#------------------------------------------------------------------------------
#$Date: 2019-11-23 08:35:45 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232572 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/78/4347893.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347893
loop_
_publ_author_name
'Li, Lei-Lei'
'Cao, Gao-Juan'
'Zhao, Jun-Wei'
'He, Huan'
'Yang, Bai-Feng'
'Yang, Guo-Yu'
_publ_section_title
;
 Lanthanide Germanate Cluster Organic Frameworks Based on {Ln8Ge12}
 Clusters: From One-Dimensional Chains to Two-Dimensional Layers and
 Three-Dimensional Frameworks.
;
_journal_issue                   11
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5671
_journal_page_last               5683
_journal_paper_doi               10.1021/acs.inorgchem.6b00754
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C72 H148 Ge24 Nd16 O126, 16(O)'
_chemical_formula_sum            'C72 H188 Ge24 Nd16 O142'
_chemical_formula_weight         7376.22
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2016-05-04
_audit_creation_method
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_cell_angle_alpha                107.175(5)
_cell_angle_beta                 91.052(3)
_cell_angle_gamma                97.001(6)
_cell_formula_units_Z            1
_cell_length_a                   15.1938(14)
_cell_length_b                   16.548(2)
_cell_length_c                   19.731(2)
_cell_measurement_reflns_used    6873
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      3.0148
_cell_volume                     4696.6(9)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean none
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0947
_diffrn_reflns_av_unetI/netI     0.1784
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            36809
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.04
_diffrn_source                   'fine-focus sealed tube'
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    8.216
_exptl_absorpt_correction_T_max  0.3531
_exptl_absorpt_correction_T_min  0.2069
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            PINK
_exptl_crystal_density_diffrn    2.608
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             3484
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.16
_platon_squeeze_details
;

;
_refine_diff_density_max         3.010
_refine_diff_density_min         -4.587
_refine_diff_density_rms         0.426
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1146
_refine_ls_number_reflns         21289
_refine_ls_number_restraints     3860
_refine_ls_restrained_S_all      0.990
_refine_ls_R_factor_all          0.1858
_refine_ls_R_factor_gt           0.1167
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1300P)²+209.2635P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2623
_refine_ls_wR_factor_ref         0.3361
_reflns_number_gt                12114
_reflns_number_total             21289
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic6b00754_si_007.cif
_cod_data_source_block           6
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4347893
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H,H) groups, All O(H,H) groups
2. Restrained distances
 C1-C2 = C2-C3 = C5-C6 = C8-C9 = C11-C12 = C13-C14 = C14-C15
 1.53 with sigma of 0.01
 C17-C18 = C19-C20 = C20-C21 = C22-C23 = C23-C24 = C35-C36
 1.53 with sigma of 0.01
 C25-C26 = C26-C27 = C31-C32 = C32-C33 = C29-C30 = C34-C35
 1.53 with sigma of 0.01
 O15W-O38
 3 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 3.8A with sigma of 0.02 and sigma
for terminal atoms of 0.04
4.a Riding coordinates:
 O1W(H1A,H1B), O2W(H2A,H2B), O3W(H3A,H3B), O4W(H4A,H4B), O6W(H6A,H6B), O7W(H7A,
 H7B), O8W(H8A,H8B), O9W(H9A,H9B), O10W(H10A,H10B), O11W(H11A,H11B), O12W(H12A,
 H12B), O13W(H13A,H13B), O14W(H14A,H14B)
4.b Secondary CH2 refined with riding coordinates:
 C1(H1C,H1D), C2(H2C,H2D), C4(H4C,H4D), C5(H5C,H5D), C7(H7C,H7D), C8(H8C,H8D),
 C10(H10C,H10D), C11(H11C,H11D), C13(H13C,H13D), C14(H14C,H14D), C16(H16A,H16B),
  C17(H17A,H17B), C19(H19A,H19B), C20(H20A,H20B), C22(H22A,H22B), C23(H23A,
 H23B), C25(H25A,H25B), C26(H26A,H26B), C28(H28A,H28B), C29(H29A,H29B),
 C31(H31A,H31B), C32(H32A,H32B), C34(H34A,H34B), C35(H35A,H35B)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
Nd1 Nd 0.20005(8) -0.15397(8) -0.09911(7) 0.0283(3) Uani 1 d . . . U
Nd2 Nd 0.18943(8) 0.17479(8) 0.11235(7) 0.0283(3) Uani 1 d . . . U
Nd3 Nd -0.10745(8) -0.18468(8) 0.07426(7) 0.0292(3) Uani 1 d . . . U
Nd4 Nd 0.08355(8) -0.00776(8) 0.18521(7) 0.0270(3) Uani 1 d . . . U
Nd5 Nd 0.59892(9) 0.65683(9) 0.36013(8) 0.0339(3) Uani 1 d . . . U
Nd6 Nd 0.72701(8) 0.43501(8) 0.51661(7) 0.0264(3) Uani 1 d . . . U
Nd7 Nd 0.32226(8) 0.36008(8) 0.33743(7) 0.0262(3) Uani 1 d . . . U
Nd8 Nd 0.55744(8) 0.29649(8) 0.35956(7) 0.0266(3) Uani 1 d . . . U
Ge1 Ge 0.26617(16) -0.03997(16) 0.07669(13) 0.0276(5) Uani 1 d . . . U
Ge2 Ge 0.12056(16) -0.21162(16) 0.05071(14) 0.0280(5) Uani 1 d . . . U
Ge3 Ge -0.00308(16) -0.28267(16) -0.09618(14) 0.0297(5) Uani 1 d . . . U
Ge4 Ge 0.01600(16) -0.18050(16) -0.21328(13) 0.0280(5) Uani 1 d . . . U
Ge5 Ge 0.16011(16) -0.00894(16) -0.19015(13) 0.0292(5) Uani 1 d . . . U
Ge6 Ge 0.28592(16) 0.06081(16) -0.04380(13) 0.0279(5) Uani 1 d . . . U
Ge7 Ge 0.37118(16) 0.58751(17) 0.32995(14) 0.0304(5) Uani 1 d . . . U
Ge8 Ge 0.43827(16) 0.74608(16) 0.47433(14) 0.0285(5) Uani 1 d . . . U
Ge9 Ge 0.63385(16) 0.77277(16) 0.54963(14) 0.0275(5) Uani 1 d . . . U
Ge10 Ge 0.76941(15) 0.63420(15) 0.48435(13) 0.0264(5) Uani 1 d . . . U
Ge11 Ge 0.70366(16) 0.47748(16) 0.34364(13) 0.0287(5) Uani 1 d . . . U
Ge12 Ge 0.50669(16) 0.44814(17) 0.26032(13) 0.0298(5) Uani 1 d . . . U
O1 O 0.2185(10) -0.1479(11) 0.0327(9) 0.033(3) Uani 1 d . . . U
O2 O 0.0993(11) -0.2618(11) -0.0429(10) 0.036(3) Uani 1 d . . . U
O3 O 0.0566(11) -0.2413(11) -0.1600(9) 0.034(3) Uani 1 d . . . U
O4 O 0.1246(10) -0.1211(11) -0.2009(9) 0.032(3) Uani 1 d . . . U
O5 O 0.2438(11) -0.0152(11) -0.1288(9) 0.033(3) Uani 1 d . . . U
O6 O 0.2923(10) -0.0270(10) -0.0092(8) 0.029(2) Uani 1 d . . . U
O7 O 0.1893(10) 0.0290(10) 0.1084(9) 0.031(2) Uani 1 d . . . U
O8 O 0.0481(11) -0.1389(11) 0.0875(9) 0.035(3) Uani 1 d . . . U
O9 O -0.0772(11) -0.2177(11) -0.0491(9) 0.033(3) Uani 1 d . . . U
O10 O -0.0572(10) -0.1179(11) -0.1591(9) 0.031(3) Uani 1 d . . . U
O11 O 0.0735(10) 0.0438(10) -0.1532(9) 0.030(3) Uani 1 d . . . U
O12 O 0.2002(11) 0.1181(11) -0.0130(9) 0.034(3) Uani 1 d . . . U
O13 O 0.2153(12) -0.0852(12) 0.1805(10) 0.043(3) Uani 1 d . . . U
O14 O 0.2829(13) -0.1174(14) 0.2675(13) 0.057(5) Uani 1 d . . . U
O15 O -0.0260(12) -0.3125(12) 0.0494(10) 0.042(3) Uani 1 d . . . U
O16 O -0.0524(18) -0.4049(18) 0.1075(17) 0.088(7) Uani 1 d . . . U
O17 O -0.1280(11) -0.2938(11) -0.1926(9) 0.039(3) Uani 1 d . . . U
O18 O -0.1786(11) -0.3932(11) -0.2920(10) 0.039(3) Uani 1 d . . . U
O19 O -0.0109(11) -0.0758(12) -0.2862(10) 0.041(3) Uani 1 d . . . U
O20 O 0.0176(13) -0.0796(14) -0.3942(11) 0.052(5) Uani 1 d . . . U
O21 O 0.2354(11) 0.1408(11) -0.1514(10) 0.039(3) Uani 1 d . . . U
O22 O 0.3333(13) 0.2173(12) -0.1985(11) 0.048(4) Uani 1 d . . . U
O23 O 0.3526(11) 0.1392(12) 0.0847(10) 0.040(3) Uani 1 d . . . U
O24 O 0.4929(13) 0.1801(14) 0.1239(11) 0.054(4) Uani 1 d . . . U
O25 O 0.4403(11) 0.6844(11) 0.3825(10) 0.037(3) Uani 1 d . . . U
O26 O 0.5576(11) 0.7611(11) 0.4771(9) 0.035(3) Uani 1 d . . . U
O27 O 0.7151(11) 0.7245(11) 0.4929(9) 0.035(3) Uani 1 d . . . U
O28 O 0.7282(11) 0.5883(11) 0.3934(9) 0.034(3) Uani 1 d . . . U
O29 O 0.6164(10) 0.5009(11) 0.2944(9) 0.034(3) Uani 1 d . . . U
O30 O 0.4673(11) 0.5527(11) 0.2828(10) 0.037(3) Uani 1 d . . . U
O31 O 0.3432(11) 0.5123(11) 0.3748(9) 0.034(3) Uani 1 d . . . U
O32 O 0.4002(11) 0.6692(11) 0.5155(9) 0.036(3) Uani 1 d . . . U
O33 O 0.5914(10) 0.7105(10) 0.5991(9) 0.031(3) Uani 1 d . . . U
O34 O 0.7206(10) 0.5827(10) 0.5428(9) 0.031(3) Uani 1 d . . . U
O35 O 0.6584(10) 0.4238(10) 0.4011(9) 0.031(2) Uani 1 d . . . U
O36 O 0.4714(11) 0.3868(11) 0.3152(9) 0.034(2) Uani 1 d . . . U
O37 O 0.2632(12) 0.6567(12) 0.4030(11) 0.042(3) Uani 1 d . . . U
O38 O 0.1382(15) 0.7115(15) 0.3833(12) 0.076(6) Uani 1 d . . D U
O39 O 0.4696(11) 0.8294(11) 0.5949(10) 0.038(3) Uani 1 d . . . U
O40 O 0.4602(15) 0.9581(12) 0.6645(12) 0.058(5) Uani 1 d . . . U
O41 O 0.7769(11) 0.7700(12) 0.6493(10) 0.040(3) Uani 1 d . . . U
O42 O 0.7999(12) 0.8934(12) 0.7350(10) 0.044(4) Uani 1 d . . . U
O43 O 0.8343(10) 0.4958(11) 0.4482(9) 0.034(3) Uani 1 d . . . U
O44 O 0.9634(12) 0.4552(13) 0.4233(11) 0.051(4) Uani 1 d . . . U
O45 O 0.6412(11) 0.3162(11) 0.2574(9) 0.036(3) Uani 1 d . . . U
O46 O 0.7377(11) 0.2275(11) 0.2072(10) 0.038(3) Uani 1 d . . . U
O47 O 0.3419(11) 0.3878(11) 0.2143(10) 0.038(3) Uani 1 d . . . U
O48 O 0.2844(11) 0.3106(11) 0.1109(9) 0.037(3) Uani 1 d . . . U
O1W O 0.3339(11) -0.2190(11) -0.0770(8) 0.032(4) Uani 1 d . . . U
H1A H 0.3841 -0.2064 -0.0923 0.038 Uiso 1 d . . R .
H1B H 0.3413 -0.2479 -0.0486 0.038 Uiso 1 d . . R .
O2W O 0.0806(10) -0.0703(10) -0.0406(9) 0.033(3) Uani 1 d . . . U
H2A H 0.0306 -0.0690 -0.0600 0.039 Uiso 1 d . . R .
H2B H 0.0851 -0.0345 0.0007 0.039 Uiso 1 d . . R .
O3W O -0.0805(16) -0.2156(15) 0.1906(12) 0.066(5) Uani 1 d . . . U
H3A H -0.1023 -0.2641 0.1937 0.079 Uiso 1 d . . R .
H3B H -0.0470 -0.1894 0.2275 0.079 Uiso 1 d . . R .
O4W O -0.2321(14) -0.3114(14) 0.0243(13) 0.063(5) Uani 1 d . . . U
H4A H -0.2526 -0.3264 -0.0186 0.075 Uiso 1 d . . R .
H4B H -0.2378 -0.3548 0.0394 0.075 Uiso 1 d . . R .
O6W O 0.3110(12) 0.2187(12) 0.2230(10) 0.044(3) Uani 1 d . . . U
H6A H 0.3614 0.2204 0.2050 0.053 Uiso 1 d . . R .
H6B H 0.3067 0.1767 0.2397 0.053 Uiso 1 d . . R .
O7W O 0.5524(14) 0.7568(13) 0.2972(13) 0.059(4) Uani 1 d . . . U
H7A H 0.5884 0.7656 0.2668 0.070 Uiso 1 d . . R .
H7B H 0.5204 0.7970 0.3077 0.070 Uiso 1 d . . R .
O8W O 0.6761(16) 0.6377(16) 0.2440(12) 0.068(5) Uani 1 d . . . U
H8A H 0.6695 0.6839 0.2352 0.081 Uiso 1 d . . R .
H8B H 0.7051 0.6086 0.2112 0.081 Uiso 1 d . . R .
O9W O 0.7272(17) 0.7807(16) 0.3744(13) 0.074(5) Uani 1 d . . . U
H9A H 0.7576 0.8296 0.3908 0.089 Uiso 1 d . . R .
H9B H 0.7204 0.7587 0.4082 0.089 Uiso 1 d . . R .
O10W O 0.5409(11) 0.5672(11) 0.4410(9) 0.034(3) Uani 1 d . . . U
H10A H 0.5596 0.5216 0.4432 0.041 Uiso 1 d . . R .
H10B H 0.5001 0.5778 0.4700 0.041 Uiso 1 d . . R .
O11W O 0.8649(10) 0.4890(11) 0.5953(10) 0.040(4) Uani 1 d . . . U
H11A H 0.9183 0.5053 0.5882 0.048 Uiso 1 d . . R .
H11B H 0.8490 0.5259 0.6313 0.048 Uiso 1 d . . R .
O12W O 0.8335(12) 0.3271(12) 0.4584(11) 0.050(4) Uani 1 d . . . U
H12A H 0.7945 0.3033 0.4248 0.059 Uiso 1 d . . R .
H12B H 0.8497 0.2887 0.4747 0.059 Uiso 1 d . . R .
O13W O 0.6987(12) 0.2162(12) 0.3457(10) 0.045(4) Uani 1 d . . . U
H13A H 0.7119 0.2209 0.3052 0.054 Uiso 1 d . . R .
H13B H 0.7378 0.2480 0.3766 0.054 Uiso 1 d . . R .
O14W O 0.5031(13) 0.1673(13) 0.2614(10) 0.053(5) Uani 1 d . . . U
H14A H 0.5032 0.1580 0.2167 0.064 Uiso 1 d . . R .
H14B H 0.5150 0.1230 0.2712 0.064 Uiso 1 d . . R .
O15W O 0.1536(19) 0.8187(18) 0.5352(13) 0.096(5) Uani 1 d A 1 D U
O16W O 0.112(2) 0.882(2) 0.485(2) 0.126(9) Uani 1 d B 2 . U
O17W O 0.4524(15) 0.8800(15) 0.3280(13) 0.063(5) Uani 1 d . . . U
O18W O 0.796(2) 0.934(2) 0.4422(18) 0.106(6) Uani 1 d . . . U
O19W O 0.977(2) 0.651(2) 0.273(2) 0.126(8) Uani 1 d . . . U
O20W O 0.369(4) 0.683(5) 0.024(4) 0.27(4) Uani 1 d . . . U
O21W O 0.780(3) 0.564(3) 0.129(3) 0.191(16) Uani 1 d . . . U
O22W O 0.880(3) 0.793(3) 0.354(2) 0.139(8) Uani 1 d . . . U
O23W O -0.0925(16) -0.4133(15) -0.2787(13) 0.071(4) Uani 1 d . . . U
C1 C 0.3772(15) -0.0287(15) 0.1312(12) 0.033(3) Uani 1 d . . D U
H1C H 0.4230 -0.0477 0.0988 0.040 Uiso 1 calc . . R .
H1D H 0.3951 0.0310 0.1569 0.040 Uiso 1 calc . . R .
C2 C 0.3695(15) -0.0803(19) 0.1837(15) 0.054(5) Uani 1 d . . D U
H2C H 0.4128 -0.0530 0.2231 0.064 Uiso 1 calc . . R .
H2D H 0.3852 -0.1365 0.1604 0.064 Uiso 1 calc . . R .
C3 C 0.2784(14) -0.0909(17) 0.2137(14) 0.037(3) Uani 1 d . . D U
C4 C 0.1499(17) -0.2870(17) 0.1034(15) 0.039(3) Uani 1 d . . . U
H4C H 0.2124 -0.2935 0.0993 0.047 Uiso 1 calc . . R .
H4D H 0.1406 -0.2612 0.1532 0.047 Uiso 1 calc . . R .
C5 C 0.0960(14) -0.3736(19) 0.0784(17) 0.048(4) Uani 1 d . . D U
H5C H 0.1062 -0.4049 0.1116 0.058 Uiso 1 calc . . R .
H5D H 0.1151 -0.4049 0.0325 0.058 Uiso 1 calc . . R .
C6 C -0.0032(14) -0.3675(18) 0.0718(16) 0.045(4) Uani 1 d . . D U
C7 C -0.0445(18) -0.4026(17) -0.1404(14) 0.040(3) Uani 1 d . . . U
H7C H 0.0021 -0.4352 -0.1339 0.048 Uiso 1 calc . . R .
H7D H -0.0951 -0.4187 -0.1157 0.048 Uiso 1 calc . . R .
C8 C -0.0703(16) -0.4267(15) -0.2161(13) 0.036(4) Uani 1 d . . D U
H8C H -0.0994 -0.4851 -0.2312 0.043 Uiso 1 calc . . R .
H8D H -0.0172 -0.4244 -0.2425 0.043 Uiso 1 calc . . R .
C9 C -0.1328(15) -0.3687(15) -0.2342(13) 0.034(3) Uani 1 d . . D U
C10 C -0.0034(17) -0.2527(17) -0.3109(13) 0.039(3) Uani 1 d . . . U
H10C H 0.0237 -0.3043 -0.3169 0.046 Uiso 1 calc . . R .
H10D H -0.0666 -0.2687 -0.3231 0.046 Uiso 1 calc . . R .
C11 C 0.0382(16) -0.2029(13) -0.3593(14) 0.038(4) Uani 1 d . . D U
H11C H 0.1023 -0.1984 -0.3532 0.046 Uiso 1 calc . . R .
H11D H 0.0213 -0.2358 -0.4082 0.046 Uiso 1 calc . . R .
C12 C 0.0133(16) -0.1132(14) -0.3471(15) 0.038(4) Uani 1 d . . D U
C13 C 0.2129(14) 0.0046(16) -0.2748(14) 0.039(3) Uani 1 d . . D U
H13C H 0.2277 -0.0503 -0.3031 0.046 Uiso 1 calc . . R .
H13D H 0.1693 0.0216 -0.3025 0.046 Uiso 1 calc . . R .
C14 C 0.2966(14) 0.0700(13) -0.2609(12) 0.038(4) Uani 1 d . . D U
H14C H 0.3470 0.0441 -0.2502 0.046 Uiso 1 calc . . R .
H14D H 0.3081 0.0867 -0.3034 0.046 Uiso 1 calc . . R .
C15 C 0.2869(15) 0.1491(13) -0.1991(11) 0.031(3) Uani 1 d . . D U
C16 C 0.4004(16) 0.1124(17) -0.0595(14) 0.038(3) Uani 1 d . . . U
H16A H 0.4219 0.0778 -0.1031 0.046 Uiso 1 calc . . R .
H16B H 0.3960 0.1685 -0.0642 0.046 Uiso 1 calc . . R .
C17 C 0.4667(18) 0.1205(19) 0.0046(12) 0.049(4) Uani 1 d . . D U
H17A H 0.4853 0.0650 -0.0004 0.059 Uiso 1 calc . . R .
H17B H 0.5192 0.1592 0.0024 0.059 Uiso 1 calc . . R .
C18 C 0.4288(16) 0.1525(17) 0.0777(12) 0.037(3) Uani 1 d . . D U
C19 C 0.2896(18) 0.6031(17) 0.2618(16) 0.046(4) Uani 1 d . . D U
H19A H 0.3226 0.6178 0.2244 0.056 Uiso 1 calc . . R .
H19B H 0.2515 0.5497 0.2403 0.056 Uiso 1 calc . . R .
C20 C 0.232(2) 0.6727(18) 0.2940(14) 0.056(5) Uani 1 d . . D U
H20A H 0.2622 0.7267 0.2912 0.068 Uiso 1 calc . . R .
H20B H 0.1767 0.6604 0.2653 0.068 Uiso 1 calc . . R .
C21 C 0.211(2) 0.6826(19) 0.3710(14) 0.050(4) Uani 1 d . . D U
C22 C 0.3827(19) 0.8469(16) 0.4806(14) 0.048(3) Uani 1 d . . D U
H22A H 0.3925 0.8630 0.4376 0.058 Uiso 1 calc . . R .
H22B H 0.3192 0.8333 0.4832 0.058 Uiso 1 calc . . R .
C23 C 0.4175(19) 0.9228(15) 0.5446(12) 0.049(4) Uani 1 d . . D U
H23A H 0.3693 0.9561 0.5602 0.059 Uiso 1 calc . . R .
H23B H 0.4632 0.9587 0.5293 0.059 Uiso 1 calc . . R .
C24 C 0.4557(18) 0.9015(17) 0.6084(13) 0.043(4) Uani 1 d . . D U
C25 C 0.6823(13) 0.8911(17) 0.5943(15) 0.043(3) Uani 1 d . . D U
H25A H 0.6735 0.9239 0.5619 0.052 Uiso 1 calc . . R .
H25B H 0.6508 0.9141 0.6366 0.052 Uiso 1 calc . . R .
C26 C 0.7816(14) 0.9000(17) 0.6147(14) 0.045(4) Uani 1 d . . D U
H26A H 0.8140 0.8759 0.5732 0.054 Uiso 1 calc . . R .
H26B H 0.8055 0.9596 0.6353 0.054 Uiso 1 calc . . R .
C27 C 0.7894(17) 0.8514(16) 0.6689(13) 0.038(4) Uani 1 d . . D U
C28 C 0.8991(16) 0.6683(17) 0.4927(15) 0.041(4) Uani 1 d . . . U
H28A H 0.9120 0.7233 0.4842 0.049 Uiso 1 calc . . R .
H28B H 0.9212 0.6746 0.5406 0.049 Uiso 1 calc . . R .
