#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:59:59 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179520 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/17/4341709.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4341709
loop_
_publ_author_name
'Liu, Xiao-Cun'
'Wu, Zhen'
'Xia, Sheng-Qing'
'Tao, Xu-Tang'
'Bobev, Svilen'
_publ_section_title
;
 Structural Variability versus Structural Flexibility. A Case Study of
 Eu9Cd4+xSb9 and Ca9Mn4+xSb9 (x ≈ (1)/2).
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              947
_journal_page_last               955
_journal_paper_doi               10.1021/ic5023505
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Ca9 Mn4.43 Sb9'
_chemical_formula_weight         1699.58
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.4668(16)
_cell_length_b                   4.6177(6)
_cell_length_c                   44.110(6)
_cell_measurement_reflns_used    5110
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      28.18
_cell_measurement_theta_min      2.83
_cell_volume                     2539.3(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0530
_diffrn_reflns_av_sigmaI/netI    0.0283
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       55
_diffrn_reflns_limit_l_min       -55
_diffrn_reflns_number            26576
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.70
_exptl_absorpt_coefficient_mu    13.319
_exptl_absorpt_correction_T_max  0.7765
_exptl_absorpt_correction_T_min  0.2571
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.446
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             2999
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_refine_diff_density_max         8.329
_refine_diff_density_min         -2.145
_refine_diff_density_rms         0.331
_refine_ls_extinction_coef       0.000043(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.114
_refine_ls_matrix_type           full
_refine_ls_number_parameters     153
_refine_ls_number_reflns         2940
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.114
_refine_ls_R_factor_all          0.0432
_refine_ls_R_factor_gt           0.0362
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0230P)²+49.2919P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0769
_refine_ls_wR_factor_ref         0.0810
_reflns_number_gt                2572
_reflns_number_total             2940
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5023505_si_003.cif
_cod_data_source_block           IV
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341703--4341709.cif.
;
_cod_original_cell_volume        2539.4(6)
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341709
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sb1 Sb 0.25079(6) 0.2500 0.449519(16) 0.01251(17) Uani 1 2 d S
Sb2 Sb 0.27498(6) 0.2500 0.298355(16) 0.00946(16) Uani 1 2 d S
Sb3 Sb 0.50643(6) 0.2500 0.620252(16) 0.01121(17) Uani 1 2 d S
Sb4 Sb 0.55196(7) 0.2500 0.779787(18) 0.01814(19) Uani 1 2 d S
Sb5 Sb 0.60601(6) 0.2500 0.468301(17) 0.01230(17) Uani 1 2 d S
Sb6 Sb 0.62060(6) 0.2500 0.295230(16) 0.00942(16) Uani 1 2 d S
Sb7 Sb 0.87554(7) 0.2500 0.629729(18) 0.01599(18) Uani 1 2 d S
Sb8 Sb 0.81232(6) 0.2500 0.375489(17) 0.01252(17) Uani 1 2 d S
Sb9A Sb 0.05552(13) 0.2500 0.54587(4) 0.0128(3) Uani 0.579(2) 2 d SP
Sb9B Sb 0.08896(19) 0.2500 0.53479(5) 0.0128(3) Uani 0.421(2) 2 d SP
Mn1 Mn 0.44131(14) 0.2500 0.25424(4) 0.0112(3) Uani 1 2 d S
Mn2 Mn 0.59200(13) 0.2500 0.35946(4) 0.0112(3) Uani 1 2 d S
Mn3 Mn 0.8217(3) 0.2500 0.68382(9) 0.0099(14) Uani 0.403(7) 2 d SP
Mn4 Mn 0.0689(3) 0.2500 0.60948(7) 0.0094(5) Uani 0.479(3) 2 d SP
Mn5 Mn 0.8493(2) 0.2500 0.57114(7) 0.0094(5) Uani 0.521(3) 2 d SP
Mn6A Mn 0.3025(4) 0.2500 0.50841(12) 0.0153(5) Uani 0.338(3) 2 d SP
Mn6B Mn 0.3988(2) 0.2500 0.49752(6) 0.0153(5) Uani 0.662(3) 2 d SP
Ca1 Ca 0.0154(3) 0.1644(7) 0.41931(8) 0.0217(9) Uani 0.50 1 d P
Ca2 Ca 0.02486(19) 0.2500 0.32725(5) 0.0199(5) Uani 1 2 d S
Ca3 Ca 0.2419(2) 0.2500 0.67121(5) 0.0158(5) Uani 1 2 d S
Ca4 Ca 0.2895(2) 0.2500 0.57926(6) 0.0193(5) Uani 1 2 d S
Ca5 Ca 0.30165(18) 0.2500 0.37500(5) 0.0129(5) Uani 1 2 d S
Ca6 Ca 0.3057(2) 0.2500 0.75229(7) 0.0245(6) Uani 1 2 d S
Ca7 Ca 0.55270(18) 0.2500 0.69092(5) 0.0117(4) Uani 1 2 d S
Ca8 Ca 0.5746(2) 0.2500 0.55096(6) 0.0273(6) Uani 1 2 d S
Ca9 Ca 0.8483(3) 0.2500 0.50122(7) 0.0497(10) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Mn6A Sb1 Mn5 115.24(7) . 5_666
Mn6A Sb1 Mn5 115.24(7) . 5_656
Mn5 Sb1 Mn5 112.44(11) 5_666 5_656
Mn6A Sb1 Mn6B 27.14(13) . .
Mn5 Sb1 Mn6B 122.84(5) 5_666 .
Mn5 Sb1 Mn6B 122.84(5) 5_656 .
Mn6A Sb1 Ca8 80.87(10) . 5_666
Mn5 Sb1 Ca8 72.60(7) 5_666 5_666
Mn5 Sb1 Ca8 155.58(8) 5_656 5_666
Mn6B Sb1 Ca8 63.53(6) . 5_666
Mn6A Sb1 Ca8 80.87(9) . 5_656
Mn5 Sb1 Ca8 155.58(8) 5_666 5_656
Mn5 Sb1 Ca8 72.60(7) 5_656 5_656
Mn6B Sb1 Ca8 63.53(6) . 5_656
Ca8 Sb1 Ca8 93.37(7) 5_666 5_656
Mn6A Sb1 Ca1 128.02(13) . 7_565
Mn5 Sb1 Ca1 50.09(8) 5_666 7_565
Mn5 Sb1 Ca1 63.95(8) 5_656 7_565
Mn6B Sb1 Ca1 154.58(8) . 7_565
Ca8 Sb1 Ca1 121.91(7) 5_666 7_565
Ca8 Sb1 Ca1 134.89(8) 5_656 7_565
Mn6A Sb1 Ca1 128.02(13) . .
Mn5 Sb1 Ca1 63.95(8) 5_666 .
Mn5 Sb1 Ca1 50.09(8) 5_656 .
Mn6B Sb1 Ca1 154.58(9) . .
Ca8 Sb1 Ca1 134.89(8) 5_666 .
Ca8 Sb1 Ca1 121.91(7) 5_656 .
Ca1 Sb1 Ca1 13.99(12) 7_565 .
Mn6A Sb1 Ca5 155.15(12) . .
Mn5 Sb1 Ca5 76.29(7) 5_666 .
Mn5 Sb1 Ca5 76.29(7) 5_656 .
Mn6B Sb1 Ca5 128.01(7) . .
Ca8 Sb1 Ca5 82.16(6) 5_666 .
Ca8 Sb1 Ca5 82.16(6) 5_656 .
Ca1 Sb1 Ca5 76.60(7) 7_565 .
Ca1 Sb1 Ca5 76.59(7) . .
Mn6A Sb1 Ca9 57.83(9) . 5_666
Mn5 Sb1 Ca9 58.83(8) 5_666 5_666
Mn5 Sb1 Ca9 127.62(8) 5_656 5_666
Mn6B Sb1 Ca9 75.94(7) . 5_666
Ca8 Sb1 Ca9 76.09(6) 5_666 5_666
Ca8 Sb1 Ca9 138.33(8) 5_656 5_666
Ca1 Sb1 Ca9 81.45(9) 7_565 5_666
Ca1 Sb1 Ca9 90.96(9) . 5_666
Ca5 Sb1 Ca9 134.09(5) . 5_666
Mn6A Sb1 Ca9 57.83(9) . 5_656
Mn5 Sb1 Ca9 127.62(8) 5_666 5_656
Mn5 Sb1 Ca9 58.83(8) 5_656 5_656
Mn6B Sb1 Ca9 75.94(7) . 5_656
Ca8 Sb1 Ca9 138.33(8) 5_666 5_656
Ca8 Sb1 Ca9 76.09(6) 5_656 5_656
Ca1 Sb1 Ca9 90.95(9) 7_565 5_656
Ca1 Sb1 Ca9 81.46(9) . 5_656
Ca5 Sb1 Ca9 134.09(5) . 5_656
Ca9 Sb1 Ca9 85.46(7) 5_666 5_656
Mn3 Sb2 Mn3 116.14(15) 5_666 5_656
Mn3 Sb2 Mn1 121.38(7) 5_666 .
Mn3 Sb2 Mn1 121.38(7) 5_656 .
Mn3 Sb2 Ca7 68.96(8) 5_666 5_666
Mn3 Sb2 Ca7 150.45(10) 5_656 5_666
Mn1 Sb2 Ca7 67.07(5) . 5_666
Mn3 Sb2 Ca7 150.45(10) 5_666 5_656
Mn3 Sb2 Ca7 68.96(8) 5_656 5_656
Mn1 Sb2 Ca7 67.07(5) . 5_656
Ca7 Sb2 Ca7 92.77(6) 5_666 5_656
Mn3 Sb2 Ca6 55.82(9) 5_666 2_564
Mn3 Sb2 Ca6 130.50(10) 5_656 2_564
Mn1 Sb2 Ca6 78.28(6) . 2_564
Ca7 Sb2 Ca6 77.64(5) 5_666 2_564
Ca7 Sb2 Ca6 145.00(7) 5_656 2_564
Mn3 Sb2 Ca6 130.50(10) 5_666 2_554
Mn3 Sb2 Ca6 55.82(9) 5_656 2_554
Mn1 Sb2 Ca6 78.28(6) . 2_554
Ca7 Sb2 Ca6 145.00(7) 5_666 2_554
Ca7 Sb2 Ca6 77.64(5) 5_656 2_554
Ca6 Sb2 Ca6 91.05(7) 2_564 2_554
Mn3 Sb2 Ca2 58.71(8) 5_666 .
Mn3 Sb2 Ca2 58.71(8) 5_656 .
Mn1 Sb2 Ca2 159.05(6) . .
Ca7 Sb2 Ca2 124.57(4) 5_666 .
Ca7 Sb2 Ca2 124.57(4) 5_656 .
Ca6 Sb2 Ca2 87.13(6) 2_564 .
Ca6 Sb2 Ca2 87.13(6) 2_554 .
Mn3 Sb2 Ca5 75.86(9) 5_666 .
Mn3 Sb2 Ca5 75.86(9) 5_656 .
Mn1 Sb2 Ca5 127.57(6) . .
Ca7 Sb2 Ca5 77.66(5) 5_666 .
Ca7 Sb2 Ca5 77.66(5) 5_656 .
Ca6 Sb2 Ca5 130.94(5) 2_564 .
Ca6 Sb2 Ca5 130.94(5) 2_554 .
Ca2 Sb2 Ca5 73.38(6) . .
Mn2 Sb3 Mn2 113.33(6) 5_666 5_656
Mn2 Sb3 Ca7 76.25(4) 5_666 .
Mn2 Sb3 Ca7 76.25(4) 5_656 .
Mn2 Sb3 Ca8 115.53(4) 5_666 .
Mn2 Sb3 Ca8 115.53(4) 5_656 .
Ca7 Sb3 Ca8 153.97(7) . .
Mn2 Sb3 Ca4 79.10(5) 5_666 .
Mn2 Sb3 Ca4 79.10(5) 5_656 .
Ca7 Sb3 Ca4 134.26(7) . .
Ca8 Sb3 Ca4 71.77(7) . .
Mn2 Sb3 Ca5 73.71(4) 5_666 5_666
Mn2 Sb3 Ca5 151.34(6) 5_656 5_666
Ca7 Sb3 Ca5 78.90(5) . 5_666
Ca8 Sb3 Ca5 82.42(6) . 5_666
Ca4 Sb3 Ca5 129.19(4) . 5_666
Mn2 Sb3 Ca5 151.34(6) 5_666 5_656
Mn2 Sb3 Ca5 73.71(4) 5_656 5_656
Ca7 Sb3 Ca5 78.90(5) . 5_656
Ca8 Sb3 Ca5 82.42(5) . 5_656
Ca4 Sb3 Ca5 129.19(4) . 5_656
Ca5 Sb3 Ca5 87.74(6) 5_666 5_656
Mn1 Sb4 Mn1 113.88(6) 5_666 5_656
Mn1 Sb4 Ca3 110.17(4) 5_666 6_657
Mn1 Sb4 Ca3 110.17(4) 5_656 6_657
Mn1 Sb4 Ca2 76.42(4) 5_666 2_565
Mn1 Sb4 Ca2 162.20(6) 5_656 2_565
Ca3 Sb4 Ca2 77.53(5) 6_657 2_565
Mn1 Sb4 Ca2 162.20(6) 5_666 2
Mn1 Sb4 Ca2 76.42(4) 5_656 2
Ca3 Sb4 Ca2 77.53(5) 6_657 2
Ca2 Sb4 Ca2 90.16(6) 2_565 2
Mn1 Sb4 Ca6 80.11(5) 5_666 .
