#------------------------------------------------------------------------------
#$Date: 2019-11-23 07:06:42 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232387 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/75/4347581.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347581
loop_
_publ_author_name
'Chang, Stephanie W.'
'Lewis, Andrew R.'
'Prosser, Kathleen E.'
'Thompson, John R.'
'Gladkikh, Margarita'
'Bally, Marcel B.'
'Warren, Jeffrey J.'
'Walsby, Charles J.'
_publ_section_title
;
 CF3 Derivatives of the Anticancer Ru(III) Complexes KP1019, NKP-1339, and
 Their Imidazole and Pyridine Analogues Show Enhanced Lipophilicity,
 Albumin Interactions, and Cytotoxicity.
;
_journal_issue                   10
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4850
_journal_page_last               4863
_journal_paper_doi               10.1021/acs.inorgchem.6b00359
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C8 H6 Cl4 F6 N4 Ru, C24 H20 P'
_chemical_formula_sum            'C32 H26 Cl4 F6 N4 P Ru'
_chemical_formula_weight         854.41
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_cell_angle_alpha                66.2780(16)
_cell_angle_beta                 84.0270(17)
_cell_angle_gamma                89.0000(18)
_cell_formula_units_Z            2
_cell_length_a                   10.9244(12)
_cell_length_b                   12.2867(14)
_cell_length_c                   14.6192(16)
_cell_measurement_reflns_used    9169
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      30.13
_cell_measurement_theta_min      2.29
_cell_volume                     1786.1(3)
_computing_cell_refinement       'Bruker SAINT (Bruker, 2013)'
_computing_data_collection       'Bruker APEX2 (Bruker, 2014)'
_computing_data_reduction        'Bruker SAINT (Bruker, 2013)'
_computing_structure_refinement  'SHELXL-2015 (Sheldrick 2015)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0261
_diffrn_reflns_av_unetI/netI     0.0183
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            42753
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.371
_diffrn_reflns_theta_min         1.811
_exptl_absorpt_coefficient_mu    0.844
_exptl_absorpt_correction_T_max  0.7460
_exptl_absorpt_correction_T_min  0.6757
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Sheldrick , 1996)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.589
_exptl_crystal_description       Block
_exptl_crystal_F_000             854
_refine_diff_density_max         2.108
_refine_diff_density_min         -0.635
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.044
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     467
_refine_ls_number_reflns         7281
_refine_ls_number_restraints     438
_refine_ls_restrained_S_all      1.065
_refine_ls_R_factor_all          0.0524
_refine_ls_R_factor_gt           0.0431
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0630P)²+3.8394P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1176
_refine_ls_wR_factor_ref         0.1260
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6179
_reflns_number_total             7281
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic6b00359_si_002.cif
_cod_data_source_block           2c
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_database_code               4347581
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.5000 0.0000 1.0000 0.02920(11) Uani 1 2 d S U P . .
N1 N 0.6360(3) 0.0083(3) 0.8868(2) 0.0372(7) Uani 1 1 d . U . . .
Cl1 Cl 0.52144(10) 0.20716(8) 0.95440(7) 0.0464(2) Uani 1 1 d . U . . .
Ru2 Ru 0.5000 0.0000 0.5000 0.03064(12) Uani 1 2 d S U P . .
N2 N 0.4755(3) 0.1130(3) 0.3530(2) 0.0336(6) Uani 1 1 d . U . . .
Cl2 Cl 0.34809(9) 0.03277(10) 0.88862(7) 0.0471(2) Uani 1 1 d . U . . .
P300 P 0.84408(9) 0.49936(9) 0.28616(7) 0.0353(2) Uani 1 1 d . U . . .
