#------------------------------------------------------------------------------
#$Date: 2019-11-23 07:19:09 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232410 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/76/4347634.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347634
loop_
_publ_author_name
'Lim, Kwang Soo'
'Baldoví, José J'
'Lee, Woo Ram'
'Song, Jeong Hwa'
'Yoon, Sung Won'
'Suh, Byoung Jin'
'Coronado, Eugenio'
'Gaita-Ariño, Alejandro'
'Hong, Chang Seop'
_publ_section_title
;
 Switching of Slow Magnetic Relaxation Dynamics in Mononuclear
 Dysprosium(III) Compounds with Charge Density.
;
_journal_issue                   11
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5398
_journal_page_last               5404
_journal_paper_doi               10.1021/acs.inorgchem.6b00410
_journal_volume                  55
_journal_year                    2016
_chemical_formula_sum            'C22 H46 Co2 Dy N O21 P6'
_chemical_formula_weight         1126.78
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 102.686(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.3285(7)
_cell_length_b                   19.4664(10)
_cell_length_c                   16.7740(10)
_cell_measurement_reflns_used    63845
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      21.1745
_cell_measurement_theta_min      2.489
_cell_volume                     3927.3(4)
_computing_cell_refinement       'Bruker SMART APEXll'
_computing_data_collection       'Bruker SMART APEXll'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    WingX
_computing_publication_material  WingX
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SHELXTL
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'omega & phi scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0848
_diffrn_reflns_av_sigmaI/netI    0.0685
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            62195
_diffrn_reflns_theta_full        28.38
_diffrn_reflns_theta_max         28.38
_diffrn_reflns_theta_min         1.63
_exptl_absorpt_coefficient_mu    3.042
_exptl_absorpt_correction_T_max  0.7117
_exptl_absorpt_correction_T_min  0.5676
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.906
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2252
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.12
_refine_diff_density_max         2.231
_refine_diff_density_min         -0.978
_refine_diff_density_rms         0.156
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     490
_refine_ls_number_reflns         9809
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.061
_refine_ls_R_factor_all          0.0958
_refine_ls_R_factor_gt           0.0495
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0501P)²+1.7202P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1084
_refine_ls_wR_factor_ref         0.1286
_reflns_number_gt                5826
_reflns_number_total             9809
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic6b00410_si_002.cif
_cod_data_source_block           complex2
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      P(2)1/c
_cod_database_code               4347634
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.295274(19) 0.216907(13) 0.760357(16) 0.03153(9) Uani 1 1 d .
O1 O 0.4754(3) 0.25977(19) 0.7721(2) 0.0398(10) Uani 1 1 d .
P1 P 0.59161(11) 0.23929(8) 0.81182(10) 0.0354(4) Uani 1 1 d .
O7 O 0.6497(3) 0.3024(2) 0.8654(3) 0.0536(12) Uani 1 1 d .
C6 C 0.5959(6) 0.3657(3) 0.8698(5) 0.067(2) Uani 1 1 d .
H6A H 0.5791 0.3867 0.8168 0.100 Uiso 1 1 calc R
H6B H 0.6438 0.3954 0.9078 0.100 Uiso 1 1 calc R
H6C H 0.5283 0.3580 0.8880 0.100 Uiso 1 1 calc R
O8 O 0.6634(3) 0.2341(2) 0.7438(3) 0.0463(11) Uani 1 1 d .
C7 C 0.6598(6) 0.2898(3) 0.6874(4) 0.0609(19) Uani 1 1 d .
H7A H 0.5849 0.2960 0.6568 0.091 Uiso 1 1 calc R
H7B H 0.7072 0.2796 0.6505 0.091 Uiso 1 1 calc R
H7C H 0.6848 0.3312 0.7169 0.091 Uiso 1 1 calc R
O2 O 0.4053(3) 0.12417(18) 0.7405(2) 0.0388(9) Uani 1 1 d .
P2 P 0.51175(12) 0.09208(7) 0.78234(10) 0.0358(4) Uani 1 1 d .
O9 O 0.5856(3) 0.0749(2) 0.7178(2) 0.0440(10) Uani 1 1 d .
C8 C 0.5401(6) 0.0362(3) 0.6459(4) 0.0587(19) Uani 1 1 d .
H8A H 0.5241 -0.0097 0.6610 0.088 Uiso 1 1 calc R
H8B H 0.5927 0.0346 0.6115 0.088 Uiso 1 1 calc R
H8C H 0.4727 0.0576 0.6170 0.088 Uiso 1 1 calc R
O10 O 0.4851(3) 0.0155(2) 0.8071(3) 0.0509(11) Uani 1 1 d .
