#------------------------------------------------------------------------------
#$Date: 2019-11-23 06:11:59 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232303 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/73/4347395.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347395
loop_
_publ_author_name
'Giansiracusa, Marcus J.'
'Vonci, Michele'
'Van den Heuvel, Willem'
'Gable, Robert W.'
'Moubaraki, Boujemaa'
'Murray, Keith S.'
'Yu, Dehong'
'Mole, Richard A.'
'Soncini, Alessandro'
'Boskovic, Colette'
_publ_section_title
;
 Carbonate-Bridged Lanthanoid Triangles: Single-Molecule Magnet Behavior,
 Inelastic Neutron Scattering, and Ab Initio Studies.
;
_journal_issue                   11
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5201
_journal_page_last               5214
_journal_paper_doi               10.1021/acs.inorgchem.6b00108
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C Dy3 Na11 O103.52 P2 W18, 8.55(O1.46)'
_chemical_formula_sum            'C H84 Dy3 Na11 O116 P2 W18'
_chemical_formula_weight         6064.31
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_audit_creation_date             2015-12-15
_audit_creation_method
;
Olex2 1.2
(compiled 2015.09.30 svn.r3233 for OlexSys, GUI svn.r5103)
;
_cell_angle_alpha                90
_cell_angle_beta                 111.6424(7)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.38612(11)
_cell_length_b                   26.04781(13)
_cell_length_c                   23.41801(14)
_cell_measurement_reflns_used    36003
_cell_measurement_temperature    130.01(10)
_cell_measurement_theta_max      74.5550
_cell_measurement_theta_min      3.2070
_cell_volume                     9857.69(11)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      130.01(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 10.2273
_diffrn_detector_type            Atlas
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
  1 omega  -36.00   25.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      -41.0592   37.0000  -60.0000 61

#__ type_ start__ end____ width___ exp.time_
  2 omega  -53.00  -17.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      -41.0592  125.0000   60.0000 36

#__ type_ start__ end____ width___ exp.time_
  3 omega   31.00   98.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -       41.0592 -125.0000 -120.0000 67

#__ type_ start__ end____ width___ exp.time_
  4 omega   40.00   93.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -45.0000 -120.0000 53

#__ type_ start__ end____ width___ exp.time_
  5 omega   97.00  133.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -61.0000  -60.0000 36

#__ type_ start__ end____ width___ exp.time_
  6 omega   76.00  115.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393 -111.0000   30.0000 39

#__ type_ start__ end____ width___ exp.time_
  7 omega   65.00  142.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -77.0000   60.0000 77

#__ type_ start__ end____ width___ exp.time_
  8 omega   78.00  178.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393   30.0000  -60.0000 100

#__ type_ start__ end____ width___ exp.time_
  9 omega  102.00  167.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  111.0000 -150.0000 65

#__ type_ start__ end____ width___ exp.time_
 10 omega   82.00  177.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393   61.0000 -180.0000 95

#__ type_ start__ end____ width___ exp.time_
 11 omega   54.00   90.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -30.0000   30.0000 36

#__ type_ start__ end____ width___ exp.time_
 12 omega   62.00   88.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -30.0000   60.0000 26

#__ type_ start__ end____ width___ exp.time_
 13 omega   42.00   90.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -30.0000  150.0000 48

#__ type_ start__ end____ width___ exp.time_
 14 omega   32.00   82.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -       41.0592 -125.0000   60.0000 50

#__ type_ start__ end____ width___ exp.time_
 15 omega   33.00   88.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -45.0000  -60.0000 55

#__ type_ start__ end____ width___ exp.time_
 16 omega   29.00  109.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  -94.0000 -120.0000 80

#__ type_ start__ end____ width___ exp.time_
 17 omega   87.00  112.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393 -111.0000 -180.0000 25

#__ type_ start__ end____ width___ exp.time_
 18 omega  111.00  142.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  178.0000   90.0000 31

#__ type_ start__ end____ width___ exp.time_
 19 omega   63.00   88.00   1.0000   12.5000
omega____ theta____ kappa____ phi______ frames
    -      107.9393  178.0000   90.0000 25