Mn1 Sb4 Ca6 80.11(5) 5_656 .
Ca3 Sb4 Ca6 159.16(7) 6_657 .
Ca2 Sb4 Ca6 87.86(6) 2_565 .
Ca2 Sb4 Ca6 87.86(6) 2 .
Mn1 Sb4 Ca6 75.51(4) 5_666 6_657
Mn1 Sb4 Ca6 75.51(4) 5_656 6_657
Ca3 Sb4 Ca6 66.50(7) 6_657 6_657
Ca2 Sb4 Ca6 122.03(5) 2_565 6_657
Ca2 Sb4 Ca6 122.03(5) 2 6_657
Ca6 Sb4 Ca6 134.34(3) . 6_657
Mn6B Sb5 Mn6B 113.68(10) 5_666 5_656
Mn6B Sb5 Mn6A 27.05(12) 5_666 5_666
Mn6B Sb5 Mn6A 120.23(11) 5_656 5_666
Mn6B Sb5 Mn6A 120.23(11) 5_666 5_656
Mn6B Sb5 Mn6A 27.05(12) 5_656 5_656
Mn6A Sb5 Mn6A 112.74(18) 5_666 5_656
Mn6B Sb5 Mn6B 74.72(7) 5_666 .
Mn6B Sb5 Mn6B 74.72(7) 5_656 .
Mn6A Sb5 Mn6B 101.70(11) 5_666 .
Mn6A Sb5 Mn6B 101.70(11) 5_656 .
Mn6B Sb5 Ca8 62.93(7) 5_666 5_666
Mn6B Sb5 Ca8 134.75(7) 5_656 5_666
Mn6A Sb5 Ca8 78.22(10) 5_666 5_666
Mn6A Sb5 Ca8 161.56(12) 5_656 5_666
Mn6B Sb5 Ca8 60.63(5) . 5_666
Mn6B Sb5 Ca8 134.75(7) 5_666 5_656
Mn6B Sb5 Ca8 62.93(7) 5_656 5_656
Mn6A Sb5 Ca8 161.56(11) 5_666 5_656
Mn6A Sb5 Ca8 78.22(10) 5_656 5_656
Mn6B Sb5 Ca8 60.63(5) . 5_656
Ca8 Sb5 Ca8 87.62(7) 5_666 5_656
Mn6B Sb5 Ca9 77.46(6) 5_666 .
Mn6B Sb5 Ca9 77.46(6) 5_656 .
Mn6A Sb5 Ca9 57.90(10) 5_666 .
Mn6A Sb5 Ca9 57.90(10) 5_656 .
Mn6B Sb5 Ca9 127.80(8) . .
Ca8 Sb5 Ca9 135.96(4) 5_666 .
Ca8 Sb5 Ca9 135.96(4) 5_656 .
Mn6B Sb5 Ca4 77.04(6) 5_666 5_666
Mn6B Sb5 Ca4 156.83(7) 5_656 5_666
Mn6A Sb5 Ca4 60.18(11) 5_666 5_666
Mn6A Sb5 Ca4 129.80(12) 5_656 5_666
Mn6B Sb5 Ca4 128.45(5) . 5_666
Ca8 Sb5 Ca4 68.23(6) 5_666 5_666
Ca8 Sb5 Ca4 125.09(6) 5_656 5_666
Ca9 Sb5 Ca4 85.51(6) . 5_666
Mn6B Sb5 Ca4 156.83(7) 5_666 5_656
Mn6B Sb5 Ca4 77.04(6) 5_656 5_656
Mn6A Sb5 Ca4 129.81(12) 5_666 5_656
Mn6A Sb5 Ca4 60.18(11) 5_656 5_656
Mn6B Sb5 Ca4 128.45(5) . 5_656
Ca8 Sb5 Ca4 125.09(6) 5_666 5_656
Ca8 Sb5 Ca4 68.23(6) 5_656 5_656
Ca9 Sb5 Ca4 85.51(6) . 5_656
Ca4 Sb5 Ca4 86.16(6) 5_666 5_656
Mn6B Sb5 Ca8 56.92(5) 5_666 .
Mn6B Sb5 Ca8 56.92(5) 5_656 .
Mn6A Sb5 Ca8 71.06(11) 5_666 .
Mn6A Sb5 Ca8 71.06(11) 5_656 .
Mn6B Sb5 Ca8 57.35(7) . .
Ca8 Sb5 Ca8 100.44(6) 5_666 .
Ca8 Sb5 Ca8 100.44(6) 5_656 .
Ca9 Sb5 Ca8 70.45(7) . .
Ca4 Sb5 Ca8 131.16(4) 5_666 .
Ca4 Sb5 Ca8 131.16(4) 5_656 .
Mn2 Sb6 Mn1 121.80(5) . .
Mn2 Sb6 Ca7 74.21(5) . 5_666
Mn1 Sb6 Ca7 66.29(5) . 5_666
Mn2 Sb6 Ca7 74.21(5) . 5_656
Mn1 Sb6 Ca7 66.29(5) . 5_656
Ca7 Sb6 Ca7 91.60(6) 5_666 5_656
Mn2 Sb6 Ca3 67.18(5) . 5_666
Mn1 Sb6 Ca3 134.42(3) . 5_666
Ca7 Sb6 Ca3 75.93(5) 5_666 5_666
Ca7 Sb6 Ca3 141.30(6) 5_656 5_666
Mn2 Sb6 Ca3 67.18(5) . 5_656
Mn1 Sb6 Ca3 134.42(3) . 5_656
Ca7 Sb6 Ca3 141.30(6) 5_666 5_656
Ca7 Sb6 Ca3 75.93(5) 5_656 5_656
Ca3 Sb6 Ca3 91.09(7) 5_666 5_656
Mn2 Sb6 Ca6 132.46(4) . 5_666
Mn1 Sb6 Ca6 79.30(6) . 5_666
Ca7 Sb6 Ca6 78.63(5) 5_666 5_666
Ca7 Sb6 Ca6 145.20(7) 5_656 5_666
Ca3 Sb6 Ca6 68.79(6) 5_666 5_666
Ca3 Sb6 Ca6 130.70(6) 5_656 5_666
Mn2 Sb6 Ca6 132.45(4) . 5_656
Mn1 Sb6 Ca6 79.30(6) . 5_656
Ca7 Sb6 Ca6 145.20(7) 5_666 5_656
Ca7 Sb6 Ca6 78.63(5) 5_656 5_656
Ca3 Sb6 Ca6 130.70(6) 5_666 5_656
Ca3 Sb6 Ca6 68.79(6) 5_656 5_656
Ca6 Sb6 Ca6 90.50(7) 5_666 5_656
Mn3 Sb7 Mn4 126.04(12) . 1_655
Mn3 Sb7 Mn5 157.05(12) . .
Mn4 Sb7 Mn5 76.90(10) 1_655 .
Mn3 Sb7 Ca1 140.15(7) . 3_656
Mn4 Sb7 Ca1 50.60(8) 1_655 3_656
Mn5 Sb7 Ca1 51.78(8) . 3_656
Mn3 Sb7 Ca1 140.15(7) . 5_656
Mn4 Sb7 Ca1 50.60(8) 1_655 5_656
Mn5 Sb7 Ca1 51.78(8) . 5_656
Ca1 Sb7 Ca1 73.67(12) 3_656 5_656
Mn3 Sb7 Ca5 82.86(8) . 5_666
Mn4 Sb7 Ca5 128.63(5) 1_655 5_666
Mn5 Sb7 Ca5 81.29(6) . 5_666
Ca1 Sb7 Ca5 79.48(7) 3_656 5_666
Ca1 Sb7 Ca5 132.99(8) 5_656 5_666
Mn3 Sb7 Ca5 82.86(8) . 5_656
Mn4 Sb7 Ca5 128.63(5) 1_655 5_656
Mn5 Sb7 Ca5 81.29(6) . 5_656
Ca1 Sb7 Ca5 132.99(8) 3_656 5_656
Ca1 Sb7 Ca5 79.47(7) 5_656 5_656
Ca5 Sb7 Ca5 92.28(6) 5_666 5_656
Mn3 Sb7 Ca2 62.58(7) . 5_666
Mn4 Sb7 Ca2 81.02(7) 1_655 5_666
Mn5 Sb7 Ca2 129.05(5) . 5_666
Ca1 Sb7 Ca2 78.83(7) 3_656 5_666
Ca1 Sb7 Ca2 131.43(8) 5_656 5_666
Ca5 Sb7 Ca2 77.79(5) 5_666 5_666
Ca5 Sb7 Ca2 144.81(6) 5_656 5_666
Mn3 Sb7 Ca2 62.58(7) . 5_656
Mn4 Sb7 Ca2 81.02(7) 1_655 5_656
Mn5 Sb7 Ca2 129.05(5) . 5_656
Ca1 Sb7 Ca2 131.43(8) 3_656 5_656
Ca1 Sb7 Ca2 78.83(7) 5_656 5_656
Ca5 Sb7 Ca2 144.81(6) 5_666 5_656
Ca5 Sb7 Ca2 77.79(5) 5_656 5_656
Ca2 Sb7 Ca2 91.02(6) 5_666 5_656
Mn3 Sb7 Ca1 131.20(6) . 5_666
Mn4 Sb7 Ca1 57.01(7) 1_655 5_666
Mn5 Sb7 Ca1 57.94(6) . 5_666
Ca1 Sb7 Ca1 9.79(8) 3_656 5_666
Ca1 Sb7 Ca1 83.47(8) 5_656 5_666
Ca5 Sb7 Ca1 71.94(6) 5_666 5_666
Ca5 Sb7 Ca1 137.59(7) 5_656 5_666
Ca2 Sb7 Ca1 71.47(7) 5_666 5_666
Ca2 Sb7 Ca1 136.00(7) 5_656 5_666
Mn3 Sb7 Ca1 131.20(6) . 3_646
Mn4 Sb7 Ca1 57.01(7) 1_655 3_646
Mn5 Sb7 Ca1 57.94(6) . 3_646
Ca1 Sb7 Ca1 83.47(8) 3_656 3_646
Ca1 Sb7 Ca1 9.79(8) 5_656 3_646
Ca5 Sb7 Ca1 137.59(7) 5_666 3_646
Ca5 Sb7 Ca1 71.94(6) 5_656 3_646
Ca2 Sb7 Ca1 136.00(7) 5_666 3_646
Ca2 Sb7 Ca1 71.47(6) 5_656 3_646
Ca1 Sb7 Ca1 93.26(11) 5_666 3_646
Mn4 Sb8 Mn4 109.82(11) 5_666 5_656
Mn4 Sb8 Mn2 124.52(6) 5_666 .
Mn4 Sb8 Mn2 124.52(6) 5_656 .
Mn4 Sb8 Ca3 70.63(7) 5_666 5_666
Mn4 Sb8 Ca3 149.46(8) 5_656 5_666
Mn2 Sb8 Ca3 68.36(5) . 5_666
Mn4 Sb8 Ca3 149.46(8) 5_666 5_656
Mn4 Sb8 Ca3 70.62(7) 5_656 5_656
Mn2 Sb8 Ca3 68.36(5) . 5_656
Ca3 Sb8 Ca3 93.61(7) 5_666 5_656
Mn4 Sb8 Ca1 49.00(8) 5_666 7_665
Mn4 Sb8 Ca1 62.96(8) 5_656 7_665
Mn2 Sb8 Ca1 156.07(7) . 7_665
Ca3 Sb8 Ca1 118.05(7) 5_666 7_665
Ca3 Sb8 Ca1 130.52(7) 5_656 7_665
Mn4 Sb8 Ca1 62.96(8) 5_666 1_655
Mn4 Sb8 Ca1 49.00(8) 5_656 1_655
Mn2 Sb8 Ca1 156.07(7) . 1_655
Ca3 Sb8 Ca1 130.52(8) 5_666 1_655
Ca3 Sb8 Ca1 118.05(7) 5_656 1_655
Ca1 Sb8 Ca1 14.15(12) 7_665 1_655
Mn4 Sb8 Ca4 59.21(7) 5_666 5_666
Mn4 Sb8 Ca4 129.13(8) 5_656 5_666
Mn2 Sb8 Ca4 77.20(5) . 5_666
Ca3 Sb8 Ca4 78.56(5) 5_666 5_666
Ca3 Sb8 Ca4 145.08(7) 5_656 5_666
Ca1 Sb8 Ca4 81.57(8) 7_665 5_666
Ca1 Sb8 Ca4 91.46(8) 1_655 5_666
Mn4 Sb8 Ca4 129.13(8) 5_666 5_656
Mn4 Sb8 Ca4 59.21(7) 5_656 5_656
Mn2 Sb8 Ca4 77.20(5) . 5_656
Ca3 Sb8 Ca4 145.08(7) 5_666 5_656
Ca3 Sb8 Ca4 78.56(5) 5_656 5_656
Ca1 Sb8 Ca4 91.46(8) 7_665 5_656
Ca1 Sb8 Ca4 81.57(8) 1_655 5_656
Ca4 Sb8 Ca4 88.60(7) 5_666 5_656
Mn4 Sb8 Ca2 74.82(7) 5_666 1_655
Mn4 Sb8 Ca2 74.82(7) 5_656 1_655
Mn2 Sb8 Ca2 126.80(6) . 1_655
Ca3 Sb8 Ca2 76.06(5) 5_666 1_655
Ca3 Sb8 Ca2 76.06(5) 5_656 1_655
Ca1 Sb8 Ca2 76.23(8) 7_665 1_655
Ca1 Sb8 Ca2 76.23(8) 1_655 1_655
Ca4 Sb8 Ca2 132.66(4) 5_666 1_655
Ca4 Sb8 Ca2 132.66(4) 5_656 1_655
Sb9B Sb9A Ca1 131.93(10) . 3_556
Sb9B Sb9A Ca1 131.93(10) . 5_556
Ca1 Sb9A Ca1 94.38(16) 3_556 5_556
Sb9B Sb9A Mn5 153.9(3) . 1_455
Ca1 Sb9A Mn5 56.95(9) 3_556 1_455
Ca1 Sb9A Mn5 56.95(9) 5_556 1_455
Sb9B Sb9A Mn4 136.1(3) . .