C9 C 0.4053(5) 0.0048(3) 0.8557(4) 0.0616(19) Uani 1 1 d .
H9A H 0.4375 0.0164 0.9115 0.092 Uiso 1 1 calc R
H9B H 0.3830 -0.0426 0.8526 0.092 Uiso 1 1 calc R
H9C H 0.3415 0.0332 0.8359 0.092 Uiso 1 1 calc R
O3 O 0.3732(3) 0.1918(2) 0.8940(2) 0.0407(10) Uani 1 1 d .
P3 P 0.48782(12) 0.17585(8) 0.94228(9) 0.0374(4) Uani 1 1 d .
O11 O 0.4780(3) 0.1188(2) 1.0082(3) 0.0531(12) Uani 1 1 d .
C10 C 0.3911(5) 0.1204(4) 1.0517(4) 0.064(2) Uani 1 1 d .
H10A H 0.4012 0.1592 1.0879 0.096 Uiso 1 1 calc R
H10B H 0.3926 0.0789 1.0828 0.096 Uiso 1 1 calc R
H10C H 0.3207 0.1242 1.0136 0.096 Uiso 1 1 calc R
O12 O 0.5328(3) 0.2411(2) 0.9965(3) 0.0571(13) Uani 1 1 d .
C11 C 0.4614(6) 0.2918(3) 1.0206(5) 0.068(2) Uani 1 1 d .
H11A H 0.4038 0.3041 0.9743 0.102 Uiso 1 1 calc R
H11B H 0.5042 0.3319 1.0407 0.102 Uiso 1 1 calc R
H11C H 0.4286 0.2734 1.0629 0.102 Uiso 1 1 calc R
Co1 Co 0.61970(6) 0.14564(4) 0.88232(5) 0.03414(19) Uani 1 1 d .
C1 C 0.7285(5) 0.1344(4) 0.9942(4) 0.060(2) Uani 1 1 d .
H1 H 0.7151 0.1507 1.0433 0.072 Uiso 1 1 calc R
C2 C 0.7817(5) 0.1707(4) 0.9428(4) 0.0546(18) Uani 1 1 d .
H2 H 0.8104 0.2150 0.9507 0.065 Uiso 1 1 calc R
C3 C 0.7837(4) 0.1275(3) 0.8767(4) 0.0451(16) Uani 1 1 d .
H3 H 0.8140 0.1387 0.8323 0.054 Uiso 1 1 calc R
C4 C 0.7332(5) 0.0651(3) 0.8873(4) 0.0520(17) Uani 1 1 d .
H4 H 0.7245 0.0277 0.8521 0.062 Uiso 1 1 calc R
C5 C 0.6980(5) 0.0695(3) 0.9610(4) 0.0507(17) Uani 1 1 d .
H5 H 0.6611 0.0355 0.9836 0.061 Uiso 1 1 calc R
O4 O 0.2175(3) 0.1908(2) 0.6270(2) 0.0393(9) Uani 1 1 d .
P4 P 0.10739(13) 0.16498(8) 0.57980(9) 0.0394(4) Uani 1 1 d .
O13 O 0.0607(4) 0.2193(2) 0.5106(3) 0.0704(16) Uani 1 1 d .
C17 C 0.1255(8) 0.2712(5) 0.4863(6) 0.115(4) Uani 1 1 d .
H17A H 0.1830 0.2848 0.5320 0.172 Uiso 1 1 calc R
H17B H 0.0793 0.3101 0.4668 0.172 Uiso 1 1 calc R
H17C H 0.1585 0.2543 0.4433 0.172 Uiso 1 1 calc R
O14 O 0.1288(4) 0.0995(2) 0.5290(3) 0.0721(15) Uani 1 1 d .
C18 C 0.2267(8) 0.0952(5) 0.4961(6) 0.129(5) Uani 1 1 d .
H18A H 0.2143 0.1194 0.4450 0.193 Uiso 1 1 calc R
H18B H 0.2429 0.0479 0.4876 0.193 Uiso 1 1 calc R
H18C H 0.2883 0.1155 0.5338 0.193 Uiso 1 1 calc R
O5 O 0.1913(3) 0.12112(19) 0.7800(2) 0.0452(10) Uani 1 1 d .
P5 P 0.08141(12) 0.08978(8) 0.74311(10) 0.0374(4) Uani 1 1 d .
O15 O 0.1013(4) 0.0101(2) 0.7263(3) 0.0566(12) Uani 1 1 d .
C19 C 0.1818(6) -0.0092(4) 0.6808(5) 0.080(2) Uani 1 1 d .
