(6) 5_656 1_455
Sb8 Mn4 Mn5 124.85(6) 5_666 1_455
Ca4 Mn4 Mn5 122.35(12) . 1_455
Ca1 Mn4 Mn5 60.50(8) 3_546 1_455
Ca1 Mn4 Mn5 60.50(9) 5_566 1_455
Ca1 Mn4 Ca3 130.36(10) 5_556 .
Ca1 Mn4 Ca3 130.36(10) 3_556 .
Sb7 Mn4 Ca3 108.10(11) 1_455 .
Sb9A Mn4 Ca3 144.40(12) . .
Sb8 Mn4 Ca3 59.26(6) 5_656 .
Sb8 Mn4 Ca3 59.26(6) 5_666 .
Ca4 Mn4 Ca3 77.20(9) . .
Ca1 Mn4 Ca3 121.26(8) 3_546 .
Ca1 Mn4 Ca3 121.26(8) 5_566 .
Mn5 Mn4 Ca3 160.45(12) 1_455 .
Ca1 Mn4 Ca2 77.17(10) 5_556 5_556
Ca1 Mn4 Ca2 134.56(14) 3_556 5_556
Sb7 Mn4 Ca2 57.12(6) 1_455 5_556
Sb9A Mn4 Ca2 135.86(7) . 5_556
Sb8 Mn4 Ca2 59.70(5) 5_656 5_556
Sb8 Mn4 Ca2 119.04(10) 5_666 5_556
Ca4 Mn4 Ca2 126.45(8) . 5_556
Ca1 Mn4 Ca2 70.98(8) 3_546 5_556
Ca1 Mn4 Ca2 135.26(12) 5_566 5_556
Mn5 Mn4 Ca2 97.40(9) 1_455 5_556
Ca3 Mn4 Ca2 67.42(7) . 5_556
Ca1 Mn5 Ca1 96.58(19) 5_656 3_656
Ca1 Mn5 Sb7 76.17(11) 5_656 .
Ca1 Mn5 Sb7 76.17(11) 3_656 .
Ca1 Mn5 Sb1 74.31(8) 5_656 5_656
Ca1 Mn5 Sb1 164.94(14) 3_656 5_656
Sb7 Mn5 Sb1 112.22(7) . 5_656
Ca1 Mn5 Sb1 164.94(14) 5_656 5_666
Ca1 Mn5 Sb1 74.31(8) 3_656 5_666
Sb7 Mn5 Sb1 112.21(7) . 5_666
Sb1 Mn5 Sb1 111.77(10) 5_656 5_666
Ca1 Mn5 Sb9A 58.43(10) 5_656 1_655
Ca1 Mn5 Sb9A 58.43(10) 3_656 1_655
Sb7 Mn5 Sb9A 107.06(11) . 1_655
Sb1 Mn5 Sb9A 106.56(7) 5_656 1_655
Sb1 Mn5 Sb9A 106.56(7) 5_666 1_655
Ca1 Mn5 Ca9 100.27(12) 5_656 .
Ca1 Mn5 Ca9 100.27(12) 3_656 .
Sb7 Mn5 Ca9 174.50(14) . .
Sb1 Mn5 Ca9 70.33(7) 5_656 .
Sb1 Mn5 Ca9 70.33(7) 5_666 .
Sb9A Mn5 Ca9 67.43(10) 1_655 .
Ca1 Mn5 Q1 46.0(2) 5_656 5_656
Ca1 Mn5 Q1 113.7(2) 3_656 5_656
Sb7 Mn5 Q1 121.34(19) . 5_656
Sb1 Mn5 Q1 51.39(18) 5_656 5_656
Sb1 Mn5 Q1 126.3(2) 5_666 5_656
Sb9A Mn5 Q1 55.28(18) 1_655 5_656
Ca9 Mn5 Q1 55.98(18) . 5_656
Ca1 Mn5 Q1 113.7(2) 5_656 5_666
Ca1 Mn5 Q1 46.0(2) 3_656 5_666
Sb7 Mn5 Q1 121.34(19) . 5_666
Sb1 Mn5 Q1 126.3(2) 5_656 5_666
Sb1 Mn5 Q1 51.39(18) 5_666 5_666
Sb9A Mn5 Q1 55.28(18) 1_655 5_666
Ca9 Mn5 Q1 55.98(18) . 5_666
Q1 Mn5 Q1 94.5(3) 5_656 5_666
Ca1 Mn5 Mn4 50.62(10) 5_656 1_655
Ca1 Mn5 Mn4 50.62(10) 3_656 1_655
Sb7 Mn5 Mn4 51.41(8) . 1_655
Sb1 Mn5 Mn4 124.03(5) 5_656 1_655
Sb1 Mn5 Mn4 124.03(5) 5_666 1_655
Sb9A Mn5 Mn4 55.66(8) 1_655 1_655
Ca9 Mn5 Mn4 123.09(13) . 1_655
Q1 Mn5 Mn4 89.1(2) 5_656 1_655
Q1 Mn5 Mn4 89.1(2) 5_666 1_655
Ca1 Mn5 Ca1 9.22(9) 5_656 3_646
Ca1 Mn5 Ca1 105.80(15) 3_656 3_646
Sb7 Mn5 Ca1 78.88(9) . 3_646
Sb1 Mn5 Ca1 65.31(7) 5_656 3_646
Sb1 Mn5 Ca1 168.22(13) 5_666 3_646
Sb9A Mn5 Ca1 65.00(8) 1_655 3_646
Ca9 Mn5 Ca1 98.28(9) . 3_646
Q1 Mn5 Ca1 42.46(18) 5_656 3_646
Q1 Mn5 Ca1 120.1(2) 5_666 3_646
Mn4 Mn5 Ca1 59.19(8) 1_655 3_646
Ca1 Mn5 Ca1 105.80(15) 5_656 5_666
Ca1 Mn5 Ca1 9.22(8) 3_656 5_666
Sb7 Mn5 Ca1 78.88(9) . 5_666
Sb1 Mn5 Ca1 168.22(13) 5_656 5_666
Sb1 Mn5 Ca1 65.30(7) 5_666 5_666
Sb9A Mn5 Ca1 65.00(8) 1_655 5_666
Ca9 Mn5 Ca1 98.28(9) . 5_666
Q1 Mn5 Ca1 120.1(2) 5_656 5_666
Q1 Mn5 Ca1 42.46(19) 5_666 5_666
Mn4 Mn5 Ca1 59.19(8) 1_655 5_666
Ca1 Mn5 Ca1 115.03(16) 3_646 5_666
Mn6B Mn6A Sb1 81.6(3) . .
Mn6B Mn6A Sb5 75.75(19) . 5_656
Sb1 Mn6A Sb5 117.05(13) . 5_656
Mn6B Mn6A Sb5 75.75(19) . 5_666
Sb1 Mn6A Sb5 117.05(13) . 5_666
Sb5 Mn6A Sb5 112.8(2) 5_656 5_666
Mn6B Mn6A Sb9B 179.1(4) . .
Sb1 Mn6A Sb9B 99.3(2) . .
Sb5 Mn6A Sb9B 103.80(15) 5_656 .
Sb5 Mn6A Sb9B 103.80(15) 5_666 .
Mn6B Mn6A Ca9 121.21(19) . 5_656
Sb1 Mn6A Ca9 73.48(14) . 5_656
Sb5 Mn6A Ca9 70.32(7) 5_656 5_656
Sb5 Mn6A Ca9 162.3(3) 5_666 5_656
Sb9B Mn6A Ca9 59.18(13) . 5_656
Mn6B Mn6A Ca9 121.21(19) . 5_666
Sb1 Mn6A Ca9 73.48(14) . 5_666
Sb5 Mn6A Ca9 162.3(3) 5_656 5_666
Sb5 Mn6A Ca9 70.32(7) 5_666 5_666
Sb9B Mn6A Ca9 59.18(12) . 5_666
Ca9 Mn6A Ca9 101.5(2) 5_656 5_666
Mn6B Mn6A Ca4 115.0(4) . .
Sb1 Mn6A Ca4 163.3(3) . .
Sb5 Mn6A Ca4 69.81(13) 5_656 .
Sb5 Mn6A Ca4 69.81(13) 5_666 .
Sb9B Mn6A Ca4 64.09(14) . .
Ca9 Mn6A Ca4 96.34(16) 5_656 .
Ca9 Mn6A Ca4 96.34(16) 5_666 .
