#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:59:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179520 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341708.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341708
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Ca9 Mn4.43 Sb9'
_chemical_formula_weight         1699.58
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.453(2)
_cell_length_b                   4.6206(8)
_cell_length_c                   44.078(8)
_cell_measurement_reflns_used    822
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.89
_cell_measurement_theta_min      2.83
_cell_volume                     2536.3(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0549
_diffrn_reflns_av_sigmaI/netI    0.0376
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       55
_diffrn_reflns_limit_l_min       -55
_diffrn_reflns_number            18916
_diffrn_reflns_theta_full        26.73
_diffrn_reflns_theta_max         26.73
_diffrn_reflns_theta_min         1.70
_exptl_absorpt_coefficient_mu    13.335
_exptl_absorpt_correction_T_max  0.8782
_exptl_absorpt_correction_T_min  0.6673
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.451
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             2999
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_refine_diff_density_max         6.244
_refine_diff_density_min         -2.211
_refine_diff_density_rms         0.324
_refine_ls_extinction_coef       0.000047(13)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.295
_refine_ls_matrix_type           full
_refine_ls_number_parameters     153
_refine_ls_number_reflns         3031
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.295
_refine_ls_R_factor_all          0.0518
_refine_ls_R_factor_gt           0.0434
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0192P)²+30.2633P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0849
_refine_ls_wR_factor_ref         0.0878
_reflns_number_gt                2671
_reflns_number_total             3031
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_003.cif
_cod_data_source_block           III
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_cell_volume        2536.2(8)
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341708
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sb1 Sb 0.25091(7) 0.2500 0.449519(19) 0.01074(19) Uani 1 2 d S
Sb2 Sb 0.27508(7) 0.2500 0.298412(18) 0.00748(18) Uani 1 2 d S
Sb3 Sb 0.50602(7) 0.2500 0.620314(19) 0.00909(19) Uani 1 2 d S
Sb4 Sb 0.55179(8) 0.2500 0.77978(2) 0.0160(2) Uani 1 2 d S
Sb5 Sb 0.60584(7) 0.2500 0.468287(19) 0.01009(19) Uani 1 2 d S
Sb6 Sb 0.62098(7) 0.2500 0.295167(18) 0.00724(18) Uani 1 2 d S
Sb7 Sb 0.87528(8) 0.2500 0.62972(2) 0.0138(2) Uani 1 2 d S
Sb8 Sb 0.81246(7) 0.2500 0.375580(19) 0.01072(19) Uani 1 2 d S
Sb9A Sb 0.05557(16) 0.2500 0.54580(4) 0.0123(3) Uani 0.585(2) 2 d SP
Sb9B Sb 0.0884(2) 0.2500 0.53465(7) 0.0123(3) Uani 0.415(2) 2 d SP
Mn1 Mn 0.44151(16) 0.2500 0.25417(4) 0.0094(4) Uani 1 2 d S
Mn2 Mn 0.59224(16) 0.2500 0.35944(4) 0.0091(4) Uani 1 2 d S
Mn3 Mn 0.8216(4) 0.2500 0.68376(10) 0.0093(15) Uani 0.417(8) 2 d SP
Mn4 Mn 0.0685(3) 0.2500 0.60952(8) 0.0068(5) Uani 0.481(3) 2 d SP
Mn5 Mn 0.8499(3) 0.2500 0.57111(8) 0.0068(5) Uani 0.519(3) 2 d SP
Mn6A Mn 0.3025(5) 0.2500 0.50854(14) 0.0136(6) Uani 0.319(4) 2 d SP
Mn6B Mn 0.3992(2) 0.2500 0.49749(7) 0.0136(6) Uani 0.681(4) 2 d SP
Ca1 Ca 0.0151(3) 0.1648(8) 0.41924(9) 0.0208(10) Uani 0.50 1 d P
Ca2 Ca 0.0249(2) 0.2500 0.32714(6) 0.0182(6) Uani 1 2 d S
Ca3 Ca 0.2416(2) 0.2500 0.67118(6) 0.0137(6) Uani 1 2 d S
Ca4 Ca 0.2896(2) 0.2500 0.57931(7) 0.0187(6) Uani 1 2 d S
Ca5 Ca 0.3018(2) 0.2500 0.37482(6) 0.0117(5) Uani 1 2 d S
Ca6 Ca 0.3054(3) 0.2500 0.75226(8) 0.0229(7) Uani 1 2 d S
Ca7 Ca 0.5528(2) 0.2500 0.69103(6) 0.0097(5) Uani 1 2 d S
Ca8 Ca 0.5745(2) 0.2500 0.55110(7) 0.0251(7) Uani 1 2 d S
Ca9 Ca 0.8476(3) 0.2500 0.50121(8) 0.0489(12) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Mn6A Sb1 Mn5 115.18(9) . 5_666
Mn6A Sb1 Mn5 115.18(9) . 5_656
Mn5 Sb1 Mn5 112.27(13) 5_666 5_656
Mn6A Sb1 Mn6B 27.26(16) . .
Mn5 Sb1 Mn6B 122.89(6) 5_666 .
Mn5 Sb1 Mn6B 122.89(6) 5_656 .
Mn6A Sb1 Ca8 81.04(12) . 5_666
Mn5 Sb1 Ca8 72.64(8) 5_666 5_666
Mn5 Sb1 Ca8 155.67(9) 5_656 5_666
Mn6B Sb1 Ca8 63.63(7) . 5_666
Mn6A Sb1 Ca8 81.04(11) . 5_656
Mn5 Sb1 Ca8 155.67(9) 5_666 5_656
Mn5 Sb1 Ca8 72.64(8) 5_656 5_656
Mn6B Sb1 Ca8 63.63(7) . 5_656
Ca8 Sb1 Ca8 93.49(9) 5_666 5_656
Mn6A Sb1 Ca1 127.97(16) . 7_565
Mn5 Sb1 Ca1 50.01(9) 5_666 7_565
Mn5 Sb1 Ca1 63.80(9) 5_656 7_565
Mn6B Sb1 Ca1 154.65(10) . 7_565
Ca8 Sb1 Ca1 121.83(9) 5_666 7_565
Ca8 Sb1 Ca1 134.74(9) 5_656 7_565
Mn6A Sb1 Ca1 127.97(16) . .
Mn5 Sb1 Ca1 63.80(9) 5_666 .
Mn5 Sb1 Ca1 50.01(9) 5_656 .
Mn6B Sb1 Ca1 154.65(10) . .
Ca8 Sb1 Ca1 134.74(9) 5_666 .
Ca8 Sb1 Ca1 121.83(9) 5_656 .
Ca1 Sb1 Ca1 13.92(14) 7_565 .
Mn6A Sb1 Ca5 155.25(15) . .
Mn5 Sb1 Ca5 76.36(8) 5_666 .
Mn5 Sb1 Ca5 76.36(8) 5_656 .
Mn6B Sb1 Ca5 127.99(8) . .
Ca8 Sb1 Ca5 82.07(7) 5_666 .
Ca8 Sb1 Ca5 82.07(7) 5_656 .
Ca1 Sb1 Ca5 76.55(9) 7_565 .
Ca1 Sb1 Ca5 76.55(9) . .
Mn6A Sb1 Ca9 57.75(11) . 5_666
Mn5 Sb1 Ca9 58.78(9) 5_666 5_666
Mn5 Sb1 Ca9 127.60(9) 5_656 5_666
Mn6B Sb1 Ca9 75.89(8) . 5_666
Ca8 Sb1 Ca9 75.99(7) 5_666 5_666
Ca8 Sb1 Ca9 138.39(9) 5_656 5_666
Ca1 Sb1 Ca9 81.59(10) 7_565 5_666
Ca1 Sb1 Ca9 91.06(10) . 5_666
Ca5 Sb1 Ca9 134.06(5) . 5_666
Mn6A Sb1 Ca9 57.75(11) . 5_656
Mn5 Sb1 Ca9 127.60(9) 5_666 5_656
Mn5 Sb1 Ca9 58.78(9) 5_656 5_656
Mn6B Sb1 Ca9 75.89(8) . 5_656
Ca8 Sb1 Ca9 138.39(9) 5_666 5_656
Ca8 Sb1 Ca9 75.99(7) 5_656 5_656
Ca1 Sb1 Ca9 91.06(10) 7_565 5_656
Ca1 Sb1 Ca9 81.59(10) . 5_656
Ca5 Sb1 Ca9 134.06(5) . 5_656
Ca9 Sb1 Ca9 85.61(9) 5_666 5_656
Mn3 Sb2 Mn3 116.22(17) 5_666 5_656
Mn3 Sb2 Mn1 121.34(8) 5_666 .
Mn3 Sb2 Mn1 121.34(8) 5_656 .
Mn3 Sb2 Ca7 68.89(10) 5_666 5_666
Mn3 Sb2 Ca7 150.60(11) 5_656 5_666
Mn1 Sb2 Ca7 67.04(5) . 5_666
Mn3 Sb2 Ca7 150.60(11) 5_666 5_656
Mn3 Sb2 Ca7 68.89(10) 5_656 5_656
Mn1 Sb2 Ca7 67.04(5) . 5_656
Ca7 Sb2 Ca7 92.96(7) 5_666 5_656
Mn3 Sb2 Ca6 55.85(11) 5_666 2_564
Mn3 Sb2 Ca6 130.58(11) 5_656 2_564
Mn1 Sb2 Ca6 78.16(7) . 2_564
Ca7 Sb2 Ca6 77.44(6) 5_666 2_564
Ca7 Sb2 Ca6 144.84(8) 5_656 2_564
Mn3 Sb2 Ca6 130.58(11) 5_666 2_554
Mn3 Sb2 Ca6 55.85(11) 5_656 2_554
Mn1 Sb2 Ca6 78.16(7) . 2_554
Ca7 Sb2 Ca6 144.84(8) 5_666 2_554
Ca7 Sb2 Ca6 77.44(6) 5_656 2_554
Ca6 Sb2 Ca6 91.07(8) 2_564 2_554
Mn3 Sb2 Ca2 58.76(9) 5_666 .
Mn3 Sb2 Ca2 58.76(9) 5_656 .
Mn1 Sb2 Ca2 158.87(7) . .
Ca7 Sb2 Ca2 124.64(5) 5_666 .
Ca7 Sb2 Ca2 124.64(5) 5_656 .
Ca6 Sb2 Ca2 87.13(7) 2_564 .
Ca6 Sb2 Ca2 87.13(7) 2_554 .
Mn3 Sb2 Ca5 75.88(10) 5_666 .
Mn3 Sb2 Ca5 75.88(10) 5_656 .
Mn1 Sb2 Ca5 127.62(7) . .
Ca7 Sb2 Ca5 77.80(6) 5_666 .
Ca7 Sb2 Ca5 77.80(6) 5_656 .
Ca6 Sb2 Ca5 130.98(5) 2_564 .
Ca6 Sb2 Ca5 130.98(5) 2_554 .
Ca2 Sb2 Ca5 73.51(7) . .
Mn2 Sb3 Mn2 113.51(8) 5_666 5_656
Mn2 Sb3 Ca8 115.49(5) 5_666 .
Mn2 Sb3 Ca8 115.49(5) 5_656 .
Mn2 Sb3 Ca7 76.34(5) 5_666 .
Mn2 Sb3 Ca7 76.34(5) 5_656 .
Ca8 Sb3 Ca7 153.80(8) . .
Mn2 Sb3 Ca4 79.17(5) 5_666 .
Mn2 Sb3 Ca4 79.17(5) 5_656 .
Ca8 Sb3 Ca4 71.78(8) . .
Ca7 Sb3 Ca4 134.42(8) . .
Mn2 Sb3 Ca5 73.60(5) 5_666 5_666
Mn2 Sb3 Ca5 151.26(7) 5_656 5_666
Ca8 Sb3 Ca5 82.45(6) . 5_666
Ca7 Sb3 Ca5 78.75(6) . 5_666
Ca4 Sb3 Ca5 129.21(5) . 5_666
Mn2 Sb3 Ca5 151.26(7) 5_666 5_656
Mn2 Sb3 Ca5 73.60(5) 5_656 5_656
Ca8 Sb3 Ca5 82.45(6) . 5_656
Ca7 Sb3 Ca5 78.75(6) . 5_656
Ca4 Sb3 Ca5 129.21(5) . 5_656
Ca5 Sb3 Ca5 87.74(7) 5_666 5_656
Mn1 Sb4 Mn1 114.05(7) 5_666 5_656
Mn1 Sb4 Ca3 110.15(5) 5_666 6_657
Mn1 Sb4 Ca3 110.15(5) 5_656 6_657
Mn1 Sb4 Ca2 76.24(5) 5_666 2_565
Mn1 Sb4 Ca2 162.22(7) 5_656 2_565
Ca3 Sb4 Ca2 77.52(6) 6_657 2_565
Mn1 Sb4 Ca2 162.22(7) 5_666 2
Mn1 Sb4 Ca2 76.24(5) 5_656 2
Ca3 Sb4 Ca2 77.52(6) 6_657 2
Ca2 Sb4 Ca2 90.36(7) 2_565 2
Mn1 Sb4 Ca6 80.12(5) 5_666 .
Mn1 Sb4 Ca6 80.12(5) 5_656 .
Ca3 Sb4 Ca6 159.12(8) 6_657 .
