#------------------------------------------------------------------------------
#$Date: 2019-11-25 01:44:56 +0200 (Mon, 25 Nov 2019) $
#$Revision: 239898 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/35/04/4350446.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4350446
loop_
_publ_author_name
'Dan, Meenakshi'
'Cheetham, A. K.'
'Rao, C. N. R.'
_publ_section_title
;
 Diverse structures and dimensionalities in hybrid frameworks of strontium
 and lanthanum with isomeric dihydroxybenzoates.
;
_journal_issue                   20
_journal_name_full               'Inorganic chemistry'
_journal_page_first              8227
_journal_page_last               8238
_journal_paper_doi               10.1021/ic060917k
_journal_volume                  45
_journal_year                    2006
_chemical_formula_sum            'C28 H31 O23 Sr2'
_chemical_formula_weight         910.77
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                98.156(4)
_cell_angle_beta                 96.206(4)
_cell_angle_gamma                96.373(4)
_cell_formula_units_Z            2
_cell_length_a                   10.240(2)
_cell_length_b                   10.502(2)
_cell_length_c                   16.441(4)
_cell_measurement_temperature    293(2)
_cell_volume                     1725.5(6)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0423
_diffrn_reflns_av_sigmaI/netI    0.0590
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            18642
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.98
_exptl_absorpt_coefficient_mu    3.186
_exptl_absorpt_correction_T_max  1.000000
_exptl_absorpt_correction_T_min  0.658585
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.753
_exptl_crystal_description       block
_exptl_crystal_F_000             918
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.497
_refine_diff_density_min         -0.354
_refine_diff_density_rms         0.080
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.009
_refine_ls_goodness_of_fit_obs   1.058
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     554
_refine_ls_number_reflns         7014
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.010
_refine_ls_restrained_S_obs      1.058
_refine_ls_R_factor_all          0.0684
_refine_ls_R_factor_obs          0.0399
_refine_ls_shift/esd_max         -0.001
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0383P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0886
_refine_ls_wR_factor_obs         0.0777
_reflns_number_observed          5085
_reflns_number_total             7016
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic060917ksi20060526_012106.cif
_cod_data_source_block           compound_I
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0383P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. A new data item '_refine_ls_weighting_details' was
created with the value set to
'w=1/[\s^2^(Fo^2^)+(0.0383P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        1725.5(7)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4350446
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Sr1 Sr 0.45736(3) 0.35394(3) 0.15339(2) 0.02611(10) Uani 1 d .
Sr2 Sr 0.57273(3) 0.66923(3) 0.35783(2) 0.02585(10) Uani 1 d .
O11 O 0.4179(3) 0.5888(3) 0.2137(2) 0.0315(6) Uani 1 d .
O10 O 0.6252(3) 0.4406(3) 0.2911(2) 0.0325(7) Uani 1 d .
O15 O 0.6097(3) 0.1681(3) 0.1682(2) 0.0393(7) Uani 1 d .
O2 O 0.6611(2) 0.5850(3) 0.4942(2) 0.0349(6) Uani 1 d .
O9 O 0.6780(3) 0.8104(3) 0.2610(2) 0.0414(7) Uani 1 d .
O4 O 0.4198(3) 0.8533(3) 0.3384(2) 0.0378(7) Uani 1 d .
O1 O 0.8259(3) 0.7015(3) 0.4075(2) 0.0338(6) Uani 1 d .
O3 O 0.4820(3) 0.7882(3) 0.4832(2) 0.0359(7) Uani 1 d .
O18 O 0.5306(3) 0.2046(2) -0.12928(14) 0.0373(6) Uani 1 d .
O7 O 0.4287(3) 0.7765(2) 0.62793(14) 0.0386(7) Uani 1 d .
O13 O 0.3405(2) 0.4179(3) 0.0203(2) 0.0360(7) Uani 1 d .
O14 O 0.2002(3) 0.3113(3) 0.1230(2) 0.0388(7) Uani 1 d .
O16 O 0.5188(3) 0.2189(3) 0.0234(2) 0.0341(7) Uani 1 d .
O8 O 0.3111(3) 0.9180(2) 0.69035(14) 0.0401(7) Uani 1 d .
O5 O 0.3780(2) 0.5187(3) 0.3820(2) 0.0416(7) Uani 1 d .