Mn6B Mn6A Ca8 51.05(17) . 5_656
Sb1 Mn6A Ca8 54.74(10) . 5_656
Sb5 Mn6A Ca8 65.57(9) 5_656 5_656
Sb5 Mn6A Ca8 126.2(2) 5_666 5_656
Sb9B Mn6A Ca8 129.51(14) . 5_656
Ca9 Mn6A Ca8 71.36(10) 5_656 5_656
Ca9 Mn6A Ca8 127.9(2) 5_666 5_656
Ca4 Mn6A Ca8 135.30(12) . 5_656
Mn6B Mn6A Ca8 51.05(17) . 5_666
Sb1 Mn6A Ca8 54.74(10) . 5_666
Sb5 Mn6A Ca8 126.2(2) 5_656 5_666
Sb5 Mn6A Ca8 65.57(9) 5_666 5_666
Sb9B Mn6A Ca8 129.51(14) . 5_666
Ca9 Mn6A Ca8 127.9(2) 5_656 5_666
Ca9 Mn6A Ca8 71.36(10) 5_666 5_666
Ca4 Mn6A Ca8 135.30(12) . 5_666
Ca8 Mn6A Ca8 74.18(12) 5_656 5_666
Mn6A Mn6B Sb5 76.90(16) . 5_656
Mn6A Mn6B Sb5 76.90(16) . 5_666
Sb5 Mn6B Sb5 113.62(9) 5_656 5_666
Mn6A Mn6B Sb1 70.9(3) . .
Sb5 Mn6B Sb1 113.38(6) 5_656 .
Sb5 Mn6B Sb1 113.38(6) 5_666 .
Mn6A Mn6B Sb5 175.3(3) . .
Sb5 Mn6B Sb5 105.47(6) 5_656 .
Sb5 Mn6B Sb5 105.47(6) 5_666 .
Sb1 Mn6B Sb5 104.38(8) . .
Mn6A Mn6B Ca8 110.3(2) . 5_656
Sb5 Mn6B Ca8 76.40(4) 5_656 5_656
Sb5 Mn6B Ca8 169.25(9) 5_666 5_656
Sb1 Mn6B Ca8 63.48(7) . 5_656
Sb5 Mn6B Ca8 66.82(7) . 5_656
Mn6A Mn6B Ca8 110.3(2) . 5_666
Sb5 Mn6B Ca8 169.25(9) 5_656 5_666
Sb5 Mn6B Ca8 76.40(4) 5_666 5_666
Sb1 Mn6B Ca8 63.48(7) . 5_666
Sb5 Mn6B Ca8 66.82(7) . 5_666
Ca8 Mn6B Ca8 93.36(10) 5_656 5_666
Mn6A Mn6B Ca8 110.6(3) . .
Sb5 Mn6B Ca8 67.27(6) 5_656 .
Sb5 Mn6B Ca8 67.27(6) 5_666 .
Sb1 Mn6B Ca8 178.45(11) . .
Sb5 Mn6B Ca8 74.06(8) . .
Ca8 Mn6B Ca8 115.61(8) 5_656 .
Ca8 Mn6B Ca8 115.61(8) 5_666 .
Mn6A Mn6B Ca9 41.80(13) . 5_656
Sb5 Mn6B Ca9 57.82(6) 5_656 5_656
Sb5 Mn6B Ca9 118.49(9) 5_666 5_656
Sb1 Mn6B Ca9 59.24(7) . 5_656
Sb5 Mn6B Ca9 136.04(6) . 5_656
Ca8 Mn6B Ca9 69.60(7) 5_656 5_656
Ca8 Mn6B Ca9 121.95(10) 5_666 5_656
Ca8 Mn6B Ca9 121.86(8) . 5_656
Mn6A Mn6B Ca9 41.80(13) . 5_666
Sb5 Mn6B Ca9 118.49(9) 5_656 5_666
Sb5 Mn6B Ca9 57.81(6) 5_666 5_666
Sb1 Mn6B Ca9 59.24(6) . 5_666
Sb5 Mn6B Ca9 136.04(6) . 5_666
Ca8 Mn6B Ca9 121.95(10) 5_656 5_666
Ca8 Mn6B Ca9 69.60(7) 5_666 5_666
Ca8 Mn6B Ca9 121.86(8) . 5_666
Ca9 Mn6B Ca9 74.21(8) 5_656 5_666
Ca1 Q1 Ca1 19.29(19) 7_565 .
Ca1 Q1 Sb1 83.0(3) 7_565 .
Ca1 Q1 Sb1 83.0(3) . .
Ca1 Q1 Sb9A 78.7(3) 7_565 5_556
Ca1 Q1 Sb9A 61.7(2) . 5_556
Sb1 Q1 Sb9A 113.1(2) . 5_556
Ca1 Q1 Sb9A 61.7(2) 7_565 5_566
Ca1 Q1 Sb9A 78.7(3) . 5_566
Sb1 Q1 Sb9A 113.1(2) . 5_566
Sb9A Q1 Sb9A 112.7(4) 5_556 5_566
Ca1 Q1 Sb9B 169.2(2) 7_565 .
Ca1 Q1 Sb9B 169.2(2) . .
Sb1 Q1 Sb9B 102.0(4) . .
Sb9A Q1 Sb9B 107.5(3) 5_556 .
Sb9A Q1 Sb9B 107.5(3) 5_566 .
Ca1 Q1 Sb9B 87.0(3) 7_565 5_556
Ca1 Q1 Sb9B 71.5(2) . 5_556
Sb1 Q1 Sb9B 123.6(2) . 5_556
Sb9A Q1 Sb9B 12.26(5) 5_556 5_556
Sb9A Q1 Sb9B 109.9(4) 5_566 5_556
Sb9B Q1 Sb9B 97.9(3) . 5_556
Ca1 Q1 Sb9B 71.5(2) 7_565 5_566
Ca1 Q1 Sb9B 87.0(3) . 5_566
Sb1 Q1 Sb9B 123.6(2) . 5_566
Sb9A Q1 Sb9B 109.9(4) 5_556 5_566
Sb9A Q1 Sb9B 12.26(5) 5_566 5_566
Sb9B Q1 Sb9B 97.9(3) . 5_566
Sb9B Q1 Sb9B 104.7(3) 5_556 5_566
Ca1 Q1 Ca9 130.7(3) 7_565 5_656
Ca1 Q1 Ca9 112.8(2) . 5_656
Sb1 Q1 Ca9 75.7(2) . 5_656
Sb9A Q1 Ca9 70.17(7) 5_556 5_656
Sb9A Q1 Ca9 166.9(4) 5_566 5_656
Sb9B Q1 Ca9 60.0(2) . 5_656
Sb9B Q1 Ca9 70.00(10) 5_556 5_656
Sb9B Q1 Ca9 155.0(4) 5_566 5_656
Ca1 Q1 Ca9 112.8(2) 7_565 5_666
Ca1 Q1 Ca9 130.7(3) . 5_666
Sb1 Q1 Ca9 75.7(2) . 5_666
Sb9A Q1 Ca9 166.9(4) 5_556 5_666
Sb9A Q1 Ca9 70.17(7) 5_566 5_666
Sb9B Q1 Ca9 60.0(2) . 5_666
Sb9B Q1 Ca9 155.0(4) 5_556 5_666
Sb9B Q1 Ca9 70.00(10) 5_566 5_666
Ca9 Q1 Ca9 104.1(4) 5_656 5_666
Ca1 Q1 Ca9 105.3(4) 7_565 1_455
Ca1 Q1 Ca9 105.3(4) . 1_455
Sb1 Q1 Ca9 171.6(4) . 1_455
Sb9A Q1 Ca9 70.7(2) 5_556 1_455
Sb9A Q1 Ca9 70.7(2) 5_566 1_455
Sb9B Q1 Ca9 69.6(3) . 1_455
Sb9B Q1 Ca9 59.31(19) 5_556 1_455
Sb9B Q1 Ca9 59.3(2) 5_566 1_455
Ca9 Q1 Ca9 99.4(3) 5_656 1_455
Ca9 Q1 Ca9 99.4(3) 5_666 1_455
Ca1 Q1 Mn5 69.9(3) 7_565 5_656
Ca1 Q1 Mn5 53.87(19) . 5_656
Sb1 Q1 Mn5 57.21(18) . 5_656
Sb9A Q1 Mn5 56.01(11) 5_556 5_656
Sb9A Q1 Mn5 131.6(4) 5_566 5_656
Sb9B Q1 Mn5 120.9(2) . 5_656
Sb9B Q1 Mn5 67.24(11) 5_556 5_656
Sb9B Q1 Mn5 140.9(4) 5_566 5_656
Ca9 Q1 Mn5 61.14(12) 5_656 5_656
Ca9 Q1 Mn5 132.5(4) 5_666 5_656
Ca9 Q1 Mn5 126.5(2) 1_455 5_656
Ca1 Ca1 Q1 80.35(10) 7_565 .
