#------------------------------------------------------------------------------
#$Date: 2017-07-11 15:10:40 +0300 (Tue, 11 Jul 2017) $
#$Revision: 198633 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/50/32/4503251.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4503251
loop_
_publ_author_name
'Carlucci, Lucia'
'Ciani, Gianfranco'
'Maggini, Simona'
'Proserpio, Davide M.'
_publ_section_title
;
 A New Polycatenated 3D Array of Interlaced 2D Brickwall Layers and 1D
 Molecular Ladders in [Mn2(bix)3(NO3)4]·2CHCl3[bix =
 1,4-bis(imidazol-1-ylmethyl)benzene] That Undergoes Supramolecular
 Isomerization upon Guest Removal
;
_journal_issue                   1
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              162
_journal_paper_doi               10.1021/cg700884q
_journal_volume                  8
_journal_year                    2008
_chemical_formula_sum            'C28 H28 Mn N10 O6'
_chemical_formula_weight         655.54
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                105.611(3)
_cell_angle_beta                 101.059(3)
_cell_angle_gamma                90.899(3)
_cell_formula_units_Z            2
_cell_length_a                   9.634(3)
_cell_length_b                   10.025(3)
_cell_length_c                   15.868(4)
_cell_measurement_reflns_used    2615
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      20
_cell_measurement_theta_min      3
_cell_volume                     1444.9(7)
_computing_molecular_graphics    SCHAKAL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR92
_diffrn_ambient_temperature      293(2)
_diffrn_detector_type            CCD_plate
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.903
_diffrn_measurement_device       SMART
_diffrn_measurement_method       omega-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0980
_diffrn_reflns_av_sigmaI/netI    0.1800
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            18040
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         29.69
_diffrn_reflns_theta_min         2.11
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    0.519
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  0.79
_exptl_absorpt_correction_type   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.507
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             678
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.573
_refine_diff_density_min         -0.467
_refine_diff_density_rms         0.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   0.924
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     409
_refine_ls_number_reflns         7406
_refine_ls_number_restraints     31
_refine_ls_restrained_S_all      0.938
_refine_ls_R_factor_all          0.2289
_refine_ls_R_factor_obs          0.0685
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0648P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1815
_refine_ls_wR_factor_obs         0.1287
_reflns_number_observed          2630
_reflns_number_total             7406
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            cg700884q-file001.cif
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_hydrogen_treatment' value 'const' was replaced with the
value 'constr' as specified in the replacement file
'src/cod-tools/trunk/data/replacement-values/replacement_values.lst'.

Automatic conversion script
Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4503251
#BEGIN Tags that were not found in dictionaries:
_diffrn_measurement_domega       0.50
_diffrn_measurement_rtime        30
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.0306(5) -0.3341(5) -0.0470(3) 0.0431(13) Uani 1 1 d .
H1 H 0.0092 -0.3343 0.0112 0.052 Uiso 1 1 calc R
C2 C -0.0986(5) -0.4459(5) -0.1119(3) 0.0450(13) Uani 1 1 d .
H2 H -0.1146 -0.5348 -0.1067 0.054 Uiso 1 1 calc R
C3 C -0.0952(5) -0.2662(5) -0.1648(3) 0.0428(12) Uani 1 1 d .
H3 H -0.1097 -0.2116 -0.2042 0.051 Uiso 1 1 calc R
C4 C -0.2290(5) -0.4797(6) -0.2705(3) 0.0517(14) Uani 1 1 d .
H4A H -0.2007 -0.5741 -0.2867 0.062 Uiso 1 1 calc R
H4B H -0.2167 -0.4378 -0.3173 0.062 Uiso 1 1 calc R
C5 C -0.3828(5) -0.4819(5) -0.2637(3) 0.0429(12) Uani 1 1 d .
C6 C -0.4491(5) -0.5948(5) -0.2526(3) 0.0505(14) Uani 1 1 d .
H6 H -0.3986 -0.6720 -0.2488 0.061 Uiso 1 1 calc R
C7 C -0.4587(6) -0.3677(5) -0.2683(3) 0.0523(14) Uani 1 1 d .
H7 H -0.4141 -0.2891 -0.2746 0.063 Uiso 1 1 calc R
C8 C -0.5902(5) -0.5965(6) -0.2471(3) 0.0521(14) Uani 1 1 d .