C29 C 0.9476(18) 0.6034(13) 0.4401(16) 0.045(4) Uani 1 d . . D U
H29A H 1.0107 0.6146 0.4535 0.054 Uiso 1 calc . . R .
H29B H 0.9397 0.6091 0.3929 0.054 Uiso 1 calc . . R .
C30 C 0.9119(15) 0.5125(13) 0.4390(14) 0.033(3) Uani 1 d . . D U
C31 C 0.8001(15) 0.4409(15) 0.2829(11) 0.033(3) Uani 1 d . . D U
H31A H 0.8336 0.4904 0.2744 0.040 Uiso 1 calc . . R .
H31B H 0.8399 0.4158 0.3074 0.040 Uiso 1 calc . . R .
C32 C 0.7670(15) 0.3758(13) 0.2113(11) 0.036(4) Uani 1 d . . D U
H32A H 0.7330 0.4027 0.1840 0.044 Uiso 1 calc . . R .
H32B H 0.8174 0.3567 0.1846 0.044 Uiso 1 calc . . R .
C33 C 0.7088(15) 0.2990(14) 0.2222(13) 0.034(3) Uani 1 d . . D U
C34 C 0.5091(14) 0.4026(18) 0.1607(13) 0.040(4) Uani 1 d . . D U
H34A H 0.5544 0.4384 0.1448 0.049 Uiso 1 calc . . R .
H34B H 0.5283 0.3467 0.1508 0.049 Uiso 1 calc . . R .
C35 C 0.4239(12) 0.3929(18) 0.1147(12) 0.039(4) Uani 1 d . . D U
H35A H 0.4162 0.4474 0.1081 0.047 Uiso 1 calc . . R .
H35B H 0.4286 0.3525 0.0684 0.047 Uiso 1 calc . . R .
C36 C 0.3435(14) 0.3615(16) 0.1501(13) 0.034(3) Uani 1 d . . D U
O5W O 0.0663(18) -0.0943(16) 0.2735(14) 0.081(6) Uani 1 d . . . U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nd Nd -0.1943 3.0179 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge4 Nd1 Ge1 137.08(7) . .
Ge4 Nd1 Ge6 108.30(7) . .
Ge6 Nd1 Ge1 56.29(6) . .
O1 Nd1 Ge1 29.9(4) . .
O1 Nd1 Ge4 133.0(4) . .
O1 Nd1 Ge6 86.2(4) . .
O1 Nd1 O2 57.4(5) . .
O2 Nd1 Ge1 85.1(4) . .
O2 Nd1 Ge4 85.0(4) . .
O2 Nd1 Ge6 136.1(4) . .
O3 Nd1 Ge1 133.8(4) . .
O3 Nd1 Ge4 30.2(4) . .
O3 Nd1 Ge6 136.0(4) . .
O3 Nd1 O1 113.0(5) . .
O3 Nd1 O2 57.4(5) . .
O3 Nd1 O5 115.6(5) . .
O3 Nd1 O6 154.3(5) . .
O4 Nd1 Ge1 135.1(4) . .
O4 Nd1 Ge4 29.9(4) . .
O4 Nd1 Ge6 85.7(4) . .
O4 Nd1 O1 152.8(5) . .
O4 Nd1 O2 114.8(5) . .
O4 Nd1 O3 58.9(5) . .
O4 Nd1 O5 58.0(5) . .
O4 Nd1 O6 115.6(5) . .
O5 Nd1 Ge1 86.9(4) . .
O5 Nd1 Ge4 85.3(4) . .
O5 Nd1 Ge6 30.6(4) . .
O5 Nd1 O1 116.8(5) . .
O5 Nd1 O2 155.6(5) . .
O5 Nd1 O6 59.4(5) . .
O6 Nd1 Ge1 30.3(3) . .
O6 Nd1 Ge4 135.2(4) . .
O6 Nd1 Ge6 29.9(4) . .
O6 Nd1 O1 59.1(5) . .
O6 Nd1 O2 115.4(5) . .
O46 Nd1 Ge1 140.0(4) 2_655 .
O46 Nd1 Ge4 81.9(4) 2_655 .
O46 Nd1 Ge6 110.9(4) 2_655 .
O46 Nd1 O1 135.5(6) 2_655 .
O46 Nd1 O2 112.4(6) 2_655 .
O46 Nd1 O3 83.4(6) 2_655 .
O46 Nd1 O4 71.5(6) 2_655 .
O46 Nd1 O5 88.2(6) 2_655 .
O46 Nd1 O6 120.0(5) 2_655 .
O46 Nd1 O1W 67.7(5) 2_655 .
O46 Nd1 O2W 148.0(6) 2_655 .
O1W Nd1 Ge1 77.3(4) . .
O1W Nd1 Ge4 144.0(4) . .
O1W Nd1 Ge6 100.4(4) . .
O1W Nd1 O1 69.0(5) . .
O1W Nd1 O2 89.3(5) . .
O1W Nd1 O3 123.2(5) . .
O1W Nd1 O4 138.2(5) . .
O1W Nd1 O5 111.4(5) . .
O1W Nd1 O6 78.8(5) . .
O1W Nd1 O2W 144.4(5) . .
O2W Nd1 Ge1 69.4(4) . .
O2W Nd1 Ge4 67.7(4) . .
O2W Nd1 Ge6 71.7(4) . .
O2W Nd1 O1 75.8(5) . .
O2W Nd1 O2 75.7(5) . .
O2W Nd1 O3 75.3(5) . .
O2W Nd1 O4 77.0(5) . .
O2W Nd1 O5 79.9(5) . .
O2W Nd1 O6 78.9(5) . .
Nd4 Nd2 Nd3 119.94(4) . 2
O7 Nd2 Nd3 109.3(4) . 2
O7 Nd2 Nd4 34.9(4) . .
O7 Nd2 O10 67.2(5) . 2
O7 Nd2 O17 133.1(6) . 2
O7 Nd2 O23 73.6(5) . .
O7 Nd2 O48 145.3(5) . .
O7 Nd2 O6W 88.3(6) . .
O9 Nd2 Nd3 35.1(4) 2 2
O9 Nd2 Nd4 109.3(4) 2 .
O9 Nd2 O7 121.5(6) 2 .
O9 Nd2 O10 79.8(5) 2 2
O9 Nd2 O12 69.2(5) 2 .
O9 Nd2 O17 70.7(6) 2 2
O9 Nd2 O23 133.6(5) 2 .
O9 Nd2 O48 86.4(6) 2 .
O9 Nd2 O6W 147.6(6) 2 .
O10 Nd2 Nd3 104.2(4) 2 2
O10 Nd2 Nd4 34.8(4) 2 .
O10 Nd2 O17 71.9(6) 2 2
O10 Nd2 O23 138.9(6) 2 .
O10 Nd2 O48 144.2(5) 2 .
O10 Nd2 O6W 103.5(6) 2 .
O12 Nd2 Nd3 35.2(4) . 2
O12 Nd2 Nd4 108.7(4) . .
O12 Nd2 O7 82.8(6) . .
O12 Nd2 O10 115.2(6) . 2
O12 Nd2 O17 136.8(6) . 2
O12 Nd2 O23 70.2(5) . .
O12 Nd2 O48 89.8(6) . .
O12 Nd2 O6W 132.6(5) . .
O17 Nd2 Nd3 102.1(4) 2 2
O17 Nd2 Nd4 99.0(4) 2 .
O17 Nd2 O23 134.2(6) 2 .
O17 Nd2 O48 72.4(6) 2 .
O17 Nd2 O6W 79.7(6) 2 .
O23 Nd2 Nd3 99.8(4) . 2
O23 Nd2 Nd4 104.1(4) . .
O23 Nd2 O6W 62.6(5) . .
O48 Nd2 Nd3 81.1(4) . 2
O48 Nd2 Nd4 158.8(4) . .
O48 Nd2 O23 72.0(6) . .
O48 Nd2 O6W 72.0(6) . .
O6W Nd2 Nd3 151.3(4) . 2
O6W Nd2 Nd4 87.6(4) . .
Nd2 Nd3 Nd4 118.81(4) 2 .
O8 Nd3 Nd2 107.1(4) . 2
O8 Nd3 Nd4 35.0(4) . .
O8 Nd3 O9 81.5(6) . .
O8 Nd3 O11 68.5(5) . 2
O8 Nd3 O12 118.9(6) . 2
O8 Nd3 O15 70.7(6) . .
O8 Nd3 O21 133.3(6) . 2
O8 Nd3 O3W 83.2(7) . .
O8 Nd3 O4W 146.1(7) . .
O9 Nd3 Nd2 34.9(4) . 2
O9 Nd3 Nd4 108.4(4) . .
O9 Nd3 O12 68.8(6) . 2
O9 Nd3 O15 74.8(6) . .
O9 Nd3 O21 137.7(6) . 2
O9 Nd3 O3W 146.5(7) . .
O9 Nd3 O4W 81.4(7) . .
O11 Nd3 Nd2 109.6(4) 2 2
O11 Nd3 Nd4 34.5(4) 2 .
O11 Nd3 O9 121.6(6) 2 .
O11 Nd3 O12 83.3(6) 2 2
O11 Nd3 O15 132.0(6) 2 .
O11 Nd3 O21 68.3(5) 2 2
O11 Nd3 O3W 79.2(7) 2 .
O11 Nd3 O4W 144.7(7) 2 .
O12 Nd3 Nd2 35.0(4) 2 2
O12 Nd3 Nd4 108.0(4) 2 .
O12 Nd3 O15 139.7(6) 2 .
O12 Nd3 O21 72.3(6) 2 2
O12 Nd3 O3W 144.0(7) 2 .
O12 Nd3 O4W 81.2(6) 2 .
O15 Nd3 Nd2 105.5(4) . 2
O15 Nd3 Nd4 99.3(4) . .
O15 Nd3 O21 132.5(6) . 2
O15 Nd3 O3W 72.0(7) . .
O15 Nd3 O4W 76.7(7) . .
O21 Nd3 Nd2 103.4(4) 2 2
O21 Nd3 Nd4 98.8(4) 2 .
O21 Nd3 O4W 76.8(7) 2 .
O3W Nd3 Nd2 168.3(6) . 2
O3W Nd3 Nd4 72.9(6) . .
O3W Nd3 O21 72.1(7) . 2
O3W Nd3 O4W 95.4(7) . .
O4W Nd3 Nd2 72.9(5) . 2
O4W Nd3 Nd4 168.3(5) . .
Nd2 Nd4 Nd3 121.25(4) . .
Ge4 Nd4 Nd2 59.96(5) 2 .
Ge4 Nd4 Nd3 102.05(5) 2 .
O7 Nd4 Nd2 35.1(4) . .
O7 Nd4 Nd3 110.3(4) . .
O7 Nd4 Ge4 94.3(4) . 2
O7 Nd4 O8 83.9(6) . .
O7 Nd4 O11 123.3(6) . 2
O7 Nd4 O13 68.4(6) . .
O7 Nd4 O19 133.3(6) . 2
O7 Nd4 O42 73.9(6) . 2_666
O7 Nd4 O5W 139.8(8) . .
O8 Nd4 Nd2 109.6(4) . .
O8 Nd4 Nd3 34.1(4) . .
O8 Nd4 Ge4 126.6(4) . 2
O8 Nd4 O13 74.6(6) . .
O8 Nd4 O19 138.0(6) . 2
O8 Nd4 O42 149.2(6) . 2_666
O8 Nd4 O5W 89.7(7) . .
O10 Nd4 Nd2 35.9(4) 2 .
O10 Nd4 Nd3 104.5(4) 2 .
O10 Nd4 Ge4 26.6(4) 2 2
O10 Nd4 O7 68.5(5) 2 .
O10 Nd4 O8 115.1(6) 2 .
O10 Nd4 O11 81.1(5) 2 2
O10 Nd4 O13 134.2(6) 2 .
O10 Nd4 O19 73.6(6) 2 2
O10 Nd4 O42 76.5(6) 2 2_666
O10 Nd4 O5W 146.7(8) 2 .
O11 Nd4 Nd2 111.6(4) 2 .
O11 Nd4 Nd3 34.0(4) 2 .
O11 Nd4 Ge4 70.2(4) 2 2
O11 Nd4 O8 67.0(5) 2 .
O11 Nd4 O13 137.2(6) 2 .
O11 Nd4 O19 74.6(6) 2 2
O11 Nd4 O42 143.5(5) 2 2_666
O11 Nd4 O5W 89.5(7) 2 .
O13 Nd4 Nd2 98.3(4) . .
O13 Nd4 Nd3 104.2(4) . .
O13 Nd4 Ge4 152.3(4) . 2
O13 Nd4 O42 77.5(6) . 2_666
O13 Nd4 O5W 71.6(8) . .
O19 Nd4 Nd2 99.7(4) 2 .
O19 Nd4 Nd3 104.6(4) 2 .
O19 Nd4 Ge4 47.9(5) 2 2
O19 Nd4 O13 130.7(6) 2 .
O19 Nd4 O42 71.6(6) 2 2_666
O19 Nd4 O5W 73.1(8) 2 .
O42 Nd4 Nd2 62.0(4) 2_666 .
O42 Nd4 Nd3 175.7(4) 2_666 .
O42 Nd4 Ge4 77.0(4) 2_666 2
O42 Nd4 O5W 93.7(7) 2_666 .
O5W Nd4 Nd2 155.5(5) . .
O5W Nd4 Nd3 83.2(5) . .
O5W Nd4 Ge4 120.5(7) . 2
Ge7 Nd5 Ge8 56.15(6) . .
Ge7 Nd5 H9B 153.0 . .
Ge8 Nd5 H9B 99.0 . .
Ge11 Nd5 Ge7 107.15(7) . .
Ge11 Nd5 Ge8 131.86(7) . .
Ge11 Nd5 H9B 97.5 . .
O25 Nd5 Ge7 30.2(4) . .
O25 Nd5 Ge8 29.3(4) . .
O25 Nd5 Ge11 132.1(4) . .
O25 Nd5 O26 58.3(6) . .
O25 Nd5 O28 145.7(5) . .
O25 Nd5 O29 114.6(5) . .
O25 Nd5 O30 59.5(6) . .
O25 Nd5 O8W 127.3(7) . .
O25 Nd5 O9W 121.7(7) . .
O25 Nd5 H9B 122.9 . .
O25 Nd5 O10W 73.8(5) . .
O26 Nd5 Ge7 85.7(4) . .
O26 Nd5 Ge8 29.6(4) . .
O26 Nd5 Ge11 126.4(4) . .
O26 Nd5 O30 115.8(5) . .
O26 Nd5 O9W 80.6(7) . .
O26 Nd5 H9B 70.7 . .
O28 Nd5 Ge7 132.4(4) . .
O28 Nd5 Ge8 126.0(4) . .
O28 Nd5 Ge11 30.0(4) . .
O28 Nd5 O26 106.0(6) . .
O28 Nd5 O29 59.2(5) . .
O28 Nd5 O30 116.2(5) . .
O28 Nd5 O9W 80.2(7) . .
O28 Nd5 H9B 69.0 . .
O28 Nd5 O10W 72.3(5) . .
O29 Nd5 Ge7 85.0(4) . .
O29 Nd5 Ge8 131.5(4) . .
O29 Nd5 Ge11 29.7(4) . .
O29 Nd5 O26 145.5(5) . .
O29 Nd5 O30 58.9(5) . .
O29 Nd5 O9W 122.1(7) . .
O29 Nd5 H9B 121.9 . .
O29 Nd5 O10W 73.2(5) . .
O30 Nd5 Ge7 30.3(4) . .
O30 Nd5 Ge8 86.4(4) . .
O30 Nd5 Ge11 86.4(4) . .
O30 Nd5 H9B 168.1 . .
O7W Nd5 Ge7 79.0(5) . .
O7W Nd5 Ge8 80.8(5) . .
O7W Nd5 Ge11 145.0(5) . .
O7W Nd5 O25 68.3(6) . .
O7W Nd5 O26 88.0(7) . .
O7W Nd5 O28 145.5(6) . .
O7W Nd5 O29 122.4(7) . .
O7W Nd5 O30 83.3(6) . .
O7W Nd5 O8W 69.5(8) . .
O7W Nd5 O9W 71.0(7) . .
O7W Nd5 H9B 87.1 . .
O7W Nd5 O10W 142.1(6) . .
O8W Nd5 Ge7 111.5(5) . .
O8W Nd5 Ge8 149.9(6) . .
O8W Nd5 Ge11 76.4(6) . .
O8W Nd5 O26 147.3(7) . .
O8W Nd5 O28 83.3(7) . .
O8W Nd5 O29 66.1(7) . .
O8W Nd5 O30 85.6(7) . .
O8W Nd5 O9W 70.0(8) . .
O8W Nd5 H9B 84.4 . .
O8W Nd5 O10W 139.1(7) . .
O9W Nd5 Ge7 147.3(6) . .
O9W Nd5 Ge8 105.2(6) . .
O9W Nd5 Ge11 104.9(6) . .
O9W Nd5 O30 149.3(7) . .
O9W Nd5 H9B 18.8 . .
O10W Nd5 Ge7 67.6(4) . .
O10W Nd5 Ge8 66.1(4) . .
O10W Nd5 Ge11 65.9(4) . .
O10W Nd5 O26 72.5(5) . .
O10W Nd5 O30 77.0(5) . .
O10W Nd5 O9W 133.7(7) . .
O10W Nd5 H9B 114.9 . .
Nd7 Nd6 Nd8 124.64(4) 2_666 .
Ge7 Nd6 Nd7 61.32(5) 2_666 2_666
Ge7 Nd6 Nd8 104.49(6) 2_666 .
Ge7 Nd6 Ge10 122.15(7) 2_666 .
Ge10 Nd6 Nd7 60.96(5) . 2_666
Ge10 Nd6 Nd8 104.30(6) . .
O31 Nd6 Nd7 35.0(4) 2_666 2_666
O31 Nd6 Nd8 112.7(4) 2_666 .
O31 Nd6 Ge7 27.0(4) 2_666 2_666
O31 Nd6 Ge10 95.3(4) 2_666 .
O31 Nd6 O35 122.8(6) 2_666 .
O31 Nd6 O37 67.6(6) 2_666 2_666
O31 Nd6 O43 135.7(6) 2_666 .
O31 Nd6 O11W 82.8(6) 2_666 .
O31 Nd6 O12W 141.2(6) 2_666 .
O32 Nd6 Nd7 111.5(4) 2_666 2_666
O32 Nd6 Nd8 34.9(4) 2_666 .
O32 Nd6 Ge7 70.5(4) 2_666 2_666
O32 Nd6 Ge10 129.7(4) 2_666 .
O32 Nd6 O31 84.9(6) 2_666 2_666
O32 Nd6 O35 67.3(6) 2_666 .
O32 Nd6 O37 74.6(6) 2_666 2_666
O32 Nd6 O43 133.4(6) 2_666 .
O32 Nd6 O11W 146.0(6) 2_666 .
O32 Nd6 O12W 93.2(6) 2_666 .
O34 Nd6 Nd7 35.3(4) . 2_666
O34 Nd6 Nd8 112.8(4) . .
O34 Nd6 Ge7 96.1(4) . 2_666
O34 Nd6 Ge10 26.2(4) . .
O34 Nd6 O31 69.2(6) . 2_666
O34 Nd6 O32 123.2(6) . 2_666
O34 Nd6 O35 85.4(6) . .
O34 Nd6 O37 130.9(6) . 2_666
O34 Nd6 O43 70.4(5) . .
O34 Nd6 O11W 81.2(6) . .
O34 Nd6 O12W 138.0(6) . .
O35 Nd6 Nd7 111.8(4) . 2_666
O35 Nd6 Nd8 34.2(4) . .
O35 Nd6 Ge7 129.7(4) . 2_666
O35 Nd6 Ge10 71.0(4) . .
O35 Nd6 O37 138.4(6) . 2_666
O35 Nd6 O43 70.4(5) . .
O35 Nd6 O11W 144.3(6) . .
O35 Nd6 O12W 91.4(6) . .
O37 Nd6 Nd7 96.8(4) 2_666 2_666
O37 Nd6 Nd8 104.5(4) 2_666 .
O37 Nd6 Ge7 42.8(4) 2_666 2_666
O37 Nd6 Ge10 150.5(5) 2_666 .
O37 Nd6 O12W 74.5(6) 2_666 .
O43 Nd6 Nd7 101.4(4) . 2_666
O43 Nd6 Nd8 99.0(4) . .
O43 Nd6 Ge7 156.1(4) . 2_666
O43 Nd6 Ge10 45.6(4) . .
O43 Nd6 O37 134.0(6) . 2_666
O43 Nd6 O11W 73.9(6) . .
O43 Nd6 O12W 69.1(6) . .
O11W Nd6 Nd7 73.6(4) . 2_666
O11W Nd6 Nd8 161.7(4) . .
O11W Nd6 Ge7 84.8(4) . 2_666
O11W Nd6 Ge10 83.1(4) . .
O11W Nd6 O37 71.4(6) . 2_666
O11W Nd6 O12W 77.3(6) . .
O12W Nd6 Nd7 150.9(4) . 2_666
O12W Nd6 Nd8 84.4(4) . .
O12W Nd6 Ge7 117.1(5) . 2_666
O12W Nd6 Ge10 114.7(4) . .
Nd8 Nd7 Nd6 114.35(4) . 2_666
O18 Nd7 Nd6 75.9(4) 2 2_666
O18 Nd7 Nd8 166.1(4) 2 .
O18 Nd7 O41 83.1(6) 2 2_666
O18 Nd7 O47 69.6(6) 2 .
O18 Nd7 O6W 88.7(6) 2 .
O31 Nd7 Nd6 35.0(4) . 2_666
O31 Nd7 Nd8 104.9(4) . .
O31 Nd7 O18 77.9(6) . 2
O31 Nd7 O33 117.5(6) . 2_666
O31 Nd7 O34 68.4(6) . 2_666
O31 Nd7 O41 143.0(6) . 2_666
O31 Nd7 O47 80.1(6) . .
O31 Nd7 O6W 144.4(6) . .
O33 Nd7 Nd6 104.1(4) 2_666 2_666
O33 Nd7 Nd8 36.3(4) 2_666 .
O33 Nd7 O18 153.7(6) 2_666 2
O33 Nd7 O41 72.0(6) 2_666 2_666
O33 Nd7 O47 131.3(5) 2_666 .
O33 Nd7 O6W 88.5(6) 2_666 .
O34 Nd7 Nd6 34.5(4) 2_666 2_666
O34 Nd7 Nd8 104.4(4) 2_666 .
O34 Nd7 O18 89.4(6) 2_666 2
O34 Nd7 O33 78.3(5) 2_666 2_666
O34 Nd7 O41 80.0(6) 2_666 2_666
O34 Nd7 O47 145.4(6) 2_666 .
O34 Nd7 O6W 145.2(6) 2_666 .
O36 Nd7 Nd6 105.4(4) . 2_666
O36 Nd7 Nd8 35.9(4) . .
O36 Nd7 O18 134.6(6) . 2
O36 Nd7 O31 79.6(6) . .
O36 Nd7 O33 71.3(6) . 2_666
O36 Nd7 O34 117.7(6) . 2_666
O36 Nd7 O41 134.1(6) . 2_666
O36 Nd7 O47 68.0(6) . .
O36 Nd7 O6W 87.2(6) . .
O41 Nd7 Nd6 109.5(4) 2_666 2_666
O41 Nd7 Nd8 101.0(4) 2_666 .
O41 Nd7 O47 122.2(6) 2_666 .
O41 Nd7 O6W 65.2(6) 2_666 .