Ca1 Ca1 Mn4 139.64(10) 7_565 5_556
Q1 Ca1 Mn4 134.1(2) . 5_556
Ca1 Ca1 Mn5 138.29(10) 7_565 5_656
Q1 Ca1 Mn5 80.1(2) . 5_656
Mn4 Ca1 Mn5 77.29(12) 5_556 5_656
Ca1 Ca1 Sb9A 137.01(8) 7_565 5_556
Q1 Ca1 Sb9A 68.14(17) . 5_556
Mn4 Ca1 Sb9A 66.14(11) 5_556 5_556
Mn5 Ca1 Sb9A 64.97(10) 5_656 5_556
Ca1 Ca1 Sb9B 128.56(7) 7_565 5_556
Q1 Ca1 Sb9B 63.66(19) . 5_556
Mn4 Ca1 Sb9B 71.51(11) 5_556 5_556
Mn5 Ca1 Sb9B 72.17(11) 5_656 5_556
Sb9A Ca1 Sb9B 8.58(3) 5_556 5_556
Ca1 Ca1 Mn4 31.27(8) 7_565 5_566
Q1 Ca1 Mn4 108.18(15) . 5_566
Mn4 Ca1 Mn4 108.37(16) 5_556 5_566
Mn5 Ca1 Mn4 156.57(17) 5_656 5_566
Sb9A Ca1 Mn4 138.39(15) 5_556 5_566
Sb9B Ca1 Mn4 131.25(14) 5_556 5_566
Ca1 Ca1 Sb7 127.06(6) 7_565 5_656
Q1 Ca1 Sb7 131.3(2) . 5_656
Mn4 Ca1 Sb7 51.70(10) 5_556 5_656
Mn5 Ca1 Sb7 52.20(9) 5_656 5_656
Sb9A Ca1 Sb7 95.91(11) 5_556 5_656
Sb9B Ca1 Sb7 104.37(10) 5_556 5_656
Mn4 Ca1 Sb7 112.73(12) 5_566 5_656
Ca1 Ca1 Mn5 32.49(8) 7_565 5_666
Q1 Ca1 Mn5 67.63(18) . 5_666
Mn4 Ca1 Mn5 157.55(16) 5_556 5_666
Mn5 Ca1 Mn5 105.80(15) 5_656 5_666
Sb9A Ca1 Mn5 135.75(14) 5_556 5_666
Sb9B Ca1 Mn5 130.87(13) 5_556 5_666
Mn4 Ca1 Mn5 60.30(9) 5_566 5_666
Sb7 Ca1 Mn5 112.14(12) 5_656 5_666
Ca1 Ca1 Sb8 83.10(6) 7_565 1_455
Q1 Ca1 Sb8 136.5(3) . 1_455
Mn4 Ca1 Sb8 57.70(9) 5_556 1_455
Mn5 Ca1 Sb8 134.34(14) 5_656 1_455
Sb9A Ca1 Sb8 99.80(12) 5_556 1_455
Sb9B Ca1 Sb8 98.12(11) 5_556 1_455
Mn4 Ca1 Sb8 52.83(8) 5_566 1_455
Sb7 Ca1 Sb8 90.32(9) 5_656 1_455
Mn5 Ca1 Sb8 112.99(11) 5_666 1_455
Ca1 Ca1 Sb9A 33.66(7) 7_565 5_566
Q1 Ca1 Sb9A 57.20(15) . 5_566
Mn4 Ca1 Sb9A 139.33(16) 5_556 5_566
Mn5 Ca1 Sb9A 136.16(15) 5_656 5_566
Sb9A Ca1 Sb9A 103.35(12) 5_556 5_566
Sb9B Ca1 Sb9A 94.92(11) 5_556 5_566
Mn4 Ca1 Sb9A 52.28(8) 5_566 5_566
Sb7 Ca1 Sb9A 160.67(13) 5_656 5_566
Mn5 Ca1 Sb9A 51.58(8) 5_666 5_566
Sb8 Ca1 Sb9A 88.11(9) 1_455 5_566
Ca1 Ca1 Sb1 83.19(6) 7_565 .
Q1 Ca1 Sb1 52.4(3) . .
Mn4 Ca1 Sb1 132.01(14) 5_556 .
Mn5 Ca1 Sb1 55.82(9) 5_656 .
Sb9A Ca1 Sb1 98.75(11) 5_556 .
Sb9B Ca1 Sb1 100.20(11) 5_556 .
Mn4 Ca1 Sb1 111.27(12) 5_566 .
Sb7 Ca1 Sb1 88.01(9) 5_656 .
Mn5 Ca1 Sb1 51.33(7) 5_666 .
Sb8 Ca1 Sb1 161.45(12) 1_455 .
Sb9A Ca1 Sb1 87.40(9) 5_566 .
Mn3 Ca2 Mn3 99.31(14) 5_656 5_666
Mn3 Ca2 Sb7 46.33(8) 5_656 5_656
Mn3 Ca2 Sb7 113.37(10) 5_666 5_656
Mn3 Ca2 Sb7 113.37(10) 5_656 5_666
Mn3 Ca2 Sb7 46.33(8) 5_666 5_666
Sb7 Ca2 Sb7 90.99(6) 5_656 5_666
Mn3 Ca2 Sb4 62.90(8) 5_656 2_554
Mn3 Ca2 Sb4 128.66(11) 5_666 2_554
Sb7 Ca2 Sb4 89.086(19) 5_656 2_554
Sb7 Ca2 Sb4 174.21(9) 5_666 2_554
Mn3 Ca2 Sb4 128.66(11) 5_656 2_564
Mn3 Ca2 Sb4 62.90(8) 5_666 2_564
Sb7 Ca2 Sb4 174.21(9) 5_656 2_564
Sb7 Ca2 Sb4 89.085(19) 5_666 2_564
Sb4 Ca2 Sb4 90.26(6) 2_554 2_564
Mn3 Ca2 Sb2 50.11(7) 5_656 .
Mn3 Ca2 Sb2 50.11(7) 5_666 .
Sb7 Ca2 Sb2 82.29(5) 5_656 .
Sb7 Ca2 Sb2 82.29(5) 5_666 .
Sb4 Ca2 Sb2 91.98(6) 2_554 .
Sb4 Ca2 Sb2 91.98(6) 2_564 .
Mn3 Ca2 Sb8 126.05(8) 5_656 1_455
Mn3 Ca2 Sb8 126.05(8) 5_666 1_455
Sb7 Ca2 Sb8 85.97(5) 5_656 1_455
Sb7 Ca2 Sb8 85.97(5) 5_666 1_455
Sb4 Ca2 Sb8 99.81(6) 2_554 1_455
Sb4 Ca2 Sb8 99.81(6) 2_564 1_455
Sb2 Ca2 Sb8 163.22(8) . 1_455
Mn3 Ca2 Mn1 91.37(10) 5_656 6_556
Mn3 Ca2 Mn1 91.37(10) 5_666 6_556
Sb7 Ca2 Mn1 132.16(4) 5_656 6_556
Sb7 Ca2 Mn1 132.16(4) 5_666 6_556
Sb4 Ca2 Mn1 45.76(3) 2_554 6_556
Sb4 Ca2 Mn1 45.76(3) 2_564 6_556
Sb2 Ca2 Mn1 84.26(6) . 6_556
Sb8 Ca2 Mn1 112.52(7) 1_455 6_556
Mn3 Ca2 Mn4 81.17(8) 5_656 5_556
Mn3 Ca2 Mn4 140.38(12) 5_666 5_556
Sb7 Ca2 Mn4 41.70(5) 5_656 5_556
Sb7 Ca2 Mn4 96.77(7) 5_666 5_556
Sb4 Ca2 Mn4 87.13(5) 2_554 5_556
Sb4 Ca2 Mn4 144.00(9) 2_564 5_556
Sb2 Ca2 Mn4 123.98(7) . 5_556
Sb8 Ca2 Mn4 45.69(5) 1_455 5_556
Mn1 Ca2 Mn4 128.24(7) 6_556 5_556
Mn3 Ca2 Mn4 140.38(12) 5_656 5_566
Mn3 Ca2 Mn4 81.17(8) 5_666 5_566
Sb7 Ca2 Mn4 96.77(7) 5_656 5_566
Sb7 Ca2 Mn4 41.70(5) 5_666 5_566
Sb4 Ca2 Mn4 144.00(9) 2_554 5_566
Sb4 Ca2 Mn4 87.13(5) 2_564 5_566
Sb2 Ca2 Mn4 123.98(7) . 5_566
Sb8 Ca2 Mn4 45.69(5) 1_455 5_566
Mn1 Ca2 Mn4 128.24(7) 6_556 5_566
Mn4 Ca2 Mn4 74.62(7) 5_556 5_566
Mn3 Ca2 Ca5 63.03(9) 5_656 .
Mn3 Ca2 Ca5 63.03(9) 5_666 .
Sb7 Ca2 Ca5 50.78(4) 5_656 .
Sb7 Ca2 Ca5 50.78(4) 5_666 .