F11 F 1.0021(10) -0.0417(12) 0.7399(12) 0.1343(17) Uani 0.531(6) 1 d D U P A 1
F12 F 0.9370(8) -0.1873(9) 0.8690(9) 0.1343(17) Uani 0.531(6) 1 d D U P A 1
F13 F 0.8877(8) -0.1767(11) 0.7407(11) 0.1343(17) Uani 0.531(6) 1 d D U P A 1
F13A F 0.8913(8) -0.0679(11) 0.6637(9) 0.1343(17) Uani 0.469(6) 1 d D U P A 2
F12A F 0.9085(10) -0.2025(10) 0.8164(11) 0.1343(17) Uani 0.469(6) 1 d D U P A 2
F11A F 0.9988(11) -0.0256(14) 0.7642(14) 0.1343(17) Uani 0.469(6) 1 d D U P A 2
F21 F 0.2903(7) 0.4217(5) 0.1980(4) 0.110(2) Uani 0.885(9) 1 d . U P B 1
F22 F 0.4625(6) 0.4647(4) 0.1088(4) 0.111(2) Uani 0.885(9) 1 d . U P B 1
F23 F 0.3297(6) 0.3686(4) 0.0746(4) 0.099(2) Uani 0.885(9) 1 d . U P B 1
F21A F 0.259(3) 0.358(3) 0.131(3) 0.077(7) Uani 0.115(9) 1 d . U P B 2
F22A F 0.437(4) 0.425(3) 0.067(2) 0.075(7) Uani 0.115(9) 1 d . U P B 2
F23A F 0.365(4) 0.454(3) 0.180(3) 0.071(6) Uani 0.115(9) 1 d . U P B 2
Cl4 Cl 0.31677(9) 0.06565(9) 0.55938(7) 0.0457(2) Uani 1 1 d . U . . .
Cl3 Cl 0.38578(10) -0.15395(9) 0.48483(7) 0.0466(2) Uani 1 1 d . U . . .
N12 N 0.7324(4) 0.0529(5) 0.7367(3) 0.0688(12) Uani 1 1 d . U . . .
H12 H 0.7515 0.0876 0.6728 0.18(4) Uiso 1 1 calc R . . . .
N22 N 0.4797(3) 0.1855(3) 0.1890(2) 0.0383(7) Uani 1 1 d . U . . .
H22 H 0.498(4) 0.192(4) 0.126(4) 0.054(13) Uiso 1 1 d . . . . .
C11 C 0.7304(4) -0.0687(4) 0.8966(4) 0.0498(10) Uani 1 1 d . U . . .
H11 H 0.7502 -0.1292 0.9559 0.060 Uiso 1 1 calc R U . . .
C12 C 0.7901(5) -0.0397(6) 0.8027(5) 0.0690(13) Uani 1 1 d . U . . .
C13 C 0.6408(4) 0.0789(4) 0.7904(3) 0.0498(10) Uani 1 1 d . U . . .
H13 H 0.5862 0.1396 0.7635 0.060 Uiso 1 1 calc R U . . .
C21 C 0.5101(3) 0.0947(3) 0.2710(3) 0.0345(7) Uani 1 1 d . U . . .
H21 H 0.5503 0.0276 0.2704 0.041 Uiso 1 1 calc R U . . .
C22 C 0.4225(4) 0.2668(3) 0.2200(3) 0.0414(8) Uani 1 1 d . U . . .
C23 C 0.4200(4) 0.2210(3) 0.3217(3) 0.0419(9) Uani 1 1 d . U . . .
H23 H 0.3862 0.2570 0.3633 0.050 Uiso 1 1 calc R U . . .
C24 C 0.3749(6) 0.3791(4) 0.1502(4) 0.0630(12) Uani 1 1 d . U . . .
C301 C 0.8255(3) 0.4127(3) 0.2149(3) 0.0371(8) Uani 1 1 d . U . . .
C302 C 0.8400(5) 0.4657(4) 0.1099(3) 0.0528(11) Uani 1 1 d . U . . .
H302 H 0.8618 0.5460 0.0760 0.063 Uiso 1 1 calc R U . . .
C303 C 0.8215(5) 0.3970(5) 0.0574(4) 0.0655(13) Uani 1 1 d . U . . .
H303 H 0.8300 0.4316 -0.0124 0.079 Uiso 1 1 calc R U . . .
C304 C 0.7906(5) 0.2783(5) 0.1071(4) 0.0614(12) Uani 1 1 d . U . . .
H304 H 0.7786 0.2331 0.0707 0.074 Uiso 1 1 calc R U . . .