#__ type_ start__ end____ width___ exp.time_
 20 omega -110.00   37.00   1.0000    5.0000
omega____ theta____ kappa____ phi______ frames
    -      -41.0592    0.0000  -90.0000 147
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      0.0018484000
_diffrn_orient_matrix_UB_12      -0.0398433000
_diffrn_orient_matrix_UB_13      -0.0331666000
_diffrn_orient_matrix_UB_21      -0.0188021000
_diffrn_orient_matrix_UB_22      -0.0405153000
_diffrn_orient_matrix_UB_23      0.0240401000
_diffrn_orient_matrix_UB_31      -0.0419637000
_diffrn_orient_matrix_UB_32      0.0164338000
_diffrn_orient_matrix_UB_33      -0.0212743000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0467
_diffrn_reflns_av_unetI/netI     0.0377
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            68519
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         74.845
_diffrn_reflns_theta_min         3.222
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_type              'SuperNova (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    51.623
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.57040
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    4.086
_exptl_crystal_description       'hexagonal-faced rod'
_exptl_crystal_F_000             10796
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.11
_refine_diff_density_max         2.980
_refine_diff_density_min         -1.782
_refine_diff_density_rms         0.312
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.048
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1318
_refine_ls_number_reflns         19888
_refine_ls_number_restraints     24
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.0380
_refine_ls_R_factor_gt           0.0326
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0440P)²+54.9948P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0758
_refine_ls_wR_factor_ref         0.0796
_reflns_Friedel_coverage         0.000
_reflns_number_gt                18153
_reflns_number_total             19888
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic6b00108_si_002.cif
_cod_data_source_block           mg1dysp
_cod_original_cell_volume        9857.68(11)
_cod_database_code               4347395
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_reflns_odcompleteness_completeness 99.96
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     67.62
_olex2_refinement_description
;
1. Uiso/Uaniso restraints and constraints
Uanis(O5) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.01
Uanis(O8) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(O10) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(O26) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uiso(O90) = Uiso(O90A)
Uanis(O91) = Uanis(O91A)
Uanis(O92) = Uanis(O92A)
Uanis(O93) = Uanis(O93A)
Uiso(O95) = Uiso(O95A)
Uanis(Na9) = Uanis(Na9A)
Uanis(Na8) = Uanis(Na8A)
2. Others
 Sof(O90A)=1-FVAR(1)
 Sof(O90)=FVAR(1)
 Sof(O91A)=1-FVAR(2)
 Sof(O91)=FVAR(2)
 Sof(O92A)=1-FVAR(3)
 Sof(O92)=FVAR(3)
 Sof(O93A)=1-FVAR(4)
 Sof(O93)=FVAR(4)
 Sof(O95A)=1-FVAR(5)
 Sof(O95)=FVAR(5)
 Sof(Na9A)=1-FVAR(6)
 Sof(Na9)=FVAR(6)
 Sof(Na8A)=1-FVAR(7)
 Sof(Na8)=FVAR(7)
 Sof(O107)=1-FVAR(8)
 Sof(O89)=FVAR(8)
;
_shelx_shelxl_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W15 W -0.10577(2) 0.62065(2) 0.31879(2) 0.01236(7) Uani 1 1 d . . . .
W17 W -0.39009(2) 0.53911(2) 0.25690(2) 0.01071(7) Uani 1 1 d . . . .
W6 W 0.12395(2) 0.40882(2) 0.11297(2) 0.01069(7) Uani 1 1 d . . . .
W12 W -0.23858(2) 0.53287(2) 0.05648(2) 0.01001(7) Uani 1 1 d . . . .
W5 W 0.07651(2) 0.28810(2) 0.32194(2) 0.01180(7) Uani 1 1 d . . . .
W11 W -0.28639(2) 0.41235(2) 0.26800(2) 0.01115(7) Uani 1 1 d . . . .
W10 W -0.31359(2) 0.42003(2) 0.11686(2) 0.01024(7) Uani 1 1 d . . . .
W7 W 0.18662(2) 0.39396(2) 0.42751(2) 0.01155(7) Uani 1 1 d . . . .
W4 W 0.04850(2) 0.29443(2) 0.17133(2) 0.01123(7) Uani 1 1 d . . . .
W1 W 0.27450(2) 0.31248(2) 0.21191(2) 0.01258(7) Uani 1 1 d . . . .
W8 W 0.22693(2) 0.50376(2) 0.21150(2) 0.01144(7) Uani 1 1 d . . . .
W13 W -0.17665(2) 0.51803(2) 0.37322(2) 0.01178(7) Uani 1 1 d . . . .
W3 W 0.37722(2) 0.40817(2) 0.31026(2) 0.01337(7) Uani 1 1 d . . . .
W14 W -0.13930(2) 0.62766(2) 0.15296(2) 0.01140(7) Uani 1 1 d . . . .
W18 W -0.31925(2) 0.64267(2) 0.20178(2) 0.01075(7) Uani 1 1 d . . . .
W16 W -0.41952(2) 0.54594(2) 0.10458(2) 0.01023(7) Uani 1 1 d . . . .
W2 W 0.30436(2) 0.30511(2) 0.36419(2) 0.01304(7) Uani 1 1 d . . . .
W9 W 0.25974(2) 0.49563(2) 0.37686(2) 0.01208(7) Uani 1 1 d . . . .
Dy3 Dy -0.00904(3) 0.51218(2) 0.14504(2) 0.01145(9) Uani 1 1 d . . . .
Dy2 Dy 0.03247(3) 0.50277(2) 0.36051(2) 0.01171(9) Uani 1 1 d . . . .
Dy1 Dy -0.10807(3) 0.36408(2) 0.22346(2) 0.01159(9) Uani 1 1 d . . . .
P1 P -0.21816(10) 0.52401(7) 0.21317(8) 0.0098(3) Uani 1 1 d . . . .
P2 P 0.16081(11) 0.39445(7) 0.27187(8) 0.0107(3) Uani 1 1 d . . . .
O52 O 0.2644(3) 0.4491(2) 0.4418(2) 0.0154(10) Uani 1 1 d . . . .
O66 O 0.1984(3) 0.2794(2) 0.3371(2) 0.0145(10) Uani 1 1 d . . . .
O41 O 0.1262(3) 0.5349(2) 0.1831(2) 0.0146(10) Uani 1 1 d . . . .
O27 O -0.1822(3) 0.54292(19) 0.1656(2) 0.0123(10) Uani 1 1 d . . . .
O45 O -0.0526(3) 0.3186(2) 0.1639(2) 0.0134(10) Uani 1 1 d . . . .
O73 O 0.3590(4) 0.2602(2) 0.4197(3) 0.0206(12) Uani 1 1 d . . . .
O7 O -0.2497(3) 0.6434(2) 0.1577(2) 0.0147(10) Uani 1 1 d . . . .
O54 O 0.1193(3) 0.3389(2) 0.3850(2) 0.0153(10) Uani 1 1 d . . . .
O28 O -0.1595(3) 0.5375(2) 0.2787(2) 0.0118(10) Uani 1 1 d . . . .
O43 O 0.1006(3) 0.4354(2) 0.4194(2) 0.0132(10) Uani 1 1 d . . . .
O35 O 0.0075(3) 0.5621(2) 0.0619(2) 0.0153(10) Uani 1 1 d . . . .
O47 O 0.1198(3) 0.3985(2) 0.0388(2) 0.0136(10) Uani 1 1 d . . . .
O62 O 0.2455(3) 0.3662(2) 0.2843(2) 0.0128(10) Uani 1 1 d . . . .
O44 O -0.0257(3) 0.3133(2) 0.2991(2) 0.0146(10) Uani 1 1 d . . . .
O57 O 0.0215(3) 0.2454(2) 0.1183(3) 0.0175(11) Uani 1 1 d . . . .
O33 O -0.2236(3) 0.3789(2) 0.1412(2) 0.0136(10) Uani 1 1 d . . . .
O24 O -0.3803(3) 0.3842(2) 0.0578(3) 0.0175(11) Uani 1 1 d . . . .
O30 O -0.0103(3) 0.5854(2) 0.3436(3) 0.0151(10) Uani 1 1 d . . . .
O15 O -0.2052(3) 0.6030(2) 0.0713(2) 0.0138(10) Uani 1 1 d . . . .
O21 O -0.2241(3) 0.4560(2) 0.3329(2) 0.0159(10) Uani 1 1 d . . . .
O61 O 0.0919(3) 0.3544(2) 0.2572(2) 0.0137(10) Uani 1 1 d . . . .
O10 O -0.3028(3) 0.5520(2) 0.2000(2) 0.0118(10) Uani 1 1 d U . . .
O68 O 0.2241(3) 0.3647(2) 0.1557(2) 0.0145(10) Uani 1 1 d . . . .
O48 O 0.1997(3) 0.4652(2) 0.1352(2) 0.0124(10) Uani 1 1 d . . . .
O26 O -0.2337(3) 0.46546(19) 0.2068(2) 0.0106(9) Uani 1 1 d U . . .
O8 O -0.2265(3) 0.6386(2) 0.2744(2) 0.0136(10) Uani 1 1 d U . . .
O11 O -0.2934(3) 0.5442(2) 0.3253(2) 0.0137(10) Uani 1 1 d . . . .
O14 O -0.2823(3) 0.5333(2) -0.0229(2) 0.0157(10) Uani 1 1 d . . . .
O32 O -0.1968(3) 0.3740(2) 0.2733(2) 0.0150(10) Uani 1 1 d . . . .
O56 O 0.0583(3) 0.2564(2) 0.2445(2) 0.0137(10) Uani 1 1 d . . . .
O40 O -0.0360(3) 0.4353(2) 0.2884(2) 0.0157(10) Uani 1 1 d . . . .
O38 O -0.0562(3) 0.4397(2) 0.1889(2) 0.0125(10) Uani 1 1 d . . . .
O23 O -0.3468(3) 0.3937(2) 0.1834(2) 0.0119(10) Uani 1 1 d . . . .
O6 O -0.4621(3) 0.5380(2) 0.1703(2) 0.0127(10) Uani 1 1 d . . . .
O12 O -0.3937(3) 0.4755(2) 0.1138(2) 0.0127(10) Uani 1 1 d . . . .
O50 O 0.2428(3) 0.5156(2) 0.2946(2) 0.0136(10) Uani 1 1 d . . . .
O64 O 0.3420(3) 0.4473(2) 0.3621(2) 0.0161(11) Uani 1 1 d . . . .
O36 O 0.0881(3) 0.5413(2) 0.4603(2) 0.0164(11) Uani 1 1 d . . . .
O42 O 0.1633(3) 0.5234(2) 0.3717(3) 0.0152(10) Uani 1 1 d . . . .
O70 O 0.3687(3) 0.3570(2) 0.2474(3) 0.0166(11) Uani 1 1 d . . . .
O74 O 0.3154(4) 0.2771(2) 0.2906(2) 0.0163(11) Uani 1 1 d . . . .
O46 O 0.0341(3) 0.4485(2) 0.0982(2) 0.0132(10) Uani 1 1 d . . . .
O51 O 0.3300(3) 0.5405(2) 0.4201(3) 0.0186(11) Uani 1 1 d . . . .
