#------------------------------------------------------------------------------
#$Date: 2019-11-23 06:11:59 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232303 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/73/4347394.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347394
loop_
_publ_author_name
'Giansiracusa, Marcus J.'
'Vonci, Michele'
'Van den Heuvel, Willem'
'Gable, Robert W.'
'Moubaraki, Boujemaa'
'Murray, Keith S.'
'Yu, Dehong'
'Mole, Richard A.'
'Soncini, Alessandro'
'Boskovic, Colette'
_publ_section_title
;
 Carbonate-Bridged Lanthanoid Triangles: Single-Molecule Magnet Behavior,
 Inelastic Neutron Scattering, and Ab Initio Studies.
;
_journal_issue                   11
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5201
_journal_page_last               5214
_journal_paper_doi               10.1021/acs.inorgchem.6b00108
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C Na11 O104.25 P2 Tb3 W18, 10.63(O)'
_chemical_formula_sum            'C H84 Na11 O116 P2 Tb3 W18'
_chemical_formula_weight         6053.57
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_audit_creation_date             2015-12-16
_audit_creation_method
;
Olex2 1.2
(compiled 2015.09.30 svn.r3233 for OlexSys, GUI svn.r5103)
;
_cell_angle_alpha                90
_cell_angle_beta                 111.6016(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.38631(15)
_cell_length_b                   26.04125(18)
_cell_length_c                   23.4293(2)
_cell_measurement_reflns_used    23422
_cell_measurement_temperature    130.01(10)
_cell_measurement_theta_max      73.4620
_cell_measurement_theta_min      3.9240
_cell_volume                     9862.85(15)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      130.01(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 10.2273
_diffrn_detector_type            Atlas
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
  1 omega  -44.00   12.00   1.0000    2.5000
omega____ theta____ kappa____ phi______ frames
    -      -42.1173   37.0000  -90.0000 56

#__ type_ start__ end____ width___ exp.time_
  2 omega  -31.00   10.00   1.0000    2.5000
omega____ theta____ kappa____ phi______ frames
    -      -42.1173   37.0000   90.0000 41

#__ type_ start__ end____ width___ exp.time_
  3 omega   32.00   84.00   1.0000    2.5000
omega____ theta____ kappa____ phi______ frames
    -       42.1173 -125.0000   30.0000 52

#__ type_ start__ end____ width___ exp.time_
  4 omega   31.00  127.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -77.0000  -60.0000 96

#__ type_ start__ end____ width___ exp.time_
  5 omega   94.00  122.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158 -125.0000   60.0000 28

#__ type_ start__ end____ width___ exp.time_
  6 omega   51.00   97.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -94.0000  -90.0000 46

#__ type_ start__ end____ width___ exp.time_
  7 omega   34.00   83.00   1.0000    2.5000
omega____ theta____ kappa____ phi______ frames
    -       42.1173 -125.0000 -150.0000 49

#__ type_ start__ end____ width___ exp.time_
  8 omega   29.00  102.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -94.0000 -150.0000 73

#__ type_ start__ end____ width___ exp.time_
  9 omega   29.00   83.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -30.0000  -60.0000 54

#__ type_ start__ end____ width___ exp.time_
 10 omega   54.00  138.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158   15.0000    0.0000 84

#__ type_ start__ end____ width___ exp.time_
 11 omega   76.00  166.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158   30.0000 -150.0000 90

#__ type_ start__ end____ width___ exp.time_
 12 omega   94.00  175.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  125.0000 -150.0000 81

#__ type_ start__ end____ width___ exp.time_
 13 omega   28.00   68.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -30.0000    0.0000 40

#__ type_ start__ end____ width___ exp.time_
 14 omega   30.00   87.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -30.0000   60.0000 57

#__ type_ start__ end____ width___ exp.time_
 15 omega   47.00   97.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -94.0000  150.0000 50

#__ type_ start__ end____ width___ exp.time_
 16 omega   28.00   89.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      104.6158  -30.0000 -180.0000 61