Ca2 Sb4 Ca6 87.87(7) 2_565 .
Ca2 Sb4 Ca6 87.87(7) 2 .
Mn1 Sb4 Ca6 75.55(5) 5_666 6_657
Mn1 Sb4 Ca6 75.55(5) 5_656 6_657
Ca3 Sb4 Ca6 66.54(8) 6_657 6_657
Ca2 Sb4 Ca6 121.97(6) 2_565 6_657
Ca2 Sb4 Ca6 121.97(6) 2 6_657
Ca6 Sb4 Ca6 134.34(3) . 6_657
Mn6B Sb5 Mn6B 113.67(11) 5_666 5_656
Mn6B Sb5 Mn6A 27.16(15) 5_666 5_666
Mn6B Sb5 Mn6A 120.37(13) 5_656 5_666
Mn6B Sb5 Mn6A 120.37(13) 5_666 5_656
Mn6B Sb5 Mn6A 27.16(15) 5_656 5_656
Mn6A Sb5 Mn6A 112.9(2) 5_666 5_656
Mn6B Sb5 Mn6B 74.65(8) 5_666 .
Mn6B Sb5 Mn6B 74.65(8) 5_656 .
Mn6A Sb5 Mn6B 101.74(14) 5_666 .
Mn6A Sb5 Mn6B 101.74(14) 5_656 .
Mn6B Sb5 Ca8 62.92(8) 5_666 5_666
Mn6B Sb5 Ca8 134.83(8) 5_656 5_666
Mn6A Sb5 Ca8 78.13(12) 5_666 5_666
Mn6A Sb5 Ca8 161.72(14) 5_656 5_666
Mn6B Sb5 Ca8 60.80(6) . 5_666
Mn6B Sb5 Ca8 134.83(8) 5_666 5_656
Mn6B Sb5 Ca8 62.92(8) 5_656 5_656
Mn6A Sb5 Ca8 161.72(14) 5_666 5_656
Mn6A Sb5 Ca8 78.13(12) 5_656 5_656
Mn6B Sb5 Ca8 60.80(6) . 5_656
Ca8 Sb5 Ca8 87.74(8) 5_666 5_656
Mn6B Sb5 Ca9 77.47(7) 5_666 .
Mn6B Sb5 Ca9 77.47(7) 5_656 .
Mn6A Sb5 Ca9 57.93(12) 5_666 .
Mn6A Sb5 Ca9 57.93(12) 5_656 .
Mn6B Sb5 Ca9 127.69(9) . .
Ca8 Sb5 Ca9 135.91(4) 5_666 .
Ca8 Sb5 Ca9 135.91(4) 5_656 .
Mn6B Sb5 Ca4 77.05(7) 5_666 5_666
Mn6B Sb5 Ca4 156.89(8) 5_656 5_666
Mn6A Sb5 Ca4 60.04(13) 5_666 5_666
Mn6A Sb5 Ca4 129.75(15) 5_656 5_666
Mn6B Sb5 Ca4 128.46(6) . 5_666
Ca8 Sb5 Ca4 68.09(7) 5_666 5_666
Ca8 Sb5 Ca4 125.02(7) 5_656 5_666
Ca9 Sb5 Ca4 85.56(7) . 5_666
Mn6B Sb5 Ca4 156.89(8) 5_666 5_656
Mn6B Sb5 Ca4 77.05(7) 5_656 5_656
Mn6A Sb5 Ca4 129.75(15) 5_666 5_656
Mn6A Sb5 Ca4 60.04(13) 5_656 5_656
Mn6B Sb5 Ca4 128.46(6) . 5_656
Ca8 Sb5 Ca4 125.02(7) 5_666 5_656
Ca8 Sb5 Ca4 68.09(7) 5_656 5_656
Ca9 Sb5 Ca4 85.56(7) . 5_656
Ca4 Sb5 Ca4 86.19(8) 5_666 5_656
Mn6B Sb5 Ca8 56.92(5) 5_666 .
Mn6B Sb5 Ca8 56.92(5) 5_656 .
Mn6A Sb5 Ca8 71.18(13) 5_666 .
Mn6A Sb5 Ca8 71.18(13) 5_656 .
Mn6B Sb5 Ca8 57.33(8) . .
Ca8 Sb5 Ca8 100.57(7) 5_666 .
Ca8 Sb5 Ca8 100.57(7) 5_656 .
Ca9 Sb5 Ca8 70.36(8) . .
Ca4 Sb5 Ca8 131.13(5) 5_666 .
Ca4 Sb5 Ca8 131.13(5) 5_656 .
Mn2 Sb6 Mn1 121.75(6) . .
Mn2 Sb6 Ca7 74.25(5) . 5_666
Mn1 Sb6 Ca7 66.21(5) . 5_666
Mn2 Sb6 Ca7 74.25(5) . 5_656
Mn1 Sb6 Ca7 66.21(5) . 5_656
Ca7 Sb6 Ca7 91.58(7) 5_666 5_656
Mn2 Sb6 Ca3 67.13(5) . 5_666
Mn1 Sb6 Ca3 134.40(4) . 5_666
Ca7 Sb6 Ca3 75.92(6) 5_666 5_666
Ca7 Sb6 Ca3 141.30(7) 5_656 5_666
Mn2 Sb6 Ca3 67.13(5) . 5_656
Mn1 Sb6 Ca3 134.40(4) . 5_656
Ca7 Sb6 Ca3 141.30(7) 5_666 5_656
Ca7 Sb6 Ca3 75.92(6) 5_656 5_656
Ca3 Sb6 Ca3 91.14(7) 5_666 5_656
Mn2 Sb6 Ca6 132.37(5) . 5_666
Mn1 Sb6 Ca6 79.33(7) . 5_666
Ca7 Sb6 Ca6 78.53(6) 5_666 5_666
Ca7 Sb6 Ca6 145.17(8) 5_656 5_666
Ca3 Sb6 Ca6 68.77(7) 5_666 5_666
Ca3 Sb6 Ca6 130.83(8) 5_656 5_666
Mn2 Sb6 Ca6 132.37(5) . 5_656
Mn1 Sb6 Ca6 79.33(7) . 5_656
Ca7 Sb6 Ca6 145.17(8) 5_666 5_656
Ca7 Sb6 Ca6 78.53(6) 5_656 5_656
Ca3 Sb6 Ca6 130.83(8) 5_666 5_656
Ca3 Sb6 Ca6 68.77(7) 5_656 5_656
Ca6 Sb6 Ca6 90.69(8) 5_666 5_656
Mn3 Sb7 Mn4 125.99(14) . 1_655
Mn3 Sb7 Mn5 157.35(14) . .
Mn4 Sb7 Mn5 76.66(12) 1_655 .
Mn3 Sb7 Ca1 140.03(9) . 3_656
Mn4 Sb7 Ca1 50.54(9) 1_655 3_656
Mn5 Sb7 Ca1 51.75(9) . 3_656
Mn3 Sb7 Ca1 140.03(8) . 5_656
Mn4 Sb7 Ca1 50.54(9) 1_655 5_656
Mn5 Sb7 Ca1 51.75(9) . 5_656
Ca1 Sb7 Ca1 73.77(14) 3_656 5_656
Mn3 Sb7 Ca5 82.76(9) . 5_666
Mn4 Sb7 Ca5 128.65(5) 1_655 5_666
Mn5 Sb7 Ca5 81.63(7) . 5_666
Ca1 Sb7 Ca5 79.57(9) 3_656 5_666
Ca1 Sb7 Ca5 133.30(9) 5_656 5_666
Mn3 Sb7 Ca5 82.76(9) . 5_656
Mn4 Sb7 Ca5 128.65(5) 1_655 5_656
Mn5 Sb7 Ca5 81.63(7) . 5_656
Ca1 Sb7 Ca5 133.30(9) 3_656 5_656
Ca1 Sb7 Ca5 79.57(9) 5_656 5_656
Ca5 Sb7 Ca5 92.45(8) 5_666 5_656
Mn3 Sb7 Ca2 62.53(8) . 5_666
Mn4 Sb7 Ca2 81.02(8) 1_655 5_666
Mn5 Sb7 Ca2 128.98(5) . 5_666
Ca1 Sb7 Ca2 78.74(9) 3_656 5_666
Ca1 Sb7 Ca2 131.35(10) 5_656 5_666
Ca5 Sb7 Ca2 77.65(6) 5_666 5_666
Ca5 Sb7 Ca2 144.67(7) 5_656 5_666
Mn3 Sb7 Ca2 62.53(8) . 5_656
Mn4 Sb7 Ca2 81.02(8) 1_655 5_656
Mn5 Sb7 Ca2 128.98(5) . 5_656
Ca1 Sb7 Ca2 131.35(10) 3_656 5_656
Ca1 Sb7 Ca2 78.74(8) 5_656 5_656
Ca5 Sb7 Ca2 144.67(7) 5_666 5_656
Ca5 Sb7 Ca2 77.65(6) 5_656 5_656
Ca2 Sb7 Ca2 90.97(7) 5_666 5_656
Mn3 Sb7 Ca1 131.14(7) . 5_666
Mn4 Sb7 Ca1 56.93(8) 1_655 5_666
Mn5 Sb7 Ca1 57.89(8) . 5_666
Ca1 Sb7 Ca1 9.75(10) 3_656 5_666
Ca1 Sb7 Ca1 83.52(9) 5_656 5_666
Ca5 Sb7 Ca1 72.05(8) 5_666 5_666
Ca5 Sb7 Ca1 137.87(8) 5_656 5_666
Ca2 Sb7 Ca1 71.42(8) 5_666 5_666
Ca2 Sb7 Ca1 135.90(9) 5_656 5_666
Mn3 Sb7 Ca1 131.14(7) . 3_646
Mn4 Sb7 Ca1 56.93(8) 1_655 3_646
Mn5 Sb7 Ca1 57.89(8) . 3_646
Ca1 Sb7 Ca1 83.52(9) 3_656 3_646
Ca1 Sb7 Ca1 9.75(10) 5_656 3_646
Ca5 Sb7 Ca1 137.87(8) 5_666 3_646
Ca5 Sb7 Ca1 72.05(8) 5_656 3_646
Ca2 Sb7 Ca1 135.90(9) 5_666 3_646
Ca2 Sb7 Ca1 71.42(8) 5_656 3_646
Ca1 Sb7 Ca1 93.27(12) 5_666 3_646
Mn4 Sb8 Mn4 109.88(13) 5_666 5_656
Mn4 Sb8 Mn2 124.53(7) 5_666 .
Mn4 Sb8 Mn2 124.53(7) 5_656 .
Mn4 Sb8 Ca3 70.49(8) 5_666 5_666
Mn4 Sb8 Ca3 149.30(9) 5_656 5_666
Mn2 Sb8 Ca3 68.35(6) . 5_666
Mn4 Sb8 Ca3 149.30(9) 5_666 5_656
Mn4 Sb8 Ca3 70.49(8) 5_656 5_656
Mn2 Sb8 Ca3 68.35(6) . 5_656
Ca3 Sb8 Ca3 93.64(8) 5_666 5_656
Mn4 Sb8 Ca1 49.06(10) 5_666 7_665
Mn4 Sb8 Ca1 63.02(10) 5_656 7_665
Mn2 Sb8 Ca1 156.19(9) . 7_665
Ca3 Sb8 Ca1 117.99(9) 5_666 7_665
Ca3 Sb8 Ca1 130.46(9) 5_656 7_665
Mn4 Sb8 Ca1 63.02(10) 5_666 1_655
Mn4 Sb8 Ca1 49.06(9) 5_656 1_655
Mn2 Sb8 Ca1 156.19(9) . 1_655
Ca3 Sb8 Ca1 130.46(9) 5_666 1_655
Ca3 Sb8 Ca1 117.99(8) 5_656 1_655
Ca1 Sb8 Ca1 14.14(14) 7_665 1_655
Mn4 Sb8 Ca4 59.30(8) 5_666 5_666
Mn4 Sb8 Ca4 129.39(9) 5_656 5_666
Mn2 Sb8 Ca4 77.21(6) . 5_666
Ca3 Sb8 Ca4 78.45(6) 5_666 5_666
Ca3 Sb8 Ca4 145.08(8) 5_656 5_666
Ca1 Sb8 Ca4 81.67(9) 7_665 5_666
Ca1 Sb8 Ca4 91.57(9) 1_655 5_666
Mn4 Sb8 Ca4 129.40(9) 5_666 5_656
Mn4 Sb8 Ca4 59.30(8) 5_656 5_656
Mn2 Sb8 Ca4 77.21(6) . 5_656
Ca3 Sb8 Ca4 145.08(8) 5_666 5_656
Ca3 Sb8 Ca4 78.45(6) 5_656 5_656
Ca1 Sb8 Ca4 91.57(9) 7_665 5_656
Ca1 Sb8 Ca4 81.67(9) 1_655 5_656
Ca4 Sb8 Ca4 88.78(8) 5_666 5_656
Mn4 Sb8 Ca2 74.78(8) 5_666 1_655
Mn4 Sb8 Ca2 74.78(8) 5_656 1_655
Mn2 Sb8 Ca2 126.56(7) . 1_655
Ca3 Sb8 Ca2 75.93(6) 5_666 1_655
Ca3 Sb8 Ca2 75.93(6) 5_656 1_655
Ca1 Sb8 Ca2 76.34(9) 7_665 1_655
Ca1 Sb8 Ca2 76.34(9) 1_655 1_655
Ca4 Sb8 Ca2 132.66(5) 5_666 1_655
Ca4 Sb8 Ca2 132.66(5) 5_656 1_655
Sb9B Sb9A Ca1 131.98(12) . 3_556
Sb9B Sb9A Ca1 131.98(12) . 5_556
Ca1 Sb9A Ca1 94.42(19) 3_556 5_556
Sb9B Sb9A Mn5 153.3(4) . 1_455
Ca1 Sb9A Mn5 57.01(11) 3_556 1_455
Ca1 Sb9A Mn5 57.01(11) 5_556 1_455
Sb9B Sb9A Mn4 137.0(4) . .