O18 O -0.0755(3) 0.6793(2) 0.3544(3) 0.0181(11) Uani 1 1 d . . . .
O25 O -0.2716(3) 0.4664(2) 0.0743(2) 0.0157(10) Uani 1 1 d . . . .
O29 O -0.0481(3) 0.5937(2) 0.1557(2) 0.0145(10) Uani 1 1 d . . . .
O67 O 0.1707(3) 0.2853(2) 0.2001(2) 0.0137(10) Uani 1 1 d . . . .
O17 O -0.1027(3) 0.6330(2) 0.2400(2) 0.0151(10) Uani 1 1 d . . . .
O4 O -0.4060(3) 0.6176(2) 0.1283(2) 0.0137(10) Uani 1 1 d . . . .
O2 O -0.4670(3) 0.5381(2) 0.2876(3) 0.0171(11) Uani 1 1 d . . . .
O65 O 0.2768(3) 0.3529(2) 0.4116(2) 0.0152(10) Uani 1 1 d . . . .
O63 O 0.3172(3) 0.4521(2) 0.2453(2) 0.0134(10) Uani 1 1 d . . . .
O22 O -0.3343(3) 0.3730(2) 0.3042(3) 0.0178(11) Uani 1 1 d . . . .
O19 O -0.1439(3) 0.5890(2) 0.3774(2) 0.0157(11) Uani 1 1 d . . . .
O59 O 0.1455(3) 0.43122(19) 0.2176(2) 0.0112(10) Uani 1 1 d . . . .
O1 O -0.3478(3) 0.7069(2) 0.1999(3) 0.0161(10) Uani 1 1 d . . . .
O58 O 0.0676(3) 0.3495(2) 0.1262(2) 0.0142(10) Uani 1 1 d . . . .
O37 O -0.1777(3) 0.2805(2) 0.2093(2) 0.0150(10) Uani 1 1 d . . . .
O39 O 0.0084(3) 0.5031(2) 0.2518(3) 0.0151(10) Uani 1 1 d . . . .
O20 O -0.1942(3) 0.5122(2) 0.4412(2) 0.0172(11) Uani 1 1 d . . . .
O60 O 0.1685(3) 0.4251(2) 0.3302(2) 0.0115(10) Uani 1 1 d . . . .
O55 O 0.0723(3) 0.2345(2) 0.3649(3) 0.0192(11) Uani 1 1 d . . . .
O31 O -0.0737(3) 0.4941(2) 0.3937(2) 0.0155(10) Uani 1 1 d . . . .
O9 O -0.3401(3) 0.5547(2) 0.0694(2) 0.0122(10) Uani 1 1 d . . . .
O118 O 0.2136(3) 0.3717(2) 0.5024(2) 0.0164(11) Uani 1 1 d . . . .
O3 O -0.5110(3) 0.5483(2) 0.0420(2) 0.0141(10) Uani 1 1 d . . . .
O71 O 0.4783(3) 0.4279(2) 0.3286(3) 0.0194(11) Uani 1 1 d . . . .
O49 O 0.2875(3) 0.5503(2) 0.1978(3) 0.0147(10) Uani 1 1 d . . . .
O16 O -0.1187(3) 0.6879(2) 0.1326(3) 0.0177(11) Uani 1 1 d . . . .
O72 O 0.3934(3) 0.3503(2) 0.3651(3) 0.0150(10) Uani 1 1 d . . . .
O69 O 0.3113(4) 0.2723(2) 0.1704(3) 0.0202(11) Uani 1 1 d . . . .
O13 O -0.3697(3) 0.4692(2) 0.2493(2) 0.0141(10) Uani 1 1 d . . . .
O34 O -0.1351(3) 0.5094(2) 0.0701(2) 0.0127(10) Uani 1 1 d . . . .
O99 O -0.6159(3) 0.4614(2) 0.1523(3) 0.0187(11) Uani 1 1 d . . . .
O101 O -0.5256(4) 0.3471(2) 0.1806(3) 0.0225(12) Uani 1 1 d . . . .
O102 O -0.5486(3) 0.4077(2) 0.0544(2) 0.0167(11) Uani 1 1 d . . . .
Na1 Na -0.1483(2) 0.24012(13) 0.12614(15) 0.0208(6) Uani 1 1 d . . . .
Na2 Na -0.48489(18) 0.43186(12) 0.16032(14) 0.0165(6) Uani 1 1 d . . . .
Na3 Na -0.1964(3) 0.75777(16) 0.07646(18) 0.0350(9) Uani 1 1 d . . . .
Na4 Na -0.5890(2) 0.31869(14) 0.06944(16) 0.0242(7) Uani 1 1 d . . . .
Na5 Na -0.1351(2) 0.73894(14) 0.41123(16) 0.0258(7) Uani 1 1 d . . . .
Na6 Na 0.40423(19) 0.55317(13) 0.16950(17) 0.0230(7) Uani 1 1 d . . . .
Na7 Na 0.2111(2) 0.61466(13) 0.05077(17) 0.0255(7) Uani 1 1 d . . . .
Na8 Na -0.0861(5) 0.0300(3) 0.0210(4) 0.0493(16) Uani 0.607(9) 1 d . P A 1
Na8A Na -0.0229(8) -0.0009(5) 0.0140(6) 0.0493(16) Uani 0.393(9) 1 d . P A 2
Na9 Na 0.5296(5) 0.5048(3) 0.3846(4) 0.0543(18) Uani 0.671(10) 1 d . P B 1
Na9A Na 0.4736(10) 0.5304(7) 0.3819(7) 0.0543(18) Uani 0.329(10) 1 d . P B 2
Na10 Na -0.0404(3) 0.1449(2) 0.09354(19) 0.0507(13) Uani 1 1 d . . . .
Na11 Na 0.0233(3) 0.65234(19) 0.1131(2) 0.0434(10) Uani 1 1 d . . . .
O82 O -0.3243(4) 0.7020(3) 0.0408(3) 0.0339(15) Uani 1 1 d . . . .
O108 O -0.0565(4) 0.1758(3) 0.1838(3) 0.0271(13) Uani 1 1 d . . . .
O109 O -0.1480(4) 0.2013(3) 0.0355(3) 0.0257(13) Uani 1 1 d . . . .
O106 O -0.2611(4) 0.2902(2) 0.0666(3) 0.0241(12) Uani 1 1 d . . . .
O80 O -0.1647(7) 0.7271(5) -0.0077(5) 0.069(3) Uani 1 1 d . . . .
O81 O -0.2229(5) 0.7695(3) 0.1695(3) 0.0349(16) Uani 1 1 d . . . .
O79 O -0.0615(7) 0.8065(3) 0.1284(4) 0.060(3) Uani 1 1 d . . . .
O89 O 0.0628(13) 0.6721(9) 0.2830(10) 0.057(6) Uiso 0.46(2) 1 d . P . .
O90 O 0.0460(12) 0.7202(8) 0.1728(9) 0.036(2) Uiso 0.387(14) 1 d . P C 1
O90A O 0.0685(8) 0.7011(5) 0.2096(6) 0.036(2) Uiso 0.613(14) 1 d . P C 2
O91 O -0.2988(13) 0.8196(8) 0.0298(9) 0.034(2) Uani 0.348(14) 1 d . P D 1
O91A O -0.2470(7) 0.8434(4) 0.0559(5) 0.034(2) Uani 0.652(14) 1 d . P D 2
O92 O 0.0643(7) 0.0811(6) 0.1491(6) 0.048(3) Uani 0.674(16) 1 d . P E 1
O92A O 0.0945(14) 0.1246(12) 0.1468(12) 0.048(3) Uani 0.326(16) 1 d . P E 2
O93 O -0.5929(16) 0.2242(10) 0.0798(14) 0.036(3) Uani 0.38(2) 1 d . P F 1
O93A O -0.5863(9) 0.2299(6) 0.1099(8) 0.036(3) Uani 0.62(2) 1 d . P F 2
O103 O -0.4777(4) 0.2964(3) 0.0376(3) 0.0302(14) Uani 1 1 d . . . .
O97 O -0.1559(4) 0.7868(2) 0.3232(3) 0.0228(12) Uani 1 1 d . . . .
O100 O -0.7195(4) 0.3498(3) 0.0568(3) 0.0299(14) Uani 1 1 d . . . .
O98 O -0.0826(5) 0.6989(4) 0.5042(4) 0.047(2) Uani 1 1 d . . . .
O96 O 0.3372(4) 0.5746(3) 0.0628(3) 0.0348(16) Uani 1 1 d . . . .
O88 O 0.1436(4) 0.5352(2) 0.0394(3) 0.0186(11) Uani 1 1 d . . . .
O87 O 0.2672(4) 0.6976(3) 0.0566(3) 0.0281(14) Uani 1 1 d . . . .
O86 O 0.1059(4) 0.6283(3) -0.0431(3) 0.0358(16) Uani 1 1 d . . . .
O111 O -0.0516(5) 0.1083(4) -0.0038(3) 0.0438(19) Uani 1 1 d . . . .
O84 O 0.0029(5) 0.6947(3) 0.0221(4) 0.047(2) Uani 1 1 d . . . .
O105 O -0.2523(4) 0.1784(2) 0.1186(3) 0.0217(12) Uani 1 1 d . . . .
O94 O 0.4138(5) 0.6374(3) 0.1974(4) 0.0426(18) Uani 1 1 d . . . .
O110 O -0.1380(4) 0.0762(4) 0.0815(4) 0.054(3) Uani 1 1 d . . . .
O85 O 0.1625(5) 0.6318(3) 0.1322(3) 0.0340(15) Uani 1 1 d . . . .
C1 C -0.0283(4) 0.4592(3) 0.2429(3) 0.0126(14) Uani 1 1 d . . . .
O5 O -0.3848(3) 0.6127(2) 0.2451(2) 0.0138(10) Uani 1 1 d U . . .
O95 O 0.6508(12) 0.4460(8) 0.4123(9) 0.055(3) Uiso 0.521(19) 1 d . P B 1
O95A O 0.6640(13) 0.4660(9) 0.4438(10) 0.055(3) Uiso 0.479(19) 1 d . P B 2
O77 O 0.6188(4) 0.3878(3) 0.3907(3) 0.0299(14) Uiso 1 1 d . . . .
O75 O 0.1916(8) 0.6283(5) 0.4358(6) 0.084(4) Uiso 1 1 d . . . .
O83 O -0.0566(7) 0.7584(4) 0.2509(5) 0.063(3) Uiso 1 1 d . . . .
O115 O -0.1178(5) 0.3556(3) 0.4028(4) 0.0394(17) Uiso 1 1 d . . . .
O116 O 0.0116(4) 0.4065(2) 0.4930(3) 0.0257(13) Uiso 1 1 d . . . .
O114 O 0.2879(5) 0.6791(3) 0.2265(4) 0.0412(17) Uiso 1 1 d . . . .
O104 O -0.0646(4) 0.2560(3) 0.4177(3) 0.0351(15) Uiso 1 1 d . . . .
O76 O 0.1845(8) 0.6896(5) 0.3719(6) 0.082(3) Uiso 1 1 d . . . .
O112 O 0.4035(7) 0.6245(4) 0.5168(5) 0.063(3) Uiso 1 1 d . . . .
O107 O -0.4443(8) 0.3399(5) -0.0624(6) 0.034(4) Uiso 0.54(2) 1 d . P . .
O113 O 0.2705(13) 0.6365(9) 0.3246(10) 0.141(7) Uiso 1 1 d . . . .
O117 O 0.1150(10) 0.6125(6) 0.2792(7) 0.100(4) Uiso 1 1 d . . . .
O78 O 0.1490(13) 0.1991(8) 0.0767(9) 0.131(6) Uiso 1 1 d . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -9.8046 9.8477 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.1353 0.1239 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -5.4734 5.5774 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O30 W15 O28 81.1(2) . .
O30 W15 O8 160.8(2) . .
O30 W15 O17 92.7(2) . .
O30 W15 O19 94.1(2) . .
O8 W15 O28 80.12(19) . .
O18 W15 O28 171.6(2) . .
O18 W15 O30 102.5(3) . .
O18 W15 O8 96.7(2) . .
O18 W15 O17 101.9(3) . .
O18 W15 O19 99.1(3) . .
O17 W15 O28 85.4(2) . .
O17 W15 O8 81.7(2) . .
O17 W15 O19 155.9(2) . .
O19 W15 O28 72.9(2) . .
O19 W15 O8 84.3(2) . .
O10 W17 Na2 89.81(13) . .
O10 W17 Na6 113.01(14) . 1_455
O11 W17 O10 84.9(2) . .
O11 W17 O6 158.5(2) . .
O11 W17 O13 90.5(2) . .
O11 W17 Na2 131.38(17) . .
O11 W17 Na6 157.72(17) . 1_455
O11 W17 O5 88.6(2) . .
O6 W17 O10 73.61(19) . .
O6 W17 Na2 50.49(17) . .
O6 W17 Na6 41.58(15) . 1_455
O2 W17 O10 168.5(2) . .
O2 W17 O11 103.6(2) . .
O2 W17 O6 97.6(2) . .
O2 W17 O13 103.1(2) . .
O2 W17 Na2 90.21(19) . .
O2 W17 Na6 56.94(19) . 1_455
O2 W17 O5 99.1(2) . .
O13 W17 O10 84.4(2) . .
O13 W17 O6 87.6(2) . .
O13 W17 Na2 40.86(16) . .
O13 W17 Na6 103.85(17) . 1_455
O13 W17 O5 157.4(2) . .
Na6 W17 Na2 64.58(7) 1_455 .
O5 W17 O10 73.0(2) . .
O5 W17 O6 85.0(2) . .
O5 W17 Na2 135.47(16) . .