O47 Nd7 Nd6 111.5(4) . 2_666
O47 Nd7 Nd8 97.3(4) . .
O47 Nd7 O6W 64.2(6) . .
O6W Nd7 Nd6 164.4(4) . 2_666
O6W Nd7 Nd8 81.2(4) . .
Nd7 Nd8 Nd6 121.00(4) . .
O32 Nd8 Nd6 34.1(4) 2_666 .
O32 Nd8 Nd7 109.4(4) 2_666 .
O32 Nd8 O33 83.1(5) 2_666 2_666
O32 Nd8 O36 121.2(6) 2_666 .
O32 Nd8 O39 67.2(6) 2_666 2_666
O32 Nd8 O45 131.9(6) 2_666 .
O32 Nd8 O13W 82.6(6) 2_666 .
O32 Nd8 O14W 137.0(6) 2_666 .
O33 Nd8 Nd6 109.9(4) 2_666 .
O33 Nd8 Nd7 36.2(4) 2_666 .
O33 Nd8 O36 69.6(5) 2_666 .
O33 Nd8 O39 71.7(5) 2_666 2_666
O33 Nd8 O45 141.5(6) 2_666 .
O33 Nd8 O13W 141.5(5) 2_666 .
O33 Nd8 O14W 87.0(6) 2_666 .
O35 Nd8 Nd6 35.3(4) . .
O35 Nd8 Nd7 107.8(4) . .
O35 Nd8 O32 67.6(6) . 2_666
O35 Nd8 O33 120.5(6) . 2_666
O35 Nd8 O36 82.9(6) . .
O35 Nd8 O39 130.8(6) . 2_666
O35 Nd8 O45 72.1(6) . .
O35 Nd8 O13W 86.0(6) . .
O35 Nd8 O14W 148.2(6) . .
O36 Nd8 Nd6 110.9(4) . .
O36 Nd8 Nd7 34.2(4) . .
O36 Nd8 O39 138.5(6) . 2_666
O36 Nd8 O45 77.1(6) . .
O36 Nd8 O13W 146.5(6) . .
O36 Nd8 O14W 93.5(7) . .
O39 Nd8 Nd6 95.8(4) 2_666 .
O39 Nd8 Nd7 104.7(4) 2_666 .
O39 Nd8 O13W 69.8(6) 2_666 .
O45 Nd8 Nd6 99.3(4) . .
O45 Nd8 Nd7 106.8(4) . .
O45 Nd8 O39 130.6(6) . 2_666
O45 Nd8 O13W 69.5(6) . .
O13W Nd8 Nd6 74.7(4) . .
O13W Nd8 Nd7 164.2(4) . .
O14W Nd8 Nd6 153.8(5) . .
O14W Nd8 Nd7 84.6(5) . .
O14W Nd8 O39 69.9(6) . 2_666
O14W Nd8 O45 76.3(6) . .
O14W Nd8 O13W 79.7(7) . .
O1 Ge1 Nd1 45.9(5) . .
O1 Ge1 O6 89.1(7) . .
O1 Ge1 C1 114.6(9) . .
O6 Ge1 Nd1 45.2(5) . .
O6 Ge1 C1 108.1(8) . .
O7 Ge1 Nd1 107.6(6) . .
O7 Ge1 O1 114.3(7) . .
O7 Ge1 O6 105.0(8) . .
O7 Ge1 C1 120.1(9) . .
C1 Ge1 Nd1 131.1(7) . .
O1 Ge2 C4 112.3(9) . .
O2 Ge2 O1 89.5(8) . .
O2 Ge2 C4 114.5(10) . .
O8 Ge2 O1 105.2(8) . .
O8 Ge2 O2 113.6(8) . .
O8 Ge2 C4 117.7(10) . .
O2 Ge3 O3 88.4(8) . .
O2 Ge3 C7 114.3(10) . .
O3 Ge3 C7 108.6(10) . .
O9 Ge3 O2 108.5(8) . .
O9 Ge3 O3 114.5(8) . .
O9 Ge3 C7 118.6(10) . .
Nd1 Ge4 Nd4 112.65(7) . 2
O3 Ge4 Nd1 44.9(5) . .
O3 Ge4 Nd4 137.4(5) . 2
O3 Ge4 C10 108.8(10) . .
O4 Ge4 Nd1 44.6(5) . .
O4 Ge4 Nd4 91.3(5) . 2
O4 Ge4 O3 87.4(7) . .
O4 Ge4 C10 109.4(9) . .
O10 Ge4 Nd1 103.0(5) . .
O10 Ge4 Nd4 36.7(5) . 2
O10 Ge4 O3 104.8(7) . .
O10 Ge4 O4 109.3(8) . .
O10 Ge4 C10 129.1(10) . .
C10 Ge4 Nd1 127.8(8) . .
C10 Ge4 Nd4 111.7(8) . 2
O4 Ge5 Nd1 43.8(5) . .
O4 Ge5 C13 110.3(9) . .
O5 Ge5 Nd1 44.3(5) . .
O5 Ge5 O4 86.4(7) . .
O5 Ge5 C13 109.9(9) . .
O11 Ge5 Nd1 108.9(6) . .
O11 Ge5 O4 105.7(7) . .
O11 Ge5 O5 115.4(8) . .
O11 Ge5 C13 122.8(10) . .
C13 Ge5 Nd1 128.0(8) . .
O5 Ge6 Nd1 45.4(5) . .
O5 Ge6 C16 106.3(9) . .
O6 Ge6 Nd1 45.3(5) . .
O6 Ge6 O5 88.8(7) . .
O6 Ge6 C16 112.5(10) . .
O12 Ge6 Nd1 107.7(6) . .
O12 Ge6 O5 105.6(8) . .
O12 Ge6 O6 113.9(8) . .
O12 Ge6 C16 123.2(10) . .
C16 Ge6 Nd1 128.1(8) . .
Nd5 Ge7 Nd6 111.91(8) . 2_666
O25 Ge7 Nd5 44.3(5) . .
O25 Ge7 Nd6 90.3(6) . 2_666
O25 Ge7 O37 80.0(7) . .
O25 Ge7 C19 115.0(10) . .
O30 Ge7 Nd5 46.6(6) . .
O30 Ge7 Nd6 135.6(6) . 2_666
O30 Ge7 O25 89.3(8) . .
O30 Ge7 O37 169.3(7) . .
O30 Ge7 C19 106.5(10) . .
O31 Ge7 Nd5 108.4(6) . .
O31 Ge7 Nd6 38.3(5) . 2_666
O31 Ge7 O25 114.8(8) . .
O31 Ge7 O30 103.9(8) . .
O31 Ge7 O37 81.3(7) . .
O31 Ge7 C19 120.9(11) . .
O37 Ge7 Nd5 123.0(5) . .
O37 Ge7 Nd6 45.9(4) . 2_666
C19 Ge7 Nd5 129.3(9) . .
C19 Ge7 Nd6 113.7(8) . 2_666
C19 Ge7 O37 77.9(9) . .
O25 Ge8 Nd5 43.5(5) . .
O25 Ge8 O39 167.6(7) . .
O25 Ge8 C22 109.5(10) . .
O26 Ge8 Nd5 45.2(6) . .
O26 Ge8 O25 87.6(8) . .
O26 Ge8 O39 80.0(7) . .
O26 Ge8 C22 115.4(10) . .
O32 Ge8 Nd5 105.5(5) . .
O32 Ge8 O25 103.1(8) . .
O32 Ge8 O26 110.2(8) . .
O32 Ge8 O39 80.9(7) . .
O32 Ge8 C22 123.9(11) . .
O39 Ge8 Nd5 124.2(4) . .
C22 Ge8 Nd5 129.6(9) . .
C22 Ge8 O39 76.8(9) . .
O26 Ge9 O27 92.7(8) . .
O26 Ge9 C25 111.9(10) . .
O27 Ge9 C25 107.1(9) . .
O33 Ge9 O26 109.1(8) . .
O33 Ge9 O27 111.7(8) . .
O33 Ge9 C25 120.8(11) . .
O27 Ge10 Nd6 137.9(5) . .
O27 Ge10 O28 91.4(8) . .
O27 Ge10 C28 109.5(10) . .
O28 Ge10 Nd6 91.5(5) . .
O28 Ge10 C28 112.0(10) . .
O34 Ge10 Nd6 36.5(5) . .
O34 Ge10 O27 106.3(8) . .
O34 Ge10 O28 114.3(8) . .
O34 Ge10 C28 119.3(10) . .
C28 Ge10 Nd6 108.1(8) . .
O28 Ge11 Nd5 45.4(5) . .
O28 Ge11 C31 110.6(8) . .
O29 Ge11 Nd5 45.8(6) . .
O29 Ge11 O28 90.3(8) . .
O29 Ge11 C31 110.6(9) . .
O35 Ge11 Nd5 109.0(5) . .
O35 Ge11 O28 107.3(8) . .
O35 Ge11 O29 109.2(8) . .
O35 Ge11 C31 123.6(9) . .
C31 Ge11 Nd5 127.3(8) . .
O29 Ge12 O30 89.0(8) . .
O29 Ge12 C34 108.0(9) . .
O30 Ge12 C34 109.9(10) . .
O36 Ge12 O29 106.5(8) . .
O36 Ge12 O30 114.5(8) . .
O36 Ge12 C34 123.2(10) . .
Ge1 O1 Nd1 104.2(7) . .
Ge1 O1 Ge2 130.9(9) . .
Ge2 O1 Nd1 106.4(7) . .
Ge2 O2 Nd1 102.4(7) . .
Ge2 O2 Ge3 129.6(9) . .
Ge3 O2 Nd1 101.7(7) . .
Ge3 O3 Nd1 108.3(8) . .
Ge4 O3 Nd1 104.8(7) . .
Ge4 O3 Ge3 127.4(9) . .
Ge4 O4 Nd1 105.6(7) . .
Ge4 O4 Ge5 130.8(9) . .
Ge5 O4 Nd1 106.2(7) . .
Ge5 O5 Nd1 106.6(7) . .
Ge5 O5 Ge6 130.0(10) . .
Ge6 O5 Nd1 103.9(7) . .
Ge1 O6 Nd1 104.6(7) . .
Ge6 O6 Nd1 104.8(7) . .
Ge6 O6 Ge1 131.1(9) . .
Nd4 O7 Nd2 110.0(6) . .
Ge1 O7 Nd2 130.3(8) . .
Ge1 O7 Nd4 117.9(8) . .
Nd3 O8 Nd4 110.9(6) . .
Ge2 O8 Nd3 119.4(9) . .
Ge2 O8 Nd4 126.4(9) . .
Nd2 O9 Nd3 110.0(6) 2 .
Ge3 O9 Nd2 119.6(8) . 2
Ge3 O9 Nd3 129.1(9) . .
Nd4 O10 Nd2 109.2(6) 2 2
Ge4 O10 Nd2 124.8(8) . 2
Ge4 O10 Nd4 116.7(8) . 2
Nd3 O11 Nd4 111.5(6) 2 2
Ge5 O11 Nd3 118.2(8) . 2
Ge5 O11 Nd4 129.2(8) . 2
Nd2 O12 Nd3 109.9(6) . 2
Ge6 O12 Nd2 118.7(9) . .
Ge6 O12 Nd3 129.3(9) . 2
C3 O13 Nd4 143.8(18) . .
C6 O15 Nd3 145.8(19) . .
C9 O17 Nd2 153.7(16) . 2
C9 O18 Nd7 135.9(15) . 2
C12 O19 Nd4 166.1(17) . 2
C15 O21 Nd3 151.3(16) . 2
C18 O23 Nd2 157.5(18) . .
Ge7 O25 Nd5 105.6(8) . .
Ge8 O25 Nd5 107.1(8) . .
Ge8 O25 Ge7 131.0(10) . .
Ge8 O26 Nd5 105.2(8) . .
Ge9 O26 Nd5 113.0(8) . .
Ge9 O26 Ge8 128.6(10) . .
Ge10 O27 Ge9 134.3(10) . .
Ge10 O28 Nd5 113.5(8) . .
Ge11 O28 Nd5 104.6(7) . .
Ge11 O28 Ge10 128.3(10) . .
Ge11 O29 Nd5 104.5(8) . .
Ge11 O29 Ge12 134.5(10) . .
Ge12 O29 Nd5 106.3(7) . .
Ge7 O30 Nd5 103.1(8) . .
Ge7 O30 Ge12 129.4(10) . .
Ge12 O30 Nd5 104.0(7) . .
Nd7 O31 Nd6 110.0(6) . 2_666
Ge7 O31 Nd6 114.7(8) . 2_666
Ge7 O31 Nd7 132.8(9) . .
Nd6 O32 Nd8 111.1(7) 2_666 2_666
Ge8 O32 Nd6 128.4(9) . 2_666
Ge8 O32 Nd8 116.0(8) . 2_666
Nd7 O33 Nd8 107.5(6) 2_666 2_666
Ge9 O33 Nd7 125.2(8) . 2_666
Ge9 O33 Nd8 125.9(8) . 2_666
Nd6 O34 Nd7 110.2(6) . 2_666
Ge10 O34 Nd6 117.4(8) . .
Ge10 O34 Nd7 130.5(8) . 2_666
Nd8 O35 Nd6 110.5(6) . .
Ge11 O35 Nd6 124.1(8) . .
Ge11 O35 Nd8 121.7(8) . .
Nd7 O36 Nd8 109.8(7) . .
Ge12 O36 Nd7 122.0(8) . .
Ge12 O36 Nd8 127.1(8) . .
Ge7 O37 Nd6 91.3(6) . 2_666
C21 O37 Nd6 142.2(18) . 2_666
C21 O37 Ge7 113.1(17) . .
Ge8 O39 Nd8 93.6(6) . 2_666
C24 O39 Nd8 140.8(17) . 2_666
C24 O39 Ge8 115.3(16) . .
C27 O41 Nd7 143.9(16) . 2_666
C27 O42 Nd4 136.3(16) . 2_666
C30 O43 Nd6 145.9(17) . .
C33 O45 Nd8 144.9(16) . .
C33 O46 Nd1 127.8(16) . 2_655
C36 O47 Nd7 150.5(17) . .
C36 O48 Nd2 136.2(17) . .
Nd1 O1W H1A 121.9 . .
Nd1 O1W H1B 128.9 . .
H1A O1W H1B 108.3 . .
Nd1 O2W H2A 126.0 . .
Nd1 O2W H2B 125.8 . .
H2A O2W H2B 108.0 . .
Nd3 O3W H3A 117.8 . .
Nd3 O3W H3B 132.6 . .
H3A O3W H3B 109.0 . .
Nd3 O4W H4A 122.4 . .
Nd3 O4W H4B 122.2 . .
H4A O4W H4B 108.9 . .
Nd2 O6W Nd7 126.2(7) . .
Nd2 O6W H6A 105.8 . .
Nd2 O6W H6B 105.7 . .
Nd7 O6W H6A 105.8 . .
Nd7 O6W H6B 105.7 . .
H6A O6W H6B 106.2 . .
Nd5 O7W H7A 113.6 . .
Nd5 O7W H7B 134.0 . .
H7A O7W H7B 108.4 . .
Nd5 O8W H8A 101.3 . .
Nd5 O8W H8B 150.5 . .
H8A O8W H8B 108.1 . .
Nd5 O9W H9A 159.5 . .
Nd5 O9W H9B 61.8 . .
H9A O9W H9B 108.2 . .
Nd5 O10W H10A 125.6 . .
Nd5 O10W H10B 126.4 . .
H10A O10W H10B 108.0 . .
Nd6 O11W H11A 133.7 . .
Nd6 O11W H11B 104.3 . .
H11A O11W H11B 108.3 . .
Nd6 O12W H12A 89.4 . .
Nd6 O12W H12B 126.0 . .
H12A O12W H12B 108.1 . .
Nd8 O13W H13A 97.3 . .
Nd8 O13W H13B 106.3 . .
H13A O13W H13B 108.5 . .
Nd8 O14W H14A 130.7 . .
Nd8 O14W H14B 110.3 . .
H14A O14W H14B 108.9 . .
Ge1 C1 H1C 109.2 . .
Ge1 C1 H1D 109.2 . .
H1C C1 H1D 107.9 . .
C2 C1 Ge1 112.2(17) . .
C2 C1 H1C 109.2 . .
C2 C1 H1D 109.2 . .
C1 C2 H2C 108.3 . .
C1 C2 H2D 108.3 . .
C1 C2 C3 116(2) . .
H2C C2 H2D 107.4 . .
C3 C2 H2C 108.3 . .
C3 C2 H2D 108.3 . .
O13 C3 O14 129(2) . .
O13 C3 C2 119(2) . .
O14 C3 C2 111(2) . .
Ge2 C4 H4C 108.9 . .
Ge2 C4 H4D 108.9 . .
H4C C4 H4D 107.8 . .
C5 C4 Ge2 113.2(19) . .
C5 C4 H4C 108.9 . .
C5 C4 H4D 108.9 . .
C4 C5 H5C 109.3 . .
C4 C5 H5D 109.3 . .
C4 C5 C6 112(2) . .
H5C C5 H5D 108.0 . .
C6 C5 H5C 109.3 . .
C6 C5 H5D 109.3 . .
O15 C6 O16 123(2) . .
O15 C6 C5 118(2) . .
O16 C6 C5 116(3) . .
Ge3 C7 H7C 108.4 . .
Ge3 C7 H7D 108.4 . .
H7C C7 H7D 107.5 . .
C8 C7 Ge3 115.5(19) . .
C8 C7 H7C 108.4 . .
C8 C7 H7D 108.4 . .
C7 C8 H8C 109.0 . .
C7 C8 H8D 109.0 . .
C7 C8 C9 113(2) . .
H8C C8 H8D 107.8 . .
C9 C8 H8C 109.0 . .
C9 C8 H8D 109.0 . .
O17 C9 C8 117(2) . .
O18 C9 O17 122.5(19) . .
O18 C9 C8 120(2) . .
Ge4 C10 H10C 110.0 . .
Ge4 C10 H10D 110.0 . .
H10C C10 H10D 108.4 . .
C11 C10 Ge4 108.4(17) . .
C11 C10 H10C 110.0 . .
C11 C10 H10D 110.0 . .
C10 C11 H11C 108.3 . .
C10 C11 H11D 108.3 . .
H11C C11 H11D 107.4 . .
C12 C11 C10 116(2) . .
C12 C11 H11C 108.3 . .
C12 C11 H11D 108.3 . .
O19 C12 C11 117(2) . .
O20 C12 O19 122(2) . .
O20 C12 C11 121(2) . .
Ge5 C13 H13C 108.7 . .
Ge5 C13 H13D 108.7 . .
H13C C13 H13D 107.6 . .
C14 C13 Ge5 114.4(17) . .
C14 C13 H13C 108.7 . .
C14 C13 H13D 108.7 . .
C13 C14 H14C 109.3 . .
C13 C14 H14D 109.3 . .
H14C C14 H14D 108.0 . .
C15 C14 C13 111.5(19) . .
C15 C14 H14C 109.3 . .
C15 C14 H14D 109.3 . .
O21 C15 C14 118(2) . .
O22 C15 O21 125(2) . .
O22 C15 C14 117.0(19) . .
Ge6 C16 H16A 109.8 . .
Ge6 C16 H16B 109.8 . .
H16A C16 H16B 108.2 . .
C17 C16 Ge6 109.5(17) . .
C17 C16 H16A 109.8 . .
C17 C16 H16B 109.8 . .
C16 C17 H17A 108.7 . .
C16 C17 H17B 108.7 . .
H17A C17 H17B 107.6 . .
C18 C17 C16 114(2) . .
C18 C17 H17A 108.7 . .
C18 C17 H17B 108.7 . .
O23 C18 O24 130(2) . .
O23 C18 C17 121(2) . .
O24 C18 C17 108(2) . .
Ge7 C19 H19A 109.0 . .
Ge7 C19 H19B 109.0 . .
H19A C19 H19B 107.8 . .
C20 C19 Ge7 113(2) . .
C20 C19 H19A 109.0 . .
C20 C19 H19B 109.0 . .
C19 C20 H20A 108.5 . .
C19 C20 H20B 108.5 . .
H20A C20 H20B 107.5 . .
C21 C20 C19 115(2) . .
C21 C20 H20A 108.5 . .
C21 C20 H20B 108.5 . .
O37 C21 O38 136(3) . .
O37 C21 C20 114(3) . .
O38 C21 C20 110(2) . .
Ge8 C22 H22A 108.9 . .
Ge8 C22 H22B 108.9 . .
H22A C22 H22B 107.7 . .
C23 C22 Ge8 113.5(19) . .
C23 C22 H22A 108.9 . .
C23 C22 H22B 108.9 . .
C22 C23 H23A 108.2 . .
C22 C23 H23B 108.2 . .
C22 C23 C24 116(2) . .
H23A C23 H23B 107.4 . .
C24 C23 H23A 108.2 . .
C24 C23 H23B 108.2 . .
O39 C24 O40 131(2) . .
O39 C24 C23 113(2) . .
O40 C24 C23 115(2) . .
Ge9 C25 H25A 109.4 . .
Ge9 C25 H25B 109.4 . .
H25A C25 H25B 108.0 . .
C26 C25 Ge9 111.3(18) . .
C26 C25 H25A 109.4 . .
C26 C25 H25B 109.4 . .
C25 C26 H26A 110.5 . .
C25 C26 H26B 110.5 . .
H26A C26 H26B 108.7 . .
C27 C26 C25 106(2) . .
C27 C26 H26A 110.5 . .
C27 C26 H26B 110.5 . .
O41 C27 O42 120(2) . .
O41 C27 C26 120(2) . .
O42 C27 C26 119(2) . .
Ge10 C28 H28A 109.2 . .
Ge10 C28 H28B 109.2 . .
H28A C28 H28B 107.9 . .
C29 C28 Ge10 112.3(18) . .
C29 C28 H28A 109.2 . .
C29 C28 H28B 109.2 . .
C28 C29 H29A 109.5 . .
C28 C29 H29B 109.5 . .
C28 C29 C30 111(2) . .
H29A C29 H29B 108.1 . .
C30 C29 H29A 109.5 . .
C30 C29 H29B 109.5 . .
O43 C30 O44 122(2) . .
O43 C30 C29 119(2) . .
O44 C30 C29 119(2) . .
Ge11 C31 H31A 109.0 . .
Ge11 C31 H31B 109.0 . .
H31A C31 H31B 107.8 . .
C32 C31 Ge11 112.8(15) . .
C32 C31 H31A 109.0 . .
C32 C31 H31B 109.0 . .
C31 C32 H32A 109.5 . .
C31 C32 H32B 109.5 . .
H32A C32 H32B 108.1 . .
C33 C32 C31 110.8(18) . .
C33 C32 H32A 109.5 . .
C33 C32 H32B 109.5 . .
O45 C33 O46 124.1(19) . .
O45 C33 C32 115(2) . .
O46 C33 C32 119(2) . .
Ge12 C34 H34A 107.6 . .
Ge12 C34 H34B 107.6 . .
H34A C34 H34B 107.0 . .
C35 C34 Ge12 118.9(17) . .
C35 C34 H34A 107.6 . .
C35 C34 H34B 107.6 . .
C34 C35 H35A 109.6 . .
C34 C35 H35B 109.6 . .
H35A C35 H35B 108.1 . .
C36 C35 C34 110.4(19) . .
C36 C35 H35A 109.6 . .
C36 C35 H35B 109.6 . .
O47 C36 O48 124.4(19) . .
O47 C36 C35 118(2) . .
O48 C36 C35 117(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Nd1 Ge1 3.485(3) .
Nd1 Ge4 3.460(3) .
Nd1 Ge6 3.472(3) .
Nd1 O1 2.582(17) .
