#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:29:14 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179581 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/46/4504649.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4504649
loop_
_publ_author_name
'Wu, Jing-Yun'
'Yeh, Tzu-Tang'
'Wen, Yuh-Sheng'
'Twu, Jen'
'Lu, Kuang-Lieh'
_publ_section_title
;
 Unusual Robust Luminescent Porous Frameworks Self-Assembled from
 Lanthanide Ions and 2,2‘-Bipyridine-4,4‘-dicarboxylate
;
_journal_issue                   2
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              467
_journal_paper_doi               10.1021/cg050393j
_journal_volume                  6
_journal_year                    2006
_chemical_formula_sum            'C36 H26 Eu2 N6 O16'
_chemical_formula_weight         1102.55
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                95.01(3)
_cell_angle_beta                 103.48(3)
_cell_angle_gamma                100.86(3)
_cell_formula_units_Z            2
_cell_length_a                   11.378(2)
_cell_length_b                   12.208(2)
_cell_length_c                   14.342(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1884.5(7)
_computing_cell_refinement       'CAD4 Express (Enraf Nonius, 1994)'
_computing_data_collection       'CAD4 Express (Enraf Nonius, 1994)'
_computing_data_reduction        'XCAD4 (Harms & Wocadlo, 1995)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Enraf Nonius TurboCAD4'
_diffrn_measurement_method       'non-profiled omega/2theta scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0194
_diffrn_reflns_av_sigmaI/netI    0.0363
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            6990
_diffrn_reflns_theta_full        24.97
_diffrn_reflns_theta_max         24.97
_diffrn_reflns_theta_min         1.47
_exptl_absorpt_coefficient_mu    3.382
_exptl_absorpt_correction_T_max  0.9993
_exptl_absorpt_correction_T_min  0.7561
_exptl_absorpt_correction_type   psi-scan
_exptl_crystal_colour            pale-yellow
_exptl_crystal_density_diffrn    1.943
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1076
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.686
_refine_diff_density_min         -2.430
_refine_diff_density_rms         0.173
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.044
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     629
_refine_ls_number_reflns         6623
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.044
_refine_ls_R_factor_all          0.0437
_refine_ls_R_factor_gt           0.0325
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0617P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0869
_refine_ls_wR_factor_ref         0.0933
_reflns_number_gt                5439
_reflns_number_total             6623
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg050393jsi20050808_100251.cif
_cod_data_source_block           compound_2_i5964
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4504649
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Eu1 Eu 0.70698(2) 0.636245(18) 0.110594(15) 0.01802(9) Uani 1 1 d .
Eu2 Eu 0.895394(19) 0.834484(17) 0.365600(15) 0.01457(9) Uani 1 1 d .
O1 O 0.8475(3) 0.6254(3) 0.2585(3) 0.0277(8) Uani 1 1 d .
O2 O 0.9030(4) 0.6473(3) 0.4173(3) 0.0291(8) Uani 1 1 d .
O3 O 0.7946(3) 0.8386(3) 0.1947(2) 0.0233(7) Uani 1 1 d .
O4 O 0.7433(4) 0.8086(3) 0.0356(2) 0.0348(9) Uani 1 1 d .
O5 O 0.5968(4) 0.6403(3) 0.2298(3) 0.0369(10) Uani 1 1 d .
O6 O 0.6917(3) 0.7552(3) 0.3667(3) 0.0280(8) Uani 1 1 d .
O7 O 0.9347(3) 0.8630(3) 0.5304(2) 0.0260(8) Uani 1 1 d .
O8 O 1.0147(3) 1.0046(3) 0.3423(2) 0.0255(8) Uani 1 1 d .
O9 O 0.6442(4) 0.4435(3) 0.1023(3) 0.0344(9) Uani 1 1 d .
O10 O 0.4922(3) 0.6247(3) 0.0391(2) 0.0280(8) Uani 1 1 d .
