#------------------------------------------------------------------------------
#$Date: 2019-11-01 20:27:12 +0200 (Fri, 01 Nov 2019) $
#$Revision: 220621 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/59/4345993.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4345993
loop_
_publ_author_name
'Nateghi, Bahareh'
'Domasevitch, Kostiantyn V.'
'Bulánek, Roman'
'Janiak, Christoph'
'Boldog, Ishtvan'
_publ_section_title
;
 Ligand Excess "Inverse-Defected" Zr₆ Tetrahedral
 Tetracarboxylate Framework and Its Thermal Transformation.
;
_journal_issue                   19
_journal_name_full               'Inorganic chemistry'
_journal_page_first              12786
_journal_page_last               12797
_journal_paper_doi               10.1021/acs.inorgchem.9b01721
_journal_volume                  58
_journal_year                    2019
_chemical_formula_sum            'C80 H64 O32 Zr12.8'
_chemical_formula_weight         2705
_space_group_IT_number           87
_space_group_name_Hall           '-I 4'
_space_group_name_H-M_alt        'I 4/m'
_symmetry_cell_setting           tetragonal
_symmetry_Int_Tables_number      87
_symmetry_space_group_name_Hall  '-I 4'
_symmetry_space_group_name_H-M   'I 4/m'
_audit_creation_method           'Jana2006 Version : 25/10/2015'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   17.9142
_cell_length_b                   17.9142
_cell_length_c                   31.5291
_cell_measurement_temperature    293
_cell_volume                     10118.273
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.54051
_exptl_absorpt_coefficient_mu    5.546
_exptl_crystal_density_diffrn    0.8878
_exptl_crystal_F_000             2624
_pd_instr_location               ' ?'
_pd_meas_2theta_range_max        20.007
_pd_meas_2theta_range_min        3.016
_pd_meas_number_of_points        439
_pd_proc_2theta_range_max        20.007
_pd_proc_2theta_range_min        3.016
_pd_proc_ls_background_function  '9 Legendre polynoms'
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function     Lorentzian
_pd_proc_ls_prof_R_factor        0.1189
_pd_proc_ls_prof_wR_expected     0.0195
_pd_proc_ls_prof_wR_factor       0.1502
_refine_ls_goodness_of_fit_all   7.72
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_constraints    104
_refine_ls_number_parameters     10
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1553
_refine_ls_R_factor_gt           0.1553
_refine_ls_shift/su_max          0.0009
_refine_ls_shift/su_mean         0.0001
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.2065
_refine_ls_wR_factor_gt          0.2065
_cod_data_source_file            ic9b01721_si_002.cif
_cod_data_source_block           2_Guest__Rietveld_with_Zr_modelled_guests
_cod_depositor_comments
;
The following automatic conversions were performed:

'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according
to