Nd1 O2 2.706(17) .
Nd1 O3 2.528(17) .
Nd1 O4 2.521(17) .
Nd1 O5 2.548(16) .
Nd1 O6 2.553(16) .
Nd1 O46 2.396(17) 2_655
Nd1 O1W 2.503(16) .
Nd1 O2W 2.508(15) .
Nd2 Nd3 3.921(2) 2
Nd2 Nd4 3.9044(18) .
Nd2 O7 2.390(16) .
Nd2 O9 2.389(17) 2
Nd2 O10 2.427(15) 2
Nd2 O12 2.389(17) .
Nd2 O17 2.433(17) 2
Nd2 O23 2.647(17) .
Nd2 O48 2.527(17) .
Nd2 O6W 2.701(19) .
Nd3 Nd2 3.921(2) 2
Nd3 Nd4 3.9617(18) .
Nd3 O8 2.377(17) .
Nd3 O9 2.399(16) .
Nd3 O11 2.380(16) 2
Nd3 O12 2.401(17) 2
Nd3 O15 2.509(18) .
Nd3 O21 2.534(16) 2
Nd3 O3W 2.53(2) .
Nd3 O4W 2.59(2) .
Nd4 Ge4 3.530(3) 2
Nd4 O7 2.375(15) .
Nd4 O8 2.434(17) .
Nd4 O10 2.362(17) 2
Nd4 O11 2.413(16) 2
Nd4 O13 2.493(18) .
Nd4 O19 2.434(18) 2
Nd4 O42 2.553(19) 2_666
Nd4 O5W 2.56(2) .
Nd5 Ge7 3.492(3) .
Nd5 Ge8 3.512(3) .
Nd5 Ge11 3.471(3) .
Nd5 O25 2.530(16) .
Nd5 O26 2.581(17) .
Nd5 O28 2.552(17) .
Nd5 O29 2.571(17) .
Nd5 O30 2.606(18) .
Nd5 O7W 2.499(19) .
Nd5 O8W 2.55(2) .
Nd5 O9W 2.60(3) .
Nd5 H9B 2.3190 .
Nd5 O10W 2.579(16) .
Nd6 Nd7 3.9092(18) 2_666
Nd6 Nd8 3.9455(18) .
Nd6 Ge7 3.497(3) 2_666
Nd6 Ge10 3.524(3) .
Nd6 O31 2.387(16) 2_666
Nd6 O32 2.368(17) 2_666
Nd6 O34 2.359(16) .
Nd6 O35 2.435(16) .
Nd6 O37 2.511(18) 2_666
Nd6 O43 2.444(16) .
Nd6 O11W 2.491(17) .
Nd6 O12W 2.586(18) .
Nd7 Nd6 3.9092(18) 2_666
Nd7 Nd8 3.8984(18) .
Nd7 O18 2.526(17) 2
Nd7 O31 2.385(17) .
Nd7 O33 2.415(16) 2_666
Nd7 O34 2.407(16) 2_666
Nd7 O36 2.331(16) .
Nd7 O41 2.555(18) 2_666
Nd7 O47 2.618(18) .
Nd7 O6W 2.714(18) .
Nd8 O32 2.417(18) 2_666
Nd8 O33 2.420(15) 2_666
Nd8 O35 2.368(16) .
Nd8 O36 2.432(17) .
Nd8 O39 2.495(17) 2_666
Nd8 O45 2.483(17) .
Nd8 O13W 2.636(18) .
Nd8 O14W 2.464(19) .
Ge1 O1 1.793(17) .
Ge1 O6 1.815(16) .
Ge1 O7 1.729(15) .
Ge1 C1 1.94(2) .
Ge2 O1 1.819(16) .
Ge2 O2 1.791(18) .
Ge2 O8 1.739(16) .
Ge2 C4 1.93(3) .
Ge3 O2 1.800(18) .
Ge3 O3 1.810(16) .
Ge3 O9 1.741(16) .
Ge3 C7 1.94(3) .
Ge4 Nd4 3.530(3) 2
Ge4 O3 1.803(18) .
Ge4 O4 1.788(16) .
Ge4 O10 1.767(16) .
Ge4 C10 1.94(3) .
Ge5 O4 1.816(17) .
Ge5 O5 1.773(17) .
Ge5 O11 1.721(15) .
Ge5 C13 1.93(2) .
Ge6 O5 1.822(17) .
Ge6 O6 1.790(16) .
Ge6 O12 1.718(16) .
Ge6 C16 1.91(2) .
Ge7 Nd6 3.497(3) 2_666
Ge7 O25 1.821(18) .
Ge7 O30 1.808(17) .
Ge7 O31 1.746(17) .
Ge7 O37 2.376(19) .
Ge7 C19 1.91(3) .
Ge8 O25 1.801(19) .
Ge8 O26 1.798(17) .
Ge8 O32 1.750(17) .
Ge8 O39 2.376(18) .
Ge8 C22 1.93(3) .
Ge9 O26 1.774(18) .
Ge9 O27 1.784(16) .
Ge9 O33 1.699(16) .
Ge9 C25 1.94(3) .
Ge10 O27 1.760(17) .
Ge10 O28 1.796(18) .
Ge10 O34 1.750(16) .
Ge10 C28 1.97(2) .
Ge11 O28 1.795(17) .
Ge11 O29 1.776(17) .
Ge11 O35 1.739(16) .
Ge11 C31 1.95(2) .
Ge12 O29 1.803(16) .
Ge12 O30 1.833(18) .
Ge12 O36 1.739(17) .
Ge12 C34 1.89(2) .
O9 Nd2 2.389(17) 2
O10 Nd2 2.427(15) 2
O10 Nd4 2.362(17) 2
O11 Nd3 2.380(16) 2
O11 Nd4 2.413(16) 2
O12 Nd3 2.401(17) 2
O13 C3 1.18(3) .
O14 C3 1.27(3) .
O15 C6 1.20(3) .
O16 C6 1.27(4) .
O17 Nd2 2.433(17) 2
O17 C9 1.26(3) .
O18 Nd7 2.526(17) 2
O18 C9 1.26(3) .
O19 Nd4 2.434(18) 2
O19 C12 1.26(3) .
O20 C12 1.21(3) .
O21 Nd3 2.534(16) 2
O21 C15 1.26(3) .
O22 C15 1.25(3) .
O23 C18 1.17(3) .
O24 C18 1.26(3) .
O31 Nd6 2.387(16) 2_666
O32 Nd6 2.368(16) 2_666
O32 Nd8 2.417(18) 2_666
O33 Nd7 2.414(16) 2_666
O33 Nd8 2.420(15) 2_666
O34 Nd7 2.407(16) 2_666
O37 Nd6 2.511(18) 2_666
O37 C21 1.20(3) .
O38 C21 1.25(3) .
O39 Nd8 2.495(17) 2_666
O39 C24 1.19(3) .
O40 C24 1.21(3) .
O41 Nd7 2.555(18) 2_666
O41 C27 1.28(3) .
O42 Nd4 2.553(19) 2_666
O42 C27 1.28(3) .
O43 C30 1.21(3) .
O44 C30 1.28(3) .
O45 C33 1.26(3) .
O46 Nd1 2.397(17) 2_655
O46 C33 1.27(3) .
O47 C36 1.21(3) .
O48 C36 1.23(3) .
O1W H1A 0.8500 .
O1W H1B 0.8502 .
O2W H2A 0.8500 .
O2W H2B 0.8500 .
O3W H3A 0.8501 .
O3W H3B 0.8501 .
O4W H4A 0.8500 .
O4W H4B 0.8500 .
O6W H6A 0.8500 .
O6W H6B 0.8500 .
O7W H7A 0.8499 .
O7W H7B 0.8500 .
O8W H8A 0.8502 .
O8W H8B 0.8501 .
O9W H9A 0.8500 .
O9W H9B 0.8500 .
O10W H10A 0.8500 .
O10W H10B 0.8500 .
O11W H11A 0.8500 .
O11W H11B 0.8501 .
O12W H12A 0.8500 .
O12W H12B 0.8500 .
O13W H13A 0.8499 .
O13W H13B 0.8499 .
O14W H14A 0.8499 .
O14W H14B 0.8500 .
C1 H1C 0.9700 .
C1 H1D 0.9700 .
C1 C2 1.523(9) .
C2 H2C 0.9700 .
C2 H2D 0.9700 .
C2 C3 1.526(9) .
C4 H4C 0.9700 .
C4 H4D 0.9700 .
C4 C5 1.50(4) .
C5 H5C 0.9700 .
C5 H5D 0.9700 .
C5 C6 1.529(9) .
C7 H7C 0.9700 .
C7 H7D 0.9700 .
C7 C8 1.46(3) .
C8 H8C 0.9700 .
C8 H8D 0.9700 .
C8 C9 1.537(9) .
C10 H10C 0.9700 .
C10 H10D 0.9700 .
C10 C11 1.53(3) .
C11 H11C 0.9700 .
C11 H11D 0.9700 .
C11 C12 1.528(9) .
C13 H13C 0.9700 .
C13 H13D 0.9700 .
C13 C14 1.529(9) .
C14 H14C 0.9700 .
C14 H14D 0.9700 .
C14 C15 1.527(9) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C16 C17 1.57(4) .
C17 H17A 0.9700 .
C17 H17B 0.9700 .
C17 C18 1.533(9) .
C19 H19A 0.9700 .
C19 H19B 0.9700 .
C19 C20 1.525(9) .
C20 H20A 0.9700 .
C20 H20B 0.9700 .
C20 C21 1.525(9) .
C22 H22A 0.9700 .
C22 H22B 0.9700 .
C22 C23 1.526(9) .
C23 H23A 0.9700 .
C23 H23B 0.9700 .
C23 C24 1.527(9) .
C25 H25A 0.9700 .
C25 H25B 0.9700 .
C25 C26 1.533(9) .
C26 H26A 0.9700 .
C26 H26B 0.9700 .
C26 C27 1.526(9) .
C28 H28A 0.9700 .
C28 H28B 0.9700 .
C28 C29 1.53(4) .
C29 H29A 0.9700 .
C29 H29B 0.9700 .
C29 C30 1.529(9) .
C31 H31A 0.9700 .
C31 H31B 0.9700 .
C31 C32 1.533(9) .
C32 H32A 0.9700 .
C32 H32B 0.9700 .
C32 C33 1.528(9) .
C34 H34A 0.9700 .
C34 H34B 0.9700 .
C34 C35 1.530(9) .
C35 H35A 0.9700 .
C35 H35B 0.9700 .
C35 C36 1.529(9) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Nd1 Ge1 O1 Ge2 -127.1(15) . .
Nd1 Ge1 O6 Ge6 125.2(14) . .
Nd1 Ge1 O7 Nd2 -93.6(10) . .
Nd1 Ge1 O7 Nd4 103.4(7) . .
Nd1 Ge1 C1 C2 -105.1(18) . .
Nd1 Ge4 O3 Ge3 127.7(15) . .
Nd1 Ge4 O4 Ge5 -128.6(15) . .
Nd1 Ge4 O10 Nd2 -106.5(8) . 2
Nd1 Ge4 O10 Nd4 110.6(7) . 2
Nd1 Ge4 C10 C11 -85.8(18) . .
Nd1 Ge5 O4 Ge4 128.4(15) . .
Nd1 Ge5 O5 Ge6 -125.3(14) . .
Nd1 Ge5 O11 Nd3 101.7(7) . 2
Nd1 Ge5 O11 Nd4 -91.2(10) . 2
Nd1 Ge5 C13 C14 -91.6(19) . .
Nd1 Ge6 O5 Ge5 126.3(14) . .
Nd1 Ge6 O6 Ge1 -125.1(14) . .
Nd1 Ge6 O12 Nd2 103.1(7) . .
Nd1 Ge6 O12 Nd3 -95.2(10) . 2
Nd1 Ge6 C16 C17 -92.4(18) . .
Nd1 O46 C33 O45 142(2) 2_655 .
Nd1 O46 C33 C32 -51(3) 2_655 .
Nd2 Nd3 Nd4 Nd2 0.24(7) 2 .
Nd2 Nd3 Nd4 Ge4 62.26(6) 2 2
Nd2 Nd3 Nd4 O7 -37.0(4) 2 .
Nd2 Nd3 Nd4 O8 -78.4(7) 2 .
Nd2 Nd3 Nd4 O10 35.1(4) 2 2
Nd2 Nd3 Nd4 O11 82.8(7) 2 2
Nd2 Nd3 Nd4 O13 -108.9(5) 2 .
Nd2 Nd3 Nd4 O19 111.5(5) 2 2
Nd2 Nd3 Nd4 O42 139(6) 2 2_666
Nd2 Nd3 Nd4 O5W -178.0(7) 2 .
Nd2 Nd3 O8 Nd4 116.1(6) 2 .
Nd2 Nd3 O8 Ge2 -83.3(9) 2 .
Nd2 Nd3 O9 Ge3 -166.4(16) 2 .
Nd2 Nd3 O15 C6 -153(3) 2 .
Nd2 Nd4 O7 Ge1 166.3(14) . .
Nd2 Nd4 O8 Nd3 -117.2(6) . .
Nd2 Nd4 O8 Ge2 83.9(10) . .
Nd2 Nd4 O13 C3 92(3) . .
Nd2 O17 C9 O18 64(5) 2 .
Nd2 O17 C9 C8 -123(3) 2 .
Nd2 O23 C18 O24 77(6) . .
Nd2 O23 C18 C17 -115(4) . .
Nd2 O48 C36 O47 -43(4) . .
Nd2 O48 C36 C35 136.9(19) . .
Nd3 Nd2 Nd4 Nd3 -0.24(7) 2 .
Nd3 Nd2 Nd4 Ge4 -86.30(6) 2 2
Nd3 Nd2 Nd4 O7 80.8(7) 2 .
Nd3 Nd2 Nd4 O8 35.4(4) 2 .
Nd3 Nd2 Nd4 O10 -70.6(7) 2 2
Nd3 Nd2 Nd4 O11 -36.8(4) 2 2
Nd3 Nd2 Nd4 O13 112.0(4) 2 .
Nd3 Nd2 Nd4 O19 -114.0(4) 2 2
Nd3 Nd2 Nd4 O42 -177.0(5) 2 2_666
Nd3 Nd2 Nd4 O5W 175.5(17) 2 .
Nd3 Nd2 O7 Nd4 -115.0(5) 2 .
Nd3 Nd2 O7 Ge1 81.0(11) 2 .
Nd3 Nd2 O12 Ge6 165.0(14) 2 .
Nd3 Nd2 O23 C18 85(5) 2 .
Nd3 Nd2 O48 C36 -176(2) 2 .
Nd3 Nd2 O6W Nd7 87.0(11) 2 .
Nd3 Nd4 O7 Nd2 115.8(5) . .
Nd3 Nd4 O7 Ge1 -78.0(9) . .
Nd3 Nd4 O8 Ge2 -158.9(16) . .
Nd3 Nd4 O13 C3 -143(3) . .
Nd3 O15 C6 O16 39(5) . .
Nd3 O15 C6 C5 -121(3) . .
Nd3 O21 C15 O22 54(5) 2 .
Nd3 O21 C15 C14 -128(3) 2 .
Nd4 Nd2 O7 Ge1 -164.0(16) . .
Nd4 Nd2 O12 Nd3 115.7(5) . 2
Nd4 Nd2 O12 Ge6 -79.3(9) . .
Nd4 Nd2 O23 C18 -151(4) . .
Nd4 Nd2 O48 C36 10(3) . .
Nd4 Nd2 O6W Nd7 -108.8(8) . .
Nd4 Nd3 O8 Ge2 160.6(15) . .
Nd4 Nd3 O9 Nd2 -114.3(5) . 2
Nd4 Nd3 O9 Ge3 79.3(11) . .
Nd4 Nd3 O15 C6 83(3) . .
Nd4 Ge4 O3 Nd1 -73.5(8) 2 .
Nd4 Ge4 O3 Ge3 54.2(15) 2 .
Nd4 Ge4 O4 Nd1 121.8(5) 2 .
Nd4 Ge4 O4 Ge5 -6.9(12) 2 .
Nd4 Ge4 O10 Nd2 143.0(15) 2 2
Nd4 Ge4 C10 C11 60.7(18) 2 .
Nd4 O13 C3 O14 67(5) . .
Nd4 O13 C3 C2 -124(3) . .
Nd4 O19 C12 O20 40(9) 2 .
Nd4 O19 C12 C11 -140(6) 2 .
Nd4 O42 C27 O41 125(2) 2_666 .
Nd4 O42 C27 C26 -62(3) 2_666 .
Nd5 Ge7 O25 Ge8 -130.4(16) . .
Nd5 Ge7 O30 Ge12 120.9(16) . .
Nd5 Ge7 O31 Nd6 102.4(7) . 2_666
Nd5 Ge7 O31 Nd7 -97.9(11) . .
Nd5 Ge7 O37 Nd6 -89.4(5) . 2_666
Nd5 Ge7 O37 C21 120.2(19) . .
Nd5 Ge7 C19 C20 -103(2) . .
Nd5 Ge8 O25 Ge7 129.9(16) . .
Nd5 Ge8 O26 Ge9 -137.3(16) . .
Nd5 Ge8 O32 Nd6 -96.2(9) . 2_666
Nd5 Ge8 O32 Nd8 110.0(7) . 2_666
Nd5 Ge8 O39 Nd8 -91.2(5) . 2_666
Nd5 Ge8 O39 C24 116.2(18) . .
Nd5 Ge8 C22 C23 -105(2) . .
Nd5 Ge11 O28 Ge10 137.0(15) . .
Nd5 Ge11 O29 Ge12 -131.3(17) . .
Nd5 Ge11 O35 Nd6 -99.7(8) . .
Nd5 Ge11 O35 Nd8 104.1(8) . .
Nd5 Ge11 C31 C32 -94.9(17) . .
Nd6 Nd7 Nd8 Nd6 -0.98(7) 2_666 .
Nd6 Nd7 Nd8 O32 34.6(4) 2_666 2_666
Nd6 Nd7 Nd8 O33 80.5(7) 2_666 2_666
Nd6 Nd7 Nd8 O35 -37.2(4) 2_666 .
Nd6 Nd7 Nd8 O36 -82.6(7) 2_666 .
Nd6 Nd7 Nd8 O39 105.3(4) 2_666 2_666
Nd6 Nd7 Nd8 O45 -113.3(4) 2_666 .
Nd6 Nd7 Nd8 O13W 172.7(15) 2_666 .
Nd6 Nd7 Nd8 O14W 172.9(5) 2_666 .
Nd6 Nd7 O31 Ge7 -160.5(17) 2_666 .
Nd6 Nd7 O36 Nd8 110.4(6) 2_666 .
Nd6 Nd7 O36 Ge12 -80.4(10) 2_666 .
Nd6 Nd7 O47 C36 -162(3) 2_666 .
Nd6 Nd7 O6W Nd2 16(2) 2_666 .
Nd6 Nd8 O35 Ge11 159.1(14) . .
Nd6 Nd8 O36 Nd7 -114.8(5) . .
Nd6 Nd8 O36 Ge12 76.7(11) . .
Nd6 Nd8 O45 C33 69(3) . .
Nd6 Ge7 O25 Nd5 121.9(6) 2_666 .
Nd6 Ge7 O25 Ge8 -8.5(12) 2_666 .
Nd6 Ge7 O30 Nd5 -76.7(9) 2_666 .
Nd6 Ge7 O30 Ge12 44.3(17) 2_666 .
Nd6 Ge7 O31 Nd7 159.8(17) 2_666 .
Nd6 Ge7 O37 C21 -150(2) 2_666 .
Nd6 Ge7 C19 C20 50(2) 2_666 .
Nd6 Ge10 O27 Ge9 28(2) . .
Nd6 Ge10 O28 Nd5 121.7(6) . .
Nd6 Ge10 O28 Ge11 -12.3(11) . .
Nd6 Ge10 O34 Nd7 162.8(16) . 2_666
Nd6 Ge10 C28 C29 59(2) . .
Nd6 O37 C21 O38 42(6) 2_666 .
Nd6 O37 C21 C20 -132(2) 2_666 .
Nd6 O43 C30 O44 58(4) . .
Nd6 O43 C30 C29 -127(3) . .
Nd7 Nd6 Nd8 Nd7 1.09(8) 2_666 .
Nd7 Nd6 Nd8 O32 -77.6(7) 2_666 2_666
Nd7 Nd6 Nd8 O33 -37.3(4) 2_666 2_666
Nd7 Nd6 Nd8 O35 77.7(7) 2_666 .
Nd7 Nd6 Nd8 O36 37.6(4) 2_666 .
Nd7 Nd6 Nd8 O39 -109.9(4) 2_666 2_666
Nd7 Nd6 Nd8 O45 117.2(4) 2_666 .
Nd7 Nd6 Nd8 O13W -177.1(4) 2_666 .
Nd7 Nd6 Nd8 O14W -164.9(10) 2_666 .
Nd7 Nd6 Ge10 O27 -46.5(9) 2_666 .
Nd7 Nd6 Ge10 O28 -140.3(5) 2_666 .
Nd7 Nd6 Ge10 O34 -9.1(9) 2_666 .
Nd7 Nd6 Ge10 C28 105.9(9) 2_666 .
Nd7 Nd6 O34 Ge10 166.1(13) 2_666 .
Nd7 Nd6 O35 Nd8 -120.0(5) 2_666 .
Nd7 Nd6 O35 Ge11 81.5(10) 2_666 .
Nd7 Nd6 O43 C30 96(3) 2_666 .
Nd7 Nd8 O35 Nd6 118.9(5) . .
Nd7 Nd8 O35 Ge11 -82.1(9) . .
Nd7 Nd8 O36 Ge12 -168.5(16) . .
Nd7 Nd8 O45 C33 -164(3) . .
Nd7 O18 C9 O17 -33(4) 2 .
Nd7 O18 C9 C8 155.2(18) 2 .
Nd7 O41 C27 O42 56(4) 2_666 .
Nd7 O41 C27 C26 -117(3) 2_666 .
Nd7 O47 C36 O48 51(5) . .
Nd7 O47 C36 C35 -128(3) . .
Nd8 Nd6 Ge10 O27 75.4(9) . .
Nd8 Nd6 Ge10 O28 -18.4(5) . .
Nd8 Nd6 Ge10 O34 112.8(9) . .
Nd8 Nd6 Ge10 C28 -132.1(9) . .
Nd8 Nd6 O34 Nd7 118.2(5) . 2_666
Nd8 Nd6 O34 Ge10 -75.6(8) . .
Nd8 Nd6 O35 Ge11 -158.5(15) . .
Nd8 Nd6 O43 C30 -136(3) . .
Nd8 Nd7 O31 Nd6 -111.3(5) . 2_666
Nd8 Nd7 O31 Ge7 88.3(11) . .
Nd8 Nd7 O36 Ge12 169.2(15) . .
Nd8 Nd7 O47 C36 79(3) . .
Nd8 Nd7 O6W Nd2 -164.2(8) . .
Nd8 O39 C24 O40 42(5) 2_666 .
Nd8 O39 C24 C23 -131(2) 2_666 .
Nd8 O45 C33 O46 39(4) . .
Nd8 O45 C33 C32 -128(2) . .
Ge1 Nd1 Ge4 Nd4 35.40(13) . 2
Ge1 Nd1 Ge4 O3 -99.9(7) . .
Ge1 Nd1 Ge4 O4 102.5(8) . .
Ge1 Nd1 Ge4 O10 -1.9(6) . .
Ge1 Nd1 Ge4 C10 -178.4(10) . .
Ge1 Nd1 Ge5 O4 -156.5(7) . .
Ge1 Nd1 Ge5 O5 44.3(8) . .