O5 W17 Na6 84.45(16) . 1_455
O47 W6 O68 96.8(2) . .
O47 W6 O48 99.3(2) . .
O47 W6 O46 100.7(2) . .
O47 W6 O59 172.0(2) . .
O47 W6 O58 101.7(2) . .
O68 W6 O59 81.46(19) . .
O48 W6 O68 85.5(2) . .
O48 W6 O59 72.80(19) . .
O48 W6 O58 156.6(2) . .
O46 W6 O68 162.4(2) . .
O46 W6 O48 94.2(2) . .
O46 W6 O59 81.6(2) . .
O46 W6 O58 92.0(2) . .
O58 W6 O68 81.9(2) . .
O58 W6 O59 85.9(2) . .
O15 W12 O27 74.0(2) . .
O15 W12 O25 156.8(2) . .
O15 W12 O9 85.8(2) . .
O14 W12 O27 173.2(2) . .
O14 W12 O15 100.0(2) . .
O14 W12 O25 101.0(2) . .
O14 W12 O9 95.7(2) . .
O14 W12 O34 101.9(2) . .
O25 W12 O27 84.5(2) . .
O25 W12 O9 82.6(2) . .
O9 W12 O27 80.96(19) . .
O34 W12 O27 81.9(2) . .
O34 W12 O15 94.3(2) . .
O34 W12 O25 90.8(2) . .
O34 W12 O9 162.2(2) . .
O66 W5 O61 80.7(2) . .
O54 W5 O66 81.9(2) . .
O54 W5 O61 83.5(2) . .
O44 W5 O66 163.0(2) . .
O44 W5 O54 92.2(2) . .
O44 W5 O61 82.8(2) . .
O44 W5 O56 94.4(2) . .
O56 W5 O66 85.1(2) . .
O56 W5 O54 155.7(2) . .
O56 W5 O61 74.2(2) . .
O55 W5 O66 94.2(2) . .
O55 W5 O54 101.3(3) . .
O55 W5 O44 102.7(3) . .
O55 W5 O61 172.5(2) . .
O55 W5 O56 100.0(2) . .
O21 W11 O26 84.4(2) . .
O21 W11 O23 155.7(2) . .
O21 W11 O13 83.4(2) . .
O21 W11 Na2 128.11(17) . .
O26 W11 Na2 88.76(13) . .
O32 W11 O21 93.1(2) . .
O32 W11 O26 81.4(2) . .
O32 W11 O23 93.4(2) . .
O32 W11 O13 162.6(2) . .
O32 W11 Na2 136.56(18) . .
O23 W11 O26 73.45(19) . .
O23 W11 O13 83.4(2) . .
O23 W11 Na2 43.49(15) . .
O22 W11 O21 101.5(3) . .
O22 W11 O26 173.3(2) . .
O22 W11 O32 101.4(2) . .
O22 W11 O23 100.2(2) . .
O22 W11 O13 96.0(2) . .
O22 W11 Na2 85.0(2) . .
O13 W11 O26 81.25(19) . .
O13 W11 Na2 44.76(16) . .
O33 W10 O26 81.9(2) . .
O33 W10 O23 90.9(2) . .
O33 W10 O12 162.8(2) . .
O33 W10 O25 95.1(2) . .
O33 W10 Na2 133.74(17) . .
O24 W10 O33 100.5(3) . .
O24 W10 O26 171.4(2) . .
O24 W10 O23 98.0(2) . .
O24 W10 O12 96.3(2) . .
O24 W10 O25 101.7(3) . .
O24 W10 Na2 83.54(19) . .
O26 W10 Na2 88.88(13) . .
O23 W10 O26 73.60(19) . .
O23 W10 O12 82.9(2) . .
O23 W10 Na2 43.32(15) . .
O12 W10 O26 80.95(19) . .
O12 W10 Na2 44.52(15) . .
O25 W10 O26 86.3(2) . .
O25 W10 O23 158.0(2) . .
O25 W10 O12 85.3(2) . .
O25 W10 Na2 129.61(17) . .
O52 W7 O65 83.4(2) . .
O52 W7 O60 75.1(2) . .
O54 W7 O52 157.4(2) . .
O54 W7 O65 82.8(2) . .
O54 W7 O60 85.1(2) . .
O43 W7 O52 94.3(2) . .
O43 W7 O54 94.1(2) . .
O43 W7 O65 163.8(2) . .
O43 W7 O60 83.2(2) . .
O65 W7 O60 80.75(19) . .
O118 W7 O52 99.4(2) . .
O118 W7 O54 99.3(2) . .
O118 W7 O43 102.2(2) . .
O118 W7 O65 94.0(2) . .
O118 W7 O60 172.7(2) . .
O45 W4 O61 81.4(2) . .
O45 W4 O56 91.7(2) . .
O45 W4 O67 161.6(2) . .
O45 W4 O58 92.7(2) . .
O45 W4 Na1 45.88(18) . .
O57 W4 O45 101.0(2) . .
O57 W4 O61 172.0(2) . .
O57 W4 O56 99.8(2) . .
O57 W4 O67 97.4(2) . .
O57 W4 O58 102.6(2) . .
O57 W4 Na1 60.25(19) . .
O61 W4 Na1 118.76(13) . .
O56 W4 O61 72.4(2) . .
O56 W4 O67 84.5(2) . .
O56 W4 Na1 79.45(16) . .
O67 W4 O61 80.3(2) . .
O67 W4 Na1 149.19(16) . .
O58 W4 O61 84.8(2) . .
O58 W4 O56 155.9(2) . .
O58 W4 O67 83.9(2) . .
O58 W4 Na1 119.70(17) . .
O68 W1 O62 84.7(2) . .
O68 W1 O70 88.3(2) . .
O68 W1 O74 157.5(2) . .
O70 W1 O62 73.2(2) . .
O70 W1 O74 85.4(2) . .
O74 W1 O62 72.8(2) . .
O67 W1 O62 83.2(2) . .
O67 W1 O68 89.7(2) . .
O67 W1 O70 156.3(2) . .
O67 W1 O74 87.5(2) . .
O69 W1 O62 170.0(2) . .
O69 W1 O68 102.8(2) . .
O69 W1 O70 100.2(3) . .
O69 W1 O74 99.6(2) . .
O69 W1 O67 103.2(3) . .
O41 W8 O48 91.1(2) . .
O41 W8 O50 93.4(2) . .
O41 W8 O63 162.9(2) . .
O41 W8 O59 82.1(2) . .
O48 W8 O63 84.6(2) . .
O48 W8 O59 72.52(19) . .
O50 W8 O48 157.4(2) . .
O50 W8 O63 84.7(2) . .
O50 W8 O59 86.1(2) . .
O63 W8 O59 80.79(19) . .
O49 W8 O41 101.1(2) . .
O49 W8 O48 98.7(2) . .
O49 W8 O50 102.2(2) . .
O49 W8 O63 96.0(2) . .
O49 W8 O59 170.8(2) . .
O21 W13 O28 84.3(2) . .
O21 W13 O11 81.4(2) . .
O21 W13 O19 155.2(2) . .
O11 W13 O28 81.88(19) . .
O19 W13 O28 73.0(2) . .
O19 W13 O11 85.6(2) . .
O20 W13 O28 172.3(2) . .
O20 W13 O21 100.9(3) . .
O20 W13 O11 93.3(2) . .
O20 W13 O19 100.8(3) . .
O20 W13 O31 102.8(2) . .
O31 W13 O28 82.4(2) . .
O31 W13 O21 92.5(2) . .
O31 W13 O11 163.6(2) . .
O31 W13 O19 94.2(2) . .
O62 W3 Na9 154.38(18) . .
O62 W3 Na9A 137.4(3) . .
O64 W3 O62 84.3(2) . .
O64 W3 O70 156.7(2) . .
O64 W3 O63 88.7(2) . .
O64 W3 O72 89.8(2) . .
O64 W3 Na9 70.2(2) . .
O64 W3 Na9A 55.5(3) . .
O70 W3 O62 72.4(2) . .
O70 W3 Na9 132.9(2) . .
O70 W3 Na9A 145.7(3) . .
O63 W3 O62 83.1(2) . .
O63 W3 O70 86.6(2) . .
O63 W3 O72 155.9(2) . .
O63 W3 Na9 93.2(2) . .
O63 W3 Na9A 82.4(3) . .
O71 W3 O62 170.3(2) . .
O71 W3 O64 103.0(2) . .
O71 W3 O70 100.3(2) . .
O71 W3 O63 103.3(3) . .
O71 W3 O72 100.5(3) . .
O71 W3 Na9 34.1(2) . .
O71 W3 Na9A 51.8(3) . .
O72 W3 O62 72.8(2) . .
O72 W3 O70 85.4(2) . .
O72 W3 Na9 108.9(2) . .
O72 W3 Na9A 116.1(3) . .
O27 W14 Na11 123.17(15) . .
O7 W14 O27 80.4(2) . .
O7 W14 Na11 154.07(18) . .
O15 W14 O27 73.6(2) . .
O15 W14 O7 83.9(2) . .
O15 W14 Na11 92.34(17) . .
O29 W14 O27 81.5(2) . .
O29 W14 O7 161.7(2) . .
O29 W14 O15 93.7(2) . .
O29 W14 O17 93.2(2) . .
O29 W14 Na11 43.90(19) . .
O17 W14 O27 86.0(2) . .
O17 W14 O7 82.8(2) . .
O17 W14 O15 157.3(2) . .
O17 W14 Na11 107.54(18) . .
O16 W14 O27 171.4(2) . .
O16 W14 O7 97.5(2) . .
O16 W14 O15 97.9(2) . .
O16 W14 O29 100.8(2) . .
O16 W14 O17 102.0(3) . .
O16 W14 Na11 57.5(2) . .
O7 W18 O10 83.9(2) . .
O7 W18 O8 89.2(2) . .
O7 W18 O4 87.9(2) . .
O7 W18 O5 157.0(2) . .
O8 W18 O10 83.7(2) . .
O8 W18 O4 156.8(2) . .
O8 W18 O5 88.7(2) . .
O4 W18 O10 73.1(2) . .
O4 W18 O5 85.1(2) . .
O1 W18 O7 102.3(3) . .
O1 W18 O10 171.0(2) . .
O1 W18 O8 102.7(2) . .
O1 W18 O4 100.4(2) . .
O1 W18 O5 100.5(2) . .
O5 W18 O10 73.10(19) . .
O10 W16 Na2 89.35(13) . .
O6 W16 O10 73.12(19) . .
O6 W16 Na2 50.38(17) . .
O12 W16 O10 82.8(2) . .
O12 W16 O6 87.1(2) . .
O12 W16 O4 155.2(2) . .
O12 W16 Na2 41.11(16) . .
O4 W16 O10 72.46(19) . .
O4 W16 O6 85.3(2) . .
O4 W16 Na2 135.57(16) . .
O9 W16 O10 83.9(2) . .
O9 W16 O6 157.0(2) . .
O9 W16 O12 89.2(2) . .
O9 W16 O4 88.7(2) . .
O9 W16 Na2 130.30(16) . .
O3 W16 O10 170.5(2) . .
O3 W16 O6 100.1(2) . .
O3 W16 O12 103.8(2) . .
O3 W16 O4 100.7(2) . .
O3 W16 O9 102.8(2) . .
O3 W16 Na2 91.30(19) . .
O66 W2 O62 83.5(2) . .
O66 W2 O74 88.4(2) . .
O66 W2 O65 90.2(2) . .
O66 W2 O72 156.8(2) . .
O73 W2 O66 102.3(3) . .
O73 W2 O62 172.3(2) . .
O73 W2 O74 101.7(2) . .
O73 W2 O65 101.3(2) . .
O73 W2 O72 100.7(3) . .
O74 W2 O62 73.1(2) . .
O65 W2 O62 83.7(2) . .
O65 W2 O74 156.7(2) . .
O65 W2 O72 88.1(2) . .
O72 W2 O62 73.3(2) . .
O72 W2 O74 84.1(2) . .
O52 W9 O64 85.2(2) . .
O52 W9 O60 73.0(2) . .
O52 W9 Na8 47.6(2) . 4_666
O50 W9 O52 156.2(2) . .
O50 W9 O64 81.6(2) . .
O50 W9 O60 85.4(2) . .
O50 W9 Na8 143.1(2) . 4_666
O64 W9 O60 80.60(19) . .
O64 W9 Na8 73.1(2) . 4_666
O42 W9 O52 94.2(2) . .
O42 W9 O50 91.7(2) . .
O42 W9 O64 160.3(2) . .
O42 W9 O60 80.4(2) . .
O42 W9 Na8 120.4(2) . 4_666
O51 W9 O52 98.6(3) . .
O51 W9 O50 102.7(3) . .
O51 W9 O64 97.4(2) . .
O51 W9 O42 102.1(3) . .
O51 W9 O60 171.4(2) . .
O51 W9 Na8 56.0(2) . 4_666
O60 W9 Na8 115.58(19) . 4_666
O41 Dy3 O35 76.40(18) . .
O41 Dy3 O38 119.95(18) . .
O41 Dy3 O29 91.25(19) . .
O41 Dy3 O39 84.38(18) . .
O41 Dy3 Na11 67.69(15) . .
O41 Dy3 C1 103.1(2) . .
O35 Dy3 Na11 42.67(15) . .
O35 Dy3 C1 177.4(2) . .
O38 Dy3 O35 154.98(18) . .
O38 Dy3 Na11 157.56(14) . .
O38 Dy3 C1 27.2(2) . .
O46 Dy3 O41 84.30(19) . .
O46 Dy3 O35 81.21(18) . .
O46 Dy3 O38 81.85(18) . .
O46 Dy3 O29 154.75(19) . .
O46 Dy3 O39 119.43(18) . .
O46 Dy3 Na11 120.55(15) . .
O46 Dy3 C1 101.3(2) . .
O29 Dy3 O35 73.59(19) . .
O29 Dy3 O38 121.28(18) . .
O29 Dy3 O39 84.66(18) . .
O29 Dy3 Na11 36.59(14) . .
O29 Dy3 C1 103.9(2) . .
O39 Dy3 O35 150.37(18) . .
O39 Dy3 O38 54.59(17) . .
O39 Dy3 Na11 109.01(15) . .
O39 Dy3 C1 27.4(2) . .
O34 Dy3 O41 152.62(19) . .