Ca1 Sb9A Mn4 55.41(9) 3_556 .
Ca1 Sb9A Mn4 55.41(9) 5_556 .
Mn5 Sb9A Mn4 69.97(10) 1_455 .
Sb9B Sb9A Ca1 122.62(8) . 5_566
Ca1 Sb9A Ca1 9.57(8) 3_556 5_566
Ca1 Sb9A Ca1 103.94(12) 5_556 5_566
Mn5 Sb9A Ca1 63.90(7) 1_455 5_566
Mn4 Sb9A Ca1 62.74(7) . 5_566
Sb9B Sb9A Ca1 122.62(8) . 3_546
Ca1 Sb9A Ca1 103.94(12) 3_556 3_546
Ca1 Sb9A Ca1 9.57(8) 5_556 3_546
Mn5 Sb9A Ca1 63.90(7) 1_455 3_546
Mn4 Sb9A Ca1 62.74(7) . 3_546
Ca1 Sb9A Ca1 113.51(13) 5_566 3_546
Sb9B Sb9A Ca9 93.1(3) . 1_455
Ca1 Sb9A Ca9 95.01(10) 3_556 1_455
Ca1 Sb9A Ca9 95.01(10) 5_556 1_455
Mn5 Sb9A Ca9 60.75(9) 1_455 1_455
Mn4 Sb9A Ca9 130.73(10) . 1_455
Ca1 Sb9A Ca9 94.04(8) 5_566 1_455
Ca1 Sb9A Ca9 94.04(8) 3_546 1_455
Sb9B Sb9A Ca4 76.3(3) . .
Ca1 Sb9A Ca4 92.14(9) 3_556 .
Ca1 Sb9A Ca4 92.14(9) 5_556 .
Mn5 Sb9A Ca4 129.77(10) 1_455 .
Mn4 Sb9A Ca4 59.80(9) . .
Ca1 Sb9A Ca4 91.73(8) 5_566 .
Ca1 Sb9A Ca4 91.73(8) 3_546 .
Ca9 Sb9A Ca4 169.47(9) 1_455 .
Sb9B Sb9A Ca9 44.89(7) . 5_666
Ca1 Sb9A Ca9 88.90(8) 3_556 5_666
Ca1 Sb9A Ca9 176.72(10) 5_556 5_666
Mn5 Sb9A Ca9 125.36(7) 1_455 5_666
Mn4 Sb9A Ca9 126.97(7) . 5_666
Ca1 Sb9A Ca9 79.34(7) 5_566 5_666
Ca1 Sb9A Ca9 167.16(8) 3_546 5_666
Ca9 Sb9A Ca9 84.74(8) 1_455 5_666
Ca4 Sb9A Ca9 87.69(8) . 5_666
Sb9B Sb9A Ca9 44.89(7) . 5_656
Ca1 Sb9A Ca9 176.72(10) 3_556 5_656
Ca1 Sb9A Ca9 88.90(8) 5_556 5_656
Mn5 Sb9A Ca9 125.36(7) 1_455 5_656
Mn4 Sb9A Ca9 126.97(7) . 5_656
Ca1 Sb9A Ca9 167.16(9) 5_566 5_656
Ca1 Sb9A Ca9 79.34(7) 3_546 5_656
Ca9 Sb9A Ca9 84.74(8) 1_455 5_656
Ca4 Sb9A Ca9 87.69(8) . 5_656
Ca9 Sb9A Ca9 87.82(8) 5_666 5_656
Sb9A Sb9B Mn6A 154.1(3) . .
Sb9A Sb9B Ca9 126.15(9) . 5_666
Mn6A Sb9B Ca9 62.29(9) . 5_666
Sb9A Sb9B Ca9 126.14(9) . 5_656
Mn6A Sb9B Ca9 62.29(9) . 5_656
Ca9 Sb9B Ca9 105.03(12) 5_666 5_656
Sb9A Sb9B Ca1 39.13(9) . 3_556
Mn6A Sb9B Ca1 130.66(10) . 3_556
Ca9 Sb9B Ca1 88.83(8) 5_666 3_556
Ca9 Sb9B Ca1 165.26(11) 5_656 3_556
Sb9A Sb9B Ca1 39.13(9) . 5_556
Mn6A Sb9B Ca1 130.66(10) . 5_556
Ca9 Sb9B Ca1 165.26(11) 5_666 5_556
Ca9 Sb9B Ca1 88.83(8) 5_656 5_556
Ca1 Sb9B Ca1 76.96(14) 3_556 5_556
Sb9A Sb9B Ca4 92.3(3) . .
Mn6A Sb9B Ca4 61.73(12) . .
Ca9 Sb9B Ca4 97.20(9) 5_666 .
Ca9 Sb9B Ca4 97.20(9) 5_656 .
Ca1 Sb9B Ca4 85.79(9) 3_556 .
Ca1 Sb9B Ca4 85.79(9) 5_556 .
Sb9A Sb9B Ca9 75.8(3) . 1_455
Mn6A Sb9B Ca9 130.13(14) . 1_455
Ca9 Sb9B Ca9 89.98(9) 5_666 1_455
Ca9 Sb9B Ca9 89.98(9) 5_656 1_455
Ca1 Sb9B Ca9 84.94(9) 3_556 1_455
Ca1 Sb9B Ca9 84.94(9) 5_556 1_455
Ca4 Sb9B Ca9 168.14(11) . 1_455
Sb9A Sb9B Ca1 48.79(7) . 5_566
Mn6A Sb9B Ca1 123.61(9) . 5_566
Ca9 Sb9B Ca1 79.01(7) 5_666 5_566
Ca9 Sb9B Ca1 174.11(11) 5_656 5_566
Ca1 Sb9B Ca1 9.84(8) 3_556 5_566
Ca1 Sb9B Ca1 86.81(10) 5_556 5_566
Ca4 Sb9B Ca1 86.42(8) . 5_566
Ca9 Sb9B Ca1 85.70(8) 1_455 5_566
Sb9A Sb9B Ca1 48.79(7) . 3_546
Mn6A Sb9B Ca1 123.60(8) . 3_546
Ca9 Sb9B Ca1 174.11(11) 5_666 3_546
Ca9 Sb9B Ca1 79.01(7) 5_656 3_546
Ca1 Sb9B Ca1 86.81(10) 3_556 3_546
Ca1 Sb9B Ca1 9.84(8) 5_556 3_546
Ca4 Sb9B Ca1 86.42(8) . 3_546
Ca9 Sb9B Ca1 85.70(8) 1_455 3_546
Ca1 Sb9B Ca1 96.65(12) 5_566 3_546
Sb4 Mn1 Sb4 113.88(6) 5_666 5_656
Sb4 Mn1 Sb2 113.26(4) 5_666 .
Sb4 Mn1 Sb2 113.26(4) 5_656 .
Sb4 Mn1 Sb6 108.60(4) 5_666 .
Sb4 Mn1 Sb6 108.60(4) 5_656 .
Sb2 Mn1 Sb6 97.85(5) . .
Sb4 Mn1 Ca7 79.33(3) 5_666 5_666
Sb4 Mn1 Ca7 166.34(6) 5_656 5_666
Sb2 Mn1 Ca7 61.40(5) . 5_666
Sb6 Mn1 Ca7 61.82(5) . 5_666
Sb4 Mn1 Ca7 166.35(6) 5_666 5_656
Sb4 Mn1 Ca7 79.33(3) 5_656 5_656
Sb2 Mn1 Ca7 61.40(5) . 5_656
Sb6 Mn1 Ca7 61.82(5) . 5_656
Ca7 Mn1 Ca7 87.29(7) 5_666 5_656
Sb4 Mn1 Ca2 57.88(3) 5_666 6_656
Sb4 Mn1 Ca2 57.88(3) 5_656 6_656
Sb2 Mn1 Ca2 149.34(7) . 6_656
Sb6 Mn1 Ca2 112.81(7) . 6_656
Ca7 Mn1 Ca2 133.51(4) 5_666 6_656
Ca7 Mn1 Ca2 133.51(4) 5_656 6_656
Sb3 Mn2 Sb3 113.33(6) 5_666 5_656
Sb3 Mn2 Sb8 110.44(4) 5_666 .
Sb3 Mn2 Sb8 110.44(4) 5_656 .
Sb3 Mn2 Sb6 112.13(4) 5_666 .
Sb3 Mn2 Sb6 112.13(4) 5_656 .
Sb8 Mn2 Sb6 97.26(5) . .
Sb3 Mn2 Ca3 80.28(3) 5_666 5_666
Sb3 Mn2 Ca3 166.23(6) 5_656 5_666
Sb8 Mn2 Ca3 60.46(5) . 5_666
Sb6 Mn2 Ca3 61.76(5) . 5_666
Sb3 Mn2 Ca3 166.23(6) 5_666 5_656
Sb3 Mn2 Ca3 80.28(3) 5_656 5_656
Sb8 Mn2 Ca3 60.46(5) . 5_656
Sb6 Mn2 Ca3 61.76(5) . 5_656
Ca3 Mn2 Ca3 86.05(7) 5_666 5_656
Sb3 Mn2 Ca7 56.86(4) 5_666 5_666
Sb3 Mn2 Ca7 120.16(6) 5_656 5_666
Sb8 Mn2 Ca7 128.73(5) . 5_666
Sb6 Mn2 Ca7 57.43(4) . 5_666
Ca3 Mn2 Ca7 68.30(5) 5_666 5_666
Ca3 Mn2 Ca7 119.15(7) 5_656 5_666
Sb3 Mn2 Ca7 120.16(6) 5_666 5_656
Sb3 Mn2 Ca7 56.86(4) 5_656 5_656
Sb8 Mn2 Ca7 128.73(5) . 5_656
Sb6 Mn2 Ca7 57.43(4) . 5_656
Ca3 Mn2 Ca7 119.15(7) 5_666 5_656
Ca3 Mn2 Ca7 68.30(5) 5_656 5_656
Ca7 Mn2 Ca7 77.79(6) 5_666 5_656
Sb3 Mn2 Ca5 60.23(3) 5_666 .
Sb3 Mn2 Ca5 60.23(3) 5_656 .
Sb8 Mn2 Ca5 154.84(7) . .
Sb6 Mn2 Ca5 107.90(6) . .
Ca3 Mn2 Ca5 132.51(4) 5_666 .
Ca3 Mn2 Ca5 132.51(4) 5_656 .
Ca7 Mn2 Ca5 68.31(5) 5_666 .
Ca7 Mn2 Ca5 68.31(5) 5_656 .
Sb7 Mn3 Sb2 113.47(9) . 5_666
Sb7 Mn3 Sb2 113.47(9) . 5_656
Sb2 Mn3 Sb2 116.15(15) 5_666 5_656
Sb7 Mn3 Ca6 168.33(19) . 6_657
Sb2 Mn3 Ca6 71.36(9) 5_666 6_657
Sb2 Mn3 Ca6 71.36(9) 5_656 6_657
Sb7 Mn3 Ca2 71.01(9) . 5_666
Sb2 Mn3 Ca2 71.36(4) 5_666 5_666
Sb2 Mn3 Ca2 166.02(16) 5_656 5_666
Ca6 Mn3 Ca2 101.82(11) 6_657 5_666
Sb7 Mn3 Ca2 71.01(9) . 5_656
Sb2 Mn3 Ca2 166.02(16) 5_666 5_656
Sb2 Mn3 Ca2 71.36(4) 5_656 5_656
Ca6 Mn3 Ca2 101.82(11) 6_657 5_656
Ca2 Mn3 Ca2 98.92(14) 5_666 5_656
Sb7 Mn3 Ca7 111.05(14) . .
Sb2 Mn3 Ca7 62.11(8) 5_666 .
Sb2 Mn3 Ca7 62.11(8) 5_656 .
Ca6 Mn3 Ca7 80.62(12) 6_657 .
Ca2 Mn3 Ca7 129.94(7) 5_666 .
Ca2 Mn3 Ca7 129.94(7) 5_656 .