Ge1 Nd1 Ge5 O11 -63.2(6) . .
Ge1 Nd1 Ge5 C13 123.8(8) . .
Ge1 Nd1 Ge6 O5 -178.3(7) . .
Ge1 Nd1 Ge6 O6 22.7(7) . .
Ge1 Nd1 Ge6 O12 -83.7(6) . .
Ge1 Nd1 Ge6 C16 107.5(11) . .
Ge1 Nd1 O1 Ge2 141.1(12) . .
Ge1 Nd1 O2 Ge2 2.1(6) . .
Ge1 Nd1 O2 Ge3 137.5(6) . .
Ge1 Nd1 O3 Ge3 -26.8(10) . .
Ge1 Nd1 O3 Ge4 111.8(6) . .
Ge1 Nd1 O4 Ge4 -109.6(6) . .
Ge1 Nd1 O4 Ge5 32.4(9) . .
Ge1 Nd1 O5 Ge5 -138.5(7) . .
Ge1 Nd1 O5 Ge6 1.4(6) . .
Ge1 Nd1 O6 Ge6 -140.4(11) . .
Ge1 C1 C2 C3 -31(3) . .
Ge2 C4 C5 C6 -49(3) . .
Ge3 C7 C8 C9 -49(3) . .
Ge4 Nd1 Ge1 O1 97.9(7) . .
Ge4 Nd1 Ge1 O6 -103.1(7) . .
Ge4 Nd1 Ge1 O7 -9.2(6) . .
Ge4 Nd1 Ge1 C1 -176.4(9) . .
Ge4 Nd1 Ge5 O4 -21.6(7) . .
Ge4 Nd1 Ge5 O5 179.2(8) . .
Ge4 Nd1 Ge5 O11 71.7(6) . .
Ge4 Nd1 Ge5 C13 -101.4(8) . .
Ge4 Nd1 Ge6 O5 -43.4(7) . .
Ge4 Nd1 Ge6 O6 157.7(7) . .
Ge4 Nd1 Ge6 O12 51.3(6) . .
Ge4 Nd1 Ge6 C16 -117.6(10) . .
Ge4 Nd1 O1 Ge1 -112.8(6) . .
Ge4 Nd1 O1 Ge2 28.2(10) . .
Ge4 Nd1 O2 Ge2 -136.1(6) . .
Ge4 Nd1 O2 Ge3 -0.7(6) . .
Ge4 Nd1 O3 Ge3 -138.5(12) . .
Ge4 Nd1 O4 Ge5 142.0(12) . .
Ge4 Nd1 O5 Ge5 -0.7(6) . .
Ge4 Nd1 O5 Ge6 139.1(6) . .
Ge4 Nd1 O6 Ge1 109.6(6) . .
Ge4 Nd1 O6 Ge6 -30.8(9) . .
Ge4 Nd4 O7 Nd2 11.2(6) 2 .
Ge4 Nd4 O7 Ge1 177.5(8) 2 .
Ge4 Nd4 O8 Nd3 -50.6(8) 2 .
Ge4 Nd4 O8 Ge2 150.5(8) 2 .
Ge4 Nd4 O13 C3 56(3) 2 .
Ge4 C10 C11 C12 -50(3) . .
Ge5 C13 C14 C15 -41(3) . .
Ge6 Nd1 Ge1 O1 178.5(7) . .
Ge6 Nd1 Ge1 O6 -22.5(7) . .
Ge6 Nd1 Ge1 O7 71.4(6) . .
Ge6 Nd1 Ge1 C1 -95.8(9) . .
Ge6 Nd1 Ge4 Nd4 -24.42(9) . 2
Ge6 Nd1 Ge4 O3 -159.7(7) . .
Ge6 Nd1 Ge4 O4 42.6(8) . .
Ge6 Nd1 Ge4 O10 -61.7(6) . .
Ge6 Nd1 Ge4 C10 121.8(10) . .
Ge6 Nd1 Ge5 O4 -177.4(7) . .
Ge6 Nd1 Ge5 O5 23.4(8) . .
Ge6 Nd1 Ge5 O11 -84.0(6) . .
Ge6 Nd1 Ge5 C13 102.9(8) . .
Ge6 Nd1 O1 Ge1 -1.2(6) . .
Ge6 Nd1 O1 Ge2 139.8(7) . .
Ge6 Nd1 O2 Ge2 -24.8(10) . .
Ge6 Nd1 O2 Ge3 110.6(6) . .
Ge6 Nd1 O3 Ge3 -110.3(7) . .
Ge6 Nd1 O3 Ge4 28.3(10) . .
Ge6 Nd1 O4 Ge4 -139.8(7) . .
Ge6 Nd1 O4 Ge5 2.2(6) . .
Ge6 Nd1 O5 Ge5 -139.8(12) . .
Ge6 Nd1 O6 Ge1 140.4(11) . .
Ge6 C16 C17 C18 -44(3) . .
Ge7 Nd5 Ge8 O25 -21.3(8) . .
Ge7 Nd5 Ge8 O26 174.9(8) . .
Ge7 Nd5 Ge8 O32 71.6(6) . .
Ge7 Nd5 Ge8 O39 161.0(5) . .
Ge7 Nd5 Ge8 C22 -97.2(9) . .
Ge7 Nd5 Ge11 O28 -151.1(8) . .
Ge7 Nd5 Ge11 O29 43.4(7) . .
Ge7 Nd5 Ge11 O35 -55.2(6) . .
Ge7 Nd5 Ge11 C31 126.3(7) . .
Ge7 Nd5 O25 Ge8 143.1(13) . .
Ge7 Nd5 O26 Ge8 -4.3(6) . .
Ge7 Nd5 O26 Ge9 140.6(8) . .
Ge7 Nd5 O28 Ge10 -105.6(7) . .
Ge7 Nd5 O28 Ge11 38.7(10) . .
Ge7 Nd5 O29 Ge11 -138.8(7) . .
Ge7 Nd5 O29 Ge12 7.3(7) . .
Ge7 Nd5 O30 Ge12 -136.9(12) . .
Ge7 Nd6 Nd8 Nd7 66.00(7) 2_666 .
Ge7 Nd6 Nd8 O32 -12.7(7) 2_666 2_666
Ge7 Nd6 Nd8 O33 27.6(4) 2_666 2_666
Ge7 Nd6 Nd8 O35 142.6(7) 2_666 .
Ge7 Nd6 Nd8 O36 102.5(4) 2_666 .
Ge7 Nd6 Nd8 O39 -45.0(4) 2_666 2_666
Ge7 Nd6 Nd8 O45 -177.8(4) 2_666 .
Ge7 Nd6 Nd8 O13W -112.2(4) 2_666 .
Ge7 Nd6 Nd8 O14W -100.0(10) 2_666 .
Ge7 Nd6 Ge10 O27 -42.3(9) 2_666 .
Ge7 Nd6 Ge10 O28 -136.1(5) 2_666 .
Ge7 Nd6 Ge10 O34 -4.9(9) 2_666 .
Ge7 Nd6 Ge10 C28 110.2(9) 2_666 .
Ge7 Nd6 O34 Nd7 9.7(6) 2_666 2_666
Ge7 Nd6 O34 Ge10 175.8(8) 2_666 .
Ge7 Nd6 O35 Nd8 -49.9(8) 2_666 .
Ge7 Nd6 O35 Ge11 151.6(7) 2_666 .
Ge7 Nd6 O43 C30 55(3) 2_666 .
Ge7 O37 C21 O38 168(3) . .
Ge7 O37 C21 C20 -6(3) . .
Ge7 C19 C20 C21 -32(3) . .
Ge8 Nd5 Ge7 Nd6 -45.40(7) . 2_666
Ge8 Nd5 Ge7 O25 20.8(8) . .
Ge8 Nd5 Ge7 O30 -178.2(8) . .
Ge8 Nd5 Ge7 O31 -86.2(6) . .
Ge8 Nd5 Ge7 O37 5.3(5) . .
Ge8 Nd5 Ge7 C19 107.4(10) . .
Ge8 Nd5 Ge11 O28 -91.5(8) . .
Ge8 Nd5 Ge11 O29 103.0(7) . .
Ge8 Nd5 Ge11 O35 4.4(6) . .
Ge8 Nd5 Ge11 C31 -174.1(7) . .
Ge8 Nd5 O25 Ge7 -143.1(13) . .
Ge8 Nd5 O26 Ge9 144.9(13) . .
Ge8 Nd5 O28 Ge10 -31.3(9) . .
Ge8 Nd5 O28 Ge11 113.1(6) . .
Ge8 Nd5 O29 Ge11 -104.3(6) . .
Ge8 Nd5 O29 Ge12 41.7(10) . .
Ge8 Nd5 O30 Ge7 1.5(6) . .
Ge8 Nd5 O30 Ge12 -135.4(7) . .
Ge8 O39 C24 O40 175(3) . .
Ge8 O39 C24 C23 2(3) . .
Ge8 C22 C23 C24 -26(3) . .
Ge9 C25 C26 C27 -62(3) . .
Ge10 Nd6 Nd8 Nd7 -63.27(6) . .
Ge10 Nd6 Nd8 O32 -142.0(7) . 2_666
Ge10 Nd6 Nd8 O33 -101.7(4) . 2_666
Ge10 Nd6 Nd8 O35 13.3(7) . .
Ge10 Nd6 Nd8 O36 -26.7(4) . .
Ge10 Nd6 Nd8 O39 -174.3(4) . 2_666
Ge10 Nd6 Nd8 O45 52.9(4) . .
Ge10 Nd6 Nd8 O13W 118.5(4) . .
Ge10 Nd6 Nd8 O14W 130.7(10) . .
Ge10 Nd6 O34 Nd7 -166.1(13) . 2_666
Ge10 Nd6 O35 Nd8 -166.3(7) . .
Ge10 Nd6 O35 Ge11 35.2(8) . .
Ge10 Nd6 O43 C30 123(3) . .
Ge10 C28 C29 C30 -45(3) . .
Ge11 Nd5 Ge7 Nd6 83.94(9) . 2_666
Ge11 Nd5 Ge7 O25 150.1(8) . .
Ge11 Nd5 Ge7 O30 -48.8(8) . .
Ge11 Nd5 Ge7 O31 43.2(6) . .
Ge11 Nd5 Ge7 O37 134.6(5) . .
Ge11 Nd5 Ge7 C19 -123.3(10) . .
Ge11 Nd5 Ge8 O25 -104.2(8) . .
Ge11 Nd5 Ge8 O26 92.0(8) . .
Ge11 Nd5 Ge8 O32 -11.3(6) . .
Ge11 Nd5 Ge8 O39 78.2(5) . .
Ge11 Nd5 Ge8 C22 179.9(9) . .
Ge11 Nd5 O25 Ge7 -40.0(10) . .
Ge11 Nd5 O25 Ge8 103.1(7) . .
Ge11 Nd5 O26 Ge8 -112.4(6) . .
Ge11 Nd5 O26 Ge9 32.5(10) . .
Ge11 Nd5 O28 Ge10 -144.3(13) . .
Ge11 Nd5 O29 Ge12 146.1(13) . .
Ge11 Nd5 O30 Ge7 133.9(7) . .
Ge11 Nd5 O30 Ge12 -3.0(6) . .
Ge11 C31 C32 C33 -55(2) . .
Ge12 C34 C35 C36 -40(3) . .
O1 Nd1 Ge1 O6 159.0(10) . .
O1 Nd1 Ge1 O7 -107.1(9) . .
O1 Nd1 Ge1 C1 85.7(11) . .
O1 Nd1 Ge4 Nd4 77.8(5) . 2
O1 Nd1 Ge4 O3 -57.5(9) . .
O1 Nd1 Ge4 O4 144.9(9) . .
O1 Nd1 Ge4 O10 40.5(8) . .
O1 Nd1 Ge4 C10 -135.9(11) . .
O1 Nd1 Ge5 O4 -140.9(9) . .
O1 Nd1 Ge5 O5 59.9(9) . .
O1 Nd1 Ge5 O11 -47.6(8) . .
O1 Nd1 Ge5 C13 139.3(9) . .
O1 Nd1 Ge6 O5 -177.6(8) . .
O1 Nd1 Ge6 O6 23.5(7) . .
O1 Nd1 Ge6 O12 -83.0(7) . .
O1 Nd1 Ge6 C16 108.2(11) . .
O1 Nd1 O2 Ge2 14.2(6) . .
O1 Nd1 O2 Ge3 149.6(9) . .
O1 Nd1 O3 Ge3 -0.6(9) . .
O1 Nd1 O3 Ge4 137.9(7) . .
O1 Nd1 O4 Ge4 -66.8(14) . .
O1 Nd1 O4 Ge5 75.2(13) . .
O1 Nd1 O5 Ge5 -137.2(7) . .
O1 Nd1 O5 Ge6 2.7(9) . .
O1 Nd1 O6 Ge1 -12.0(6) . .
O1 Nd1 O6 Ge6 -152.4(9) . .
O1 Ge1 O6 Nd1 14.9(7) . .
O1 Ge1 O6 Ge6 140.0(12) . .
O1 Ge1 O7 Nd2 -142.5(10) . .
O1 Ge1 O7 Nd4 54.5(11) . .
O1 Ge1 C1 C2 -53(2) . .
O1 Ge2 O2 Nd1 -17.0(7) . .
O1 Ge2 O2 Ge3 -133.9(13) . .
O1 Ge2 O8 Nd3 152.7(9) . .
O1 Ge2 O8 Nd4 -50.0(12) . .
O1 Ge2 C4 C5 -139.7(18) . .
O2 Nd1 Ge1 O1 20.7(8) . .
O2 Nd1 Ge1 O6 179.7(8) . .
O2 Nd1 Ge1 O7 -86.4(7) . .
O2 Nd1 Ge1 C1 106.4(9) . .
O2 Nd1 Ge4 Nd4 112.7(4) . 2
O2 Nd1 Ge4 O3 -22.6(8) . .
O2 Nd1 Ge4 O4 179.7(8) . .
O2 Nd1 Ge4 O10 75.3(7) . .
O2 Nd1 Ge4 C10 -101.1(11) . .
O2 Nd1 Ge5 O4 -54.0(9) . .
O2 Nd1 Ge5 O5 146.7(9) . .
O2 Nd1 Ge5 O11 39.3(8) . .
O2 Nd1 Ge5 C13 -133.8(9) . .
O2 Nd1 Ge6 O5 -145.5(9) . .
O2 Nd1 Ge6 O6 55.6(8) . .
O2 Nd1 Ge6 O12 -50.8(8) . .
O2 Nd1 Ge6 C16 140.3(12) . .
O2 Nd1 O1 Ge1 -155.3(9) . .
O2 Nd1 O1 Ge2 -14.2(6) . .
O2 Nd1 O3 Ge3 14.4(6) . .
O2 Nd1 O3 Ge4 152.9(9) . .
O2 Nd1 O4 Ge4 -0.3(9) . .
O2 Nd1 O4 Ge5 141.7(6) . .
O2 Nd1 O5 Ge5 -67.5(16) . .
O2 Nd1 O5 Ge6 72.4(15) . .
O2 Nd1 O6 Ge1 -0.3(9) . .
O2 Nd1 O6 Ge6 -140.7(6) . .
O2 Ge2 O1 Nd1 18.2(8) . .
O2 Ge2 O1 Ge1 144.5(13) . .
O2 Ge2 O8 Nd3 56.4(11) . .
O2 Ge2 O8 Nd4 -146.3(10) . .
O2 Ge2 C4 C5 -40(2) . .
O2 Ge3 O3 Nd1 -18.3(8) . .
O2 Ge3 O3 Ge4 -144.6(12) . .
O2 Ge3 O9 Nd2 152.1(8) . 2
O2 Ge3 O9 Nd3 -42.6(13) . .
O2 Ge3 C7 C8 -131.5(18) . .
O3 Nd1 Ge1 O1 54.5(9) . .
O3 Nd1 Ge1 O6 -146.5(9) . .
O3 Nd1 Ge1 O7 -52.6(8) . .
O3 Nd1 Ge1 C1 140.2(10) . .
O3 Nd1 Ge4 Nd4 135.3(7) . 2
O3 Nd1 Ge4 O4 -157.6(10) . .
O3 Nd1 Ge4 O10 98.0(9) . .
O3 Nd1 Ge4 C10 -78.5(12) . .
O3 Nd1 Ge5 O4 -21.3(8) . .
O3 Nd1 Ge5 O5 179.5(8) . .
O3 Nd1 Ge5 O11 72.1(7) . .
O3 Nd1 Ge5 C13 -101.0(9) . .
O3 Nd1 Ge6 O5 -57.9(9) . .
O3 Nd1 Ge6 O6 143.1(9) . .
O3 Nd1 Ge6 O12 36.7(8) . .
O3 Nd1 Ge6 C16 -132.1(12) . .
O3 Nd1 O1 Ge1 -140.3(7) . .
O3 Nd1 O1 Ge2 0.8(9) . .
O3 Nd1 O2 Ge2 -149.4(9) . .
O3 Nd1 O2 Ge3 -14.0(6) . .
O3 Nd1 O4 Ge4 12.9(6) . .
O3 Nd1 O4 Ge5 155.0(9) . .
O3 Nd1 O5 Ge5 -0.6(9) . .
O3 Nd1 O5 Ge6 139.3(6) . .
O3 Nd1 O6 Ge1 66.8(15) . .
O3 Nd1 O6 Ge6 -73.6(14) . .
O3 Ge3 O2 Nd1 16.5(7) . .
O3 Ge3 O2 Ge2 133.7(13) . .
O3 Ge3 O9 Nd2 55.1(11) . 2
O3 Ge3 O9 Nd3 -139.6(10) . .
O3 Ge3 C7 C8 -35(2) . .
O3 Ge4 O4 Nd1 -15.6(7) . .
O3 Ge4 O4 Ge5 -144.3(13) . .
O3 Ge4 O10 Nd2 -60.1(11) . 2
O3 Ge4 O10 Nd4 156.9(8) . 2
O3 Ge4 C10 C11 -132.8(16) . .
O4 Nd1 Ge1 O1 141.4(9) . .
O4 Nd1 Ge1 O6 -59.5(9) . .
O4 Nd1 Ge1 O7 34.3(8) . .
O4 Nd1 Ge1 C1 -132.9(10) . .
O4 Nd1 Ge4 Nd4 -67.1(8) . 2
O4 Nd1 Ge4 O3 157.6(10) . .
O4 Nd1 Ge4 O10 -104.4(9) . .
O4 Nd1 Ge4 C10 79.2(12) . .
O4 Nd1 Ge5 O5 -159.2(10) . .
O4 Nd1 Ge5 O11 93.3(9) . .
O4 Nd1 Ge5 C13 -79.7(11) . .
O4 Nd1 Ge6 O5 -23.6(8) . .
O4 Nd1 Ge6 O6 177.4(8) . .
O4 Nd1 Ge6 O12 71.0(7) . .
O4 Nd1 Ge6 C16 -97.8(11) . .
O4 Nd1 O1 Ge1 -74.1(13) . .
O4 Nd1 O1 Ge2 66.9(14) . .
O4 Nd1 O2 Ge2 -135.9(7) . .
O4 Nd1 O2 Ge3 -0.5(9) . .
O4 Nd1 O3 Ge3 -151.3(10) . .
O4 Nd1 O3 Ge4 -12.8(6) . .
O4 Nd1 O5 Ge5 12.1(6) . .
O4 Nd1 O5 Ge6 151.9(9) . .
O4 Nd1 O6 Ge1 137.6(6) . .
O4 Nd1 O6 Ge6 -2.8(8) . .
O4 Ge4 O3 Nd1 15.5(7) . .
O4 Ge4 O3 Ge3 143.2(12) . .
O4 Ge4 O10 Nd2 -152.5(9) . 2
O4 Ge4 O10 Nd4 64.5(10) . 2
O4 Ge4 C10 C11 -38.8(19) . .
O4 Ge5 O5 Nd1 -14.3(7) . .
O4 Ge5 O5 Ge6 -139.5(12) . .
O4 Ge5 O11 Nd3 147.6(8) . 2
O4 Ge5 O11 Nd4 -45.3(12) . 2
O4 Ge5 C13 C14 -138.2(18) . .
O5 Nd1 Ge1 O1 177.7(8) . .
O5 Nd1 Ge1 O6 -23.3(8) . .
O5 Nd1 Ge1 O7 70.6(7) . .
O5 Nd1 Ge1 C1 -96.7(9) . .
O5 Nd1 Ge4 Nd4 -45.0(4) . 2
O5 Nd1 Ge4 O3 179.7(8) . .
O5 Nd1 Ge4 O4 22.1(8) . .
O5 Nd1 Ge4 O10 -82.3(7) . .
O5 Nd1 Ge4 C10 101.3(11) . .
O5 Nd1 Ge5 O4 159.2(10) . .
O5 Nd1 Ge5 O11 -107.4(10) . .
O5 Nd1 Ge5 C13 79.5(11) . .
O5 Nd1 Ge6 O6 -158.9(10) . .
O5 Nd1 Ge6 O12 94.6(9) . .
O5 Nd1 Ge6 C16 -74.2(13) . .
O5 Nd1 O1 Ge1 -2.6(9) . .
O5 Nd1 O1 Ge2 138.5(7) . .
O5 Nd1 O2 Ge2 -69.2(15) . .
O5 Nd1 O2 Ge3 66.2(16) . .
O5 Nd1 O3 Ge3 -138.9(7) . .
O5 Nd1 O3 Ge4 -0.3(9) . .
O5 Nd1 O4 Ge4 -153.8(10) . .
O5 Nd1 O4 Ge5 -11.7(6) . .
O5 Nd1 O6 Ge1 152.7(9) . .
O5 Nd1 O6 Ge6 12.3(6) . .
O5 Ge5 O4 Nd1 14.4(7) . .
O5 Ge5 O4 Ge4 142.8(13) . .
O5 Ge5 O11 Nd3 54.1(11) . 2
O5 Ge5 O11 Nd4 -138.8(10) . 2
O5 Ge5 C13 C14 -45(2) . .
O5 Ge6 O6 Nd1 -14.8(7) . .
O5 Ge6 O6 Ge1 -139.9(12) . .
O5 Ge6 O12 Nd2 150.6(8) . .
O5 Ge6 O12 Nd3 -47.7(12) . 2
O5 Ge6 C16 C17 -138.0(17) . .
O6 Nd1 Ge1 O1 -159.0(10) . .
O6 Nd1 Ge1 O7 93.9(9) . .
O6 Nd1 Ge1 C1 -73.4(11) . .
O6 Nd1 Ge4 Nd4 -8.8(5) . 2
O6 Nd1 Ge4 O3 -144.1(9) . .
O6 Nd1 Ge4 O4 58.2(9) . .
O6 Nd1 Ge4 O10 -46.1(7) . .
O6 Nd1 Ge4 C10 137.4(11) . .
O6 Nd1 Ge5 O4 -176.7(8) . .
O6 Nd1 Ge5 O5 24.0(8) . .
O6 Nd1 Ge5 O11 -83.4(7) . .
O6 Nd1 Ge5 C13 103.5(9) . .
O6 Nd1 Ge6 O5 158.9(10) . .
O6 Nd1 Ge6 O12 -106.4(9) . .
O6 Nd1 Ge6 C16 84.7(12) . .
O6 Nd1 O1 Ge1 12.1(6) . .
O6 Nd1 O1 Ge2 153.2(9) . .
O6 Nd1 O2 Ge2 2.3(9) . .
O6 Nd1 O2 Ge3 137.7(6) . .
O6 Nd1 O3 Ge3 -66.7(15) . .
O6 Nd1 O3 Ge4 71.9(14) . .
