#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:32:33 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179584 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/49/4504963.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4504963
loop_
_publ_author_name
'Lü, Xing-Qiang'
'Jiang, Ji-Jun'
'Zhang, Li'
'Chen, Chun-Long'
'Su, Cheng-Yong'
'Kang, Bei-Sheng'
_publ_section_title
;
 Nonpenetrating Architectures of Cd(II) Complexes Constructed by
 Bispyridyl-Substituted Diphthalic Diimide Ligands of Varied Geometry
;
_journal_issue                   2
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              419
_journal_paper_doi               10.1021/cg049693b
_journal_volume                  5
_journal_year                    2005
_chemical_formula_sum            'C43 H28 Cd Cl3 N8 O12'
_chemical_formula_weight         1067.48
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 112.694(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.917(4)
_cell_length_b                   26.670(9)
_cell_length_c                   15.241(5)
_cell_measurement_temperature    293(2)
_cell_volume                     4469(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0311
_diffrn_reflns_av_sigmaI/netI    0.0448
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            23530
_diffrn_reflns_theta_full        27.07
_diffrn_reflns_theta_max         27.07
_diffrn_reflns_theta_min         1.64
_exptl_absorpt_coefficient_mu    0.740
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.587
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       column
_exptl_crystal_F_000             2148
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.751
_refine_diff_density_min         -0.823
_refine_diff_density_rms         0.096
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.026
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     604
_refine_ls_number_reflns         9646
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.026
_refine_ls_R_factor_all          0.0928
_refine_ls_R_factor_gt           0.0556
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1102P)²+3.3472P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1596
_refine_ls_wR_factor_ref         0.1882
_reflns_number_gt                6343
_reflns_number_total             9646
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg049693bsi20040906_041712.cif
_cod_data_source_block           1
_cod_original_cell_volume        4469(2)
_cod_original_sg_symbol_H-M      P21/n
_cod_database_code               4504963
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cd1 Cd 0.81301(3) 0.369506(12) 0.82492(2) 0.04691(14) Uani 1 1 d .
N1 N 0.7890(4) 0.43379(14) 0.9162(3) 0.0471(9) Uani 1 1 d .
O8 O 0.4459(4) 0.35827(16) 0.6828(3) 0.0739(11) Uani 1 1 d .
N7 N 0.5548(4) 0.36143(14) 0.7267(3) 0.0506(10) Uani 1 1 d .
O7 O 0.6095(4) 0.33414(13) 0.7980(3) 0.0639(10) Uani 1 1 d .
O9 O 0.6184(3) 0.39172(13) 0.7022(3) 0.0590(9) Uani 1 1 d .
O12 O 1.0280(4) 0.38955(16) 0.8640(3) 0.0685(10) Uani 1 1 d .
N5 N 0.8307(4) 0.30407(15) 0.7332(3) 0.0520(10) Uani 1 1 d .
O10 O 0.9005(4) 0.41995(16) 0.7348(3) 0.0729(11) Uani 1 1 d .
C1 C 0.7185(5) 0.42454(17) 0.9648(3) 0.0502(11) Uani 1 1 d .
H1A H 0.6820 0.3932 0.9579 0.060 Uiso 1 1 calc R
O11 O 1.0945(4) 0.42990(18) 0.7713(3) 0.0816(12) Uani 1 1 d .
C2 C 0.6970(4) 0.45811(18) 1.0236(3) 0.0480(11) Uani 1 1 d .
N3 N 0.8886(4) 0.32343(14) 0.9660(3) 0.0519(10) Uani 1 1 d .
N8 N 1.0089(5) 0.41319(16) 0.7895(3) 0.0570(11) Uani 1 1 d .
C3 C 0.7513(5) 0.50408(19) 1.0334(4) 0.0577(13) Uani 1 1 d .
H3A H 0.7381 0.5282 1.0724 0.069 Uiso 1 1 calc R
C17 C 0.9844(6) 0.2768(2) 1.1403(4) 0.0681(15) Uani 1 1 d .
H17A H 1.0165 0.2608 1.1990 0.082 Uiso 1 1 calc R
C16 C 1.0320(4) 0.32125(17) 1.1270(3) 0.0472(11) Uani 1 1 d .