Sb7 Mn3 Ca5 56.78(8) . 5_666
Sb2 Mn3 Ca5 60.15(6) 5_666 5_666
Sb2 Mn3 Ca5 122.28(13) 5_656 5_666
Ca6 Mn3 Ca5 130.76(10) 6_657 5_666
Ca2 Mn3 Ca5 71.53(7) 5_666 5_666
Ca2 Mn3 Ca5 127.38(13) 5_656 5_666
Ca7 Mn3 Ca5 70.15(8) . 5_666
Sb7 Mn3 Ca5 56.78(8) . 5_656
Sb2 Mn3 Ca5 122.28(13) 5_666 5_656
Sb2 Mn3 Ca5 60.15(6) 5_656 5_656
Ca6 Mn3 Ca5 130.76(10) 6_657 5_656
Ca2 Mn3 Ca5 127.38(13) 5_666 5_656
Ca2 Mn3 Ca5 71.53(7) 5_656 5_656
Ca7 Mn3 Ca5 70.15(8) . 5_656
Ca5 Mn3 Ca5 74.87(9) 5_666 5_656
Ca1 Mn4 Ca1 98.49(19) 3_556 5_556
Ca1 Mn4 Sb7 77.53(11) 3_556 1_455
Ca1 Mn4 Sb7 77.53(11) 5_556 1_455
Ca1 Mn4 Sb9A 58.22(10) 3_556 .
Ca1 Mn4 Sb9A 58.22(10) 5_556 .
Sb7 Mn4 Sb9A 106.91(12) 1_455 .
Ca1 Mn4 Sb8 73.55(8) 3_556 5_666
Ca1 Mn4 Sb8 163.03(16) 5_556 5_666
Sb7 Mn4 Sb8 114.22(8) 1_455 5_666
Sb9A Mn4 Sb8 105.42(8) . 5_666
Ca1 Mn4 Sb8 163.03(16) 3_556 5_656
Ca1 Mn4 Sb8 73.55(8) 5_556 5_656
Sb7 Mn4 Sb8 114.22(8) 1_455 5_656
Sb9A Mn4 Sb8 105.42(8) . 5_656
Sb8 Mn4 Sb8 109.82(11) 5_666 5_656
Ca1 Mn4 Ca4 98.94(12) 3_556 .
Ca1 Mn4 Ca4 98.94(12) 5_556 .
Sb7 Mn4 Ca4 174.47(14) 1_455 .
Sb9A Mn4 Ca4 67.55(9) . .
Sb8 Mn4 Ca4 68.31(7) 5_666 .
Sb8 Mn4 Ca4 68.31(7) 5_656 .
Ca1 Mn4 Ca1 9.38(8) 3_556 5_566
Ca1 Mn4 Ca1 107.87(16) 5_556 5_566
Sb7 Mn4 Ca1 80.09(9) 1_455 5_566
Sb9A Mn4 Ca1 65.17(8) . 5_566
Sb8 Mn4 Ca1 64.52(7) 5_666 5_566
Sb8 Mn4 Ca1 165.26(14) 5_656 5_566
Ca4 Mn4 Ca1 97.12(10) . 5_566
Ca1 Mn4 Ca1 107.87(16) 3_556 3_546
Ca1 Mn4 Ca1 9.38(8) 5_556 3_546
Sb7 Mn4 Ca1 80.09(9) 1_455 3_546
Sb9A Mn4 Ca1 65.17(8) . 3_546
Sb8 Mn4 Ca1 165.26(14) 5_666 3_546
Sb8 Mn4 Ca1 64.52(7) 5_656 3_546
Ca4 Mn4 Ca1 97.12(10) . 3_546
Ca1 Mn4 Ca1 117.25(16) 5_566 3_546
Ca1 Mn4 Mn5 51.79(10) 3_556 1_455
Ca1 Mn4 Mn5 51.79(10) 5_556 1_455
Sb7 Mn4 Mn5 52.02(8) 1_455 1_455
Sb9A Mn4 Mn5 54.89(9) . 1_455
Sb8 Mn4 Mn5 124.74(6) 5_666 1_455
Sb8 Mn4 Mn5 124.74(6) 5_656 1_455
Ca4 Mn4 Mn5 122.44(12) . 1_455
Ca1 Mn4 Mn5 60.45(8) 5_566 1_455
Ca1 Mn4 Mn5 60.44(8) 3_546 1_455
Ca1 Mn4 Ca3 130.74(10) 3_556 .
Ca1 Mn4 Ca3 130.74(9) 5_556 .
Sb7 Mn4 Ca3 108.04(11) 1_455 .
Sb9A Mn4 Ca3 145.04(13) . .
Sb8 Mn4 Ca3 59.34(6) 5_666 .
Sb8 Mn4 Ca3 59.34(6) 5_656 .
Ca4 Mn4 Ca3 77.49(10) . .
Ca1 Mn4 Ca3 121.37(8) 5_566 .
Ca1 Mn4 Ca3 121.37(8) 3_546 .
Mn5 Mn4 Ca3 160.07(13) 1_455 .
Ca1 Mn4 Ca2 77.36(9) 3_556 5_566
Ca1 Mn4 Ca2 134.44(14) 5_556 5_566
Sb7 Mn4 Ca2 57.12(6) 1_455 5_566
Sb9A Mn4 Ca2 135.53(7) . 5_566
Sb8 Mn4 Ca2 59.50(5) 5_666 5_566
Sb8 Mn4 Ca2 119.03(10) 5_656 5_566
Ca4 Mn4 Ca2 126.61(8) . 5_566
Ca1 Mn4 Ca2 70.98(7) 5_566 5_566
Ca1 Mn4 Ca2 135.22(12) 3_546 5_566
Mn5 Mn4 Ca2 97.11(9) 1_455 5_566
Ca3 Mn4 Ca2 67.41(7) . 5_566
Ca1 Mn5 Ca1 95.48(18) 3_656 5_656
Ca1 Mn5 Sb7 75.89(10) 3_656 .
Ca1 Mn5 Sb7 75.89(10) 5_656 .
Ca1 Mn5 Sb1 74.41(8) 3_656 5_666
Ca1 Mn5 Sb1 164.06(14) 5_656 5_666
Sb7 Mn5 Sb1 112.44(7) . 5_666
Ca1 Mn5 Sb1 164.06(14) 3_656 5_656
Ca1 Mn5 Sb1 74.41(8) 5_656 5_656
Sb7 Mn5 Sb1 112.44(7) . 5_656
Sb1 Mn5 Sb1 112.44(11) 5_666 5_656
Ca1 Mn5 Sb9A 57.74(10) 3_656 1_655
Ca1 Mn5 Sb9A 57.74(10) 5_656 1_655
Sb7 Mn5 Sb9A 106.21(11) . 1_655
Sb1 Mn5 Sb9A 106.35(7) 5_666 1_655
Sb1 Mn5 Sb9A 106.35(7) 5_656 1_655
Ca1 Mn5 Ca9 99.53(12) 3_656 .
Ca1 Mn5 Ca9 99.53(12) 5_656 .
Sb7 Mn5 Ca9 173.00(14) . .
Sb1 Mn5 Ca9 70.75(7) 5_666 .
Sb1 Mn5 Ca9 70.75(7) 5_656 .
Sb9A Mn5 Ca9 66.79(10) 1_655 .
Ca1 Mn5 Ca1 9.52(8) 3_656 5_666
Ca1 Mn5 Ca1 105.00(15) 5_656 5_666
Sb7 Mn5 Ca1 78.69(9) . 5_666
Sb1 Mn5 Ca1 65.13(7) 5_666 5_666
Sb1 Mn5 Ca1 167.88(13) 5_656 5_666
Sb9A Mn5 Ca1 64.58(8) 1_655 5_666
Ca9 Mn5 Ca1 97.65(9) . 5_666
Ca1 Mn5 Ca1 105.00(15) 3_656 3_646
Ca1 Mn5 Ca1 9.52(8) 5_656 3_646
Sb7 Mn5 Ca1 78.69(8) . 3_646
Sb1 Mn5 Ca1 167.88(13) 5_666 3_646
Sb1 Mn5 Ca1 65.13(6) 5_656 3_646
Sb9A Mn5 Ca1 64.58(8) 1_655 3_646
Ca9 Mn5 Ca1 97.65(9) . 3_646
Ca1 Mn5 Ca1 114.52(15) 5_666 3_646
Ca1 Mn5 Mn4 50.15(9) 3_656 1_655
Ca1 Mn5 Mn4 50.15(9) 5_656 1_655
Sb7 Mn5 Mn4 51.07(8) . 1_655
Sb1 Mn5 Mn4 123.66(5) 5_666 1_655
Sb1 Mn5 Mn4 123.66(5) 5_656 1_655
Sb9A Mn5 Mn4 55.13(9) 1_655 1_655
Ca9 Mn5 Mn4 121.92(13) . 1_655
Ca1 Mn5 Mn4 58.98(8) 5_666 1_655
Ca1 Mn5 Mn4 58.98(8) 3_646 1_655
Ca1 Mn5 Ca8 132.26(9) 3_656 .
Ca1 Mn5 Ca8 132.26(9) 5_656 .
Sb7 Mn5 Ca8 111.80(11) . .
Sb1 Mn5 Ca8 58.87(6) 5_666 .
Sb1 Mn5 Ca8 58.87(6) 5_656 .
Sb9A Mn5 Ca8 142.00(12) 1_655 .
Ca9 Mn5 Ca8 75.21(10) . .
Ca1 Mn5 Ca8 122.74(8) 5_666 .
Ca1 Mn5 Ca8 122.74(8) 3_646 .
Mn4 Mn5 Ca8 162.87(12) 1_655 .
Ca1 Mn5 Ca5 76.82(9) 3_656 5_666
Ca1 Mn5 Ca5 131.99(13) 5_656 5_666
Sb7 Mn5 Ca5 56.18(6) . 5_666
Sb1 Mn5 Ca5 58.61(5) 5_666 5_666
Sb1 Mn5 Ca5 119.11(10) 5_656 5_666
Sb9A Mn5 Ca5 134.51(7) 1_655 5_666
Ca9 Mn5 Ca5 128.44(8) . 5_666
Ca1 Mn5 Ca5 70.58(7) 5_666 5_666
Ca1 Mn5 Ca5 133.40(11) 3_646 5_666
Mn4 Mn5 Ca5 95.30(9) 1_655 5_666
Ca8 Mn5 Ca5 71.28(7) . 5_666
Mn6B Mn6A Sb1 82.1(3) . .
Mn6B Mn6A Sb5 75.84(16) . 5_666
Sb1 Mn6A Sb5 117.31(11) . 5_666
Mn6B Mn6A Sb5 75.84(16) . 5_656
Sb1 Mn6A Sb5 117.31(11) . 5_656
Sb5 Mn6A Sb5 112.74(18) 5_666 5_656
Mn6B Mn6A Sb9B 178.2(4) . .
Sb1 Mn6A Sb9B 99.69(17) . .
Sb5 Mn6A Sb9B 103.21(13) 5_666 .
Sb5 Mn6A Sb9B 103.21(13) 5_656 .
Mn6B Mn6A Ca9 121.87(17) . 5_666
Sb1 Mn6A Ca9 73.29(12) . 5_666
Sb5 Mn6A Ca9 70.74(6) 5_666 5_666
Sb5 Mn6A Ca9 161.6(2) 5_656 5_666
Sb9B Mn6A Ca9 58.93(11) . 5_666
Mn6B Mn6A Ca9 121.87(17) . 5_656
Sb1 Mn6A Ca9 73.29(12) . 5_656
Sb5 Mn6A Ca9 161.6(2) 5_666 5_656
Sb5 Mn6A Ca9 70.74(6) 5_656 5_656
Sb9B Mn6A Ca9 58.93(11) . 5_656
Ca9 Mn6A Ca9 100.31(19) 5_666 5_656
Mn6B Mn6A Ca4 114.7(3) . .
Sb1 Mn6A Ca4 163.1(2) . .
Sb5 Mn6A Ca4 69.58(11) 5_666 .
Sb5 Mn6A Ca4 69.58(11) 5_656 .
Sb9B Mn6A Ca4 63.44(12) . .
Ca9 Mn6A Ca4 96.25(14) 5_666 .
Ca9 Mn6A Ca4 96.25(14) 5_656 .
Mn6B Mn6A Ca8 51.09(15) . 5_666
Sb1 Mn6A Ca8 55.26(9) . 5_666
Sb5 Mn6A Ca8 65.47(8) 5_666 5_666
Sb5 Mn6A Ca8 126.39(17) 5_656 5_666
Sb9B Mn6A Ca8 130.05(12) . 5_666
Ca9 Mn6A Ca8 71.90(9) 5_666 5_666
Ca9 Mn6A Ca8 128.25(17) 5_656 5_666
Ca4 Mn6A Ca8 134.96(11) . 5_666
Mn6B Mn6A Ca8 51.09(15) . 5_656
Sb1 Mn6A Ca8 55.26(9) . 5_656
Sb5 Mn6A Ca8 126.40(17) 5_666 5_656
Sb5 Mn6A Ca8 65.47(8) 5_656 5_656
Sb9B Mn6A Ca8 130.05(12) . 5_656
Ca9 Mn6A Ca8 128.25(17) 5_666 5_656
Ca9 Mn6A Ca8 71.90(9) 5_656 5_656
Ca4 Mn6A Ca8 134.96(11) . 5_656
Ca8 Mn6A Ca8 74.54(11) 5_666 5_656
Mn6A Mn6B Sb5 77.11(14) . 5_666
Mn6A Mn6B Sb5 77.11(14) . 5_656
Sb5 Mn6B Sb5 113.67(10) 5_666 5_656
Mn6A Mn6B Sb1 70.7(3) . .
Sb5 Mn6B Sb1 113.44(6) 5_666 .
Sb5 Mn6B Sb1 113.44(6) 5_656 .