/home/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_original_cell_volume        10118.3
_cod_database_code               4345993
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,z
3 -y,x,z
4 y,-x,z
5 -x,-y,-z
6 x,y,-z
7 y,-x,-z
8 -y,x,-z
9 x+1/2,y+1/2,z+1/2
10 -x+1/2,-y+1/2,z+1/2
11 -y+1/2,x+1/2,z+1/2
12 y+1/2,-x+1/2,z+1/2
13 -x+1/2,-y+1/2,-z+1/2
14 x+1/2,y+1/2,-z+1/2
15 y+1/2,-x+1/2,-z+1/2
16 -y+1/2,x+1/2,-z+1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
C1 C 0.1727 0.0456 0.1014 Uiso 0.05 16 1 d
C2 C 0.2356 0.03579 0.13476 Uiso 0.05 16 1 d
C3 C 0.22071 0.02265 0.17742 Uiso 0.05 16 1 d
C4 C 0.28174 0.01339 0.20559 Uiso 0.05 16 1 d
C5 C 0.35789 0.01735 0.19118 Uiso 0.05 16 1 d
C6 C 0.37293 0.03062 0.1486 Uiso 0.05 16 1 d
C7 C 0.31178 0.03985 0.12033 Uiso 0.05 16 1 d
C8 C 0.4257 0.00733 0.22168 Uiso 0.05 16 1 d
C9 C 0.42197 -0.06342 0.25053 Uiso 0.05 16 1 d
H9a H 0.37795 -0.05834 0.2684 Uiso 0.06 16 1 d
H9b H 0.41635 -0.10814 0.23323 Uiso 0.06 16 1 d
C10 C 0.5 0 0.1952 Uiso 0.05 8 2 d
H10a H 0.49559 -0.04472 0.17779 Uiso 0.06 16 1 d
H10b H 0.50441 0.04472 0.17779 Uiso 0.06 16 1 d
H3 H 0.16865 0.01989 0.18723 Uiso 0.05 16 1 d
H4 H 0.27156 0.00428 0.23482 Uiso 0.05 16 1 d
H6 H 0.42497 0.03332 0.13869 Uiso 0.05 16 1 d
H7 H 0.32203 0.04883 0.09113 Uiso 0.05 16 1 d
O1a O -0.076 0.0387 0.0328 Uiso 0.05 16 0.5 d
O1b O -0.1056 0.0536 0.042 Uiso 0.05 16 0.5 d
O2 O 0.1046 0.0307 0.1134 Uiso 0.05 16 1 d
O3 O 0.1929 0.0622 0.0647 Uiso 0.05 16 1 d
O4 O 0.1922 0.1605 0 Uiso 0.05 8 1 d
O5 O 0.2496 -0.0179 0 Uiso 0.05 8 1 d
Zr1 Zr 0 0 0.0777 Uiso 0.05 4 1 d
Zr2 Zr 0.138 0.0456 0 Uiso 0.05 8 1 d
Zr11 Zr 0.5 0 0 Uiso 0.05 4 1 d
Zr12 Zr 0.4 0 0 Uiso 0.05 8 1 d
Zr13 Zr 0.5 0.1 0 Uiso 0.05 8 0.2 d
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 0.0191 0.0095 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
O 0.0516 0.0335 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Zr -0.1709 2.2794 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
C1 C2 . 1.5551
C1 O2 . 1.304
C1 O3 . 1.2552
C2 C3 . 1.3998
C2 C7 . 1.4396
C3 C4 . 1.4209
C3 H3 . 0.9833
C4 C5 . 1.4388
C4 H4 . 0.9593
C5 C6 . 1.3982
C5 C8 . 1.5624
C6 C7 . 1.4245
C6 H6 . 0.9839
C7 H7 . 0.9583
C8 C9 . 1.5637
C8 C9 15_555 1.5543
C9 H9a . 0.9748
C9 H9b . 0.9756
C10 H10a . 0.9755
C10 H10a 2_655 0.9755
H6 Zr17 . 1.9144
O1a O1b . 0.6609
O1a Zr1 . 2.0878
O1a Zr2 3_555 2.1297
Zr11 Zr12 . 1.7891
Zr11 Zr12 2_655 1.7891
Zr11 Zr17 . 3.1738
Zr11 Zr17 5_655 3.1738
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
C6 H6 C10 0.98 2.32 2.7669 106.74
C6 H6 Zr17 0.98 1.91 2.8014 148.57
C7 H7 O3 0.96 2.47 2.7930 99.54
loop_
_pd_proc_point_id
_pd_proc_2theta_corrected
_pd_proc_intensity_net
_pd_calc_intensity_net
_pd_proc_ls_weight
1 3.0160 3976.73 4058.33 63.06
2 3.0420 3944.68 3999.87 62.81
3 3.0550 3918.11 3971.37 62.59
4 3.0810 3860.41 3915.78 62.13
5 3.0940 3807.50 3888.68 61.70
6 3.1330 3754.63 3810.11 61.28
7 3.1720 3699.93 3735.47 60.83