O6 Nd1 O4 Ge4 -138.4(7) . .
O6 Nd1 O4 Ge5 3.6(9) . .
O6 Nd1 O5 Ge5 -151.9(9) . .
O6 Nd1 O5 Ge6 -12.0(6) . .
O6 Ge1 O1 Nd1 -14.7(7) . .
O6 Ge1 O1 Ge2 -141.8(13) . .
O6 Ge1 O7 Nd2 -46.5(12) . .
O6 Ge1 O7 Nd4 150.5(8) . .
O6 Ge1 C1 C2 -150.7(18) . .
O6 Ge6 O5 Nd1 14.8(7) . .
O6 Ge6 O5 Ge5 141.1(12) . .
O6 Ge6 O12 Nd2 54.8(11) . .
O6 Ge6 O12 Nd3 -143.5(10) . 2
O6 Ge6 C16 C17 -42(2) . .
O7 Nd2 Nd4 Nd3 -81.0(7) . .
O7 Nd2 Nd4 Ge4 -167.1(7) . 2
O7 Nd2 Nd4 O8 -45.3(8) . .
O7 Nd2 Nd4 O10 -151.4(10) . 2
O7 Nd2 Nd4 O11 -117.6(8) . 2
O7 Nd2 Nd4 O13 31.2(8) . .
O7 Nd2 Nd4 O19 165.2(8) . 2
O7 Nd2 Nd4 O42 102.2(8) . 2_666
O7 Nd2 Nd4 O5W 94.7(18) . .
O7 Nd2 O12 Nd3 139.3(7) . 2
O7 Nd2 O12 Ge6 -55.7(9) . .
O7 Nd2 O23 C18 -168(5) . .
O7 Nd2 O48 C36 -65(2) . .
O7 Nd2 O6W Nd7 -143.7(9) . .
O7 Nd4 O8 Nd3 -141.5(8) . .
O7 Nd4 O8 Ge2 59.6(11) . .
O7 Nd4 O13 C3 111(3) . .
O7 Ge1 O1 Nd1 91.4(8) . .
O7 Ge1 O1 Ge2 -35.7(15) . .
O7 Ge1 O6 Nd1 -100.1(7) . .
O7 Ge1 O6 Ge6 25.1(13) . .
O7 Ge1 C1 C2 89.0(19) . .
O8 Nd3 Nd4 Nd2 78.6(7) . .
O8 Nd3 Nd4 Ge4 140.6(7) . 2
O8 Nd3 Nd4 O7 41.3(8) . .
O8 Nd3 Nd4 O10 113.4(8) . 2
O8 Nd3 Nd4 O11 161.2(10) . 2
O8 Nd3 Nd4 O13 -30.5(9) . .
O8 Nd3 Nd4 O19 -170.1(9) . 2
O8 Nd3 Nd4 O42 -143(6) . 2_666
O8 Nd3 Nd4 O5W -99.6(10) . .
O8 Nd3 O9 Nd2 -137.0(7) . 2
O8 Nd3 O9 Ge3 56.6(11) . .
O8 Nd3 O15 C6 104(3) . .
O8 Nd4 O7 Nd2 137.6(7) . .
O8 Nd4 O7 Ge1 -56.1(9) . .
O8 Nd4 O13 C3 -160(3) . .
O8 Ge2 O1 Nd1 -96.1(8) . .
O8 Ge2 O1 Ge1 30.2(14) . .
O8 Ge2 O2 Nd1 89.4(8) . .
O8 Ge2 O2 Ge3 -27.5(15) . .
O8 Ge2 C4 C5 98(2) . .
O9 Nd2 Nd4 Nd3 36.8(4) 2 .
O9 Nd2 Nd4 Ge4 -49.3(4) 2 2
O9 Nd2 Nd4 O7 117.8(8) 2 .
O9 Nd2 Nd4 O8 72.5(6) 2 .
O9 Nd2 Nd4 O10 -33.6(8) 2 2
O9 Nd2 Nd4 O11 0.2(6) 2 2
O9 Nd2 Nd4 O13 149.0(6) 2 .
O9 Nd2 Nd4 O19 -77.0(6) 2 2
O9 Nd2 Nd4 O42 -140.0(6) 2 2_666
O9 Nd2 Nd4 O5W -147.5(17) 2 .
O9 Nd2 O7 Nd4 -78.4(8) 2 .
O9 Nd2 O7 Ge1 117.6(11) 2 .
O9 Nd2 O12 Nd3 11.5(6) 2 2
O9 Nd2 O12 Ge6 176.5(11) 2 .
O9 Nd2 O23 C18 74(5) 2 .
O9 Nd2 O48 C36 149(2) 2 .
O9 Nd2 O6W Nd7 14.7(16) 2 .
O9 Nd3 Nd4 Nd2 36.8(4) . .
O9 Nd3 Nd4 Ge4 98.8(4) . 2
O9 Nd3 Nd4 O7 -0.5(6) . .
O9 Nd3 Nd4 O8 -41.8(8) . .
O9 Nd3 Nd4 O10 71.6(6) . 2
O9 Nd3 Nd4 O11 119.4(8) . 2
O9 Nd3 Nd4 O13 -72.3(6) . .
O9 Nd3 Nd4 O19 148.1(6) . 2
O9 Nd3 Nd4 O42 175(6) . 2_666
O9 Nd3 Nd4 O5W -141.4(8) . .
O9 Nd3 O8 Nd4 140.2(8) . .
O9 Nd3 O8 Ge2 -59.2(10) . .
O9 Nd3 O15 C6 -170(3) . .
O9 Ge3 O2 Nd1 -98.9(8) . .
O9 Ge3 O2 Ge2 18.3(15) . .
O9 Ge3 O3 Nd1 91.3(9) . .
O9 Ge3 O3 Ge4 -35.0(15) . .
O9 Ge3 C7 C8 98(2) . .
O10 Nd2 Nd4 Nd3 70.3(7) 2 .
O10 Nd2 Nd4 Ge4 -15.7(7) 2 2
O10 Nd2 Nd4 O7 151.4(10) 2 .
O10 Nd2 Nd4 O8 106.0(8) 2 .
O10 Nd2 Nd4 O11 33.8(8) 2 2
O10 Nd2 Nd4 O13 -177.4(8) 2 .
O10 Nd2 Nd4 O19 -43.5(8) 2 2
O10 Nd2 Nd4 O42 -106.4(8) 2 2_666
O10 Nd2 Nd4 O5W -114.0(18) 2 .
O10 Nd2 O7 Nd4 -17.3(6) 2 .
O10 Nd2 O7 Ge1 178.7(13) 2 .
O10 Nd2 O12 Nd3 78.6(8) 2 2
O10 Nd2 O12 Ge6 -116.3(9) 2 .
O10 Nd2 O23 C18 -150(4) 2 .
O10 Nd2 O48 C36 82(2) 2 .
O10 Nd2 O6W Nd7 -77.6(9) 2 .
O10 Nd4 O7 Nd2 17.6(6) 2 .
O10 Nd4 O7 Ge1 -176.1(11) 2 .
O10 Nd4 O8 Nd3 -78.7(8) 2 .
O10 Nd4 O8 Ge2 122.5(10) 2 .
O10 Nd4 O13 C3 90(3) 2 .
O10 Ge4 O3 Nd1 -93.7(8) . .
O10 Ge4 O3 Ge3 33.9(13) . .
O10 Ge4 O4 Nd1 89.1(8) . .
O10 Ge4 O4 Ge5 -39.5(14) . .
O10 Ge4 C10 C11 98.7(18) . .
O11 Nd3 Nd4 Nd2 -82.6(7) 2 .
O11 Nd3 Nd4 Ge4 -20.5(7) 2 2
O11 Nd3 Nd4 O7 -119.9(8) 2 .
O11 Nd3 Nd4 O8 -161.2(10) 2 .
O11 Nd3 Nd4 O10 -47.7(8) 2 2
O11 Nd3 Nd4 O13 168.3(8) 2 .
O11 Nd3 Nd4 O19 28.7(8) 2 2
O11 Nd3 Nd4 O42 56(6) 2 2_666
O11 Nd3 Nd4 O5W 99.2(10) 2 .
O11 Nd3 O8 Nd4 11.3(6) 2 .
O11 Nd3 O8 Ge2 171.9(11) 2 .
O11 Nd3 O9 Nd2 -78.8(8) 2 2
O11 Nd3 O9 Ge3 114.7(11) 2 .
O11 Nd3 O15 C6 71(3) 2 .
O11 Nd4 O7 Nd2 80.3(8) 2 .
O11 Nd4 O7 Ge1 -113.4(9) 2 .
O11 Nd4 O8 Nd3 -11.3(6) 2 .
O11 Nd4 O8 Ge2 -170.2(13) 2 .
O11 Nd4 O13 C3 -133(3) 2 .
O11 Ge5 O4 Nd1 -101.0(8) . .
O11 Ge5 O4 Ge4 27.4(14) . .
O11 Ge5 O5 Nd1 91.4(9) . .
O11 Ge5 O5 Ge6 -33.8(14) . .
O11 Ge5 C13 C14 96(2) . .
O12 Nd2 Nd4 Nd3 -37.0(4) . .
O12 Nd2 Nd4 Ge4 -123.1(4) . 2
O12 Nd2 Nd4 O7 44.0(8) . .
O12 Nd2 Nd4 O8 -1.3(6) . .
O12 Nd2 Nd4 O10 -107.4(8) . 2
O12 Nd2 Nd4 O11 -73.6(6) . 2
O12 Nd2 Nd4 O13 75.2(6) . .
O12 Nd2 Nd4 O19 -150.8(6) . 2
O12 Nd2 Nd4 O42 146.2(6) . 2_666
O12 Nd2 Nd4 O5W 138.7(17) . .
O12 Nd2 O7 Nd4 -138.5(7) . .
O12 Nd2 O7 Ge1 57.5(11) . .
O12 Nd2 O23 C18 104(5) . .
O12 Nd2 O48 C36 -142(2) . .
O12 Nd2 O6W Nd7 137.8(8) . .
O12 Nd3 Nd4 Nd2 -36.2(4) 2 .
O12 Nd3 Nd4 Ge4 25.8(4) 2 2
O12 Nd3 Nd4 O7 -73.5(6) 2 .
O12 Nd3 Nd4 O8 -114.8(8) 2 .
O12 Nd3 Nd4 O10 -1.4(6) 2 2
O12 Nd3 Nd4 O11 46.4(8) 2 2
O12 Nd3 Nd4 O13 -145.4(6) 2 .
O12 Nd3 Nd4 O19 75.1(6) 2 2
O12 Nd3 Nd4 O42 102(6) 2 2_666
O12 Nd3 Nd4 O5W 145.6(8) 2 .
O12 Nd3 O8 Nd4 80.2(8) 2 .
O12 Nd3 O8 Ge2 -119.2(9) 2 .
O12 Nd3 O9 Nd2 -11.5(6) 2 2
O12 Nd3 O9 Ge3 -177.9(13) 2 .
O12 Nd3 O15 C6 -144(3) 2 .
O12 Ge6 O5 Nd1 -99.7(8) . .
O12 Ge6 O5 Ge5 26.5(13) . .
O12 Ge6 O6 Nd1 91.7(8) . .
O12 Ge6 O6 Ge1 -33.4(14) . .
O12 Ge6 C16 C17 100.3(19) . .
O13 Nd4 O7 Nd2 -146.5(8) . .
O13 Nd4 O7 Ge1 19.8(8) . .
O13 Nd4 O8 Nd3 149.3(8) . .
O13 Nd4 O8 Ge2 -9.6(10) . .
O15 Nd3 Nd4 Nd2 113.8(4) . .
O15 Nd3 Nd4 Ge4 175.8(4) . 2
O15 Nd3 Nd4 O7 76.5(6) . .
O15 Nd3 Nd4 O8 35.2(9) . .
O15 Nd3 Nd4 O10 148.6(6) . 2
O15 Nd3 Nd4 O11 -163.7(8) . 2
O15 Nd3 Nd4 O13 4.6(6) . .
O15 Nd3 Nd4 O19 -135.0(6) . 2
O15 Nd3 Nd4 O42 -108(6) . 2_666
O15 Nd3 Nd4 O5W -64.4(8) . .
O15 Nd3 O8 Nd4 -143.0(9) . .
O15 Nd3 O8 Ge2 17.6(9) . .
O15 Nd3 O9 Nd2 150.8(8) . 2
O15 Nd3 O9 Ge3 -15.6(10) . .
O17 Nd2 Nd4 Nd3 109.3(4) 2 .
O17 Nd2 Nd4 Ge4 23.3(4) 2 2
O17 Nd2 Nd4 O7 -169.7(8) 2 .
O17 Nd2 Nd4 O8 145.0(6) 2 .
O17 Nd2 Nd4 O10 39.0(8) 2 2
O17 Nd2 Nd4 O11 72.7(6) 2 2
O17 Nd2 Nd4 O13 -138.4(6) 2 .
O17 Nd2 Nd4 O19 -4.5(6) 2 2
O17 Nd2 Nd4 O42 -67.5(6) 2 2_666
O17 Nd2 Nd4 O5W -75.0(17) 2 .
O17 Nd2 O7 Nd4 14.0(11) 2 .
O17 Nd2 O7 Ge1 -150.0(10) 2 .
O17 Nd2 O12 Nd3 -11.2(11) 2 2
O17 Nd2 O12 Ge6 153.8(8) 2 .
O17 Nd2 O23 C18 -33(5) 2 .
O17 Nd2 O48 C36 78(2) 2 .
O17 Nd2 O6W Nd7 -9.2(8) 2 .
O18 Nd7 Nd8 Nd6 135.2(17) 2 .
O18 Nd7 Nd8 O32 170.9(18) 2 2_666
O18 Nd7 Nd8 O33 -143.3(19) 2 2_666
O18 Nd7 Nd8 O35 99.0(18) 2 .
O18 Nd7 Nd8 O36 53.6(19) 2 .
O18 Nd7 Nd8 O39 -118.5(18) 2 2_666
O18 Nd7 Nd8 O45 23.0(18) 2 .
O18 Nd7 Nd8 O13W -51(2) 2 .
O18 Nd7 Nd8 O14W -50.9(18) 2 .
O18 Nd7 O31 Nd6 82.7(7) 2 2_666
O18 Nd7 O31 Ge7 -77.8(12) 2 .
O18 Nd7 O36 Nd8 -164.3(6) 2 .
O18 Nd7 O36 Ge12 4.9(15) 2 .
O18 Nd7 O47 C36 -97(3) 2 .
O18 Nd7 O6W Nd2 6.2(9) 2 .
O19 Nd4 O7 Nd2 -20.3(11) 2 .
O19 Nd4 O7 Ge1 146.0(8) 2 .
O19 Nd4 O8 Nd3 14.4(13) 2 .
O19 Nd4 O8 Ge2 -144.5(10) 2 .
O19 Nd4 O13 C3 -18(3) 2 .
O21 Nd3 Nd4 Nd2 -110.4(4) 2 .
O21 Nd3 Nd4 Ge4 -48.4(4) 2 2
O21 Nd3 Nd4 O7 -147.7(6) 2 .
O21 Nd3 Nd4 O8 171.0(9) 2 .
O21 Nd3 Nd4 O10 -75.5(6) 2 2
O21 Nd3 Nd4 O11 -27.8(8) 2 2
O21 Nd3 Nd4 O13 140.5(6) 2 .
O21 Nd3 Nd4 O19 0.9(6) 2 2
O21 Nd3 Nd4 O42 28(6) 2 2_666
O21 Nd3 Nd4 O5W 71.4(8) 2 .
O21 Nd3 O8 Nd4 -12.2(12) 2 .
O21 Nd3 O8 Ge2 148.3(8) 2 .
O21 Nd3 O9 Nd2 13.0(12) 2 2
O21 Nd3 O9 Ge3 -153.5(9) 2 .
O21 Nd3 O15 C6 -28(3) 2 .
O23 Nd2 Nd4 Nd3 -110.6(4) . .
O23 Nd2 Nd4 Ge4 163.4(4) . 2
O23 Nd2 Nd4 O7 -29.6(8) . .
O23 Nd2 Nd4 O8 -74.9(6) . .
O23 Nd2 Nd4 O10 179.1(8) . 2
O23 Nd2 Nd4 O11 -147.2(6) . 2
O23 Nd2 Nd4 O13 1.7(6) . .
O23 Nd2 Nd4 O19 135.6(6) . 2
O23 Nd2 Nd4 O42 72.6(6) . 2_666
O23 Nd2 Nd4 O5W 65.1(17) . .
O23 Nd2 O7 Nd4 150.1(8) . .
O23 Nd2 O7 Ge1 -14.0(11) . .
O23 Nd2 O12 Nd3 -145.6(8) . 2
O23 Nd2 O12 Ge6 19.4(8) . .
O23 Nd2 O48 C36 -73(2) . .
O23 Nd2 O6W Nd7 144.0(11) . .
O25 Nd5 Ge7 Nd6 -66.2(8) . 2_666
O25 Nd5 Ge7 O30 161.1(11) . .
O25 Nd5 Ge7 O31 -106.9(10) . .
O25 Nd5 Ge7 O37 -15.5(9) . .
O25 Nd5 Ge7 C19 86.6(12) . .
O25 Nd5 Ge8 O26 -163.8(11) . .
O25 Nd5 Ge8 O32 92.9(10) . .
O25 Nd5 Ge8 O39 -177.7(9) . .
O25 Nd5 Ge8 C22 -75.9(12) . .
O25 Nd5 Ge11 O28 -131.4(9) . .
O25 Nd5 Ge11 O29 63.1(9) . .
O25 Nd5 Ge11 O35 -35.5(8) . .
O25 Nd5 Ge11 C31 146.1(9) . .
O25 Nd5 O26 Ge8 9.2(6) . .
O25 Nd5 O26 Ge9 154.1(10) . .
O25 Nd5 O28 Ge10 -63.4(13) . .
O25 Nd5 O28 Ge11 81.0(12) . .
O25 Nd5 O29 Ge11 -133.3(7) . .
O25 Nd5 O29 Ge12 12.7(10) . .
O25 Nd5 O30 Ge7 -10.9(6) . .
O25 Nd5 O30 Ge12 -147.8(10) . .
O25 Ge7 O30 Nd5 13.1(8) . .
O25 Ge7 O30 Ge12 134.0(13) . .
O25 Ge7 O31 Nd6 55.0(10) . 2_666
O25 Ge7 O31 Nd7 -145.2(10) . .
O25 Ge7 O37 Nd6 -100.3(7) . 2_666
O25 Ge7 O37 C21 109(2) . .
O25 Ge7 C19 C20 -52(2) . .
O25 Ge8 O26 Nd5 -11.1(8) . .
O25 Ge8 O26 Ge9 -148.4(13) . .
O25 Ge8 O32 Nd6 -51.3(12) . 2_666
O25 Ge8 O32 Nd8 154.9(8) . 2_666
O25 Ge8 O39 Nd8 -99(3) . 2_666
O25 Ge8 O39 C24 109(4) . .
O25 Ge8 C22 C23 -150.0(19) . .
O26 Nd5 Ge7 Nd6 -42.9(4) . 2_666
O26 Nd5 Ge7 O25 23.3(9) . .
O26 Nd5 Ge7 O30 -175.6(9) . .
O26 Nd5 Ge7 O31 -83.6(7) . .
O26 Nd5 Ge7 O37 7.8(6) . .
O26 Nd5 Ge7 C19 109.9(10) . .
O26 Nd5 Ge8 O25 163.8(11) . .
O26 Nd5 Ge8 O32 -103.3(10) . .
O26 Nd5 Ge8 O39 -13.9(9) . .
O26 Nd5 Ge8 C22 87.9(12) . .
O26 Nd5 Ge11 O28 -53.7(9) . .
O26 Nd5 Ge11 O29 140.8(9) . .
O26 Nd5 Ge11 O35 42.2(7) . .
O26 Nd5 Ge11 C31 -136.3(9) . .
O26 Nd5 O25 Ge7 -152.4(10) . .
O26 Nd5 O25 Ge8 -9.3(6) . .
O26 Nd5 O28 Ge10 -6.8(9) . .
O26 Nd5 O28 Ge11 137.6(7) . .
O26 Nd5 O29 Ge11 -64.0(12) . .
O26 Nd5 O29 Ge12 82.0(12) . .
O26 Nd5 O30 Ge7 4.8(10) . .
O26 Nd5 O30 Ge12 -132.1(7) . .
O26 Ge8 O25 Nd5 11.4(8) . .
O26 Ge8 O25 Ge7 141.3(13) . .
O26 Ge8 O32 Nd6 -143.6(10) . 2_666
O26 Ge8 O32 Nd8 62.7(10) . 2_666
O26 Ge8 O39 Nd8 -101.1(7) . 2_666
O26 Ge8 O39 C24 106(2) . .
O26 Ge8 C22 C23 -53(2) . .
O26 Ge9 O27 Ge10 -120.7(15) . .
O26 Ge9 O33 Nd7 146.9(9) . 2_666
O26 Ge9 O33 Nd8 -48.3(12) . 2_666
O26 Ge9 C25 C26 -139.7(17) . .
O27 Ge9 O26 Nd5 14.8(8) . .
O27 Ge9 O26 Ge8 149.5(12) . .
O27 Ge9 O33 Nd7 45.9(12) . 2_666
O27 Ge9 O33 Nd8 -149.3(9) . 2_666
O27 Ge9 C25 C26 -40(2) . .
O27 Ge10 O28 Nd5 -16.3(8) . .
O27 Ge10 O28 Ge11 -150.3(12) . .
O27 Ge10 O34 Nd6 154.9(8) . .
O27 Ge10 O34 Nd7 -42.3(12) . 2_666
O27 Ge10 C28 C29 -139.9(18) . .
O28 Nd5 Ge7 Nd6 64.8(5) . 2_666
O28 Nd5 Ge7 O25 131.0(10) . .
O28 Nd5 Ge7 O30 -67.9(9) . .
O28 Nd5 Ge7 O31 24.1(8) . .
O28 Nd5 Ge7 O37 115.5(7) . .
O28 Nd5 Ge7 C19 -142.4(11) . .
O28 Nd5 Ge8 O25 -142.4(9) . .
O28 Nd5 Ge8 O26 53.8(9) . .
O28 Nd5 Ge8 O32 -49.5(8) . .
O28 Nd5 Ge8 O39 40.0(7) . .
O28 Nd5 Ge8 C22 141.7(10) . .
O28 Nd5 Ge11 O29 -165.5(10) . .
O28 Nd5 Ge11 O35 95.9(10) . .
O28 Nd5 Ge11 C31 -82.6(11) . .
O28 Nd5 O25 Ge7 -81.8(12) . .
O28 Nd5 O25 Ge8 61.3(13) . .
O28 Nd5 O26 Ge8 -137.2(7) . .
O28 Nd5 O26 Ge9 7.7(9) . .
O28 Nd5 O29 Ge11 8.4(6) . .
O28 Nd5 O29 Ge12 154.4(10) . .
O28 Nd5 O30 Ge7 130.2(7) . .
O28 Nd5 O30 Ge12 -6.7(9) . .
O28 Ge10 O27 Ge9 121.4(14) . .
O28 Ge10 O34 Nd6 55.6(10) . .
O28 Ge10 O34 Nd7 -141.6(10) . 2_666
O28 Ge10 C28 C29 -40(2) . .
O28 Ge11 O29 Nd5 -10.2(7) . .
O28 Ge11 O29 Ge12 -141.6(14) . .
O28 Ge11 O35 Nd6 -51.8(11) . .
O28 Ge11 O35 Nd8 152.0(9) . .
O28 Ge11 C31 C32 -143.8(16) . .