Mn6A Mn6B Sb5 175.3(3) . .
Sb5 Mn6B Sb5 105.28(7) 5_666 .
Sb5 Mn6B Sb5 105.28(7) 5_656 .
Sb1 Mn6B Sb5 104.55(9) . .
Mn6A Mn6B Ca8 110.36(18) . 5_666
Sb5 Mn6B Ca8 76.17(4) 5_666 5_666
Sb5 Mn6B Ca8 169.25(9) 5_656 5_666
Sb1 Mn6B Ca8 63.85(7) . 5_666
Sb5 Mn6B Ca8 66.71(7) . 5_666
Mn6A Mn6B Ca8 110.36(18) . 5_656
Sb5 Mn6B Ca8 169.25(9) 5_666 5_656
Sb5 Mn6B Ca8 76.17(4) 5_656 5_656
Sb1 Mn6B Ca8 63.85(7) . 5_656
Sb5 Mn6B Ca8 66.71(7) . 5_656
Ca8 Mn6B Ca8 93.70(10) 5_666 5_656
Mn6A Mn6B Ca8 111.1(3) . .
Sb5 Mn6B Ca8 67.33(6) 5_666 .
Sb5 Mn6B Ca8 67.33(6) 5_656 .
Sb1 Mn6B Ca8 178.16(11) . .
Sb5 Mn6B Ca8 73.60(8) . .
Ca8 Mn6B Ca8 115.07(8) 5_666 .
Ca8 Mn6B Ca8 115.07(8) 5_656 .
Ca1 Ca1 Mn4 139.25(9) 7_565 5_556
Ca1 Ca1 Mn5 137.74(9) 7_565 5_656
Mn4 Ca1 Mn5 78.05(12) 5_556 5_656
Ca1 Ca1 Sb9A 137.18(8) 7_565 5_556
Mn4 Ca1 Sb9A 66.37(11) 5_556 5_556
Mn5 Ca1 Sb9A 65.31(10) 5_656 5_556
Ca1 Ca1 Sb9B 128.48(7) 7_565 5_556
Mn4 Ca1 Sb9B 71.54(11) 5_556 5_556
Mn5 Ca1 Sb9B 73.04(11) 5_656 5_556
Sb9A Ca1 Sb9B 8.94(3) 5_556 5_556
Ca1 Ca1 Mn4 31.38(8) 7_565 5_566
Mn4 Ca1 Mn4 107.87(16) 5_556 5_566
Mn5 Ca1 Mn4 156.06(16) 5_656 5_566
Sb9A Ca1 Mn4 138.57(15) 5_556 5_566
Sb9B Ca1 Mn4 130.90(13) 5_556 5_566
Ca1 Ca1 Sb7 126.84(6) 7_565 5_656
Mn4 Ca1 Sb7 51.87(10) 5_556 5_656
Mn5 Ca1 Sb7 52.33(9) 5_656 5_656
Sb9A Ca1 Sb7 95.95(10) 5_556 5_656
Sb9B Ca1 Sb7 104.68(10) 5_556 5_656
Mn4 Ca1 Sb7 112.43(12) 5_566 5_656
Ca1 Ca1 Sb8 82.93(6) 7_565 1_455
Mn4 Ca1 Sb8 57.46(9) 5_556 1_455
Mn5 Ca1 Sb8 134.74(14) 5_656 1_455
Sb9A Ca1 Sb8 100.22(11) 5_556 1_455
Sb9B Ca1 Sb8 98.01(11) 5_556 1_455
Mn4 Ca1 Sb8 52.51(7) 5_566 1_455
Sb7 Ca1 Sb8 90.10(9) 5_656 1_455
Ca1 Ca1 Mn5 32.74(8) 7_565 5_666
Mn4 Ca1 Mn5 157.16(16) 5_556 5_666
Mn5 Ca1 Mn5 105.00(15) 5_656 5_666
Sb9A Ca1 Mn5 135.87(14) 5_556 5_666
Sb9B Ca1 Mn5 131.24(13) 5_556 5_666
Mn4 Ca1 Mn5 60.57(9) 5_566 5_666
Sb7 Ca1 Mn5 111.70(12) 5_656 5_666
Sb8 Ca1 Mn5 112.91(11) 1_455 5_666
Ca1 Ca1 Sb9A 33.24(7) 7_565 5_566
Mn4 Ca1 Sb9A 139.33(15) 5_556 5_566
Mn5 Ca1 Sb9A 136.06(14) 5_656 5_566
Sb9A Ca1 Sb9A 103.94(12) 5_556 5_566
Sb9B Ca1 Sb9A 95.26(10) 5_556 5_566
Mn4 Ca1 Sb9A 52.09(8) 5_566 5_566
Sb7 Ca1 Sb9A 160.03(12) 5_656 5_566
Sb8 Ca1 Sb9A 88.12(9) 1_455 5_566
Mn5 Ca1 Sb9A 51.52(8) 5_666 5_566
Ca1 Ca1 Sb1 83.00(6) 7_565 .
Mn4 Ca1 Sb1 132.45(14) 5_556 .
Mn5 Ca1 Sb1 55.50(8) 5_656 .
Sb9A Ca1 Sb1 98.87(11) 5_556 .
Sb9B Ca1 Sb1 100.84(11) 5_556 .
Mn4 Ca1 Sb1 111.15(11) 5_566 .
Sb7 Ca1 Sb1 88.07(9) 5_656 .
Sb8 Ca1 Sb1 160.91(12) 1_455 .
Mn5 Ca1 Sb1 50.92(7) 5_666 .
Sb9A Ca1 Sb1 87.16(9) 5_566 .
Ca1 Ca1 Sb9B 41.67(6) 7_565 5_566
Mn4 Ca1 Sb9B 134.21(15) 5_556 5_566
Mn5 Ca1 Sb9B 134.12(14) 5_656 5_566
Sb9A Ca1 Sb9B 95.54(11) 5_556 5_566
Sb9B Ca1 Sb9B 86.80(10) 5_556 5_566
Mn4 Ca1 Sb9B 57.80(8) 5_566 5_566
Sb7 Ca1 Sb9B 168.50(12) 5_656 5_566
Sb8 Ca1 Sb9B 87.78(9) 1_455 5_566
Mn5 Ca1 Sb9B 59.14(8) 5_666 5_566
Sb9A Ca1 Sb9B 8.60(3) 5_566 5_566
Sb1 Ca1 Sb9B 90.25(9) . 5_566
Mn3 Ca2 Mn3 98.92(14) 5_666 5_656
Mn3 Ca2 Sb7 46.41(8) 5_666 5_666
Mn3 Ca2 Sb7 113.25(10) 5_656 5_666
Mn3 Ca2 Sb7 113.25(10) 5_666 5_656
Mn3 Ca2 Sb7 46.41(8) 5_656 5_656
Sb7 Ca2 Sb7 91.03(6) 5_666 5_656
Mn3 Ca2 Sb4 62.85(8) 5_666 2_564
Mn3 Ca2 Sb4 128.31(11) 5_656 2_564
Sb7 Ca2 Sb4 89.086(18) 5_666 2_564
Sb7 Ca2 Sb4 173.93(9) 5_656 2_564
Mn3 Ca2 Sb4 128.31(11) 5_666 2_554
Mn3 Ca2 Sb4 62.85(8) 5_656 2_554
Sb7 Ca2 Sb4 173.93(9) 5_666 2_554
Sb7 Ca2 Sb4 89.085(18) 5_656 2_554
Sb4 Ca2 Sb4 90.16(6) 2_564 2_554
Mn3 Ca2 Sb2 49.93(7) 5_666 .
Mn3 Ca2 Sb2 49.93(7) 5_656 .
Sb7 Ca2 Sb2 82.34(5) 5_666 .
Sb7 Ca2 Sb2 82.34(5) 5_656 .
Sb4 Ca2 Sb2 91.66(5) 2_564 .
Sb4 Ca2 Sb2 91.66(5) 2_554 .
Mn3 Ca2 Sb8 126.28(8) 5_666 1_455
Mn3 Ca2 Sb8 126.28(8) 5_656 1_455
Sb7 Ca2 Sb8 86.10(5) 5_666 1_455
Sb7 Ca2 Sb8 86.10(5) 5_656 1_455
Sb4 Ca2 Sb8 99.96(6) 2_564 1_455
Sb4 Ca2 Sb8 99.96(6) 2_554 1_455
Sb2 Ca2 Sb8 163.47(8) . 1_455
Mn3 Ca2 Mn1 91.20(9) 5_666 6_556
Mn3 Ca2 Mn1 91.20(9) 5_656 6_556
Sb7 Ca2 Mn1 132.07(4) 5_666 6_556
Sb7 Ca2 Mn1 132.07(4) 5_656 6_556
Sb4 Ca2 Mn1 45.69(3) 2_564 6_556
Sb4 Ca2 Mn1 45.69(3) 2_554 6_556
Sb2 Ca2 Mn1 83.93(6) . 6_556
Sb8 Ca2 Mn1 112.61(7) 1_455 6_556
Mn3 Ca2 Mn4 81.39(8) 5_666 5_566
Mn3 Ca2 Mn4 140.57(11) 5_656 5_566
Sb7 Ca2 Mn4 41.86(5) 5_666 5_566
Sb7 Ca2 Mn4 96.93(7) 5_656 5_566
Sb4 Ca2 Mn4 87.19(5) 2_564 5_566
Sb4 Ca2 Mn4 144.11(9) 2_554 5_566
Sb2 Ca2 Mn4 124.18(7) . 5_566
Sb8 Ca2 Mn4 45.68(5) 1_455 5_566
Mn1 Ca2 Mn4 128.23(7) 6_556 5_566
Mn3 Ca2 Mn4 140.57(11) 5_666 5_556
Mn3 Ca2 Mn4 81.39(8) 5_656 5_556
Sb7 Ca2 Mn4 96.93(7) 5_666 5_556
Sb7 Ca2 Mn4 41.86(5) 5_656 5_556
Sb4 Ca2 Mn4 144.11(9) 2_564 5_556
Sb4 Ca2 Mn4 87.19(5) 2_554 5_556
Sb2 Ca2 Mn4 124.18(7) . 5_556
Sb8 Ca2 Mn4 45.68(5) 1_455 5_556
Mn1 Ca2 Mn4 128.22(7) 6_556 5_556
Mn4 Ca2 Mn4 74.69(7) 5_566 5_556
Mn3 Ca2 Ca5 63.01(8) 5_666 .
Mn3 Ca2 Ca5 63.01(8) 5_656 .
Sb7 Ca2 Ca5 50.73(4) 5_666 .
Sb7 Ca2 Ca5 50.73(4) 5_656 .
Sb4 Ca2 Ca5 125.82(5) 2_564 .
Sb4 Ca2 Ca5 125.82(5) 2_554 .
Sb2 Ca2 Ca5 53.63(5) . .
Sb8 Ca2 Ca5 109.83(7) 1_455 .
Mn1 Ca2 Ca5 137.56(8) 6_556 .
Mn4 Ca2 Ca5 83.12(7) 5_566 .
Mn4 Ca2 Ca5 83.12(7) 5_556 .
Sb8 Ca3 Sb8 93.61(7) 5_666 5_656
Sb8 Ca3 Sb4 106.32(6) 5_666 6_557
Sb8 Ca3 Sb4 106.32(6) 5_656 6_557
Sb8 Ca3 Sb6 83.71(2) 5_666 5_666
Sb8 Ca3 Sb6 158.62(9) 5_656 5_666
Sb4 Ca3 Sb6 94.75(6) 6_557 5_666
Sb8 Ca3 Sb6 158.62(9) 5_666 5_656
Sb8 Ca3 Sb6 83.71(2) 5_656 5_656
Sb4 Ca3 Sb6 94.75(6) 6_557 5_656
Sb6 Ca3 Sb6 91.09(7) 5_666 5_656
Sb8 Ca3 Mn2 51.18(4) 5_666 5_666
Sb8 Ca3 Mn2 111.59(7) 5_656 5_666
Sb4 Ca3 Mn2 136.18(4) 6_557 5_666
Sb6 Ca3 Mn2 51.07(4) 5_666 5_666
Sb6 Ca3 Mn2 110.22(8) 5_656 5_666
Sb8 Ca3 Mn2 111.59(7) 5_666 5_656
Sb8 Ca3 Mn2 51.18(4) 5_656 5_656
Sb4 Ca3 Mn2 136.18(4) 6_557 5_656
Sb6 Ca3 Mn2 110.22(8) 5_666 5_656
Sb6 Ca3 Mn2 51.07(4) 5_656 5_656
Mn2 Ca3 Mn2 86.05(7) 5_666 5_656
Sb8 Ca3 Mn4 50.03(4) 5_666 .
Sb8 Ca3 Mn4 50.03(4) 5_656 .
Sb4 Ca3 Mn4 94.02(9) 6_557 .
Sb6 Ca3 Mn4 133.46(4) 5_666 .
Sb6 Ca3 Mn4 133.46(4) 5_656 .
Mn2 Ca3 Mn4 93.81(7) 5_666 .
Mn2 Ca3 Mn4 93.81(7) 5_656 .
Sb8 Ca3 Ca6 132.94(3) 5_666 .
Sb8 Ca3 Ca6 132.94(3) 5_656 .
Sb4 Ca3 Ca6 60.14(6) 6_557 .
Sb6 Ca3 Ca6 55.82(4) 5_666 .