8 3.2110 3635.99 3664.61 60.30
9 3.2500 3578.29 3597.36 59.82
10 3.2890 3517.11 3533.57 59.31
11 3.3280 3465.01 3473.08 58.86
12 3.3670 3412.59 3415.76 58.42
13 3.4060 3368.36 3361.46 58.04
14 3.4450 3319.35 3310.04 57.61
15 3.4840 3273.45 3261.38 57.21
16 3.5230 3227.00 3215.35 56.81
17 3.5620 3191.37 3171.82 56.49
18 3.6010 3157.43 3130.67 56.19
19 3.6400 3123.37 3091.79 55.89
20 3.6790 3090.32 3055.06 55.59
21 3.7180 3058.75 3020.38 55.31
22 3.7570 3032.17 2987.65 55.07
23 3.7960 3011.12 2956.76 54.87
24 3.8350 3005.87 2927.62 54.83
25 3.8740 2999.35 2900.13 54.77
26 3.9130 2988.09 2874.21 54.66
27 3.9520 2962.88 2849.76 54.43
28 3.9910 2935.92 2826.71 54.18
29 4.0300 2895.16 2804.97 53.81
30 4.0690 2849.35 2784.46 53.38
31 4.1080 2812.87 2765.12 53.04
32 4.1470 2785.88 2746.87 52.78
33 4.1860 2765.73 2754.15 52.59
34 4.2250 2748.25 2879.37 52.42
35 4.2640 2740.95 2873.37 52.35
36 4.3030 2738.87 2869.01 52.33
37 4.3420 2744.16 2866.34 52.38
38 4.3810 2749.75 2865.41 52.44
39 4.4200 2766.17 2866.30 52.59
40 4.4590 2788.55 2869.12 52.81
41 4.4980 2824.31 2873.98 53.14
42 4.5370 2862.03 2881.06 53.50
43 4.5760 2906.29 2890.55 53.91
44 4.6150 2954.98 2902.71 54.36
45 4.6540 3006.79 2917.83 54.83
46 4.6930 3054.55 2936.31 55.27
47 4.7320 3094.84 2958.62 55.63
48 4.7710 3137.12 2985.35 56.01
49 4.8100 3180.45 3017.22 56.40
50 4.8490 3233.93 3055.15 56.87
51 4.8880 3286.27 3100.32 57.33
52 4.9270 3351.57 3154.20 57.89
53 4.9660 3425.89 3218.69 58.53
54 5.0050 3518.21 3296.30 59.31
55 5.0440 3599.93 3390.30 60.00
56 5.0830 3665.47 3505.09 60.54
57 5.1220 3729.29 3646.68 61.07
58 5.1610 3792.35 3823.38 61.58
59 5.2000 3884.12 4047.03 62.32
60 5.2390 4011.60 4334.79 63.34
61 5.2780 4241.61 4716.15 65.13
62 5.3170 4591.32 5223.36 67.76
63 5.3560 5171.83 5923.39 71.92
64 5.3950 6089.49 6921.51 78.04
65 5.4340 7657.71 8399.57 87.51
66 5.4730 10478.20 10680.30 102.36
67 5.5120 15717.10 14322.70 125.37
68 5.5510 24461.90 20105.10 156.40
69 5.5900 34747.90 28285.10 186.41
70 5.6290 42577.70 37143.30 206.34
71 5.6680 44866.20 41164.10 211.82
72 5.7070 41289.20 34737.40 203.20
73 5.7460 32853.70 24558.90 181.26
74 5.7850 22163.90 16977.10 148.88
75 5.8240 13029.00 12265.40 114.14
76 5.8630 7930.07 9368.14 89.05
77 5.9020 6036.47 7521.66 77.69
78 5.9410 5166.61 6292.03 71.88
79 5.9800 4568.31 5438.69 67.59
80 6.0190 4136.53 4824.62 64.32
81 6.0580 3836.35 4368.73 61.94
82 6.0970 3619.23 4021.05 60.16
83 6.1360 3468.54 3749.67 58.89
84 6.1750 3344.27 3533.55 57.83
85 6.2140 3249.15 3358.39 57.00
86 6.2530 3164.74 3214.23 56.26
87 6.2920 3101.64 3094.01 55.69
88 6.3310 3043.68 2992.61 55.17
89 6.3700 2993.63 2906.29 54.71
90 6.4090 2939.89 2832.28 54.22
91 6.4480 2878.27 2768.58 53.65
92 6.4870 2818.13 2713.72 53.09
93 6.5260 2756.01 2666.74 52.50
94 6.5650 2703.79 2627.13 52.00
95 6.6040 2653.21 2594.85 51.51
96 6.6430 2611.69 2570.47 51.10