O29 Nd5 Ge7 Nd6 103.9(4) . 2_666
O29 Nd5 Ge7 O25 170.1(9) . .
O29 Nd5 Ge7 O30 -28.8(9) . .
O29 Nd5 Ge7 O31 63.1(7) . .
O29 Nd5 Ge7 O37 154.6(7) . .
O29 Nd5 Ge7 C19 -103.3(10) . .
O29 Nd5 Ge8 O25 -64.0(9) . .
O29 Nd5 Ge8 O26 132.2(9) . .
O29 Nd5 Ge8 O32 28.8(8) . .
O29 Nd5 Ge8 O39 118.3(7) . .
O29 Nd5 Ge8 C22 -140.0(11) . .
O29 Nd5 Ge11 O28 165.5(11) . .
O29 Nd5 Ge11 O35 -98.6(9) . .
O29 Nd5 Ge11 C31 83.0(10) . .
O29 Nd5 O25 Ge7 -10.9(10) . .
O29 Nd5 O25 Ge8 132.2(7) . .
O29 Nd5 O26 Ge8 -78.8(12) . .
O29 Nd5 O26 Ge9 66.1(13) . .
O29 Nd5 O28 Ge10 -152.6(10) . .
O29 Nd5 O28 Ge11 -8.3(6) . .
O29 Nd5 O30 Ge7 145.9(10) . .
O29 Nd5 O30 Ge12 9.0(6) . .
O29 Ge11 O28 Nd5 10.3(7) . .
O29 Ge11 O28 Ge10 147.4(12) . .
O29 Ge11 O35 Nd6 -148.4(9) . .
O29 Ge11 O35 Nd8 55.5(11) . .
O29 Ge11 C31 C32 -45(2) . .
O29 Ge12 O30 Nd5 -11.0(8) . .
O29 Ge12 O30 Ge7 -131.5(13) . .
O29 Ge12 O36 Nd7 148.6(9) . .
O29 Ge12 O36 Nd8 -44.2(12) . .
O29 Ge12 C34 C35 -151.3(19) . .
O30 Nd5 Ge7 Nd6 132.8(8) . 2_666
O30 Nd5 Ge7 O25 -161.1(11) . .
O30 Nd5 Ge7 O31 92.0(10) . .
O30 Nd5 Ge7 O37 -176.5(9) . .
O30 Nd5 Ge7 C19 -74.5(12) . .
O30 Nd5 Ge8 O25 -22.2(9) . .
O30 Nd5 Ge8 O26 174.0(9) . .
O30 Nd5 Ge8 O32 70.6(7) . .
O30 Nd5 Ge8 O39 160.1(6) . .
O30 Nd5 Ge8 C22 -98.2(10) . .
O30 Nd5 Ge11 O28 -173.4(8) . .
O30 Nd5 Ge11 O29 21.0(8) . .
O30 Nd5 Ge11 O35 -77.6(7) . .
O30 Nd5 Ge11 C31 104.0(8) . .
O30 Nd5 O25 Ge7 10.9(6) . .
O30 Nd5 O25 Ge8 154.0(10) . .
O30 Nd5 O26 Ge8 -6.7(10) . .
O30 Nd5 O26 Ge9 138.2(8) . .
O30 Nd5 O28 Ge10 -137.0(7) . .
O30 Nd5 O28 Ge11 7.3(9) . .
O30 Nd5 O29 Ge11 -155.3(9) . .
O30 Nd5 O29 Ge12 -9.2(6) . .
O30 Ge7 O25 Nd5 -13.6(8) . .
O30 Ge7 O25 Ge8 -144.1(13) . .
O30 Ge7 O31 Nd6 150.8(8) . 2_666
O30 Ge7 O31 Nd7 -49.4(13) . .
O30 Ge7 O37 Nd6 -103(4) . 2_666
O30 Ge7 O37 C21 107(4) . .
O30 Ge7 C19 C20 -150(2) . .
O30 Ge12 O29 Nd5 11.2(8) . .
O30 Ge12 O29 Ge11 142.0(14) . .
O30 Ge12 O36 Nd7 52.1(12) . .
O30 Ge12 O36 Nd8 -140.7(10) . .
O30 Ge12 C34 C35 -56(2) . .
O31 Nd6 Nd8 Nd7 38.8(4) 2_666 .
O31 Nd6 Nd8 O32 -39.9(8) 2_666 2_666
O31 Nd6 Nd8 O33 0.4(6) 2_666 2_666
O31 Nd6 Nd8 O35 115.4(8) 2_666 .
O31 Nd6 Nd8 O36 75.4(6) 2_666 .
O31 Nd6 Nd8 O39 -72.2(6) 2_666 2_666
O31 Nd6 Nd8 O45 155.0(6) 2_666 .
O31 Nd6 Nd8 O13W -139.4(6) 2_666 .
O31 Nd6 Nd8 O14W -127.2(11) 2_666 .
O31 Nd6 Ge10 O27 -39.6(10) 2_666 .
O31 Nd6 Ge10 O28 -133.4(7) 2_666 .
O31 Nd6 Ge10 O34 -2.2(10) 2_666 .
O31 Nd6 Ge10 C28 112.9(10) 2_666 .
O31 Nd6 O34 Nd7 11.6(6) 2_666 2_666
O31 Nd6 O34 Ge10 177.7(10) 2_666 .
O31 Nd6 O35 Nd8 -82.4(8) 2_666 .
O31 Nd6 O35 Ge11 119.1(9) 2_666 .
O31 Nd6 O43 C30 88(3) 2_666 .
O31 Nd7 Nd8 Nd6 34.9(4) . .
O31 Nd7 Nd8 O32 70.6(6) . 2_666
O31 Nd7 Nd8 O33 116.4(8) . 2_666
O31 Nd7 Nd8 O35 -1.3(6) . .
O31 Nd7 Nd8 O36 -46.7(8) . .
O31 Nd7 Nd8 O39 141.2(6) . 2_666
O31 Nd7 Nd8 O45 -77.3(6) . .
O31 Nd7 Nd8 O13W -151.3(15) . .
O31 Nd7 Nd8 O14W -151.2(6) . .
O31 Nd7 O36 Nd8 134.4(8) . .
O31 Nd7 O36 Ge12 -56.5(10) . .
O31 Nd7 O47 C36 -177(3) . .
O31 Nd7 O6W Nd2 -60.8(13) . .
O31 Ge7 O25 Nd5 91.4(9) . .
O31 Ge7 O25 Ge8 -39.1(15) . .
O31 Ge7 O30 Nd5 -102.3(8) . .
O31 Ge7 O30 Ge12 18.6(15) . .
O31 Ge7 O37 Nd6 16.9(7) . 2_666
O31 Ge7 O37 C21 -133(2) . .
O31 Ge7 C19 C20 92(2) . .
O32 Nd6 Nd8 Nd7 78.7(7) 2_666 .
O32 Nd6 Nd8 O33 40.3(8) 2_666 2_666
O32 Nd6 Nd8 O35 155.3(10) 2_666 .
O32 Nd6 Nd8 O36 115.3(8) 2_666 .
O32 Nd6 Nd8 O39 -32.3(8) 2_666 2_666
O32 Nd6 Nd8 O45 -165.1(8) 2_666 .
O32 Nd6 Nd8 O13W -99.5(8) 2_666 .
O32 Nd6 Nd8 O14W -87.3(12) 2_666 .
O32 Nd6 Ge10 O27 48.2(10) 2_666 .
O32 Nd6 Ge10 O28 -45.6(7) 2_666 .
O32 Nd6 Ge10 O34 85.6(10) 2_666 .
O32 Nd6 Ge10 C28 -159.3(10) 2_666 .
O32 Nd6 O34 Nd7 80.3(8) 2_666 2_666
O32 Nd6 O34 Ge10 -113.6(9) 2_666 .
O32 Nd6 O35 Nd8 -15.0(6) 2_666 .
O32 Nd6 O35 Ge11 -173.5(12) 2_666 .
O32 Nd6 O43 C30 -129(3) 2_666 .
O32 Nd8 O35 Nd6 14.6(6) 2_666 .
O32 Nd8 O35 Ge11 173.7(11) 2_666 .
O32 Nd8 O36 Nd7 -78.5(8) 2_666 .
O32 Nd8 O36 Ge12 113.0(10) 2_666 .
O32 Nd8 O45 C33 58(3) 2_666 .
O32 Ge8 O25 Nd5 -98.8(8) . .
O32 Ge8 O25 Ge7 31.1(14) . .
O32 Ge8 O26 Nd5 92.0(8) . .
O32 Ge8 O26 Ge9 -45.3(14) . .
O32 Ge8 O39 Nd8 11.4(7) . 2_666
O32 Ge8 O39 C24 -141(2) . .
O32 Ge8 C22 C23 88(2) . .
O33 Nd7 Nd8 Nd6 -81.5(7) 2_666 .
O33 Nd7 Nd8 O32 -45.8(8) 2_666 2_666
O33 Nd7 Nd8 O35 -117.7(8) 2_666 .
O33 Nd7 Nd8 O36 -163.1(10) 2_666 .
O33 Nd7 Nd8 O39 24.8(8) 2_666 2_666
O33 Nd7 Nd8 O45 166.3(8) 2_666 .
O33 Nd7 Nd8 O13W 92.3(16) 2_666 .
O33 Nd7 Nd8 O14W 92.4(8) 2_666 .
O33 Nd7 O31 Nd6 -74.6(8) 2_666 2_666
O33 Nd7 O31 Ge7 125.0(11) 2_666 .
O33 Nd7 O36 Nd8 10.5(6) 2_666 .
O33 Nd7 O36 Ge12 179.6(12) 2_666 .
O33 Nd7 O47 C36 64(3) 2_666 .
O33 Nd7 O6W Nd2 160.0(9) 2_666 .
O33 Nd8 O35 Nd6 81.5(8) 2_666 .
O33 Nd8 O35 Ge11 -119.5(9) 2_666 .
O33 Nd8 O36 Nd7 -10.6(6) 2_666 .
O33 Nd8 O36 Ge12 -179.0(12) 2_666 .
O33 Nd8 O45 C33 -151(2) 2_666 .
O33 Ge9 O26 Nd5 -99.3(8) . .
O33 Ge9 O26 Ge8 35.4(14) . .
O33 Ge9 O27 Ge10 -8.8(17) . .
O33 Ge9 C25 C26 89.7(19) . .
O34 Nd6 Nd8 Nd7 -37.1(4) . .
O34 Nd6 Nd8 O32 -115.9(8) . 2_666
O34 Nd6 Nd8 O33 -75.5(6) . 2_666
O34 Nd6 Nd8 O35 39.5(8) . .
O34 Nd6 Nd8 O36 -0.6(6) . .
O34 Nd6 Nd8 O39 -148.1(6) . 2_666
O34 Nd6 Nd8 O45 79.0(6) . .
O34 Nd6 Nd8 O13W 144.6(6) . .
O34 Nd6 Nd8 O14W 156.9(11) . .
O34 Nd6 Ge10 O27 -37.4(13) . .
O34 Nd6 Ge10 O28 -131.2(10) . .
O34 Nd6 Ge10 C28 115.1(12) . .
O34 Nd6 O35 Nd8 -144.0(7) . .
O34 Nd6 O35 Ge11 57.5(10) . .
O34 Nd6 O43 C30 113(3) . .
O34 Nd7 Nd8 Nd6 -36.1(4) 2_666 .
O34 Nd7 Nd8 O32 -0.5(6) 2_666 2_666
O34 Nd7 Nd8 O33 45.4(8) 2_666 2_666
O34 Nd7 Nd8 O35 -72.3(6) 2_666 .
O34 Nd7 Nd8 O36 -117.7(8) 2_666 .
O34 Nd7 Nd8 O39 70.1(6) 2_666 2_666
O34 Nd7 Nd8 O45 -148.4(6) 2_666 .
O34 Nd7 Nd8 O13W 137.6(15) 2_666 .
O34 Nd7 Nd8 O14W 137.7(6) 2_666 .
O34 Nd7 O31 Nd6 -11.5(6) 2_666 2_666
O34 Nd7 O31 Ge7 -171.9(13) 2_666 .
O34 Nd7 O36 Nd8 75.6(8) 2_666 .
O34 Nd7 O36 Ge12 -115.2(10) 2_666 .
O34 Nd7 O47 C36 -153(3) 2_666 .
O34 Nd7 O6W Nd2 93.2(12) 2_666 .
O34 Ge10 O27 Ge9 5.5(16) . .
O34 Ge10 O28 Nd5 92.3(9) . .
O34 Ge10 O28 Ge11 -41.7(14) . .
O34 Ge10 C28 C29 97(2) . .
O35 Nd6 Nd8 Nd7 -76.6(7) . .
O35 Nd6 Nd8 O32 -155.3(10) . 2_666
O35 Nd6 Nd8 O33 -115.0(8) . 2_666
O35 Nd6 Nd8 O36 -40.1(8) . .
O35 Nd6 Nd8 O39 172.4(8) . 2_666
O35 Nd6 Nd8 O45 39.6(8) . .
O35 Nd6 Nd8 O13W 105.2(8) . .
O35 Nd6 Nd8 O14W 117.4(12) . .
O35 Nd6 Ge10 O27 83.3(10) . .
O35 Nd6 Ge10 O28 -10.5(6) . .
O35 Nd6 Ge10 O34 120.7(10) . .
O35 Nd6 Ge10 C28 -124.2(9) . .
O35 Nd6 O34 Nd7 139.3(7) . 2_666
O35 Nd6 O34 Ge10 -54.6(9) . .
O35 Nd6 O43 C30 -155(3) . .
O35 Nd8 O36 Nd7 -136.9(7) . .
O35 Nd8 O36 Ge12 54.7(11) . .
O35 Nd8 O45 C33 92(3) . .
O35 Ge11 O28 Nd5 -99.9(8) . .
O35 Ge11 O28 Ge10 37.1(13) . .
O35 Ge11 O29 Nd5 98.3(8) . .
O35 Ge11 O29 Ge12 -33.1(16) . .
O35 Ge11 C31 C32 86.9(18) . .
O36 Nd7 Nd8 Nd6 81.7(7) . .
O36 Nd7 Nd8 O32 117.3(8) . 2_666
O36 Nd7 Nd8 O33 163.1(10) . 2_666
O36 Nd7 Nd8 O35 45.4(8) . .
O36 Nd7 Nd8 O39 -172.1(8) . 2_666
O36 Nd7 Nd8 O45 -30.6(8) . .
O36 Nd7 Nd8 O13W -104.6(16) . .
O36 Nd7 Nd8 O14W -104.5(9) . .
O36 Nd7 O31 Nd6 -137.0(8) . 2_666
O36 Nd7 O31 Ge7 62.5(12) . .
O36 Nd7 O47 C36 100(3) . .
O36 Nd7 O6W Nd2 -128.6(9) . .
O36 Nd8 O35 Nd6 142.7(7) . .
O36 Nd8 O35 Ge11 -58.2(9) . .
O36 Nd8 O45 C33 178(3) . .
O36 Ge12 O29 Nd5 -104.0(8) . .
O36 Ge12 O29 Ge11 26.7(16) . .
O36 Ge12 O30 Nd5 96.7(8) . .
O36 Ge12 O30 Ge7 -23.8(16) . .
O36 Ge12 C34 C35 84(2) . .
O37 Nd6 Nd8 Nd7 110.3(4) 2_666 .
O37 Nd6 Nd8 O32 31.6(8) 2_666 2_666
O37 Nd6 Nd8 O33 71.9(6) 2_666 2_666
O37 Nd6 Nd8 O35 -173.1(8) 2_666 .
O37 Nd6 Nd8 O36 146.8(6) 2_666 .
O37 Nd6 Nd8 O39 -0.7(6) 2_666 2_666
O37 Nd6 Nd8 O45 -133.6(6) 2_666 .
O37 Nd6 Nd8 O13W -67.9(6) 2_666 .
O37 Nd6 Nd8 O14W -55.7(11) 2_666 .
O37 Nd6 Ge10 O27 -91.9(12) 2_666 .
O37 Nd6 Ge10 O28 174.4(10) 2_666 .
O37 Nd6 Ge10 O34 -54.4(12) 2_666 .
O37 Nd6 Ge10 C28 60.6(12) 2_666 .
O37 Nd6 O34 Nd7 -18.2(10) 2_666 2_666
O37 Nd6 O34 Ge10 148.0(8) 2_666 .
O37 Nd6 O35 Nd8 10.1(12) 2_666 .
O37 Nd6 O35 Ge11 -148.4(9) 2_666 .
O37 Nd6 O43 C30 -15(3) 2_666 .
O37 Ge7 O25 Nd5 166.9(8) . .
O37 Ge7 O25 Ge8 36.4(12) . .
O37 Ge7 O30 Nd5 16(4) . .
O37 Ge7 O30 Ge12 137(3) . .
O37 Ge7 O31 Nd6 -19.7(8) . 2_666
O37 Ge7 O31 Nd7 140.1(12) . .
O37 Ge7 C19 C20 20(2) . .
O39 Nd8 O35 Nd6 -10.0(10) 2_666 .
O39 Nd8 O35 Ge11 149.1(8) 2_666 .
O39 Nd8 O36 Nd7 11.5(12) 2_666 .
O39 Nd8 O36 Ge12 -156.9(9) 2_666 .
O39 Nd8 O45 C33 -37(3) 2_666 .
O39 Ge8 O25 Nd5 9(4) . .
O39 Ge8 O25 Ge7 139(3) . .
O39 Ge8 O26 Nd5 168.4(8) . .
O39 Ge8 O26 Ge9 31.1(11) . .
O39 Ge8 O32 Nd6 140.7(11) . 2_666
O39 Ge8 O32 Nd8 -13.1(8) . 2_666
O39 Ge8 C22 C23 19(2) . .
O41 Nd7 Nd8 Nd6 -118.5(4) 2_666 .
O41 Nd7 Nd8 O32 -82.9(6) 2_666 2_666
O41 Nd7 Nd8 O33 -37.0(8) 2_666 2_666
O41 Nd7 Nd8 O35 -154.7(6) 2_666 .
O41 Nd7 Nd8 O36 159.8(8) 2_666 .
O41 Nd7 Nd8 O39 -12.3(6) 2_666 2_666
O41 Nd7 Nd8 O45 129.2(6) 2_666 .
O41 Nd7 Nd8 O13W 55.2(15) 2_666 .
O41 Nd7 Nd8 O14W 55.3(6) 2_666 .
O41 Nd7 O31 Nd6 21.9(13) 2_666 2_666
O41 Nd7 O31 Ge7 -138.6(10) 2_666 .
O41 Nd7 O36 Nd8 -28.1(11) 2_666 .
O41 Nd7 O36 Ge12 141.1(9) 2_666 .
O41 Nd7 O47 C36 -29(3) 2_666 .
O41 Nd7 O6W Nd2 89.2(9) 2_666 .
O42 Nd4 O7 Nd2 -63.9(7) 2_666 .
O42 Nd4 O7 Ge1 102.4(10) 2_666 .
O42 Nd4 O8 Nd3 174.9(9) 2_666 .
O42 Nd4 O8 Ge2 16.1(19) 2_666 .
O42 Nd4 O13 C3 33(3) 2_666 .
O43 Nd6 Nd8 Nd7 -109.6(4) . .
O43 Nd6 Nd8 O32 171.7(8) . 2_666
O43 Nd6 Nd8 O33 -148.0(6) . 2_666
O43 Nd6 Nd8 O35 -33.0(8) . .
O43 Nd6 Nd8 O36 -73.0(6) . .
O43 Nd6 Nd8 O39 139.4(6) . 2_666
O43 Nd6 Nd8 O45 6.6(6) . .
O43 Nd6 Nd8 O13W 72.2(6) . .
O43 Nd6 Nd8 O14W 84.4(11) . .
O43 Nd6 Ge10 O27 164.1(11) . .
O43 Nd6 Ge10 O28 70.3(8) . .
O43 Nd6 Ge10 O34 -158.5(11) . .
O43 Nd6 Ge10 C28 -43.4(10) . .
O43 Nd6 O34 Nd7 -150.0(8) . 2_666
O43 Nd6 O34 Ge10 16.1(8) . .
O43 Nd6 O35 Nd8 145.2(8) . .
O43 Nd6 O35 Ge11 -13.3(9) . .
O45 Nd8 O35 Nd6 -138.7(8) . .
O45 Nd8 O35 Ge11 20.4(9) . .
O45 Nd8 O36 Nd7 150.0(8) . .
O45 Nd8 O36 Ge12 -18.5(10) . .
O46 Nd1 Ge1 O1 -98.8(10) 2_655 .
O46 Nd1 Ge1 O6 60.2(10) 2_655 .
O46 Nd1 Ge1 O7 154.1(9) 2_655 .
O46 Nd1 Ge1 C1 -13.1(11) 2_655 .
O46 Nd1 Ge4 Nd4 -133.8(4) 2_655 2
O46 Nd1 Ge4 O3 90.8(9) 2_655 .
O46 Nd1 Ge4 O4 -66.8(9) 2_655 .
O46 Nd1 Ge4 O10 -171.2(7) 2_655 .
O46 Nd1 Ge4 C10 12.4(11) 2_655 .
O46 Nd1 Ge5 O4 62.4(8) 2_655 .
O46 Nd1 Ge5 O5 -96.8(9) 2_655 .
O46 Nd1 Ge5 O11 155.8(7) 2_655 .
O46 Nd1 Ge5 C13 -17.3(9) 2_655 .
O46 Nd1 Ge6 O5 44.7(8) 2_655 .
O46 Nd1 Ge6 O6 -114.2(8) 2_655 .
O46 Nd1 Ge6 O12 139.4(8) 2_655 .
O46 Nd1 Ge6 C16 -29.5(12) 2_655 .
O46 Nd1 O1 Ge1 115.0(8) 2_655 .
O46 Nd1 O1 Ge2 -103.9(9) 2_655 .
O46 Nd1 O2 Ge2 144.9(7) 2_655 .
O46 Nd1 O2 Ge3 -79.7(8) 2_655 .
O46 Nd1 O3 Ge3 136.3(8) 2_655 .
O46 Nd1 O3 Ge4 -85.2(8) 2_655 .
O46 Nd1 O4 Ge4 106.4(8) 2_655 .
O46 Nd1 O4 Ge5 -111.6(8) 2_655 .
O46 Nd1 O5 Ge5 81.3(8) 2_655 .
O46 Nd1 O5 Ge6 -138.9(8) 2_655 .
O46 Nd1 O6 Ge1 -139.8(7) 2_655 .
O46 Nd1 O6 Ge6 79.7(8) 2_655 .
O47 Nd7 Nd8 Nd6 116.6(4) . .
O47 Nd7 Nd8 O32 152.3(6) . 2_666
O47 Nd7 Nd8 O33 -161.9(8) . 2_666
O47 Nd7 Nd8 O35 80.4(6) . .
O47 Nd7 Nd8 O36 35.0(8) . .
O47 Nd7 Nd8 O39 -137.1(6) . 2_666
O47 Nd7 Nd8 O45 4.4(6) . .
O47 Nd7 Nd8 O13W -69.6(15) . .
O47 Nd7 Nd8 O14W -69.5(6) . .
O47 Nd7 O31 Nd6 153.7(8) . 2_666
O47 Nd7 O31 Ge7 -6.7(11) . .
O47 Nd7 O36 Nd8 -142.2(8) . .
O47 Nd7 O36 Ge12 27.0(9) . .
O47 Nd7 O6W Nd2 -61.7(8) . .
O48 Nd2 Nd4 Nd3 173.0(11) . .
O48 Nd2 Nd4 Ge4 87.0(11) . 2
O48 Nd2 Nd4 O7 -106.0(13) . .