C305 C 0.7773(4) 0.2257(4) 0.2105(4) 0.0529(10) Uani 1 1 d . U . . .
H305 H 0.7572 0.1450 0.2437 0.063 Uiso 1 1 calc R U . . .
C306 C 0.7938(4) 0.2926(4) 0.2646(3) 0.0450(9) Uani 1 1 d . U . . .
H306 H 0.7838 0.2574 0.3345 0.054 Uiso 1 1 calc R U . . .
C307 C 0.6987(4) 0.5495(4) 0.3211(3) 0.0408(8) Uani 1 1 d . U . . .
C308 C 0.5903(4) 0.5024(4) 0.3098(4) 0.0566(12) Uani 1 1 d . U . . .
H308 H 0.5919 0.4454 0.2830 0.068 Uiso 1 1 calc R U . . .
C309 C 0.4784(5) 0.5414(5) 0.3392(5) 0.0740(16) Uani 1 1 d . U . . .
H309 H 0.4048 0.5103 0.3317 0.089 Uiso 1 1 calc R U . . .
C310 C 0.4762(5) 0.6252(5) 0.3790(4) 0.0647(13) Uani 1 1 d . U . . .
H310 H 0.4012 0.6507 0.3986 0.078 Uiso 1 1 calc R U . . .
C311 C 0.5827(5) 0.6710(5) 0.3899(4) 0.0666(13) Uani 1 1 d . U . . .
H311 H 0.5803 0.7275 0.4173 0.080 Uiso 1 1 calc R U . . .
C312 C 0.6947(5) 0.6348(4) 0.3608(4) 0.0585(12) Uani 1 1 d . U . . .
H312 H 0.7674 0.6676 0.3679 0.070 Uiso 1 1 calc R U . . .
C313 C 0.9128(4) 0.4051(4) 0.3969(3) 0.0459(9) Uani 1 1 d . U . . .
C314 C 0.8691(5) 0.3997(5) 0.4905(3) 0.0631(13) Uani 1 1 d . U . . .
H314 H 0.8042 0.4466 0.4977 0.076 Uiso 1 1 calc R U . . .
C315 C 0.9237(7) 0.3227(6) 0.5747(4) 0.0886(18) Uani 1 1 d . U . . .
H315 H 0.8939 0.3162 0.6387 0.106 Uiso 1 1 calc R U . . .
C316 C 1.0216(7) 0.2571(6) 0.5617(6) 0.097(2) Uani 1 1 d . U . . .
H316 H 1.0590 0.2075 0.6175 0.116 Uiso 1 1 calc R U . . .
C317 C 1.0646(7) 0.2625(7) 0.4708(6) 0.099(2) Uani 1 1 d . U . . .
H317 H 1.1314 0.2174 0.4639 0.118 Uiso 1 1 calc R U . . .
C318 C 1.0102(5) 0.3347(5) 0.3878(4) 0.0733(15) Uani 1 1 d . U . . .
H318 H 1.0386 0.3365 0.3250 0.088 Uiso 1 1 calc R U . . .
C319 C 0.9427(4) 0.6272(4) 0.2128(3) 0.0411(8) Uani 1 1 d . U . . .
C320 C 0.8938(5) 0.7374(4) 0.1637(4) 0.0607(12) Uani 1 1 d . U . . .
H320 H 0.8090 0.7467 0.1687 0.073 Uiso 1 1 calc R U . . .
C321 C 0.9718(6) 0.8343(5) 0.1067(5) 0.0759(16) Uani 1 1 d . U . . .
H321 H 0.9390 0.9085 0.0737 0.091 Uiso 1 1 calc R U . . .
C322 C 1.0973(5) 0.8213(5) 0.0988(4) 0.0659(13) Uani 1 1 d . U . . .
H322 H 1.1491 0.8866 0.0607 0.079 Uiso 1 1 calc R U . . .
C323 C 1.1452(5) 0.7124(5) 0.1469(4) 0.0607(12) Uani 1 1 d . U . . .
H323 H 1.2300 0.7035 0.1410 0.073 Uiso 1 1 calc R U . . .
C324 C 1.0690(4) 0.6148(4) 0.2045(3) 0.0516(10) Uani 1 1 d . U . . .