O11 O 1.0904(3) 0.8058(3) 0.3576(3) 0.0310(9) Uani 1 1 d .
O12 O 1.1067(4) 0.7869(6) 0.2063(3) 0.0745(19) Uani 1 1 d .
O81 O 0.6756(4) 0.5713(4) -0.0621(3) 0.0362(11) Uani 1 1 d .
O82 O 0.9081(4) 0.6428(5) 0.0870(3) 0.0510(13) Uani 1 1 d .
O83 O 0.7906(4) 0.9880(3) 0.3940(3) 0.0258(8) Uani 1 1 d .
O91 O 0.9645(8) 0.5795(5) 0.9236(5) 0.092(3) Uani 1 1 d .
N1 N 0.8413(4) 0.2305(3) 0.3466(3) 0.0239(9) Uani 1 1 d .
N2 N 0.8724(5) 0.2293(4) 0.1019(3) 0.0359(11) Uani 1 1 d .
N11 N 0.3280(5) 0.5137(4) 0.4444(3) 0.0344(11) Uani 1 1 d .
N12 N 0.2692(5) 0.3173(4) 0.2284(3) 0.0342(11) Uani 1 1 d .
N21 N 0.4982(5) 0.0350(4) 0.1242(3) 0.0393(12) Uani 1 1 d .
N31 N 1.5423(4) 0.9563(4) 0.3909(3) 0.0241(9) Uani 1 1 d .
C1 C 0.8494(5) 0.2732(4) 0.2635(3) 0.0214(10) Uani 1 1 d .
C2 C 0.8606(5) 0.3878(4) 0.2575(4) 0.0219(10) Uani 1 1 d .
C3 C 0.8640(4) 0.4607(4) 0.3384(3) 0.0204(10) Uani 1 1 d .
C4 C 0.8586(5) 0.4170(4) 0.4239(3) 0.0240(11) Uani 1 1 d .
C5 C 0.8463(5) 0.3024(4) 0.4244(4) 0.0269(11) Uani 1 1 d .
C6 C 0.8727(4) 0.5852(4) 0.3379(3) 0.0191(10) Uani 1 1 d .
C7 C 0.8446(5) 0.1903(4) 0.1800(4) 0.0241(11) Uani 1 1 d .
C8 C 0.8136(5) 0.0753(4) 0.1845(4) 0.0230(10) Uani 1 1 d .
C9 C 0.8146(5) 0.9980(4) 0.1076(3) 0.0228(10) Uani 1 1 d .
C10 C 0.8401(7) 1.0394(5) 0.0256(4) 0.0387(15) Uani 1 1 d .
C11 C 0.8696(7) 0.1540(5) 0.0269(4) 0.0458(17) Uani 1 1 d .
C12 C 0.7829(4) 0.8754(4) 0.1124(3) 0.0207(10) Uani 1 1 d .
C13 C 0.3460(5) 0.4673(4) 0.3619(3) 0.0227(10) Uani 1 1 d .
C14 C 0.4339(5) 0.5193(4) 0.3191(4) 0.0249(11) Uani 1 1 d .
C15 C 0.5102(4) 0.6225(4) 0.3624(3) 0.0204(10) Uani 1 1 d .
C16 C 0.4941(5) 0.6695(4) 0.4474(4) 0.0265(11) Uani 1 1 d .
C17 C 0.4016(6) 0.6132(5) 0.4848(4) 0.0362(14) Uani 1 1 d .
C18 C 0.6070(5) 0.6767(4) 0.3161(4) 0.0230(10) Uani 1 1 d .
C19 C 0.2672(5) 0.3535(4) 0.3192(4) 0.0266(11) Uani 1 1 d .
C20 C 0.2022(5) 0.2867(4) 0.3718(4) 0.0225(10) Uani 1 1 d .
C21 C 0.1410(4) 0.1780(4) 0.3329(3) 0.0208(10) Uani 1 1 d .