#__ type_ start__ end____ width___ exp.time_
 17 omega -117.00   24.00   1.0000    2.5000
omega____ theta____ kappa____ phi______ frames
    -      -42.1173    0.0000 -120.0000 141
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      -0.0152321000
_diffrn_orient_matrix_UB_12      0.0425053000
_diffrn_orient_matrix_UB_13      -0.0486833000
_diffrn_orient_matrix_UB_21      -0.0638367000
_diffrn_orient_matrix_UB_22      -0.0344873000
_diffrn_orient_matrix_UB_23      -0.0477136000
_diffrn_orient_matrix_UB_31      -0.0690713000
_diffrn_orient_matrix_UB_32      0.0224865000
_diffrn_orient_matrix_UB_33      0.0188637000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0512
_diffrn_reflns_av_unetI/netI     0.0466
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            69343
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         73.630
_diffrn_reflns_theta_min         3.955
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_type              'SuperNova (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    50.014
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.47886
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    4.077
_exptl_crystal_description       'Hexagonal faceted rod'
_exptl_crystal_F_000             10784
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.11
_refine_diff_density_max         2.623
_refine_diff_density_min         -1.430
_refine_diff_density_rms         0.252
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1346
_refine_ls_number_reflns         19554
_refine_ls_number_restraints     33
_refine_ls_restrained_S_all      1.065
_refine_ls_R_factor_all          0.0382
_refine_ls_R_factor_gt           0.0315
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0252P)²+21.3118P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0693
_refine_ls_wR_factor_ref         0.0723
_reflns_Friedel_coverage         0.000
_reflns_number_gt                17245
_reflns_number_total             19554
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic6b00108_si_002.cif
_cod_data_source_block           mjg1_138_tb_abs
_cod_original_cell_volume        9862.84(15)
_cod_database_code               4347394
_chemical_oxdiff_formula         'Tb3 W18 O74 P2 Na11'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_reflns_odcompleteness_completeness 99.96
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.49
_olex2_refinement_description
;
1. Uiso/Uaniso restraints and constraints
Uanis(O5) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.01
Uanis(O8) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(O10) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(O26) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(W3A) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uiso(O90) = Uiso(O90A) = Uiso(O89)
Uanis(O91) = Uanis(O91A)
Uanis(O92) = Uanis(O92A)
Uanis(O93) = Uanis(O93A)
Uanis(Na8) = Uanis(Na8A)
Uanis(Na9) = Uanis(O9A)
2. Others
 1*[Sof(Na8)]+1*[Sof(Na8A)]+1*[Sof(Na9)]+1*[Sof(Na1)]=2 with esd of 0.001
 1*[Sof(Na8)]+1*[Sof(Na9)]=1 with esd of 0.001
 1*[Sof(O121)]+1*[Sof(O107)]+1*[Sof(O9A)]+1*[Sof(O89)]=2 with esd of 0.001
 Sof(O90A)=1-FVAR(1)
 Sof(O90)=FVAR(1)
 Sof(O91A)=1-FVAR(2)
 Sof(O91)=FVAR(2)
 Sof(O92A)=1-FVAR(3)
 Sof(O92)=FVAR(3)
 Sof(O93A)=1-FVAR(4)
 Sof(O93)=FVAR(4)
 Sof(W1A)=Sof(W2A)=Sof(W3A)=1-FVAR(6)
 Sof(W1)=Sof(W2)=Sof(W3)=Sof(O70)=Sof(O72)=Sof(O74)=FVAR(6)
;
_shelx_shelxl_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.27527(2) 0.31288(2) 0.21210(2) 0.01433(9) Uani 0.9600(11) 1 d . P A 1
W1A W 0.2676(7) 0.2784(4) 0.2860(4) 0.018(2) Uani 0.0400(11) 1 d . P A 2
W2 W 0.30524(2) 0.30555(2) 0.36435(2) 0.01508(9) Uani 0.9600(11) 1 d . P A 1
W2A W 0.3643(5) 0.3755(4) 0.3844(4) 0.018(2) Uani 0.0400(11) 1 d . P A 2
W3 W 0.37770(2) 0.40873(2) 0.31031(2) 0.01541(9) Uani 0.9600(11) 1 d . P A 1
W3A W 0.3398(6) 0.3825(5) 0.2328(5) 0.018(2) Uani 0.0400(11) 1 d U P A 2
W4 W 0.04955(2) 0.29454(2) 0.17169(2) 0.01370(7) Uani 1 1 d . . . .
W5 W 0.07759(2) 0.28831(2) 0.32237(2) 0.01455(7) Uani 1 1 d . . . .
W6 W 0.12468(2) 0.40903(2) 0.11317(2) 0.01321(7) Uani 1 1 d . . . .
W7 W 0.18740(2) 0.39416(2) 0.42790(2) 0.01486(7) Uani 1 1 d . . . .
W8 W 0.22731(2) 0.50423(2) 0.21173(2) 0.01396(7) Uani 1 1 d . . . .
W9 W 0.26022(2) 0.49613(2) 0.37712(2) 0.01511(7) Uani 1 1 d . . . .
W10 W -0.31359(2) 0.42000(2) 0.11677(2) 0.01268(7) Uani 1 1 d . . . .
W11 W -0.28656(2) 0.41244(2) 0.26794(2) 0.01344(7) Uani 1 1 d . . . .
W12 W -0.23894(2) 0.53293(2) 0.05624(2) 0.01228(7) Uani 1 1 d . . . .
W13 W -0.17730(2) 0.51828(2) 0.37310(2) 0.01390(7) Uani 1 1 d . . . .
W14 W -0.13984(2) 0.62808(2) 0.15261(2) 0.01368(7) Uani 1 1 d . . . .
W15 W -0.10637(2) 0.62101(2) 0.31840(2) 0.01441(7) Uani 1 1 d . . . .
W16 W -0.41967(2) 0.54580(2) 0.10445(2) 0.01267(7) Uani 1 1 d . . . .
W17 W -0.39052(2) 0.53911(2) 0.25664(2) 0.01330(7) Uani 1 1 d . . . .
W18 W -0.31982(2) 0.64274(2) 0.20156(2) 0.01331(7) Uani 1 1 d . . . .
Tb1 Tb -0.10754(3) 0.36405(2) 0.22371(2) 0.01382(9) Uani 1 1 d . . . .
Tb2 Tb 0.03267(3) 0.50314(2) 0.36095(2) 0.01398(9) Uani 1 1 d . . . .
Tb3 Tb -0.00895(3) 0.51258(2) 0.14502(2) 0.01386(9) Uani 1 1 d . . . .
P1 P -0.21791(10) 0.52406(7) 0.21312(9) 0.0109(3) Uani 1 1 d . . . .
P2 P 0.16144(11) 0.39491(8) 0.27225(9) 0.0121(3) Uani 1 1 d . . . .
Na1 Na 0.6183(4) 0.3879(3) 0.3905(4) 0.042(2) Uani 0.624(11) 1 d . P A .
Na2 Na -0.48516(18) 0.43220(14) 0.16022(15) 0.0199(7) Uani 1 1 d . . . .
Na3 Na -0.1972(3) 0.75891(19) 0.0767(2) 0.0435(10) Uani 1 1 d . . . .
Na4 Na -0.5883(2) 0.31833(16) 0.06955(18) 0.0301(8) Uani 1 1 d . . . .
Na5 Na -0.1359(2) 0.73888(16) 0.41124(18) 0.0303(8) Uani 1 1 d . . . .
Na6 Na 0.4038(2) 0.55337(15) 0.16863(19) 0.0279(8) Uani 1 1 d . . . .
Na7 Na 0.2104(2) 0.61503(15) 0.05058(18) 0.0277(8) Uani 1 1 d . . . .
Na8 Na -0.0856(6) 0.0301(5) 0.0204(5) 0.048(2) Uani 0.493(10) 1 d . P B 1
Na8A Na -0.0222(8) 0.0007(6) 0.0148(6) 0.048(2) Uani 0.375(11) 1 d . P B 2
Na9 Na 0.5301(5) 0.5049(4) 0.3844(4) 0.041(2) Uani 0.508(10) 1 d . P A 1
Na10 Na -0.0384(3) 0.1447(3) 0.0944(2) 0.0570(15) Uani 1 1 d . . . .
Na11 Na 0.0230(3) 0.6537(2) 0.1129(2) 0.0494(12) Uani 1 1 d . . . .
Na12 Na -0.1473(2) 0.23986(14) 0.12617(16) 0.0243(7) Uani 1 1 d . . . .
O1 O -0.3492(3) 0.7069(2) 0.1994(3) 0.0182(11) Uani 1 1 d . . . .
O2 O -0.4674(3) 0.5378(2) 0.2874(3) 0.0197(12) Uani 1 1 d . . . .
O3 O -0.5108(3) 0.5484(2) 0.0425(3) 0.0167(11) Uani 1 1 d . . . .
O4 O -0.4064(4) 0.6173(2) 0.1281(3) 0.0177(11) Uani 1 1 d . . . .
O5 O -0.3849(3) 0.6135(2) 0.2444(3) 0.0162(11) Uani 1 1 d U . . .
O6 O -0.4619(3) 0.5376(2) 0.1699(3) 0.0170(11) Uani 1 1 d . . . .
O7 O -0.2502(3) 0.6438(2) 0.1567(2) 0.0134(10) Uani 1 1 d . . . .
O8 O -0.2271(3) 0.6388(2) 0.2744(3) 0.0159(11) Uani 1 1 d U . . .
O9 O -0.3403(3) 0.5549(2) 0.0693(3) 0.0134(10) Uani 1 1 d . . . .
O10 O -0.3026(3) 0.5520(2) 0.1996(3) 0.0137(10) Uani 1 1 d U . . .
O11 O -0.2936(3) 0.5446(2) 0.3252(3) 0.0154(11) Uani 1 1 d . . . .
O12 O -0.3930(3) 0.4761(2) 0.1139(2) 0.0123(10) Uani 1 1 d . . . .
O13 O -0.3703(3) 0.4694(2) 0.2489(3) 0.0155(11) Uani 1 1 d . . . .
O14 O -0.2827(3) 0.5335(2) -0.0227(3) 0.0178(11) Uani 1 1 d . . . .
O15 O -0.2054(3) 0.6028(2) 0.0710(3) 0.0164(11) Uani 1 1 d . . . .
O16 O -0.1199(4) 0.6885(2) 0.1322(3) 0.0225(13) Uani 1 1 d . . . .
O17 O -0.1024(3) 0.6335(2) 0.2395(3) 0.0183(11) Uani 1 1 d . . . .
O18 O -0.0761(3) 0.6795(2) 0.3539(3) 0.0182(12) Uani 1 1 d . . . .
O19 O -0.1440(3) 0.5891(2) 0.3771(2) 0.0158(11) Uani 1 1 d . . . .
O20 O -0.1945(3) 0.5117(3) 0.4413(3) 0.0212(12) Uani 1 1 d . . . .
O21 O -0.2244(3) 0.4560(2) 0.3328(3) 0.0172(11) Uani 1 1 d . . . .
O22 O -0.3348(3) 0.3730(2) 0.3039(3) 0.0192(12) Uani 1 1 d . . . .
O23 O -0.3461(3) 0.3939(2) 0.1832(3) 0.0151(11) Uani 1 1 d . . . .
O24 O -0.3803(3) 0.3842(2) 0.0582(3) 0.0172(11) Uani 1 1 d . . . .
O25 O -0.2722(3) 0.4666(2) 0.0742(3) 0.0163(11) Uani 1 1 d . . . .
O26 O -0.2337(3) 0.4660(2) 0.2069(3) 0.0129(10) Uani 1 1 d U . . .