Ca1 Sb9A Mn4 55.28(10) 3_556 .
Ca1 Sb9A Mn4 55.28(10) 5_556 .
Mn5 Sb9A Mn4 69.74(11) 1_455 .
Sb9B Sb9A Ca1 122.70(10) . 5_566
Ca1 Sb9A Ca1 9.52(10) 3_556 5_566
Ca1 Sb9A Ca1 103.94(14) 5_556 5_566
Mn5 Sb9A Ca1 63.92(9) 1_455 5_566
Mn4 Sb9A Ca1 62.61(8) . 5_566
Sb9B Sb9A Ca1 122.70(9) . 3_546
Ca1 Sb9A Ca1 103.94(14) 3_556 3_546
Ca1 Sb9A Ca1 9.52(10) 5_556 3_546
Mn5 Sb9A Ca1 63.92(9) 1_455 3_546
Mn4 Sb9A Ca1 62.61(8) . 3_546
Ca1 Sb9A Ca1 113.46(15) 5_566 3_546
Sb9B Sb9A Ca9 92.6(4) . 1_455
Ca1 Sb9A Ca9 95.06(11) 3_556 1_455
Ca1 Sb9A Ca9 95.06(12) 5_556 1_455
Mn5 Sb9A Ca9 60.74(10) 1_455 1_455
Mn4 Sb9A Ca9 130.48(12) . 1_455
Ca1 Sb9A Ca9 94.09(9) 5_566 1_455
Ca1 Sb9A Ca9 94.09(9) 3_546 1_455
Sb9B Sb9A Ca4 77.1(4) . .
Ca1 Sb9A Ca4 91.94(11) 3_556 .
Ca1 Sb9A Ca4 91.94(11) 5_556 .
Mn5 Sb9A Ca4 129.59(11) 1_455 .
Mn4 Sb9A Ca4 59.84(10) . .
Ca1 Sb9A Ca4 91.57(9) 5_566 .
Ca1 Sb9A Ca4 91.57(9) 3_546 .
Ca9 Sb9A Ca4 169.67(11) 1_455 .
Sb9B Sb9A Ca9 44.76(8) . 5_666
Ca1 Sb9A Ca9 88.85(10) 3_556 5_666
Ca1 Sb9A Ca9 176.71(11) 5_556 5_666
Mn5 Sb9A Ca9 125.49(8) 1_455 5_666
Mn4 Sb9A Ca9 126.92(8) . 5_666
Ca1 Sb9A Ca9 79.33(8) 5_566 5_666
Ca1 Sb9A Ca9 167.21(10) 3_546 5_666
Ca9 Sb9A Ca9 84.95(10) 1_455 5_666
Ca4 Sb9A Ca9 87.62(9) . 5_666
Sb9B Sb9A Ca9 44.76(8) . 5_656
Ca1 Sb9A Ca9 176.72(12) 3_556 5_656
Ca1 Sb9A Ca9 88.85(10) 5_556 5_656
Mn5 Sb9A Ca9 125.48(8) 1_455 5_656
Mn4 Sb9A Ca9 126.92(8) . 5_656
Ca1 Sb9A Ca9 167.21(10) 5_566 5_656
Ca1 Sb9A Ca9 79.33(8) 3_546 5_656
Ca9 Sb9A Ca9 84.95(10) 1_455 5_656
Ca4 Sb9A Ca9 87.62(9) . 5_656
Ca9 Sb9A Ca9 87.88(10) 5_666 5_656
Sb9A Sb9B Mn6A 153.1(4) . .
Sb9A Sb9B Ca9 126.33(10) . 5_666
Mn6A Sb9B Ca9 62.20(10) . 5_666
Sb9A Sb9B Ca9 126.33(10) . 5_656
Mn6A Sb9B Ca9 62.20(10) . 5_656
Ca9 Sb9B Ca9 105.09(15) 5_666 5_656
Sb9A Sb9B Ca1 39.12(10) . 3_556
Mn6A Sb9B Ca1 130.28(13) . 3_556
Ca9 Sb9B Ca1 88.79(10) 5_666 3_556
Ca9 Sb9B Ca1 165.45(13) 5_656 3_556
Sb9A Sb9B Ca1 39.12(10) . 5_556
Mn6A Sb9B Ca1 130.28(12) . 5_556
Ca9 Sb9B Ca1 165.45(13) 5_666 5_556
Ca9 Sb9B Ca1 88.79(10) 5_656 5_556
Ca1 Sb9B Ca1 77.06(16) 3_556 5_556
Sb9A Sb9B Ca4 91.6(4) . .
Mn6A Sb9B Ca4 61.51(15) . .
Ca9 Sb9B Ca4 96.92(11) 5_666 .
Ca9 Sb9B Ca4 96.92(11) 5_656 .
Ca1 Sb9B Ca4 85.49(11) 3_556 .
Ca1 Sb9B Ca4 85.49(11) 5_556 .
Sb9A Sb9B Ca9 76.4(4) . 1_455
Mn6A Sb9B Ca9 130.48(17) . 1_455
Ca9 Sb9B Ca9 90.34(11) 5_666 1_455
Ca9 Sb9B Ca9 90.34(11) 5_656 1_455
Ca1 Sb9B Ca9 85.14(11) 3_556 1_455
Ca1 Sb9B Ca9 85.14(11) 5_556 1_455
Ca4 Sb9B Ca9 168.01(13) . 1_455
Sb9A Sb9B Ca1 48.75(9) . 5_566
Mn6A Sb9B Ca1 123.33(10) . 5_566
Ca9 Sb9B Ca1 79.01(9) 5_666 5_566
Ca9 Sb9B Ca1 174.46(13) 5_656 5_566
Ca1 Sb9B Ca1 9.80(10) 3_556 5_566
Ca1 Sb9B Ca1 86.86(12) 5_556 5_566
Ca4 Sb9B Ca1 86.16(10) . 5_566
Ca9 Sb9B Ca1 85.87(10) 1_455 5_566
Sb9A Sb9B Ca1 48.75(9) . 3_546
Mn6A Sb9B Ca1 123.33(10) . 3_546
Ca9 Sb9B Ca1 174.46(13) 5_666 3_546
Ca9 Sb9B Ca1 79.01(9) 5_656 3_546
Ca1 Sb9B Ca1 86.86(12) 3_556 3_546
Ca1 Sb9B Ca1 9.80(10) 5_556 3_546
Ca4 Sb9B Ca1 86.16(10) . 3_546
Ca9 Sb9B Ca1 85.87(10) 1_455 3_546
Ca1 Sb9B Ca1 96.65(14) 5_566 3_546
Sb4 Mn1 Sb4 114.04(7) 5_666 5_656
Sb4 Mn1 Sb2 113.23(5) 5_666 .
Sb4 Mn1 Sb2 113.23(5) 5_656 .
Sb4 Mn1 Sb6 108.55(5) 5_666 .
Sb4 Mn1 Sb6 108.55(5) 5_656 .
Sb2 Mn1 Sb6 97.79(6) . .
Sb4 Mn1 Ca7 79.18(4) 5_666 5_666
Sb4 Mn1 Ca7 166.34(7) 5_656 5_666
Sb2 Mn1 Ca7 61.35(5) . 5_666
Sb6 Mn1 Ca7 61.91(5) . 5_666
Sb4 Mn1 Ca7 166.34(7) 5_666 5_656
Sb4 Mn1 Ca7 79.18(4) 5_656 5_656
Sb2 Mn1 Ca7 61.35(5) . 5_656
Sb6 Mn1 Ca7 61.91(5) . 5_656
Ca7 Mn1 Ca7 87.43(8) 5_666 5_656
Sb4 Mn1 Ca2 57.97(4) 5_666 6_656
Sb4 Mn1 Ca2 57.97(4) 5_656 6_656
Sb2 Mn1 Ca2 149.42(8) . 6_656
Sb6 Mn1 Ca2 112.79(8) . 6_656
Ca7 Mn1 Ca2 133.47(5) 5_666 6_656
Ca7 Mn1 Ca2 133.47(5) 5_656 6_656
Sb3 Mn2 Sb3 113.51(8) 5_666 5_656
Sb3 Mn2 Sb8 110.35(5) 5_666 .
Sb3 Mn2 Sb8 110.35(5) 5_656 .
Sb3 Mn2 Sb6 112.08(5) 5_666 .
Sb3 Mn2 Sb6 112.08(5) 5_656 .
Sb8 Mn2 Sb6 97.34(6) . .
Sb3 Mn2 Ca3 80.13(4) 5_666 5_666
Sb3 Mn2 Ca3 166.19(7) 5_656 5_666
Sb8 Mn2 Ca3 60.53(6) . 5_666
Sb6 Mn2 Ca3 61.80(6) . 5_666
Sb3 Mn2 Ca3 166.20(7) 5_666 5_656
Sb3 Mn2 Ca3 80.13(4) 5_656 5_656
Sb8 Mn2 Ca3 60.53(6) . 5_656
Sb6 Mn2 Ca3 61.80(6) . 5_656
Ca3 Mn2 Ca3 86.16(8) 5_666 5_656
Sb3 Mn2 Ca5 60.34(4) 5_666 .
Sb3 Mn2 Ca5 60.34(4) 5_656 .
Sb8 Mn2 Ca5 154.85(8) . .
Sb6 Mn2 Ca5 107.81(7) . .
Ca3 Mn2 Ca5 132.43(5) 5_666 .
Ca3 Mn2 Ca5 132.43(5) 5_656 .
Sb3 Mn2 Ca7 56.84(4) 5_666 5_666
Sb3 Mn2 Ca7 120.19(7) 5_656 5_666
Sb8 Mn2 Ca7 128.80(6) . 5_666
Sb6 Mn2 Ca7 57.44(5) . 5_666
Ca3 Mn2 Ca7 68.29(6) 5_666 5_666
Ca3 Mn2 Ca7 119.18(8) 5_656 5_666
Ca5 Mn2 Ca7 68.23(6) . 5_666
Sb3 Mn2 Ca7 120.19(7) 5_666 5_656
Sb3 Mn2 Ca7 56.84(4) 5_656 5_656
Sb8 Mn2 Ca7 128.80(6) . 5_656
Sb6 Mn2 Ca7 57.44(5) . 5_656
Ca3 Mn2 Ca7 119.18(8) 5_666 5_656
Ca3 Mn2 Ca7 68.29(6) 5_656 5_656
Ca5 Mn2 Ca7 68.23(6) . 5_656
Ca7 Mn2 Ca7 77.76(6) 5_666 5_656
Sb7 Mn3 Sb2 113.43(11) . 5_666
Sb7 Mn3 Sb2 113.43(11) . 5_656
Sb2 Mn3 Sb2 116.22(17) 5_666 5_656
Sb7 Mn3 Ca6 168.4(2) . 6_657
Sb2 Mn3 Ca6 71.36(10) 5_666 6_657
Sb2 Mn3 Ca6 71.36(10) 5_656 6_657
Sb7 Mn3 Ca2 71.18(11) . 5_666
Sb2 Mn3 Ca2 71.23(5) 5_666 5_666
Sb2 Mn3 Ca2 165.95(19) 5_656 5_666
Ca6 Mn3 Ca2 101.70(13) 6_657 5_666
Sb7 Mn3 Ca2 71.18(11) . 5_656
Sb2 Mn3 Ca2 165.95(19) 5_666 5_656
Sb2 Mn3 Ca2 71.23(5) 5_656 5_656
Ca6 Mn3 Ca2 101.70(13) 6_657 5_656
Ca2 Mn3 Ca2 99.07(16) 5_666 5_656
Sb7 Mn3 Ca7 111.15(17) . .
Sb2 Mn3 Ca7 62.10(9) 5_666 .
Sb2 Mn3 Ca7 62.10(9) 5_656 .
Ca6 Mn3 Ca7 80.44(13) 6_657 .
Ca2 Mn3 Ca7 129.91(8) 5_666 .
Ca2 Mn3 Ca7 129.91(8) 5_656 .
Sb7 Mn3 Ca5 56.88(9) . 5_666
Sb2 Mn3 Ca5 59.99(7) 5_666 5_666
Sb2 Mn3 Ca5 122.35(16) 5_656 5_666
Ca6 Mn3 Ca5 130.59(11) 6_657 5_666
Ca2 Mn3 Ca5 71.55(8) 5_666 5_666
Ca2 Mn3 Ca5 127.66(15) 5_656 5_666
Ca7 Mn3 Ca5 70.21(10) . 5_666
Sb7 Mn3 Ca5 56.88(9) . 5_656
Sb2 Mn3 Ca5 122.35(16) 5_666 5_656
Sb2 Mn3 Ca5 59.99(7) 5_656 5_656
Ca6 Mn3 Ca5 130.59(11) 6_657 5_656
Ca2 Mn3 Ca5 127.66(15) 5_666 5_656
Ca2 Mn3 Ca5 71.55(8) 5_656 5_656
Ca7 Mn3 Ca5 70.21(10) . 5_656
Ca5 Mn3 Ca5 75.12(10) 5_666 5_656
Ca1 Mn4 Ca1 98.9(2) 3_556 5_556
Ca1 Mn4 Sb7 77.73(13) 3_556 1_455
Ca1 Mn4 Sb7 77.73(13) 5_556 1_455
Ca1 Mn4 Sb9A 58.31(12) 3_556 .