C22 C 0.1454(6) 0.1383(5) 0.2396(4) 0.0336(13) Uani 1 1 d .
C23 C 0.2071(6) 0.2128(5) 0.1901(4) 0.0415(15) Uani 1 1 d .
H23 H 0.2050 0.1885 0.1263 0.050 Uiso 1 1 calc R
C24 C 1.0688(4) 1.1006(4) 0.3863(3) 0.0168(9) Uani 1 1 d .
C25 C 0.5084(5) 0.0515(4) 0.0346(4) 0.0270(11) Uani 1 1 d .
C26 C 0.5298(5) 0.1568(4) 0.0065(4) 0.0280(11) Uani 1 1 d .
C27 C 0.5480(5) 0.2508(4) 0.0750(4) 0.0256(11) Uani 1 1 d .
C28 C 0.5409(6) 0.2350(4) 0.1673(4) 0.0326(13) Uani 1 1 d .
C29 C 0.5149(7) 0.1281(5) 0.1888(4) 0.0421(16) Uani 1 1 d .
C30 C 0.5681(5) 0.3653(4) 0.0437(4) 0.0227(10) Uani 1 1 d .
C31 C 1.4681(4) 0.9685(4) 0.4504(3) 0.0209(10) Uani 1 1 d .
C32 C 1.3417(5) 0.9227(5) 0.4218(4) 0.0270(11) Uani 1 1 d .
C33 C 1.2880(5) 0.8646(4) 0.3289(4) 0.0260(11) Uani 1 1 d .
C34 C 1.3648(5) 0.8534(5) 0.2665(4) 0.0298(12) Uani 1 1 d .
C35 C 1.4899(5) 0.8998(5) 0.3021(4) 0.0276(11) Uani 1 1 d .
C36 C 1.1506(5) 0.8145(5) 0.2953(4) 0.0323(12) Uani 1 1 d .
H2 H 0.870(5) 0.417(4) 0.197(4) 0.022(13) Uiso 1 1 d .
H4 H 0.854(6) 0.470(5) 0.491(5) 0.045(18) Uiso 1 1 d .
H5 H 0.835(4) 0.271(4) 0.481(4) 0.012(12) Uiso 1 1 d .
H8 H 0.779(5) 0.047(5) 0.232(4) 0.028(15) Uiso 1 1 d .
H10 H 0.837(6) 0.988(6) -0.023(5) 0.05(2) Uiso 1 1 d .
H11 H 0.887(6) 0.183(5) -0.024(5) 0.043(18) Uiso 1 1 d .
H14 H 0.435(5) 0.495(4) 0.273(4) 0.014(14) Uiso 1 1 d .
H16 H 0.534(5) 0.727(5) 0.476(4) 0.019(14) Uiso 1 1 d .
H17 H 0.399(7) 0.635(6) 0.545(5) 0.06(2) Uiso 1 1 d .
H20 H 0.200(4) 0.310(4) 0.427(4) 0.010(12) Uiso 1 1 d .
H22 H 0.097(5) 0.060(5) 0.210(4) 0.026(14) Uiso 1 1 d .
H26 H 0.539(7) 0.171(6) -0.051(6) 0.06(2) Uiso 1 1 d .
H28 H 0.551(7) 0.295(6) 0.213(5) 0.06(2) Uiso 1 1 d .
H29 H 0.481(6) 0.114(5) 0.248(5) 0.040(17) Uiso 1 1 d .
H32 H 1.307(6) 0.937(5) 0.462(5) 0.033(17) Uiso 1 1 d .
H34 H 1.331(5) 0.814(5) 0.205(4) 0.032(15) Uiso 1 1 d .
H35 H 1.538(6) 0.892(5) 0.259(5) 0.043(18) Uiso 1 1 d .
H81A H 0.638(5) 0.529(4) -0.086(4) 0.008(15) Uiso 1 1 d .