O34 Dy3 O35 76.27(18) . .
O34 Dy3 O38 85.45(18) . .
O34 Dy3 O46 89.97(19) . .
O34 Dy3 O29 82.62(19) . .
O34 Dy3 O39 121.28(18) . .
O34 Dy3 Na11 92.87(15) . .
O34 Dy3 C1 104.3(2) . .
C1 Dy3 Na11 134.73(17) . .
O43 Dy2 O40 82.80(18) . .
O43 Dy2 O36 78.41(19) . .
O43 Dy2 O39 119.26(18) . .
O43 Dy2 C1 101.9(2) . .
O30 Dy2 O43 154.59(19) . .
O30 Dy2 O40 121.48(19) . .
O30 Dy2 O36 76.20(19) . .
O30 Dy2 O39 83.93(19) . .
O30 Dy2 C1 103.4(2) . .
O40 Dy2 C1 27.3(2) . .
O36 Dy2 O40 154.33(18) . .
O36 Dy2 O39 151.01(19) . .
O36 Dy2 C1 178.1(2) . .
O42 Dy2 O43 80.58(19) . .
O42 Dy2 O30 92.65(19) . .
O42 Dy2 O40 117.92(19) . .
O42 Dy2 O36 76.11(19) . .
O42 Dy2 O39 84.06(18) . .
O42 Dy2 O31 154.1(2) . .
O42 Dy2 C1 102.1(2) . .
O39 Dy2 O40 54.60(17) . .
O39 Dy2 C1 27.4(2) . .
O31 Dy2 O43 91.31(19) . .
O31 Dy2 O30 84.2(2) . .
O31 Dy2 O40 85.03(19) . .
O31 Dy2 O36 78.13(19) . .
O31 Dy2 O39 120.98(18) . .
O31 Dy2 C1 103.7(2) . .
O45 Dy1 O40 122.57(18) . .
O45 Dy1 O38 85.68(18) . .
O45 Dy1 O37 75.94(18) . .
O45 Dy1 C1 105.2(2) . .
O44 Dy1 O45 83.49(19) . .
O44 Dy1 O32 91.08(19) . .
O44 Dy1 O40 85.69(19) . .
O44 Dy1 O38 122.21(18) . .
O44 Dy1 O37 73.94(19) . .
O44 Dy1 C1 105.1(2) . .
O33 Dy1 O45 90.65(19) . .
O33 Dy1 O44 152.18(19) . .
O33 Dy1 O32 81.82(19) . .
O33 Dy1 O40 119.78(19) . .
O33 Dy1 O38 84.20(18) . .
O33 Dy1 O37 78.26(18) . .
O33 Dy1 C1 102.7(2) . .
O32 Dy1 O45 152.84(19) . .
O32 Dy1 O40 83.28(19) . .
O32 Dy1 O38 119.14(18) . .
O32 Dy1 O37 76.99(19) . .
O32 Dy1 C1 101.9(2) . .
O40 Dy1 O37 151.12(18) . .
O40 Dy1 C1 27.3(2) . .
O38 Dy1 O40 54.62(17) . .
O38 Dy1 O37 154.27(17) . .
O38 Dy1 C1 27.29(19) . .
O37 Dy1 C1 178.44(19) . .
O27 P1 O10 108.0(3) . .
O27 P1 O26 110.3(3) . .
O28 P1 O27 110.5(3) . .
O28 P1 O10 108.6(3) . .
O28 P1 O26 110.4(3) . .
O26 P1 O10 108.8(3) . .
O61 P2 O62 108.9(3) . .
O61 P2 O59 110.9(3) . .
O61 P2 O60 110.9(3) . .
O59 P2 O62 108.1(3) . .
O59 P2 O60 110.0(3) . .
O60 P2 O62 107.9(3) . .
W7 O52 W9 120.8(3) . .
W7 O52 Na8 136.7(3) . 4_666
W9 O52 Na8 99.8(3) . 4_666
W2 O66 W5 150.3(3) . .
W8 O41 Dy3 138.4(3) . .
W14 O27 W12 89.57(18) . .
P1 O27 W12 128.3(3) . .
P1 O27 W14 127.8(3) . .
W4 O45 Dy1 136.9(3) . .
W4 O45 Na1 103.8(2) . .
Dy1 O45 Na1 104.8(2) . .
W18 O7 W14 149.5(3) . .
W7 O54 W5 157.0(3) . .
W13 O28 W15 89.60(17) . .
P1 O28 W15 127.8(3) . .
P1 O28 W13 127.7(3) . .
W7 O43 Dy2 138.9(3) . .
Dy3 O35 Na11 97.9(2) . .
W1 O62 W3 90.83(17) . .
W2 O62 W1 91.38(18) . .
W2 O62 W3 90.67(17) . .
P2 O62 W1 124.7(3) . .
P2 O62 W3 124.9(3) . .
P2 O62 W2 124.1(3) . .
W5 O44 Dy1 136.7(3) . .
W4 O57 Na10 145.3(3) . .
W10 O33 Dy1 140.4(3) . .
W15 O30 Dy2 138.4(3) . .
W12 O15 W14 121.7(3) . .
W11 O21 W13 158.0(3) . .
W5 O61 W4 89.25(17) . .
P2 O61 W5 127.9(3) . .
P2 O61 W4 127.0(3) . .
W17 O10 W16 90.96(16) . .
W18 O10 W17 91.40(17) . .
W18 O10 W16 90.91(17) . .
P1 O10 W17 124.7(3) . .
P1 O10 W18 124.7(3) . .
P1 O10 W16 124.1(3) . .
W1 O68 W6 149.1(3) . .
W6 O48 W8 123.7(3) . .
W10 O26 W11 90.86(17) . .
P1 O26 W11 127.0(3) . .
P1 O26 W10 127.1(3) . .
W18 O8 W15 149.9(3) . .
W17 O11 W13 148.6(3) . .
W11 O32 Dy1 139.2(3) . .
W5 O56 W4 123.3(3) . .
Dy2 O40 Dy1 174.8(2) . .
C1 O40 Dy2 92.9(4) . .
C1 O40 Dy1 92.2(4) . .
Dy1 O38 Dy3 174.9(2) . .
C1 O38 Dy3 92.5(4) . .
C1 O38 Dy1 92.6(4) . .
W11 O23 W10 121.1(3) . .
W11 O23 Na2 103.9(2) . .
W10 O23 Na2 103.4(2) . .
W17 O6 Na2 96.9(2) . .
W17 O6 Na6 105.0(2) . 1_455
W16 O6 W17 122.3(2) . .
W16 O6 Na2 97.1(2) . .
W16 O6 Na6 129.6(3) . 1_455
Na6 O6 Na2 93.24(19) 1_455 .
W10 O12 Na2 101.6(2) . .
W16 O12 W10 147.8(3) . .
W16 O12 Na2 109.3(2) . .
W8 O50 W9 154.8(3) . .
W3 O64 W9 151.2(3) . .
W9 O42 Dy2 142.3(3) . .
W1 O70 W3 123.6(3) . .
W2 O74 W1 122.7(3) . .
W6 O46 Dy3 138.4(3) . .
W9 O51 Na8 94.7(3) . 4_666
W9 O51 Na8A 116.3(4) . 4_666
W9 O51 Na9A 104.9(4) . .
Na8A O51 Na9A 65.7(4) 4_666 .
W15 O18 Na5 133.9(3) . .
W10 O25 W12 154.6(3) . .
W14 O29 Dy3 138.8(3) . .
W14 O29 Na11 104.9(3) . .
Dy3 O29 Na11 109.1(2) . .
W1 O67 W4 149.2(3) . .
W15 O17 W14 155.9(3) . .
W18 O4 W16 123.5(3) . .
W17 O2 Na6 92.6(2) . 1_455
W17 O2 Na9 132.4(4) . 1_455
W17 O2 Na9A 154.4(5) . 1_455
Na9 O2 Na6 131.6(3) 1_455 1_455
Na9A O2 Na6 113.0(4) 1_455 1_455
W2 O65 W7 148.2(3) . .
W3 O63 W8 148.3(3) . .
W15 O19 W13 123.4(3) . .
W8 O59 W6 90.25(16) . .
P2 O59 W6 127.3(3) . .
P2 O59 W8 128.0(3) . .
W4 O58 W6 155.9(3) . .
Na1 O37 Dy1 104.7(2) . .
Dy3 O39 Dy2 174.0(3) . .
C1 O39 Dy3 93.1(4) . .
C1 O39 Dy2 92.8(4) . .
W7 O60 W9 89.60(17) . .
P2 O60 W7 128.5(3) . .
P2 O60 W9 128.6(3) . .
W13 O31 Dy2 137.4(3) . .
W16 O9 W12 151.5(3) . .
W3 O71 Na9 121.9(3) . .
W3 O71 Na9A 101.0(4) . .
W8 O49 Na6 136.7(3) . .
W14 O16 Na3 136.5(3) . .
W14 O16 Na11 91.7(2) . .
Na3 O16 Na11 121.2(3) . .
W3 O72 W2 123.1(3) . .
W17 O13 W11 147.5(3) . .
W17 O13 Na2 109.7(2) . .
W11 O13 Na2 100.8(2) . .
W12 O34 Dy3 138.1(3) . .
Na2 O99 Na6 103.5(2) . 1_455
Na2 O101 Na4 96.4(2) . .
Na2 O102 Na4 98.3(2) . .
W4 Na1 Na5 156.13(12) . 2_445
O45 Na1 W4 30.35(12) . .
O45 Na1 Na5 125.83(17) . 2_445
O37 Na1 W4 93.11(16) . .
O37 Na1 O45 71.46(19) . .
O37 Na1 Na5 71.48(16) . 2_445
O108 Na1 W4 74.57(17) . .
O108 Na1 O45 98.7(2) . .
O108 Na1 O37 98.4(2) . .
O108 Na1 Na5 124.60(19) . 2_445
O108 Na1 O105 84.1(2) . .
O109 Na1 W4 96.89(18) . .
O109 Na1 O45 115.8(2) . .
O109 Na1 O37 168.8(3) . .
O109 Na1 Na5 97.4(2) . 2_445
O109 Na1 O108 89.2(3) . .
O109 Na1 O105 84.1(2) . .
O106 Na1 W4 117.86(19) . .
O106 Na1 O45 93.2(2) . .
O106 Na1 O37 81.9(2) . .
O106 Na1 Na5 43.61(17) . 2_445
O106 Na1 O108 167.6(3) . .
O106 Na1 O109 89.0(2) . .
O106 Na1 O105 83.4(2) . .
O105 Na1 W4 158.6(2) . .
O105 Na1 O45 159.9(2) . .
O105 Na1 O37 88.4(2) . .
O105 Na1 Na5 42.67(17) . 2_445
W17 Na2 W16 56.79(5) . .
W17 Na2 Na6 55.54(7) . 1_455
W11 Na2 W17 63.57(5) . .
W11 Na2 W10 58.31(5) . .
W11 Na2 W16 91.26(7) . .
W11 Na2 Na6 118.37(10) . 1_455
W10 Na2 W17 90.55(7) . .
W10 Na2 W16 63.26(5) . .
W10 Na2 Na6 127.01(10) . 1_455
W16 Na2 Na6 64.04(7) . 1_455
O23 Na2 W17 89.52(15) . .
O23 Na2 W11 32.59(12) . .
O23 Na2 W10 33.27(12) . .
O23 Na2 W16 89.97(15) . .
O23 Na2 O6 106.46(19) . .
O23 Na2 O12 63.70(18) . .
O23 Na2 O13 63.72(19) . .
O23 Na2 Na6 143.73(17) . 1_455
O6 Na2 W17 32.65(11) . .
O6 Na2 W11 90.66(13) . .
O6 Na2 W10 90.09(13) . .
O6 Na2 W16 32.56(11) . .
O6 Na2 Na6 38.77(12) . 1_455
O12 Na2 W17 72.75(14) . .
O12 Na2 W11 76.35(14) . .
O12 Na2 W10 33.88(13) . .
O12 Na2 W16 29.60(13) . .
O12 Na2 O6 59.54(17) . .
O12 Na2 Na6 93.64(16) . 1_455
O13 Na2 W17 29.47(13) . .
O13 Na2 W11 34.45(13) . .
O13 Na2 W10 76.69(14) . .
O13 Na2 W16 73.54(14) . .
O13 Na2 O6 59.85(18) . .
O13 Na2 O12 75.17(19) . .
O13 Na2 Na6 83.96(16) . 1_455
O99 Na2 W17 90.11(17) . .
O99 Na2 W11 141.30(18) . .
O99 Na2 W10 155.72(19) . .
O99 Na2 W16 97.32(18) . .
O99 Na2 O23 171.0(2) . .
O99 Na2 O6 77.6(2) . .
O99 Na2 O12 124.6(2) . .
O99 Na2 O13 113.3(2) . .
O99 Na2 O101 88.2(2) . .
O99 Na2 O102 86.5(2) . .
O99 Na2 Na6 39.03(16) . 1_455
O101 Na2 W17 133.32(19) . .
O101 Na2 W11 90.46(17) . .
O101 Na2 W10 108.60(17) . .
O101 Na2 W16 168.73(19) . .
O101 Na2 O23 85.5(2) . .
O101 Na2 O6 158.5(2) . .
O101 Na2 O12 141.1(2) . .
O101 Na2 O13 113.3(2) . .
O101 Na2 Na6 124.35(18) . 1_455
O102 Na2 W17 141.76(18) . .
O102 Na2 W11 131.91(17) . .
O102 Na2 W10 78.13(15) . .
O102 Na2 W16 85.90(16) . .
O102 Na2 O23 99.3(2) . .
O102 Na2 O6 110.1(2) . .
O102 Na2 O12 78.1(2) . .
O102 Na2 O13 152.7(2) . .
O102 Na2 O101 84.7(2) . .
O102 Na2 Na6 103.24(17) . 1_455
O16 Na3 O82 89.7(2) . .
O16 Na3 O80 86.7(4) . .
O16 Na3 O81 81.6(3) . .
O16 Na3 O79 83.2(3) . .
O16 Na3 O91A 158.3(4) . .
O82 Na3 O79 171.0(3) . .
O80 Na3 O82 88.7(4) . .
O80 Na3 O81 167.3(4) . .
O80 Na3 O79 96.3(4) . .
O80 Na3 O91A 109.2(4) . .
O81 Na3 O82 86.2(3) . .
O81 Na3 O79 87.4(3) . .