O27 O -0.1825(3) 0.5433(2) 0.1660(3) 0.0152(11) Uani 1 1 d . . . .
O28 O -0.1596(3) 0.5374(2) 0.2783(2) 0.0144(11) Uani 1 1 d . . . .
O29 O -0.0480(3) 0.5945(2) 0.1554(3) 0.0162(11) Uani 1 1 d . . . .
O30 O -0.0105(3) 0.5859(2) 0.3434(3) 0.0190(12) Uani 1 1 d . . . .
O31 O -0.0748(3) 0.4942(2) 0.3939(3) 0.0167(11) Uani 1 1 d . . . .
O32 O -0.1972(3) 0.3737(2) 0.2738(3) 0.0201(12) Uani 1 1 d . . . .
O33 O -0.2233(3) 0.3785(2) 0.1411(3) 0.0156(11) Uani 1 1 d . . . .
O34 O -0.1356(3) 0.5096(2) 0.0693(3) 0.0155(11) Uani 1 1 d . . . .
O35 O 0.0072(3) 0.5623(2) 0.0617(3) 0.0203(12) Uani 1 1 d . . . .
O36 O 0.0881(3) 0.5415(2) 0.4611(3) 0.0203(12) Uani 1 1 d . . . .
O37 O -0.1767(3) 0.2800(2) 0.2093(3) 0.0188(12) Uani 1 1 d . . . .
O38 O -0.0557(3) 0.4399(2) 0.1893(3) 0.0161(11) Uani 1 1 d . . . .
O39 O 0.0080(3) 0.5034(2) 0.2520(3) 0.0160(11) Uani 1 1 d . . . .
O40 O -0.0363(3) 0.4356(2) 0.2883(3) 0.0160(11) Uani 1 1 d . . . .
O41 O 0.1269(3) 0.5354(2) 0.1830(3) 0.0142(10) Uani 1 1 d . . . .
O42 O 0.1645(3) 0.5243(2) 0.3729(3) 0.0189(12) Uani 1 1 d . . . .
O43 O 0.1008(3) 0.4354(2) 0.4201(3) 0.0178(11) Uani 1 1 d . . . .
O44 O -0.0249(3) 0.3131(2) 0.3001(3) 0.0161(11) Uani 1 1 d . . . .
O45 O -0.0524(3) 0.3184(2) 0.1638(3) 0.0166(11) Uani 1 1 d . . . .
O46 O 0.0340(3) 0.4487(2) 0.0981(3) 0.0167(11) Uani 1 1 d . . . .
O47 O 0.1209(3) 0.3983(2) 0.0398(3) 0.0179(11) Uani 1 1 d . . . .
O48 O 0.1992(3) 0.4664(2) 0.1346(2) 0.0133(10) Uani 1 1 d . . . .
O49 O 0.2876(3) 0.5513(2) 0.1978(3) 0.0187(12) Uani 1 1 d . . . .
O50 O 0.2433(3) 0.5159(2) 0.2950(3) 0.0175(11) Uani 1 1 d . . . .
O51 O 0.3310(3) 0.5408(3) 0.4195(3) 0.0242(13) Uani 1 1 d . . . .
O52 O 0.2642(3) 0.4502(2) 0.4420(3) 0.0179(11) Uani 1 1 d . . . .
O54 O 0.1207(3) 0.3387(2) 0.3853(3) 0.0169(11) Uani 1 1 d . . . .
O55 O 0.0739(4) 0.2345(2) 0.3648(3) 0.0198(12) Uani 1 1 d . . . .
O56 O 0.0592(3) 0.2566(2) 0.2451(3) 0.0178(11) Uani 1 1 d . . . .
O57 O 0.0233(3) 0.2451(2) 0.1190(3) 0.0190(12) Uani 1 1 d . . . .
O58 O 0.0686(3) 0.3493(2) 0.1266(3) 0.0166(11) Uani 1 1 d . . . .
O59 O 0.1464(3) 0.4317(2) 0.2180(2) 0.0143(11) Uani 1 1 d . . . .
O60 O 0.1690(3) 0.4251(2) 0.3299(3) 0.0162(11) Uani 1 1 d . . . .
O61 O 0.0921(3) 0.3545(2) 0.2574(3) 0.0164(11) Uani 1 1 d . . . .
O62 O 0.2456(3) 0.3665(2) 0.2844(3) 0.0146(11) Uani 1 1 d . . . .
O63 O 0.3168(3) 0.4524(2) 0.2449(3) 0.0199(12) Uani 1 1 d . . . .
O64 O 0.3422(3) 0.4478(2) 0.3624(3) 0.0189(12) Uani 1 1 d . . . .
O65 O 0.2775(3) 0.3537(2) 0.4119(3) 0.0167(11) Uani 1 1 d . . . .
O66 O 0.1993(3) 0.2797(2) 0.3365(3) 0.0177(11) Uani 1 1 d . . . .
O67 O 0.1718(3) 0.2857(2) 0.2004(3) 0.0172(11) Uani 1 1 d . . . .
O68 O 0.2246(3) 0.3658(2) 0.1561(3) 0.0199(12) Uani 1 1 d . . . .
O69 O 0.3125(3) 0.2729(2) 0.1701(3) 0.0219(12) Uani 1 1 d . . . .
O70 O 0.3697(4) 0.3572(3) 0.2479(3) 0.0179(12) Uani 0.9600(11) 1 d . P A 1
O71 O 0.4787(4) 0.4288(3) 0.3288(3) 0.0250(13) Uani 1 1 d . . . .
O72 O 0.3945(3) 0.3508(3) 0.3653(3) 0.0189(13) Uani 0.9600(11) 1 d . P A 1
O73 O 0.3597(4) 0.2607(3) 0.4196(3) 0.0264(14) Uani 1 1 d . . . .
O74 O 0.3174(5) 0.2773(2) 0.2912(3) 0.0180(12) Uani 0.9600(11) 1 d . P A 1
O75 O 0.6542(11) 0.4592(9) 0.4272(9) 0.127(6) Uiso 1 1 d . . . .
O79 O -0.0609(7) 0.8069(4) 0.1288(5) 0.062(3) Uani 1 1 d . . . .
O80 O -0.1665(8) 0.7283(7) -0.0076(6) 0.088(4) Uani 1 1 d . . . .
O81 O -0.2238(5) 0.7695(3) 0.1695(4) 0.0398(17) Uani 1 1 d . . . .
O82 O -0.3250(5) 0.7021(4) 0.0408(3) 0.0413(19) Uani 1 1 d . . . .
O84 O 0.0010(5) 0.6956(4) 0.0215(4) 0.053(2) Uani 1 1 d . . . .
O85 O 0.1612(5) 0.6322(3) 0.1322(3) 0.0349(16) Uani 1 1 d . . . .
O86 O 0.1056(4) 0.6285(3) -0.0443(4) 0.0413(19) Uani 1 1 d . . . .
O87 O 0.2650(4) 0.6982(3) 0.0558(3) 0.0314(15) Uani 1 1 d . . . .
O88 O 0.1432(3) 0.5350(2) 0.0393(3) 0.0212(12) Uani 1 1 d . . . .
O90 O 0.0458(13) 0.7209(9) 0.1722(11) 0.038(2) Uiso 0.354(15) 1 d . P C 1
O90A O 0.0657(7) 0.7020(5) 0.2081(6) 0.038(2) Uiso 0.646(15) 1 d . P C 2
O91 O -0.3017(12) 0.8210(8) 0.0303(10) 0.038(2) Uani 0.366(14) 1 d . P D 1
O91A O -0.2467(7) 0.8439(5) 0.0571(6) 0.038(2) Uani 0.634(14) 1 d . P D 2
O92 O 0.0657(8) 0.0809(7) 0.1499(7) 0.062(4) Uani 0.714(18) 1 d . P E 1
O92A O 0.0937(19) 0.1262(16) 0.1499(17) 0.062(4) Uani 0.286(18) 1 d . P E 2
O93 O -0.5923(15) 0.2247(10) 0.0785(13) 0.037(3) Uani 0.37(2) 1 d . P F 1
O93A O -0.5869(8) 0.2297(6) 0.1098(7) 0.037(3) Uani 0.63(2) 1 d . P F 2
O94 O 0.4134(5) 0.6375(3) 0.1971(4) 0.047(2) Uani 1 1 d . . . .
O96 O 0.3368(4) 0.5763(4) 0.0627(3) 0.042(2) Uani 1 1 d . . . .
O97 O -0.1572(4) 0.7873(3) 0.3225(3) 0.0288(14) Uani 1 1 d . . . .
O98 O -0.0832(5) 0.6988(4) 0.5044(4) 0.054(2) Uani 1 1 d . . . .
O99 O -0.6159(3) 0.4625(3) 0.1524(3) 0.0223(13) Uani 1 1 d . . . .
O100 O -0.7192(4) 0.3492(3) 0.0568(4) 0.0354(17) Uani 1 1 d . . . .
O101 O -0.5247(4) 0.3471(3) 0.1808(3) 0.0262(14) Uani 1 1 d . . . .
O102 O -0.5488(3) 0.4074(3) 0.0544(3) 0.0224(13) Uani 1 1 d . . . .
O103 O -0.4766(4) 0.2960(3) 0.0382(4) 0.0351(16) Uani 1 1 d . . . .
O105 O -0.2511(4) 0.1781(3) 0.1188(3) 0.0229(13) Uani 1 1 d . . . .
O106 O -0.2600(4) 0.2900(3) 0.0661(3) 0.0275(14) Uani 1 1 d . . . .
O108 O -0.0554(4) 0.1755(3) 0.1847(3) 0.0287(15) Uani 1 1 d . . . .
O109 O -0.1462(4) 0.2007(3) 0.0361(3) 0.0303(15) Uani 1 1 d . . . .
O110 O -0.1369(5) 0.0756(5) 0.0821(4) 0.057(3) Uani 1 1 d . . . .
O111 O -0.0502(6) 0.1076(5) -0.0039(4) 0.059(3) Uani 1 1 d . . . .
O112 O 0.0977(7) 0.1250(5) -0.0151(6) 0.077(3) Uiso 1 1 d . . . .
O118 O 0.2147(3) 0.3721(2) 0.5024(3) 0.0195(12) Uani 1 1 d . . . .
O121 O 0.1484(15) 0.1969(11) 0.0765(12) 0.138(9) Uiso 0.81(2) 1 d . P . .
C1 C -0.0279(4) 0.4600(3) 0.2430(4) 0.0135(14) Uiso 1 1 d . . . .
O1A O 0.1911(9) 0.6297(6) 0.4360(7) 0.091(4) Uiso 1 1 d . . . .
O122 O 0.2296(13) 0.1384(10) 0.1733(10) 0.150(8) Uiso 1 1 d . . . .
O83 O -0.0572(7) 0.7583(5) 0.2503(5) 0.070(3) Uiso 1 1 d . . . .
O115 O -0.1168(5) 0.3561(4) 0.4032(4) 0.0454(19) Uiso 1 1 d . . . .
O114 O 0.2877(5) 0.6795(3) 0.2265(4) 0.0428(18) Uiso 1 1 d . . . .
O107 O -0.4449(7) 0.3393(5) -0.0626(6) 0.026(3) Uiso 0.509(19) 1 d . P . .
O116 O 0.0136(4) 0.4064(3) 0.4938(3) 0.0310(15) Uiso 1 1 d . . . .
O76 O 0.1885(10) 0.6924(7) 0.3771(8) 0.108(5) Uiso 1 1 d . . . .
O9A O 0.4727(13) 0.5294(10) 0.3816(9) 0.041(2) Uani 0.373(16) 1 d . P G 2
O120 O 0.1145(12) 0.6159(9) 0.2815(9) 0.135(7) Uiso 1 1 d . . . .
O89 O 0.0600(15) 0.6763(10) 0.2810(12) 0.038(2) Uiso 0.311(16) 1 d . P H 1
O104 O -0.0644(5) 0.2569(3) 0.4176(4) 0.0410(18) Uiso 1 1 d . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.1353 0.1239 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Tb Tb -9.1472 9.1891 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -5.4734 5.5774 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O67 W1 O62 83.0(2) . .
O67 W1 O68 89.8(3) . .
O67 W1 O70 156.3(3) . .
O67 W1 O74 87.9(3) . .
O68 W1 O62 84.2(2) . .
O68 W1 O70 88.3(3) . .
O68 W1 O74 157.3(3) . .
O69 W1 O62 170.2(2) . .
O69 W1 O67 103.5(3) . .
O69 W1 O68 102.9(3) . .
O69 W1 O70 99.9(3) . .
O69 W1 O74 99.6(3) . .
O70 W1 O62 73.4(2) . .
O70 W1 O74 84.8(3) . .
O74 W1 O62 73.1(2) . .
O66 W1A O62 81.9(4) . .
O66 W1A O67 97.6(5) . .
O67 W1A O62 80.0(4) . .
O65 W2 O62 83.5(2) . .
O65 W2 O72 88.1(3) . .
O65 W2 O74 157.0(3) . .
O66 W2 O62 82.9(2) . .
O66 W2 O65 90.7(2) . .
O66 W2 O72 156.5(3) . .
O66 W2 O74 88.2(3) . .
O72 W2 O62 73.7(2) . .
O72 W2 O74 83.9(3) . .
O73 W2 O62 172.5(2) . .
O73 W2 O65 101.4(3) . .
O73 W2 O66 102.6(3) . .
O73 W2 O72 100.6(3) . .
O73 W2 O74 101.2(3) . .
O74 W2 O62 73.5(2) . .
O62 W2A O111 162.8(5) . 4_666
O64 W2A O62 80.1(4) . .
O64 W2A O111 95.1(5) . 4_666
O65 W2A O62 78.9(4) . .
O65 W2A O64 105.5(5) . .
O65 W2A O111 86.6(4) . 4_666
O62 W3 Na9 154.5(2) . .
O63 W3 Na9 93.7(2) . .
O63 W3 O62 82.7(2) . .
O63 W3 O70 86.7(3) . .
O63 W3 O72 155.8(2) . .
O64 W3 Na9 70.5(2) . .
O64 W3 O62 84.2(2) . .
O64 W3 O63 88.9(3) . .
O64 W3 O70 156.7(2) . .
O64 W3 O72 89.7(3) . .
O70 W3 Na9 132.6(2) . .
O70 W3 O62 72.5(2) . .