H82A H 0.964(5) 0.678(5) 0.119(4) 0.018(15) Uiso 1 1 d .
H83A H 0.823(6) 1.051(6) 0.394(5) 0.037(18) Uiso 1 1 d .
H83B H 0.717(7) 0.978(6) 0.401(5) 0.040(18) Uiso 1 1 d .
H91A H 1.016(12) 0.610(11) 0.903(10) 0.15(5) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 Eu1 O5 83.34(15) . .
O9 Eu1 O1 85.37(13) . .
O5 Eu1 O1 73.70(14) . .
O9 Eu1 O82 98.55(18) . .
O5 Eu1 O82 143.21(15) . .
O1 Eu1 O82 69.87(15) . .
O9 Eu1 O10 83.30(13) . .
O5 Eu1 O10 69.19(13) . .
O1 Eu1 O10 142.16(13) . .
O82 Eu1 O10 147.59(14) . .
O9 Eu1 O4 152.19(12) . .
O5 Eu1 O4 116.26(15) . .
O1 Eu1 O4 117.96(12) . .
O82 Eu1 O4 77.73(18) . .
O10 Eu1 O4 85.73(13) . .
O9 Eu1 O81 77.69(14) . .
O5 Eu1 O81 140.78(14) . .
O1 Eu1 O81 137.18(15) . .
O82 Eu1 O81 74.15(16) . .
O10 Eu1 O81 74.70(15) . .
O4 Eu1 O81 74.78(13) . .
O9 Eu1 O3 155.81(12) . .
O5 Eu1 O3 79.54(13) . .
O1 Eu1 O3 73.53(12) . .
O82 Eu1 O3 85.40(16) . .
O10 Eu1 O3 106.09(12) . .
O4 Eu1 O3 51.99(11) . .
O81 Eu1 O3 126.02(13) . .
O9 Eu1 Eu2 121.56(10) . .
O5 Eu1 Eu2 64.84(9) . .
O1 Eu1 Eu2 40.52(9) . .
O82 Eu1 Eu2 83.81(12) . .
O10 Eu1 Eu2 122.87(9) . .
O4 Eu1 Eu2 85.73(8) . .
O81 Eu1 Eu2 153.09(11) . .
O3 Eu1 Eu2 34.77(7) . .
O7 Eu2 O11 97.03(14) . .
O7 Eu2 O6 85.99(13) . .
O11 Eu2 O6 147.85(13) . .
O7 Eu2 O8 99.18(12) . .
O11 Eu2 O8 71.28(13) . .
O6 Eu2 O8 140.03(13) . .
O7 Eu2 O83 77.45(13) . .
O11 Eu2 O83 140.34(14) . .
O6 Eu2 O83 71.63(13) . .
O8 Eu2 O83 70.97(13) . .
O7 Eu2 O3 159.56(13) . .
O11 Eu2 O3 102.19(13) . .
O6 Eu2 O3 81.45(13) . .
O8 Eu2 O3 80.70(12) . .
O83 Eu2 O3 83.29(12) . .
O7 Eu2 O2 74.53(12) . .
O11 Eu2 O2 75.13(13) . .
O6 Eu2 O2 74.91(13) . .
O8 Eu2 O2 144.78(13) . .
O83 Eu2 O2 137.35(13) . .
O3 Eu2 O2 117.06(11) . .
O7 Eu2 O1 123.61(12) . .
O11 Eu2 O1 75.60(13) . .
O6 Eu2 O1 76.18(12) . .
O8 Eu2 O1 128.29(12) . .
O83 Eu2 O1 139.96(12) . .
O3 Eu2 O1 68.77(11) . .
O2 Eu2 O1 49.31(11) . .
O7 Eu2 Eu1 148.25(9) . .
O11 Eu2 Eu1 95.54(10) . .
O6 Eu2 Eu1 68.33(9) . .