H324 H 1.1026 0.5409 0.2375 0.062 Uiso 1 1 calc R U . . .
C14 C 0.8982(7) -0.0918(8) 0.7714(8) 0.129(2) Uani 1 1 d D U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ru1 N1 180.0 2_657 .
N1 Ru1 Cl2 90.27(9) 2_657 2_657
N1 Ru1 Cl2 89.73(9) . 2_657
N1 Ru1 Cl2 89.73(9) 2_657 .
N1 Ru1 Cl2 90.27(9) . .
Cl2 Ru1 Cl2 180.00(3) 2_657 .
N1 Ru1 Cl1 91.03(9) 2_657 2_657
N1 Ru1 Cl1 88.97(9) . 2_657
Cl2 Ru1 Cl1 90.52(4) 2_657 2_657
Cl2 Ru1 Cl1 89.48(4) . 2_657
N1 Ru1 Cl1 88.97(9) 2_657 .
N1 Ru1 Cl1 91.03(9) . .
Cl2 Ru1 Cl1 89.48(4) 2_657 .
Cl2 Ru1 Cl1 90.52(4) . .
Cl1 Ru1 Cl1 180.0 2_657 .
C13 N1 C11 106.7(4) . .
C13 N1 Ru1 127.2(3) . .
C11 N1 Ru1 125.7(3) . .
N2 Ru2 N2 180.0 2_656 .
N2 Ru2 Cl4 89.39(9) 2_656 .
N2 Ru2 Cl4 90.61(9) . .
N2 Ru2 Cl4 90.61(9) 2_656 2_656
N2 Ru2 Cl4 89.39(9) . 2_656
Cl4 Ru2 Cl4 180.00(5) . 2_656
N2 Ru2 Cl3 89.53(9) 2_656 .
N2 Ru2 Cl3 90.47(9) . .
Cl4 Ru2 Cl3 89.71(4) . .
Cl4 Ru2 Cl3 90.29(4) 2_656 .
N2 Ru2 Cl3 90.46(9) 2_656 2_656
N2 Ru2 Cl3 89.54(9) . 2_656
Cl4 Ru2 Cl3 90.29(4) . 2_656
Cl4 Ru2 Cl3 89.71(4) 2_656 2_656
Cl3 Ru2 Cl3 180.0 . 2_656
C21 N2 C23 106.2(3) . .
C21 N2 Ru2 126.8(2) . .
C23 N2 Ru2 126.9(2) . .
C301 P300 C307 111.06(18) . .
C301 P300 C319 109.82(18) . .
C307 P300 C319 108.65(19) . .
C301 P300 C313 106.96(19) . .
C307 P300 C313 110.0(2) . .
C319 P300 C313 110.3(2) . .
C13 N12 C12 106.1(4) . .
C21 N22 C22 107.3(3) . .
C12 C11 N1 106.8(5) . .
N12 C12 C11 108.4(4) . .
N12 C12 C14 122.2(6) . .
C11 C12 C14 129.4(7) . .
N1 C13 N12 112.0(5) . .
N2 C21 N22 111.0(3) . .
C23 C22 N22 106.6(3) . .
C23 C22 C24 130.5(4) . .
N22 C22 C24 123.0(4) . .
C22 C23 N2 108.9(3) . .
F23A C24 F22A 105(2) . .
F23 C24 F21 109.7(6) . .
F23 C24 F22 105.5(5) . .
F21 C24 F22 105.3(6) . .
F23A C24 F21A 106(2) . .
F22A C24 F21A 106(2) . .
F23A C24 C22 114.9(16) . .
F22A C24 C22 114.5(15) . .
F23 C24 C22 112.9(4) . .
F21 C24 C22 110.8(4) . .
F22 C24 C22 112.3(5) . .
F21A C24 C22 109.1(12) . .
C306 C301 C302 120.0(4) . .
C306 C301 P300 119.5(3) . .
C302 C301 P300 120.4(3) . .
C303 C302 C301 118.9(4) . .
C304 C303 C302 120.8(5) . .
C303 C304 C305 120.4(4) . .