O91 Na3 O16 165.6(6) . .
O91 Na3 O82 79.5(6) . .
O91 Na3 O80 102.3(6) . .
O91 Na3 O81 88.2(6) . .
O91 Na3 O79 106.6(6) . .
O91A Na3 O82 104.9(3) . .
O91A Na3 O81 83.4(3) . .
O91A Na3 O79 80.6(4) . .
O102 Na4 O101 80.5(2) . .
O102 Na4 O82 98.5(3) . 3_465
O102 Na4 O93A 162.3(4) . .
O82 Na4 O101 169.6(3) 3_465 .
O93 Na4 O101 101.9(7) . .
O93 Na4 O102 163.9(6) . .
O93 Na4 O82 82.0(7) . 3_465
O93A Na4 O101 86.6(4) . .
O93A Na4 O82 96.4(5) . 3_465
O103 Na4 O101 107.2(2) . .
O103 Na4 O102 83.0(2) . .
O103 Na4 O82 82.9(3) . 3_465
O103 Na4 O93 81.1(6) . .
O103 Na4 O93A 89.4(4) . .
O100 Na4 O101 93.6(2) . .
O100 Na4 O102 88.3(2) . .
O100 Na4 O82 75.9(3) . 3_465
O100 Na4 O93 107.4(6) . .
O100 Na4 O93A 104.7(4) . .
O100 Na4 O103 155.6(3) . .
O18 Na5 Na1 119.02(18) . 2_455
O106 Na5 O18 158.8(3) 2_455 .
O106 Na5 Na1 41.20(17) 2_455 2_455
O103 Na5 O18 103.3(2) 2_455 .
O103 Na5 Na1 135.7(2) 2_455 2_455
O103 Na5 O106 94.8(3) 2_455 2_455
O103 Na5 O105 167.9(3) 2_455 2_455
O97 Na5 O18 79.7(2) . .
O97 Na5 Na1 88.45(19) . 2_455
O97 Na5 O106 90.6(2) . 2_455
O97 Na5 O103 86.5(3) . 2_455
O97 Na5 O105 104.5(2) . 2_455
O98 Na5 O18 97.2(3) . .
O98 Na5 Na1 104.8(2) . 2_455
O98 Na5 O106 96.5(3) . 2_455
O98 Na5 O103 81.0(3) . 2_455
O98 Na5 O97 166.1(3) . .
O98 Na5 O105 88.5(3) . 2_455
O105 Na5 O18 83.8(2) 2_455 .
O105 Na5 Na1 41.97(16) 2_455 2_455
O105 Na5 O106 80.5(2) 2_455 2_455
W17 Na6 Na2 59.87(7) 1_655 1_655
W17 Na6 Na7 157.12(12) 1_655 .
O6 Na6 W17 33.41(13) 1_655 1_655
O6 Na6 O2 63.37(18) 1_655 1_655
O6 Na6 O49 160.7(3) 1_655 .
O6 Na6 O99 85.3(2) 1_655 1_655
O6 Na6 Na2 47.99(15) 1_655 1_655
O6 Na6 Na7 132.48(19) 1_655 .
O6 Na6 O96 98.4(2) 1_655 .
O2 Na6 W17 30.44(11) 1_655 1_655
O2 Na6 Na2 72.84(14) 1_655 1_655
O2 Na6 Na7 156.82(17) 1_655 .
O49 Na6 W17 130.30(19) . 1_655
O49 Na6 O2 99.9(2) . 1_655
O49 Na6 O99 85.9(2) . 1_655
O49 Na6 Na2 120.23(18) . 1_655
O49 Na6 Na7 66.57(16) . .
O49 Na6 O96 99.3(2) . .
O99 Na6 W17 92.80(16) 1_655 1_655
O99 Na6 O2 92.2(2) 1_655 1_655
O99 Na6 Na2 37.47(14) 1_655 1_655
O99 Na6 Na7 104.88(18) 1_655 .
Na2 Na6 Na7 129.95(12) 1_655 .
O96 Na6 W17 130.3(2) . 1_655
O96 Na6 O2 160.2(2) . 1_655
O96 Na6 O99 94.1(3) . 1_655
O96 Na6 Na2 101.5(2) . 1_655
O96 Na6 Na7 35.77(18) . .
O94 Na6 W17 89.0(2) . 1_655
O94 Na6 O6 101.1(3) . 1_655
O94 Na6 O2 84.7(3) . 1_655
O94 Na6 O49 86.0(3) . .
O94 Na6 O99 170.7(3) . 1_655
O94 Na6 Na2 147.5(3) . 1_655
O94 Na6 Na7 76.0(2) . .
O94 Na6 O96 91.7(3) . .
Na6 Na7 Na11 115.81(12) . .
O96 Na7 Na6 36.68(18) . .
O96 Na7 Na11 151.9(2) . .
O96 Na7 O87 93.0(3) . .
O96 Na7 O85 125.1(3) . .
O88 Na7 Na6 88.94(18) . .
O88 Na7 Na11 79.80(17) . .
O88 Na7 O96 91.6(3) . .
O88 Na7 O87 174.8(3) . .
O88 Na7 O85 86.9(2) . .
O87 Na7 Na6 96.2(2) . .
O87 Na7 Na11 97.2(2) . .
O87 Na7 O85 92.4(3) . .
O86 Na7 Na6 158.3(3) . .
O86 Na7 Na11 81.3(2) . .
O86 Na7 O96 124.0(3) . .
O86 Na7 O88 80.8(3) . .
O86 Na7 O87 94.6(3) . .
O86 Na7 O85 109.9(3) . .
O85 Na7 Na6 88.4(2) . .
O85 Na7 Na11 28.7(2) . .
W9 Na8 Na8 93.9(3) 4_565 3
O52 Na8 W9 32.64(16) 4_565 4_565
O52 Na8 O51 59.5(2) 4_565 4_565
O52 Na8 Na8 124.6(4) 4_565 3
O51 Na8 W9 29.28(14) 4_565 4_565
O51 Na8 Na8 74.8(3) 4_565 3
Na9 Na8 W9 145.2(4) 2_545 4_565
Na9 Na8 O52 137.7(4) 2_545 4_565
Na9 Na8 O51 122.5(5) 2_545 4_565
Na9 Na8 Na8 92.0(4) 2_545 3
Na9 Na8 O111 118.2(5) 2_545 .
Na9 Na8 O110 70.1(4) 2_545 .
O111 Na8 W9 96.0(3) . 4_565
O111 Na8 O52 85.3(4) . 4_565
O111 Na8 O51 117.4(4) . 4_565
O111 Na8 Na8 89.8(4) . 3
O111 Na8 O110 83.5(4) . .
O110 Na8 W9 111.1(3) . 4_565
O110 Na8 O52 79.3(3) . 4_565
O110 Na8 O51 129.7(4) . 4_565
O110 Na8 Na8 154.7(5) . 3
O51 Na8A Na9A 58.3(4) 4_565 4_565
O51 Na8A O111 100.6(5) 4_565 .
Na8A Na8A O51 100.1(14) 3 4_565
Na8A Na8A Na9A 41.9(12) 3 4_565
Na8A Na8A Na9A 118.6(15) 3 2_545
Na8A Na8A O111 89.8(14) 3 .
Na9A Na8A O51 141.1(7) 2_545 4_565
Na9A Na8A Na9A 160.5(6) 2_545 4_565
Na9A Na8A O111 77.9(6) 2_545 .
O111 Na8A Na9A 99.1(5) . 4_565
W3 Na9 Na10 138.6(3) . 2
O2 Na9 W3 93.7(3) 1_655 .
O2 Na9 Na10 76.2(3) 1_655 2
O2 Na9 O92 70.3(4) 1_655 2
O2 Na9 O110 76.3(3) 1_655 2
O2 Na9 O95 98.7(6) 1_655 .
O71 Na9 W3 23.99(16) . .
O71 Na9 O2 85.3(3) . 1_655
O71 Na9 Na10 154.2(4) . 2
O71 Na9 O92 115.1(4) . 2
O71 Na9 O110 150.1(4) . 2
O71 Na9 O95 74.7(6) . .
Na8 Na9 W3 133.0(4) 2 .
Na8 Na9 O2 133.0(4) 2 1_655
Na8 Na9 O71 139.1(5) 2 .
Na8 Na9 Na10 64.9(3) 2 2
Na8 Na9 O92 94.5(5) 2 2
Na8 Na9 O110 57.1(3) 2 2
Na8 Na9 O95 84.2(6) 2 .
O92 Na9 W3 97.1(4) 2 .
O92 Na9 Na10 41.6(3) 2 2
O92 Na9 O110 80.8(4) 2 2
O110 Na9 W3 169.9(3) 2 .
O110 Na9 Na10 40.7(3) 2 2
O95 Na9 W3 95.6(5) . .
O95 Na9 Na10 125.4(5) . 2
O95 Na9 O92 163.7(6) . 2
O95 Na9 O110 84.9(6) . 2
O51 Na9A W3 85.5(4) . .
O51 Na9A O71 111.4(5) . .
O51 Na9A Na8A 56.0(4) . 4_666
O51 Na9A Na10 98.9(6) . 2
O2 Na9A W3 86.6(4) 1_655 .
O2 Na9A O51 147.1(7) 1_655 .
O2 Na9A O71 69.7(4) 1_655 .
O2 Na9A Na8A 156.7(8) 1_655 4_666
O2 Na9A Na10 81.8(4) 1_655 2
O2 Na9A O110 65.9(4) 1_655 2
O71 Na9A W3 27.26(18) . .
O71 Na9A Na8A 101.5(6) . 4_666
O71 Na9A Na10 149.1(6) . 2
Na8A Na9A W3 95.7(6) 2 .
Na8A Na9A W3 94.4(5) 4_666 .
Na8A Na9A O51 75.5(5) 2 .
Na8A Na9A O2 137.2(8) 2 1_655
Na8A Na9A O71 93.8(7) 2 .
Na8A Na9A Na8A 19.5(6) 2 4_666
Na8A Na9A Na10 99.5(6) 2 2
Na8A Na9A Na10 100.2(5) 4_666 2
Na8A Na9A O92A 121.3(9) 2 2
Na8A Na9A O110 84.1(6) 2 2
Na10 Na9A W3 164.8(5) 2 .
O92A Na9A W3 125.8(7) 2 .
O92A Na9A O51 69.7(7) 2 .
O92A Na9A O2 89.7(8) 2 1_655
O92A Na9A O71 142.4(8) 2 .
O92A Na9A Na8A 108.2(8) 2 4_666
O92A Na9A Na10 44.7(6) 2 2
O92A Na9A O110 89.7(7) 2 2
O110 Na9A W3 135.7(6) 2 .
O110 Na9A O51 136.0(6) 2 .
O110 Na9A O71 108.4(6) 2 .
O110 Na9A Na8A 98.5(5) 2 4_666
O110 Na9A Na10 46.4(3) 2 2
O57 Na10 Na9 154.1(2) . 2_545
O57 Na10 Na9A 138.7(4) . 2_545
O108 Na10 O57 70.2(2) . .
O108 Na10 Na9 103.3(3) . 2_545
O108 Na10 Na9A 108.2(4) . 2_545
O108 Na10 O92 93.8(4) . .
O108 Na10 O111 168.8(3) . .
O108 Na10 O110 92.7(3) . .
O109 Na10 O57 72.7(2) . .
O109 Na10 Na9 133.0(3) . 2_545
O109 Na10 Na9A 147.5(4) . 2_545
O109 Na10 O108 88.4(3) . .
O109 Na10 O92 175.6(5) . .
O109 Na10 O111 86.0(3) . .
O109 Na10 O110 91.1(3) . .
O92 Na10 O57 111.7(4) . .
O92 Na10 Na9 42.7(4) . 2_545
O92A Na10 O57 82.2(8) . .
O92A Na10 Na9A 56.5(9) . 2_545
O92A Na10 O108 91.5(7) . .
O92A Na10 O109 153.3(9) . .
O92A Na10 O111 97.7(7) . .
O92A Na10 O110 115.5(9) . .
O111 Na10 O57 117.1(3) . .
O111 Na10 Na9 73.9(3) . 2_545
O111 Na10 Na9A 72.4(4) . 2_545
O111 Na10 O92 91.1(4) . .
O110 Na10 O57 156.3(3) . .
O110 Na10 Na9 43.8(3) . 2_545
O110 Na10 Na9A 61.2(4) . 2_545
O110 Na10 O92 85.0(4) . .
O110 Na10 O111 77.8(3) . .
W14 Na11 Dy3 63.93(7) . .
W14 Na11 Na7 154.91(15) . .
Dy3 Na11 Na7 91.98(12) . .
O35 Na11 W14 89.90(16) . .
O35 Na11 Dy3 39.46(13) . .
O35 Na11 O16 114.8(2) . .
O35 Na11 Na7 65.72(15) . .
O29 Na11 W14 31.21(14) . .
O29 Na11 Dy3 34.28(14) . .
O29 Na11 O35 68.6(2) . .
O29 Na11 O16 61.7(2) . .
O29 Na11 Na7 126.0(2) . .
O29 Na11 O90A 89.2(4) . .
O16 Na11 W14 30.80(12) . .
O16 Na11 Dy3 94.67(15) . .
O16 Na11 Na7 168.6(2) . .
O90 Na11 W14 87.1(5) . .
O90 Na11 Dy3 130.6(6) . .
O90 Na11 O35 169.1(6) . .
O90 Na11 O29 104.3(6) . .
O90 Na11 O16 66.2(5) . .
O90 Na11 Na7 115.7(5) . .
O90 Na11 O84 97.7(6) . .
O90 Na11 O85 97.5(6) . .
O90A Na11 W14 81.9(3) . .
O90A Na11 Dy3 109.6(3) . .
O90A Na11 O35 146.5(4) . .
O90A Na11 O16 71.6(3) . .
O90A Na11 Na7 114.8(3) . .
O84 Na11 W14 119.4(3) . .
O84 Na11 Dy3 131.0(3) . .
O84 Na11 O35 93.0(3) . .
O84 Na11 O29 139.4(3) . .
O84 Na11 O16 98.5(3) . .
O84 Na11 Na7 70.2(3) . .
O84 Na11 O90A 119.4(4) . .
O84 Na11 O85 94.6(3) . .
O85 Na11 W14 144.8(3) . .
O85 Na11 Dy3 87.8(2) . .
O85 Na11 O35 79.0(3) . .
O85 Na11 O29 115.4(3) . .
O85 Na11 O16 160.3(3) . .
O85 Na11 Na7 29.24(19) . .
O85 Na11 O90A 89.1(4) . .