O8 Eu2 Eu1 112.46(9) . .
O83 Eu2 Eu1 109.73(10) . .
O3 Eu2 Eu1 36.36(8) . .
O2 Eu2 Eu1 80.75(8) . .
O1 Eu2 Eu1 34.04(7) . .
C6 O1 Eu1 150.8(3) . .
C6 O1 Eu2 87.8(3) . .
Eu1 O1 Eu2 105.44(13) . .
C6 O2 Eu2 101.7(3) . .
C12 O3 Eu2 155.3(3) . .
C12 O3 Eu1 90.8(3) . .
Eu2 O3 Eu1 108.87(12) . .
C12 O4 Eu1 96.7(3) . .
C18 O5 Eu1 143.0(3) . .
C18 O6 Eu2 135.7(3) . .
C24 O7 Eu2 160.8(3) 2_776 .
C24 O8 Eu2 140.8(3) . .
C30 O9 Eu1 136.5(3) . .
C30 O10 Eu1 133.6(3) 2_665 .
C36 O11 Eu2 134.5(4) . .
C5 N1 C1 118.0(4) . .
C7 N2 C11 118.0(5) . .
C17 N11 C13 116.6(4) . .
C23 N12 C19 117.6(5) . .
C25 N21 C29 117.0(5) . .
C35 N31 C31 117.8(4) . .
N1 C1 C2 121.8(4) . .
N1 C1 C7 115.8(4) . .
C2 C1 C7 122.4(4) . .
C3 C2 C1 119.4(5) . .
C2 C3 C4 118.6(4) . .
C2 C3 C6 123.1(4) . .
C4 C3 C6 118.2(4) . .
C5 C4 C3 118.8(5) . .
N1 C5 C4 123.3(5) . .
O2 C6 O1 121.2(4) . .
O2 C6 C3 118.3(4) . .
O1 C6 C3 120.6(4) . .
N2 C7 C8 121.6(5) . .
N2 C7 C1 118.1(4) . .
C8 C7 C1 120.3(5) . .
C9 C8 C7 120.0(5) 1_545 .
C10 C9 C8 117.9(5) . 1_565
C10 C9 C12 121.8(5) . .
C8 C9 C12 120.3(4) 1_565 .
C11 C10 C9 118.4(5) 1_565 .
N2 C11 C10 124.0(5) . 1_545
O4 C12 O3 120.5(4) . .
O4 C12 C9 119.2(4) . .
O3 C12 C9 120.4(4) . .
N11 C13 C14 122.5(5) . .
N11 C13 C19 116.4(4) . .
C14 C13 C19 121.0(5) . .
C13 C14 C15 120.2(5) . .
C16 C15 C14 117.8(5) . .
C16 C15 C18 122.8(4) . .
C14 C15 C18 119.4(4) . .
C15 C16 C17 118.7(5) . .
N11 C17 C16 124.2(5) . .
O5 C18 O6 125.3(5) . .
O5 C18 C15 117.2(4) . .
O6 C18 C15 117.6(4) . .
N12 C19 C20 122.0(5) . .
N12 C19 C13 115.7(4) . .
C20 C19 C13 122.1(5) . .
C21 C20 C19 120.1(5) . .
C20 C21 C22 118.3(5) . .
C20 C21 C24 122.9(4) . 1_445
C22 C21 C24 118.8(4) . 1_445
C23 C22 C21 117.8(5) . .
N12 C23 C22 124.0(5) . .
O7 C24 O8 124.9(4) 2_776 .
O7 C24 C21 118.3(4) 2_776 1_665
O8 C24 C21 116.8(4) . 1_665
N21 C25 C26 122.8(5) . .
N21 C25 C25 116.1(6) . 2_655
C26 C25 C25 121.0(6) . 2_655
C25 C26 C27 118.7(5) . .
C28 C27 C26 119.0(5) . .