Ca1 Mn4 Sb9A 58.31(12) 5_556 .
Sb7 Mn4 Sb9A 107.03(14) 1_455 .
Ca1 Mn4 Sb8 73.25(10) 3_556 5_666
Ca1 Mn4 Sb8 162.85(18) 5_556 5_666
Sb7 Mn4 Sb8 114.32(9) 1_455 5_666
Sb9A Mn4 Sb8 105.21(9) . 5_666
Ca1 Mn4 Sb8 162.85(18) 3_556 5_656
Ca1 Mn4 Sb8 73.25(10) 5_556 5_656
Sb7 Mn4 Sb8 114.32(9) 1_455 5_656
Sb9A Mn4 Sb8 105.21(9) . 5_656
Sb8 Mn4 Sb8 109.88(13) 5_666 5_656
Ca1 Mn4 Ca4 98.78(14) 3_556 .
Ca1 Mn4 Ca4 98.78(14) 5_556 .
Sb7 Mn4 Ca4 174.50(16) 1_455 .
Sb9A Mn4 Ca4 67.47(10) . .
Sb8 Mn4 Ca4 68.19(8) 5_666 .
Sb8 Mn4 Ca4 68.19(8) 5_656 .
Ca1 Mn4 Ca1 9.32(10) 3_556 5_566
Ca1 Mn4 Ca1 108.19(18) 5_556 5_566
Sb7 Mn4 Ca1 80.24(11) 1_455 5_566
Sb9A Mn4 Ca1 65.22(10) . 5_566
Sb8 Mn4 Ca1 64.30(8) 5_666 5_566
Sb8 Mn4 Ca1 165.01(16) 5_656 5_566
Ca4 Mn4 Ca1 97.00(11) . 5_566
Ca1 Mn4 Ca1 108.19(19) 3_556 3_546
Ca1 Mn4 Ca1 9.32(9) 5_556 3_546
Sb7 Mn4 Ca1 80.24(11) 1_455 3_546
Sb9A Mn4 Ca1 65.22(10) . 3_546
Sb8 Mn4 Ca1 165.01(16) 5_666 3_546
Sb8 Mn4 Ca1 64.30(8) 5_656 3_546
Ca4 Mn4 Ca1 97.00(11) . 3_546
Ca1 Mn4 Ca1 117.51(19) 5_566 3_546
Ca1 Mn4 Mn5 51.99(12) 3_556 1_455
Ca1 Mn4 Mn5 51.99(12) 5_556 1_455
Sb7 Mn4 Mn5 52.19(9) 1_455 1_455
Sb9A Mn4 Mn5 54.84(10) . 1_455
Sb8 Mn4 Mn5 124.67(7) 5_666 1_455
Sb8 Mn4 Mn5 124.67(7) 5_656 1_455
Ca4 Mn4 Mn5 122.31(14) . 1_455
Ca1 Mn4 Mn5 60.58(10) 5_566 1_455
Ca1 Mn4 Mn5 60.58(10) 3_546 1_455
Ca1 Mn4 Ca3 130.55(11) 3_556 .
Ca1 Mn4 Ca3 130.55(11) 5_556 .
Sb7 Mn4 Ca3 108.11(13) 1_455 .
Sb9A Mn4 Ca3 144.86(15) . .
Sb8 Mn4 Ca3 59.43(7) 5_666 .
Sb8 Mn4 Ca3 59.43(7) 5_656 .
Ca4 Mn4 Ca3 77.39(11) . .
Ca1 Mn4 Ca3 121.24(9) 5_566 .
Ca1 Mn4 Ca3 121.24(9) 3_546 .
Mn5 Mn4 Ca3 160.30(15) 1_455 .
Ca1 Mn4 Ca2 77.37(11) 3_556 5_566
Ca1 Mn4 Ca2 134.72(16) 5_556 5_566
Sb7 Mn4 Ca2 57.23(7) 1_455 5_566
Sb9A Mn4 Ca2 135.63(8) . 5_566
Sb8 Mn4 Ca2 59.54(6) 5_666 5_566
Sb8 Mn4 Ca2 119.13(12) 5_656 5_566
Ca4 Mn4 Ca2 126.48(10) . 5_566
Ca1 Mn4 Ca2 71.00(9) 5_566 5_566
Ca1 Mn4 Ca2 135.43(14) 3_546 5_566
Mn5 Mn4 Ca2 97.34(10) 1_455 5_566
Ca3 Mn4 Ca2 67.37(8) . 5_566
Ca1 Mn5 Ca1 95.7(2) 3_656 5_656
Ca1 Mn5 Sb7 75.99(12) 3_656 .
Ca1 Mn5 Sb7 75.99(12) 5_656 .
Ca1 Mn5 Sb1 74.43(9) 3_656 5_666
Ca1 Mn5 Sb1 164.38(17) 5_656 5_666
Sb7 Mn5 Sb1 112.28(8) . 5_666
Ca1 Mn5 Sb1 164.38(17) 3_656 5_656
Ca1 Mn5 Sb1 74.43(10) 5_656 5_656
Sb7 Mn5 Sb1 112.28(8) . 5_656
Sb1 Mn5 Sb1 112.27(12) 5_666 5_656
Ca1 Mn5 Sb9A 57.96(11) 3_656 1_655
Ca1 Mn5 Sb9A 57.96(11) 5_656 1_655
Sb7 Mn5 Sb9A 106.57(13) . 1_655
Sb1 Mn5 Sb9A 106.46(9) 5_666 1_655
Sb1 Mn5 Sb9A 106.46(9) 5_656 1_655
Ca1 Mn5 Ca9 99.82(14) 3_656 .
Ca1 Mn5 Ca9 99.82(14) 5_656 .
Sb7 Mn5 Ca9 173.57(16) . .
Sb1 Mn5 Ca9 70.67(8) 5_666 .
Sb1 Mn5 Ca9 70.67(8) 5_656 .
Sb9A Mn5 Ca9 66.99(11) 1_655 .
Ca1 Mn5 Mn4 50.27(11) 3_656 1_655
Ca1 Mn5 Mn4 50.27(11) 5_656 1_655
Sb7 Mn5 Mn4 51.15(9) . 1_655
Sb1 Mn5 Mn4 123.77(6) 5_666 1_655
Sb1 Mn5 Mn4 123.77(6) 5_656 1_655
Sb9A Mn5 Mn4 55.42(10) 1_655 1_655
Ca9 Mn5 Mn4 122.42(15) . 1_655
Ca1 Mn5 Ca1 9.46(9) 3_656 5_666
Ca1 Mn5 Ca1 105.20(18) 5_656 5_666
Sb7 Mn5 Ca1 78.76(10) . 5_666
Sb1 Mn5 Ca1 65.19(8) 5_666 5_666
Sb1 Mn5 Ca1 168.08(15) 5_656 5_666
Sb9A Mn5 Ca1 64.73(10) 1_655 5_666
Ca9 Mn5 Ca1 97.89(11) . 5_666
Mn4 Mn5 Ca1 59.05(9) 1_655 5_666
Ca1 Mn5 Ca1 105.20(18) 3_656 3_646
Ca1 Mn5 Ca1 9.46(10) 5_656 3_646
Sb7 Mn5 Ca1 78.76(10) . 3_646
Sb1 Mn5 Ca1 168.08(15) 5_666 3_646
Sb1 Mn5 Ca1 65.19(8) 5_656 3_646
Sb9A Mn5 Ca1 64.73(9) 1_655 3_646
Ca9 Mn5 Ca1 97.89(11) . 3_646
Mn4 Mn5 Ca1 59.05(9) 1_655 3_646
Ca1 Mn5 Ca1 114.66(18) 5_666 3_646
Ca1 Mn5 Ca8 132.13(11) 3_656 .
Ca1 Mn5 Ca8 132.13(11) 5_656 .
Sb7 Mn5 Ca8 111.39(12) . .
Sb1 Mn5 Ca8 58.77(7) 5_666 .
Sb1 Mn5 Ca8 58.77(7) 5_656 .
Sb9A Mn5 Ca8 142.04(14) 1_655 .
Ca9 Mn5 Ca8 75.04(12) . .
Mn4 Mn5 Ca8 162.54(14) 1_655 .
Ca1 Mn5 Ca8 122.67(9) 5_666 .
Ca1 Mn5 Ca8 122.67(9) 3_646 .
Ca1 Mn5 Ca5 76.73(11) 3_656 5_666
Ca1 Mn5 Ca5 131.88(15) 5_656 5_666
Sb7 Mn5 Ca5 55.98(7) . 5_666
Sb1 Mn5 Ca5 58.56(6) 5_666 5_666
Sb1 Mn5 Ca5 118.88(11) 5_656 5_666
Sb9A Mn5 Ca5 134.64(8) 1_655 5_666
Ca9 Mn5 Ca5 128.28(10) . 5_666
Mn4 Mn5 Ca5 95.18(10) 1_655 5_666
Ca1 Mn5 Ca5 70.55(9) 5_666 5_666
Ca1 Mn5 Ca5 133.27(13) 3_646 5_666
Ca8 Mn5 Ca5 71.12(8) . 5_666
Mn6B Mn6A Sb1 81.8(3) . .
Mn6B Mn6A Sb5 75.9(2) . 5_666
Sb1 Mn6A Sb5 117.16(14) . 5_666
Mn6B Mn6A Sb5 75.9(2) . 5_656
Sb1 Mn6A Sb5 117.16(14) . 5_656
Sb5 Mn6A Sb5 112.9(2) 5_666 5_656
Mn6B Mn6A Sb9B 178.7(4) . .
Sb1 Mn6A Sb9B 99.5(2) . .
Sb5 Mn6A Sb9B 103.42(16) 5_666 .
Sb5 Mn6A Sb9B 103.42(16) 5_656 .
Mn6B Mn6A Ca9 121.6(2) . 5_666
Sb1 Mn6A Ca9 73.25(15) . 5_666
Sb5 Mn6A Ca9 70.61(7) 5_666 5_666
Sb5 Mn6A Ca9 161.9(3) 5_656 5_666
Sb9B Mn6A Ca9 59.01(13) . 5_666
Mn6B Mn6A Ca9 121.6(2) . 5_656
Sb1 Mn6A Ca9 73.25(15) . 5_656
Sb5 Mn6A Ca9 161.9(3) 5_666 5_656
Sb5 Mn6A Ca9 70.60(7) 5_656 5_656
Sb9B Mn6A Ca9 59.01(13) . 5_656
Ca9 Mn6A Ca9 100.6(2) 5_666 5_656
Mn6B Mn6A Ca4 115.0(4) . .
Sb1 Mn6A Ca4 163.2(3) . .
Sb5 Mn6A Ca4 69.70(13) 5_666 .
Sb5 Mn6A Ca4 69.70(13) 5_656 .
Sb9B Mn6A Ca4 63.71(15) . .
Ca9 Mn6A Ca4 96.37(17) 5_666 .
Ca9 Mn6A Ca4 96.37(17) 5_656 .
Mn6B Mn6A Ca8 50.98(18) . 5_666
Sb1 Mn6A Ca8 55.11(11) . 5_666
Sb5 Mn6A Ca8 65.45(9) 5_666 5_666
Sb5 Mn6A Ca8 126.3(2) 5_656 5_666
Sb9B Mn6A Ca8 129.85(15) . 5_666
Ca9 Mn6A Ca8 71.68(10) 5_666 5_666
Ca9 Mn6A Ca8 128.0(2) 5_656 5_666
Ca4 Mn6A Ca8 135.06(13) . 5_666
Mn6B Mn6A Ca8 50.98(18) . 5_656
Sb1 Mn6A Ca8 55.11(11) . 5_656
Sb5 Mn6A Ca8 126.3(2) 5_666 5_656
Sb5 Mn6A Ca8 65.45(9) 5_656 5_656
Sb9B Mn6A Ca8 129.85(15) . 5_656
Ca9 Mn6A Ca8 128.0(2) 5_666 5_656
Ca9 Mn6A Ca8 71.68(10) 5_656 5_656
Ca4 Mn6A Ca8 135.06(13) . 5_656
Ca8 Mn6A Ca8 74.42(13) 5_666 5_656
Mn6A Mn6B Sb5 76.94(17) . 5_666
Mn6A Mn6B Sb5 76.94(17) . 5_656
Sb5 Mn6B Sb5 113.67(11) 5_666 5_656
Mn6A Mn6B Sb1 70.9(3) . .
Sb5 Mn6B Sb1 113.38(7) 5_666 .
Sb5 Mn6B Sb1 113.38(7) 5_656 .
Mn6A Mn6B Sb5 175.4(3) . .
Sb5 Mn6B Sb5 105.35(8) 5_666 .