O71 W3 Na9 33.7(3) . .
O71 W3 O62 170.4(3) . .
O71 W3 O63 103.6(3) . .
O71 W3 O64 102.9(3) . .
O71 W3 O70 100.4(3) . .
O71 W3 O72 100.3(3) . .
O72 W3 Na9 108.5(2) . .
O72 W3 O62 73.1(2) . .
O72 W3 O70 85.1(3) . .
O63 W3A O62 82.6(4) . .
O63 W3A O68 97.6(5) . .
O68 W3A O62 78.0(3) . .
O45 W4 Na12 45.6(2) . .
O45 W4 O56 91.6(2) . .
O45 W4 O58 92.9(3) . .
O45 W4 O61 81.6(2) . .
O45 W4 O67 161.9(2) . .
O56 W4 Na12 79.52(18) . .
O56 W4 O61 72.2(2) . .
O56 W4 O67 84.7(2) . .
O57 W4 Na12 60.39(19) . .
O57 W4 O45 101.0(3) . .
O57 W4 O56 99.7(3) . .
O57 W4 O58 102.7(3) . .
O57 W4 O61 171.6(2) . .
O57 W4 O67 97.1(2) . .
O58 W4 Na12 119.66(17) . .
O58 W4 O56 155.9(2) . .
O58 W4 O61 85.0(2) . .
O58 W4 O67 83.7(2) . .
O61 W4 Na12 118.67(14) . .
O67 W4 Na12 149.30(18) . .
O67 W4 O61 80.4(2) . .
O44 W5 O54 92.4(2) . .
O44 W5 O56 94.6(2) . .
O44 W5 O61 83.1(2) . .
O44 W5 O66 163.1(2) . .
O54 W5 O61 83.8(2) . .
O54 W5 O66 82.0(2) . .
O55 W5 O44 102.5(3) . .
O55 W5 O54 101.5(3) . .
O55 W5 O56 99.6(3) . .
O55 W5 O61 172.0(2) . .
O55 W5 O66 94.2(3) . .
O56 W5 O54 155.8(2) . .
O56 W5 O61 74.1(2) . .
O56 W5 O66 84.7(2) . .
O66 W5 O61 80.5(2) . .
O46 W6 O48 93.5(2) . .
O46 W6 O58 92.1(2) . .
O46 W6 O59 81.8(2) . .
O46 W6 O68 162.3(2) . .
O47 W6 O46 100.8(3) . .
O47 W6 O48 99.3(3) . .
O47 W6 O58 101.4(3) . .
O47 W6 O59 172.0(2) . .
O47 W6 O68 96.7(2) . .
O48 W6 O58 157.1(2) . .
O48 W6 O59 72.9(2) . .
O48 W6 O68 85.9(2) . .
O58 W6 O59 86.0(2) . .
O58 W6 O68 82.0(2) . .
O68 W6 O59 81.1(2) . .
O43 W7 O52 93.8(3) . .
O43 W7 O54 94.3(3) . .
O43 W7 O60 83.6(2) . .
O43 W7 O65 163.9(2) . .
O52 W7 O60 75.0(2) . .
O52 W7 O65 83.8(2) . .
O54 W7 O52 157.3(2) . .
O54 W7 O60 84.8(2) . .
O54 W7 O65 82.6(2) . .
O65 W7 O60 80.5(2) . .
O118 W7 O43 102.1(3) . .
O118 W7 O52 99.4(3) . .
O118 W7 O54 99.5(3) . .
O118 W7 O60 172.5(2) . .
O118 W7 O65 94.0(3) . .
O41 W8 O48 90.2(2) . .
O41 W8 O50 93.8(2) . .
O41 W8 O59 82.5(2) . .
O41 W8 O63 162.9(2) . .
O48 W8 O59 72.9(2) . .
O48 W8 O63 85.0(2) . .
O49 W8 O41 100.4(3) . .
O49 W8 O48 98.4(3) . .
O49 W8 O50 102.3(3) . .
O49 W8 O59 171.0(2) . .
O49 W8 O63 96.5(3) . .
O50 W8 O48 157.8(2) . .
O50 W8 O59 85.9(2) . .
O50 W8 O63 84.8(2) . .
O63 W8 O59 80.4(2) . .
O42 W9 Na8 120.1(3) . 4_666
O42 W9 O50 92.2(3) . .
O42 W9 O52 93.5(3) . .
O42 W9 O60 81.3(2) . .
O42 W9 O64 160.9(3) . .
O50 W9 Na8 143.0(2) . 4_666
O50 W9 O52 156.4(3) . .
O50 W9 O60 85.0(2) . .
O50 W9 O64 81.6(2) . .
O51 W9 Na8 56.4(3) . 4_666
O51 W9 O42 102.0(3) . .
O51 W9 O50 102.2(3) . .
O51 W9 O52 99.0(3) . .
O51 W9 O60 171.8(3) . .
O51 W9 O64 96.9(3) . .
O52 W9 Na8 47.7(2) . 4_666
O52 W9 O60 73.2(2) . .
O52 W9 O64 85.7(2) . .
O60 W9 Na8 115.4(2) . 4_666
O64 W9 Na8 72.8(2) . 4_666
O64 W9 O60 80.3(2) . .
O12 W10 Na2 44.77(16) . .
O12 W10 O26 80.3(2) . .
O23 W10 Na2 43.63(16) . .
O23 W10 O12 83.2(2) . .
O23 W10 O26 73.4(2) . .
O24 W10 Na2 83.33(19) . .
O24 W10 O12 96.6(2) . .
O24 W10 O23 98.0(3) . .
O24 W10 O25 101.9(3) . .
O24 W10 O26 171.1(2) . .
O24 W10 O33 100.4(3) . .
O25 W10 Na2 129.13(18) . .
O25 W10 O12 84.6(2) . .
O25 W10 O23 157.7(2) . .
O25 W10 O26 86.2(2) . .
O26 W10 Na2 88.72(13) . .
O33 W10 Na2 133.86(18) . .
O33 W10 O12 162.6(2) . .
O33 W10 O23 90.8(2) . .
O33 W10 O25 95.5(2) . .
O33 W10 O26 82.3(2) . .
O13 W11 Na2 44.48(17) . .
O13 W11 O26 81.1(2) . .
O21 W11 Na2 128.02(18) . .
O21 W11 O13 83.6(2) . .
O21 W11 O23 155.4(2) . .
O21 W11 O26 84.2(2) . .
O22 W11 Na2 84.9(2) . .
O22 W11 O13 96.0(2) . .
O22 W11 O21 101.7(3) . .
O22 W11 O23 100.4(3) . .
O22 W11 O26 173.2(2) . .
O22 W11 O32 100.9(3) . .
O23 W11 Na2 43.90(16) . .
O23 W11 O13 83.4(2) . .
O23 W11 O26 73.2(2) . .
O26 W11 Na2 88.69(13) . .
O32 W11 Na2 136.8(2) . .
O32 W11 O13 163.1(2) . .
O32 W11 O21 93.0(3) . .
O32 W11 O23 93.4(2) . .
O32 W11 O26 82.1(2) . .
O9 W12 O27 80.7(2) . .
O14 W12 O9 95.6(2) . .
O14 W12 O15 99.8(3) . .
O14 W12 O25 101.2(3) . .
O14 W12 O27 172.8(2) . .
O14 W12 O34 101.7(3) . .
O15 W12 O9 85.8(2) . .
O15 W12 O25 156.8(2) . .
O15 W12 O27 73.9(2) . .
O25 W12 O9 82.5(2) . .
O25 W12 O27 84.5(2) . .
O34 W12 O9 162.4(2) . .
O34 W12 O15 94.1(2) . .
O34 W12 O25 91.2(2) . .
O34 W12 O27 82.4(2) . .
O11 W13 O28 81.9(2) . .
O19 W13 O11 85.7(2) . .
O19 W13 O28 73.0(2) . .
O20 W13 O11 93.9(2) . .
O20 W13 O19 101.5(3) . .
O20 W13 O21 100.7(3) . .
O20 W13 O28 173.3(3) . .
O20 W13 O31 102.0(3) . .
O21 W13 O11 81.6(2) . .
O21 W13 O19 155.1(2) . .
O21 W13 O28 84.0(2) . .
O31 W13 O11 163.8(2) . .
O31 W13 O19 94.1(2) . .
O31 W13 O21 92.3(2) . .
O31 W13 O28 82.5(2) . .
O7 W14 Na11 153.58(19) . .
O7 W14 O27 80.4(2) . .
O15 W14 Na11 92.48(18) . .
O15 W14 O7 83.8(2) . .
O15 W14 O27 73.6(2) . .
O16 W14 Na11 57.6(2) . .
O16 W14 O7 97.0(3) . .
O16 W14 O15 98.1(3) . .
O16 W14 O17 101.9(3) . .
O16 W14 O27 171.5(2) . .
O16 W14 O29 100.8(3) . .
O17 W14 Na11 106.95(19) . .
O17 W14 O7 83.6(2) . .
O17 W14 O15 157.4(2) . .
O17 W14 O27 85.9(2) . .
O27 W14 Na11 123.70(16) . .
O29 W14 Na11 43.9(2) . .
O29 W14 O7 162.2(2) . .
O29 W14 O15 93.6(2) . .
O29 W14 O17 92.7(2) . .
O29 W14 O27 82.0(2) . .
O8 W15 O28 80.3(2) . .
O17 W15 O8 82.4(2) . .
O17 W15 O19 156.2(2) . .
O17 W15 O28 85.5(2) . .
O18 W15 O8 96.8(2) . .
O18 W15 O17 101.8(3) . .
O18 W15 O19 99.3(3) . .
O18 W15 O28 171.8(2) . .
O18 W15 O30 102.2(3) . .
O19 W15 O8 84.3(2) . .
O19 W15 O28 72.8(2) . .
O30 W15 O8 161.0(2) . .
O30 W15 O17 92.5(3) . .
O30 W15 O19 93.7(3) . .
O30 W15 O28 81.1(2) . .
O3 W16 Na2 91.3(2) . .
O3 W16 O4 100.4(3) . .
O3 W16 O6 100.0(2) . .
O3 W16 O9 103.0(3) . .
O3 W16 O10 170.3(2) . .
O3 W16 O12 104.5(3) . .
O4 W16 Na2 135.35(18) . .
O4 W16 O6 85.4(3) . .
O4 W16 O10 72.5(2) . .
O6 W16 Na2 50.04(19) . .
O6 W16 O10 73.3(2) . .
O9 W16 Na2 130.69(18) . .
O9 W16 O4 88.5(2) . .
O9 W16 O6 156.9(2) . .
O9 W16 O10 83.6(2) . .
O9 W16 O12 89.1(2) . .
O10 W16 Na2 89.55(14) . .
O12 W16 Na2 41.61(17) . .
O12 W16 O4 154.8(2) . .
O12 W16 O6 87.1(2) . .
O12 W16 O10 82.4(2) . .
Na6 W17 Na2 64.50(8) 1_455 .
O2 W17 Na2 90.1(2) . .
O2 W17 Na6 57.3(2) . 1_455
O2 W17 O5 99.6(3) . .
O2 W17 O6 98.1(3) . .
O2 W17 O10 168.7(2) . .
O2 W17 O11 103.6(3) . .
O2 W17 O13 102.8(3) . .
O5 W17 Na2 135.22(18) . .
O5 W17 Na6 84.38(17) . 1_455
O5 W17 O10 72.8(2) . .
O6 W17 Na2 50.18(19) . .
O6 W17 Na6 41.74(17) . 1_455
O6 W17 O5 85.1(2) . .
O6 W17 O10 73.35(19) . .
O10 W17 Na2 89.81(14) . .
O10 W17 Na6 112.80(14) . 1_455
O11 W17 Na2 131.68(18) . .
O11 W17 Na6 157.82(18) . 1_455
O11 W17 O5 88.5(2) . .
O11 W17 O6 158.1(2) . .
O11 W17 O10 84.8(2) . .
O11 W17 O13 90.9(2) . .
O13 W17 Na2 40.82(17) . .
O13 W17 Na6 103.78(17) . 1_455
O13 W17 O5 157.1(2) . .
O13 W17 O6 87.1(2) . .
O13 W17 O10 84.3(2) . .
O1 W18 O4 100.3(3) . .
O1 W18 O5 100.0(3) . .
O1 W18 O7 102.3(3) . .
O1 W18 O8 102.9(3) . .
O1 W18 O10 170.8(2) . .
O4 W18 O10 72.9(2) . .
O5 W18 O4 85.1(2) . .
O5 W18 O10 73.7(2) . .
O7 W18 O4 87.6(2) . .
O7 W18 O5 157.5(2) . .
O7 W18 O10 83.8(2) . .
O8 W18 O4 156.7(2) . .
O8 W18 O5 88.7(2) . .
O8 W18 O7 89.7(2) . .
O8 W18 O10 83.8(2) . .
O32 Tb1 Na12 112.81(17) . .
O32 Tb1 O37 77.1(2) . .
O32 Tb1 O38 119.2(2) . .
O32 Tb1 O40 83.3(2) . .
O32 Tb1 O45 152.5(2) . .
O32 Tb1 C1 102.0(2) . .
O33 Tb1 Na12 73.92(16) . .
O33 Tb1 O32 82.0(2) . .
O33 Tb1 O37 78.1(2) . .
O33 Tb1 O38 84.42(19) . .
O33 Tb1 O40 119.7(2) . .
O33 Tb1 O44 152.0(2) . .
O33 Tb1 O45 90.2(2) . .
O33 Tb1 C1 102.8(2) . .
O37 Tb1 Na12 37.24(14) . .
O37 Tb1 C1 178.7(2) . .
O38 Tb1 Na12 119.39(14) . .
O38 Tb1 O37 154.22(19) . .
O38 Tb1 O40 54.35(19) . .
O38 Tb1 C1 27.1(2) . .
O40 Tb1 Na12 161.16(14) . .
O40 Tb1 O37 151.43(19) . .
O40 Tb1 C1 27.3(2) . .
O44 Tb1 Na12 84.33(16) . .
O44 Tb1 O32 90.7(2) . .
O44 Tb1 O37 74.0(2) . .
O44 Tb1 O38 122.20(19) . .
O44 Tb1 O40 85.8(2) . .
O44 Tb1 O45 83.9(2) . .
O44 Tb1 C1 105.2(2) . .
O45 Tb1 Na12 39.87(15) . .
O45 Tb1 O37 75.5(2) . .
O45 Tb1 O38 85.9(2) . .
O45 Tb1 O40 122.98(19) . .
O45 Tb1 C1 105.4(2) . .
C1 Tb1 Na12 143.85(16) . .
O30 Tb2 O31 84.3(2) . .
O30 Tb2 O36 76.6(2) . .
O30 Tb2 O39 83.6(2) . .
O30 Tb2 O40 120.95(19) . .
O30 Tb2 O42 92.5(2) . .