C29 C 0.9190(5) 0.27013(17) 0.7711(3) 0.0484(11) Uani 1 1 d .
H29A H 0.9723 0.2743 0.8340 0.058 Uiso 1 1 calc R
C4 C 0.8246(5) 0.51446(18) 0.9860(4) 0.0598(13) Uani 1 1 d .
H4A H 0.8628 0.5455 0.9932 0.072 Uiso 1 1 calc R
C15 C 0.9823(5) 0.34288(18) 1.0387(3) 0.0502(11) Uani 1 1 d .
H15A H 1.0157 0.3728 1.0288 0.060 Uiso 1 1 calc R
C19 C 0.8428(5) 0.28026(18) 0.9808(4) 0.0600(13) Uani 1 1 d .
H19A H 0.7774 0.2662 0.9312 0.072 Uiso 1 1 calc R
C18 C 0.8882(6) 0.2556(2) 1.0664(4) 0.0730(17) Uani 1 1 d .
H18A H 0.8549 0.2253 1.0744 0.088 Uiso 1 1 calc R
N4 N 1.1064(4) 0.37144(14) 1.2745(3) 0.0501(9) Uani 1 1 d .
O2 O 0.7524(4) 0.38099(14) 1.2278(3) 0.0746(12) Uani 1 1 d .
C30 C 0.9350(4) 0.22916(16) 0.7214(3) 0.0447(10) Uani 1 1 d .
C28 C 1.1343(5) 0.3524(2) 1.3667(4) 0.0586(13) Uani 1 1 d .
O3 O 1.0302(4) 0.44395(15) 1.1924(3) 0.0717(11) Uani 1 1 d .
N2 N 0.6539(4) 0.45574(16) 1.1709(3) 0.0560(11) Uani 1 1 d .
C20 C 1.1389(5) 0.3463(2) 1.2035(4) 0.0566(12) Uani 1 1 d .
H20A H 1.2003 0.3212 1.2346 0.068 Uiso 1 1 calc R
H20B H 1.1742 0.3705 1.1742 0.068 Uiso 1 1 calc R
C32 C 0.7637(6) 0.2577(2) 0.5889(4) 0.0709(16) Uani 1 1 d .
H32A H 0.7092 0.2542 0.5262 0.085 Uiso 1 1 calc R
C14 C 0.7126(5) 0.42063(19) 1.2414(4) 0.0548(12) Uani 1 1 d .
C31 C 0.8540(6) 0.22350(19) 0.6283(4) 0.0635(15) Uani 1 1 d .
H31A H 0.8613 0.1963 0.5926 0.076 Uiso 1 1 calc R
C33 C 0.7543(6) 0.2977(2) 0.6433(4) 0.0621(14) Uani 1 1 d .
H33A H 0.6923 0.3209 0.6162 0.075 Uiso 1 1 calc R
C5 C 0.8419(5) 0.47870(17) 0.9274(3) 0.0492(11) Uani 1 1 d .
H5A H 0.8917 0.4860 0.8948 0.059 Uiso 1 1 calc R
C6 C 0.6106(5) 0.4439(2) 1.0701(4) 0.0618(14) Uani 1 1 d .
H6A H 0.5339 0.4611 1.0374 0.074 Uiso 1 1 calc R
H6B H 0.5950 0.4082 1.0620 0.074 Uiso 1 1 calc R
C21 C 1.0575(4) 0.41996(18) 1.2644(3) 0.0499(11) Uani 1 1 d .
O1 O 0.5544(4) 0.53074(16) 1.1596(3) 0.0733(11) Uani 1 1 d .
C24 C 1.0196(4) 0.47753(17) 1.4812(3) 0.0451(10) Uani 1 1 d .
C23 C 1.0131(5) 0.47421(18) 1.3885(3) 0.0499(11) Uani 1 1 d .
H23A H 0.9833 0.5009 1.3468 0.060 Uiso 1 1 calc R
C22 C 1.0512(4) 0.43104(16) 1.3588(3) 0.0430(10) Uani 1 1 d .
C12 C 0.7524(5) 0.42270(18) 1.4211(4) 0.0544(12) Uani 1 1 d .