O20 O 0.8230(2) 0.5139(3) 0.2070(2) 0.0428(7) Uani 1 d .
O17 O 0.6639(3) 0.0812(3) -0.1924(2) 0.0511(8) Uani 1 d .
O19 O 0.6475(2) 0.4945(3) 0.1119(2) 0.0419(7) Uani 1 d .
O6 O 0.2108(2) 0.5655(3) 0.2985(2) 0.0449(7) Uani 1 d .
O12 O 0.3592(4) 0.2133(4) 0.2517(2) 0.0641(11) Uani 1 d .
C1 C 0.7607(4) 0.0044(3) -0.0405(2) 0.0334(9) Uani 1 d .
H1A H 0.7950(4) -0.0306(3) -0.0876(2) 0.040 Uiso 1 calc R
C2 C 0.7922(3) 0.6041(3) 0.5249(2) 0.0262(8) Uani 1 d .
C3 C 0.3555(4) 0.8676(3) 0.6274(2) 0.0288(8) Uani 1 d .
C4 C 0.9745(3) 0.5861(3) 0.6258(2) 0.0329(9) Uani 1 d .
H4A H 1.0071(3) 0.5585(3) 0.6745(2) 0.040 Uiso 1 calc R
C5 C 0.6158(4) 0.1243(4) -0.1294(2) 0.0328(9) Uani 1 d .
C6 C 0.6619(3) 0.1096(3) 0.1014(2) 0.0283(8) Uani 1 d .
C7 C 0.8801(3) 0.6661(3) 0.4797(2) 0.0268(8) Uani 1 d .
C8 C 0.3214(3) 0.9105(3) 0.5453(2) 0.0264(8) Uani 1 d .
C9 C 0.7577(4) 0.0279(3) 0.1060(2) 0.0315(9) Uani 1 d .
H9B H 0.7898(4) 0.0079(3) 0.1571(2) 0.038 Uiso 1 calc R
C10 C 0.6143(3) 0.1385(3) 0.0236(2) 0.0259(8) Uani 1 d .
C11 C 0.2548(4) 0.5123(4) 0.3573(2) 0.0310(9) Uani 1 d .
C12 C 0.9905(3) 0.6159(4) 0.0972(2) 0.0354(9) Uani 1 d .
H12B H 1.0326(3) 0.5979(4) 0.1465(2) 0.042 Uiso 1 calc R
C13 C 0.6628(3) 0.0864(3) -0.0478(2) 0.0269(8) Uani 1 d .
C14 C 0.3844(3) 0.8661(3) 0.4777(2) 0.0260(8) Uani 1 d .
C15 C 1.0598(4) 0.6503(4) 0.5826(2) 0.0386(10) Uani 1 d .
H15A H 1.1495(4) 0.6672(4) 0.6024(2) 0.046 Uiso 1 calc R
C16 C 0.7708(4) 0.5281(4) 0.1370(2) 0.0325(9) Uani 1 d .
C17 C 0.3502(3) 0.9020(3) 0.4003(2) 0.0276(8) Uani 1 d .
C18 C 0.8396(3) 0.5616(3) 0.5982(2) 0.0271(8) Uani 1 d .
C19 C 0.1893(4) 1.0236(4) 0.4573(2) 0.0404(10) Uani 1 d .
H19A H 0.1227(4) 1.0759(4) 0.4501(2) 0.048 Uiso 1 calc R
C20 C 1.0644(4) 0.6701(4) 0.0432(2) 0.0391(10) Uani 1 d .
H20A H 1.1558(4) 0.6887(4) 0.0562(2) 0.047 Uiso 1 calc R
C21 C 0.8530(3) 0.5872(3) 0.0793(2) 0.0289(8) Uani 1 d .
C22 C 0.2232(4) 0.9904(3) 0.5340(2) 0.0328(9) Uani 1 d .
H22A H 0.1804(4) 1.0214(3) 0.5785(2) 0.039 Uiso 1 calc R
C23 C 1.0129(3) 0.6906(3) 0.5085(2) 0.0334(9) Uani 1 d .
H23A H 1.0713(3) 0.7339(3) 0.4790(2) 0.040 Uiso 1 calc R
C24 C 0.2068(3) 0.3880(3) -0.0034(2) 0.0287(8) Uani 1 d .