Sb4 Ca2 Ca5 125.90(5) 2_554 .
Sb4 Ca2 Ca5 125.90(5) 2_564 .
Sb2 Ca2 Ca5 53.40(5) . .
Sb8 Ca2 Ca5 109.82(7) 1_455 .
Mn1 Ca2 Ca5 137.66(8) 6_556 .
Mn4 Ca2 Ca5 83.05(7) 5_556 .
Mn4 Ca2 Ca5 83.05(7) 5_566 .
Sb8 Ca3 Sb8 93.48(7) 5_656 5_666
Sb8 Ca3 Sb4 106.35(6) 5_656 6_557
Sb8 Ca3 Sb4 106.34(6) 5_666 6_557
Sb8 Ca3 Sb6 83.78(2) 5_656 5_656
Sb8 Ca3 Sb6 158.68(8) 5_666 5_656
Sb4 Ca3 Sb6 94.68(6) 6_557 5_656
Sb8 Ca3 Sb6 158.68(8) 5_656 5_666
Sb8 Ca3 Sb6 83.78(2) 5_666 5_666
Sb4 Ca3 Sb6 94.68(6) 6_557 5_666
Sb6 Ca3 Sb6 91.11(6) 5_656 5_666
Sb8 Ca3 Mn2 51.20(4) 5_656 5_656
Sb8 Ca3 Mn2 111.64(7) 5_666 5_656
Sb4 Ca3 Mn2 136.09(4) 6_557 5_656
Sb6 Ca3 Mn2 51.03(4) 5_656 5_656
Sb6 Ca3 Mn2 110.30(7) 5_666 5_656
Sb8 Ca3 Mn2 111.64(7) 5_656 5_666
Sb8 Ca3 Mn2 51.20(4) 5_666 5_666
Sb4 Ca3 Mn2 136.09(4) 6_557 5_666
Sb6 Ca3 Mn2 110.30(7) 5_656 5_666
Sb6 Ca3 Mn2 51.03(4) 5_666 5_666
Mn2 Ca3 Mn2 86.22(7) 5_656 5_666
Sb8 Ca3 Mn4 50.04(4) 5_656 .
Sb8 Ca3 Mn4 50.04(4) 5_666 .
Sb4 Ca3 Mn4 93.83(8) 6_557 .
Sb6 Ca3 Mn4 133.51(4) 5_656 .
Sb6 Ca3 Mn4 133.51(4) 5_666 .
Mn2 Ca3 Mn4 94.00(7) 5_656 .
Mn2 Ca3 Mn4 94.00(7) 5_666 .
Sb8 Ca3 Ca6 132.99(3) 5_656 .
Sb8 Ca3 Ca6 132.99(3) 5_666 .
Sb4 Ca3 Ca6 60.07(6) 6_557 .
Sb6 Ca3 Ca6 55.80(4) 5_656 .
Sb6 Ca3 Ca6 55.80(4) 5_666 .
Mn2 Ca3 Ca6 104.89(7) 5_656 .
Mn2 Ca3 Ca6 104.89(7) 5_666 .
Mn4 Ca3 Ca6 153.91(10) . .
Sb8 Ca3 Ca7 110.61(6) 5_656 .
Sb8 Ca3 Ca7 110.61(6) 5_666 .
Sb4 Ca3 Ca7 124.84(8) 6_557 .
Sb6 Ca3 Ca7 51.88(4) 5_656 .
Sb6 Ca3 Ca7 51.88(4) 5_666 .
Mn2 Ca3 Ca7 59.43(5) 5_656 .
Mn2 Ca3 Ca7 59.43(5) 5_666 .
Mn4 Ca3 Ca7 141.33(9) . .
Ca6 Ca3 Ca7 64.77(7) . .
Sb8 Ca3 Ca2 54.69(4) 5_656 5_556
Sb8 Ca3 Ca2 104.55(7) 5_666 5_556
Sb4 Ca3 Ca2 51.72(4) 6_557 5_556
Sb6 Ca3 Ca2 91.14(4) 5_656 5_556
Sb6 Ca3 Ca2 146.39(8) 5_666 5_556
Mn2 Ca3 Ca2 96.96(4) 5_656 5_556
Mn2 Ca3 Ca2 154.06(8) 5_666 5_556
Mn4 Ca3 Ca2 60.14(6) . 5_556
Ca6 Ca3 Ca2 99.17(7) . 5_556
Ca7 Ca3 Ca2 142.89(4) . 5_556
Sb8 Ca3 Ca2 104.55(7) 5_656 5_566
Sb8 Ca3 Ca2 54.69(4) 5_666 5_566
Sb4 Ca3 Ca2 51.72(4) 6_557 5_566
Sb6 Ca3 Ca2 146.39(8) 5_656 5_566
Sb6 Ca3 Ca2 91.14(4) 5_666 5_566
Mn2 Ca3 Ca2 154.06(8) 5_656 5_566
Mn2 Ca3 Ca2 96.96(4) 5_666 5_566
Mn4 Ca3 Ca2 60.14(6) . 5_566
Ca6 Ca3 Ca2 99.17(7) . 5_566
Ca7 Ca3 Ca2 142.89(4) . 5_566
Ca2 Ca3 Ca2 69.40(6) 5_556 5_566
Mn4 Ca4 Mn6A 118.75(15) . .
Mn4 Ca4 Sb9B 63.66(9) . .
Mn6A Ca4 Sb9B 55.09(14) . .
Mn4 Ca4 Sb3 120.25(10) . .
Mn6A Ca4 Sb3 121.01(15) . .
Sb9B Ca4 Sb3 176.09(11) . .
Mn4 Ca4 Sb9A 52.64(8) . .
Mn6A Ca4 Sb9A 66.11(13) . .
Sb9B Ca4 Sb9A 11.02(4) . .
Sb3 Ca4 Sb9A 172.88(10) . .
Mn4 Ca4 Sb8 52.48(5) . 5_656
Mn6A Ca4 Sb8 128.48(7) . 5_656
Sb9B Ca4 Sb8 93.81(7) . 5_656
Sb3 Ca4 Sb8 88.98(6) . 5_656
Sb9A Ca4 Sb8 85.93(6) . 5_656
Mn4 Ca4 Sb8 52.48(5) . 5_666
Mn6A Ca4 Sb8 128.48(7) . 5_666
Sb9B Ca4 Sb8 93.81(7) . 5_666
Sb3 Ca4 Sb8 88.98(6) . 5_666
Sb9A Ca4 Sb8 85.93(6) . 5_666
Sb8 Ca4 Sb8 88.63(7) 5_656 5_666
Mn4 Ca4 Sb5 128.18(6) . 5_656
Mn6A Ca4 Sb5 50.42(7) . 5_656
Sb9B Ca4 Sb5 85.80(6) . 5_656
Sb3 Ca4 Sb5 91.35(6) . 5_656
Sb9A Ca4 Sb5 93.84(6) . 5_656
Sb8 Ca4 Sb5 92.540(17) 5_656 5_656
Sb8 Ca4 Sb5 178.79(7) 5_666 5_656
Mn4 Ca4 Sb5 128.18(6) . 5_666
Mn6A Ca4 Sb5 50.42(7) . 5_666
Sb9B Ca4 Sb5 85.80(6) . 5_666
Sb3 Ca4 Sb5 91.35(6) . 5_666
Sb9A Ca4 Sb5 93.84(6) . 5_666
Sb8 Ca4 Sb5 178.79(7) 5_656 5_666
Sb8 Ca4 Sb5 92.539(17) 5_666 5_666
Sb5 Ca4 Sb5 86.29(7) 5_656 5_666
Mn4 Ca4 Ca8 173.19(11) . .
Mn6A Ca4 Ca8 68.07(14) . .
Sb9B Ca4 Ca8 123.15(10) . .
Sb3 Ca4 Ca8 52.94(6) . .
Sb9A Ca4 Ca8 134.18(10) . .
Sb8 Ca4 Ca8 124.07(6) 5_656 .
Sb8 Ca4 Ca8 124.07(6) 5_666 .
Sb5 Ca4 Ca8 55.41(5) 5_656 .
Sb5 Ca4 Ca8 55.41(5) 5_666 .
Mn4 Ca4 Ca3 55.88(8) . .
Mn6A Ca4 Ca3 174.63(15) . .
Sb9B Ca4 Ca3 119.54(9) . .
Sb3 Ca4 Ca3 64.37(6) . .
Sb9A Ca4 Ca3 108.52(8) . .
Sb8 Ca4 Ca3 49.26(4) 5_656 .
Sb8 Ca4 Ca3 49.26(4) 5_666 .
Sb5 Ca4 Ca3 131.89(4) 5_656 .
Sb5 Ca4 Ca3 131.89(4) 5_666 .
Ca8 Ca4 Ca3 117.31(8) . .