C306 C305 C304 119.9(4) . .
C305 C306 C301 120.0(4) . .
C308 C307 C312 119.7(4) . .
C308 C307 P300 120.3(3) . .
C312 C307 P300 120.0(3) . .
C307 C308 C309 119.2(4) . .
C310 C309 C308 120.3(5) . .
C311 C310 C309 120.2(5) . .
C310 C311 C312 120.7(5) . .
C311 C312 C307 119.8(5) . .
C314 C313 C318 119.5(5) . .
C314 C313 P300 121.3(4) . .
C318 C313 P300 119.2(4) . .
C313 C314 C315 119.1(6) . .
C316 C315 C314 119.3(6) . .
C317 C316 C315 121.7(6) . .
C316 C317 C318 119.9(7) . .
C317 C318 C313 120.4(6) . .
C320 C319 C324 119.5(4) . .
C320 C319 P300 120.8(3) . .
C324 C319 P300 119.7(3) . .
C319 C320 C321 119.7(5) . .
C322 C321 C320 120.6(5) . .
C323 C322 C321 119.6(5) . .
C322 C323 C324 120.7(5) . .
C319 C324 C323 120.0(5) . .
F11 C14 F13 109.9(7) . .
F12A C14 F11A 115.4(12) . .
F11 C14 C12 125.3(8) . .
F12A C14 C12 117.0(8) . .
F13 C14 C12 121.1(7) . .
F11A C14 C12 109.1(7) . .
F12A C14 F13A 106.3(9) . .
F11A C14 F13A 100.9(11) . .
C12 C14 F13A 106.5(8) . .
F11 C14 F12 95.9(11) . .
F13 C14 F12 87.0(9) . .
C12 C14 F12 104.9(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ru1 N1 2.078(3) 2_657
Ru1 N1 2.078(3) .
Ru1 Cl2 2.3620(9) 2_657
Ru1 Cl2 2.3620(9) .
Ru1 Cl1 2.3666(10) 2_657
Ru1 Cl1 2.3666(10) .
N1 C13 1.320(5) .
N1 C11 1.366(5) .
Ru2 N2 2.079(3) 2_656
Ru2 N2 2.079(3) .
Ru2 Cl4 2.3572(9) .
Ru2 Cl4 2.3572(9) 2_656
Ru2 Cl3 2.3794(10) .
Ru2 Cl3 2.3795(10) 2_656
N2 C21 1.323(4) .
N2 C23 1.371(5) .
P300 C301 1.790(4) .
P300 C307 1.793(4) .
P300 C319 1.800(4) .
P300 C313 1.800(4) .
F11 C14 1.252(12) .
F12 C14 1.535(13) .
F13 C14 1.301(11) .
F13A C14 1.490(13) .
F12A C14 1.259(13) .
F11A C14 1.349(12) .
F21 C24 1.326(7) .
F22 C24 1.338(7) .
F23 C24 1.309(7) .
F21A C24 1.37(3) .
F22A C24 1.24(3) .
F23A C24 1.16(3) .
N12 C13 1.321(6) .
N12 C12 1.357(8) .
N22 C21 1.336(5) .
N22 C22 1.371(5) .
C11 C12 1.366(7) .
C12 C14 1.453(8) .
C22 C23 1.358(5) .
C22 C24 1.473(6) .
C301 C306 1.389(6) .
C301 C302 1.397(6) .
C302 C303 1.379(6) .
C303 C304 1.372(7) .
C304 C305 1.376(7) .
C305 C306 1.375(6) .
C307 C308 1.380(6) .
C307 C312 1.387(6) .
C308 C309 1.394(7) .
C309 C310 1.371(8) .
C310 C311 1.352(8) .
C311 C312 1.379(7) .
C313 C314 1.377(6) .
C313 C318 1.389(7) .
C314 C315 1.401(8) .
C315 C316 1.371(11) .
C316 C317 1.338(11) .
C317 C318 1.370(8) .
C319 C320 1.381(6) .
C319 C324 1.384(6) .
C320 C321 1.388(7) .
C321 C322 1.375(8) .
C322 C323 1.362(8) .
C323 C324 1.385(7) .