H19A H 0.1479 -0.0090 0.6235 0.120 Uiso 1 1 calc R
H19B H 0.2090 -0.0545 0.6969 0.120 Uiso 1 1 calc R
H19C H 0.2424 0.0228 0.6915 0.120 Uiso 1 1 calc R
O16 O 0.0122(3) 0.0801(2) 0.8116(3) 0.0513(11) Uani 1 1 d .
C20 C 0.0646(6) 0.0520(4) 0.8887(4) 0.066(2) Uani 1 1 d .
H20A H 0.0893 0.0062 0.8813 0.100 Uiso 1 1 calc R
H20B H 0.0126 0.0510 0.9237 0.100 Uiso 1 1 calc R
H20C H 0.1273 0.0799 0.9132 0.100 Uiso 1 1 calc R
O6 O 0.1134(3) 0.2557(2) 0.7480(2) 0.0412(10) Uani 1 1 d .
P6 P -0.00100(12) 0.23616(8) 0.70372(10) 0.0371(4) Uani 1 1 d .
O17 O -0.0810(3) 0.2389(2) 0.7663(3) 0.0590(13) Uani 1 1 d .
C21 C -0.0766(6) 0.2950(4) 0.8206(5) 0.076(2) Uani 1 1 d .
H21A H -0.0025 0.2995 0.8531 0.114 Uiso 1 1 calc R
H21B H -0.1273 0.2871 0.8557 0.114 Uiso 1 1 calc R
H21C H -0.0972 0.3364 0.7899 0.114 Uiso 1 1 calc R
O18 O -0.0494(4) 0.2955(2) 0.6418(3) 0.0627(14) Uani 1 1 d .
C22 C -0.0052(7) 0.3604(4) 0.6393(5) 0.095(3) Uani 1 1 d .
H22A H -0.0016 0.3830 0.6907 0.143 Uiso 1 1 calc R
H22B H -0.0516 0.3865 0.5964 0.143 Uiso 1 1 calc R
H22C H 0.0682 0.3569 0.6290 0.143 Uiso 1 1 calc R
Co2 Co -0.02650(6) 0.13912(4) 0.63984(5) 0.03585(19) Uani 1 1 d .
C12 C -0.1940(5) 0.1268(4) 0.6417(4) 0.0519(17) Uani 1 1 d .
H12 H -0.2272 0.1439 0.6823 0.062 Uiso 1 1 calc R
C13 C -0.1858(5) 0.1602(4) 0.5701(5) 0.060(2) Uani 1 1 d .
H13 H -0.2142 0.2035 0.5539 0.071 Uiso 1 1 calc R
C14 C -0.1292(6) 0.1189(4) 0.5274(4) 0.065(2) Uani 1 1 d .
H14 H -0.1115 0.1300 0.4778 0.079 Uiso 1 1 calc R
C15 C -0.1022(5) 0.0581(4) 0.5695(5) 0.060(2) Uani 1 1 d .
H15 H -0.0644 0.0212 0.5531 0.072 Uiso 1 1 calc R
C16 C -0.1425(5) 0.0621(3) 0.6415(5) 0.0572(19) Uani 1 1 d .
H16 H -0.1364 0.0283 0.6815 0.069 Uiso 1 1 calc R
O19 O 0.2985(3) 0.3329(2) 0.8258(3) 0.0466(10) Uani 1 1 d .
O20 O 0.2786(3) 0.3325(2) 0.6948(3) 0.0456(10) Uani 1 1 d .
N1 N 0.2809(4) 0.3647(3) 0.7593(4) 0.0487(14) Uani 1 1 d .