H8 H -0.6336 -0.6742 -0.2388 0.063 Uiso 1 1 calc R
C9 C -0.6004(5) -0.3690(5) -0.2636(3) 0.0494(14) Uani 1 1 d .
H9 H -0.6506 -0.2915 -0.2673 0.059 Uiso 1 1 calc R
C10 C -0.6677(5) -0.4838(5) -0.2537(3) 0.0413(12) Uani 1 1 d .
C11 C -0.8229(5) -0.4828(5) -0.2495(3) 0.0482(13) Uani 1 1 d .
H11A H -0.8319 -0.4417 -0.1882 0.058 Uiso 1 1 calc R
H11B H -0.8690 -0.4253 -0.2853 0.058 Uiso 1 1 calc R
C12 C -0.9198(6) -0.7080(6) -0.2328(4) 0.0519(14) Uani 1 1 d .
H12 H -0.9021 -0.6865 -0.1708 0.062 Uiso 1 1 calc R
C13 C -0.9328(5) -0.6941(6) -0.3673(3) 0.0440(13) Uani 1 1 d .
H13 H -0.9265 -0.6592 -0.4152 0.053 Uiso 1 1 calc R
C14 C -0.9750(6) -0.8301(6) -0.2900(4) 0.0533(14) Uani 1 1 d .
H14 H -1.0043 -0.9070 -0.2739 0.064 Uiso 1 1 calc R
C15 C -0.3200(5) -0.1051(5) -0.0158(3) 0.0421(12) Uani 1 1 d .
H15 H -0.3294 -0.1418 -0.0772 0.051 Uiso 1 1 calc R
C16 C -0.3670(6) -0.0565(6) 0.1153(4) 0.0531(14) Uani 1 1 d .
H16 H -0.4117 -0.0521 0.1629 0.064 Uiso 1 1 calc R
C17 C -0.2393(6) 0.0033(5) 0.1195(4) 0.0512(14) Uani 1 1 d .
H17 H -0.1810 0.0581 0.1713 0.061 Uiso 1 1 calc R
C18 C -0.5449(5) -0.2180(5) -0.0062(4) 0.0496(14) Uani 1 1 d .
H18A H -0.5804 -0.2202 -0.0681 0.059 Uiso 1 1 calc R
H18B H -0.6174 -0.1830 0.0272 0.059 Uiso 1 1 calc R
C19 C -0.5187(5) -0.3623(5) -0.0009(3) 0.0402(12) Uani 1 1 d .
C20 C -0.3877(5) -0.4137(5) 0.0021(4) 0.0526(15) Uani 1 1 d .
H20 H -0.3102 -0.3566 0.0029 0.063 Uiso 1 1 calc R
C21 C -0.6313(5) -0.4491(6) -0.0040(4) 0.0551(15) Uani 1 1 d .
H21 H -0.7216 -0.4166 -0.0073 0.066 Uiso 1 1 calc R
C22 C -1.6286(5) -0.5556(5) -0.4970(3) 0.0428(13) Uani 1 1 d .
H22 H -1.7171 -0.5931 -0.4961 0.051 Uiso 1 1 calc R
C23 C -1.3876(5) -0.5812(5) -0.5063(3) 0.0428(13) Uani 1 1 d .
H23 H -1.3113 -0.6364 -0.5116 0.051 Uiso 1 1 calc R
C24 C -1.5173(5) -0.6391(5) -0.5017(3) 0.0384(12) Uani 1 1 d .
C25 C -1.5398(5) -0.7879(5) -0.5008(4) 0.0504(14) Uani 1 1 d .
H25A H -1.5377 -0.7904 -0.4399 0.060 Uiso 1 1 calc R
H25B H -1.6331 -0.8249 -0.5359 0.060 Uiso 1 1 calc R
C26 C -1.3049(5) -0.8910(5) -0.4913(3) 0.0443(13) Uani 1 1 d .
H26 H -1.2742 -0.8528 -0.4300 0.053 Uiso 1 1 calc R
C27 C -1.4366(6) -0.9448(5) -0.6229(4) 0.0524(14) Uani 1 1 d .