97 6.6820 2564.07 2555.35 50.64
98 6.7210 2515.02 2552.18 50.15
99 6.7600 2462.50 2565.74 49.62
100 6.7990 2414.53 2604.30 49.14
101 6.8380 2375.99 2681.18 48.74
102 6.8770 2344.88 2817.24 48.42
103 6.9160 2315.43 3002.65 48.12
104 6.9550 2286.27 3156.24 47.81
105 6.9940 2260.30 3118.83 47.54
106 7.0330 2237.34 2904.98 47.30
107 7.0720 2210.25 2652.43 47.01
108 7.1110 2188.73 2479.40 46.78
109 7.1500 2169.99 2225.38 46.58
110 7.1890 2161.47 2146.63 46.49
111 7.2280 2154.20 2089.63 46.41
112 7.2670 2149.54 2046.28 46.36
113 7.3060 2142.69 2011.74 46.29
114 7.3450 2138.74 1983.04 46.25
115 7.3840 2136.97 1958.34 46.23
116 7.4230 2129.42 1936.47 46.15
117 7.4620 2119.65 1916.66 46.04
118 7.5010 2108.98 1899.77 45.92
119 7.5400 2095.85 1882.70 45.78
120 7.5790 2075.92 1866.55 45.56
121 7.6180 2053.76 1873.71 45.32
122 7.6570 2037.98 1859.70 45.14
123 7.6960 2023.91 1846.25 44.99
124 7.7350 2019.67 1833.29 44.94
125 7.7740 2016.69 1820.78 44.91
126 7.8130 2022.03 1808.68 44.97
127 7.8520 2025.93 1796.98 45.01
128 7.8910 2035.09 1785.67 45.11
129 7.9300 2032.11 1774.75 45.08
130 7.9690 2029.38 1764.23 45.05
131 8.0080 2026.51 1754.14 45.02
132 8.0470 2028.67 1744.49 45.04
133 8.0860 2026.01 1735.32 45.01
134 8.1250 2031.69 1726.68 45.07
135 8.1640 2037.84 1718.63 45.14
136 8.2030 2040.05 1711.24 45.17
137 8.2420 2030.99 1704.61 45.07
138 8.2810 2026.17 1698.87 45.01
139 8.3200 2019.74 1694.16 44.94
140 8.3590 2016.25 1690.70 44.90
141 8.3980 2012.89 1688.74 44.87
142 8.4370 2020.22 1688.65 44.95
143 8.4760 2023.79 1690.92 44.99
144 8.5150 2027.65 1696.22 45.03
145 8.5540 2026.01 1705.50 45.01
146 8.5930 2028.53 1720.12 45.04
147 8.6320 2028.59 1742.11 45.04
148 8.6710 2030.00 1777.51 45.06
149 8.7100 2032.54 1821.32 45.08
150 8.7490 2035.23 1890.63 45.11
151 8.7880 2036.66 1994.15 45.13
152 8.8270 2038.93 2137.27 45.15
153 8.8660 2042.83 2322.53 45.20
154 8.9050 2046.02 2513.58 45.23
155 8.9440 2051.39 2613.97 45.29
156 8.9830 2059.68 2548.27 45.38
157 9.0220 2064.40 2371.31 45.44
158 9.0610 2061.98 2186.62 45.41
159 9.1000 2057.01 2043.27 45.35
160 9.1390 2056.65 1945.43 45.35
161 9.1780 2055.39 1883.97 45.34
162 9.2170 2056.15 1849.85 45.34
163 9.2560 2055.65 1836.96 45.34
164 9.2950 2056.61 1841.90 45.35
165 9.3340 2050.75 1863.48 45.29
166 9.3730 2047.72 1902.30 45.25
167 9.4120 2048.45 1960.69 45.26
168 9.4510 2066.06 2042.98 45.45
169 9.4900 2091.13 2156.04 45.73
170 9.5290 2128.90 2310.32 46.14
171 9.5680 2181.15 2521.32 46.70
172 9.6070 2288.90 2811.28 47.84
173 9.6460 2517.02 3209.96 50.17
174 9.6850 2971.49 3750.82 54.51
175 9.7240 3683.46 4458.11 60.69
176 9.7630 4574.46 5324.71 67.63
177 9.8020 5331.74 6258.09 73.02
178 9.8410 5688.64 6964.23 75.42
179 9.8800 5501.49 7018.65 74.17
180 9.9190 4882.67 6344.06 69.88
181 9.9580 4013.64 5336.87 63.35
182 9.9970 3197.23 4385.23 56.54
183 10.0360 2632.93 3632.98 51.31
184 10.0750 2364.25 3076.36 48.62