Sb6 Ca3 Ca6 55.82(4) 5_656 .
Mn2 Ca3 Ca6 104.92(7) 5_666 .
Mn2 Ca3 Ca6 104.92(7) 5_656 .
Mn4 Ca3 Ca6 154.16(10) . .
Sb8 Ca3 Ca7 110.52(6) 5_666 .
Sb8 Ca3 Ca7 110.52(6) 5_656 .
Sb4 Ca3 Ca7 124.96(8) 6_557 .
Sb6 Ca3 Ca7 51.87(4) 5_666 .
Sb6 Ca3 Ca7 51.87(4) 5_656 .
Mn2 Ca3 Ca7 59.36(5) 5_666 .
Mn2 Ca3 Ca7 59.36(5) 5_656 .
Mn4 Ca3 Ca7 141.02(9) . .
Ca6 Ca3 Ca7 64.82(7) . .
Sb8 Ca3 Ca2 54.55(4) 5_666 5_566
Sb8 Ca3 Ca2 104.56(7) 5_656 5_566
Sb4 Ca3 Ca2 51.84(4) 6_557 5_566
Sb6 Ca3 Ca2 91.18(4) 5_666 5_566
Sb6 Ca3 Ca2 146.58(8) 5_656 5_566
Mn2 Ca3 Ca2 96.91(4) 5_666 5_566
Mn2 Ca3 Ca2 153.96(8) 5_656 5_566
Mn4 Ca3 Ca2 60.22(6) . 5_566
Ca6 Ca3 Ca2 99.31(7) . 5_566
Ca7 Ca3 Ca2 142.91(4) . 5_566
Sb8 Ca3 Ca2 104.56(7) 5_666 5_556
Sb8 Ca3 Ca2 54.55(4) 5_656 5_556
Sb4 Ca3 Ca2 51.84(4) 6_557 5_556
Sb6 Ca3 Ca2 146.58(8) 5_666 5_556
Sb6 Ca3 Ca2 91.18(4) 5_656 5_556
Mn2 Ca3 Ca2 153.96(8) 5_666 5_556
Mn2 Ca3 Ca2 96.91(4) 5_656 5_556
Mn4 Ca3 Ca2 60.22(6) . 5_556
Ca6 Ca3 Ca2 99.31(7) . 5_556
Ca7 Ca3 Ca2 142.91(4) . 5_556
Ca2 Ca3 Ca2 69.53(6) 5_566 5_556
Mn4 Ca4 Mn6A 118.81(14) . .
Mn4 Ca4 Sb9B 63.98(9) . .
Mn6A Ca4 Sb9B 54.84(12) . .
Mn4 Ca4 Sb3 120.36(10) . .
Mn6A Ca4 Sb3 120.82(13) . .
Sb9B Ca4 Sb3 175.66(10) . .
Mn4 Ca4 Sb9A 52.65(8) . .
Mn6A Ca4 Sb9A 66.16(11) . .
Sb9B Ca4 Sb9A 11.33(4) . .
Sb3 Ca4 Sb9A 173.01(10) . .
Mn4 Ca4 Sb8 52.48(5) . 5_666
Mn6A Ca4 Sb8 128.52(6) . 5_666
Sb9B Ca4 Sb8 94.04(7) . 5_666
Sb3 Ca4 Sb8 89.06(6) . 5_666
Sb9A Ca4 Sb8 85.94(6) . 5_666
Mn4 Ca4 Sb8 52.48(5) . 5_656
Mn6A Ca4 Sb8 128.52(7) . 5_656
Sb9B Ca4 Sb8 94.04(7) . 5_656
Sb3 Ca4 Sb8 89.06(6) . 5_656
Sb9A Ca4 Sb8 85.94(6) . 5_656
Sb8 Ca4 Sb8 88.60(7) 5_666 5_656
Mn4 Ca4 Sb5 128.12(6) . 5_666
Mn6A Ca4 Sb5 50.24(6) . 5_666
Sb9B Ca4 Sb5 85.41(6) . 5_666
Sb3 Ca4 Sb5 91.42(6) . 5_666
Sb9A Ca4 Sb5 93.68(6) . 5_666
Sb8 Ca4 Sb5 92.619(16) 5_666 5_666
Sb8 Ca4 Sb5 178.70(7) 5_656 5_666
Mn4 Ca4 Sb5 128.12(6) . 5_656
Mn6A Ca4 Sb5 50.24(6) . 5_656
Sb9B Ca4 Sb5 85.41(6) . 5_656
Sb3 Ca4 Sb5 91.42(6) . 5_656
Sb9A Ca4 Sb5 93.68(6) . 5_656
Sb8 Ca4 Sb5 178.70(7) 5_666 5_656
Sb8 Ca4 Sb5 92.618(16) 5_656 5_656
Sb5 Ca4 Sb5 86.16(6) 5_666 5_656
Mn4 Ca4 Ca8 173.49(11) . .
Mn6A Ca4 Ca8 67.70(12) . .
Sb9B Ca4 Ca8 122.53(10) . .
Sb3 Ca4 Ca8 53.12(6) . .
Sb9A Ca4 Ca8 133.86(10) . .
Sb8 Ca4 Ca8 124.23(6) 5_666 .
Sb8 Ca4 Ca8 124.23(5) 5_656 .
Sb5 Ca4 Ca8 55.31(5) 5_666 .
Sb5 Ca4 Ca8 55.31(5) 5_656 .
Mn4 Ca4 Ca3 55.80(8) . .
Mn6A Ca4 Ca3 174.62(13) . .
Sb9B Ca4 Ca3 119.78(9) . .
Sb3 Ca4 Ca3 64.56(6) . .
Sb9A Ca4 Ca3 108.45(8) . .
Sb8 Ca4 Ca3 49.22(4) 5_666 .
Sb8 Ca4 Ca3 49.22(4) 5_656 .
Sb5 Ca4 Ca3 132.05(4) 5_666 .
Sb5 Ca4 Ca3 132.05(4) 5_656 .
Ca8 Ca4 Ca3 117.68(8) . .
Mn4 Ca4 Ca1 35.89(6) . 3_556
Mn6A Ca4 Ca1 93.49(11) . 3_556
Sb9B Ca4 Ca1 46.09(6) . 3_556
Sb3 Ca4 Ca1 137.24(7) . 3_556
Sb9A Ca4 Ca1 37.76(6) . 3_556
Sb8 Ca4 Ca1 48.24(6) 5_666 3_556
Sb8 Ca4 Ca1 87.81(7) 5_656 3_556
Sb5 Ca4 Ca1 92.65(6) 5_666 3_556
Sb5 Ca4 Ca1 131.32(8) 5_656 3_556
Ca8 Ca4 Ca1 147.95(7) . 3_556
Ca3 Ca4 Ca1 81.71(7) . 3_556
Sb7 Ca5 Sb7 92.28(6) 5_666 5_656
Sb7 Ca5 Sb3 89.990(17) 5_666 5_666
Sb7 Ca5 Sb3 177.71(6) 5_656 5_666
Sb7 Ca5 Sb3 177.71(6) 5_666 5_656
Sb7 Ca5 Sb3 89.989(17) 5_656 5_656
Sb3 Ca5 Sb3 87.74(6) 5_666 5_656
Sb7 Ca5 Sb1 86.18(5) 5_666 .
Sb7 Ca5 Sb1 86.18(5) 5_656 .
Sb3 Ca5 Sb1 94.26(5) 5_666 .
Sb3 Ca5 Sb1 94.26(5) 5_656 .
Sb7 Ca5 Sb2 82.39(5) 5_666 .
Sb7 Ca5 Sb2 82.39(5) 5_656 .
Sb3 Ca5 Sb2 97.63(5) 5_666 .
Sb3 Ca5 Sb2 97.63(5) 5_656 .
Sb1 Ca5 Sb2 163.47(8) . .
Sb7 Ca5 Mn2 131.73(4) 5_666 .
Sb7 Ca5 Mn2 131.73(4) 5_656 .
Sb3 Ca5 Mn2 46.06(3) 5_666 .
Sb3 Ca5 Mn2 46.06(3) 5_656 .
Sb1 Ca5 Mn2 111.64(7) . .
Sb2 Ca5 Mn2 84.89(6) . .
Sb7 Ca5 Mn3 40.36(6) 5_666 5_666
Sb7 Ca5 Mn3 96.58(7) 5_656 5_666
Sb3 Ca5 Mn3 84.97(6) 5_666 5_666
Sb3 Ca5 Mn3 139.01(9) 5_656 5_666
Sb1 Ca5 Mn3 126.45(7) . 5_666
Sb2 Ca5 Mn3 43.99(5) . 5_666
Mn2 Ca5 Mn3 105.70(8) . 5_666
Sb7 Ca5 Mn3 96.58(7) 5_666 5_656
Sb7 Ca5 Mn3 40.36(6) 5_656 5_656
Sb3 Ca5 Mn3 139.01(9) 5_666 5_656
Sb3 Ca5 Mn3 84.97(6) 5_656 5_656
Sb1 Ca5 Mn3 126.45(7) . 5_656
Sb2 Ca5 Mn3 43.99(5) . 5_656
Mn2 Ca5 Mn3 105.70(8) . 5_656
Mn3 Ca5 Mn3 74.87(9) 5_666 5_656
Sb7 Ca5 Mn5 42.53(5) 5_666 5_666
Sb7 Ca5 Mn5 97.87(7) 5_656 5_666
Sb3 Ca5 Mn5 84.00(5) 5_666 5_666
Sb3 Ca5 Mn5 137.34(8) 5_656 5_666
Sb1 Ca5 Mn5 45.10(4) . 5_666
Sb2 Ca5 Mn5 124.91(6) . 5_666
Mn2 Ca5 Mn5 126.96(6) . 5_666
Mn3 Ca5 Mn5 81.82(7) 5_666 5_666
Mn3 Ca5 Mn5 126.48(9) 5_656 5_666
Sb7 Ca5 Mn5 97.87(7) 5_666 5_656
Sb7 Ca5 Mn5 42.53(5) 5_656 5_656
Sb3 Ca5 Mn5 137.34(8) 5_666 5_656
Sb3 Ca5 Mn5 84.00(5) 5_656 5_656
Sb1 Ca5 Mn5 45.10(4) . 5_656
Sb2 Ca5 Mn5 124.91(6) . 5_656
Mn2 Ca5 Mn5 126.96(6) . 5_656
Mn3 Ca5 Mn5 126.48(9) 5_666 5_656
Mn3 Ca5 Mn5 81.82(7) 5_656 5_656
Mn5 Ca5 Mn5 74.61(7) 5_666 5_656
Sb7 Ca5 Ca2 51.48(4) 5_666 .
Sb7 Ca5 Ca2 51.48(4) 5_656 .
Sb3 Ca5 Ca2 130.22(4) 5_666 .
Sb3 Ca5 Ca2 130.22(4) 5_656 .
Sb1 Ca5 Ca2 110.48(7) . .
Sb2 Ca5 Ca2 52.98(5) . .
Mn2 Ca5 Ca2 137.87(8) . .
Mn3 Ca5 Ca2 45.46(6) 5_666 .
Mn3 Ca5 Ca2 45.46(6) 5_656 .
Mn5 Ca5 Ca2 84.46(7) 5_666 .
Mn5 Ca5 Ca2 84.46(7) 5_656 .
Mn3 Ca6 Sb2 52.81(6) 6_557 2_565
Mn3 Ca6 Sb2 52.81(6) 6_557 2
Sb2 Ca6 Sb2 91.05(7) 2_565 2
Mn3 Ca6 Sb6 128.55(7) 6_557 5_666
Sb2 Ca6 Sb6 89.196(16) 2_565 5_666
Sb2 Ca6 Sb6 178.12(11) 2 5_666
Mn3 Ca6 Sb6 128.55(7) 6_557 5_656
Sb2 Ca6 Sb6 178.12(11) 2_565 5_656
Sb2 Ca6 Sb6 89.195(16) 2 5_656
Sb6 Ca6 Sb6 90.50(7) 5_666 5_656
Mn3 Ca6 Sb4 64.40(11) 6_557 .
Sb2 Ca6 Sb4 93.34(7) 2_565 .
Sb2 Ca6 Sb4 93.34(7) 2 .
Sb6 Ca6 Sb4 88.50(6) 5_666 .
Sb6 Ca6 Sb4 88.50(6) 5_656 .
Mn3 Ca6 Sb4 118.15(12) 6_557 6_557
Sb2 Ca6 Sb4 88.44(6) 2_565 6_557
Sb2 Ca6 Sb4 88.44(6) 2 6_557
Sb6 Ca6 Sb4 89.70(7) 5_666 6_557
Sb6 Ca6 Sb4 89.70(7) 5_656 6_557
Sb4 Ca6 Sb4 177.45(9) . 6_557
Mn3 Ca6 Ca3 171.51(13) 6_557 .
Sb2 Ca6 Ca3 123.06(7) 2_565 .
Sb2 Ca6 Ca3 123.06(7) 2 .
Sb6 Ca6 Ca3 55.39(5) 5_666 .
Sb6 Ca6 Ca3 55.39(5) 5_656 .
Sb4 Ca6 Ca3 124.09(8) . .
Sb4 Ca6 Ca3 53.37(6) 6_557 .