O30 Tb2 O43 154.9(2) . .
O30 Tb2 C1 102.9(2) . .
O31 Tb2 O36 78.2(2) . .
O31 Tb2 O39 120.43(19) . .
O31 Tb2 O40 84.78(19) . .
O31 Tb2 O43 91.3(2) . .
O31 Tb2 C1 103.6(2) . .
O36 Tb2 O39 151.4(2) . .
O36 Tb2 O40 154.3(2) . .
O36 Tb2 C1 178.0(2) . .
O39 Tb2 O40 54.25(19) . .
O39 Tb2 C1 26.9(2) . .
O40 Tb2 C1 27.4(2) . .
O42 Tb2 O31 153.9(2) . .
O42 Tb2 O36 75.8(2) . .
O42 Tb2 O39 84.7(2) . .
O42 Tb2 O40 118.4(2) . .
O42 Tb2 O43 80.7(2) . .
O42 Tb2 C1 102.3(2) . .
O43 Tb2 O36 78.3(2) . .
O43 Tb2 O39 119.4(2) . .
O43 Tb2 O40 83.0(2) . .
O43 Tb2 C1 102.2(2) . .
O29 Tb3 Na11 36.25(15) . .
O29 Tb3 O35 73.5(2) . .
O29 Tb3 O38 121.53(19) . .
O29 Tb3 O39 84.8(2) . .
O29 Tb3 C1 104.0(2) . .
O34 Tb3 Na11 92.80(16) . .
O34 Tb3 O29 82.8(2) . .
O34 Tb3 O35 75.9(2) . .
O34 Tb3 O38 85.76(19) . .
O34 Tb3 O39 121.27(19) . .
O34 Tb3 O41 152.3(2) . .
O34 Tb3 O46 89.7(2) . .
O34 Tb3 C1 104.6(2) . .
O35 Tb3 Na11 42.93(17) . .
O35 Tb3 C1 177.4(2) . .
O38 Tb3 Na11 157.44(15) . .
O38 Tb3 O35 154.9(2) . .
O38 Tb3 C1 27.3(2) . .
O39 Tb3 Na11 109.04(16) . .
O39 Tb3 O35 150.7(2) . .
O39 Tb3 O38 54.28(19) . .
O39 Tb3 C1 27.0(2) . .
O41 Tb3 Na11 67.75(15) . .
O41 Tb3 O29 91.17(19) . .
O41 Tb3 O35 76.44(19) . .
O41 Tb3 O38 119.83(18) . .
O41 Tb3 O39 84.73(19) . .
O41 Tb3 C1 103.1(2) . .
O46 Tb3 Na11 120.72(16) . .
O46 Tb3 O29 154.5(2) . .
O46 Tb3 O35 81.1(2) . .
O46 Tb3 O38 81.8(2) . .
O46 Tb3 O39 119.5(2) . .
O46 Tb3 O41 84.3(2) . .
O46 Tb3 C1 101.5(2) . .
C1 Tb3 Na11 134.45(18) . .
O26 P1 O10 108.5(3) . .
O27 P1 O10 107.4(3) . .
O27 P1 O26 111.0(3) . .
O28 P1 O10 108.9(3) . .
O28 P1 O26 110.4(3) . .
O28 P1 O27 110.5(3) . .
O59 P2 O61 111.0(3) . .
O59 P2 O62 108.0(3) . .
O60 P2 O59 110.1(3) . .
O60 P2 O61 110.9(3) . .
O60 P2 O62 108.1(3) . .
O61 P2 O62 108.6(3) . .
Na9 Na1 Na3 167.9(3) . 2_545
O22 Na1 Na3 79.3(2) 1_655 2_545
O22 Na1 Na9 112.7(3) 1_655 .
O22 Na1 O71 97.6(3) 1_655 .
O71 Na1 Na3 135.8(3) . 2_545
O71 Na1 Na9 44.0(2) . .
O75 Na1 Na3 136.3(6) . 2_545
O75 Na1 Na9 42.7(6) . .
O75 Na1 O22 110.2(6) . 1_655
O75 Na1 O71 86.5(6) . .
O75 Na1 O79 162.9(7) . 2_545
O75 Na1 O91A 97.8(7) . 2_545
O75 Na1 O112 82.2(7) . 4_666
O79 Na1 Na3 45.0(3) 2_545 2_545
O79 Na1 Na9 131.1(4) 2_545 .
O79 Na1 O22 86.9(4) 2_545 1_655
O79 Na1 O71 91.0(4) 2_545 .
O79 Na1 O91A 85.3(5) 2_545 2_545
O79 Na1 O112 81.5(5) 2_545 4_666
O91A Na1 Na3 40.3(3) 2_545 2_545
O91A Na1 O22 79.6(4) 2_545 1_655
O91A Na1 O71 175.5(5) 2_545 .
O112 Na1 Na3 81.2(4) 4_666 2_545
O112 Na1 Na9 86.8(4) 4_666 .
O112 Na1 O22 160.3(5) 4_666 1_655
O112 Na1 O71 98.4(4) 4_666 .
O112 Na1 O91A 83.6(5) 4_666 2_545
W10 Na2 W16 63.27(5) . .
W10 Na2 W17 90.64(7) . .
W10 Na2 Na6 127.07(11) . 1_455
W11 Na2 W10 58.28(5) . .
W11 Na2 W16 91.31(7) . .
W11 Na2 W17 63.59(6) . .
W11 Na2 Na6 118.64(11) . 1_455
W16 Na2 Na6 64.06(8) . 1_455
W17 Na2 W16 56.95(5) . .
W17 Na2 Na6 55.76(8) . 1_455
O6 Na2 W10 89.96(14) . .
O6 Na2 W11 90.63(14) . .
O6 Na2 W16 32.45(12) . .
O6 Na2 W17 32.77(12) . .
O6 Na2 Na6 39.03(13) . 1_455
O12 Na2 W10 33.94(12) . .
O12 Na2 W11 76.17(14) . .
O12 Na2 W16 29.51(13) . .
O12 Na2 W17 72.61(14) . .
O12 Na2 Na6 93.57(17) . 1_455
O12 Na2 O6 59.22(18) . .
O13 Na2 W10 76.74(15) . .
O13 Na2 W11 34.51(13) . .
O13 Na2 W16 73.61(15) . .
O13 Na2 W17 29.43(14) . .
O13 Na2 Na6 84.16(17) . 1_455
O13 Na2 O6 59.84(19) . .
O13 Na2 O12 75.0(2) . .
O23 Na2 W10 33.02(14) . .
O23 Na2 W11 32.63(14) . .
O23 Na2 W16 89.75(16) . .
O23 Na2 W17 89.47(16) . .
O23 Na2 Na6 143.78(19) . 1_455
O23 Na2 O6 106.2(2) . .
O23 Na2 O12 63.40(19) . .
O23 Na2 O13 63.7(2) . .
O99 Na2 W10 155.6(2) . .
O99 Na2 W11 141.1(2) . .
O99 Na2 W16 97.0(2) . .
O99 Na2 W17 89.71(18) . .
O99 Na2 Na6 38.53(18) . 1_455
O99 Na2 O6 77.4(2) . .
O99 Na2 O12 124.4(2) . .
O99 Na2 O13 113.0(2) . .
O99 Na2 O23 171.3(3) . .
O99 Na2 O101 89.2(2) . .
O99 Na2 O102 86.9(2) . .
O101 Na2 W10 108.04(18) . .
O101 Na2 W11 89.93(17) . .
O101 Na2 W16 168.4(2) . .
O101 Na2 W17 133.2(2) . .
O101 Na2 Na6 124.86(19) . 1_455
O101 Na2 O6 159.0(2) . .
O101 Na2 O12 140.8(2) . .
O101 Na2 O13 112.9(2) . .
O101 Na2 O23 85.1(2) . .
O102 Na2 W10 78.06(16) . .
O102 Na2 W11 131.66(18) . .
O102 Na2 W16 86.15(18) . .
O102 Na2 W17 142.2(2) . .
O102 Na2 Na6 103.35(19) . 1_455
O102 Na2 O6 110.4(2) . .
O102 Na2 O12 78.5(2) . .
O102 Na2 O13 152.9(2) . .
O102 Na2 O23 99.0(2) . .
O102 Na2 O101 84.5(2) . .
O16 Na3 Na1 120.8(3) . 2
O16 Na3 O79 82.9(3) . .
O16 Na3 O80 86.6(4) . .
O16 Na3 O81 81.4(3) . .
O16 Na3 O82 88.9(3) . .
O16 Na3 O91 164.8(6) . .
O79 Na3 Na1 39.6(3) . 2
O80 Na3 Na1 107.9(4) . 2
O80 Na3 O79 96.3(4) . .
O80 Na3 O81 166.7(5) . .
O80 Na3 O82 88.1(4) . .
O80 Na3 O91 102.6(7) . .
O81 Na3 Na1 83.4(3) . 2
O81 Na3 O79 88.0(3) . .
O81 Na3 O82 86.0(3) . .
O82 Na3 Na1 146.2(3) . 2
O82 Na3 O79 170.5(4) . .
O91 Na3 Na1 68.3(5) . 2
O91 Na3 O79 107.7(6) . .
O91 Na3 O81 88.1(6) . .
O91 Na3 O82 79.5(6) . .
O91A Na3 Na1 41.3(3) . 2
O91A Na3 O16 158.3(4) . .
O91A Na3 O79 80.9(4) . .
O91A Na3 O80 109.4(5) . .
O91A Na3 O81 83.7(4) . .
O91A Na3 O82 105.7(4) . .
O82 Na4 O101 169.5(3) 3_465 .
O93 Na4 O82 81.6(7) . 3_465
O93 Na4 O101 102.8(7) . .
O93 Na4 O102 163.8(6) . .
O93A Na4 O82 96.4(4) . 3_465
O93A Na4 O101 86.9(4) . .
O100 Na4 O82 75.8(3) . 3_465
O100 Na4 O93 107.3(6) . .
O100 Na4 O93A 104.0(4) . .
O100 Na4 O101 93.8(3) . .
O100 Na4 O102 88.2(3) . .
O100 Na4 O103 155.9(3) . .
O102 Na4 O82 98.2(3) . 3_465
O102 Na4 O93A 162.9(4) . .
O102 Na4 O101 80.3(2) . .
O103 Na4 O82 83.1(3) . 3_465
O103 Na4 O93 80.5(6) . .
O103 Na4 O93A 89.7(4) . .
O103 Na4 O101 107.0(3) . .
O103 Na4 O102 83.4(3) . .
O18 Na5 Na12 118.99(19) . 2_455
O97 Na5 Na12 88.3(2) . 2_455
O97 Na5 O18 79.5(2) . .
O97 Na5 O103 86.5(3) . 2_455
O97 Na5 O105 104.4(3) . 2_455
O97 Na5 O106 90.7(3) . 2_455
O98 Na5 Na12 104.8(3) . 2_455
O98 Na5 O18 97.5(3) . .
O98 Na5 O97 166.1(3) . .
O98 Na5 O103 81.0(3) . 2_455
O98 Na5 O105 88.6(3) . 2_455
O98 Na5 O106 96.3(4) . 2_455
O103 Na5 Na12 136.0(2) 2_455 2_455
O103 Na5 O18 102.9(3) 2_455 .
O103 Na5 O105 168.2(3) 2_455 2_455
O103 Na5 O106 95.1(3) 2_455 2_455
O105 Na5 Na12 41.93(16) 2_455 2_455
O105 Na5 O18 83.9(2) 2_455 .
O105 Na5 O106 80.4(2) 2_455 2_455
O106 Na5 Na12 41.23(18) 2_455 2_455
O106 Na5 O18 158.8(3) 2_455 .
W17 Na6 Na2 59.75(7) 1_655 1_655
W17 Na6 Na7 157.45(13) 1_655 .
Na2 Na6 Na7 130.38(13) 1_655 .
O2 Na6 W17 30.42(11) 1_655 1_655
O2 Na6 Na2 72.57(15) 1_655 1_655
O2 Na6 Na7 156.56(19) 1_655 .
O6 Na6 W17 33.42(14) 1_655 1_655
O6 Na6 Na2 47.68(17) 1_655 1_655
O6 Na6 Na7 133.1(2) 1_655 .
O6 Na6 O2 63.31(19) 1_655 1_655
O6 Na6 O96 99.1(3) 1_655 .
O6 Na6 O99 85.0(2) 1_655 1_655
O49 Na6 W17 129.6(2) . 1_655
O49 Na6 Na2 120.6(2) . 1_655
O49 Na6 Na7 66.50(18) . .
O49 Na6 O2 99.2(2) . 1_655
O49 Na6 O6 160.2(3) . 1_655
O49 Na6 O96 99.4(3) . .
O49 Na6 O99 86.3(2) . 1_655
O94 Na6 W17 88.9(2) . 1_655
O94 Na6 Na2 147.5(3) . 1_655
O94 Na6 Na7 76.0(2) . .
O94 Na6 O2 84.6(3) . 1_655
O94 Na6 O6 101.5(3) . 1_655
O94 Na6 O49 85.1(3) . .
O94 Na6 O96 91.1(3) . .
O94 Na6 O99 170.0(3) . 1_655
O96 Na6 W17 130.7(2) . 1_655
O96 Na6 Na2 102.6(2) . 1_655
O96 Na6 Na7 35.47(18) . .
O96 Na6 O2 160.4(3) . 1_655
O96 Na6 O99 95.4(3) . 1_655
O99 Na6 W17 92.56(17) 1_655 1_655
O99 Na6 Na2 37.51(15) 1_655 1_655
O99 Na6 Na7 105.22(19) 1_655 .
O99 Na6 O2 91.7(2) 1_655 1_655
Na6 Na7 Na11 116.18(13) . .
O85 Na7 Na6 88.8(2) . .
O85 Na7 Na11 28.6(2) . .
O86 Na7 Na6 157.5(3) . .
O86 Na7 Na11 81.9(2) . .
O86 Na7 O85 110.4(3) . .
O86 Na7 O87 94.0(3) . .
O86 Na7 O88 81.1(3) . .
O86 Na7 O96 123.5(3) . .
O87 Na7 Na6 96.8(2) . .
O87 Na7 Na11 96.5(2) . .
O87 Na7 O85 92.4(3) . .
O87 Na7 O88 174.5(3) . .
O88 Na7 Na6 88.71(19) . .
O88 Na7 Na11 80.38(18) . .
O88 Na7 O85 87.0(3) . .
O96 Na7 Na6 36.5(2) . .
O96 Na7 Na11 152.3(3) . .
O96 Na7 O85 125.2(3) . .
O96 Na7 O87 92.7(3) . .
O96 Na7 O88 92.1(3) . .
W9 Na8 Na8 94.1(4) 4_565 3
Na9 Na8 W9 144.7(5) 2_545 4_565
Na9 Na8 Na8 92.3(5) 2_545 3
Na9 Na8 O51 122.5(6) 2_545 4_565
Na9 Na8 O52 136.5(5) 2_545 4_565
Na9 Na8 O75 55.8(5) 2_545 2_545
Na9 Na8 O110 68.8(4) 2_545 .