Sb5 Mn6B Sb5 105.35(8) 5_656 .
Sb1 Mn6B Sb5 104.55(10) . .
Mn6A Mn6B Ca8 110.4(2) . 5_666
Sb5 Mn6B Ca8 76.20(5) 5_666 5_666
Sb5 Mn6B Ca8 169.28(11) 5_656 5_666
Sb1 Mn6B Ca8 63.80(8) . 5_666
Sb5 Mn6B Ca8 66.74(8) . 5_666
Mn6A Mn6B Ca8 110.4(2) . 5_656
Sb5 Mn6B Ca8 169.28(11) 5_666 5_656
Sb5 Mn6B Ca8 76.20(5) 5_656 5_656
Sb1 Mn6B Ca8 63.80(8) . 5_656
Sb5 Mn6B Ca8 66.74(8) . 5_656
Ca8 Mn6B Ca8 93.67(12) 5_666 5_656
Mn6A Mn6B Ca8 110.7(3) . .
Sb5 Mn6B Ca8 67.29(7) 5_666 .
Sb5 Mn6B Ca8 67.29(7) 5_656 .
Sb1 Mn6B Ca8 178.38(13) . .
Sb5 Mn6B Ca8 73.83(9) . .
Ca8 Mn6B Ca8 115.25(9) 5_666 .
Ca8 Mn6B Ca8 115.25(9) 5_656 .
Ca1 Ca1 Mn4 139.44(11) 7_565 5_556
Ca1 Ca1 Mn5 137.86(11) 7_565 5_656
Mn4 Ca1 Mn5 77.74(14) 5_556 5_656
Ca1 Ca1 Sb9A 137.20(9) 7_565 5_556
Mn4 Ca1 Sb9A 66.42(13) 5_556 5_556
Mn5 Ca1 Sb9A 65.03(12) 5_656 5_556
Ca1 Ca1 Sb9B 128.52(8) 7_565 5_556
Mn4 Ca1 Sb9B 71.69(13) 5_556 5_556
Mn5 Ca1 Sb9B 72.66(13) 5_656 5_556
Sb9A Ca1 Sb9B 8.89(4) 5_556 5_556
Ca1 Ca1 Mn4 31.25(9) 7_565 5_566
Mn4 Ca1 Mn4 108.19(18) 5_556 5_566
Mn5 Ca1 Mn4 156.07(19) 5_656 5_566
Sb9A Ca1 Mn4 138.85(18) 5_556 5_566
Sb9B Ca1 Mn4 131.26(16) 5_556 5_566
Ca1 Ca1 Sb7 126.89(7) 7_565 5_656
Mn4 Ca1 Sb7 51.74(11) 5_556 5_656
Mn5 Ca1 Sb7 52.27(10) 5_656 5_656
Sb9A Ca1 Sb7 95.87(12) 5_556 5_656
Sb9B Ca1 Sb7 104.58(12) 5_556 5_656
Mn4 Ca1 Sb7 112.52(13) 5_566 5_656
Ca1 Ca1 Sb8 82.93(7) 7_565 1_455
Mn4 Ca1 Sb8 57.69(11) 5_556 1_455
Mn5 Ca1 Sb8 134.71(16) 5_656 1_455
Sb9A Ca1 Sb8 100.34(14) 5_556 1_455
Sb9B Ca1 Sb8 98.26(13) 5_556 1_455
Mn4 Ca1 Sb8 52.68(9) 5_566 1_455
Sb7 Ca1 Sb8 90.26(10) 5_656 1_455
Ca1 Ca1 Mn5 32.67(9) 7_565 5_666
Mn4 Ca1 Mn5 157.22(18) 5_556 5_666
Mn5 Ca1 Mn5 105.20(18) 5_656 5_666
Sb9A Ca1 Mn5 135.72(16) 5_556 5_666
Sb9B Ca1 Mn5 131.01(15) 5_556 5_666
Mn4 Ca1 Mn5 60.37(11) 5_566 5_666
Sb7 Ca1 Mn5 111.78(14) 5_656 5_666
Sb8 Ca1 Mn5 112.89(13) 1_455 5_666
Ca1 Ca1 Sb9A 33.26(8) 7_565 5_566
Mn4 Ca1 Sb9A 139.67(18) 5_556 5_566
Mn5 Ca1 Sb9A 135.94(17) 5_656 5_566
Sb9A Ca1 Sb9A 103.94(14) 5_556 5_566
Sb9B Ca1 Sb9A 95.29(12) 5_556 5_566
Mn4 Ca1 Sb9A 52.17(9) 5_566 5_566
Sb7 Ca1 Sb9A 160.08(14) 5_656 5_566
Sb8 Ca1 Sb9A 88.23(11) 1_455 5_566
Mn5 Ca1 Sb9A 51.35(9) 5_666 5_566
Ca1 Ca1 Sb1 83.04(7) 7_565 .
Mn4 Ca1 Sb1 132.17(17) 5_556 .
Mn5 Ca1 Sb1 55.57(10) 5_656 .
Sb9A Ca1 Sb1 98.69(13) 5_556 .
Sb9B Ca1 Sb1 100.54(13) 5_556 .
Mn4 Ca1 Sb1 111.01(13) 5_566 .
Sb7 Ca1 Sb1 87.93(10) 5_656 .
Sb8 Ca1 Sb1 160.97(14) 1_455 .
Mn5 Ca1 Sb1 51.01(8) 5_666 .
Sb9A Ca1 Sb1 87.07(10) 5_566 .
Ca1 Ca1 Sb9B 41.67(7) 7_565 5_566
Mn4 Ca1 Sb9B 134.64(18) 5_556 5_566
Mn5 Ca1 Sb9B 133.88(16) 5_656 5_566
Sb9A Ca1 Sb9B 95.56(13) 5_556 5_566
Sb9B Ca1 Sb9B 86.86(12) 5_556 5_566
Mn4 Ca1 Sb9B 57.94(10) 5_566 5_566
Sb7 Ca1 Sb9B 168.56(14) 5_656 5_566
Sb8 Ca1 Sb9B 87.99(11) 1_455 5_566
Mn5 Ca1 Sb9B 58.89(10) 5_666 5_566
Sb9A Ca1 Sb9B 8.55(3) 5_566 5_566
Sb1 Ca1 Sb9B 90.04(11) . 5_566
Mn3 Ca2 Mn3 99.07(16) 5_666 5_656
Mn3 Ca2 Sb7 46.29(9) 5_666 5_666
Mn3 Ca2 Sb7 113.20(12) 5_656 5_666
Mn3 Ca2 Sb7 113.20(12) 5_666 5_656
Mn3 Ca2 Sb7 46.29(9) 5_656 5_656
Sb7 Ca2 Sb7 90.98(7) 5_666 5_656
Mn3 Ca2 Sb4 62.84(9) 5_666 2_564
Mn3 Ca2 Sb4 128.52(12) 5_656 2_564
Sb7 Ca2 Sb4 89.01(2) 5_666 2_564
Sb7 Ca2 Sb4 173.97(10) 5_656 2_564
Mn3 Ca2 Sb4 128.52(12) 5_666 2_554
Mn3 Ca2 Sb4 62.84(9) 5_656 2_554
Sb7 Ca2 Sb4 173.97(10) 5_666 2_554
Sb7 Ca2 Sb4 89.01(2) 5_656 2_554
Sb4 Ca2 Sb4 90.36(7) 2_564 2_554
Mn3 Ca2 Sb2 50.01(8) 5_666 .
Mn3 Ca2 Sb2 50.01(8) 5_656 .
Sb7 Ca2 Sb2 82.28(6) 5_666 .
Sb7 Ca2 Sb2 82.28(6) 5_656 .
Sb4 Ca2 Sb2 91.74(6) 2_564 .
Sb4 Ca2 Sb2 91.74(6) 2_554 .
Mn3 Ca2 Sb8 126.10(9) 5_666 1_455
Mn3 Ca2 Sb8 126.10(9) 5_656 1_455
Sb7 Ca2 Sb8 85.98(6) 5_666 1_455
Sb7 Ca2 Sb8 85.98(6) 5_656 1_455
Sb4 Ca2 Sb8 100.03(7) 2_564 1_455
Sb4 Ca2 Sb8 100.03(7) 2_554 1_455
Sb2 Ca2 Sb8 163.22(9) . 1_455
Mn3 Ca2 Mn1 91.33(11) 5_666 6_556
Mn3 Ca2 Mn1 91.33(11) 5_656 6_556
Sb7 Ca2 Mn1 132.10(4) 5_666 6_556
Sb7 Ca2 Mn1 132.10(4) 5_656 6_556
Sb4 Ca2 Mn1 45.79(4) 2_564 6_556
Sb4 Ca2 Mn1 45.79(4) 2_554 6_556
Sb2 Ca2 Mn1 84.04(7) . 6_556
Sb8 Ca2 Mn1 112.74(8) 1_455 6_556
Mn3 Ca2 Mn4 81.18(9) 5_666 5_566
Mn3 Ca2 Mn4 140.38(13) 5_656 5_566
Sb7 Ca2 Mn4 41.75(6) 5_666 5_566
Sb7 Ca2 Mn4 96.87(8) 5_656 5_566
Sb4 Ca2 Mn4 87.13(5) 2_564 5_566
Sb4 Ca2 Mn4 144.20(11) 2_554 5_566
Sb2 Ca2 Mn4 124.02(8) . 5_566
Sb8 Ca2 Mn4 45.69(6) 1_455 5_566
Mn1 Ca2 Mn4 128.27(8) 6_556 5_566
Mn3 Ca2 Mn4 140.39(13) 5_666 5_556
Mn3 Ca2 Mn4 81.18(9) 5_656 5_556
Sb7 Ca2 Mn4 96.87(8) 5_666 5_556
Sb7 Ca2 Mn4 41.75(6) 5_656 5_556
Sb4 Ca2 Mn4 144.20(11) 2_564 5_556
Sb4 Ca2 Mn4 87.13(5) 2_554 5_556
Sb2 Ca2 Mn4 124.02(8) . 5_556
Sb8 Ca2 Mn4 45.69(6) 1_455 5_556
Mn1 Ca2 Mn4 128.27(8) 6_556 5_556
Mn4 Ca2 Mn4 74.75(9) 5_566 5_556
Mn3 Ca2 Ca5 62.93(10) 5_666 .
Mn3 Ca2 Ca5 62.93(10) 5_656 .
Sb7 Ca2 Ca5 50.73(4) 5_666 .
Sb7 Ca2 Ca5 50.73(4) 5_656 .
Sb4 Ca2 Ca5 125.74(6) 2_564 .
Sb4 Ca2 Ca5 125.74(6) 2_554 .
Sb2 Ca2 Ca5 53.49(6) . .
Sb8 Ca2 Ca5 109.73(8) 1_455 .
Mn1 Ca2 Ca5 137.53(9) 6_556 .
Mn4 Ca2 Ca5 83.07(8) 5_566 .
Mn4 Ca2 Ca5 83.07(8) 5_556 .
Sb8 Ca3 Sb8 93.64(8) 5_666 5_656
Sb8 Ca3 Sb4 106.39(7) 5_666 6_557
Sb8 Ca3 Sb4 106.39(7) 5_656 6_557
Sb8 Ca3 Sb6 83.68(3) 5_666 5_666
Sb8 Ca3 Sb6 158.65(10) 5_656 5_666
Sb4 Ca3 Sb6 94.64(6) 6_557 5_666
Sb8 Ca3 Sb6 158.65(10) 5_666 5_656
Sb8 Ca3 Sb6 83.68(3) 5_656 5_656
Sb4 Ca3 Sb6 94.64(6) 6_557 5_656
Sb6 Ca3 Sb6 91.14(7) 5_666 5_656
Sb8 Ca3 Mn2 51.12(4) 5_666 5_666
Sb8 Ca3 Mn2 111.62(9) 5_656 5_666
Sb4 Ca3 Mn2 136.11(4) 6_557 5_666
Sb6 Ca3 Mn2 51.07(4) 5_666 5_666
Sb6 Ca3 Mn2 110.32(9) 5_656 5_666
Sb8 Ca3 Mn2 111.62(9) 5_666 5_656
Sb8 Ca3 Mn2 51.12(4) 5_656 5_656
Sb4 Ca3 Mn2 136.11(4) 6_557 5_656
Sb6 Ca3 Mn2 110.32(9) 5_666 5_656
Sb6 Ca3 Mn2 51.07(4) 5_656 5_656
Mn2 Ca3 Mn2 86.16(8) 5_666 5_656
Sb8 Ca3 Mn4 50.08(5) 5_666 .
Sb8 Ca3 Mn4 50.08(5) 5_656 .
Sb4 Ca3 Mn4 94.02(10) 6_557 .
Sb6 Ca3 Mn4 133.47(4) 5_666 .
Sb6 Ca3 Mn4 133.47(4) 5_656 .
Mn2 Ca3 Mn4 93.87(8) 5_666 .
Mn2 Ca3 Mn4 93.87(8) 5_656 .
Sb8 Ca3 Ca6 132.93(4) 5_666 .
Sb8 Ca3 Ca6 132.93(4) 5_656 .
Sb4 Ca3 Ca6 60.09(7) 6_557 .
Sb6 Ca3 Ca6 55.78(5) 5_666 .
Sb6 Ca3 Ca6 55.78(5) 5_656 .