O21 O 0.2648(5) 0.4275(3) 0.7570(4) 0.0942(19) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
O3 Dy1 O4 154.82(15)
O3 Dy1 O2 80.89(13)
O4 Dy1 O2 79.62(13)
O3 Dy1 O5 79.38(14)
O4 Dy1 O5 80.50(13)
O2 Dy1 O5 75.82(14)
O3 Dy1 O6 110.17(13)
O4 Dy1 O6 78.28(13)
O2 Dy1 O6 144.92(13)
O5 Dy1 O6 73.92(13)
O3 Dy1 O1 78.90(13)
O4 Dy1 O1 110.33(13)
O2 Dy1 O1 73.51(12)
O5 Dy1 O1 144.69(13)
O6 Dy1 O1 140.22(14)
O3 Dy1 O20 126.93(15)
O4 Dy1 O20 78.08(14)
O2 Dy1 O20 129.18(14)
O5 Dy1 O20 142.30(13)
O6 Dy1 O20 71.59(13)
O1 Dy1 O20 72.54(12)
O3 Dy1 O19 78.53(14)
O4 Dy1 O19 126.21(14)
O2 Dy1 O19 143.91(12)
O5 Dy1 O19 128.04(14)
O6 Dy1 O19 70.73(13)
O1 Dy1 O19 73.64(13)
O20 Dy1 O19 51.08(15)
O3 Dy1 N1 103.37(16)
O4 Dy1 N1 101.77(16)
O2 Dy1 N1 144.21(13)
O5 Dy1 N1 139.96(14)
O6 Dy1 N1 67.64(13)
O1 Dy1 N1 72.58(13)
O20 Dy1 N1 25.50(14)
O19 Dy1 N1 25.65(14)
P1 O1 Dy1 137.8(2)
O1 P1 O8 109.1(2)
O1 P1 O7 108.3(2)
O8 P1 O7 101.6(2)
O1 P1 Co1 119.47(16)
O8 P1 Co1 106.90(16)
O7 P1 Co1 110.07(18)
C6 O7 P1 123.0(4)
C7 O8 P1 118.9(4)
P2 O2 Dy1 138.0(2)
O2 P2 O9 110.2(2)
O2 P2 O10 107.7(2)
O9 P2 O10 99.2(2)
O2 P2 Co1 119.53(16)
O9 P2 Co1 106.33(16)
O10 P2 Co1 111.93(18)
C8 O9 P2 120.4(4)
C9 O10 P2 119.4(4)
P3 O3 Dy1 135.8(2)
O3 P3 O12 108.2(2)
O3 P3 O11 108.3(2)
O12 P3 O11 103.3(3)
O3 P3 Co1 121.22(17)
O12 P3 Co1 106.20(17)
O11 P3 Co1 108.16(16)
C10 O11 P3 121.4(4)
C11 O12 P3 123.5(4)
C1 Co1 C3 65.1(3)
C1 Co1 C5 39.5(2)
C3 Co1 C5 65.5(2)
C1 Co1 C2 39.0(3)
C3 Co1 C2 39.1(2)
C5 Co1 C2 66.2(3)
C1 Co1 C4 65.7(3)
C3 Co1 C4 39.1(2)
C5 Co1 C4 39.2(2)
C2 Co1 C4 66.1(3)
C1 Co1 P1 125.5(2)
C3 Co1 P1 99.18(18)
C5 Co1 P1 161.28(19)
C2 Co1 P1 95.1(2)
C4 Co1 P1 132.9(2)
C1 Co1 P2 145.0(2)
C3 Co1 P2 108.81(19)
C5 Co1 P2 105.6(2)
C2 Co1 P2 148.0(2)
C4 Co1 P2 87.85(19)
P1 Co1 P2 89.13(6)
C1 Co1 P3 90.6(2)
C3 Co1 P3 154.54(19)
C5 Co1 P3 100.95(19)
C2 Co1 P3 116.4(2)
C4 Co1 P3 138.3(2)
P1 Co1 P3 88.78(6)
P2 Co1 P3 95.38(6)
C2 C1 C5 109.5(6)
C2 C1 Co1 71.5(4)
C5 C1 Co1 70.7(4)
C1 C2 C3 106.2(6)
C1 C2 Co1 69.5(4)
C3 C2 Co1 69.8(4)
C4 C3 C2 109.8(6)
C4 C3 Co1 71.1(3)
C2 C3 Co1 71.0(4)
C3 C4 C5 107.1(6)
C3 C4 Co1 69.8(3)
C5 C4 Co1 69.8(3)
C4 C5 C1 107.4(6)
C4 C5 Co1 70.9(4)
C1 C5 Co1 69.8(3)
P4 O4 Dy1 136.6(2)
O4 P4 O13 107.7(2)
O4 P4 O14 108.3(2)
O13 P4 O14 102.7(3)
O4 P4 Co2 121.65(17)
O13 P4 Co2 107.7(2)
O14 P4 Co2 107.20(17)
C17 O13 P4 123.8(5)
C18 O14 P4 120.4(4)
P5 O5 Dy1 138.4(2)
O5 P5 O16 109.4(2)
O5 P5 O15 108.0(2)
O16 P5 O15 98.1(2)
O5 P5 Co2 119.59(17)