185 10.1140 2249.87 2670.74 47.43
186 10.1530 2178.97 2373.19 46.68
187 10.1920 2123.83 2151.54 46.08
188 10.2310 2073.53 1983.43 45.54
189 10.2700 2029.39 1853.63 45.05
190 10.3090 1988.70 1754.76 44.59
191 10.3480 1953.09 1673.75 44.19
192 10.3870 1915.55 1608.51 43.77
193 10.4260 1885.03 1555.53 43.42
194 10.4650 1854.87 1512.27 43.07
195 10.5040 1824.69 1476.94 42.72
196 10.5430 1790.11 1448.25 42.31
197 10.5820 1759.84 1425.31 41.95
198 10.6210 1732.03 1407.53 41.62
199 10.6600 1706.93 1394.60 41.31
200 10.6990 1684.73 1386.46 41.05
201 10.7380 1665.46 1383.29 40.81
202 10.7770 1649.19 1385.55 40.61
203 10.8160 1630.88 1394.93 40.38
204 10.8550 1617.02 1411.05 40.21
205 10.8940 1602.71 1436.82 40.03
206 10.9330 1592.69 1474.72 39.91
207 10.9720 1578.10 1528.87 39.73
208 11.0110 1571.11 1604.67 39.64
209 11.0500 1562.56 1708.66 39.53
210 11.0890 1557.66 1842.68 39.47
211 11.1280 1550.88 2013.66 39.38
212 11.1670 1554.75 2198.80 39.43
213 11.2060 1571.16 2358.15 39.64
214 11.2450 1607.79 2456.93 40.10
215 11.2840 1655.15 2495.51 40.68
216 11.3230 1698.57 2482.74 41.21
217 11.3620 1724.91 2402.76 41.53
218 11.4010 1716.45 2246.60 41.43
219 11.4400 1676.94 2045.70 40.95
220 11.4790 1612.83 1846.26 40.16
221 11.5180 1550.54 1675.77 39.38
222 11.5570 1498.47 1540.35 38.71
223 11.5960 1459.82 1435.65 38.21
224 11.6350 1429.37 1355.02 37.81
225 11.6740 1407.47 1294.03 37.52
226 11.7130 1389.49 1244.34 37.28
227 11.7520 1369.63 1204.41 37.01
228 11.7910 1355.03 1173.95 36.81
229 11.8300 1340.81 1146.91 36.62
230 11.8690 1329.16 1124.15 36.46
231 11.9080 1317.49 1104.75 36.30
232 11.9470 1312.81 1088.03 36.23
233 11.9860 1311.04 1073.47 36.21
234 12.0250 1309.75 1059.33 36.19
235 12.0640 1302.05 1048.09 36.08
236 12.1030 1293.12 1038.12 35.96
237 12.1420 1276.85 1029.24 35.73
238 12.1810 1259.81 1000.05 35.49
239 12.2200 1246.24 995.37 35.30
240 12.2590 1239.57 989.87 35.21
241 12.2980 1231.17 985.10 35.09
242 12.3370 1225.28 981.06 35.00
243 12.3760 1222.25 977.74 34.96
244 12.4150 1221.52 975.16 34.95
245 12.4540 1218.49 973.35 34.91
246 12.4930 1213.51 972.41 34.84
247 12.5320 1207.35 972.40 34.75
248 12.5710 1199.89 973.48 34.64
249 12.6100 1190.67 975.81 34.51
250 12.6490 1187.11 979.63 34.45
251 12.6880 1183.71 985.26 34.40
252 12.7270 1185.78 993.11 34.44
253 12.7660 1185.27 1003.75 34.43
254 12.8050 1188.26 1017.94 34.47
255 12.8440 1184.54 1036.69 34.42
256 12.8830 1184.49 1061.39 34.42
257 12.9220 1175.28 1093.89 34.28
258 12.9610 1172.31 1136.55 34.24
259 13.0000 1166.73 1192.24 34.16
260 13.0390 1167.93 1264.02 34.17
261 13.0780 1164.96 1352.25 34.13
262 13.1170 1166.37 1452.54 34.15
263 13.1560 1161.05 1549.06 34.07
264 13.1950 1153.51 1613.60 33.96
265 13.2340 1145.73 1620.08 33.85
266 13.2730 1146.60 1564.01 33.86
267 13.3120 1150.21 1470.39 33.91
268 13.3510 1149.41 1368.94 33.90
269 13.3900 1147.93 1278.31 33.88
270 13.4290 1145.67 1204.71 33.85