Mn2 Ca3 Ca6 104.88(8) 5_666 .
Mn2 Ca3 Ca6 104.88(8) 5_656 .
Mn4 Ca3 Ca6 154.11(12) . .
Sb8 Ca3 Ca7 110.52(7) 5_666 .
Sb8 Ca3 Ca7 110.52(7) 5_656 .
Sb4 Ca3 Ca7 124.83(9) 6_557 .
Sb6 Ca3 Ca7 51.91(4) 5_666 .
Sb6 Ca3 Ca7 51.91(5) 5_656 .
Mn2 Ca3 Ca7 59.42(6) 5_666 .
Mn2 Ca3 Ca7 59.42(6) 5_656 .
Mn4 Ca3 Ca7 141.15(11) . .
Ca6 Ca3 Ca7 64.74(8) . .
Sb8 Ca3 Ca2 54.62(5) 5_666 5_566
Sb8 Ca3 Ca2 104.72(8) 5_656 5_566
Sb4 Ca3 Ca2 51.83(5) 6_557 5_566
Sb6 Ca3 Ca2 91.02(4) 5_666 5_566
Sb6 Ca3 Ca2 146.46(9) 5_656 5_566
Mn2 Ca3 Ca2 96.84(4) 5_666 5_566
Mn2 Ca3 Ca2 154.09(9) 5_656 5_566
Mn4 Ca3 Ca2 60.29(7) . 5_566
Ca6 Ca3 Ca2 99.21(8) . 5_566
Ca7 Ca3 Ca2 142.79(4) . 5_566
Sb8 Ca3 Ca2 104.72(8) 5_666 5_556
Sb8 Ca3 Ca2 54.62(5) 5_656 5_556
Sb4 Ca3 Ca2 51.83(5) 6_557 5_556
Sb6 Ca3 Ca2 146.46(9) 5_666 5_556
Sb6 Ca3 Ca2 91.02(4) 5_656 5_556
Mn2 Ca3 Ca2 154.09(9) 5_666 5_556
Mn2 Ca3 Ca2 96.84(4) 5_656 5_556
Mn4 Ca3 Ca2 60.29(7) . 5_556
Ca6 Ca3 Ca2 99.21(8) . 5_556
Ca7 Ca3 Ca2 142.79(4) . 5_556
Ca2 Ca3 Ca2 69.67(7) 5_566 5_556
Mn4 Ca4 Mn6A 118.75(17) . .
Mn4 Ca4 Sb9B 63.97(10) . .
Mn6A Ca4 Sb9B 54.78(14) . .
Mn4 Ca4 Sb3 120.34(12) . .
Mn6A Ca4 Sb3 120.91(16) . .
Sb9B Ca4 Sb3 175.69(12) . .
Mn4 Ca4 Sb9A 52.68(9) . .
Mn6A Ca4 Sb9A 66.07(14) . .
Sb9B Ca4 Sb9A 11.29(4) . .
Sb3 Ca4 Sb9A 173.03(12) . .
Mn4 Ca4 Sb8 52.51(6) . 5_666
Mn6A Ca4 Sb8 128.39(8) . 5_666
Sb9B Ca4 Sb8 93.98(8) . 5_666
Sb3 Ca4 Sb8 89.10(6) . 5_666
Sb9A Ca4 Sb8 85.92(7) . 5_666
Mn4 Ca4 Sb8 52.51(6) . 5_656
Mn6A Ca4 Sb8 128.39(8) . 5_656
Sb9B Ca4 Sb8 93.98(8) . 5_656
Sb3 Ca4 Sb8 89.10(6) . 5_656
Sb9A Ca4 Sb8 85.92(7) . 5_656
Sb8 Ca4 Sb8 88.78(8) 5_666 5_656
Mn4 Ca4 Sb5 128.08(7) . 5_666
Mn6A Ca4 Sb5 50.26(7) . 5_666
Sb9B Ca4 Sb5 85.38(7) . 5_666
Sb3 Ca4 Sb5 91.48(7) . 5_666
Sb9A Ca4 Sb5 93.61(7) . 5_666
Sb8 Ca4 Sb5 92.508(19) 5_666 5_666
Sb8 Ca4 Sb5 178.59(8) 5_656 5_666
Mn4 Ca4 Sb5 128.08(7) . 5_656
Mn6A Ca4 Sb5 50.26(7) . 5_656
Sb9B Ca4 Sb5 85.38(7) . 5_656
Sb3 Ca4 Sb5 91.48(7) . 5_656
Sb9A Ca4 Sb5 93.61(7) . 5_656
Sb8 Ca4 Sb5 178.59(8) 5_666 5_656
Sb8 Ca4 Sb5 92.507(19) 5_656 5_656
Sb5 Ca4 Sb5 86.20(8) 5_666 5_656
Mn4 Ca4 Ca8 173.50(13) . .
Mn6A Ca4 Ca8 67.75(15) . .
Sb9B Ca4 Ca8 122.53(12) . .
Sb3 Ca4 Ca8 53.16(7) . .
Sb9A Ca4 Ca8 133.81(11) . .
Sb8 Ca4 Ca8 124.22(6) 5_666 .
Sb8 Ca4 Ca8 124.22(6) 5_656 .
Sb5 Ca4 Ca8 55.35(5) 5_666 .
Sb5 Ca4 Ca8 55.35(5) 5_656 .
Mn4 Ca4 Ca3 55.79(9) . .
Mn6A Ca4 Ca3 174.54(16) . .
Sb9B Ca4 Ca3 119.76(11) . .
Sb3 Ca4 Ca3 64.55(7) . .
Sb9A Ca4 Ca3 108.47(10) . .
Sb8 Ca4 Ca3 49.32(5) 5_666 .
Sb8 Ca4 Ca3 49.32(5) 5_656 .
Sb5 Ca4 Ca3 132.07(5) 5_666 .
Sb5 Ca4 Ca3 132.07(5) 5_656 .
Ca8 Ca4 Ca3 117.71(10) . .
Mn4 Ca4 Ca1 35.91(7) . 3_556
Mn6A Ca4 Ca1 93.48(14) . 3_556
Sb9B Ca4 Ca1 46.17(8) . 3_556
Sb3 Ca4 Ca1 137.13(9) . 3_556
Sb9A Ca4 Ca1 37.88(7) . 3_556
Sb8 Ca4 Ca1 48.09(6) 5_666 3_556
Sb8 Ca4 Ca1 87.87(9) 5_656 3_556
Sb5 Ca4 Ca1 92.57(7) 5_666 3_556
Sb5 Ca4 Ca1 131.37(9) 5_656 3_556
Ca8 Ca4 Ca1 147.91(8) . 3_556
Ca3 Ca4 Ca1 81.65(8) . 3_556
Sb7 Ca5 Sb7 92.45(7) 5_666 5_656
Sb7 Ca5 Sb3 89.91(2) 5_666 5_666
Sb7 Ca5 Sb3 177.65(7) 5_656 5_666
Sb7 Ca5 Sb3 177.65(7) 5_666 5_656
Sb7 Ca5 Sb3 89.91(2) 5_656 5_656
Sb3 Ca5 Sb3 87.74(7) 5_666 5_656
Sb7 Ca5 Sb1 86.06(6) 5_666 .
Sb7 Ca5 Sb1 86.06(6) 5_656 .
Sb3 Ca5 Sb1 94.15(6) 5_666 .
Sb3 Ca5 Sb1 94.15(6) 5_656 .
Sb7 Ca5 Sb2 82.54(6) 5_666 .
Sb7 Ca5 Sb2 82.54(6) 5_656 .
Sb3 Ca5 Sb2 97.73(6) 5_666 .
Sb3 Ca5 Sb2 97.73(6) 5_656 .
Sb1 Ca5 Sb2 163.48(9) . .
Sb7 Ca5 Mn2 131.74(4) 5_666 .
Sb7 Ca5 Mn2 131.74(4) 5_656 .
Sb3 Ca5 Mn2 46.06(4) 5_666 .
Sb3 Ca5 Mn2 46.06(4) 5_656 .
Sb1 Ca5 Mn2 111.49(8) . .
Sb2 Ca5 Mn2 85.02(7) . .
Sb7 Ca5 Mn3 40.36(7) 5_666 5_666
Sb7 Ca5 Mn3 96.79(9) 5_656 5_666
Sb3 Ca5 Mn3 84.97(6) 5_666 5_666
Sb3 Ca5 Mn3 139.23(10) 5_656 5_666
Sb1 Ca5 Mn3 126.34(8) . 5_666
Sb2 Ca5 Mn3 44.13(6) . 5_666
Mn2 Ca5 Mn3 105.84(9) . 5_666
Sb7 Ca5 Mn3 96.79(9) 5_666 5_656
Sb7 Ca5 Mn3 40.36(7) 5_656 5_656
Sb3 Ca5 Mn3 139.23(10) 5_666 5_656
Sb3 Ca5 Mn3 84.97(6) 5_656 5_656
Sb1 Ca5 Mn3 126.34(8) . 5_656
Sb2 Ca5 Mn3 44.13(6) . 5_656
Mn2 Ca5 Mn3 105.84(9) . 5_656
Mn3 Ca5 Mn3 75.12(10) 5_666 5_656
Sb7 Ca5 Mn5 42.39(6) 5_666 5_666
Sb7 Ca5 Mn5 97.76(8) 5_656 5_666
Sb3 Ca5 Mn5 84.02(5) 5_666 5_666
Sb3 Ca5 Mn5 137.24(9) 5_656 5_666
Sb1 Ca5 Mn5 45.07(5) . 5_666
Sb2 Ca5 Mn5 124.93(7) . 5_666
Mn2 Ca5 Mn5 126.94(7) . 5_666
Mn3 Ca5 Mn5 81.72(8) 5_666 5_666
Mn3 Ca5 Mn5 126.40(11) 5_656 5_666
Sb7 Ca5 Mn5 97.76(8) 5_666 5_656
Sb7 Ca5 Mn5 42.39(6) 5_656 5_656
Sb3 Ca5 Mn5 137.24(9) 5_666 5_656
Sb3 Ca5 Mn5 84.01(5) 5_656 5_656
Sb1 Ca5 Mn5 45.07(5) . 5_656
Sb2 Ca5 Mn5 124.93(7) . 5_656
Mn2 Ca5 Mn5 126.94(7) . 5_656
Mn3 Ca5 Mn5 126.40(11) 5_666 5_656
Mn3 Ca5 Mn5 81.72(8) 5_656 5_656
Mn5 Ca5 Mn5 74.45(8) 5_666 5_656
Sb7 Ca5 Ca2 51.62(4) 5_666 .
Sb7 Ca5 Ca2 51.62(4) 5_656 .
Sb3 Ca5 Ca2 130.29(5) 5_666 .
Sb3 Ca5 Ca2 130.29(5) 5_656 .
Sb1 Ca5 Ca2 110.48(8) . .
Sb2 Ca5 Ca2 53.00(6) . .
Mn2 Ca5 Ca2 138.03(9) . .
Mn3 Ca5 Ca2 45.52(7) 5_666 .
Mn3 Ca5 Ca2 45.52(7) 5_656 .
Mn5 Ca5 Ca2 84.41(8) 5_666 .
Mn5 Ca5 Ca2 84.41(8) 5_656 .
Mn3 Ca6 Sb2 52.79(7) 6_557 2_565
Mn3 Ca6 Sb2 52.79(7) 6_557 2
Sb2 Ca6 Sb2 91.07(8) 2_565 2
Mn3 Ca6 Sb6 128.46(8) 6_557 5_666
Sb2 Ca6 Sb6 89.09(2) 2_565 5_666
Sb2 Ca6 Sb6 178.20(13) 2 5_666
Mn3 Ca6 Sb6 128.45(8) 6_557 5_656
Sb2 Ca6 Sb6 178.20(13) 2_565 5_656
Sb2 Ca6 Sb6 89.09(2) 2 5_656
Sb6 Ca6 Sb6 90.69(8) 5_666 5_656
Mn3 Ca6 Sb4 64.34(12) 6_557 .
Sb2 Ca6 Sb4 93.26(8) 2_565 .
Sb2 Ca6 Sb4 93.26(8) 2 .
Sb6 Ca6 Sb4 88.52(7) 5_666 .
Sb6 Ca6 Sb4 88.52(7) 5_656 .
Mn3 Ca6 Sb4 118.19(13) 6_557 6_557
Sb2 Ca6 Sb4 88.51(7) 2_565 6_557
Sb2 Ca6 Sb4 88.51(7) 2 6_557
Sb6 Ca6 Sb4 89.71(8) 5_666 6_557
Sb6 Ca6 Sb4 89.71(8) 5_656 6_557
Sb4 Ca6 Sb4 177.47(10) . 6_557
Mn3 Ca6 Ca3 171.56(15) 6_557 .
Sb2 Ca6 Ca3 123.11(8) 2_565 .
Sb2 Ca6 Ca3 123.11(8) 2 .
Sb6 Ca6 Ca3 55.45(6) 5_666 .
Sb6 Ca6 Ca3 55.45(6) 5_656 .
Sb4 Ca6 Ca3 124.10(10) . .
Sb4 Ca6 Ca3 53.37(7) 6_557 .