Mn3 Ca6 Ca7 55.59(10) 6_557 6_557
Sb2 Ca6 Ca7 50.66(4) 2_565 6_557
Sb2 Ca6 Ca7 50.66(4) 2 6_557
Sb6 Ca6 Ca7 128.49(5) 5_666 6_557
Sb6 Ca6 Ca7 128.49(5) 5_656 6_557
Sb4 Ca6 Ca7 119.98(9) . 6_557
Sb4 Ca6 Ca7 62.56(5) 6_557 6_557
Ca3 Ca6 Ca7 115.93(9) . 6_557
Mn3 Ca6 Ca7 127.27(13) 6_557 .
Sb2 Ca6 Ca7 130.39(5) 2_565 .
Sb2 Ca6 Ca7 130.39(5) 2 .
Sb6 Ca6 Ca7 50.35(4) 5_666 .
Sb6 Ca6 Ca7 50.35(4) 5_656 .
Sb4 Ca6 Ca7 62.87(5) . .
Sb4 Ca6 Ca7 114.58(8) 6_557 .
Ca3 Ca6 Ca7 61.22(6) . .
Ca7 Ca6 Ca7 177.15(10) 6_557 .
Sb3 Ca7 Sb2 105.58(5) . 5_666
Sb3 Ca7 Sb2 105.58(5) . 5_656
Sb2 Ca7 Sb2 92.77(6) 5_666 5_656
Sb3 Ca7 Sb6 93.70(5) . 5_666
Sb2 Ca7 Sb6 84.53(2) 5_666 5_666
Sb2 Ca7 Sb6 160.52(8) 5_656 5_666
Sb3 Ca7 Sb6 93.70(5) . 5_656
Sb2 Ca7 Sb6 160.52(8) 5_666 5_656
Sb2 Ca7 Sb6 84.53(2) 5_656 5_656
Sb6 Ca7 Sb6 91.60(6) 5_666 5_656
Sb3 Ca7 Mn1 135.66(4) . 5_666
Sb2 Ca7 Mn1 51.53(4) 5_666 5_666
Sb2 Ca7 Mn1 112.17(7) 5_656 5_666
Sb6 Ca7 Mn1 51.89(4) 5_666 5_666
Sb6 Ca7 Mn1 111.87(7) 5_656 5_666
Sb3 Ca7 Mn1 135.66(4) . 5_656
Sb2 Ca7 Mn1 112.17(7) 5_666 5_656
Sb2 Ca7 Mn1 51.53(4) 5_656 5_656
Sb6 Ca7 Mn1 111.87(7) 5_666 5_656
Sb6 Ca7 Mn1 51.89(4) 5_656 5_656
Mn1 Ca7 Mn1 87.29(7) 5_666 5_656
Sb3 Ca7 Mn3 95.15(9) . .
Sb2 Ca7 Mn3 48.93(4) 5_666 .
Sb2 Ca7 Mn3 48.93(4) 5_656 .
Sb6 Ca7 Mn3 133.28(3) 5_666 .
Sb6 Ca7 Mn3 133.28(3) 5_656 .
Mn1 Ca7 Mn3 92.58(7) 5_666 .
Mn1 Ca7 Mn3 92.58(7) 5_656 .
Sb3 Ca7 Mn2 46.88(3) . 5_666
Sb2 Ca7 Mn2 88.03(3) 5_666 5_666
Sb2 Ca7 Mn2 151.01(8) 5_656 5_666
Sb6 Ca7 Mn2 48.36(3) 5_666 5_666
Sb6 Ca7 Mn2 103.64(6) 5_656 5_666
Mn1 Ca7 Mn2 90.84(4) 5_666 5_666
Mn1 Ca7 Mn2 151.81(8) 5_656 5_666
Mn3 Ca7 Mn2 115.61(8) . 5_666
Sb3 Ca7 Mn2 46.88(4) . 5_656
Sb2 Ca7 Mn2 151.01(8) 5_666 5_656
Sb2 Ca7 Mn2 88.03(3) 5_656 5_656
Sb6 Ca7 Mn2 103.64(6) 5_666 5_656
Sb6 Ca7 Mn2 48.36(3) 5_656 5_656
Mn1 Ca7 Mn2 151.81(8) 5_666 5_656
Mn1 Ca7 Mn2 90.84(4) 5_656 5_656
Mn3 Ca7 Mn2 115.61(7) . 5_656
Mn2 Ca7 Mn2 77.78(6) 5_666 5_656
Sb3 Ca7 Ca3 66.87(5) . .
Sb2 Ca7 Ca3 133.62(3) 5_666 .
Sb2 Ca7 Ca3 133.61(3) 5_656 .
Sb6 Ca7 Ca3 52.19(4) 5_666 .
Sb6 Ca7 Ca3 52.19(4) 5_656 .
Mn1 Ca7 Ca3 100.38(6) 5_666 .
Mn1 Ca7 Ca3 100.38(6) 5_656 .
Mn3 Ca7 Ca3 162.02(10) . .
Mn2 Ca7 Ca3 52.34(4) 5_666 .
Mn2 Ca7 Ca3 52.34(4) 5_656 .
Sb3 Ca7 Ca6 138.95(8) . 6_657
Sb2 Ca7 Ca6 51.70(4) 5_666 6_657
Sb2 Ca7 Ca6 51.70(4) 5_656 6_657
Sb6 Ca7 Ca6 114.03(6) 5_666 6_657
Sb6 Ca7 Ca6 114.03(6) 5_656 6_657
Mn1 Ca7 Ca6 62.14(5) 5_666 6_657
Mn1 Ca7 Ca6 62.14(5) 5_656 6_657
Mn3 Ca7 Ca6 43.79(9) . 6_657
Mn2 Ca7 Ca6 139.46(3) 5_666 6_657
Mn2 Ca7 Ca6 139.46(3) 5_656 6_657
Ca3 Ca7 Ca6 154.18(8) . 6_657
Mn6B Ca8 Mn6B 93.70(10) 5_666 5_656
Mn6B Ca8 Sb3 132.78(5) 5_666 .
Mn6B Ca8 Sb3 132.78(5) 5_656 .
Mn6B Ca8 Sb1 52.62(5) 5_666 5_666
Mn6B Ca8 Sb1 117.04(9) 5_656 5_666
Sb3 Ca8 Sb1 100.96(7) . 5_666
Mn6B Ca8 Sb1 117.04(9) 5_666 5_656
Mn6B Ca8 Sb1 52.62(5) 5_656 5_656
Sb3 Ca8 Sb1 100.96(7) . 5_656
Sb1 Ca8 Sb1 93.37(7) 5_666 5_656
Mn6B Ca8 Mn6B 64.93(8) 5_666 .
Mn6B Ca8 Mn6B 64.93(8) 5_656 .
Sb3 Ca8 Mn6B 121.54(10) . .
Sb1 Ca8 Mn6B 117.53(7) 5_666 .
Sb1 Ca8 Mn6B 117.53(7) 5_656 .
Mn6B Ca8 Sb5 52.66(6) 5_666 5_666
Mn6B Ca8 Sb5 113.80(10) 5_656 5_666
Sb3 Ca8 Sb5 93.70(6) . 5_666
Sb1 Ca8 Sb5 87.58(2) 5_666 5_666
Sb1 Ca8 Sb5 164.83(10) 5_656 5_666
Mn6B Ca8 Sb5 49.74(4) . 5_666
Mn6B Ca8 Sb5 113.80(10) 5_666 5_656
Mn6B Ca8 Sb5 52.66(6) 5_656 5_656
Sb3 Ca8 Sb5 93.70(6) . 5_656
Sb1 Ca8 Sb5 164.83(10) 5_666 5_656
Sb1 Ca8 Sb5 87.58(2) 5_656 5_656
Mn6B Ca8 Sb5 49.74(4) . 5_656
Sb5 Ca8 Sb5 87.62(7) 5_666 5_656
Mn6B Ca8 Mn5 93.94(8) 5_666 .
Mn6B Ca8 Mn5 93.94(8) 5_656 .
Sb3 Ca8 Mn5 90.97(9) . .
Sb1 Ca8 Mn5 48.53(4) 5_666 .
Sb1 Ca8 Mn5 48.53(4) 5_656 .
Mn6B Ca8 Mn5 147.49(11) . .
Sb5 Ca8 Mn5 135.85(4) 5_666 .
Sb5 Ca8 Mn5 135.85(4) 5_656 .
Mn6B Ca8 Sb5 46.91(5) 5_666 .
Mn6B Ca8 Sb5 46.91(5) 5_656 .
Sb3 Ca8 Sb5 170.58(9) . .
Sb1 Ca8 Sb5 85.42(6) 5_666 .
Sb1 Ca8 Sb5 85.42(6) 5_656 .
Mn6B Ca8 Sb5 49.04(6) . .
Sb5 Ca8 Sb5 79.56(6) 5_666 .
Sb5 Ca8 Sb5 79.56(6) 5_656 .
Mn5 Ca8 Sb5 98.44(8) . .
Mn6B Ca8 Ca4 108.83(8) 5_666 .
Mn6B Ca8 Ca4 108.83(8) 5_656 .
Sb3 Ca8 Ca4 55.11(6) . .
Sb1 Ca8 Ca4 130.50(5) 5_666 .
Sb1 Ca8 Ca4 130.50(5) 5_656 .
Mn6B Ca8 Ca4 66.43(8) . .
Sb5 Ca8 Ca4 56.45(5) 5_666 .
Sb5 Ca8 Ca4 56.45(5) 5_656 .
Mn5 Ca8 Ca4 146.08(11) . .
Sb5 Ca8 Ca4 115.48(8) . .
Mn6B Ca8 Mn6A 18.55(9) 5_666 5_666
Mn6B Ca8 Mn6A 86.31(9) 5_656 5_666
Sb3 Ca8 Mn6A 140.30(7) . 5_666
Sb1 Ca8 Mn6A 43.87(8) 5_666 5_666
Sb1 Ca8 Mn6A 99.23(9) 5_656 5_666
Mn6B Ca8 Mn6A 76.74(10) . 5_666
Sb5 Ca8 Mn6A 71.17(8) 5_666 5_666
Sb5 Ca8 Mn6A 121.04(11) 5_656 5_666
Mn5 Ca8 Mn6A 77.51(10) . 5_666
Sb5 Ca8 Mn6A 43.46(7) . 5_666
Ca4 Ca8 Mn6A 127.36(9) . 5_666
Sb9B Ca9 Sb9B 105.04(12) 5_666 5_656
Sb9B Ca9 Mn6A 58.78(10) 5_666 5_666
Sb9B Ca9 Mn6A 134.45(16) 5_656 5_666
Sb9B Ca9 Mn6A 134.45(16) 5_666 5_656
Sb9B Ca9 Mn6A 58.78(10) 5_656 5_656
Mn6A Ca9 Mn6A 100.31(19) 5_666 5_656
Sb9B Ca9 Mn5 123.01(8) 5_666 .
Sb9B Ca9 Mn5 123.01(8) 5_656 .
Mn6A Ca9 Mn5 98.26(13) 5_666 .
Mn6A Ca9 Mn5 98.26(13) 5_656 .
Sb9B Ca9 Sb9A 96.72(9) 5_666 1_655
Sb9B Ca9 Sb9A 96.72(9) 5_656 1_655
Mn6A Ca9 Sb9A 125.63(10) 5_666 1_655
Mn6A Ca9 Sb9A 125.63(10) 5_656 1_655
Mn5 Ca9 Sb9A 52.46(9) . 1_655
Sb9B Ca9 Sb9A 8.97(3) 5_666 5_666
Sb9B Ca9 Sb9A 96.49(10) 5_656 5_666
Mn6A Ca9 Sb9A 66.71(10) 5_666 5_666
Mn6A Ca9 Sb9A 132.03(15) 5_656 5_666
Mn5 Ca9 Sb9A 128.50(8) . 5_666
Sb9A Ca9 Sb9A 95.27(8) 1_655 5_666
Sb9B Ca9 Sb9A 96.49(10) 5_666 5_656
Sb9B Ca9 Sb9A 8.97(3) 5_656 5_656
Mn6A Ca9 Sb9A 132.03(15) 5_666 5_656
Mn6A Ca9 Sb9A 66.71(10) 5_656 5_656
Mn5 Ca9 Sb9A 128.50(8) . 5_656
Sb9A Ca9 Sb9A 95.27(8) 1_655 5_656
Sb9A Ca9 Sb9A 87.82(8) 5_666 5_656
Sb9B Ca9 Sb9B 90.02(9) 5_666 1_655
Sb9B Ca9 Sb9B 90.02(9) 5_656 1_655
Mn6A Ca9 Sb9B 128.53(10) 5_666 1_655
Mn6A Ca9 Sb9B 128.53(10) 5_656 1_655
Mn5 Ca9 Sb9B 63.51(10) . 1_655
Sb9A Ca9 Sb9B 11.06(4) 1_655 1_655
Sb9A Ca9 Sb9B 87.31(8) 5_666 1_655
Sb9A Ca9 Sb9B 87.31(8) 5_656 1_655
Sb9B Ca9 Sb5 90.33(9) 5_666 .
Sb9B Ca9 Sb5 90.33(9) 5_656 .
Mn6A Ca9 Sb5 51.36(10) 5_666 .
Mn6A Ca9 Sb5 51.36(9) 5_656 .
Mn5 Ca9 Sb5 115.90(11) . .
Sb9A Ca9 Sb5 168.36(11) 1_655 .
Sb9A Ca9 Sb5 93.11(8) 5_666 .
Sb9A Ca9 Sb5 93.11(8) 5_656 .