C28 C27 C30 122.3(5) . .
C26 C27 C30 118.6(5) . .
C29 C28 C27 119.0(5) . .
N21 C29 C28 123.5(5) . .
O10 C30 O9 125.2(5) 2_665 .
O10 C30 C27 117.4(4) 2_665 .
O9 C30 C27 117.5(4) . .
N31 C31 C32 121.6(4) . .
N31 C31 C31 115.6(5) . 2_876
C32 C31 C31 122.8(6) . 2_876
C31 C32 C33 120.1(5) . .
C32 C33 C34 118.3(5) . .
C32 C33 C36 121.4(5) . .
C34 C33 C36 120.3(5) . .
C35 C34 C33 117.5(5) . .
N31 C35 C34 124.7(5) . .
O11 C36 O12 125.4(5) . .
O11 C36 C33 118.1(5) . .
O12 C36 C33 116.5(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 O9 2.311(3) .
Eu1 O5 2.345(4) .
Eu1 O1 2.371(4) .
Eu1 O82 2.379(5) .
Eu1 O10 2.391(4) .
Eu1 O4 2.456(4) .
Eu1 O81 2.456(4) .
Eu1 O3 2.558(3) .
Eu1 Eu2 4.0831(18) .
Eu2 O7 2.283(3) .
Eu2 O11 2.337(4) .
Eu2 O6 2.341(3) .
Eu2 O8 2.354(3) .
Eu2 O83 2.457(4) .
Eu2 O3 2.461(3) .
Eu2 O2 2.474(3) .
Eu2 O1 2.752(4) .
O1 C6 1.272(6) .
O2 C6 1.247(6) .
O3 C12 1.287(6) .
O4 C12 1.246(6) .
O5 C18 1.249(6) .
O6 C18 1.257(6) .
O7 C24 1.249(6) 2_776
O8 C24 1.253(6) .
O9 C30 1.256(6) .
O10 C30 1.255(6) 2_665
O11 C36 1.246(7) .
O12 C36 1.248(7) .
N1 C5 1.342(6) .
N1 C1 1.356(6) .
N2 C7 1.335(7) .
N2 C11 1.343(7) .
N11 C17 1.334(7) .
N11 C13 1.344(7) .
N12 C23 1.336(7) .
N12 C19 1.344(7) .
N21 C25 1.347(7) .
N21 C29 1.356(7) .
N31 C35 1.337(7) .
N31 C31 1.351(6) .
C1 C2 1.392(7) .
C1 C7 1.483(7) .
C2 C3 1.388(7) .
C3 C4 1.389(7) .
C3 C6 1.505(6) .
C4 C5 1.381(7) .
C7 C8 1.393(7) .
C8 C9 1.391(7) 1_545
C9 C10 1.390(7) .
C9 C8 1.391(7) 1_565
C9 C12 1.484(6) .
C10 C11 1.374(8) 1_565
C11 C10 1.374(8) 1_545
C13 C14 1.376(7) .
C13 C19 1.495(7) .
C14 C15 1.388(7) .
C15 C16 1.367(7) .
C15 C18 1.496(7) .
C16 C17 1.387(8) .
C19 C20 1.387(7) .
C20 C21 1.378(7) .
C21 C22 1.398(7) .
C21 C24 1.510(6) 1_445
C22 C23 1.390(8) .
C24 O7 1.249(6) 2_776
C24 C21 1.510(6) 1_665
C25 C26 1.376(7) .
C25 C25 1.485(9) 2_655
C26 C27 1.394(7) .
C27 C28 1.373(8) .
C27 C30 1.498(7) .
C28 C29 1.362(8) .
C30 O10 1.255(6) 2_665
C31 C32 1.390(7) .
C31 C31 1.503(9) 2_876
C32 C33 1.393(7) .
C33 C34 1.404(7) .
C33 C36 1.512(7) .
C34 C35 1.384(7) .