Mn3 Ca6 Ca7 55.62(12) 6_557 6_557
Sb2 Ca6 Ca7 50.71(4) 2_565 6_557
Sb2 Ca6 Ca7 50.71(4) 2 6_557
Sb6 Ca6 Ca7 128.42(6) 5_666 6_557
Sb6 Ca6 Ca7 128.42(6) 5_656 6_557
Sb4 Ca6 Ca7 119.96(10) . 6_557
Sb4 Ca6 Ca7 62.56(6) 6_557 6_557
Ca3 Ca6 Ca7 115.94(11) . 6_557
Mn3 Ca6 Ca7 127.13(15) 6_557 .
Sb2 Ca6 Ca7 130.31(5) 2_565 .
Sb2 Ca6 Ca7 130.31(5) 2 .
Sb6 Ca6 Ca7 50.47(4) 5_666 .
Sb6 Ca6 Ca7 50.47(4) 5_656 .
Sb4 Ca6 Ca7 62.79(6) . .
Sb4 Ca6 Ca7 114.68(10) 6_557 .
Ca3 Ca6 Ca7 61.30(7) . .
Ca7 Ca6 Ca7 177.24(11) 6_557 .
Sb3 Ca7 Sb2 105.49(6) . 5_666
Sb3 Ca7 Sb2 105.49(6) . 5_656
Sb2 Ca7 Sb2 92.96(7) 5_666 5_656
Sb3 Ca7 Sb6 93.58(6) . 5_666
Sb2 Ca7 Sb6 84.51(3) 5_666 5_666
Sb2 Ca7 Sb6 160.72(9) 5_656 5_666
Sb3 Ca7 Sb6 93.58(6) . 5_656
Sb2 Ca7 Sb6 160.72(9) 5_666 5_656
Sb2 Ca7 Sb6 84.51(3) 5_656 5_656
Sb6 Ca7 Sb6 91.58(7) 5_666 5_656
Sb3 Ca7 Mn1 135.57(4) . 5_666
Sb2 Ca7 Mn1 51.61(4) 5_666 5_666
Sb2 Ca7 Mn1 112.41(8) 5_656 5_666
Sb6 Ca7 Mn1 51.87(4) 5_666 5_666
Sb6 Ca7 Mn1 111.92(8) 5_656 5_666
Sb3 Ca7 Mn1 135.57(4) . 5_656
Sb2 Ca7 Mn1 112.41(8) 5_666 5_656
Sb2 Ca7 Mn1 51.61(4) 5_656 5_656
Sb6 Ca7 Mn1 111.92(8) 5_666 5_656
Sb6 Ca7 Mn1 51.87(4) 5_656 5_656
Mn1 Ca7 Mn1 87.43(8) 5_666 5_656
Sb3 Ca7 Mn3 95.11(10) . .
Sb2 Ca7 Mn3 49.01(4) 5_666 .
Sb2 Ca7 Mn3 49.01(4) 5_656 .
Sb6 Ca7 Mn3 133.33(4) 5_666 .
Sb6 Ca7 Mn3 133.33(4) 5_656 .
Mn1 Ca7 Mn3 92.73(9) 5_666 .
Mn1 Ca7 Mn3 92.73(9) 5_656 .
Sb3 Ca7 Mn2 46.83(4) . 5_666
Sb2 Ca7 Mn2 87.89(4) 5_666 5_666
Sb2 Ca7 Mn2 150.88(9) 5_656 5_666
Sb6 Ca7 Mn2 48.31(4) 5_666 5_666
Sb6 Ca7 Mn2 103.58(7) 5_656 5_666
Mn1 Ca7 Mn2 90.77(4) 5_666 5_666
Mn1 Ca7 Mn2 151.76(9) 5_656 5_666
Mn3 Ca7 Mn2 115.52(9) . 5_666
Sb3 Ca7 Mn2 46.83(4) . 5_656
Sb2 Ca7 Mn2 150.88(9) 5_666 5_656
Sb2 Ca7 Mn2 87.89(4) 5_656 5_656
Sb6 Ca7 Mn2 103.58(7) 5_666 5_656
Sb6 Ca7 Mn2 48.31(4) 5_656 5_656
Mn1 Ca7 Mn2 151.76(9) 5_666 5_656
Mn1 Ca7 Mn2 90.77(4) 5_656 5_656
Mn3 Ca7 Mn2 115.52(9) . 5_656
Mn2 Ca7 Mn2 77.76(6) 5_666 5_656
Sb3 Ca7 Ca3 66.70(6) . .
Sb2 Ca7 Ca3 133.52(4) 5_666 .
Sb2 Ca7 Ca3 133.52(4) 5_656 .
Sb6 Ca7 Ca3 52.18(4) 5_666 .
Sb6 Ca7 Ca3 52.18(4) 5_656 .
Mn1 Ca7 Ca3 100.37(7) 5_666 .
Mn1 Ca7 Ca3 100.37(7) 5_656 .
Mn3 Ca7 Ca3 161.81(12) . .
Mn2 Ca7 Ca3 52.29(5) 5_666 .
Mn2 Ca7 Ca3 52.29(5) 5_656 .
Sb3 Ca7 Ca6 139.04(10) . 6_657
Sb2 Ca7 Ca6 51.85(4) 5_666 6_657
Sb2 Ca7 Ca6 51.85(4) 5_656 6_657
Sb6 Ca7 Ca6 114.09(6) 5_666 6_657
Sb6 Ca7 Ca6 114.09(6) 5_656 6_657
Mn1 Ca7 Ca6 62.21(6) 5_666 6_657
Mn1 Ca7 Ca6 62.21(6) 5_656 6_657
Mn3 Ca7 Ca6 43.94(10) . 6_657
Mn2 Ca7 Ca6 139.47(4) 5_666 6_657
Mn2 Ca7 Ca6 139.47(4) 5_656 6_657
Ca3 Ca7 Ca6 154.26(10) . 6_657
Mn6B Ca8 Mn6B 93.67(12) 5_666 5_656
Mn6B Ca8 Sb3 132.77(6) 5_666 .
Mn6B Ca8 Sb3 132.77(6) 5_656 .
Mn6B Ca8 Sb1 52.57(6) 5_666 5_666
Mn6B Ca8 Sb1 117.04(11) 5_656 5_666
Sb3 Ca8 Sb1 101.12(8) . 5_666
Mn6B Ca8 Sb1 117.04(11) 5_666 5_656
Mn6B Ca8 Sb1 52.57(6) 5_656 5_656
Sb3 Ca8 Sb1 101.12(8) . 5_656
Sb1 Ca8 Sb1 93.49(9) 5_666 5_656
Mn6B Ca8 Mn6B 64.75(9) 5_666 .
Mn6B Ca8 Mn6B 64.75(9) 5_656 .
Sb3 Ca8 Mn6B 121.63(11) . .
Sb1 Ca8 Mn6B 117.31(8) 5_666 .
Sb1 Ca8 Mn6B 117.31(8) 5_656 .
Mn6B Ca8 Sb5 52.47(6) 5_666 5_666
Mn6B Ca8 Sb5 113.69(11) 5_656 5_666
Sb3 Ca8 Sb5 93.75(7) . 5_666
Sb1 Ca8 Sb5 87.41(3) 5_666 5_666
Sb1 Ca8 Sb5 164.63(11) 5_656 5_666
Mn6B Ca8 Sb5 49.79(5) . 5_666
Mn6B Ca8 Sb5 113.69(11) 5_666 5_656
Mn6B Ca8 Sb5 52.47(6) 5_656 5_656
Sb3 Ca8 Sb5 93.75(7) . 5_656
Sb1 Ca8 Sb5 164.63(11) 5_666 5_656
Sb1 Ca8 Sb5 87.41(3) 5_656 5_656
Mn6B Ca8 Sb5 49.79(5) . 5_656
Sb5 Ca8 Sb5 87.74(8) 5_666 5_656
Mn6B Ca8 Mn5 93.92(9) 5_666 .
Mn6B Ca8 Mn5 93.92(9) 5_656 .
Sb3 Ca8 Mn5 91.20(10) . .
Sb1 Ca8 Mn5 48.59(5) 5_666 .
Sb1 Ca8 Mn5 48.59(5) 5_656 .
Mn6B Ca8 Mn5 147.17(13) . .
Sb5 Ca8 Mn5 135.76(4) 5_666 .
Sb5 Ca8 Mn5 135.76(4) 5_656 .
Mn6B Ca8 Sb5 46.89(6) 5_666 .
Mn6B Ca8 Sb5 46.89(6) 5_656 .
Sb3 Ca8 Sb5 170.47(11) . .
Sb1 Ca8 Sb5 85.34(7) 5_666 .
Sb1 Ca8 Sb5 85.34(7) 5_656 .
Mn6B Ca8 Sb5 48.84(7) . .
Sb5 Ca8 Sb5 79.44(7) 5_666 .
Sb5 Ca8 Sb5 79.44(7) 5_656 .
Mn5 Ca8 Sb5 98.33(9) . .
Mn6B Ca8 Ca4 108.73(9) 5_666 .
Mn6B Ca8 Ca4 108.73(9) 5_656 .
Sb3 Ca8 Ca4 55.06(7) . .
Sb1 Ca8 Ca4 130.50(5) 5_666 .
Sb1 Ca8 Ca4 130.50(5) 5_656 .
Mn6B Ca8 Ca4 66.57(9) . .
Sb5 Ca8 Ca4 56.56(5) 5_666 .
Sb5 Ca8 Ca4 56.56(5) 5_656 .
Mn5 Ca8 Ca4 146.27(12) . .
Sb5 Ca8 Ca4 115.41(10) . .
Mn6B Ca8 Mn6A 18.58(10) 5_666 5_666
Mn6B Ca8 Mn6A 86.23(10) 5_656 5_666
Sb3 Ca8 Mn6A 140.42(8) . 5_666
Sb1 Ca8 Mn6A 43.86(9) 5_666 5_666
Sb1 Ca8 Mn6A 99.20(11) 5_656 5_666
Mn6B Ca8 Mn6A 76.50(12) . 5_666
Sb5 Ca8 Mn6A 71.01(9) 5_666 5_666
Sb5 Ca8 Mn6A 120.85(13) 5_656 5_666
Mn5 Ca8 Mn6A 77.48(12) . 5_666
Sb5 Ca8 Mn6A 43.38(8) . 5_666
Ca4 Ca8 Mn6A 127.29(11) . 5_666
Sb9B Ca9 Sb9B 105.09(15) 5_666 5_656
Sb9B Ca9 Mn6A 58.79(13) 5_666 5_666
Sb9B Ca9 Mn6A 134.69(19) 5_656 5_666
Sb9B Ca9 Mn6A 134.69(19) 5_666 5_656
Sb9B Ca9 Mn6A 58.79(13) 5_656 5_656
Mn6A Ca9 Mn6A 100.6(2) 5_666 5_656
Sb9B Ca9 Mn5 122.72(9) 5_666 .
Sb9B Ca9 Mn5 122.72(9) 5_656 .
Mn6A Ca9 Mn5 98.57(15) 5_666 .
Mn6A Ca9 Mn5 98.57(15) 5_656 .
Sb9B Ca9 Sb9A 96.34(11) 5_666 1_655
Sb9B Ca9 Sb9A 96.34(11) 5_656 1_655
Mn6A Ca9 Sb9A 125.62(13) 5_666 1_655
Mn6A Ca9 Sb9A 125.62(12) 5_656 1_655
Mn5 Ca9 Sb9A 52.27(10) . 1_655
Sb9B Ca9 Sb9A 8.91(4) 5_666 5_666
Sb9B Ca9 Sb9A 96.53(12) 5_656 5_666
Mn6A Ca9 Sb9A 66.57(12) 5_666 5_666
Mn6A Ca9 Sb9A 132.08(18) 5_656 5_666
Mn5 Ca9 Sb9A 128.25(9) . 5_666
Sb9A Ca9 Sb9A 95.05(10) 1_655 5_666
Sb9B Ca9 Sb9A 96.53(12) 5_666 5_656
Sb9B Ca9 Sb9A 8.91(4) 5_656 5_656
Mn6A Ca9 Sb9A 132.08(18) 5_666 5_656
Mn6A Ca9 Sb9A 66.57(12) 5_656 5_656
Mn5 Ca9 Sb9A 128.25(9) . 5_656
Sb9A Ca9 Sb9A 95.05(10) 1_655 5_656
Sb9A Ca9 Sb9A 87.88(10) 5_666 5_656
Sb9B Ca9 Sb5 90.61(11) 5_666 .
Sb9B Ca9 Sb5 90.61(11) 5_656 .
Mn6A Ca9 Sb5 51.47(12) 5_666 .
Mn6A Ca9 Sb5 51.47(11) 5_656 .
Mn5 Ca9 Sb5 116.27(13) . .
Sb9A Ca9 Sb5 168.53(13) 1_655 .
Sb9A Ca9 Sb5 93.20(9) 5_666 .
Sb9A Ca9 Sb5 93.20(9) 5_656 .