Sb9B Ca9 Sb5 179.41(11) 1_655 .
Sb9B Ca9 Sb1 84.71(4) 5_666 5_666
Sb9B Ca9 Sb1 169.95(9) 5_656 5_666
Mn6A Ca9 Sb1 48.88(10) 5_666 5_666
Mn6A Ca9 Sb1 112.60(13) 5_656 5_666
Mn5 Ca9 Sb1 50.42(5) . 5_666
Sb9A Ca9 Sb1 84.35(7) 1_655 5_666
Sb9A Ca9 Sb1 93.36(2) 5_666 5_666
Sb9A Ca9 Sb1 178.78(8) 5_656 5_666
Sb9B Ca9 Sb1 92.46(8) 1_655 5_666
Sb5 Ca9 Sb1 87.11(7) . 5_666
Sb9B Ca9 Sb1 169.95(9) 5_666 5_656
Sb9B Ca9 Sb1 84.71(4) 5_656 5_656
Mn6A Ca9 Sb1 112.60(13) 5_666 5_656
Mn6A Ca9 Sb1 48.88(10) 5_656 5_656
Mn5 Ca9 Sb1 50.42(5) . 5_656
Sb9A Ca9 Sb1 84.35(7) 1_655 5_656
Sb9A Ca9 Sb1 178.79(8) 5_666 5_656
Sb9A Ca9 Sb1 93.36(2) 5_656 5_656
Sb9B Ca9 Sb1 92.46(8) 1_655 5_656
Sb5 Ca9 Sb1 87.11(7) . 5_656
Sb1 Ca9 Sb1 85.46(7) 5_666 5_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 Mn6A 2.676(5) .
Sb1 Mn5 2.7778(17) 5_666
Sb1 Mn5 2.7778(18) 5_656
Sb1 Mn6B 2.809(3) .
Sb1 Ca8 3.1732(19) 5_666
Sb1 Ca8 3.1732(19) 5_656
Sb1 Ca1 3.247(4) 7_565
Sb1 Ca1 3.247(4) .
Sb1 Ca5 3.348(2) .
Sb1 Ca9 3.403(2) 5_666
Sb1 Ca9 3.403(2) 5_656
Sb2 Mn3 2.720(2) 5_666
Sb2 Mn3 2.720(2) 5_656
Sb2 Mn1 2.8438(18) .
Sb2 Ca7 3.1890(16) 5_666
Sb2 Ca7 3.1891(16) 5_656
Sb2 Ca6 3.2356(19) 2_564
Sb2 Ca6 3.2356(19) 2_554
Sb2 Ca2 3.369(3) .
Sb2 Ca5 3.397(2) .
Sb3 Mn2 2.7635(10) 5_666
Sb3 Mn2 2.7635(10) 5_656
Sb3 Ca7 3.170(2) .
Sb3 Ca8 3.172(3) .
Sb3 Ca4 3.253(3) .
Sb3 Ca5 3.3316(17) 5_666
Sb3 Ca5 3.3316(17) 5_656
Sb4 Mn1 2.7549(10) 5_666
Sb4 Mn1 2.7549(10) 5_656
Sb4 Ca3 3.206(3) 6_657
Sb4 Ca2 3.2606(18) 2_565
Sb4 Ca2 3.2606(18) 2
Sb4 Ca6 3.301(3) .
Sb4 Ca6 3.465(3) 6_657
Sb5 Mn6B 2.7580(16) 5_666
Sb5 Mn6B 2.7581(15) 5_656
Sb5 Mn6A 2.773(3) 5_666
Sb5 Mn6A 2.773(3) 5_656
Sb5 Mn6B 2.887(3) .
Sb5 Ca8 3.335(2) 5_666
Sb5 Ca8 3.335(2) 5_656
Sb5 Ca9 3.351(4) .
Sb5 Ca4 3.380(2) 5_666
Sb5 Ca4 3.380(2) 5_656
Sb5 Ca8 3.667(3) .
Sb6 Mn2 2.8556(19) .
Sb6 Mn1 2.8749(19) .
Sb6 Ca7 3.2205(16) 5_666
Sb6 Ca7 3.2206(17) 5_656
Sb6 Ca3 3.2344(18) 5_666
Sb6 Ca3 3.2345(18) 5_656
Sb6 Ca6 3.251(2) 5_666
Sb6 Ca6 3.2511(19) 5_656
Sb7 Mn3 2.479(4) .
Sb7 Mn4 2.571(3) 1_655
Sb7 Mn5 2.605(3) .
Sb7 Ca1 3.192(3) 3_656
Sb7 Ca1 3.192(3) 5_656
Sb7 Ca5 3.2021(17) 5_666
Sb7 Ca5 3.2021(17) 5_656
Sb7 Ca2 3.2364(17) 5_666
Sb7 Ca2 3.2365(17) 5_656
Sb7 Ca1 3.720(4) 5_666
Sb7 Ca1 3.720(3) 3_646
Sb8 Mn4 2.822(2) 5_666
Sb8 Mn4 2.8216(19) 5_656
Sb8 Mn2 2.8363(19) .
Sb8 Ca3 3.1671(17) 5_666
Sb8 Ca3 3.1671(17) 5_656
Sb8 Ca1 3.210(4) 7_665
Sb8 Ca1 3.210(4) 1_655
Sb8 Ca4 3.306(2) 5_666
Sb8 Ca4 3.306(2) 5_656
Sb8 Ca2 3.398(3) 1_655
Sb9A Sb9B 0.6425(19) .
Sb9A Ca1 2.608(4) 3_556
Sb9A Ca1 2.608(4) 5_556
Sb9A Mn5 2.803(4) 1_455
Sb9A Mn4 2.811(4) .
Sb9A Ca1 3.233(4) 5_566
Sb9A Ca1 3.233(4) 3_546
Sb9A Ca9 3.248(4) 1_455
Sb9A Ca4 3.268(3) .
Sb9A Ca9 3.329(3) 5_666
Sb9A Ca9 3.329(3) 5_656
Sb9B Mn6A 2.905(6) .
Sb9B Ca9 2.910(2) 5_666
Sb9B Ca9 2.910(2) 5_656
Sb9B Ca1 3.075(4) 3_556
Sb9B Ca1 3.075(4) 5_556
Sb9B Ca4 3.178(3) .
Sb9B Ca9 3.346(4) 1_455
Sb9B Ca1 3.620(4) 5_566
Sb9B Ca1 3.620(4) 3_546
Mn1 Sb4 2.7549(10) 5_666
Mn1 Sb4 2.7549(10) 5_656
Mn1 Ca7 3.345(2) 5_666
Mn1 Ca7 3.345(2) 5_656
Mn1 Ca2 3.742(3) 6_656
Mn2 Sb3 2.7636(10) 5_666
Mn2 Sb3 2.7636(10) 5_656
Mn2 Ca3 3.384(2) 5_666
Mn2 Ca3 3.384(2) 5_656
Mn2 Ca7 3.677(2) 5_666
Mn2 Ca7 3.677(2) 5_656
Mn2 Ca5 3.684(3) .
Mn3 Sb2 2.720(2) 5_666
Mn3 Sb2 2.720(2) 5_656
Mn3 Ca6 2.825(5) 6_657
Mn3 Ca2 3.038(3) 5_666
Mn3 Ca2 3.038(3) 5_656
Mn3 Ca7 3.368(5) .
Mn3 Ca5 3.798(4) 5_666
Mn3 Ca5 3.798(4) 5_656
Mn4 Ca1 2.526(4) 3_556
Mn4 Ca1 2.526(4) 5_556
Mn4 Sb7 2.571(3) 1_455
Mn4 Sb8 2.8216(19) 5_666
Mn4 Sb8 2.8216(19) 5_656
Mn4 Ca4 3.056(4) .
Mn4 Ca1 3.167(4) 5_566
Mn4 Ca1 3.167(4) 3_546
Mn4 Mn5 3.219(4) 1_455
Mn4 Ca3 3.473(4) .
Mn4 Ca2 3.806(3) 5_566
Mn5 Ca1 2.585(4) 3_656
Mn5 Ca1 2.585(4) 5_656
Mn5 Sb1 2.7777(17) 5_666
Mn5 Sb1 2.7778(17) 5_656
Mn5 Sb9A 2.803(4) 1_655
Mn5 Ca9 3.084(4) .
Mn5 Ca1 3.215(4) 5_666
Mn5 Ca1 3.215(4) 3_646
Mn5 Mn4 3.219(4) 1_655
Mn5 Ca8 3.538(4) .
Mn5 Ca5 3.810(3) 5_666
Mn6A Mn6B 1.294(6) .
Mn6A Sb5 2.773(3) 5_666
Mn6A Sb5 2.773(3) 5_656
Mn6A Ca9 3.007(4) 5_666
Mn6A Ca9 3.007(4) 5_656
Mn6A Ca4 3.130(6) .
Mn6A Ca8 3.813(5) 5_666
Mn6A Ca8 3.813(5) 5_656
Mn6B Sb5 2.7581(16) 5_666
Mn6B Sb5 2.7582(16) 5_656
Mn6B Ca8 3.165(3) 5_666
Mn6B Ca8 3.165(3) 5_656
Mn6B Ca8 3.219(4) .
Ca1 Ca1 0.791(7) 7_565
Ca1 Mn4 2.526(4) 5_556
Ca1 Mn5 2.585(4) 5_656
Ca1 Sb9A 2.608(4) 5_556
Ca1 Sb9B 3.075(4) 5_556
Ca1 Mn4 3.167(4) 5_566
Ca1 Sb7 3.192(3) 5_656
Ca1 Sb8 3.210(4) 1_455
Ca1 Mn5 3.215(4) 5_666
Ca1 Sb9A 3.233(3) 5_566
Ca1 Sb9B 3.620(4) 5_566
Ca2 Mn3 3.038(3) 5_666
Ca2 Mn3 3.038(3) 5_656
Ca2 Sb7 3.2363(17) 5_666
Ca2 Sb7 3.2364(17) 5_656
Ca2 Sb4 3.2606(18) 2_564
Ca2 Sb4 3.2606(18) 2_554
Ca2 Sb8 3.398(3) 1_455
Ca2 Mn1 3.742(3) 6_556
Ca2 Mn4 3.806(3) 5_566
Ca2 Mn4 3.806(3) 5_556
Ca2 Ca5 4.043(3) .
Ca3 Sb8 3.1670(17) 5_666
Ca3 Sb8 3.1671(17) 5_656
Ca3 Sb4 3.206(3) 6_557
Ca3 Sb6 3.2345(18) 5_666
Ca3 Sb6 3.2345(18) 5_656
Ca3 Mn2 3.384(2) 5_666
Ca3 Mn2 3.384(2) 5_656
Ca3 Ca6 3.664(4) .
Ca3 Ca7 3.971(3) .
Ca3 Ca2 4.049(3) 5_566
Ca3 Ca2 4.049(3) 5_556
Ca4 Sb8 3.306(2) 5_666
Ca4 Sb8 3.306(2) 5_656
Ca4 Sb5 3.380(2) 5_666
Ca4 Sb5 3.380(2) 5_656
Ca4 Ca8 3.767(4) .
Ca4 Ca1 4.257(4) 3_556
Ca5 Sb7 3.2021(17) 5_666
Ca5 Sb7 3.2021(17) 5_656
Ca5 Sb3 3.3316(17) 5_666
Ca5 Sb3 3.3316(17) 5_656
Ca5 Mn3 3.798(4) 5_666
Ca5 Mn3 3.798(4) 5_656
Ca5 Mn5 3.810(3) 5_666
Ca5 Mn5 3.810(3) 5_656
Ca6 Mn3 2.825(5) 6_557
Ca6 Sb2 3.2358(19) 2_565
Ca6 Sb2 3.2358(19) 2
Ca6 Sb6 3.251(2) 5_666
Ca6 Sb6 3.251(2) 5_656
Ca6 Sb4 3.465(3) 6_557
Ca6 Ca7 4.028(3) 6_557
Ca6 Ca7 4.100(3) .
Ca7 Sb2 3.1891(16) 5_666
Ca7 Sb2 3.1891(16) 5_656
Ca7 Sb6 3.2205(16) 5_666
Ca7 Sb6 3.2206(16) 5_656
Ca7 Mn1 3.345(2) 5_666
Ca7 Mn1 3.345(2) 5_656
Ca7 Mn2 3.677(2) 5_666
Ca7 Mn2 3.677(2) 5_656
Ca7 Ca6 4.028(3) 6_657
Ca8 Mn6B 3.165(3) 5_666
Ca8 Mn6B 3.165(3) 5_656
Ca8 Sb1 3.1732(19) 5_666
Ca8 Sb1 3.1732(19) 5_656
Ca8 Sb5 3.335(2) 5_666
Ca8 Sb5 3.335(2) 5_656
Ca8 Mn6A 3.813(5) 5_666
Ca9 Sb9B 2.909(2) 5_666
Ca9 Sb9B 2.909(2) 5_656
Ca9 Mn6A 3.007(4) 5_666
Ca9 Mn6A 3.007(4) 5_656
Ca9 Sb9A 3.249(4) 1_655
Ca9 Sb9A 3.329(3) 5_666
Ca9 Sb9A 3.329(3) 5_656
Ca9 Sb9B 3.346(4) 1_655
Ca9 Sb1 3.403(2) 5_666
Ca9 Sb1 3.403(2) 5_656