O48 Nd2 Nd4 O8 -151.3(11) . .
O48 Nd2 Nd4 O10 102.7(13) . 2
O48 Nd2 Nd4 O11 136.4(11) . 2
O48 Nd2 Nd4 O13 -74.7(11) . .
O48 Nd2 Nd4 O19 59.2(11) . 2
O48 Nd2 Nd4 O42 -3.8(12) . 2_666
O48 Nd2 Nd4 O5W -11(2) . .
O48 Nd2 O7 Nd4 142.4(8) . .
O48 Nd2 O7 Ge1 -21.6(18) . .
O48 Nd2 O12 Nd3 -74.7(7) . 2
O48 Nd2 O12 Ge6 90.3(9) . .
O48 Nd2 O23 C18 8(4) . .
O48 Nd2 O6W Nd7 65.4(8) . .
O1W Nd1 Ge1 O1 -69.6(8) . .
O1W Nd1 Ge1 O6 89.4(8) . .
O1W Nd1 Ge1 O7 -176.7(7) . .
O1W Nd1 Ge1 C1 16.0(9) . .
O1W Nd1 Ge4 Nd4 -165.6(7) . 2
O1W Nd1 Ge4 O3 59.1(10) . .
O1W Nd1 Ge4 O4 -98.5(10) . .
O1W Nd1 Ge4 O10 157.1(9) . .
O1W Nd1 Ge4 C10 -19.4(12) . .
O1W Nd1 Ge5 O4 113.4(9) . .
O1W Nd1 Ge5 O5 -45.8(9) . .
O1W Nd1 Ge5 O11 -153.3(8) . .
O1W Nd1 Ge5 C13 33.7(9) . .
O1W Nd1 Ge6 O5 114.6(8) . .
O1W Nd1 Ge6 O6 -44.3(8) . .
O1W Nd1 Ge6 O12 -150.7(7) . .
O1W Nd1 Ge6 C16 40.4(11) . .
O1W Nd1 O1 Ge1 101.4(8) . .
O1W Nd1 O1 Ge2 -117.5(8) . .
O1W Nd1 O2 Ge2 79.5(7) . .
O1W Nd1 O2 Ge3 -145.1(7) . .
O1W Nd1 O3 Ge3 78.5(9) . .
O1W Nd1 O3 Ge4 -143.0(6) . .
O1W Nd1 O4 Ge4 119.4(8) . .
O1W Nd1 O4 Ge5 -98.6(9) . .
O1W Nd1 O5 Ge5 146.4(7) . .
O1W Nd1 O5 Ge6 -73.8(8) . .
O1W Nd1 O6 Ge1 -84.1(7) . .
O1W Nd1 O6 Ge6 135.5(7) . .
O2W Nd1 Ge1 O1 97.3(8) . .
O2W Nd1 Ge1 O6 -103.7(8) . .
O2W Nd1 Ge1 O7 -9.8(7) . .
O2W Nd1 Ge1 C1 -177.1(9) . .
O2W Nd1 Ge4 Nd4 36.0(4) . 2
O2W Nd1 Ge4 O3 -99.3(8) . .
O2W Nd1 Ge4 O4 103.1(9) . .
O2W Nd1 Ge4 O10 -1.3(7) . .
O2W Nd1 Ge4 C10 -177.7(11) . .
O2W Nd1 Ge5 O4 -97.0(8) . .
O2W Nd1 Ge5 O5 103.8(9) . .
O2W Nd1 Ge5 O11 -3.6(7) . .
O2W Nd1 Ge5 C13 -176.7(9) . .
O2W Nd1 Ge6 O5 -101.3(8) . .
O2W Nd1 Ge6 O6 99.7(8) . .
O2W Nd1 Ge6 O12 -6.7(7) . .
O2W Nd1 Ge6 C16 -175.5(11) . .
O2W Nd1 O1 Ge1 -73.3(7) . .
O2W Nd1 O1 Ge2 67.7(7) . .
O2W Nd1 O2 Ge2 -67.9(7) . .
O2W Nd1 O2 Ge3 67.5(7) . .
O2W Nd1 O3 Ge3 -67.9(8) . .
O2W Nd1 O3 Ge4 70.7(7) . .
O2W Nd1 O4 Ge4 -67.6(7) . .
O2W Nd1 O4 Ge5 74.4(7) . .
O2W Nd1 O5 Ge5 -68.8(8) . .
O2W Nd1 O5 Ge6 71.0(7) . .
O2W Nd1 O6 Ge1 67.9(7) . .
O2W Nd1 O6 Ge6 -72.5(7) . .
O3W Nd3 Nd4 Nd2 -178.4(6) . .
O3W Nd3 Nd4 Ge4 -116.4(6) . 2
O3W Nd3 Nd4 O7 144.3(7) . .
O3W Nd3 Nd4 O8 103.0(9) . .
O3W Nd3 Nd4 O10 -143.6(7) . 2
O3W Nd3 Nd4 O11 -95.9(9) . 2
O3W Nd3 Nd4 O13 72.4(7) . .
O3W Nd3 Nd4 O19 -67.2(7) . 2
O3W Nd3 Nd4 O42 -40(6) . 2_666
O3W Nd3 Nd4 O5W 3.4(9) . .
O3W Nd3 O8 Nd4 -69.7(8) . .
O3W Nd3 O8 Ge2 90.9(11) . .
O3W Nd3 O9 Nd2 159.2(10) . 2
O3W Nd3 O9 Ge3 -7.2(19) . .
O3W Nd3 O15 C6 15(3) . .
O4W Nd3 Nd4 Nd2 -177(3) . .
O4W Nd3 Nd4 Ge4 -115(3) . 2
O4W Nd3 Nd4 O7 145(3) . .
O4W Nd3 Nd4 O8 104(3) . .
O4W Nd3 Nd4 O10 -142(3) . 2
O4W Nd3 Nd4 O11 -95(3) . 2
O4W Nd3 Nd4 O13 74(3) . .
O4W Nd3 Nd4 O19 -66(3) . 2
O4W Nd3 Nd4 O42 -39(7) . 2_666
O4W Nd3 Nd4 O5W 5(3) . .
O4W Nd3 O8 Nd4 -159.3(9) . .
O4W Nd3 O8 Ge2 1.3(18) . .
O4W Nd3 O9 Nd2 72.3(7) . 2
O4W Nd3 O9 Ge3 -94.1(11) . .
O4W Nd3 O15 C6 -86(3) . .
O6W Nd2 Nd4 Nd3 -171.5(4) . .
O6W Nd2 Nd4 Ge4 102.4(4) . 2
O6W Nd2 Nd4 O7 -90.5(8) . .
O6W Nd2 Nd4 O8 -135.9(6) . .
O6W Nd2 Nd4 O10 118.1(8) . 2
O6W Nd2 Nd4 O11 151.9(5) . 2
O6W Nd2 Nd4 O13 -59.3(6) . .
O6W Nd2 Nd4 O19 74.6(6) . 2
O6W Nd2 Nd4 O42 11.7(6) . 2_666
O6W Nd2 Nd4 O5W 4.1(17) . .
O6W Nd2 O7 Nd4 88.2(7) . .
O6W Nd2 O7 Ge1 -75.8(12) . .
O6W Nd2 O12 Nd3 -139.7(7) . 2
O6W Nd2 O12 Ge6 25.3(13) . .
O6W Nd2 O23 C18 -71(4) . .
O6W Nd2 O48 C36 -7(2) . .
O6W Nd7 Nd8 Nd6 179.0(4) . .
O6W Nd7 Nd8 O32 -145.3(6) . 2_666
O6W Nd7 Nd8 O33 -99.5(8) . 2_666
O6W Nd7 Nd8 O35 142.8(6) . .
O6W Nd7 Nd8 O36 97.4(8) . .
O6W Nd7 Nd8 O39 -74.7(6) . 2_666
O6W Nd7 Nd8 O45 66.8(6) . .
O6W Nd7 Nd8 O13W -7.2(15) . .
O6W Nd7 Nd8 O14W -7.1(6) . .
O6W Nd7 O31 Nd6 152.9(7) . 2_666
O6W Nd7 O31 Ge7 -7.6(18) . .
O6W Nd7 O36 Nd8 -78.9(7) . .
O6W Nd7 O36 Ge12 90.3(10) . .
O6W Nd7 O47 C36 2(3) . .
O7W Nd5 Ge7 Nd6 -131.7(6) . 2_666
O7W Nd5 Ge7 O25 -65.5(10) . .
O7W Nd5 Ge7 O30 95.6(10) . .
O7W Nd5 Ge7 O31 -172.4(8) . .
O7W Nd5 Ge7 O37 -80.9(8) . .
O7W Nd5 Ge7 C19 21.1(11) . .
O7W Nd5 Ge8 O25 61.5(9) . .
O7W Nd5 Ge8 O26 -102.3(9) . .
O7W Nd5 Ge8 O32 154.4(8) . .
O7W Nd5 Ge8 O39 -116.1(7) . .
O7W Nd5 Ge8 C22 -14.4(11) . .
O7W Nd5 Ge11 O28 113.7(11) . .
O7W Nd5 Ge11 O29 -51.9(11) . .
O7W Nd5 Ge11 O35 -150.5(10) . .
O7W Nd5 Ge11 C31 31.1(11) . .
O7W Nd5 O25 Ge7 106.0(10) . .
O7W Nd5 O25 Ge8 -110.9(10) . .
O7W Nd5 O26 Ge8 74.8(8) . .
O7W Nd5 O26 Ge9 -140.3(9) . .
O7W Nd5 O28 Ge10 103.8(13) . .
O7W Nd5 O28 Ge11 -111.8(12) . .
O7W Nd5 O29 Ge11 147.7(7) . .
O7W Nd5 O29 Ge12 -66.2(10) . .
O7W Nd5 O30 Ge7 -79.6(8) . .
O7W Nd5 O30 Ge12 143.5(9) . .
O8W Nd5 Ge7 Nd6 165.8(6) . 2_666
O8W Nd5 Ge7 O25 -128.1(10) . .
O8W Nd5 Ge7 O30 33.0(10) . .
O8W Nd5 Ge7 O31 125.0(8) . .
O8W Nd5 Ge7 O37 -143.5(8) . .
O8W Nd5 Ge7 C19 -41.5(11) . .
O8W Nd5 Ge8 O25 52.7(13) . .
O8W Nd5 Ge8 O26 -111.1(13) . .
O8W Nd5 Ge8 O32 145.5(12) . .
O8W Nd5 Ge8 O39 -125.0(12) . .
O8W Nd5 Ge8 C22 -23.3(14) . .
O8W Nd5 Ge11 O28 100.2(9) . .
O8W Nd5 Ge11 O29 -65.3(9) . .
O8W Nd5 Ge11 O35 -163.9(8) . .
O8W Nd5 Ge11 C31 17.6(9) . .
O8W Nd5 O25 Ge7 67.0(11) . .
O8W Nd5 O25 Ge8 -150.0(8) . .
O8W Nd5 O26 Ge8 120.1(12) . .
O8W Nd5 O26 Ge9 -95.0(14) . .
O8W Nd5 O28 Ge10 141.2(9) . .
O8W Nd5 O28 Ge11 -74.5(8) . .
O8W Nd5 O29 Ge11 105.0(9) . .
O8W Nd5 O29 Ge12 -109.0(10) . .
O8W Nd5 O30 Ge7 -149.5(9) . .
O8W Nd5 O30 Ge12 73.6(9) . .
O9W Nd5 Ge7 Nd6 -108.0(10) . 2_666
O9W Nd5 Ge7 O25 -41.8(13) . .
O9W Nd5 Ge7 O30 119.3(13) . .
O9W Nd5 Ge7 O31 -148.8(12) . .
O9W Nd5 Ge7 O37 -57.3(12) . .
O9W Nd5 Ge7 C19 44.8(14) . .
O9W Nd5 Ge8 O25 128.9(10) . .
O9W Nd5 Ge8 O26 -34.9(9) . .
O9W Nd5 Ge8 O32 -138.3(8) . .
O9W Nd5 Ge8 O39 -48.8(7) . .
O9W Nd5 Ge8 C22 53.0(11) . .
O9W Nd5 Ge11 O28 35.5(9) . .
O9W Nd5 Ge11 O29 -130.0(9) . .
O9W Nd5 Ge11 O35 131.4(8) . .
O9W Nd5 Ge11 C31 -47.0(9) . .
O9W Nd5 O25 Ge7 154.9(8) . .
O9W Nd5 O25 Ge8 -62.0(10) . .
O9W Nd5 O26 Ge8 145.9(9) . .
O9W Nd5 O26 Ge9 -69.2(9) . .
O9W Nd5 O28 Ge10 70.4(9) . .
O9W Nd5 O28 Ge11 -145.2(9) . .
O9W Nd5 O29 Ge11 60.9(10) . .
O9W Nd5 O29 Ge12 -153.0(8) . .
O9W Nd5 O30 Ge7 -112.6(13) . .
O9W Nd5 O30 Ge12 110.5(13) . .
O10W Nd5 Ge7 Nd6 30.0(4) . 2_666
O10W Nd5 Ge7 O25 96.2(9) . .
O10W Nd5 Ge7 O30 -102.8(9) . .
O10W Nd5 Ge7 O31 -10.8(7) . .
O10W Nd5 Ge7 O37 80.7(7) . .
O10W Nd5 Ge7 C19 -177.2(10) . .
O10W Nd5 Ge8 O25 -99.6(9) . .
O10W Nd5 Ge8 O26 96.6(9) . .
O10W Nd5 Ge8 O32 -6.7(7) . .
O10W Nd5 Ge8 O39 82.8(7) . .
O10W Nd5 Ge8 C22 -175.5(10) . .
O10W Nd5 Ge11 O28 -96.1(9) . .
O10W Nd5 Ge11 O29 98.4(8) . .
O10W Nd5 Ge11 O35 -0.2(7) . .
O10W Nd5 Ge11 C31 -178.7(8) . .
O10W Nd5 O25 Ge7 -73.2(8) . .
O10W Nd5 O25 Ge8 69.8(8) . .
O10W Nd5 O26 Ge8 -72.2(7) . .
O10W Nd5 O26 Ge9 72.7(8) . .
O10W Nd5 O28 Ge10 -72.0(8) . .
O10W Nd5 O28 Ge11 72.4(7) . .
O10W Nd5 O29 Ge11 -70.6(7) . .
O10W Nd5 O29 Ge12 75.4(8) . .
O10W Nd5 O30 Ge7 67.8(7) . .
O10W Nd5 O30 Ge12 -69.1(7) . .
O11W Nd6 Nd8 Nd7 -175.2(14) . .
O11W Nd6 Nd8 O32 106.0(16) . 2_666
O11W Nd6 Nd8 O33 146.4(15) . 2_666
O11W Nd6 Nd8 O35 -98.6(16) . .
O11W Nd6 Nd8 O36 -138.7(15) . .
O11W Nd6 Nd8 O39 73.8(15) . 2_666
O11W Nd6 Nd8 O45 -59.1(15) . .
O11W Nd6 Nd8 O13W 6.5(15) . .
O11W Nd6 Nd8 O14W 18.8(17) . .
O11W Nd6 Ge10 O27 -121.6(10) . .
O11W Nd6 Ge10 O28 144.6(6) . .
O11W Nd6 Ge10 O34 -84.2(10) . .
O11W Nd6 Ge10 C28 30.8(9) . .
O11W Nd6 O34 Nd7 -74.0(7) . 2_666
O11W Nd6 O34 Ge10 92.1(9) . .
O11W Nd6 O35 Nd8 147.9(7) . .
O11W Nd6 O35 Ge11 -10.6(16) . .
O11W Nd6 O43 C30 27(3) . .
O12W Nd6 Nd8 Nd7 -177.4(5) . .
O12W Nd6 Nd8 O32 103.9(8) . 2_666
O12W Nd6 Nd8 O33 144.2(6) . 2_666
O12W Nd6 Nd8 O35 -100.8(8) . .
O12W Nd6 Nd8 O36 -140.8(6) . .
O12W Nd6 Nd8 O39 71.6(6) . 2_666
O12W Nd6 Nd8 O45 -61.2(6) . .
O12W Nd6 Nd8 O13W 4.4(6) . .
O12W Nd6 Nd8 O14W 16.6(11) . .
O12W Nd6 Ge10 O27 165.8(10) . .
O12W Nd6 Ge10 O28 72.0(7) . .
O12W Nd6 Ge10 O34 -156.8(10) . .
O12W Nd6 Ge10 C28 -41.8(10) . .
O12W Nd6 O34 Nd7 -133.8(8) . 2_666
O12W Nd6 O34 Ge10 32.3(14) . .
O12W Nd6 O35 Nd8 77.9(7) . .
O12W Nd6 O35 Ge11 -80.5(10) . .
O12W Nd6 O43 C30 -55(3) . .
O13W Nd8 O35 Nd6 -68.9(7) . .
O13W Nd8 O35 Ge11 90.1(10) . .
O13W Nd8 O36 Nd7 151.5(8) . .
O13W Nd8 O36 Ge12 -17.0(18) . .
O13W Nd8 O45 C33 -1(3) . .
O14W Nd8 O35 Nd6 -132.0(11) . .
O14W Nd8 O35 Ge11 27.1(18) . .
O14W Nd8 O36 Nd7 74.9(7) . .
O14W Nd8 O36 Ge12 -93.6(11) . .
O14W Nd8 O45 C33 -85(3) . .
C1 Ge1 O1 Nd1 -124.2(8) . .
C1 Ge1 O1 Ge2 108.7(13) . .
C1 Ge1 O6 Nd1 130.5(9) . .
C1 Ge1 O6 Ge6 -104.3(13) . .
C1 Ge1 O7 Nd2 75.3(14) . .
C1 Ge1 O7 Nd4 -87.7(11) . .
C1 C2 C3 O13 24(4) . .
C1 C2 C3 O14 -165(2) . .
C4 Ge2 O1 Nd1 134.7(10) . .
C4 Ge2 O1 Ge1 -99.0(15) . .
C4 Ge2 O2 Nd1 -131.5(9) . .
C4 Ge2 O2 Ge3 111.7(14) . .
C4 Ge2 O8 Nd3 -81.4(13) . .
C4 Ge2 O8 Nd4 75.9(14) . .
C4 C5 C6 O15 39(4) . .
C4 C5 C6 O16 -123(3) . .
C7 Ge3 O2 Nd1 126.3(10) . .
C7 Ge3 O2 Ge2 -116.5(14) . .
C7 Ge3 O3 Nd1 -133.5(10) . .
C7 Ge3 O3 Ge4 100.2(14) . .
C7 Ge3 O9 Nd2 -75.3(13) . 2
C7 Ge3 O9 Nd3 90.0(14) . .
C7 C8 C9 O17 26(3) . .
C7 C8 C9 O18 -162(2) . .
C10 Ge4 O3 Nd1 125.1(9) . .
C10 Ge4 O3 Ge3 -107.2(13) . .
C10 Ge4 O4 Nd1 -124.6(10) . .
C10 Ge4 O4 Ge5 106.7(14) . .
C10 Ge4 O10 Nd2 69.9(15) . 2
C10 Ge4 O10 Nd4 -73.0(14) . 2
C10 C11 C12 O19 25(3) . .
C10 C11 C12 O20 -156(3) . .
C13 Ge5 O4 Nd1 124.2(9) . .
C13 Ge5 O4 Ge4 -107.4(14) . .
C13 Ge5 O5 Nd1 -124.5(9) . .
C13 Ge5 O5 Ge6 110.2(13) . .
C13 Ge5 O11 Nd3 -84.8(11) . 2
C13 Ge5 O11 Nd4 82.3(13) . 2
C13 C14 C15 O21 28(3) . .
C13 C14 C15 O22 -155(2) . .
C16 Ge6 O5 Nd1 127.9(10) . .
C16 Ge6 O5 Ge5 -105.8(14) . .
C16 Ge6 O6 Nd1 -122.0(9) . .
C16 Ge6 O6 Ge1 112.9(13) . .
C16 Ge6 O12 Nd2 -87.4(13) . .
C16 Ge6 O12 Nd3 74.3(15) . 2
C16 C17 C18 O23 29(4) . .
C16 C17 C18 O24 -161(2) . .
C19 Ge7 O25 Nd5 -121.6(10) . .
C19 Ge7 O25 Ge8 108.0(14) . .
C19 Ge7 O30 Nd5 129.0(10) . .
C19 Ge7 O30 Ge12 -110.1(15) . .
C19 Ge7 O31 Nd6 -89.8(12) . 2_666
C19 Ge7 O31 Nd7 69.9(15) . .
C19 Ge7 O37 Nd6 141.3(10) . 2_666
C19 Ge7 O37 C21 -9(2) . .
C19 C20 C21 O37 24(4) . .
C19 C20 C21 O38 -152(3) . .
C22 Ge8 O25 Nd5 127.6(10) . .
C22 Ge8 O25 Ge7 -102.5(15) . .
C22 Ge8 O26 Nd5 -121.5(10) . .
C22 Ge8 O26 Ge9 101.2(14) . .
C22 Ge8 O32 Nd6 73.4(14) . 2_666
C22 Ge8 O32 Nd8 -80.4(12) . 2_666
C22 Ge8 O39 Nd8 139.6(10) . 2_666
C22 Ge8 O39 C24 -13(2) . .
C22 C23 C24 O39 14(4) . .
C22 C23 C24 O40 -160(3) . .
C25 Ge9 O26 Nd5 124.4(10) . .
C25 Ge9 O26 Ge8 -100.9(14) . .
C25 Ge9 O27 Ge10 125.5(15) . .
C25 Ge9 O33 Nd7 -81.3(12) . 2_666
C25 Ge9 O33 Nd8 83.4(13) . 2_666
C25 C26 C27 O41 73(3) . .
C25 C26 C27 O42 -100(3) . .
C28 Ge10 O27 Ge9 -124.6(15) . .
C28 Ge10 O28 Nd5 -128.1(10) . .
C28 Ge10 O28 Ge11 97.9(14) . .
C28 Ge10 O34 Nd6 -80.8(12) . .
C28 Ge10 O34 Nd7 82.0(14) . 2_666
C28 C29 C30 O43 34(4) . .
C28 C29 C30 O44 -152(3) . .
C31 Ge11 O28 Nd5 122.6(9) . .
C31 Ge11 O28 Ge10 -100.4(13) . .
C31 Ge11 O29 Nd5 -122.5(8) . .
C31 Ge11 O29 Ge12 106.2(14) . .
C31 Ge11 O35 Nd6 78.8(12) . .
C31 Ge11 O35 Nd8 -77.4(12) . .
C31 C32 C33 O45 58(3) . .
C31 C32 C33 O46 -110(3) . .
C34 Ge12 O29 Nd5 121.9(10) . .
C34 Ge12 O29 Ge11 -107.4(15) . .
C34 Ge12 O30 Nd5 -119.8(9) . .
C34 Ge12 O30 Ge7 119.6(14) . .
C34 Ge12 O36 Nd7 -86.0(12) . .
C34 Ge12 O36 Nd8 81.2(13) . .
C34 C35 C36 O47 37(3) . .
C34 C35 C36 O48 -143(2) . .
O5W Nd4 O7 Nd2 -140.2(9) . .
O5W Nd4 O7 Ge1 26.1(16) . .
O5W Nd4 O8 Nd3 78.3(9) . .
O5W Nd4 O8 Ge2 -80.6(12) . .
O5W Nd4 O13 C3 -65(3) . .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.000 0.500 11 5 ' '
2 0.500 0.500 0.000 228 152 ' '
3 0.215 0.607 0.937 8 5 ' '
4 0.785 0.393 0.062 8 6 ' '