Na4 O82 Na3 125.6(3) 3_465 .
Na1 O108 Na10 90.5(3) . .
Na1 O109 Na10 90.8(3) . .
Na1 O106 Na5 95.2(3) . 2_445
Na10 O92 Na9 95.7(5) . 2_545
Na10 O92A Na9A 78.8(9) . 2_545
Na4 O103 Na5 126.9(3) . 2_445
Na7 O96 Na6 107.6(3) . .
Na8 O111 Na10 92.9(4) . .
Na10 O111 Na8A 107.6(4) . .
Na1 O105 Na5 95.4(2) . 2_445
Na8 O110 Na9 52.7(4) . 2_545
Na8 O110 Na10 92.3(3) . .
Na10 O110 Na9 95.6(3) . 2_545
Na10 O110 Na9A 72.4(4) . 2_545
Na11 O85 Na7 122.1(3) . .
Dy3 C1 Dy2 119.3(3) . .
Dy1 C1 Dy3 120.4(3) . .
Dy1 C1 Dy2 120.3(3) . .
O40 C1 Dy3 179.0(6) . .
O40 C1 Dy2 59.9(4) . .
O40 C1 Dy1 60.4(4) . .
O40 C1 O39 119.7(7) . .
O38 C1 Dy3 60.3(4) . .
O38 C1 Dy2 179.5(6) . .
O38 C1 Dy1 60.1(4) . .
O38 C1 O40 120.6(7) . .
O38 C1 O39 119.8(7) . .
O39 C1 Dy3 59.5(4) . .
O39 C1 Dy2 59.8(4) . .
O39 C1 Dy1 179.9(6) . .
W17 O5 W18 122.5(3) . .
O77 O95 Na9 109.4(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W15 O28 2.408(5) .
W15 O30 1.795(5) .
W15 O8 2.024(5) .
W15 O18 1.726(6) .
W15 O17 1.893(5) .
W15 O19 1.915(6) .
W17 O10 2.385(5) .
W17 O11 1.850(5) .
W17 O6 1.951(5) .
W17 O2 1.736(5) .
W17 O13 1.876(5) .
W17 Na2 3.590(3) .
W17 Na6 3.422(3) 1_455
W17 O5 1.944(5) .
W6 O47 1.733(5) .
W6 O68 2.017(5) .
W6 O48 1.913(5) .
W6 O46 1.797(5) .
W6 O59 2.409(5) .
W6 O58 1.915(5) .
W12 O27 2.390(5) .
W12 O15 1.909(5) .
W12 O14 1.730(5) .
W12 O25 1.918(6) .
W12 O9 1.981(5) .
W12 O34 1.814(5) .
W5 O66 2.029(5) .
W5 O54 1.916(5) .
W5 O44 1.781(5) .
W5 O61 2.378(5) .
W5 O56 1.909(5) .
W5 O55 1.737(6) .
W11 O21 1.887(6) .
W11 O26 2.404(5) .
W11 O32 1.815(5) .
W11 O23 1.931(5) .
W11 O22 1.727(5) .
W11 O13 2.004(5) .
W11 Na2 3.480(3) .
W10 O33 1.805(5) .
W10 O24 1.716(6) .
W10 O26 2.368(5) .
W10 O23 1.973(5) .
W10 O12 1.991(5) .
W10 O25 1.876(6) .
W10 Na2 3.498(3) .
W7 O52 1.916(5) .
W7 O54 1.887(6) .
W7 O43 1.796(5) .
W7 O65 2.042(5) .
W7 O60 2.328(5) .
W7 O118 1.740(5) .
W4 O45 1.814(5) .
W4 O57 1.721(6) .
W4 O61 2.436(5) .
W4 O56 1.932(5) .
W4 O67 1.992(5) .
W4 O58 1.883(5) .
W4 Na1 3.487(3) .
W1 O62 2.391(5) .
W1 O68 1.871(5) .
W1 O70 1.926(5) .
W1 O74 1.946(5) .
W1 O67 1.862(5) .
W1 O69 1.707(6) .
W8 O41 1.818(5) .
W8 O48 1.950(5) .
W8 O50 1.887(5) .
W8 O63 1.997(5) .
W8 O59 2.396(5) .
W8 O49 1.712(5) .
W13 O28 2.393(5) .
W13 O21 1.900(6) .
W13 O11 2.041(5) .
W13 O19 1.927(6) .
W13 O20 1.734(5) .
W13 O31 1.786(5) .
W3 O62 2.406(5) .
W3 O64 1.854(6) .
W3 O70 1.951(5) .
W3 O63 1.881(5) .
W3 O71 1.726(6) .
W3 O72 1.932(5) .
W3 Na9 3.603(8) .
W3 Na9A 3.700(17) .
W14 O27 2.383(5) .
W14 O7 2.005(5) .
W14 O15 1.941(5) .
W14 O29 1.796(5) .
W14 O17 1.903(5) .
W14 O16 1.716(6) .
W14 Na11 3.350(4) .
W18 O7 1.857(5) .
W18 O10 2.381(5) .
W18 O8 1.866(5) .
W18 O4 1.936(5) .
W18 O1 1.740(5) .
W18 O5 1.947(5) .
W16 O10 2.407(5) .
W16 O6 1.949(5) .
W16 O12 1.881(5) .
W16 O4 1.937(5) .
W16 O9 1.865(5) .
W16 O3 1.722(5) .
W16 Na2 3.594(3) .
W2 O66 1.839(5) .
W2 O73 1.746(6) .
W2 O62 2.380(5) .
W2 O74 1.945(5) .
W2 O65 1.845(6) .
W2 O72 1.938(5) .
W9 O52 1.924(6) .
W9 O50 1.911(5) .
W9 O64 2.028(5) .
W9 O42 1.788(5) .
W9 O51 1.725(6) .
W9 O60 2.410(5) .
W9 Na8 3.515(9) 4_666
Dy3 O41 2.265(5) .
Dy3 O35 2.444(5) .
Dy3 O38 2.433(5) .
Dy3 O46 2.264(5) .
Dy3 O29 2.271(5) .
Dy3 O39 2.416(6) .
Dy3 O34 2.247(5) .
Dy3 Na11 3.810(5) .
Dy3 C1 2.799(7) .
Dy2 O43 2.276(5) .
Dy2 O30 2.264(5) .
Dy2 O40 2.424(5) .
Dy2 O36 2.394(5) .
Dy2 O42 2.257(5) .
Dy2 O39 2.423(5) .
Dy2 O31 2.263(5) .
Dy2 C1 2.800(7) .
Dy1 O45 2.297(5) .
Dy1 O44 2.251(5) .
Dy1 O33 2.245(5) .
Dy1 O32 2.266(5) .
Dy1 O40 2.432(6) .
Dy1 O38 2.425(5) .
Dy1 O37 2.454(5) .
Dy1 C1 2.794(7) .
P1 O27 1.545(5) .
P1 O28 1.538(5) .
P1 O10 1.567(5) .
P1 O26 1.546(5) .
P2 O62 1.574(5) .
P2 O61 1.529(5) .
P2 O59 1.535(5) .
P2 O60 1.544(5) .
O52 Na8 2.634(10) 4_666
O45 Na1 2.577(6) .
O35 Na11 2.607(7) .
O57 Na10 2.809(9) .
O40 C1 1.284(9) .
O38 C1 1.282(9) .
O23 Na2 2.467(6) .
O6 Na2 2.790(6) .
O6 Na6 2.351(6) 1_455
O12 Na2 2.504(6) .
O51 Na8 2.924(11) 4_666
O51 Na8A 2.880(15) 4_666
O51 Na9A 2.958(17) .
O18 Na5 2.506(7) .
O29 Na11 2.404(6) .
O2 Na6 2.871(7) 1_455
O2 Na9 2.453(9) 1_455
O2 Na9A 2.769(17) 1_455
O37 Na1 2.428(6) .
O39 C1 1.288(9) .
O71 Na9 2.379(10) .
O71 Na9A 2.960(19) .
O49 Na6 2.357(6) .
O16 Na3 2.357(7) .
O16 Na11 2.828(7) .
O13 Na2 2.494(6) .
O99 Na2 2.345(6) .
O99 Na6 2.428(7) 1_455
O101 Na2 2.419(7) .
O101 Na4 2.535(7) .
O102 Na2 2.398(6) .
O102 Na4 2.486(7) .
Na1 Na5 3.538(5) 2_445
Na1 O108 2.364(7) .
Na1 O109 2.353(7) .
Na1 O106 2.340(7) .
Na1 O105 2.376(6) .
Na2 Na6 3.749(5) 1_455
Na3 O82 2.527(9) .
Na3 O80 2.372(11) .
Na3 O81 2.406(8) .
Na3 O79 2.547(12) .
Na3 O91 2.35(2) .
Na3 O91A 2.381(12) .
Na4 O82 2.520(8) 3_465
Na4 O93 2.48(3) .
Na4 O93A 2.493(15) .
Na4 O103 2.389(7) .
Na4 O100 2.322(7) .
Na5 Na1 3.538(5) 2_455
Na5 O106 2.450(7) 2_455
Na5 O103 2.407(7) 2_455
Na5 O97 2.320(7) .
Na5 O98 2.280(8) .
Na5 O105 2.408(7) 2_455
Na6 W17 3.422(3) 1_655
Na6 O6 2.351(6) 1_655
Na6 O2 2.871(7) 1_655
Na6 O99 2.428(7) 1_655
Na6 Na2 3.749(5) 1_655
Na6 Na7 3.832(5) .
Na6 O96 2.400(8) .
Na6 O94 2.278(8) .
Na7 Na11 4.156(6) .
Na7 O96 2.349(8) .
Na7 O88 2.345(7) .
Na7 O87 2.353(7) .
Na7 O86 2.311(8) .
Na7 O85 2.396(8) .
Na8 W9 3.515(8) 4_565
Na8 O52 2.634(10) 4_565
Na8 O51 2.924(11) 4_565
Na8 Na8 3.813(16) 3
Na8 Na9 2.163(12) 2_545
Na8 O111 2.261(13) .
Na8 O110 2.283(13) .
Na8A O51 2.880(15) 4_565
Na8A Na8A 1.21(3) 3
Na8A Na9A 3.17(2) 4_565
Na8A Na9A 2.41(2) 2_545
Na8A O111 2.893(17) .
Na9 O2 2.453(9) 1_655
Na9 Na8 2.163(12) 2
Na9 Na10 3.679(11) 2
Na9 O92 2.508(18) 2
Na9 O110 2.557(12) 2
Na9 O95 2.49(2) .
Na9A O2 2.769(16) 1_655
Na9A Na8A 2.41(2) 2
Na9A Na8A 3.17(2) 4_666
Na9A Na10 3.173(18) 2
Na9A O92A 2.70(4) 2
Na9A O110 2.918(17) 2
Na10 Na9 3.679(11) 2_545
Na10 Na9A 3.174(18) 2_545
Na10 O108 2.375(8) .
Na10 O109 2.373(8) .
Na10 O92 2.453(13) .
Na10 O92A 2.28(2) .
Na10 O111 2.410(9) .
Na10 O110 2.409(11) .
Na11 O90 2.20(2) .
Na11 O90A 2.456(13) .
Na11 O84 2.308(10) .
Na11 O85 2.355(9) .
O82 Na4 2.520(8) 3_465
O106 Na5 2.450(7) 2_445
O89 O117 1.82(3) .
O92 Na9 2.508(18) 2_545
O92A Na9A 2.70(4) 2_545
O103 Na5 2.407(7) 2_445
O105 Na5 2.408(7) 2_445
O110 Na9 2.557(12) 2_545
O110 Na9A 2.919(17) 2_545
O95 O77 1.63(2) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Dy3 O38 C1 Dy1 180.0(3) . .
Dy3 O38 C1 O40 -179.4(6) . .
Dy3 O38 C1 O39 -0.1(7) . .
Dy3 O39 C1 Dy2 -179.7(3) . .
Dy3 O39 C1 O40 179.4(6) . .
Dy3 O39 C1 O38 0.1(7) . .
Dy2 O40 C1 Dy1 -179.1(3) . .
Dy2 O40 C1 O38 -179.8(6) . .
Dy2 O40 C1 O39 0.9(7) . .
Dy2 O39 C1 Dy3 179.7(3) . .
Dy2 O39 C1 O40 -0.9(7) . .
Dy2 O39 C1 O38 179.8(6) . .
Dy1 O40 C1 Dy2 179.1(3) . .
Dy1 O40 C1 O38 -0.7(7) . .
Dy1 O40 C1 O39 -180.0(6) . .
Dy1 O38 C1 Dy3 -180.0(3) . .
Dy1 O38 C1 O40 0.7(7) . .
Dy1 O38 C1 O39 180.0(6) . .
O52 W7 O54 W5 8.9(12) . .
O52 W7 O43 Dy2 57.5(4) . .
O52 W9 O42 Dy2 -52.6(5) . .
O52 W9 O51 Na8 22.4(3) . 4_666
O52 W9 O51 Na8A 41.6(4) . 4_666
O52 W9 O51 Na9A 111.5(4) . .
O66 W5 O44 Dy1 31.5(11) . .
O66 W2 O65 W7 -21.9(6) . .
O41 W8 O50 W9 119.1(7) . .
O41 W8 O49 Na6 -145.8(4) . .
O27 W12 O34 Dy3 -17.2(4) . .
O27 W14 O29 Dy3 17.5(4) . .
O27 W14 O29 Na11 162.4(3) . .
O27 P1 O28 W15 55.1(4) . .
O27 P1 O28 W13 -178.8(3) . .
O27 P1 O10 W17 179.5(3) . .
O27 P1 O10 W18 -59.6(4) . .
O27 P1 O10 W16 59.9(4) . .
O27 P1 O26 W11 178.8(3) . .
O27 P1 O26 W10 -54.9(4) . .
O45 W4 O57 Na10 -75.8(5) . .
O45 W4 O58 W6 118.8(8) . .
O73 W2 O66 W5 123.5(6) . .
O73 W2 O65 W7 -124.5(6) . .
O7 W14 O29 Dy3 26.4(10) . .
O7 W14 O29 Na11 171.2(6) . .
O7 W14 O16 Na3 -31.0(5) . .
O7 W14 O16 Na11 -172.6(2) . .
O7 W18 O8 W15 -22.1(6) . .
O54 W5 O44 Dy1 100.6(4) . .
O54 W7 O43 Dy2 -101.5(4) . .
O28 W15 O30 Dy2 -20.1(4) . .
O28 W15 O17 W14 33.8(8) . .
O28 W13 O31 Dy2 18.2(4) . .
O28 P1 O27 W12 178.1(3) . .
O28 P1 O27 W14 -54.9(4) . .