H12A H 0.7919 0.3919 1.4355 0.065 Uiso 1 1 calc R
C27 C 1.0969(5) 0.39120(19) 1.4175(4) 0.0535(12) Uani 1 1 d .
C26 C 1.1053(6) 0.3928(2) 1.5101(4) 0.0706(16) Uani 1 1 d .
H26A H 1.1363 0.3658 1.5508 0.085 Uiso 1 1 calc R
C8 C 0.6545(4) 0.48805(17) 1.3100(3) 0.0462(10) Uani 1 1 d .
C13 C 0.7122(4) 0.44173(17) 1.3307(4) 0.0483(11) Uani 1 1 d .
C7 C 0.6145(5) 0.4968(2) 1.2071(4) 0.0553(12) Uani 1 1 d .
N6 N 0.9856(4) 0.14868(14) 0.8038(3) 0.0454(9) Uani 1 1 d .
C9 C 0.6333(4) 0.51585(16) 1.3793(3) 0.0430(10) Uani 1 1 d .
H9A H 0.5937 0.5466 1.3646 0.052 Uiso 1 1 calc R
C10 C 0.6725(4) 0.49660(16) 1.4708(3) 0.0406(9) Uani 1 1 d .
O4 O 1.1814(5) 0.31244(16) 1.3922(3) 0.0900(15) Uani 1 1 d .
C35 C 0.9825(5) 0.14522(17) 0.8935(3) 0.0472(11) Uani 1 1 d .
C11 C 0.7327(5) 0.45065(18) 1.4905(3) 0.0511(11) Uani 1 1 d .
H11A H 0.7606 0.4383 1.5523 0.061 Uiso 1 1 calc R
C34 C 1.0340(5) 0.19186(17) 0.7710(4) 0.0518(12) Uani 1 1 d .
H34A H 1.0707 0.1807 0.7276 0.062 Uiso 1 1 calc R
H34B H 1.0966 0.2078 0.8249 0.062 Uiso 1 1 calc R
C25 C 1.0664(6) 0.4356(2) 1.5408(4) 0.0629(14) Uani 1 1 d .
H25A H 1.0711 0.4369 1.6032 0.075 Uiso 1 1 calc R
O5 O 0.9288(4) 0.10061(14) 0.6678(2) 0.0616(9) Uani 1 1 d .
C36 C 0.9261(4) 0.09576(15) 0.8968(3) 0.0398(9) Uani 1 1 d .
C41 C 0.8984(4) 0.07268(16) 0.8094(3) 0.0409(10) Uani 1 1 d .
C42 C 0.9362(4) 0.10647(17) 0.7487(3) 0.0449(10) Uani 1 1 d .
O6 O 1.0209(4) 0.17704(13) 0.9545(3) 0.0688(11) Uani 1 1 d .
C40 C 0.8502(5) 0.02524(18) 0.7929(3) 0.0527(12) Uani 1 1 d .
H40A H 0.8332 0.0092 0.7350 0.063 Uiso 1 1 calc R
Cl1 Cl 0.5322(5) 0.2902(2) 0.9862(5) 0.259(3) Uani 1 1 d .
C43 C 0.3953(19) 0.2895(9) 0.8601(14) 0.333(16) Uani 1 1 d .
H43A H 0.4206 0.3018 0.8099 0.400 Uiso 1 1 calc R
C37 C 0.9029(4) 0.07271(15) 0.9692(3) 0.0427(10) Uani 1 1 d .
H37A H 0.9208 0.0888 1.0272 0.051 Uiso 1 1 calc R
C38 C 0.8518(4) 0.02460(16) 0.9533(3) 0.0390(9) Uani 1 1 d .
C39 C 0.8278(5) 0.00221(18) 0.8654(3) 0.0503(11) Uani 1 1 d .
H39A H 0.7950 -0.0299 0.8551 0.060 Uiso 1 1 calc R
Cl3 Cl 0.3660(4) 0.23091(17) 0.8492(4) 0.231(2) Uani 1 1 d .
Cl2 Cl 0.3008(6) 0.3308(2) 0.8824(4) 0.259(3) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
N1 Cd1 N5 178.04(15) .
N1 Cd1 N3 85.92(14) .
N5 Cd1 N3 93.85(14) .
N1 Cd1 O9 88.82(13) .