C25 C 0.8066(4) -0.0249(4) 0.0351(2) 0.0367(9) Uani 1 d .
H25A H 0.8709(4) -0.0804(4) 0.0389(2) 0.044 Uiso 1 calc R
C26 C 0.1312(4) 0.3320(3) 0.0510(2) 0.0302(8) Uani 1 d .
C27 C 1.0032(4) 0.6977(3) -0.0312(2) 0.0359(9) Uani 1 d .
H27A H 1.0534(4) 0.7361(3) -0.0672(2) 0.043 Uiso 1 calc R
C28 C 0.2535(4) 0.9800(3) 0.3907(2) 0.0349(9) Uani 1 d .
H28A H 0.2305(4) 1.0040(3) 0.3393(2) 0.042 Uiso 1 calc R
O100 O 0.9963(3) 0.7168(3) 0.2997(2) 0.0436(8) Uani 1 d .
O200 O 0.0593(6) 0.1881(5) 0.2223(4) 0.084(2) Uani 1 d .
O300 O 0.0389(4) -0.0733(3) 0.2066(2) 0.0781(11) Uani 1 d .
H15 H 0.6318(37) 0.1397(36) 0.2093(23) 0.041(12) Uiso 1 d .
H14 H 0.4239(38) 0.6484(39) 0.1859(24) 0.050(14) Uiso 1 d .
H13 H 0.3907(39) 0.8733(39) 0.2970(24) 0.048(14) Uiso 1 d .
H12 H 0.3539(45) 0.5924(45) 0.2337(28) 0.067(18) Uiso 1 d .
H11 H 0.6872(47) 0.4526(45) 0.2675(29) 0.077(19) Uiso 1 d .
H10 H 0.6973(50) 0.8776(45) 0.2775(30) 0.074(21) Uiso 1 d .
H8 H 0.6237(41) 0.3859(40) 0.3151(25) 0.047(15) Uiso 1 d .
H7 H 0.5043(41) 0.2299(40) -0.0227(25) 0.056(15) Uiso 1 d .
H6 H 0.9457(42) 0.6612(41) 0.2720(25) 0.054(16) Uiso 1 d .
H5 H 0.6185(47) 0.5394(48) 0.5295(30) 0.098(19) Uiso 1 d .
H4 H 1.0699(49) 0.6797(47) 0.3096(29) 0.091(20) Uiso 1 d .
H3 H 0.1527(41) 0.2738(40) 0.1498(26) 0.057(15) Uiso 1 d .
H2 H 0.0459(66) 0.2038(64) 0.2520(35) 0.072(27) Uiso 1 d .
H1 H 0.3684(41) 0.4517(41) -0.0183(26) 0.060(15) Uiso 1 d .
H19 H 0.4186(48) 0.2006(48) 0.3017(32) 0.096(18) Uiso 1 d .
H18 H 0.6316(52) 0.8053(51) 0.2148(33) 0.097(22) Uiso 1 d .
H17 H 0.3479(37) 0.2754(30) 0.2763(21) 0.005(11) Uiso 1 d .
H16 H 0.8814(40) 0.7195(40) 0.3794(25) 0.056(15) Uiso 1 d .
H9 H 0.4799(44) 0.7683(42) 0.5189(24) 0.048(17) Uiso 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sr Sr -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O19 Sr1 O12 151.44(10) . .
O19 Sr1 O16 75.74(9) . .
O12 Sr1 O16 112.52(12) . .
O19 Sr1 O13 80.29(8) . .
O12 Sr1 O13 128.26(10) . .
O16 Sr1 O13 69.13(8) . .
O19 Sr1 O14 138.84(8) . .
O12 Sr1 O14 68.58(11) . .
O16 Sr1 O14 99.87(9) . .
O13 Sr1 O14 60.66(8) . .
O19 Sr1 O11 76.82(10) . .
O12 Sr1 O11 103.93(13) . .
O16 Sr1 O11 142.32(9) . .
O13 Sr1 O11 81.22(9) . .
O14 Sr1 O11 84.41(9) . .
O19 Sr1 O15 90.18(9) . .
O12 Sr1 O15 72.81(12) . .
O16 Sr1 O15 59.95(8) . .
O13 Sr1 O15 128.96(8) . .