Mn4 Ca4 Ca1 35.75(7) . 5_556
Mn6A Ca4 Ca1 93.69(13) . 5_556
Sb9B Ca4 Ca1 46.11(7) . 5_556
Sb3 Ca4 Ca1 136.89(8) . 5_556
Sb9A Ca4 Ca1 38.00(6) . 5_556
Sb8 Ca4 Ca1 47.98(6) 5_656 5_556
Sb8 Ca4 Ca1 87.72(7) 5_666 5_556
Sb5 Ca4 Ca1 92.83(6) 5_656 5_556
Sb5 Ca4 Ca1 131.73(8) 5_666 5_556
Ca8 Ca4 Ca1 148.21(7) . 5_556
Ca3 Ca4 Ca1 81.52(7) . 5_556
Sb7 Ca5 Sb7 92.48(6) 5_656 5_666
Sb7 Ca5 Sb3 89.966(18) 5_656 5_656
Sb7 Ca5 Sb3 177.55(6) 5_666 5_656
Sb7 Ca5 Sb3 177.55(6) 5_656 5_666
Sb7 Ca5 Sb3 89.965(18) 5_666 5_666
Sb3 Ca5 Sb3 87.59(6) 5_656 5_666
Sb7 Ca5 Sb1 86.02(5) 5_656 .
Sb7 Ca5 Sb1 86.02(5) 5_666 .
Sb3 Ca5 Sb1 94.00(5) 5_656 .
Sb3 Ca5 Sb1 94.00(5) 5_666 .
Sb7 Ca5 Sb2 82.66(5) 5_656 .
Sb7 Ca5 Sb2 82.66(5) 5_666 .
Sb3 Ca5 Sb2 97.82(5) 5_656 .
Sb3 Ca5 Sb2 97.82(5) 5_666 .
Sb1 Ca5 Sb2 163.59(8) . .
Sb7 Ca5 Mn2 131.78(4) 5_656 .
Sb7 Ca5 Mn2 131.78(4) 5_666 .
Sb3 Ca5 Mn2 46.00(3) 5_656 .
Sb3 Ca5 Mn2 46.00(3) 5_666 .
Sb1 Ca5 Mn2 111.33(7) . .
Sb2 Ca5 Mn2 85.08(6) . .
Sb7 Ca5 Mn3 40.37(6) 5_656 5_656
Sb7 Ca5 Mn3 96.82(8) 5_666 5_656
Sb3 Ca5 Mn3 85.15(6) 5_656 5_656
Sb3 Ca5 Mn3 139.40(9) 5_666 5_656
Sb1 Ca5 Mn3 126.31(7) . 5_656
Sb2 Ca5 Mn3 44.20(6) . 5_656
Mn2 Ca5 Mn3 105.99(8) . 5_656
Sb7 Ca5 Mn3 96.82(8) 5_656 5_666
Sb7 Ca5 Mn3 40.37(6) 5_666 5_666
Sb3 Ca5 Mn3 139.40(9) 5_656 5_666
Sb3 Ca5 Mn3 85.15(6) 5_666 5_666
Sb1 Ca5 Mn3 126.31(7) . 5_666
Sb2 Ca5 Mn3 44.20(5) . 5_666
Mn2 Ca5 Mn3 105.99(8) . 5_666
Mn3 Ca5 Mn3 75.13(9) 5_656 5_666
Sb7 Ca5 Mn5 42.26(5) 5_656 5_656
Sb7 Ca5 Mn5 97.57(7) 5_666 5_656
Sb3 Ca5 Mn5 84.14(4) 5_656 5_656
Sb3 Ca5 Mn5 137.17(8) 5_666 5_656
Sb1 Ca5 Mn5 45.11(4) . 5_656
Sb2 Ca5 Mn5 124.91(6) . 5_656
Mn2 Ca5 Mn5 127.03(6) . 5_656
Mn3 Ca5 Mn5 81.63(7) 5_656 5_656
Mn3 Ca5 Mn5 126.19(10) 5_666 5_656
Sb7 Ca5 Mn5 97.57(7) 5_656 5_666
Sb7 Ca5 Mn5 42.25(5) 5_666 5_666
Sb3 Ca5 Mn5 137.17(8) 5_656 5_666
Sb3 Ca5 Mn5 84.14(4) 5_666 5_666
Sb1 Ca5 Mn5 45.11(4) . 5_666
Sb2 Ca5 Mn5 124.91(6) . 5_666
Mn2 Ca5 Mn5 127.03(6) . 5_666
Mn3 Ca5 Mn5 126.19(10) 5_656 5_666
Mn3 Ca5 Mn5 81.63(7) 5_666 5_666
Mn5 Ca5 Mn5 74.26(7) 5_656 5_666
Sb7 Ca5 Ca2 51.68(4) 5_656 .
Sb7 Ca5 Ca2 51.68(4) 5_666 .
Sb3 Ca5 Ca2 130.42(4) 5_656 .
Sb3 Ca5 Ca2 130.42(4) 5_666 .
Sb1 Ca5 Ca2 110.54(7) . .
Sb2 Ca5 Ca2 53.05(5) . .
Mn2 Ca5 Ca2 138.13(7) . .
Mn3 Ca5 Ca2 45.48(6) 5_656 .
Mn3 Ca5 Ca2 45.48(6) 5_666 .
Mn5 Ca5 Ca2 84.28(7) 5_656 .
Mn5 Ca5 Ca2 84.28(7) 5_666 .
Mn3 Ca6 Sb2 52.90(6) 6_557 2
Mn3 Ca6 Sb2 52.90(6) 6_557 2_565
Sb2 Ca6 Sb2 91.11(7) 2 2_565
Mn3 Ca6 Sb6 128.45(7) 6_557 5_656
Sb2 Ca6 Sb6 89.147(17) 2 5_656
Sb2 Ca6 Sb6 178.15(11) 2_565 5_656
Mn3 Ca6 Sb6 128.45(7) 6_557 5_666
Sb2 Ca6 Sb6 178.15(11) 2 5_666
Sb2 Ca6 Sb6 89.146(17) 2_565 5_666
Sb6 Ca6 Sb6 90.54(7) 5_656 5_666
Mn3 Ca6 Sb4 64.39(11) 6_557 .
Sb2 Ca6 Sb4 93.43(7) 2 .
Sb2 Ca6 Sb4 93.43(7) 2_565 .
Sb6 Ca6 Sb4 88.37(6) 5_656 .
Sb6 Ca6 Sb4 88.37(6) 5_666 .
Mn3 Ca6 Sb4 118.37(12) 6_557 6_557
Sb2 Ca6 Sb4 88.49(6) 2 6_557
Sb2 Ca6 Sb4 88.49(6) 2_565 6_557
Sb6 Ca6 Sb4 89.69(7) 5_656 6_557
Sb6 Ca6 Sb4 89.69(7) 5_666 6_557
Sb4 Ca6 Sb4 177.25(9) . 6_557
Mn3 Ca6 Ca3 171.73(14) 6_557 .
Sb2 Ca6 Ca3 123.08(7) 2 .
Sb2 Ca6 Ca3 123.08(7) 2_565 .
Sb6 Ca6 Ca3 55.39(5) 5_656 .
Sb6 Ca6 Ca3 55.39(5) 5_666 .
Sb4 Ca6 Ca3 123.88(8) . .
Sb4 Ca6 Ca3 53.37(6) 6_557 .
Mn3 Ca6 Ca7 55.87(10) 6_557 6_557
Sb2 Ca6 Ca7 50.74(4) 2 6_557
Sb2 Ca6 Ca7 50.74(4) 2_565 6_557
Sb6 Ca6 Ca7 128.44(5) 5_656 6_557
Sb6 Ca6 Ca7 128.44(5) 5_666 6_557
Sb4 Ca6 Ca7 120.25(9) . 6_557
Sb4 Ca6 Ca7 62.50(5) 6_557 6_557
Ca3 Ca6 Ca7 115.87(9) . 6_557
Mn3 Ca6 Ca7 126.97(13) 6_557 .
Sb2 Ca6 Ca7 130.31(5) 2 .
Sb2 Ca6 Ca7 130.31(5) 2_565 .
Sb6 Ca6 Ca7 50.41(4) 5_656 .
Sb6 Ca6 Ca7 50.41(4) 5_666 .
Sb4 Ca6 Ca7 62.59(5) . .
Sb4 Ca6 Ca7 114.66(9) 6_557 .
Ca3 Ca6 Ca7 61.29(6) . .
Ca7 Ca6 Ca7 177.16(10) 6_557 .