N5 Cd1 O9 90.07(14) .
N3 Cd1 O9 138.89(14) .
N1 Cd1 O10 96.32(14) .
N5 Cd1 O10 85.21(15) .
N3 Cd1 O10 135.70(15) .
O9 Cd1 O10 85.40(13) .
N1 Cd1 O12 93.01(14) .
N5 Cd1 O12 88.90(15) .
N3 Cd1 O12 83.99(14) .
O9 Cd1 O12 137.04(12) .
O10 Cd1 O12 51.73(13) .
N1 Cd1 O7 92.40(14) .
N5 Cd1 O7 85.64(15) .
N3 Cd1 O7 87.57(14) .
O9 Cd1 O7 51.92(12) .
O10 Cd1 O7 136.24(13) .
O12 Cd1 O7 169.62(13) .
C5 N1 C1 117.4(4) .
C5 N1 Cd1 125.9(3) .
C1 N1 Cd1 116.7(3) .
O8 N7 O9 121.3(4) .
O8 N7 O7 121.5(5) .
O9 N7 O7 117.2(4) .
N7 O7 Cd1 94.0(3) .
N7 O9 Cd1 96.9(3) .
N8 O12 Cd1 94.8(3) .
C33 N5 C29 118.0(4) .
C33 N5 Cd1 122.5(3) .
C29 N5 Cd1 119.5(3) .
N8 O10 Cd1 95.9(3) .
N1 C1 C2 124.1(4) .
C1 C2 C3 117.4(5) .
C1 C2 C6 118.8(4) .
C3 C2 C6 123.7(4) .
C19 N3 C15 117.4(4) .
C19 N3 Cd1 125.1(3) .
C15 N3 Cd1 117.5(3) .
O11 N8 O12 120.8(5) .
O11 N8 O10 121.8(4) .
O12 N8 O10 117.4(5) .
C4 C3 C2 120.0(5) .
C16 C17 C18 119.7(5) .
C17 C16 C15 117.8(5) .
C17 C16 C20 123.0(5) .
C15 C16 C20 119.2(5) .
N5 C29 C30 123.3(4) .
C3 C4 C5 119.4(5) .
N3 C15 C16 123.8(4) .
N3 C19 C18 122.6(5) .
C19 C18 C17 118.7(5) .
C21 N4 C28 111.7(4) .
C21 N4 C20 124.4(4) .
C28 N4 C20 123.5(4) .
C31 C30 C29 117.3(4) .
C31 C30 C34 123.0(4) .
C29 C30 C34 119.6(4) .
O4 C28 N4 123.0(5) .
O4 C28 C27 131.2(5) .
N4 C28 C27 105.7(4) .
C7 N2 C14 111.7(4) .
C7 N2 C6 123.7(5) .
C14 N2 C6 122.5(4) .
N4 C20 C16 113.2(4) .
C31 C32 C33 119.1(5) .
O2 C14 N2 124.7(5) .
O2 C14 C13 129.2(5) .
N2 C14 C13 106.0(4) .
C32 C31 C30 120.0(5) .
N5 C33 C32 122.3(5) .
N1 C5 C4 121.7(5) .
N2 C6 C2 114.5(4) .
O3 C21 N4 123.1(5) .
O3 C21 C22 132.5(5) .
N4 C21 C22 104.4(4) .
C23 C24 C25 117.2(4) .
C23 C24 C24 123.0(5) 3_768
C25 C24 C24 119.8(5) 3_768
C22 C23 C24 119.5(4) .
C27 C22 C23 122.5(4) .
C27 C22 C21 108.7(4) .
C23 C22 C21 128.7(4) .
C13 C12 C11 118.1(5) .
C22 C27 C26 120.1(5) .
C22 C27 C28 109.4(4) .
C26 C27 C28 130.5(5) .
C27 C26 C25 118.2(5) .
C13 C8 C9 121.4(4) .
C13 C8 C7 108.2(4) .
C9 C8 C7 130.2(4) .
C12 C13 C8 120.5(4) .
C12 C13 C14 131.5(5) .
C8 C13 C14 107.9(4) .
O1 C7 N2 124.5(5) .
O1 C7 C8 129.2(5) .
N2 C7 C8 106.1(4) .