271 13.4680 1141.53 1148.27 33.79
272 13.5070 1138.49 1106.72 33.74
273 13.5460 1140.27 1077.60 33.77
274 13.5850 1144.97 1058.98 33.84
275 13.6240 1145.21 1049.64 33.84
276 13.6630 1142.55 1048.95 33.80
277 13.7020 1140.80 1056.62 33.78
278 13.7410 1142.40 1072.21 33.80
279 13.7800 1143.06 1091.06 33.81
280 13.8190 1144.47 1114.97 33.83
281 13.8580 1144.67 1133.40 33.83
282 13.8970 1140.21 1138.31 33.77
283 13.9360 1135.97 1123.50 33.70
284 13.9620 1129.51 1107.83 33.61
285 14.0010 1131.12 1077.14 33.63
286 14.0400 1132.66 1045.90 33.65
287 14.0790 1144.67 1017.69 33.83
288 14.1180 1153.23 994.07 33.96
289 14.1570 1161.73 976.08 34.08
290 14.1960 1162.32 963.49 34.09
291 14.2350 1167.55 955.29 34.17
292 14.2740 1166.59 951.04 34.16
293 14.3130 1165.10 950.32 34.13
294 14.3520 1164.85 953.95 34.13
295 14.3910 1167.20 959.71 34.16
296 14.4300 1168.75 968.78 34.19
297 14.4690 1167.73 981.42 34.17
298 14.5080 1170.12 998.13 34.21
299 14.5470 1174.49 1019.62 34.27
300 14.5860 1175.92 1046.89 34.29
301 14.6250 1178.54 1081.25 34.33
302 14.6640 1183.93 1124.43 34.41
303 14.7030 1189.27 1178.49 34.49
304 14.7420 1192.52 1245.69 34.53
305 14.7810 1199.98 1327.84 34.64
306 14.8200 1205.23 1425.10 34.72
307 14.8590 1210.34 1533.90 34.79
308 14.8980 1218.76 1644.91 34.91
309 14.9370 1237.71 1743.43 35.18
310 14.9760 1261.64 1814.26 35.52
311 15.0150 1287.59 1847.79 35.88
312 15.0540 1307.26 1840.77 36.16
313 15.0930 1316.26 1794.37 36.28
314 15.1320 1307.13 1716.27 36.15
315 15.1710 1286.81 1623.19 35.87
316 15.2100 1264.61 1529.14 35.56
317 15.2490 1246.40 1447.59 35.30
318 15.2880 1236.70 1384.13 35.17
319 15.3270 1233.62 1340.00 35.12
320 15.3660 1235.25 1314.44 35.15
321 15.4050 1235.43 1306.53 35.15
322 15.4440 1239.14 1313.98 35.20
323 15.4830 1238.23 1334.79 35.19
324 15.5220 1235.87 1364.45 35.15
325 15.5610 1229.77 1395.29 35.07
326 15.6000 1224.64 1414.47 34.99
327 15.6390 1221.47 1412.15 34.95
328 15.6780 1222.37 1385.37 34.96
329 15.7170 1231.19 1340.60 35.09
330 15.7560 1244.75 1288.59 35.28
331 15.7950 1258.55 1238.23 35.48
332 15.8340 1265.87 1194.29 35.58
333 15.8730 1267.59 1158.23 35.60
334 15.9120 1265.48 1129.76 35.57
335 15.9510 1259.75 1107.90 35.49
336 15.9900 1257.27 1091.59 35.46
337 16.0290 1257.35 1079.76 35.46
338 16.0680 1264.15 1071.68 35.55
339 16.1070 1275.43 1066.78 35.71
340 16.1460 1287.20 1064.57 35.88
341 16.1850 1295.57 1061.91 35.99
342 16.2240 1299.49 1065.24 36.05
343 16.2630 1302.23 1070.02 36.09
344 16.3020 1299.43 1077.04 36.05
345 16.3410 1290.90 1086.43 35.93
346 16.3800 1281.97 1098.37 35.80
347 16.4190 1278.45 1113.07 35.76
348 16.4580 1277.59 1130.61 35.74
349 16.4970 1274.35 1150.80 35.70
350 16.5360 1276.84 1172.94 35.73
351 16.5750 1281.76 1195.84 35.80
352 16.6140 1287.10 1218.32 35.88
353 16.6530 1288.39 1239.98 35.89
354 16.6920 1290.43 1261.40 35.92
355 16.7310 1290.62 1283.19 35.93
356 16.7700 1293.06 1304.48 35.96