H27 H -1.5117 -0.9531 -0.6710 0.063 Uiso 1 1 calc R
C28 C -1.3097(6) -0.9981(5) -0.6259(4) 0.0511(14) Uani 1 1 d .
H28 H -1.2828 -1.0502 -0.6775 0.061 Uiso 1 1 calc R
N1 N -0.0292(4) -0.2212(4) -0.0799(3) 0.0413(10) Uani 1 1 d .
N2 N -0.1385(4) -0.4014(4) -0.1861(3) 0.0399(10) Uani 1 1 d .
N3 N -0.8945(4) -0.6215(4) -0.2814(3) 0.0431(10) Uani 1 1 d .
N4 N -0.9813(4) -0.8234(4) -0.3752(3) 0.0431(10) Uani 1 1 d .
N5 N -0.2076(4) -0.0281(4) 0.0365(3) 0.0418(10) Uani 1 1 d .
N6 N -0.4180(4) -0.1241(4) 0.0289(3) 0.0403(10) Uani 1 1 d .
N7 N -1.4339(4) -0.8765(4) -0.5361(3) 0.0428(10) Uani 1 1 d .
N8 N -1.2270(4) -0.9646(4) -0.5427(3) 0.0453(11) Uani 1 1 d .
N9 N 0.2090(5) -0.0868(5) 0.1574(3) 0.0536(12) Uani 1 1 d D
N10 N -0.9912(6) -0.7778(6) -0.6091(4) 0.0725(16) Uani 1 1 d D
O1A O -0.9245(4) -0.8533(4) -0.5681(3) 0.0618(11) Uani 1 1 d D
O2A O -1.0470(8) -0.8170(6) -0.6841(4) 0.151(3) Uani 1 1 d D
O3A O -1.0112(9) -0.6622(7) -0.5729(4) 0.214(5) Uani 1 1 d D
O90 O 0.2964(5) 0.0105(5) 0.1950(3) 0.1025(17) Uani 1 1 d D
O91 O 0.2373(5) -0.2035(5) 0.1546(4) 0.1186(19) Uani 1 1 d D
O92 O 0.0900(4) -0.0645(4) 0.1221(2) 0.0631(11) Uani 1 1 d D
Mn1 Mn 0.0000 0.0000 0.0000 0.0412(3) Uani 1 2 d S
Mn2 Mn -1.0000 -1.0000 -0.5000 0.0427(3) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C2 C1 N1 110.0(4) . .
C2 C1 H1 125.0 . .
N1 C1 H1 125.0 . .
C1 C2 N2 106.0(4) . .
C1 C2 H2 127.0 . .
N2 C2 H2 127.0 . .
N1 C3 N2 110.9(5) . .
N1 C3 H3 124.6 . .
N2 C3 H3 124.6 . .
N2 C4 C5 111.3(4) . .
N2 C4 H4A 109.4 . .
C5 C4 H4A 109.4 . .
N2 C4 H4B 109.4 . .
C5 C4 H4B 109.4 . .
H4A C4 H4B 108.0 . .
C6 C5 C7 118.8(5) . .
C6 C5 C4 121.2(5) . .
C7 C5 C4 120.0(5) . .
C5 C6 C8 120.9(5) . .
C5 C6 H6 119.5 . .
C8 C6 H6 119.5 . .
C5 C7 C9 120.7(5) . .
C5 C7 H7 119.7 . .
C9 C7 H7 119.7 . .
C6 C8 C10 120.6(5) . .
C6 C8 H8 119.7 . .
C10 C8 H8 119.7 . .
C10 C9 C7 120.4(5) . .
C10 C9 H9 119.8 . .
C7 C9 H9 119.8 . .
C9 C10 C8 118.6(5) . .
C9 C10 C11 119.3(5) . .
C8 C10 C11 122.1(5) . .
N3 C11 C10 112.4(4) . .
N3 C11 H11A 109.1 . .
C10 C11 H11A 109.1 . .
N3 C11 H11B 109.1 . .
C10 C11 H11B 109.1 . .
H11A C11 H11B 107.8 . .
C14 C12 N3 107.9(5) . .
C14 C12 H12 126.1 . .
N3 C12 H12 126.1 . .
N4 C13 N3 111.1(5) . .
N4 C13 H13 124.4 . .
N3 C13 H13 124.4 . .
C12 C14 N4 109.1(5) . .