Na9 Na8 O111 118.1(6) 2_545 .
O51 Na8 W9 29.27(16) 4_565 4_565
O51 Na8 Na8 74.7(4) 4_565 3
O52 Na8 W9 32.56(18) 4_565 4_565
O52 Na8 Na8 125.0(5) 4_565 3
O52 Na8 O51 59.4(3) 4_565 4_565
O52 Na8 O75 87.7(5) 4_565 2_545
O75 Na8 W9 89.6(5) 2_545 4_565
O75 Na8 Na8 110.4(7) 2_545 3
O75 Na8 O51 76.5(5) 2_545 4_565
O110 Na8 W9 111.6(4) . 4_565
O110 Na8 Na8 154.1(6) . 3
O110 Na8 O51 130.1(4) . 4_565
O110 Na8 O52 79.8(4) . 4_565
O110 Na8 O75 74.3(6) . 2_545
O111 Na8 W9 96.7(4) . 4_565
O111 Na8 Na8 89.6(5) . 3
O111 Na8 O51 117.5(5) . 4_565
O111 Na8 O52 86.7(5) . 4_565
O111 Na8 O75 158.6(7) . 2_545
O111 Na8 O110 84.4(5) . .
Na8A Na8A O51 96.5(13) 3 4_565
Na8A Na8A O111 92.9(15) 3 .
Na8A Na8A O9A 121.6(15) 3 2_545
O111 Na8A O51 101.2(5) . 4_565
O9A Na8A O51 141.8(8) 2_545 4_565
O9A Na8A O111 80.0(7) 2_545 .
W3 Na9 Na10 137.9(3) . 2
Na1 Na9 W3 68.6(2) . .
Na1 Na9 Na10 153.0(3) . 2
Na8 Na9 W3 132.4(4) 2 .
Na8 Na9 Na1 101.8(5) 2 .
Na8 Na9 Na10 65.3(4) 2 2
Na8 Na9 O2 133.9(5) 2 1_655
Na8 Na9 O71 138.8(6) 2 .
Na8 Na9 O75 73.9(6) 2 .
Na8 Na9 O92 94.7(6) 2 2
Na8 Na9 O110 57.6(4) 2 2
O2 Na9 W3 93.3(3) 1_655 .
O2 Na9 Na1 101.0(4) 1_655 .
O2 Na9 Na10 76.4(3) 1_655 2
O2 Na9 O92 70.4(4) 1_655 2
O2 Na9 O110 76.7(4) 1_655 2
O71 Na9 W3 23.93(17) . .
O71 Na9 Na1 48.8(3) . .
O71 Na9 Na10 153.7(4) . 2
O71 Na9 O2 85.1(3) . 1_655
O71 Na9 O92 114.3(5) . 2
O71 Na9 O110 150.4(5) . 2
O75 Na9 W3 104.6(6) . .
O75 Na9 Na1 36.3(6) . .
O75 Na9 Na10 117.5(6) . 2
O75 Na9 O2 104.3(6) . 1_655
O75 Na9 O71 84.9(6) . .
O75 Na9 O92 158.8(7) . 2
O75 Na9 O110 77.4(6) . 2
O92 Na9 W3 96.3(4) 2 .
O92 Na9 Na1 162.7(5) 2 .
O92 Na9 Na10 41.6(3) 2 2
O92 Na9 O110 81.4(5) 2 2
O110 Na9 W3 170.0(4) 2 .
O110 Na9 Na1 111.9(4) 2 .
O110 Na9 Na10 41.2(3) 2 2
Na12 Na10 Na9 134.2(2) . 2_545
O57 Na10 Na9 154.7(3) . 2_545
O57 Na10 Na12 58.12(17) . .
O92 Na10 Na9 43.1(4) . 2_545
O92 Na10 Na12 138.5(4) . .
O92 Na10 O57 111.8(5) . .
O92A Na10 Na12 124.9(12) . .
O92A Na10 O57 81.3(12) . .
O92A Na10 O108 89.6(10) . .
O92A Na10 O109 153.2(11) . .
O92A Na10 O110 116.0(11) . .
O92A Na10 O111 100.1(11) . .
O108 Na10 Na9 103.0(3) . 2_545
O108 Na10 Na12 44.9(2) . .
O108 Na10 O57 70.5(3) . .
O108 Na10 O92 93.8(4) . .
O108 Na10 O110 92.4(3) . .
O108 Na10 O111 168.3(4) . .
O109 Na10 Na9 132.2(3) . 2_545
O109 Na10 Na12 44.3(2) . .
O109 Na10 O57 72.9(3) . .
O109 Na10 O92 175.2(6) . .
O109 Na10 O108 88.6(3) . .
O109 Na10 O110 90.8(3) . .
O109 Na10 O111 85.7(3) . .
O110 Na10 Na9 43.2(3) . 2_545
O110 Na10 Na12 98.1(3) . .
O110 Na10 O57 156.3(3) . .
O110 Na10 O92 84.9(5) . .
O110 Na10 O111 77.5(4) . .
O111 Na10 Na9 73.7(3) . 2_545
O111 Na10 Na12 130.0(3) . .
O111 Na10 O57 117.2(4) . .
O111 Na10 O92 91.2(5) . .
W14 Na11 Tb3 63.72(8) . .
W14 Na11 Na7 154.17(18) . .
Tb3 Na11 Na7 91.49(13) . .
O16 Na11 W14 30.77(13) . .
O16 Na11 Tb3 94.43(17) . .
O16 Na11 Na7 168.7(2) . .
O29 Na11 W14 31.23(14) . .
O29 Na11 Tb3 34.06(16) . .
O29 Na11 Na7 125.3(2) . .
O29 Na11 O16 61.7(2) . .
O29 Na11 O35 68.1(2) . .
O29 Na11 O90A 89.0(4) . .
O35 Na11 W14 89.44(18) . .
O35 Na11 Tb3 39.19(15) . .
O35 Na11 Na7 65.45(17) . .
O35 Na11 O16 114.3(2) . .
O84 Na11 W14 118.9(3) . .
O84 Na11 Tb3 130.5(3) . .
O84 Na11 Na7 70.8(3) . .
O84 Na11 O16 98.1(3) . .
O84 Na11 O29 138.8(3) . .
O84 Na11 O35 92.9(3) . .
O84 Na11 O85 95.7(3) . .
O84 Na11 O90A 119.8(5) . .
O85 Na11 W14 144.0(3) . .
O85 Na11 Tb3 86.9(2) . .
O85 Na11 Na7 29.4(2) . .
O85 Na11 O16 160.5(3) . .
O85 Na11 O29 114.4(3) . .
O85 Na11 O35 78.5(3) . .
O85 Na11 O90A 90.0(4) . .
O90 Na11 W14 87.6(6) . .
O90 Na11 Tb3 130.6(7) . .
O90 Na11 Na7 115.9(6) . .
O90 Na11 O16 66.8(6) . .
O90 Na11 O29 104.6(6) . .
O90 Na11 O35 168.7(7) . .
O90 Na11 O84 98.1(7) . .
O90 Na11 O85 97.8(6) . .
O90A Na11 W14 81.5(3) . .
O90A Na11 Tb3 109.6(4) . .
O90A Na11 Na7 115.7(3) . .
O90A Na11 O16 71.2(3) . .
O90A Na11 O35 146.4(4) . .
W4 Na12 Tb1 62.43(6) . .
W4 Na12 Na5 155.90(13) . 2_445
Na5 Na12 Tb1 95.44(11) 2_445 .
Na10 Na12 W4 78.43(13) . .
Na10 Na12 Tb1 138.83(14) . .
Na10 Na12 Na5 125.07(16) . 2_445
O37 Na12 W4 92.97(17) . .
O37 Na12 Tb1 37.90(15) . .
O37 Na12 Na5 71.46(17) . 2_445
O37 Na12 Na10 142.9(2) . .
O37 Na12 O45 71.4(2) . .
O45 Na12 W4 30.42(13) . .
O45 Na12 Tb1 35.00(13) . .
O45 Na12 Na5 125.52(19) . 2_445
O45 Na12 Na10 108.6(2) . .
O105 Na12 W4 158.6(2) . .
O105 Na12 Tb1 125.1(2) . .
O105 Na12 Na5 42.83(18) . 2_445
O105 Na12 Na10 87.7(2) . .
O105 Na12 O37 88.4(2) . .
O105 Na12 O45 159.7(3) . .
O106 Na12 W4 117.7(2) . .
O106 Na12 Tb1 79.51(18) . .
O106 Na12 Na5 43.70(19) . 2_445
O106 Na12 Na10 133.7(2) . .
O106 Na12 O37 82.3(2) . .
O106 Na12 O45 93.0(2) . .
O106 Na12 O105 83.6(3) . .
O106 Na12 O108 167.6(3) . .
O106 Na12 O109 89.1(3) . .
O108 Na12 W4 74.67(17) . .
O108 Na12 Tb1 108.2(2) . .
O108 Na12 Na5 124.5(2) . 2_445
O108 Na12 Na10 45.0(2) . .
O108 Na12 O37 97.8(3) . .
O108 Na12 O45 98.8(2) . .
O108 Na12 O105 84.0(2) . .
O109 Na12 W4 96.87(19) . .
O109 Na12 Tb1 146.4(2) . .
O109 Na12 Na5 97.7(2) . 2_445
O109 Na12 Na10 44.8(2) . .
O109 Na12 O37 169.1(3) . .
O109 Na12 O45 115.8(2) . .
O109 Na12 O105 84.2(2) . .
O109 Na12 O108 89.2(3) . .
W17 O2 Na6 92.2(2) . 1_455
W17 O2 Na9 132.3(4) . 1_455
Na9 O2 Na6 132.2(3) 1_455 1_455
W16 O4 W18 123.7(3) . .
W18 O5 W17 122.5(3) . .
W16 O6 W17 122.7(3) . .
W16 O6 Na2 97.5(2) . .
W16 O6 Na6 129.1(3) . 1_455
W17 O6 Na2 97.1(2) . .
W17 O6 Na6 104.8(2) . 1_455
Na6 O6 Na2 93.3(2) 1_455 .
W18 O7 W14 148.7(3) . .
W18 O8 W15 149.5(3) . .
W16 O9 W12 151.3(3) . .
W17 O10 W16 90.66(17) . .
W18 O10 W16 90.90(18) . .
W18 O10 W17 91.03(18) . .
P1 O10 W16 124.6(3) . .
P1 O10 W17 124.5(3) . .
P1 O10 W18 124.9(3) . .
W17 O11 W13 148.5(3) . .
W10 O12 Na2 101.3(2) . .
W16 O12 W10 148.7(3) . .
W16 O12 Na2 108.9(2) . .
W11 O13 Na2 101.0(2) . .
W17 O13 W11 147.3(3) . .
W17 O13 Na2 109.7(2) . .
W12 O15 W14 122.1(3) . .
W14 O16 Na3 137.1(3) . .
W14 O16 Na11 91.7(3) . .
Na3 O16 Na11 121.1(3) . .
W14 O17 W15 155.2(3) . .
W15 O18 Na5 133.6(3) . .
W15 O19 W13 123.9(3) . .
W11 O21 W13 158.0(3) . .
W11 O22 Na1 132.1(4) . 1_455
W10 O23 Na2 103.3(2) . .
W11 O23 W10 121.8(3) . .
W11 O23 Na2 103.5(2) . .
W10 O25 W12 154.9(3) . .
W10 O26 W11 90.61(18) . .
P1 O26 W10 127.3(3) . .
P1 O26 W11 127.4(3) . .
W14 O27 W12 89.27(19) . .
P1 O27 W12 128.3(3) . .
P1 O27 W14 128.6(3) . .
W13 O28 W15 89.33(19) . .
P1 O28 W13 127.7(3) . .
P1 O28 W15 127.7(3) . .
W14 O29 Tb3 138.2(3) . .
W14 O29 Na11 104.9(3) . .
Tb3 O29 Na11 109.7(3) . .
W15 O30 Tb2 138.3(3) . .
W13 O31 Tb2 137.2(3) . .
W11 O32 Tb1 138.6(3) . .
W10 O33 Tb1 139.9(3) . .
W12 O34 Tb3 137.6(3) . .
Tb3 O35 Na11 97.9(2) . .
Na12 O37 Tb1 104.9(2) . .
Tb1 O38 Tb3 174.6(3) . .
C1 O38 Tb1 93.4(5) . .
C1 O38 Tb3 92.0(5) . .
Tb3 O39 Tb2 173.8(3) . .
C1 O39 Tb2 93.3(5) . .
C1 O39 Tb3 92.9(5) . .
Tb1 O40 Tb2 174.5(3) . .
C1 O40 Tb1 93.0(5) . .
C1 O40 Tb2 92.5(5) . .
W8 O41 Tb3 138.3(3) . .
W9 O42 Tb2 141.6(3) . .
W7 O43 Tb2 138.4(3) . .
W5 O44 Tb1 135.9(3) . .
W4 O45 Tb1 136.2(3) . .
W4 O45 Na12 104.0(3) . .
Tb1 O45 Na12 105.1(2) . .
W6 O46 Tb3 138.1(3) . .
W6 O48 W8 123.3(3) . .
W8 O49 Na6 135.9(3) . .
W8 O50 W9 155.1(4) . .
W9 O51 Na8 94.3(4) . 4_666
W9 O51 Na8A 115.5(4) . 4_666
W7 O52 Na8 135.7(4) . 4_666
W9 O52 W7 121.2(3) . .
W9 O52 Na8 99.7(3) . 4_666
W7 O54 W5 157.3(3) . .
W5 O56 W4 123.5(3) . .
W4 O57 Na10 145.4(3) . .
W4 O58 W6 156.0(3) . .
W8 O59 W6 90.30(18) . .
P2 O59 W6 127.1(3) . .
P2 O59 W8 128.3(3) . .
W7 O60 W9 89.17(19) . .
P2 O60 W7 128.8(3) . .
P2 O60 W9 128.8(3) . .
W5 O61 W4 89.5(2) . .
P2 O61 W4 126.8(3) . .
P2 O61 W5 127.7(3) . .
W1 O62 W3 90.61(17) . .
W1A O62 W2A 90.2(4) . .
W1A O62 W3A 92.3(4) . .
W2 O62 W1 91.3(2) . .
W2 O62 W3 90.43(18) . .
W3A O62 W2A 88.6(4) . .
P2 O62 W1 125.2(3) . .
P2 O62 W1A 127.3(4) . .
P2 O62 W2 124.3(3) . .
P2 O62 W2A 121.3(4) . .
P2 O62 W3 124.6(3) . .
P2 O62 W3A 126.1(4) . .
W3 O63 W8 148.2(3) . .
W3A O63 W8 140.0(4) . .
W2A O64 W9 129.7(4) . .
W3 O64 W9 151.2(3) . .
W2 O65 W7 148.1(3) . .
W2A O65 W7 131.3(4) . .
W1A O66 W5 136.8(4) . .
W2 O66 W5 149.9(3) . .
W1 O67 W4 149.4(3) . .