357 16.8090 1291.37 1322.28 35.94
358 16.8480 1292.67 1332.47 35.95
359 16.8870 1291.49 1332.43 35.94
360 16.9260 1297.73 1322.92 36.02
361 16.9650 1302.79 1306.60 36.09
362 17.0040 1314.23 1288.92 36.25
363 17.0430 1321.46 1271.39 36.35
364 17.0820 1324.76 1254.82 36.40
365 17.1210 1321.62 1239.95 36.35
366 17.1600 1316.21 1227.13 36.28
367 17.1990 1312.64 1216.76 36.23
368 17.2380 1306.44 1209.18 36.14
369 17.2770 1309.72 1204.44 36.19
370 17.3160 1316.53 1202.46 36.28
371 17.3550 1322.45 1203.08 36.37
372 17.3940 1319.19 1206.20 36.32
373 17.4330 1316.42 1211.99 36.28
374 17.4720 1313.60 1220.27 36.24
375 17.5110 1312.43 1231.16 36.23
376 17.5500 1313.12 1245.09 36.24
377 17.5890 1316.60 1262.49 36.28
378 17.6280 1317.76 1283.86 36.30
379 17.6670 1314.63 1309.69 36.26
380 17.7060 1309.45 1340.31 36.19
381 17.7450 1307.34 1375.88 36.16
382 17.7840 1305.45 1414.49 36.13
383 17.8230 1313.14 1454.01 36.24
384 17.8620 1320.13 1490.26 36.33
385 17.9010 1328.16 1519.09 36.44
386 17.9400 1329.49 1537.68 36.46
387 17.9790 1334.85 1545.81 36.54
388 18.0180 1337.15 1546.35 36.57
389 18.0570 1343.29 1542.76 36.65
390 18.0960 1349.21 1538.70 36.73
391 18.1350 1359.25 1535.85 36.87
392 18.1740 1367.55 1534.16 36.98
393 18.2130 1371.13 1528.80 37.03
394 18.2520 1372.29 1514.41 37.04
395 18.2910 1366.89 1492.06 36.97
396 18.3300 1361.10 1460.41 36.89
397 18.3690 1352.83 1422.48 36.78
398 18.4080 1352.81 1382.09 36.78
399 18.4470 1352.13 1345.50 36.77
400 18.4860 1353.41 1312.99 36.79
401 18.5250 1350.36 1285.28 36.75
402 18.5640 1348.83 1262.33 36.73
403 18.6030 1346.38 1243.78 36.69
404 18.6420 1344.86 1229.41 36.67
405 18.6810 1348.79 1218.40 36.73
406 18.7200 1356.08 1210.68 36.83
407 18.7590 1361.08 1206.10 36.89
408 18.7980 1358.46 1204.62 36.86
409 18.8370 1355.86 1206.42 36.82
410 18.8760 1352.85 1211.58 36.78
411 18.9150 1352.53 1220.53 36.78
412 18.9540 1351.21 1233.72 36.76
413 18.9930 1351.57 1251.64 36.76
414 19.0320 1352.35 1274.69 36.77
415 19.0710 1354.71 1301.35 36.81
416 19.1100 1356.10 1334.27 36.83
417 19.1490 1356.00 1369.89 36.82
418 19.1880 1351.45 1404.64 36.76
419 19.2270 1346.98 1433.40 36.70
420 19.2660 1338.17 1450.96 36.58
421 19.3050 1329.51 1454.38 36.46
422 19.3440 1317.77 1444.67 36.30
423 19.3830 1311.53 1426.31 36.22
424 19.4220 1310.54 1404.86 36.20
425 19.4610 1317.25 1384.92 36.29
426 19.5000 1322.43 1368.29 36.37
427 19.5390 1329.19 1355.55 36.46
428 19.5780 1332.59 1346.11 36.50
429 19.6170 1328.33 1339.81 36.45
430 19.6560 1315.60 1335.14 36.27
431 19.6950 1303.87 1332.17 36.11
432 19.7340 1302.13 1328.57 36.08
433 19.7730 1308.18 1322.71 36.17
434 19.8120 1316.35 1312.83 36.28
435 19.8510 1327.42 1298.48 36.43
436 19.8900 1334.59 1280.99 36.53
437 19.9290 1330.05 1262.76 36.47
438 19.9680 1314.67 1246.54 36.26
439 20.0070 1296.04 1233.75 36.00
loop_
_pd_proc_info_excluded_regions
'from -203.013 to -204.500'