C12 C14 H14 125.4 . .
N4 C14 H14 125.4 . .
N5 C15 N6 112.5(4) . .
N5 C15 H15 123.8 . .
N6 C15 H15 123.8 . .
C17 C16 N6 106.7(5) . .
C17 C16 H16 126.6 . .
N6 C16 H16 126.6 . .
C16 C17 N5 110.1(5) . .
C16 C17 H17 125.0 . .
N5 C17 H17 125.0 . .
N6 C18 C19 112.6(4) . .
N6 C18 H18A 109.1 . .
C19 C18 H18A 109.1 . .
N6 C18 H18B 109.1 . .
C19 C18 H18B 109.1 . .
H18A C18 H18B 107.8 . .
C21 C19 C20 118.4(4) . .
C21 C19 C18 118.7(4) . .
C20 C19 C18 122.8(4) . .
C19 C20 C21 120.9(4) . 2_445
C19 C20 H20 119.5 . .
C21 C20 H20 119.5 2_445 .
C19 C21 C20 120.6(4) . 2_445
C19 C21 H21 119.7 . .
C20 C21 H21 119.7 2_445 .
C23 C22 C24 121.4(5) 2_244 .
C23 C22 H22 119.3 2_244 .
C24 C22 H22 119.3 . .
C22 C23 C24 120.6(4) 2_244 .
C22 C23 H23 119.7 2_244 .
C24 C23 H23 119.7 . .
C22 C24 C23 117.9(4) . .
C22 C24 C25 119.0(4) . .
C23 C24 C25 123.0(4) . .
N7 C25 C24 113.3(4) . .
N7 C25 H25A 108.9 . .
C24 C25 H25A 108.9 . .
N7 C25 H25B 108.9 . .
C24 C25 H25B 108.9 . .
H25A C25 H25B 107.7 . .
N8 C26 N7 112.8(5) . .
N8 C26 H26 123.6 . .
N7 C26 H26 123.6 . .
C28 C27 N7 106.8(5) . .
C28 C27 H27 126.6 . .
N7 C27 H27 126.6 . .
C27 C28 N8 110.0(5) . .
C27 C28 H28 125.0 . .
N8 C28 H28 125.0 . .
C3 N1 C1 105.4(4) . .
C3 N1 Mn1 124.7(3) . .
C1 N1 Mn1 126.3(3) . .
C3 N2 C2 107.8(4) . .
C3 N2 C4 125.2(4) . .
C2 N2 C4 126.5(4) . .
C13 N3 C12 106.5(4) . .
C13 N3 C11 125.0(5) . .
C12 N3 C11 128.1(5) . .
C13 N4 C14 105.4(4) . .
C13 N4 Mn2 124.0(4) . .
C14 N4 Mn2 128.1(4) . .
C15 N5 C17 104.0(4) . .
C15 N5 Mn1 126.3(3) . .
C17 N5 Mn1 128.5(3) . .
C15 N6 C16 106.7(4) . .
C15 N6 C18 126.3(4) . .
C16 N6 C18 126.3(4) . .
C26 N7 C27 105.6(4) . .
C26 N7 C25 126.5(5) . .
C27 N7 C25 127.3(4) . .
C26 N8 C28 104.8(4) . .
C26 N8 Mn2 125.4(3) . .
C28 N8 Mn2 129.5(4) . .
O91 N9 O90 121.0(5) . .
O91 N9 O92 119.6(5) . .
O90 N9 O92 119.4(5) . .
O2A N10 O3A 114.9(6) . .
O2A N10 O1A 123.1(6) . .
O3A N10 O1A 121.9(6) . .
N10 O1A Mn2 130.4(4) . .
N9 O92 Mn1 134.9(3) . .
N5 Mn1 N5 180.0(2) . 2
N5 Mn1 N1 87.94(14) . .
N5 Mn1 N1 92.06(14) 2 .
N5 Mn1 N1 92.06(14) . 2
N5 Mn1 N1 87.94(14) 2 2
N1 Mn1 N1 180.0(3) . 2
N5 Mn1 O92 84.77(14) . .
N5 Mn1 O92 95.23(14) 2 .
N1 Mn1 O92 89.85(14) . .
N1 Mn1 O92 90.15(14) 2 .