W4 O67 W1A 135.1(4) . .
W1 O68 W6 149.1(3) . .
W6 O68 W3A 131.6(4) . .
W1 O70 W3 123.5(3) . .
W3 O71 Na1 133.0(4) . .
W3 O71 Na9 122.4(4) . .
Na9 O71 Na1 87.1(4) . .
W3 O72 W2 122.7(3) . .
W2 O74 W1 122.1(3) . .
Na1 O75 Na8 133.6(9) . 2
Na1 O75 Na9 101.0(8) . .
Na9 O75 Na8 50.3(5) . 2
Na1 O79 Na3 95.5(5) 2 .
Na4 O82 Na3 125.5(4) 3_465 .
Na11 O85 Na7 122.0(3) . .
Na3 O91A Na1 98.3(5) . 2
Na10 O92 Na9 95.2(5) . 2_545
Na7 O96 Na6 108.1(3) . .
Na2 O99 Na6 104.0(3) . 1_455
Na2 O101 Na4 96.5(3) . .
Na2 O102 Na4 98.6(3) . .
Na4 O103 Na5 127.4(4) . 2_445
Na12 O105 Na5 95.2(3) . 2_445
Na12 O106 Na5 95.1(3) . 2_445
Na12 O108 Na10 90.1(3) . .
Na12 O109 Na10 90.9(3) . .
Na8 O110 Na9 53.5(4) . 2_545
Na8 O110 Na10 92.1(4) . .
Na10 O110 Na9 95.6(4) . 2_545
W2A O111 Na8A 109.5(5) 4_565 .
Na8 O111 Na10 93.0(4) . .
Na10 O111 W2A 136.2(5) . 4_565
Na10 O111 Na8A 107.1(5) . .
Tb2 C1 Tb1 119.9(3) . .
Tb3 C1 Tb1 120.2(3) . .
Tb3 C1 Tb2 119.9(3) . .
O38 C1 Tb1 59.5(4) . .
O38 C1 Tb2 179.4(6) . .
O38 C1 Tb3 60.7(4) . .
O38 C1 O40 119.2(7) . .
O39 C1 Tb1 179.7(6) . .
O39 C1 Tb2 59.8(4) . .
O39 C1 Tb3 60.1(4) . .
O39 C1 O38 120.8(7) . .
O39 C1 O40 120.0(7) . .
O40 C1 Tb1 59.7(4) . .
O40 C1 Tb2 60.2(4) . .
O40 C1 Tb3 179.7(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O62 2.394(6) .
W1 O67 1.858(5) .
W1 O68 1.883(6) .
W1 O69 1.715(6) .
W1 O70 1.929(6) .
W1 O74 1.958(6) .
W1A O62 2.323(12) .
W1A O66 1.962(12) .
W1A O67 2.092(12) .
W2 O62 2.381(6) .
W2 O65 1.857(6) .
W2 O66 1.840(6) .
W2 O72 1.943(6) .
W2 O73 1.741(7) .
W2 O74 1.946(6) .
W2A O62 2.499(10) .
W2A O64 1.953(12) .
W2A O65 1.932(11) .
W2A O111 2.527(13) 4_666
W3 Na9 3.595(9) .
W3 O62 2.414(5) .
W3 O63 1.889(6) .
W3 O64 1.861(6) .
W3 O70 1.951(6) .
W3 O71 1.727(6) .
W3 O72 1.934(6) .
W3A O62 2.404(10) .
W3A O63 1.908(13) .
W3A O68 2.187(11) .
W4 Na12 3.492(3) .
W4 O45 1.822(5) .
W4 O56 1.936(6) .
W4 O57 1.725(6) .
W4 O58 1.874(6) .
W4 O61 2.435(6) .
W4 O67 1.992(5) .
W5 O44 1.783(5) .
W5 O54 1.909(6) .
W5 O55 1.733(6) .
W5 O56 1.908(6) .
W5 O61 2.374(6) .
W5 O66 2.030(5) .
W6 O46 1.807(5) .
W6 O47 1.720(6) .
W6 O48 1.919(5) .
W6 O58 1.923(6) .
W6 O59 2.418(6) .
W6 O68 2.003(6) .
W7 O43 1.803(6) .
W7 O52 1.922(6) .
W7 O54 1.891(6) .
W7 O60 2.341(6) .
W7 O65 2.033(5) .
W7 O118 1.729(6) .
W8 O41 1.815(5) .
W8 O48 1.956(5) .
W8 O49 1.721(6) .
W8 O50 1.891(6) .
W8 O59 2.392(6) .
W8 O63 1.989(6) .
W9 Na8 3.507(10) 4_666
W9 O42 1.787(5) .
W9 O50 1.907(6) .
W9 O51 1.720(6) .
W9 O52 1.915(6) .
W9 O60 2.421(6) .
W9 O64 2.023(6) .
W10 Na2 3.503(3) .
W10 O12 1.995(5) .
W10 O23 1.962(6) .
W10 O24 1.709(6) .
W10 O25 1.874(6) .
W10 O26 2.379(5) .
W10 O33 1.816(5) .
W11 Na2 3.484(3) .
W11 O13 2.011(5) .
W11 O21 1.885(6) .
W11 O22 1.729(5) .
W11 O23 1.932(6) .
W11 O26 2.408(5) .
W11 O32 1.815(6) .
W12 O9 1.980(5) .
W12 O14 1.723(6) .
W12 O15 1.903(6) .
W12 O25 1.917(6) .
W12 O27 2.406(6) .
W12 O34 1.812(5) .
W13 O11 2.036(5) .
W13 O19 1.924(6) .
W13 O20 1.738(6) .
W13 O21 1.903(6) .
W13 O28 2.405(5) .
W13 O31 1.780(5) .
W14 Na11 3.356(4) .
W14 O7 1.999(5) .
W14 O15 1.945(6) .
W14 O16 1.717(6) .
W14 O17 1.901(6) .
W14 O27 2.387(6) .
W14 O29 1.801(5) .
W15 O8 2.023(5) .
W15 O17 1.902(6) .
W15 O18 1.723(6) .
W15 O19 1.916(6) .
W15 O28 2.416(6) .
W15 O30 1.800(6) .
W16 Na2 3.585(3) .
W16 O3 1.712(5) .
W16 O4 1.932(6) .
W16 O6 1.940(5) .
W16 O9 1.865(5) .
W16 O10 2.407(5) .
W16 O12 1.866(5) .
W17 Na2 3.581(3) .
W17 Na6 3.427(4) 1_455
W17 O2 1.737(5) .
W17 O5 1.965(6) .
W17 O6 1.953(6) .
W17 O10 2.396(5) .
W17 O11 1.857(5) .
W17 O13 1.870(6) .
W18 O1 1.743(6) .
W18 O4 1.939(6) .
W18 O5 1.925(5) .
W18 O7 1.872(5) .
W18 O8 1.870(5) .
W18 O10 2.383(6) .
Tb1 Na12 3.872(4) .
Tb1 O32 2.283(6) .
Tb1 O33 2.252(5) .
Tb1 O37 2.461(6) .
Tb1 O38 2.428(6) .
Tb1 O40 2.432(6) .
Tb1 O44 2.266(6) .
Tb1 O45 2.301(5) .
Tb1 C1 2.813(8) .
Tb2 O30 2.268(6) .
Tb2 O31 2.280(5) .
Tb2 O36 2.400(6) .
Tb2 O39 2.428(6) .
Tb2 O40 2.435(6) .
Tb2 O42 2.273(5) .
Tb2 O43 2.286(6) .
Tb2 C1 2.804(8) .
Tb3 Na11 3.831(6) .
Tb3 O29 2.279(6) .
Tb3 O34 2.264(5) .
Tb3 O35 2.444(6) .
Tb3 O38 2.438(6) .
Tb3 O39 2.425(6) .
Tb3 O41 2.275(5) .
Tb3 O46 2.267(6) .
Tb3 C1 2.794(8) .
P1 O10 1.567(5) .
P1 O26 1.535(6) .
P1 O27 1.532(6) .
P1 O28 1.530(6) .
P2 O59 1.535(6) .
P2 O60 1.528(6) .
P2 O61 1.539(6) .
P2 O62 1.569(5) .
Na1 Na3 3.602(9) 2_545
Na1 Na9 3.392(13) .
Na1 O22 2.479(10) 1_655
Na1 O71 2.557(9) .
Na1 O75 2.05(2) .
Na1 O79 2.305(13) 2_545
Na1 O91A 2.405(13) 2_545
Na1 O112 2.392(15) 4_666
Na2 Na6 3.742(5) 1_455
Na2 O6 2.771(7) .
Na2 O12 2.516(6) .
Na2 O13 2.487(6) .
Na2 O23 2.484(6) .
Na2 O99 2.348(6) .
Na2 O101 2.420(8) .
Na2 O102 2.403(7) .
Na3 Na1 3.602(9) 2
Na3 O16 2.360(8) .
Na3 O79 2.557(12) .
Na3 O80 2.365(12) .
Na3 O81 2.399(9) .
Na3 O82 2.542(10) .
Na3 O91 2.37(2) .
Na3 O91A 2.356(13) .
Na4 O82 2.524(8) 3_465
Na4 O93 2.45(3) .
Na4 O93A 2.491(15) .
Na4 O100 2.327(7) .
Na4 O101 2.542(8) .
Na4 O102 2.482(8) .
Na4 O103 2.388(8) .
Na5 Na12 3.541(5) 2_455
Na5 O18 2.511(7) .
Na5 O97 2.341(8) .
Na5 O98 2.284(9) .
Na5 O103 2.394(8) 2_455
Na5 O105 2.418(7) 2_455
Na5 O106 2.456(8) 2_455
Na6 W17 3.427(4) 1_655
Na6 Na2 3.742(5) 1_655
Na6 Na7 3.833(5) .
Na6 O2 2.887(7) 1_655
Na6 O6 2.360(6) 1_655
Na6 O49 2.360(6) .
Na6 O94 2.279(9) .
Na6 O96 2.395(9) .
Na6 O99 2.402(8) 1_655
Na7 Na11 4.155(6) .
Na7 O85 2.407(8) .
Na7 O86 2.325(8) .
Na7 O87 2.350(7) .
Na7 O88 2.357(7) .
Na7 O96 2.340(8) .
Na8 W9 3.507(10) 4_565
Na8 Na8 3.79(2) 3
Na8 Na9 2.179(13) 2_545
Na8 O51 2.929(13) 4_565
Na8 O52 2.632(11) 4_565
Na8 O75 2.72(2) 2_545
Na8 O110 2.289(15) .
Na8 O111 2.244(16) .
Na8A Na8A 1.21(3) 3
Na8A O51 2.911(15) 4_565
Na8A O111 2.831(19) .
Na8A O9A 2.38(3) 2_545
Na9 Na8 2.179(13) 2
Na9 Na10 3.670(12) 2
Na9 O2 2.443(10) 1_655
Na9 O71 2.360(11) .
Na9 O75 2.34(2) .
Na9 O92 2.52(2) 2
Na9 O110 2.526(13) 2
Na10 Na9 3.670(12) 2_545
Na10 Na12 3.364(7) .
Na10 O57 2.804(9) .
Na10 O92 2.449(14) .
Na10 O92A 2.24(3) .
Na10 O108 2.380(8) .
Na10 O109 2.371(9) .
Na10 O110 2.427(12) .
Na10 O111 2.437(11) .
Na11 O16 2.833(8) .
Na11 O29 2.406(7) .
Na11 O35 2.634(9) .
Na11 O84 2.306(11) .
Na11 O85 2.343(9) .
Na11 O90 2.18(2) .
Na11 O90A 2.426(14) .
Na12 Na5 3.541(5) 2_445
Na12 O37 2.425(7) .
Na12 O45 2.572(7) .
Na12 O105 2.376(7) .
Na12 O106 2.343(7) .
Na12 O108 2.373(8) .
Na12 O109 2.351(8) .
O2 Na6 2.887(7) 1_455
O2 Na9 2.443(10) 1_455
O6 Na6 2.360(6) 1_455
O22 Na1 2.479(10) 1_455
O38 C1 1.282(10) .
O39 C1 1.269(10) .
O40 C1 1.291(10) .
O51 Na8 2.929(13) 4_666
O51 Na8A 2.911(15) 4_666
O52 Na8 2.632(11) 4_666
O75 Na8 2.72(2) 2
O79 Na1 2.305(13) 2
O82 Na4 2.524(8) 3_465
O91A Na1 2.405(13) 2
O92 Na9 2.52(2) 2_545
O99 Na6 2.402(8) 1_455
O103 Na5 2.394(8) 2_445
O105 Na5 2.418(7) 2_445
O106 Na5 2.456(8) 2_445
O110 Na9 2.526(13) 2_545
O111 W2A 2.527(13) 4_565
O112 Na1 2.392(15) 4_565
O9A Na8A 2.38(3) 2
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Tb1 O38 C1 Tb3 -179.8(3) . .
Tb1 O38 C1 O39 -179.9(6) . .
Tb1 O38 C1 O40 0.5(7) . .
Tb1 O40 C1 Tb2 179.7(3) . .
Tb1 O40 C1 O38 -0.5(7) . .
Tb1 O40 C1 O39 179.9(6) . .
Tb2 O39 C1 Tb3 -179.9(3) . .
Tb2 O39 C1 O38 -179.8(6) . .
Tb2 O39 C1 O40 -0.2(7) . .
Tb2 O40 C1 Tb1 -179.7(3) . .
Tb2 O40 C1 O38 179.8(6) . .
Tb2 O40 C1 O39 0.2(7) . .
Tb3 O38 C1 Tb1 179.8(3) . .
Tb3 O38 C1 O39 -0.1(7) . .
Tb3 O38 C1 O40 -179.7(6) . .
Tb3 O39 C1 Tb2 179.9(3) . .
Tb3 O39 C1 O38 0.1(7) . .
Tb3 O39 C1 O40 179.7(6) . .
Na2 W10 O25 W12 45.1(8) . .
Na2 W10 O33 Tb1 -67.6(5) . .
Na2 W11 O21 W13 -45.5(9) . .
Na2 W11 O22 Na1 -97.1(4) . 1_455
Na2 W11 O32 Tb1 60.8(6) . .
Na2 W16 O9 W12 -23.7(8) . .
Na2 W16 O12 W10 -164.2(7) . .
Na2 W17 O2 Na6 -59.15(16) . 1_455
Na2 W17 O2 Na9 101.8(5) . 1_455
Na2 W17 O11 W13 27.0(7) . .
Na2 W17 O13 W11 158.9(7) . .
Na6 W17 O2 Na9 160.9(6) 1_455 1_455
Na6 W17 O11 W13 158.1(3) 1_455 .
Na6 W17 O13 W11 174.7(5) 1_455 .
Na6 W17 O13 Na2 15.8(3) 1_455 .
Na8 W9 O42 Tb2 -96.2(5) 4_666 .
Na9 W3 O63 W8 -89.1(6) . .
Na9 W3 O64 W9 118.5(8) . .
Na9 W3 O71 Na1 120.7(7) . .
Na11 W14 O16 Na3 142.2(6) . .
Na11 W14 O29 Tb3 -145.2(6) . .
