#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:52:30 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179601 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/65/4506538.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4506538
loop_
_publ_author_name
'Peuronen, Anssi'
'Valkonen, Arto'
'Kortelainen, Minna'
'Rissanen, Kari'
'Lahtinen, Manu'
_publ_section_title
;
 Halogen Bonding-Based “Catch and Release”: Reversible
 Solid-State Entrapment of Elemental Iodine with Monoalkylated DABCO Salts
;
_journal_issue                   8
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              4157
_journal_paper_doi               10.1021/cg300669t
_journal_volume                  12
_journal_year                    2012
_chemical_formula_moiety         'C14 H29 N2, F6 P, I2'
_chemical_formula_sum            'C14 H29 F6 I2 N2 P'
_chemical_formula_weight         624.16
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 108.112(5)
_cell_angle_gamma                90.000(5)
_cell_formula_units_Z            2
_cell_length_a                   9.99610(29)
_cell_length_b                   8.76200(29)
_cell_length_c                   13.64350(50)
_cell_measurement_reflns_used    2363
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.733
_cell_measurement_theta_min      0.407
_cell_volume                     1135.77(7)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       Collect
_computing_data_reduction        DENZO-SMN
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    SHELXS-97
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type
'Bruker-Nonius Kappa CCD with APEXII detector'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0580
_diffrn_reflns_av_sigmaI/netI    0.0389
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            15714
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.81
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.887
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.5943
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS 2008/1 (Bruker,2008)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.825
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             604
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.741
_refine_diff_density_min         -0.734
_refine_diff_density_rms         0.069
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     163
_refine_ls_number_reflns         2127
_refine_ls_number_restraints     85
_refine_ls_restrained_S_all      1.045
_refine_ls_R_factor_all          0.0916
_refine_ls_R_factor_gt           0.0488
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0502P)²+2.1300P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1123
_refine_ls_wR_factor_ref         0.1334
_reflns_number_gt                1251
_reflns_number_total             2127
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            cg300669t_si_002.cif
_cod_data_source_block           3PF6-I2_RT
_cod_original_cell_volume        1135.80(10)
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               4506538
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.2440(8) 0.6143(9) 0.7273(6) 0.101(2) Uani 1 1 d .
H1A H 0.3333 0.6146 0.7132 0.121 Uiso 1 1 calc R
H1B H 0.1929 0.5232 0.6966 0.121 Uiso 1 1 calc R
C2 C 0.2707(9) 0.6109(9) 0.8426(6) 0.102(2) Uani 1 1 d .
H2A H 0.2290 0.5198 0.8612 0.123 Uiso 1 1 calc R
H2B H 0.3711 0.6083 0.8780 0.123 Uiso 1 1 calc R
C3 C 0.0289(12) 0.7500 0.7026(11) 0.124(4) Uani 1 2 d S
H3A H -0.0251 0.6604 0.6721 0.149 Uiso 0.50 1 calc PR
H3B H -0.0251 0.8396 0.6721 0.149 Uiso 0.50 1 calc PR