C35 N6 C42 112.0(4) .
C35 N6 C34 123.7(4) .
C42 N6 C34 124.3(4) .
C10 C9 C8 118.4(4) .
C9 C10 C11 119.2(4) .
C9 C10 C38 120.1(4) 2_657
C11 C10 C38 120.6(4) 2_657
O6 C35 N6 124.4(4) .
O6 C35 C36 129.6(4) .
N6 C35 C36 106.0(4) .
C12 C11 C10 122.3(5) .
N6 C34 C30 110.9(4) .
C26 C25 C24 122.5(5) .
C37 C36 C41 121.5(4) .
C37 C36 C35 130.8(4) .
C41 C36 C35 107.7(4) .
C40 C41 C36 120.9(4) .
C40 C41 C42 130.8(4) .
C36 C41 C42 108.2(4) .
O5 C42 N6 124.5(4) .
O5 C42 C41 129.6(4) .
N6 C42 C41 106.0(4) .
C41 C40 C39 117.5(4) .
Cl3 C43 Cl2 121.4(8) .
Cl3 C43 Cl1 100.1(16) .
Cl2 C43 Cl1 99.3(6) .
C36 C37 C38 118.5(4) .
C39 C38 C37 118.3(4) .
C39 C38 C10 120.1(4) 2_647
C37 C38 C10 121.6(4) 2_647
C40 C39 C38 123.3(4) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cd1 N1 2.294(4) .
Cd1 N5 2.296(4) .
Cd1 N3 2.334(4) .
Cd1 O9 2.425(4) .
Cd1 O10 2.426(4) .
Cd1 O12 2.455(4) .
Cd1 O7 2.485(4) .
N1 C5 1.333(6) .
N1 C1 1.341(6) .
O8 N7 1.212(6) .
N7 O9 1.259(5) .
N7 O7 1.260(5) .
O12 N8 1.241(5) .
N5 C33 1.331(6) .
N5 C29 1.338(6) .
O10 N8 1.252(6) .
C1 C2 1.359(6) .
O11 N8 1.239(6) .
C2 C3 1.367(7) .
C2 C6 1.505(7) .
N3 C19 1.330(6) .
N3 C15 1.338(6) .
C3 C4 1.359(7) .
C17 C16 1.364(7) .
C17 C18 1.380(8) .
C16 C15 1.370(7) .
C16 C20 1.511(7) .
C29 C30 1.384(6) .
C4 C5 1.375(7) .
C19 C18 1.371(8) .
N4 C21 1.403(6) .
N4 C28 1.409(7) .
N4 C20 1.446(6) .
O2 C14 1.209(6) .
C30 C31 1.382(7) .
C30 C34 1.505(7) .
C28 O4 1.198(6) .
C28 C27 1.460(8) .
O3 C21 1.201(6) .
N2 C7 1.389(6) .
N2 C14 1.393(7) .
N2 C6 1.454(7) .
C32 C31 1.361(8) .
C32 C33 1.381(7) .
C14 C13 1.475(7) .
C21 C22 1.500(6) .
O1 C7 1.206(6) .
C24 C23 1.388(6) .
C24 C25 1.413(7) .
C24 C24 1.480(9) 3_768
C23 C22 1.376(6) .
C22 C27 1.360(7) .
C12 C13 1.369(7) .
C12 C11 1.386(7) .
C27 C26 1.377(7) .
C26 C25 1.380(8) .
C8 C13 1.390(7) .
C8 C9 1.390(6) .
C8 C7 1.472(7) .
N6 C35 1.386(6) .
N6 C42 1.392(6) .
N6 C34 1.459(6) .
C9 C10 1.387(6) .
C10 C11 1.393(6) .
C10 C38 1.497(6) 2_657
C35 O6 1.210(6) .
C35 C36 1.490(6) .
O5 C42 1.212(5) .
C36 C37 1.381(6) .
C36 C41 1.386(6) .
C41 C40 1.372(6) .
C41 C42 1.481(6) .
C40 C39 1.376(7) .
Cl1 C43 1.98(2) .
C43 Cl3 1.60(2) .
C43 Cl2 1.70(2) .
C37 C38 1.401(6) .
C38 C39 1.392(6) .
C38 C10 1.497(6) 2_647