Na12 W4 O45 Tb1 130.4(5) . .
Na12 W4 O57 Na10 -53.4(5) . .
Na12 W4 O58 W6 157.4(7) . .
O1 W18 O7 W14 124.8(6) . .
O1 W18 O8 W15 -124.6(6) . .
O2 W17 O11 W13 129.6(6) . .
O2 W17 O13 W11 -126.2(6) . .
O2 W17 O13 Na2 74.9(3) . .
O3 W16 O9 W12 -126.9(7) . .
O3 W16 O12 W10 120.7(6) . .
O3 W16 O12 Na2 -75.1(3) . .
O4 W16 O9 W12 132.7(7) . .
O4 W16 O12 W10 -67.2(9) . .
O4 W16 O12 Na2 97.1(6) . .
O4 W18 O7 W14 -135.2(6) . .
O4 W18 O8 W15 61.1(10) . .
O5 W17 O2 Na6 76.9(2) . 1_455
O5 W17 O2 Na9 -122.2(5) . 1_455
O5 W17 O11 W13 -130.9(6) . .
O5 W17 O13 W11 66.0(9) . .
O5 W17 O13 Na2 -92.9(6) . .
O5 W18 O7 W14 -64.3(9) . .
O5 W18 O8 W15 135.5(6) . .
O6 W16 O9 W12 58.1(11) . .
O6 W16 O12 W10 -139.8(6) . .
O6 W16 O12 Na2 24.4(2) . .
O6 W17 O2 Na6 -9.4(3) . 1_455
O6 W17 O2 Na9 151.5(5) . 1_455
O6 W17 O11 W13 -58.2(10) . .
O6 W17 O13 W11 136.1(6) . .
O6 W17 O13 Na2 -22.8(2) . .
O7 W14 O16 Na3 -30.2(5) . .
O7 W14 O16 Na11 -172.4(2) . .
O7 W14 O29 Tb3 25.4(11) . .
O7 W14 O29 Na11 170.6(7) . .
O7 W18 O8 W15 -22.0(6) . .
O8 W15 O18 Na5 45.2(4) . .
O8 W15 O30 Tb2 -31.9(11) . .
O8 W18 O7 W14 21.6(6) . .
O9 W12 O34 Tb3 -32.7(11) . .
O9 W16 O12 W10 17.4(6) . .
O9 W16 O12 Na2 -178.3(3) . .
O10 W16 O9 W12 60.2(7) . .
O10 W16 O12 W10 -66.3(6) . .
O10 W16 O12 Na2 98.0(2) . .
O10 W17 O2 Na6 30.5(14) . 1_455
O10 W17 O2 Na9 -168.6(10) . 1_455
O10 W17 O11 W13 -58.1(6) . .
O10 W17 O13 W11 62.6(6) . .
O10 W17 O13 Na2 -96.3(2) . .
O10 W18 O7 W14 -62.2(6) . .
O10 W18 O8 W15 61.8(6) . .
O10 P1 O26 W10 63.6(4) . .
O10 P1 O26 W11 -63.3(4) . .
O10 P1 O27 W12 -63.6(4) . .
O10 P1 O27 W14 63.9(4) . .
O10 P1 O28 W13 62.5(5) . .
O10 P1 O28 W15 -62.8(4) . .
O11 W13 O31 Tb2 34.9(12) . .
O11 W17 O2 Na6 167.6(2) . 1_455
O11 W17 O2 Na9 -31.4(6) . 1_455
O11 W17 O13 W11 -22.1(6) . .
O11 W17 O13 Na2 179.0(3) . .
O12 W10 O25 W12 40.5(7) . .
O12 W10 O33 Tb1 9.3(11) . .
O12 W16 O9 W12 -22.2(7) . .
O13 W11 O21 W13 -43.4(8) . .
O13 W11 O22 Na1 -54.0(4) . 1_455
O13 W11 O32 Tb1 -24.7(12) . .
O13 W17 O2 Na6 -98.3(2) . 1_455
O13 W17 O2 Na9 62.6(5) . 1_455
O13 W17 O11 W13 26.2(6) . .
O14 W12 O34 Tb3 157.3(4) . .
O15 W12 O34 Tb3 56.3(5) . .
O15 W14 O16 Na3 54.5(5) . .
O15 W14 O16 Na11 -87.8(2) . .
O15 W14 O29 Tb3 -55.3(5) . .
O15 W14 O29 Na11 89.9(3) . .
O16 W14 O29 Tb3 -154.3(4) . .
O16 W14 O29 Na11 -9.1(3) . .
O17 W14 O16 Na3 -115.1(5) . .
O17 W14 O16 Na11 102.6(2) . .
O17 W14 O29 Tb3 103.0(5) . .
O17 W14 O29 Na11 -111.8(3) . .
O17 W15 O18 Na5 128.8(4) . .
O17 W15 O30 Tb2 -105.5(5) . .
O18 W15 O30 Tb2 151.9(5) . .
O19 W13 O31 Tb2 -53.5(5) . .
O19 W15 O18 Na5 -40.1(4) . .
O19 W15 O30 Tb2 51.5(5) . .
O20 W13 O31 Tb2 -156.2(4) . .
O21 W11 O22 Na1 30.7(5) . 1_455
O21 W11 O32 Tb1 -102.5(5) . .
O21 W13 O31 Tb2 102.4(5) . .
O22 W11 O21 W13 -138.2(8) . .
O22 W11 O32 Tb1 155.0(5) . .
O23 W10 O25 W12 -16.5(12) . .
O23 W10 O33 Tb1 -60.0(5) . .
O23 W11 O21 W13 15.1(12) . .
O23 W11 O22 Na1 -138.4(4) . 1_455
O23 W11 O32 Tb1 53.7(5) . .
O24 W10 O25 W12 136.1(7) . .
O24 W10 O33 Tb1 -158.3(4) . .
O25 W10 O33 Tb1 98.6(5) . .
O25 W12 O34 Tb3 -101.0(4) . .
O26 W10 O25 W12 -40.1(7) . .
O26 W10 O33 Tb1 13.2(4) . .
O26 W11 O21 W13 38.2(8) . .
O26 W11 O32 Tb1 -18.8(5) . .
O26 P1 O10 W16 -59.6(4) . .
O26 P1 O10 W17 59.8(4) . .
O26 P1 O10 W18 -179.8(3) . .
O26 P1 O27 W12 54.8(5) . .
O26 P1 O27 W14 -177.7(3) . .
O26 P1 O28 W13 -56.5(4) . .
O26 P1 O28 W15 178.1(3) . .
O27 W12 O34 Tb3 -16.8(4) . .
O27 W14 O29 Tb3 17.6(4) . .
O27 W14 O29 Na11 162.8(3) . .
O27 P1 O10 W16 60.4(4) . .
O27 P1 O10 W17 179.8(3) . .
O27 P1 O10 W18 -59.8(4) . .
O27 P1 O26 W10 -54.2(4) . .
O27 P1 O26 W11 179.0(3) . .
O27 P1 O28 W13 -179.7(3) . .
O27 P1 O28 W15 54.9(4) . .
O28 W13 O31 Tb2 18.7(4) . .
O28 W15 O30 Tb2 -20.5(4) . .
O28 P1 O10 W16 -179.8(3) . .
O28 P1 O10 W17 -60.5(4) . .
O28 P1 O10 W18 59.9(4) . .
O28 P1 O26 W10 -177.1(3) . .
O28 P1 O26 W11 56.0(4) . .
O28 P1 O27 W12 177.7(3) . .
O28 P1 O27 W14 -54.8(4) . .
O29 W14 O16 Na3 149.7(5) . .
O29 W14 O16 Na11 7.5(3) . .
O30 W15 O18 Na5 -136.0(4) . .
O32 W11 O21 W13 120.0(8) . .
O32 W11 O22 Na1 126.1(4) . 1_455
O33 W10 O25 W12 -122.1(7) . .
O41 W8 O49 Na6 -145.0(4) . .
O41 W8 O50 W9 119.2(7) . .
O42 W9 O51 Na8 118.3(3) . 4_666
O42 W9 O51 Na8A 136.6(4) . 4_666
O43 W7 O54 W5 119.0(9) . .
O45 W4 O57 Na10 -75.0(5) . .
O45 W4 O58 W6 118.4(8) . .
O47 W6 O46 Tb3 -149.7(4) . .
O48 W6 O46 Tb3 -49.5(5) . .
O48 W8 O41 Tb3 56.7(4) . .
O48 W8 O49 Na6 -53.3(5) . .
O48 W8 O50 W9 19.2(12) . .
O49 W8 O41 Tb3 155.3(4) . .
O49 W8 O50 W9 -139.3(7) . .
O50 W8 O41 Tb3 -101.5(4) . .
O50 W8 O49 Na6 118.7(5) . .
O50 W9 O42 Tb2 102.8(5) . .
O50 W9 O51 Na8 -146.8(3) . 4_666
O50 W9 O51 Na8A -128.5(4) . 4_666
O51 W9 O42 Tb2 -154.2(5) . .
O52 W7 O43 Tb2 57.2(5) . .
O52 W7 O54 W5 8.4(13) . .
O52 W9 O42 Tb2 -54.3(5) . .
O52 W9 O51 Na8 22.7(3) . 4_666
O52 W9 O51 Na8A 41.0(4) . 4_666
O54 W5 O44 Tb1 101.0(4) . .
O54 W7 O43 Tb2 -101.6(5) . .
O55 W5 O44 Tb1 -156.7(4) . .
O56 W4 O45 Tb1 56.8(5) . .
O56 W4 O45 Na12 -73.6(3) . .
O56 W4 O57 Na10 18.6(6) . .
O56 W4 O58 W6 17.9(12) . .
O56 W5 O44 Tb1 -55.8(5) . .
O57 W4 O45 Tb1 157.0(4) . .
O57 W4 O45 Na12 26.6(3) . .
O57 W4 O58 W6 -139.6(8) . .
O58 W4 O45 Tb1 -99.5(4) . .
O58 W4 O45 Na12 130.1(3) . .
O58 W4 O57 Na10 -170.5(5) . .
O58 W6 O46 Tb3 108.3(4) . .
O59 W6 O46 Tb3 22.6(4) . .
O59 W8 O41 Tb3 -16.1(4) . .
O59 W8 O50 W9 37.0(7) . .
O59 P2 O60 W7 177.6(3) . .
O59 P2 O60 W9 -54.0(5) . .
O59 P2 O61 W4 57.3(4) . .
O59 P2 O61 W5 -178.5(3) . .
O59 P2 O62 W1 -60.4(4) . .
O59 P2 O62 W1A -123.7(5) . .
O59 P2 O62 W2 178.5(3) . .
O59 P2 O62 W2A 118.5(4) . .
O59 P2 O62 W3 59.7(4) . .
O59 P2 O62 W3A 4.5(6) . .
O60 W7 O43 Tb2 -17.3(4) . .
O60 W7 O54 W5 35.9(8) . .
O60 W9 O42 Tb2 18.2(5) . .
O60 P2 O59 W6 -178.0(3) . .
O60 P2 O59 W8 54.7(4) . .
O60 P2 O61 W4 180.0(3) . .
O60 P2 O61 W5 -55.8(5) . .
O60 P2 O62 W1 -179.5(3) . .
O60 P2 O62 W1A 117.2(5) . .
O60 P2 O62 W2 59.5(4) . .
O60 P2 O62 W2A -0.6(5) . .
O60 P2 O62 W3 -59.4(4) . .
O60 P2 O62 W3A -114.6(5) . .
O61 W4 O45 Tb1 -15.0(4) . .
O61 W4 O45 Na12 -145.4(3) . .
O61 W4 O58 W6 37.1(8) . .
O61 W5 O44 Tb1 17.5(4) . .
O61 P2 O59 W6 -54.8(4) . .
O61 P2 O59 W8 178.0(3) . .
O61 P2 O60 W7 54.3(4) . .
O61 P2 O60 W9 -177.3(3) . .
O61 P2 O62 W1 60.1(4) . .
O61 P2 O62 W1A -3.2(6) . .
O61 P2 O62 W2 -61.0(4) . .
O61 P2 O62 W2A -121.0(4) . .
O61 P2 O62 W3 -179.8(3) . .
O61 P2 O62 W3A 125.0(5) . .
O62 W1 O67 W4 66.2(6) . .
O62 W1 O68 W6 -59.5(7) . .
O62 W2 O65 W7 62.0(6) . .
O62 W2 O66 W5 -63.7(7) . .
O62 W3 O63 W8 65.5(6) . .
O62 W3 O64 W9 -58.6(7) . .
O62 P2 O59 W6 64.1(4) . .
O62 P2 O59 W8 -63.1(4) . .
O62 P2 O60 W7 -64.7(4) . .
O62 P2 O60 W9 63.8(5) . .
O62 P2 O61 W4 -61.3(4) . .
O62 P2 O61 W5 62.9(4) . .
O63 W3 O64 W9 24.2(7) . .
O63 W3 O71 Na1 -163.3(5) . .
O63 W3 O71 Na9 76.0(5) . .
O63 W8 O41 Tb3 -16.7(11) . .
O63 W8 O49 Na6 32.6(5) . .
O63 W8 O50 W9 -43.7(7) . .
O64 W3 O63 W8 -18.7(7) . .
O64 W3 O71 Na1 104.7(5) . .
O64 W3 O71 Na9 -16.0(5) . .
O64 W9 O42 Tb2 32.6(12) . .
O64 W9 O51 Na8 -64.0(3) . 4_666
O64 W9 O51 Na8A -45.7(4) . 4_666
O65 W2 O66 W5 19.7(7) . .
O65 W7 O43 Tb2 -23.5(12) . .
O65 W7 O54 W5 -45.1(8) . .
O66 W2 O65 W7 -20.8(6) . .
O66 W5 O44 Tb1 30.9(11) . .
O67 W1 O68 W6 23.4(7) . .
O67 W4 O45 Tb1 -21.0(11) . .
O67 W4 O45 Na12 -151.4(7) . .
O67 W4 O57 Na10 104.4(5) . .
O67 W4 O58 W6 -43.7(8) . .
O68 W1 O67 W4 -18.0(7) . .
O68 W6 O46 Tb3 38.2(11) . .
O69 W1 O67 W4 -121.3(7) . .
O69 W1 O68 W6 127.2(7) . .
O70 W1 O67 W4 67.3(11) . .
O70 W1 O68 W6 -133.0(7) . .
O70 W3 O63 W8 138.4(7) . .
O70 W3 O64 W9 -54.8(12) . .
O70 W3 O71 Na1 -74.3(5) . .
O70 W3 O71 Na9 165.1(5) . .
O71 W3 O63 W8 -121.7(6) . .
O71 W3 O64 W9 127.9(7) . .
O72 W2 O65 W7 135.8(6) . .
O72 W2 O66 W5 -67.0(10) . .
O72 W3 O63 W8 68.0(10) . .
O72 W3 O64 W9 -131.7(7) . .
O72 W3 O71 Na1 12.6(5) . .
O72 W3 O71 Na9 -108.1(5) . .
O73 W2 O65 W7 -123.7(6) . .
O73 W2 O66 W5 121.5(7) . .
O74 W1 O67 W4 139.4(7) . .
O74 W1 O68 W6 -60.8(11) . .
O74 W2 O65 W7 66.4(10) . .
O74 W2 O66 W5 -137.3(7) . .
O118 W7 O43 Tb2 157.7(4) . .
O118 W7 O54 W5 -138.0(8) . .