Sb3 Ca7 Sb2 105.41(5) . 5_656
Sb3 Ca7 Sb2 105.41(5) . 5_666
Sb2 Ca7 Sb2 93.01(6) 5_656 5_666
Sb3 Ca7 Sb6 93.46(5) . 5_656
Sb2 Ca7 Sb6 84.58(2) 5_656 5_656
Sb2 Ca7 Sb6 160.90(8) 5_666 5_656
Sb3 Ca7 Sb6 93.46(5) . 5_666
Sb2 Ca7 Sb6 160.90(8) 5_656 5_666
Sb2 Ca7 Sb6 84.58(2) 5_666 5_666
Sb6 Ca7 Sb6 91.52(6) 5_656 5_666
Sb3 Ca7 Mn1 135.50(4) . 5_656
Sb2 Ca7 Mn1 51.67(4) 5_656 5_656
Sb2 Ca7 Mn1 112.55(7) 5_666 5_656
Sb6 Ca7 Mn1 51.92(4) 5_656 5_656
Sb6 Ca7 Mn1 112.00(7) 5_666 5_656
Sb3 Ca7 Mn1 135.50(4) . 5_666
Sb2 Ca7 Mn1 112.55(7) 5_656 5_666
Sb2 Ca7 Mn1 51.67(4) 5_666 5_666
Sb6 Ca7 Mn1 112.00(7) 5_656 5_666
Sb6 Ca7 Mn1 51.92(4) 5_666 5_666
Mn1 Ca7 Mn1 87.55(7) 5_656 5_666
Sb3 Ca7 Mn3 95.16(9) . .
Sb2 Ca7 Mn3 48.98(4) 5_656 .
Sb2 Ca7 Mn3 48.98(4) 5_666 .
Sb6 Ca7 Mn3 133.38(3) 5_656 .
Sb6 Ca7 Mn3 133.38(3) 5_666 .
Mn1 Ca7 Mn3 92.73(7) 5_656 .
Mn1 Ca7 Mn3 92.73(8) 5_666 .
Sb3 Ca7 Mn2 46.80(3) . 5_656
Sb2 Ca7 Mn2 87.87(3) 5_656 5_656
Sb2 Ca7 Mn2 150.78(8) 5_666 5_656
Sb6 Ca7 Mn2 48.23(3) 5_656 5_656
Sb6 Ca7 Mn2 103.44(6) 5_666 5_656
Mn1 Ca7 Mn2 90.73(4) 5_656 5_656
Mn1 Ca7 Mn2 151.70(8) 5_666 5_656
Mn3 Ca7 Mn2 115.57(8) . 5_656
Sb3 Ca7 Mn2 46.80(3) . 5_666
Sb2 Ca7 Mn2 150.78(8) 5_656 5_666
Sb2 Ca7 Mn2 87.87(3) 5_666 5_666
Sb6 Ca7 Mn2 103.44(6) 5_656 5_666
Sb6 Ca7 Mn2 48.23(3) 5_666 5_666
Mn1 Ca7 Mn2 151.70(8) 5_656 5_666
Mn1 Ca7 Mn2 90.73(4) 5_666 5_666
Mn3 Ca7 Mn2 115.57(8) . 5_666
Mn2 Ca7 Mn2 77.68(5) 5_656 5_666
Sb3 Ca7 Ca3 66.59(5) . .
Sb2 Ca7 Ca3 133.49(3) 5_656 .
Sb2 Ca7 Ca3 133.49(3) 5_666 .
Sb6 Ca7 Ca3 52.13(4) 5_656 .
Sb6 Ca7 Ca3 52.13(4) 5_666 .
Mn1 Ca7 Ca3 100.39(6) 5_656 .
Mn1 Ca7 Ca3 100.39(6) 5_666 .
Mn3 Ca7 Ca3 161.75(10) . .
Mn2 Ca7 Ca3 52.20(4) 5_656 .
Mn2 Ca7 Ca3 52.20(4) 5_666 .
Sb3 Ca7 Ca6 138.97(8) . 6_657
Sb2 Ca7 Ca6 51.88(4) 5_656 6_657
Sb2 Ca7 Ca6 51.88(4) 5_666 6_657
Sb6 Ca7 Ca6 114.25(5) 5_656 6_657
Sb6 Ca7 Ca6 114.25(5) 5_666 6_657
Mn1 Ca7 Ca6 62.33(5) 5_656 6_657
Mn1 Ca7 Ca6 62.33(5) 5_666 6_657
Mn3 Ca7 Ca6 43.81(9) . 6_657
Mn2 Ca7 Ca6 139.49(4) 5_656 6_657
Mn2 Ca7 Ca6 139.49(4) 5_666 6_657
Ca3 Ca7 Ca6 154.43(8) . 6_657
Sb3 Ca8 Sb1 101.50(7) . 5_656
Sb3 Ca8 Sb1 101.50(7) . 5_666
Sb1 Ca8 Sb1 93.82(8) 5_656 5_666
Sb3 Ca8 Mn6B 132.84(5) . 5_656
Sb1 Ca8 Mn6B 52.61(5) 5_656 5_656
Sb1 Ca8 Mn6B 117.09(9) 5_666 5_656
Sb3 Ca8 Mn6B 132.84(5) . 5_666
Sb1 Ca8 Mn6B 117.09(9) 5_656 5_666
Sb1 Ca8 Mn6B 52.61(5) 5_666 5_666
Mn6B Ca8 Mn6B 93.36(10) 5_656 5_666
Sb3 Ca8 Mn6B 121.40(10) . .
Sb1 Ca8 Mn6B 116.99(7) 5_656 .
Sb1 Ca8 Mn6B 116.99(7) 5_666 .
Mn6B Ca8 Mn6B 64.39(8) 5_656 .
Mn6B Ca8 Mn6B 64.39(8) 5_666 .
Sb3 Ca8 Sb5 93.65(6) . 5_656
Sb1 Ca8 Sb5 87.26(2) 5_656 5_656
Sb1 Ca8 Sb5 164.25(10) 5_666 5_656
Mn6B Ca8 Sb5 52.25(5) 5_656 5_656
Mn6B Ca8 Sb5 113.22(10) 5_666 5_656
Mn6B Ca8 Sb5 49.67(4) . 5_656
Sb3 Ca8 Sb5 93.65(6) . 5_666
Sb1 Ca8 Sb5 164.25(10) 5_656 5_666
Sb1 Ca8 Sb5 87.26(2) 5_666 5_666
Mn6B Ca8 Sb5 113.22(10) 5_656 5_666
Mn6B Ca8 Sb5 52.25(5) 5_666 5_666
Mn6B Ca8 Sb5 49.67(4) . 5_666
Sb5 Ca8 Sb5 87.53(7) 5_656 5_666
Sb3 Ca8 Mn5 91.65(9) . .
Sb1 Ca8 Mn5 48.79(4) 5_656 .
Sb1 Ca8 Mn5 48.79(4) 5_666 .
Mn6B Ca8 Mn5 94.11(8) 5_656 .
Mn6B Ca8 Mn5 94.11(8) 5_666 .
Mn6B Ca8 Mn5 146.95(11) . .
Sb5 Ca8 Mn5 135.83(4) 5_656 .
Sb5 Ca8 Mn5 135.83(4) 5_666 .
Sb3 Ca8 Sb5 169.95(9) . .
Sb1 Ca8 Sb5 85.27(6) 5_656 .
Sb1 Ca8 Sb5 85.27(6) 5_666 .
Mn6B Ca8 Sb5 46.73(5) 5_656 .
Mn6B Ca8 Sb5 46.73(5) 5_666 .
Mn6B Ca8 Sb5 48.55(6) . .
Sb5 Ca8 Sb5 79.15(6) 5_656 .
Sb5 Ca8 Sb5 79.15(6) 5_666 .
Mn5 Ca8 Sb5 98.40(8) . .
Sb3 Ca8 Ca4 55.13(6) . .
Sb1 Ca8 Ca4 130.55(5) 5_656 .
Sb1 Ca8 Ca4 130.55(5) 5_666 .
Mn6B Ca8 Ca4 108.29(8) 5_656 .
Mn6B Ca8 Ca4 108.29(8) 5_666 .
Mn6B Ca8 Ca4 66.28(8) . .
Sb5 Ca8 Ca4 56.37(5) 5_656 .
Sb5 Ca8 Ca4 56.37(5) 5_666 .
Mn5 Ca8 Ca4 146.77(11) . .
Sb5 Ca8 Ca4 114.83(9) . .