O16 P5 Co2 107.37(17)
O15 P5 Co2 112.27(18)
C19 O15 P5 120.0(4)
C20 O16 P5 119.7(4)
P6 O6 Dy1 138.4(2)
O6 P6 O18 108.7(2)
O6 P6 O17 108.6(2)
O18 P6 O17 102.1(3)
O6 P6 Co2 119.23(18)
O18 P6 Co2 108.66(18)
O17 P6 Co2 108.22(17)
C21 O17 P6 120.6(4)
C22 O18 P6 126.5(4)
C14 Co2 C15 39.1(3)
C14 Co2 C16 65.7(3)
C15 Co2 C16 39.7(3)
C14 Co2 C12 65.3(3)
C15 Co2 C12 66.2(3)
C16 Co2 C12 39.6(2)
C14 Co2 C13 38.3(3)
C15 Co2 C13 65.2(3)
C16 Co2 C13 65.5(3)
C12 Co2 C13 38.8(3)
C14 Co2 P6 127.8(3)
C15 Co2 P6 161.7(2)
C16 Co2 P6 130.6(2)
C12 Co2 P6 97.46(19)
C13 Co2 P6 97.0(2)
C14 Co2 P5 142.4(3)
C15 Co2 P5 103.9(2)
C16 Co2 P5 88.44(19)
C12 Co2 P5 111.9(2)
C13 Co2 P5 150.5(2)
P6 Co2 P5 89.66(6)
C14 Co2 P4 89.8(2)
C15 Co2 P4 101.9(2)
C16 Co2 P4 140.3(2)
C12 Co2 P4 152.7(2)
C13 Co2 P4 114.3(2)
P6 Co2 P4 89.12(6)
P5 Co2 P4 94.46(6)
C13 C12 C16 107.3(6)
C13 C12 Co2 70.9(4)
C16 C12 Co2 69.8(4)
C14 C13 C12 108.7(7)
C14 C13 Co2 69.7(4)
C12 C13 Co2 70.3(4)
C13 C14 C15 109.2(7)
C13 C14 Co2 72.0(4)
C15 C14 Co2 70.5(4)
C14 C15 C16 107.5(7)
C14 C15 Co2 70.4(4)
C16 C15 Co2 70.6(4)
C15 C16 C12 107.2(6)
C15 C16 Co2 69.8(4)
C12 C16 Co2 70.5(3)
N1 O19 Dy1 94.2(3)
N1 O20 Dy1 95.0(3)
O21 N1 O20 119.8(6)
O21 N1 O19 120.8(6)
O20 N1 O19 119.4(5)
O21 N1 Dy1 174.5(4)
O20 N1 Dy1 59.5(3)
O19 N1 Dy1 60.2(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Dy1 O3 2.289(4)
Dy1 O4 2.289(4)
Dy1 O2 2.325(4)
Dy1 O5 2.327(4)
Dy1 O6 2.331(3)
Dy1 O1 2.340(4)
Dy1 O20 2.493(4)
Dy1 O19 2.508(4)
Dy1 N1 2.883(6)
O1 P1 1.495(4)
P1 O8 1.593(4)
P1 O7 1.597(4)
P1 Co1 2.1592(17)
O7 C6 1.408(7)
O8 C7 1.435(7)
O2 P2 1.483(4)
P2 O9 1.595(4)
P2 O10 1.602(4)
P2 Co1 2.1658(17)
O9 C8 1.428(7)
O10 C9 1.425(7)
O3 P3 1.499(4)
P3 O12 1.590(4)
P3 O11 1.591(4)
P3 Co1 2.1724(16)
O11 C10 1.423(7)
O12 C11 1.438(7)
Co1 C1 2.065(6)
Co1 C3 2.074(5)
Co1 C5 2.076(6)
Co1 C2 2.090(7)
Co1 C4 2.090(6)
C1 C2 1.387(9)
C1 C5 1.399(9)
C2 C3 1.395(9)
C3 C4 1.393(8)
C4 C5 1.399(9)
O4 P4 1.500(4)
P4 O13 1.581(5)
P4 O14 1.588(4)
P4 Co2 2.1731(17)
O13 C17 1.404(8)
O14 C18 1.434(8)
O5 P5 1.491(4)
P5 O16 1.585(4)
P5 O15 1.605(4)
P5 Co2 2.1637(17)
O15 C19 1.428(8)
O16 C20 1.423(7)
O6 P6 1.492(4)
P6 O18 1.579(4)
P6 O17 1.590(4)
P6 Co2 2.1605(17)
O17 C21 1.416(7)
O18 C22 1.381(8)
Co2 C14 2.065(6)
Co2 C15 2.067(6)
Co2 C16 2.077(6)
Co2 C12 2.086(6)
Co2 C13 2.094(6)
C12 C13 1.389(9)
C12 C16 1.411(9)
C13 C14 1.366(10)
C14 C15 1.381(10)
C15 C16 1.405(9)
O19 N1 1.251(6)
O20 N1 1.246(6)
N1 O21 1.237(6)