O14 Sr1 O15 123.59(9) . .
O11 Sr1 O15 145.04(8) . .
O19 Sr1 O10 73.37(9) . .
O12 Sr1 O10 80.01(11) . .
O16 Sr1 O10 124.30(9) . .
O13 Sr1 O10 144.66(9) . .
O14 Sr1 O10 133.27(9) . .
O11 Sr1 O10 70.26(8) . .
O15 Sr1 O10 74.95(8) . .
O19 Sr1 Sr2 74.17(6) . .
O12 Sr1 Sr2 89.90(10) . .
O16 Sr1 Sr2 148.16(6) . .
O13 Sr1 Sr2 115.17(6) . .
O14 Sr1 Sr2 109.57(6) . .
O11 Sr1 Sr2 35.53(6) . .
O15 Sr1 Sr2 109.84(6) . .
O10 Sr1 Sr2 34.89(6) . .
O5 Sr2 O9 147.79(10) . .
O5 Sr2 O3 74.82(9) . .
O9 Sr2 O3 116.85(11) . .
O5 Sr2 O1 135.12(8) . .
O9 Sr2 O1 74.46(10) . .
O3 Sr2 O1 101.80(9) . .
O5 Sr2 O10 77.02(10) . .
O9 Sr2 O10 99.61(11) . .
O3 Sr2 O10 143.15(10) . .
O1 Sr2 O10 82.06(9) . .
O5 Sr2 O2 77.34(8) . .
O9 Sr2 O2 134.39(10) . .
O3 Sr2 O2 69.75(9) . .
O1 Sr2 O2 60.40(8) . .
O10 Sr2 O2 81.30(9) . .
O5 Sr2 O4 90.77(9) . .
O9 Sr2 O4 73.06(9) . .
O3 Sr2 O4 59.72(9) . .
O1 Sr2 O4 126.91(9) . .
O10 Sr2 O4 143.95(8) . .
O2 Sr2 O4 129.44(8) . .
O5 Sr2 O11 71.22(9) . .
O9 Sr2 O11 77.52(11) . .
O3 Sr2 O11 121.05(9) . .
O1 Sr2 O11 136.01(9) . .
O10 Sr2 O11 69.96(8) . .
O2 Sr2 O11 141.11(9) . .
O4 Sr2 O11 74.01(8) . .
O5 Sr2 Sr1 67.98(6) . .
O9 Sr2 Sr1 90.48(9) . .
O3 Sr2 Sr1 140.96(7) . .
O1 Sr2 Sr1 112.63(6) . .
O10 Sr2 Sr1 35.51(6) . .
O2 Sr2 Sr1 111.68(6) . .
O4 Sr2 Sr1 108.47(6) . .
O11 Sr2 Sr1 34.60(6) . .
Sr1 O11 Sr2 109.87(9) . .
Sr2 O10 Sr1 109.60(10) . .
C6 O15 Sr1 121.1(2) . .
C2 O2 Sr2 122.0(2) . .
C17 O4 Sr2 121.6(2) . .
C7 O1 Sr2 123.5(2) . .
C14 O3 Sr2 124.3(2) . .
C24 O13 Sr1 122.5(2) . .
C26 O14 Sr1 123.1(2) . .
C10 O16 Sr1 124.7(2) . .
C11 O5 Sr2 131.2(2) . .
C16 O19 Sr1 137.2(2) . .
C25 C1 C13 120.8(3) . .
O2 C2 C7 117.6(3) . .
O2 C2 C18 122.3(3) . .
C7 C2 C18 120.1(3) . .
O8 C3 O7 123.1(3) . .
O8 C3 C8 120.5(3) . .
O7 C3 C8 116.3(3) . .
C15 C4 C18 120.9(3) . .
O17 C5 O18 123.5(3) . .
O17 C5 C13 119.4(3) . .
O18 C5 C13 117.1(3) . .
O15 C6 C9 124.6(3) . .
O15 C6 C10 116.4(3) . .
C9 C6 C10 119.0(3) . .
O1 C7 C23 123.5(3) . .
O1 C7 C2 116.3(3) . .
C23 C7 C2 120.2(3) . .
C14 C8 C22 118.8(3) . .
C14 C8 C3 120.1(3) . .
C22 C8 C3 121.1(3) . .