Sb3 Ca8 Mn6A 140.70(7) . 5_656
Sb1 Ca8 Mn6A 43.84(9) 5_656 5_656
Sb1 Ca8 Mn6A 99.18(10) 5_666 5_656
Mn6B Ca8 Mn6A 18.70(10) 5_656 5_656
Mn6B Ca8 Mn6A 86.00(9) 5_666 5_656
Mn6B Ca8 Mn6A 76.24(11) . 5_656
Sb5 Ca8 Mn6A 70.91(9) 5_656 5_656
Sb5 Ca8 Mn6A 120.48(12) 5_666 5_656
Mn5 Ca8 Mn6A 77.54(11) . 5_656
Sb5 Ca8 Mn6A 43.27(8) . 5_656
Ca4 Ca8 Mn6A 126.97(11) . 5_656
Sb9B Ca9 Sb9B 104.79(13) 5_656 5_666
Sb9B Ca9 Q1 59.46(19) 5_656 5_656
Sb9B Ca9 Q1 137.9(2) 5_666 5_656
Sb9B Ca9 Q1 137.9(2) 5_656 5_666
Sb9B Ca9 Q1 59.46(19) 5_666 5_666
Q1 Ca9 Q1 104.1(4) 5_656 5_666
Sb9B Ca9 Q1 59.39(11) 5_656 1_655
Sb9B Ca9 Q1 59.39(11) 5_666 1_655
Q1 Ca9 Q1 80.6(3) 5_656 1_655
Q1 Ca9 Q1 80.6(3) 5_666 1_655
Sb9B Ca9 Mn6A 59.33(12) 5_656 5_656
Sb9B Ca9 Mn6A 135.77(18) 5_666 5_656
Q1 Ca9 Mn6A 73.4(2) 5_656 5_656
Q1 Ca9 Mn6A 159.2(3) 5_666 5_656
Q1 Ca9 Mn6A 118.51(16) 1_655 5_656
Sb9B Ca9 Mn6A 135.77(18) 5_656 5_666
Sb9B Ca9 Mn6A 59.33(12) 5_666 5_666
Q1 Ca9 Mn6A 159.2(3) 5_656 5_666
Q1 Ca9 Mn6A 73.4(2) 5_666 5_666
Q1 Ca9 Mn6A 118.51(16) 1_655 5_666
Mn6A Ca9 Mn6A 101.5(2) 5_656 5_666
Sb9B Ca9 Mn5 122.00(9) 5_656 .
Sb9B Ca9 Mn5 122.00(9) 5_666 .
Q1 Ca9 Mn5 62.9(2) 5_656 .
Q1 Ca9 Mn5 62.9(2) 5_666 .
Q1 Ca9 Mn5 116.8(2) 1_655 .
Mn6A Ca9 Mn5 98.95(14) 5_656 .
Mn6A Ca9 Mn5 98.95(14) 5_666 .
Sb9B Ca9 Sb9A 95.05(10) 5_656 1_655
Sb9B Ca9 Sb9A 95.05(10) 5_666 1_655
Q1 Ca9 Sb9A 52.71(18) 5_656 1_655
Q1 Ca9 Sb9A 52.71(18) 5_666 1_655
Q1 Ca9 Sb9A 64.8(2) 1_655 1_655
Mn6A Ca9 Sb9A 125.39(12) 5_656 1_655
Mn6A Ca9 Sb9A 125.39(12) 5_666 1_655
Mn5 Ca9 Sb9A 51.98(9) . 1_655
Sb9B Ca9 Sb5 91.67(10) 5_656 .
Sb9B Ca9 Sb5 91.67(9) 5_666 .
Q1 Ca9 Sb5 125.07(19) 5_656 .
Q1 Ca9 Sb5 125.07(19) 5_666 .
Q1 Ca9 Sb5 126.2(2) 1_655 .
Mn6A Ca9 Sb5 51.88(11) 5_656 .
Mn6A Ca9 Sb5 51.88(11) 5_666 .
Mn5 Ca9 Sb5 116.99(12) . .
Sb9A Ca9 Sb5 168.97(12) 1_655 .
Sb9B Ca9 Sb9A 8.62(4) 5_656 5_656
Sb9B Ca9 Sb9A 96.35(11) 5_666 5_656
Q1 Ca9 Sb9A 64.7(2) 5_656 5_656
Q1 Ca9 Sb9A 131.8(2) 5_666 5_656
Q1 Ca9 Sb9A 51.86(11) 1_655 5_656
Mn6A Ca9 Sb9A 66.65(12) 5_656 5_656
Mn6A Ca9 Sb9A 132.69(16) 5_666 5_656
Mn5 Ca9 Sb9A 127.53(8) . 5_656
Sb9A Ca9 Sb9A 94.17(8) 1_655 5_656
Sb5 Ca9 Sb9A 93.77(8) . 5_656
Sb9B Ca9 Sb9A 96.35(11) 5_656 5_666
Sb9B Ca9 Sb9A 8.62(4) 5_666 5_666
Q1 Ca9 Sb9A 131.8(2) 5_656 5_666
Q1 Ca9 Sb9A 64.7(2) 5_666 5_666
Q1 Ca9 Sb9A 51.86(11) 1_655 5_666
Mn6A Ca9 Sb9A 132.69(16) 5_656 5_666
Mn6A Ca9 Sb9A 66.65(12) 5_666 5_666
Mn5 Ca9 Sb9A 127.53(8) . 5_666
Sb9A Ca9 Sb9A 94.17(8) 1_655 5_666
Sb5 Ca9 Sb9A 93.77(8) . 5_666
Sb9A Ca9 Sb9A 87.87(9) 5_656 5_666
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 Q1 2.592(11) .
Sb1 Mn6A 2.681(6) .
Sb1 Mn5 2.7883(18) 5_656
Sb1 Mn5 2.7883(18) 5_666
Sb1 Mn6B 2.807(3) .
Sb1 Ca8 3.1611(19) 5_656
Sb1 Ca8 3.161(2) 5_666
Sb1 Ca1 3.245(4) 7_565
Sb1 Ca1 3.245(4) .
Sb1 Ca5 3.358(2) .
Sb1 Ca9 3.396(2) 5_656
Sb1 Ca9 3.396(2) 5_666
Sb2 Mn3 2.721(2) 5_656
Sb2 Mn3 2.721(2) 5_666
Sb2 Mn1 2.8443(18) .
Sb2 Ca7 3.1823(16) 5_656
Sb2 Ca7 3.1823(16) 5_666
Sb2 Ca6 3.2332(19) 2_554
Sb2 Ca6 3.2332(19) 2_564
Sb2 Ca2 3.357(3) .
Sb2 Ca5 3.372(2) .
Sb3 Mn2 2.7613(11) 5_656
Sb3 Mn2 2.7613(11) 5_666
Sb3 Ca8 3.160(3) .
Sb3 Ca7 3.173(2) .
Sb3 Ca4 3.249(3) .
Sb3 Ca5 3.3357(17) 5_656
Sb3 Ca5 3.3357(18) 5_666
Sb4 Mn1 2.7517(10) 5_656
Sb4 Mn1 2.7517(10) 5_666
Sb4 Ca3 3.204(2) 6_657
Sb4 Ca2 3.2576(18) 2
Sb4 Ca2 3.2576(18) 2_565
Sb4 Ca6 3.302(3) .
Sb4 Ca6 3.460(3) 6_657
Sb5 Mn6B 2.7585(15) 5_656
Sb5 Mn6B 2.7586(15) 5_666
Sb5 Mn6A 2.772(4) 5_656
Sb5 Mn6A 2.772(4) 5_666
Sb5 Mn6B 2.870(3) .
Sb5 Ca9 3.318(4) .
Sb5 Ca8 3.337(2) 5_656
Sb5 Ca8 3.337(2) 5_666
Sb5 Ca4 3.376(2) 5_656
Sb5 Ca4 3.376(2) 5_666
Sb5 Ca8 3.682(3) .
Sb6 Mn2 2.8508(18) .
Sb6 Mn1 2.8732(18) .
Sb6 Ca7 3.2220(17) 5_656
Sb6 Ca7 3.2220(17) 5_666
Sb6 Ca3 3.2333(18) 5_656
Sb6 Ca3 3.2333(18) 5_666
Sb6 Ca6 3.250(2) 5_656
Sb6 Ca6 3.250(2) 5_666
Sb7 Mn3 2.472(4) .
Sb7 Mn4 2.564(3) 1_655
Sb7 Mn5 2.598(3) .
Sb7 Ca1 3.192(4) 5_656
Sb7 Ca1 3.192(4) 3_656
Sb7 Ca5 3.1961(17) 5_656
Sb7 Ca5 3.1961(17) 5_666
Sb7 Ca2 3.2368(17) 5_656
Sb7 Ca2 3.2368(18) 5_666
Sb7 Ca1 3.707(4) 3_646
Sb7 Ca1 3.707(4) 5_666
Sb8 Mn4 2.8269(19) 5_656
Sb8 Mn4 2.8269(19) 5_666
Sb8 Mn2 2.8356(19) .
Sb8 Ca3 3.1698(17) 5_656
Sb8 Ca3 3.1698(17) 5_666
Sb8 Ca1 3.203(4) 1_655
Sb8 Ca1 3.203(4) 7_665
Sb8 Ca4 3.304(2) 5_656
Sb8 Ca4 3.304(2) 5_666
Sb8 Ca2 3.411(3) 1_655
Sb9A Sb9B 0.624(2) .