C4 C 0.0529(11) 0.7500 0.8175(12) 0.139(5) Uani 1 2 d S
H4A H 0.0096 0.8396 0.8364 0.167 Uiso 0.50 1 calc PR
H4B H 0.0096 0.6604 0.8364 0.167 Uiso 0.50 1 calc PR
C5 C 0.2253(12) 0.7500 0.9878(9) 0.100(3) Uani 1 2 d S
H5A H 0.1782 0.6608 1.0034 0.121 Uiso 0.50 1 calc PR
H5B H 0.1782 0.8392 1.0034 0.121 Uiso 0.50 1 calc PR
C6 C 0.3755(13) 0.7500 1.0583(8) 0.098(3) Uani 1 2 d S
H6A H 0.4243 0.6603 1.0454 0.118 Uiso 0.50 1 calc PR
H6B H 0.4243 0.8397 1.0454 0.118 Uiso 0.50 1 calc PR
C7 C 0.3748(15) 0.7500 1.1673(10) 0.116(4) Uani 1 2 d S
H7A H 0.3242 0.6606 1.1786 0.139 Uiso 0.50 1 calc PR
H7B H 0.3242 0.8394 1.1786 0.139 Uiso 0.50 1 calc PR
C8 C 0.5184(18) 0.7500 1.2444(10) 0.133(5) Uani 1 2 d S
H8A H 0.5696 0.8396 1.2345 0.159 Uiso 0.50 1 calc PR
H8B H 0.5696 0.6604 1.2345 0.159 Uiso 0.50 1 calc PR
C9 C 0.508(2) 0.7500 1.3566(14) 0.196(8) Uani 1 2 d SU
H9A H 0.4553 0.8394 1.3652 0.235 Uiso 0.50 1 calc PR
H9B H 0.4553 0.6606 1.3652 0.235 Uiso 0.50 1 calc PR
C10 C 0.639(2) 0.7500 1.4341(15) 0.248(10) Uani 1 2 d SDU
H10A H 0.6898 0.8388 1.4224 0.298 Uiso 0.50 1 calc PR
H10B H 0.6898 0.6612 1.4224 0.298 Uiso 0.50 1 calc PR
C11 C 0.651(2) 0.7500 1.5477(16) 0.303(13) Uani 1 2 d SDU
H11A H 0.7066 0.6613 1.5777 0.363 Uiso 0.50 1 calc PR
H11B H 0.7066 0.8387 1.5777 0.363 Uiso 0.50 1 calc PR
N1 N 0.1626(8) 0.7500 0.6807(7) 0.090(2) Uani 1 2 d S
N2 N 0.2076(8) 0.7500 0.8746(7) 0.085(2) Uani 1 2 d S
F1 F 0.6286(15) 0.8842(16) 0.9350(13) 0.123(5) Uani 0.50 1 d PU
F2 F 0.7040(16) 0.8098(16) 1.0300(12) 0.189(7) Uani 0.50 1 d PU
F4 F 0.7651(11) 0.8230(14) 0.8388(8) 0.145(5) Uani 0.50 1 d PU
F5 F 0.861(2) 0.843(3) 1.0035(13) 0.162(8) Uani 0.50 1 d PU
F3 F 0.6030(18) 0.841(2) 0.8622(13) 0.176(7) Uani 0.50 1 d PU
F6 F 0.8419(18) 0.8815(18) 0.9441(15) 0.143(6) Uani 0.50 1 d PU
P1 P 0.7319(3) 0.7500 0.9323(3) 0.0890(8) Uani 1 2 d S
I1 I 0.10240(8) 0.7500 0.48502(6) 0.1053(4) Uani 1 2 d S
I2 I 0.02712(10) 0.7500 0.27235(7) 0.1258(4) Uani 1 2 d S
C12 C 0.538(3) 0.7500 1.583(2) 0.40(2) Uani 1 2 d SDU
H12A H 0.5696 0.7500 1.6566 0.603 Uiso 1 2 calc SR
H12B H 0.4823 0.6605 1.5579 0.603 Uiso 0.50 1 calc PR
H12C H 0.4823 0.8395 1.5579 0.603 Uiso 0.50 1 calc PR
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 C1 C2 111.2(6) . .
N1 C1 H1A 109.4 . .
C2 C1 H1A 109.4 . .
N1 C1 H1B 109.4 . .
C2 C1 H1B 109.4 . .
H1A C1 H1B 108.0 . .
N2 C2 C1 109.4(7) . .
N2 C2 H2A 109.8 . .
C1 C2 H2A 109.8 . .
N2 C2 H2B 109.8 . .
C1 C2 H2B 109.8 . .
H2A C2 H2B 108.2 . .
N1 C3 C4 110.7(10) . .
N1 C3 H3A 109.5 . .
C4 C3 H3A 109.5 . .
N1 C3 H3B 109.5 . .
C4 C3 H3B 109.5 . .
H3A C3 H3B 108.1 . .
N2 C4 C3 110.2(10) . .
N2 C4 H4A 109.6 . .
C3 C4 H4A 109.6 . .
N2 C4 H4B 109.6 . .
C3 C4 H4B 109.6 . .
H4A C4 H4B 108.1 . .
N2 C5 C6 115.6(8) . .
N2 C5 H5A 108.4 . .
C6 C5 H5A 108.4 . .
N2 C5 H5B 108.4 . .
C6 C5 H5B 108.4 . .
H5A C5 H5B 107.4 . .
C7 C6 C5 108.9(10) . .
C7 C6 H6A 109.9 . .
C5 C6 H6A 109.9 . .
C7 C6 H6B 109.9 . .
C5 C6 H6B 109.9 . .
H6A C6 H6B 108.3 . .
C6 C7 C8 113.7(11) . .
C6 C7 H7A 108.8 . .
C8 C7 H7A 108.8 . .
C6 C7 H7B 108.8 . .
C8 C7 H7B 108.8 . .
H7A C7 H7B 107.7 . .
C7 C8 C9 110.3(14) . .
C7 C8 H8A 109.6 . .
C9 C8 H8A 109.6 . .
C7 C8 H8B 109.6 . .
C9 C8 H8B 109.6 . .
H8A C8 H8B 108.1 . .
C10 C9 C8 113.9(19) . .
C10 C9 H9A 108.8 . .
C8 C9 H9A 108.8 . .
C10 C9 H9B 108.8 . .
C8 C9 H9B 108.8 . .
H9A C9 H9B 107.7 . .
C9 C10 C11 122(2) . .
C9 C10 H10A 106.9 . .
C11 C10 H10A 106.9 . .
C9 C10 H10B 106.9 . .
C11 C10 H10B 106.9 . .
H10A C10 H10B 106.7 . .
C12 C11 C10 123(2) . .
C12 C11 H11A 106.5 . .
C10 C11 H11A 106.5 . .