O28 P1 O10 W17 -60.6(4) . .
O28 P1 O10 W18 60.4(4) . .
O28 P1 O10 W16 179.8(3) . .
O28 P1 O26 W11 56.3(4) . .
O28 P1 O26 W10 -177.4(3) . .
O43 W7 O54 W5 120.3(8) . .
O47 W6 O46 Dy3 -149.5(4) . .
O62 W1 O68 W6 -58.0(6) . .
O62 W1 O67 W4 66.1(6) . .
O62 W3 O64 W9 -58.0(6) . .
O62 W3 O63 W8 64.2(6) . .
O62 W2 O66 W5 -61.7(6) . .
O62 W2 O65 W7 61.5(6) . .
O62 P2 O61 W5 62.8(4) . .
O62 P2 O61 W4 -61.6(4) . .
O62 P2 O59 W6 64.3(4) . .
O62 P2 O59 W8 -62.7(4) . .
O62 P2 O60 W7 -65.0(4) . .
O62 P2 O60 W9 63.4(4) . .
O57 W4 O45 Dy1 157.0(4) . .
O57 W4 O45 Na1 26.8(3) . .
O57 W4 O58 W6 -139.3(7) . .
O33 W10 O25 W12 -122.6(7) . .
O24 W10 O33 Dy1 -158.3(4) . .
O24 W10 O25 W12 135.6(7) . .
O30 W15 O18 Na5 -136.4(4) . .
O30 W15 O17 W14 114.6(8) . .
O15 W12 O34 Dy3 55.9(4) . .
O15 W14 O29 Dy3 -55.3(4) . .
O15 W14 O29 Na11 89.5(3) . .
O15 W14 O16 Na3 53.8(5) . .
O15 W14 O16 Na11 -87.7(2) . .
O21 W11 O32 Dy1 -102.9(4) . .
O21 W13 O31 Dy2 102.1(4) . .
O61 W5 O44 Dy1 17.4(4) . .
O61 W4 O45 Dy1 -15.3(4) . .
O61 W4 O45 Na1 -145.5(2) . .
O61 W4 O58 W6 37.6(7) . .
O61 P2 O62 W1 59.8(4) . .
O61 P2 O62 W3 -179.8(3) . .
O61 P2 O62 W2 -60.5(4) . .
O61 P2 O59 W6 -55.1(4) . .
O61 P2 O59 W8 177.9(3) . .
O61 P2 O60 W7 54.2(4) . .
O61 P2 O60 W9 -177.3(3) . .
O10 W17 O11 W13 -57.5(6) . .
O10 W17 O2 Na6 31.1(12) . 1_455
O10 W17 O2 Na9 -168.7(9) . 1_455
O10 W17 O2 Na9A -148.7(12) . 1_455
O10 W17 O13 W11 62.3(5) . .
O10 W17 O13 Na2 -96.2(2) . .
O10 W18 O7 W14 -62.1(6) . .
O10 W18 O8 W15 61.8(6) . .
O10 W16 O12 W10 -65.5(5) . .
O10 W16 O12 Na2 97.4(2) . .
O10 W16 O9 W12 59.6(6) . .
O10 P1 O27 W12 -63.2(4) . .
O10 P1 O27 W14 63.8(4) . .
O10 P1 O28 W15 -63.3(4) . .
O10 P1 O28 W13 62.8(4) . .
O10 P1 O26 W11 -62.8(4) . .
O10 P1 O26 W10 63.5(4) . .
O68 W6 O46 Dy3 39.1(10) . .
O68 W1 O67 W4 -18.5(6) . .
O48 W6 O46 Dy3 -49.2(4) . .
O48 W8 O41 Dy3 55.6(4) . .
O48 W8 O50 W9 18.1(11) . .
O48 W8 O49 Na6 -53.0(5) . .
O26 W11 O21 W13 37.8(8) . .
O26 W11 O32 Dy1 -19.0(4) . .
O26 W10 O33 Dy1 13.4(4) . .
O26 W10 O25 W12 -41.1(7) . .
O26 P1 O27 W12 55.7(4) . .
O26 P1 O27 W14 -177.4(3) . .
O26 P1 O28 W15 177.5(3) . .
O26 P1 O28 W13 -56.4(4) . .
O26 P1 O10 W17 59.7(4) . .
O26 P1 O10 W18 -179.4(3) . .
O26 P1 O10 W16 -59.9(4) . .
O8 W15 O30 Dy2 -32.5(10) . .
O8 W15 O18 Na5 45.1(4) . .
O8 W15 O17 W14 -46.9(8) . .
O8 W18 O7 W14 21.7(6) . .
O11 W17 O2 Na6 168.0(2) . 1_455
O11 W17 O2 Na9 -31.7(5) . 1_455
O11 W17 O2 Na9A -11.8(11) . 1_455
O11 W17 O13 W11 -22.5(6) . .
O11 W17 O13 Na2 178.9(2) . .
O11 W13 O31 Dy2 34.6(11) . .
O14 W12 O34 Dy3 157.1(4) . .
O32 W11 O21 W13 118.9(8) . .
O56 W5 O44 Dy1 -56.0(4) . .
O56 W4 O45 Dy1 56.6(4) . .
O56 W4 O45 Na1 -73.6(2) . .
O56 W4 O57 Na10 17.8(5) . .
O56 W4 O58 W6 18.6(11) . .
O23 W11 O21 W13 13.6(12) . .
O23 W11 O32 Dy1 53.7(5) . .
O23 W10 O33 Dy1 -59.9(4) . .
O23 W10 O25 W12 -17.5(11) . .
O6 W17 O11 W13 -57.8(10) . .
O6 W17 O2 Na6 -8.9(2) . 1_455
O6 W17 O2 Na9 151.3(5) . 1_455
O6 W17 O2 Na9A 171.3(11) . 1_455
O6 W17 O13 W11 136.1(5) . .
O6 W17 O13 Na2 -22.5(2) . .
O6 W16 O12 W10 -138.9(6) . .
O6 W16 O12 Na2 24.0(2) . .
O6 W16 O9 W12 57.4(10) . .
O12 W10 O33 Dy1 8.6(10) . .
O12 W10 O25 W12 40.1(7) . .
O12 W16 O9 W12 -23.3(6) . .
O50 W8 O41 Dy3 -102.2(4) . .
O50 W8 O49 Na6 118.2(4) . .
O50 W9 O42 Dy2 104.3(5) . .
O50 W9 O51 Na8 -146.8(2) . 4_666
O50 W9 O51 Na8A -127.6(4) . 4_666
O50 W9 O51 Na9A -57.7(4) . .
O64 W3 O63 W8 -20.3(6) . .
O64 W3 O71 Na9 -16.0(4) . .
O64 W3 O71 Na9A -22.9(4) . .
O64 W9 O42 Dy2 35.0(10) . .
O64 W9 O51 Na8 -63.8(3) . 4_666
O64 W9 O51 Na8A -44.6(4) . 4_666
O64 W9 O51 Na9A 25.3(4) . .
O42 W9 O51 Na8 118.7(3) . 4_666
O42 W9 O51 Na8A 137.9(4) . 4_666
O42 W9 O51 Na9A -152.2(4) . .
O70 W1 O68 W6 -131.2(6) . .
O70 W1 O67 W4 66.5(9) . .
O70 W3 O64 W9 -53.0(10) . .
O70 W3 O63 W8 136.9(6) . .
O70 W3 O71 Na9 164.6(4) . .
O70 W3 O71 Na9A 157.8(4) . .
O74 W1 O68 W6 -57.6(10) . .
O74 W1 O67 W4 139.1(6) . .
O74 W2 O66 W5 -134.9(6) . .
O74 W2 O65 W7 64.5(9) . .
O51 W9 O42 Dy2 -152.3(5) . .
O18 W15 O30 Dy2 152.1(4) . .
O18 W15 O17 W14 -142.1(8) . .
O25 W12 O34 Dy3 -101.5(4) . .
O25 W10 O33 Dy1 98.9(4) . .
O29 W14 O16 Na3 149.1(4) . .
O29 W14 O16 Na11 7.6(3) . .
O67 W4 O45 Dy1 -20.8(10) . .
O67 W4 O45 Na1 -151.0(6) . .
O67 W4 O57 Na10 103.5(5) . .
O67 W4 O58 W6 -43.1(7) . .
O67 W1 O68 W6 25.2(6) . .
O17 W15 O30 Dy2 -105.0(4) . .
O17 W15 O18 Na5 128.0(4) . .
O17 W14 O29 Dy3 103.0(4) . .
O17 W14 O29 Na11 -112.1(3) . .
O17 W14 O16 Na3 -115.2(4) . .
O17 W14 O16 Na11 103.3(2) . .
O4 W18 O7 W14 -135.3(6) . .
O4 W18 O8 W15 60.5(9) . .
O4 W16 O12 W10 -66.6(8) . .
O4 W16 O12 Na2 96.2(5) . .
O4 W16 O9 W12 132.1(6) . .
O2 W17 O11 W13 130.4(6) . .
O2 W17 O13 W11 -126.6(5) . .
O2 W17 O13 Na2 74.8(3) . .
O65 W7 O54 W5 -43.8(8) . .
O65 W7 O43 Dy2 -23.5(11) . .
O65 W2 O66 W5 21.9(6) . .
O63 W8 O41 Dy3 -19.4(11) . .
O63 W8 O50 W9 -43.9(7) . .
O63 W8 O49 Na6 32.4(5) . .
O63 W3 O64 W9 25.2(6) . .
O63 W3 O71 Na9 75.7(4) . .
O63 W3 O71 Na9A 68.9(4) . .
O22 W11 O21 W13 -138.9(8) . .
O22 W11 O32 Dy1 154.8(4) . .
O19 W15 O30 Dy2 51.8(4) . .
O19 W15 O18 Na5 -40.2(4) . .
O19 W15 O17 W14 8.3(12) . .
O19 W13 O31 Dy2 -54.0(4) . .
O59 W6 O46 Dy3 22.7(4) . .
O59 W8 O41 Dy3 -16.6(4) . .
O59 W8 O50 W9 37.2(7) . .
O59 P2 O62 W1 -60.8(4) . .
O59 P2 O62 W3 59.6(4) . .
O59 P2 O62 W2 178.9(3) . .
O59 P2 O61 W5 -178.3(3) . .
O59 P2 O61 W4 57.2(4) . .
O59 P2 O60 W7 177.3(3) . .
O59 P2 O60 W9 -54.2(4) . .
O1 W18 O7 W14 124.5(6) . .
O1 W18 O8 W15 -124.5(6) . .
O58 W6 O46 Dy3 108.2(4) . .
O58 W4 O45 Dy1 -99.6(4) . .
O58 W4 O45 Na1 130.2(2) . .
O58 W4 O57 Na10 -171.1(5) . .
O20 W13 O31 Dy2 -156.1(4) . .
O60 W7 O54 W5 37.5(8) . .
O60 W7 O43 Dy2 -16.9(4) . .
O60 W9 O42 Dy2 19.3(4) . .
O60 P2 O62 W1 -179.7(3) . .
O60 P2 O62 W3 -59.3(4) . .
O60 P2 O62 W2 60.0(4) . .
O60 P2 O61 W5 -55.8(4) . .
O60 P2 O61 W4 179.7(3) . .
O60 P2 O59 W6 -178.2(3) . .
O60 P2 O59 W8 54.9(4) . .
O55 W5 O44 Dy1 -157.4(4) . .
O9 W12 O34 Dy3 -33.7(10) . .
O9 W16 O12 W10 18.4(6) . .
O9 W16 O12 Na2 -178.7(3) . .
O118 W7 O54 W5 -136.7(8) . .
O118 W7 O43 Dy2 158.1(4) . .
O3 W16 O12 W10 121.4(5) . .
O3 W16 O12 Na2 -75.7(3) . .
O3 W16 O9 W12 -127.3(6) . .
O71 W3 O64 W9 128.5(6) . .
O71 W3 O63 W8 -123.3(6) . .
O49 W8 O41 Dy3 154.6(4) . .
O49 W8 O50 W9 -138.9(7) . .
O16 W14 O29 Dy3 -154.1(4) . .
O16 W14 O29 Na11 -9.2(3) . .
O72 W3 O64 W9 -130.7(6) . .
O72 W3 O63 W8 66.3(9) . .
O72 W3 O71 Na9 -108.2(4) . .
O72 W3 O71 Na9A -115.1(4) . .
O72 W2 O66 W5 -63.9(9) . .
O72 W2 O65 W7 134.9(6) . .
O69 W1 O68 W6 128.7(6) . .
O69 W1 O67 W4 -121.6(6) . .
O13 W17 O11 W13 26.8(6) . .
O13 W17 O2 Na6 -98.2(2) . 1_455
O13 W17 O2 Na9 62.1(5) . 1_455
O13 W17 O2 Na9A 82.0(11) . 1_455
O13 W11 O21 W13 -44.0(8) . .
O13 W11 O32 Dy1 -25.2(11) . .
Na1 W4 O45 Dy1 130.2(5) . .
Na1 W4 O57 Na10 -53.9(4) . .
Na1 W4 O58 W6 157.9(7) . .
Na2 W17 O11 W13 27.8(7) . .
Na2 W17 O2 Na6 -59.03(15) . 1_455
Na2 W17 O2 Na9 101.2(4) . 1_455
Na2 W17 O2 Na9A 121.2(11) . 1_455
Na2 W17 O13 W11 158.6(7) . .
Na2 W11 O21 W13 -46.2(9) . .
Na2 W11 O32 Dy1 60.0(5) . .
Na2 W10 O33 Dy1 -67.2(5) . .
Na2 W10 O25 W12 44.3(8) . .
Na2 W16 O12 W10 -162.9(7) . .
Na2 W16 O9 W12 -24.4(7) . .
Na6 W17 O11 W13 157.7(3) 1_455 .
Na6 W17 O2 Na9 160.3(5) 1_455 1_455
Na6 W17 O2 Na9A -179.8(12) 1_455 1_455
Na6 W17 O13 W11 174.7(5) 1_455 .
Na6 W17 O13 Na2 16.1(2) 1_455 .
Na8 W9 O42 Dy2 -94.8(5) 4_666 .
Na9 W3 O64 W9 119.1(7) . .
Na9 W3 O63 W8 -90.3(6) . .
Na9A W3 O64 W9 106.8(8) . .
Na9A W3 O63 W8 -75.6(6) . .
Na11 W14 O29 Dy3 -144.9(6) . .
Na11 W14 O16 Na3 141.6(5) . .
O5 W17 O11 W13 -130.6(6) . .
O5 W17 O2 Na6 77.2(2) . 1_455
O5 W17 O2 Na9 -122.5(5) . 1_455
O5 W17 O2 Na9A -102.6(11) . 1_455
O5 W17 O13 W11 65.2(9) . .
O5 W17 O13 Na2 -93.3(6) . .
O5 W18 O7 W14 -63.1(9) . .
O5 W18 O8 W15 135.0(6) . .