Sb9A Ca1 2.630(4) 5_556
Sb9A Ca1 2.630(4) 3_556
Sb9A Q1 2.773(6) 5_556
Sb9A Q1 2.773(6) 5_566
Sb9A Mn5 2.797(3) 1_455
Sb9A Mn4 2.814(4) .
Sb9A Ca1 3.236(4) 3_546
Sb9A Ca1 3.236(4) 5_566
Sb9A Ca4 3.264(3) .
Sb9A Ca9 3.279(4) 1_455
Sb9A Ca9 3.327(3) 5_656
Sb9B Q1 2.896(11) .
Sb9B Ca9 2.914(3) 5_656
Sb9B Ca9 2.914(3) 5_666
Sb9B Q1 2.917(7) 5_556
Sb9B Q1 2.917(7) 5_566
Sb9B Mn6A 2.919(7) .
Sb9B Ca1 3.086(4) 5_556
Sb9B Ca1 3.086(4) 3_556
Sb9B Ca4 3.201(3) .
Sb9B Ca9 3.352(4) 1_455
Sb9B Ca1 3.616(4) 3_546
Mn1 Sb4 2.7518(10) 5_656
Mn1 Sb4 2.7518(10) 5_666
Mn1 Ca7 3.337(2) 5_656
Mn1 Ca7 3.337(2) 5_666
Mn1 Ca2 3.731(3) 6_656
Mn2 Sb3 2.7614(11) 5_656
Mn2 Sb3 2.7614(11) 5_666
Mn2 Ca3 3.378(2) 5_656
Mn2 Ca3 3.378(2) 5_666
Mn2 Ca7 3.681(2) 5_656
Mn2 Ca7 3.681(2) 5_666
Mn2 Ca5 3.683(3) .
Mn3 Sb2 2.721(2) 5_656
Mn3 Sb2 2.721(2) 5_666
Mn3 Ca6 2.816(5) 6_657
Mn3 Ca2 3.029(3) 5_656
Mn3 Ca2 3.029(3) 5_666
Mn3 Ca7 3.367(5) .
Mn3 Ca5 3.786(4) 5_656
Mn3 Ca5 3.786(4) 5_666
Mn4 Ca1 2.525(4) 5_556
Mn4 Ca1 2.525(4) 3_556
Mn4 Sb7 2.564(3) 1_455
Mn4 Sb8 2.8268(19) 5_656
Mn4 Sb8 2.8269(19) 5_666
Mn4 Ca4 3.071(4) .
Mn4 Ca1 3.151(4) 3_546
Mn4 Ca1 3.151(4) 5_566
Mn4 Mn5 3.186(4) 1_455
Mn4 Ca3 3.481(4) .
Mn4 Ca2 3.808(3) 5_556
Mn5 Ca1 2.577(4) 5_656
Mn5 Ca1 2.577(4) 3_656
Mn5 Sb1 2.7882(18) 5_656
Mn5 Sb1 2.7882(18) 5_666
Mn5 Sb9A 2.797(3) 1_655
Mn5 Ca9 3.093(4) .
Mn5 Q1 3.143(8) 5_656
Mn5 Q1 3.143(8) 5_666
Mn5 Mn4 3.186(4) 1_655
Mn5 Ca1 3.193(4) 3_646
Mn5 Ca1 3.193(4) 5_666
Mn6A Mn6B 1.308(7) .
Mn6A Sb5 2.772(4) 5_656
Mn6A Sb5 2.772(4) 5_666
Mn6A Ca9 2.982(5) 5_656
Mn6A Ca9 2.982(5) 5_666
Mn6A Ca4 3.108(7) .
Mn6A Ca8 3.828(5) 5_656
Mn6A Ca8 3.828(5) 5_666
Mn6B Sb5 2.7585(15) 5_656
Mn6B Sb5 2.7585(15) 5_666
Mn6B Ca8 3.173(3) 5_656
Mn6B Ca8 3.173(3) 5_666
Mn6B Ca8 3.226(4) .
Mn6B Ca9 3.827(4) 5_656
Mn6B Ca9 3.827(4) 5_666
Q1 Ca1 2.295(11) 7_565
Q1 Ca1 2.295(11) .
Q1 Sb9A 2.773(6) 5_556
Q1 Sb9A 2.773(6) 5_566
Q1 Sb9B 2.917(7) 5_556
Q1 Sb9B 2.917(7) 5_566
Q1 Ca9 2.927(7) 5_656
Q1 Ca9 2.927(7) 5_666
Q1 Ca9 2.973(11) 1_455
Q1 Mn5 3.144(8) 5_656
Ca1 Ca1 0.769(7) 7_565
Ca1 Mn4 2.525(4) 5_556
Ca1 Mn5 2.577(4) 5_656
Ca1 Sb9A 2.630(4) 5_556
Ca1 Sb9B 3.086(4) 5_556
Ca1 Mn4 3.151(4) 5_566
Ca1 Sb7 3.192(4) 5_656
Ca1 Mn5 3.193(4) 5_666
Ca1 Sb8 3.203(4) 1_455
Ca1 Sb9A 3.236(4) 5_566
Ca2 Mn3 3.029(3) 5_656
Ca2 Mn3 3.029(3) 5_666
Ca2 Sb7 3.2369(17) 5_656
Ca2 Sb7 3.2369(17) 5_666
Ca2 Sb4 3.2573(18) 2_554
Ca2 Sb4 3.2573(18) 2_564
Ca2 Sb8 3.411(3) 1_455
Ca2 Mn1 3.731(3) 6_556
Ca2 Mn4 3.809(3) 5_556
Ca2 Mn4 3.809(3) 5_566
Ca2 Ca5 4.029(3) .
Ca3 Sb8 3.1697(17) 5_656
Ca3 Sb8 3.1697(17) 5_666
Ca3 Sb4 3.204(2) 6_557
Ca3 Sb6 3.2334(18) 5_656
Ca3 Sb6 3.2334(18) 5_666
Ca3 Mn2 3.378(2) 5_656
Ca3 Mn2 3.378(2) 5_666
Ca3 Ca6 3.663(4) .
Ca3 Ca7 3.974(3) .
Ca3 Ca2 4.055(3) 5_556
Ca3 Ca2 4.055(3) 5_566
Ca4 Sb8 3.304(2) 5_656
Ca4 Sb8 3.304(2) 5_666
Ca4 Sb5 3.376(2) 5_656
Ca4 Sb5 3.376(2) 5_666
Ca4 Ca8 3.765(4) .
Ca4 Ca1 4.269(4) 5_556
Ca5 Sb7 3.1961(17) 5_656
Ca5 Sb7 3.1962(17) 5_666
Ca5 Sb3 3.3357(17) 5_656
Ca5 Sb3 3.3357(17) 5_666
Ca5 Mn3 3.786(4) 5_656
Ca5 Mn3 3.787(4) 5_666
Ca5 Mn5 3.824(3) 5_656
Ca5 Mn5 3.825(3) 5_666
Ca6 Mn3 2.817(5) 6_557
Ca6 Sb2 3.2335(19) 2
Ca6 Sb2 3.2335(19) 2_565
Ca6 Sb6 3.249(2) 5_656
Ca6 Sb6 3.249(2) 5_666
Ca6 Sb4 3.460(3) 6_557
Ca6 Ca7 4.011(3) 6_557
Ca6 Ca7 4.099(3) .
Ca7 Sb2 3.1822(16) 5_656
Ca7 Sb2 3.1822(16) 5_666
Ca7 Sb6 3.2221(17) 5_656
Ca7 Sb6 3.2221(17) 5_666
Ca7 Mn1 3.337(2) 5_656
Ca7 Mn1 3.337(2) 5_666
Ca7 Mn2 3.681(2) 5_656
Ca7 Mn2 3.681(2) 5_666
Ca7 Ca6 4.010(3) 6_657
Ca8 Sb1 3.1611(19) 5_656
Ca8 Sb1 3.1611(19) 5_666
Ca8 Mn6B 3.173(3) 5_656
Ca8 Mn6B 3.173(3) 5_666
Ca8 Sb5 3.337(2) 5_656
Ca8 Sb5 3.337(2) 5_666
Ca8 Mn6A 3.828(5) 5_656
Ca9 Sb9B 2.914(3) 5_656
Ca9 Sb9B 2.914(3) 5_666
Ca9 Q1 2.927(7) 5_656
Ca9 Q1 2.927(7) 5_666
Ca9 Q1 2.973(11) 1_655
Ca9 Mn6A 2.982(5) 5_656
Ca9 Mn6A 2.982(5) 5_666
Ca9 Sb9A 3.279(4) 1_655
Ca9 Sb9A 3.327(3) 5_656
Ca9 Sb9A 3.327(3) 5_666