N5 Mn1 O92 95.23(14) . 2
N5 Mn1 O92 84.77(14) 2 2
N1 Mn1 O92 90.15(14) . 2
N1 Mn1 O92 89.85(14) 2 2
O92 Mn1 O92 180.00(17) . 2
N8 Mn2 N8 180.0(2) . 2_334
N8 Mn2 O1A 86.79(14) . 2_334
N8 Mn2 O1A 93.21(14) 2_334 2_334
N8 Mn2 O1A 93.21(14) . .
N8 Mn2 O1A 86.79(14) 2_334 .
O1A Mn2 O1A 180.000(1) 2_334 .
N8 Mn2 N4 90.67(14) . .
N8 Mn2 N4 89.33(14) 2_334 .
O1A Mn2 N4 90.72(15) 2_334 .
O1A Mn2 N4 89.28(15) . .
N8 Mn2 N4 89.33(14) . 2_334
N8 Mn2 N4 90.67(14) 2_334 2_334
O1A Mn2 N4 89.28(15) 2_334 2_334
O1A Mn2 N4 90.72(15) . 2_334
N4 Mn2 N4 180.000(1) . 2_334
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C2 1.358(6) .
C1 N1 1.369(6) .
C1 H1 0.9300 .
C2 N2 1.358(6) .
C2 H2 0.9300 .
C3 N1 1.326(6) .
C3 N2 1.344(6) .
C3 H3 0.9300 .
C4 N2 1.461(6) .
C4 C5 1.506(6) .
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C5 C6 1.359(7) .
C5 C7 1.379(7) .
C6 C8 1.380(6) .
C6 H6 0.9300 .
C7 C9 1.381(7) .
C7 H7 0.9300 .
C8 C10 1.380(7) .
C8 H8 0.9300 .
C9 C10 1.372(6) .
C9 H9 0.9300 .
C10 C11 1.510(6) .
C11 N3 1.458(6) .
C11 H11A 0.9700 .
C11 H11B 0.9700 .
C12 C14 1.342(7) .
C12 N3 1.354(6) .
C12 H12 0.9300 .
C13 N4 1.336(6) .
C13 N3 1.336(6) .
C13 H13 0.9300 .
C14 N4 1.362(6) .
C14 H14 0.9300 .
C15 N5 1.320(5) .
C15 N6 1.324(6) .
C15 H15 0.9300 .
C16 C17 1.343(7) .
C16 N6 1.346(6) .
C16 H16 0.9300 .
C17 N5 1.363(6) .
C17 H17 0.9300 .
C18 N6 1.453(6) .
C18 C19 1.494(6) .
C18 H18A 0.9700 .
C18 H18B 0.9700 .
C19 C21 1.365(6) .
C19 C20 1.368(6) .
C20 C21 1.398(7) 2_445
C20 H20 0.9300 .
C21 C20 1.398(7) 2_445
C21 H21 0.9300 .
C22 C23 1.364(6) 2_244
C22 C24 1.372(6) .
C22 H22 0.9300 .
C23 C22 1.364(6) 2_244
C23 C24 1.393(6) .
C23 H23 0.9300 .
C24 C25 1.509(6) .
C25 N7 1.457(6) .
C25 H25A 0.9700 .
C25 H25B 0.9700 .
C26 N8 1.304(6) .
C26 N7 1.339(6) .
C26 H26 0.9300 .
C27 C28 1.345(7) .
C27 N7 1.359(6) .
C27 H27 0.9300 .
C28 N8 1.357(6) .
C28 H28 0.9300 .
N1 Mn1 2.221(4) .
N4 Mn2 2.248(4) .
N5 Mn1 2.220(4) .
N8 Mn2 2.225(4) .
N9 O91 1.197(5) .
N9 O90 1.218(5) .
N9 O92 1.227(5) .
N10 O2A 1.164(5) .
N10 O3A 1.184(6) .
N10 O1A 1.237(5) .
O1A Mn2 2.233(4) .
O92 Mn1 2.230(3) .
Mn1 N5 2.220(4) 2
Mn1 N1 2.221(4) 2
Mn1 O92 2.230(3) 2
Mn2 N8 2.225(4) 2_334
Mn2 O1A 2.233(4) 2_334
Mn2 N4 2.248(4) 2_334