Sb9B Ca9 Sb9B 89.66(11) 5_666 1_655
Sb9B Ca9 Sb9B 89.66(11) 5_656 1_655
Mn6A Ca9 Sb9B 128.45(12) 5_666 1_655
Mn6A Ca9 Sb9B 128.45(12) 5_656 1_655
Mn5 Ca9 Sb9B 63.30(11) . 1_655
Sb9A Ca9 Sb9B 11.03(4) 1_655 1_655
Sb9A Ca9 Sb9B 87.11(9) 5_666 1_655
Sb9A Ca9 Sb9B 87.11(9) 5_656 1_655
Sb5 Ca9 Sb9B 179.56(13) . 1_655
Sb9B Ca9 Sb1 84.62(5) 5_666 5_666
Sb9B Ca9 Sb1 170.09(11) 5_656 5_666
Mn6A Ca9 Sb1 49.00(12) 5_666 5_666
Mn6A Ca9 Sb1 112.93(16) 5_656 5_666
Mn5 Ca9 Sb1 50.55(6) . 5_666
Sb9A Ca9 Sb1 84.34(9) 1_655 5_666
Sb9A Ca9 Sb1 93.25(3) 5_666 5_666
Sb9A Ca9 Sb1 178.75(10) 5_656 5_666
Sb5 Ca9 Sb1 87.26(8) . 5_666
Sb9B Ca9 Sb1 92.42(9) 1_655 5_666
Sb9B Ca9 Sb1 170.09(11) 5_666 5_656
Sb9B Ca9 Sb1 84.62(5) 5_656 5_656
Mn6A Ca9 Sb1 112.93(16) 5_666 5_656
Mn6A Ca9 Sb1 49.00(12) 5_656 5_656
Mn5 Ca9 Sb1 50.55(6) . 5_656
Sb9A Ca9 Sb1 84.33(9) 1_655 5_656
Sb9A Ca9 Sb1 178.75(10) 5_666 5_656
Sb9A Ca9 Sb1 93.25(3) 5_656 5_656
Sb5 Ca9 Sb1 87.26(8) . 5_656
Sb9B Ca9 Sb1 92.42(9) 1_655 5_656
Sb1 Ca9 Sb1 85.61(8) 5_666 5_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 Mn6A 2.680(6) .
Sb1 Mn5 2.782(2) 5_666
Sb1 Mn5 2.782(2) 5_656
Sb1 Mn6B 2.807(3) .
Sb1 Ca8 3.172(2) 5_666
Sb1 Ca8 3.172(2) 5_656
Sb1 Ca1 3.250(4) 7_565
Sb1 Ca1 3.250(4) .
Sb1 Ca5 3.353(3) .
Sb1 Ca9 3.400(3) 5_666
Sb1 Ca9 3.400(3) 5_656
Sb2 Mn3 2.721(3) 5_666
Sb2 Mn3 2.721(3) 5_656
Sb2 Mn1 2.846(2) .
Sb2 Ca7 3.1859(19) 5_666
Sb2 Ca7 3.1860(19) 5_656
Sb2 Ca6 3.237(2) 2_564
Sb2 Ca6 3.237(2) 2_554
Sb2 Ca2 3.363(3) .
Sb2 Ca5 3.384(3) .
Sb3 Mn2 2.7624(12) 5_666
Sb3 Mn2 2.7624(12) 5_656
Sb3 Ca8 3.168(3) .
Sb3 Ca7 3.171(3) .
Sb3 Ca4 3.245(3) .
Sb3 Ca5 3.334(2) 5_666
Sb3 Ca5 3.334(2) 5_656
Sb4 Mn1 2.7539(12) 5_666
Sb4 Mn1 2.7540(12) 5_656
Sb4 Ca3 3.203(3) 6_657
Sb4 Ca2 3.257(2) 2_565
Sb4 Ca2 3.257(2) 2
Sb4 Ca6 3.299(4) .
Sb4 Ca6 3.459(4) 6_657
Sb5 Mn6B 2.7598(17) 5_666
Sb5 Mn6B 2.7599(17) 5_656
Sb5 Mn6A 2.772(4) 5_666
Sb5 Mn6A 2.772(4) 5_656
Sb5 Mn6B 2.877(3) .
Sb5 Ca8 3.334(2) 5_666
Sb5 Ca8 3.334(2) 5_656
Sb5 Ca9 3.343(4) .
Sb5 Ca4 3.381(2) 5_666
Sb5 Ca4 3.381(2) 5_656
Sb5 Ca8 3.671(3) .
Sb6 Mn2 2.856(2) .
Sb6 Mn1 2.874(2) .
Sb6 Ca7 3.223(2) 5_666
Sb6 Ca7 3.223(2) 5_656
Sb6 Ca3 3.235(2) 5_666
Sb6 Ca3 3.235(2) 5_656
Sb6 Ca6 3.248(2) 5_666
Sb6 Ca6 3.248(2) 5_656
Sb7 Mn3 2.474(5) .
Sb7 Mn4 2.566(4) 1_655
Sb7 Mn5 2.603(4) .
Sb7 Ca1 3.193(4) 3_656
Sb7 Ca1 3.193(4) 5_656
Sb7 Ca5 3.200(2) 5_666
Sb7 Ca5 3.200(2) 5_656
Sb7 Ca2 3.240(2) 5_666
Sb7 Ca2 3.240(2) 5_656
Sb7 Ca1 3.719(4) 5_666
Sb7 Ca1 3.719(4) 3_646
Sb8 Mn4 2.822(2) 5_666
Sb8 Mn4 2.822(2) 5_656
Sb8 Mn2 2.833(2) .
Sb8 Ca3 3.168(2) 5_666
Sb8 Ca3 3.168(2) 5_656
Sb8 Ca1 3.198(4) 7_665
Sb8 Ca1 3.198(4) 1_655
Sb8 Ca4 3.303(2) 5_666
Sb8 Ca4 3.303(2) 5_656
Sb8 Ca2 3.400(3) 1_655
Sb9A Sb9B 0.640(2) .
Sb9A Ca1 2.612(4) 3_556
Sb9A Ca1 2.612(4) 5_556
Sb9A Mn5 2.793(4) 1_455
Sb9A Mn4 2.813(4) .
Sb9A Ca1 3.234(4) 5_566
Sb9A Ca1 3.234(4) 3_546
Sb9A Ca9 3.251(5) 1_455
Sb9A Ca4 3.267(3) .
Sb9A Ca9 3.329(3) 5_666
Sb9A Ca9 3.329(3) 5_656
Sb9B Mn6A 2.903(7) .
Sb9B Ca9 2.910(3) 5_666
Sb9B Ca9 2.910(3) 5_656
Sb9B Ca1 3.077(5) 3_556
Sb9B Ca1 3.077(5) 5_556
Sb9B Ca4 3.186(4) .
Sb9B Ca9 3.341(5) 1_455
Sb9B Ca1 3.620(4) 5_566
Sb9B Ca1 3.620(4) 3_546
Mn1 Sb4 2.7540(12) 5_666
Mn1 Sb4 2.7541(12) 5_656
Mn1 Ca7 3.343(2) 5_666
Mn1 Ca7 3.343(2) 5_656
Mn1 Ca2 3.732(3) 6_656
Mn2 Sb3 2.7624(12) 5_666
Mn2 Sb3 2.7624(12) 5_656
Mn2 Ca3 3.382(3) 5_666
Mn2 Ca3 3.382(2) 5_656
Mn2 Ca5 3.680(3) .
Mn2 Ca7 3.681(3) 5_666
Mn2 Ca7 3.681(3) 5_656
Mn3 Sb2 2.721(3) 5_666
Mn3 Sb2 2.721(3) 5_656
Mn3 Ca6 2.827(6) 6_657
Mn3 Ca2 3.037(4) 5_666
Mn3 Ca2 3.037(4) 5_656
Mn3 Ca7 3.363(5) .
Mn3 Ca5 3.790(4) 5_666
Mn3 Ca5 3.790(4) 5_656
Mn4 Ca1 2.523(5) 3_556
Mn4 Ca1 2.523(5) 5_556
Mn4 Sb7 2.566(4) 1_455
Mn4 Sb8 2.822(2) 5_666
Mn4 Sb8 2.822(2) 5_656
Mn4 Ca4 3.058(5) .
Mn4 Ca1 3.163(4) 5_566
Mn4 Ca1 3.163(4) 3_546
Mn4 Mn5 3.205(5) 1_455
Mn4 Ca3 3.469(5) .
Mn4 Ca2 3.806(4) 5_566
Mn5 Ca1 2.584(5) 3_656
Mn5 Ca1 2.584(5) 5_656
Mn5 Sb1 2.782(2) 5_666
Mn5 Sb1 2.782(2) 5_656
Mn5 Sb9A 2.793(4) 1_655
Mn5 Ca9 3.081(5) .
Mn5 Mn4 3.206(5) 1_655
Mn5 Ca1 3.212(5) 5_666
Mn5 Ca1 3.212(4) 3_646
Mn5 Ca8 3.541(5) .
Mn5 Ca5 3.819(3) 5_666
Mn6A Mn6B 1.299(7) .
Mn6A Sb5 2.772(4) 5_666
Mn6A Sb5 2.772(4) 5_656
Mn6A Ca9 3.003(5) 5_666
Mn6A Ca9 3.003(5) 5_656
Mn6A Ca4 3.123(7) .
Mn6A Ca8 3.820(6) 5_666
Mn6A Ca8 3.820(6) 5_656
Mn6B Sb5 2.7599(17) 5_666
Mn6B Sb5 2.7599(17) 5_656
Mn6B Ca8 3.168(3) 5_666
Mn6B Ca8 3.168(3) 5_656
Mn6B Ca8 3.217(4) .
Ca1 Ca1 0.787(8) 7_565
Ca1 Mn4 2.523(5) 5_556
Ca1 Mn5 2.585(5) 5_656
Ca1 Sb9A 2.612(4) 5_556
Ca1 Sb9B 3.077(5) 5_556
Ca1 Mn4 3.163(4) 5_566
Ca1 Sb7 3.193(4) 5_656
Ca1 Sb8 3.198(4) 1_455
Ca1 Mn5 3.212(4) 5_666
Ca1 Sb9A 3.234(4) 5_566
Ca1 Sb9B 3.620(4) 5_566
Ca2 Mn3 3.037(4) 5_666
Ca2 Mn3 3.037(4) 5_656
Ca2 Sb7 3.240(2) 5_666
Ca2 Sb7 3.240(2) 5_656
Ca2 Sb4 3.257(2) 2_564
Ca2 Sb4 3.257(2) 2_554
Ca2 Sb8 3.400(3) 1_455
Ca2 Mn1 3.732(3) 6_556
Ca2 Mn4 3.806(4) 5_566
Ca2 Mn4 3.806(4) 5_556
Ca2 Ca5 4.037(4) .
Ca3 Sb8 3.168(2) 5_666
Ca3 Sb8 3.168(2) 5_656
Ca3 Sb4 3.203(3) 6_557
Ca3 Sb6 3.235(2) 5_666
Ca3 Sb6 3.235(2) 5_656
Ca3 Mn2 3.382(3) 5_666
Ca3 Mn2 3.382(2) 5_656
Ca3 Ca6 3.661(4) .
Ca3 Ca7 3.972(4) .
Ca3 Ca2 4.045(3) 5_566
Ca3 Ca2 4.045(3) 5_556
Ca4 Sb8 3.302(2) 5_666
Ca4 Sb8 3.303(2) 5_656
Ca4 Sb5 3.381(2) 5_666
Ca4 Sb5 3.381(2) 5_656
Ca4 Ca8 3.760(4) .
Ca4 Ca1 4.251(5) 3_556
Ca5 Sb7 3.200(2) 5_666
Ca5 Sb7 3.200(2) 5_656
Ca5 Sb3 3.334(2) 5_666
Ca5 Sb3 3.334(2) 5_656
Ca5 Mn3 3.790(4) 5_666
Ca5 Mn3 3.790(4) 5_656
Ca5 Mn5 3.819(3) 5_666
Ca5 Mn5 3.819(3) 5_656
Ca6 Mn3 2.827(6) 6_557
Ca6 Sb2 3.237(2) 2_565
Ca6 Sb2 3.237(2) 2
Ca6 Sb6 3.248(2) 5_666
Ca6 Sb6 3.248(2) 5_656
Ca6 Sb4 3.460(4) 6_557
Ca6 Ca7 4.018(4) 6_557
Ca6 Ca7 4.096(4) .
Ca7 Sb2 3.1860(19) 5_666
Ca7 Sb2 3.1860(19) 5_656
Ca7 Sb6 3.223(2) 5_666
Ca7 Sb6 3.223(2) 5_656
Ca7 Mn1 3.343(2) 5_666
Ca7 Mn1 3.343(2) 5_656
Ca7 Mn2 3.681(3) 5_666
Ca7 Mn2 3.681(3) 5_656
Ca7 Ca6 4.018(4) 6_657
Ca8 Mn6B 3.167(3) 5_666
Ca8 Mn6B 3.167(3) 5_656
Ca8 Sb1 3.172(2) 5_666
Ca8 Sb1 3.172(2) 5_656
Ca8 Sb5 3.334(2) 5_666
Ca8 Sb5 3.334(2) 5_656
Ca8 Mn6A 3.820(6) 5_666
Ca9 Sb9B 2.910(3) 5_666
Ca9 Sb9B 2.910(3) 5_656
Ca9 Mn6A 3.003(5) 5_666
Ca9 Mn6A 3.003(5) 5_656
Ca9 Sb9A 3.251(5) 1_655
Ca9 Sb9A 3.329(3) 5_666
Ca9 Sb9A 3.329(3) 5_656
Ca9 Sb9B 3.341(5) 1_655
Ca9 Sb1 3.400(3) 5_666
Ca9 Sb1 3.400(3) 5_656