C6 C9 C25 120.5(3) . .
O16 C10 C13 123.1(3) . .
O16 C10 C6 115.9(3) . .
C13 C10 C6 121.0(3) . .
O6 C11 O5 123.1(3) . .
O6 C11 C18 119.4(3) . 2_666
O5 C11 C18 117.5(3) . 2_666
C20 C12 C21 121.0(3) . .
C10 C13 C1 118.4(3) . .
C10 C13 C5 120.0(3) . .
C1 C13 C5 121.6(3) . .
O3 C14 C8 122.7(3) . .
O3 C14 C17 116.8(3) . .
C8 C14 C17 120.5(3) . .
C4 C15 C23 120.4(3) . .
O20 C16 O19 122.8(3) . .
O20 C16 C21 119.9(3) . .
O19 C16 C21 117.3(3) . .
C28 C17 O4 125.0(3) . .
C28 C17 C14 119.6(3) . .
O4 C17 C14 115.4(3) . .
C4 C18 C2 118.8(3) . .
C4 C18 C11 121.9(3) . 2_666
C2 C18 C11 119.3(3) . 2_666
C22 C19 C28 120.6(3) . .
C12 C20 C27 120.4(3) . .
C12 C21 C24 118.0(3) . 2_665
C12 C21 C16 121.9(3) . .
C24 C21 C16 120.0(3) 2_665 .
C19 C22 C8 120.1(3) . .
C7 C23 C15 119.6(3) . .
O13 C24 C26 117.6(3) . .
O13 C24 C21 121.7(3) . 2_665
C26 C24 C21 120.6(3) . 2_665
C1 C25 C9 120.3(3) . .
O14 C26 C27 124.3(3) . 2_665
O14 C26 C24 115.6(3) . .
C27 C26 C24 120.1(3) 2_665 .
C26 C27 C20 119.8(3) 2_665 .
C17 C28 C19 120.3(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sr1 O19 2.524(2) .
Sr1 O12 2.550(4) .
Sr1 O16 2.570(3) .
Sr1 O13 2.589(3) .
Sr1 O14 2.603(3) .
Sr1 O11 2.616(3) .
Sr1 O15 2.652(3) .
Sr1 O10 2.671(3) .
Sr1 Sr2 4.3327(9) .
Sr2 O5 2.507(2) .
Sr2 O9 2.565(3) .
Sr2 O3 2.572(3) .
Sr2 O1 2.602(3) .
Sr2 O10 2.631(3) .
Sr2 O2 2.633(3) .
Sr2 O4 2.652(3) .
Sr2 O11 2.677(3) .
O15 C6 1.371(4) .
O2 C2 1.365(4) .
O4 C17 1.376(4) .
O1 C7 1.373(4) .
O3 C14 1.363(4) .
O18 C5 1.279(4) .
O7 C3 1.280(4) .
O13 C24 1.370(4) .
O14 C26 1.369(4) .
O16 C10 1.361(4) .
O8 C3 1.247(4) .
O5 C11 1.275(4) .
O20 C16 1.251(4) .
O17 C5 1.244(4) .
O19 C16 1.279(4) .
O6 C11 1.251(4) .
C1 C25 1.370(5) .
C1 C13 1.398(5) .
C2 C7 1.392(5) .
C2 C18 1.400(4) .
C3 C8 1.501(4) .
C4 C15 1.364(5) .
C4 C18 1.391(5) .
C5 C13 1.498(5) .
C6 C9 1.375(5) .
C6 C10 1.404(4) .
C7 C23 1.374(5) .
C8 C14 1.394(5) .
C8 C22 1.394(5) .
C9 C25 1.386(5) .
C10 C13 1.389(4) .
C11 C18 1.490(5) 2_666
C12 C20 1.370(5) .
C12 C21 1.397(5) .
C14 C17 1.398(4) .
C15 C23 1.399(5) .
C16 C21 1.489(5) .
C17 C28 1.363(5) .
C18 C11 1.490(5) 2_666
C19 C22 1.374(5) .
C19 C28 1.386(5) .
C20 C27 1.395(5) .
C21 C24 1.400(5) 2_665
C24 C26 1.395(5) .
C24 C21 1.400(5) 2_665
C26 C27 1.370(5) 2_665
C27 C26 1.370(5) 2_665