C12 C11 H11B 106.5 . .
C10 C11 H11B 106.5 . .
H11A C11 H11B 106.5 . .
C3 N1 C1 109.3(6) . 4_575
C3 N1 C1 109.3(6) . .
C1 N1 C1 108.0(8) 4_575 .
C2 N2 C2 108.9(8) 4_575 .
C2 N2 C4 107.9(6) 4_575 .
C2 N2 C4 107.9(6) . .
C2 N2 C5 112.0(5) 4_575 .
C2 N2 C5 112.0(5) . .
C4 N2 C5 107.9(8) . .
F3 F1 F2 128(2) . .
F3 F1 P1 70.5(14) . .
F2 F1 P1 61.2(7) . .
F2 F2 F1 116.9(8) 4_575 .
F2 F2 P1 70.1(6) 4_575 .
F1 F2 P1 63.7(7) . .
F2 F2 F5 99.7(9) 4_575 .
F1 F2 F5 89.4(10) . .
P1 F2 F5 57.2(7) . .
F4 F4 F6 110.1(8) 4_575 .
F4 F4 P1 65.7(5) 4_575 .
F6 F4 P1 61.8(6) . .
F4 F4 F3 95.1(8) 4_575 .
F6 F4 F3 91.2(10) . .
P1 F4 F3 56.0(6) . .
F6 F5 P1 74(2) . .
F6 F5 F5 113(3) . 4_575
P1 F5 F5 58.9(9) . 4_575
F6 F5 F2 109(3) . .
P1 F5 F2 54.9(8) . .
F5 F5 F2 80.3(9) 4_575 .
F1 F3 P1 71.6(14) . .
F1 F3 F3 112.0(17) . 4_575
P1 F3 F3 59.4(8) . 4_575
F1 F3 F4 104.2(19) . .
P1 F3 F4 55.5(6) . .
F3 F3 F4 84.9(8) 4_575 .
F5 F6 F4 133(3) . .
F5 F6 P1 75(2) . .
F4 F6 P1 61.0(7) . .
F2 P1 F2 39.9(12) . 4_575
F2 P1 F4 175.1(8) . 4_575
F2 P1 F4 135.7(8) 4_575 4_575
F2 P1 F4 135.7(8) . .
F2 P1 F4 175.1(9) 4_575 .
F4 P1 F4 48.6(10) 4_575 .
F2 P1 F3 111.6(8) . 4_575
F2 P1 F3 91.2(9) 4_575 4_575
F4 P1 F3 68.5(7) 4_575 4_575
F4 P1 F3 93.0(8) . 4_575
F2 P1 F3 91.2(9) . .
F2 P1 F3 111.6(8) 4_575 .
F4 P1 F3 93.0(8) 4_575 .
F4 P1 F3 68.5(7) . .
F3 P1 F3 61.2(15) 4_575 .
F2 P1 F6 88.3(9) . .
F2 P1 F6 118.2(10) 4_575 .
F4 P1 F6 93.7(9) 4_575 .
F4 P1 F6 57.2(8) . .
F3 P1 F6 148.9(10) 4_575 .
F3 P1 F6 96.2(10) . .
F2 P1 F6 118.2(10) . 4_575
F2 P1 F6 88.3(9) 4_575 4_575
F4 P1 F6 57.2(8) 4_575 4_575
F4 P1 F6 93.7(8) . 4_575
F3 P1 F6 96.2(10) 4_575 4_575
F3 P1 F6 148.9(10) . 4_575
F6 P1 F6 94.7(13) . 4_575
F2 P1 F1 86.4(8) . 4_575
F2 P1 F1 55.1(7) 4_575 4_575
F4 P1 F1 91.2(7) 4_575 4_575
F4 P1 F1 129.5(8) . 4_575
F3 P1 F1 37.9(7) 4_575 4_575
F3 P1 F1 88.4(8) . 4_575
F6 P1 F1 173.1(10) . 4_575
F6 P1 F1 83.8(8) 4_575 4_575
F2 P1 F1 55.1(7) . .
F2 P1 F1 86.4(8) 4_575 .
F4 P1 F1 129.5(8) 4_575 .
F4 P1 F1 91.2(7) . .
F3 P1 F1 88.4(8) 4_575 .
F3 P1 F1 37.9(7) . .
F6 P1 F1 83.8(8) . .
F6 P1 F1 173.1(10) 4_575 .
F1 P1 F1 96.8(11) 4_575 .
F2 P1 F5 67.9(9) . .
F2 P1 F5 88.6(10) 4_575 .
F4 P1 F5 112.1(9) 4_575 .
F4 P1 F5 87.2(8) . .
F3 P1 F5 179.3(12) 4_575 .
F3 P1 F5 118.3(11) . .
F6 P1 F5 31.1(8) . .
F6 P1 F5 84.5(9) 4_575 .
F1 P1 F5 142.1(9) 4_575 .
F1 P1 F5 90.9(11) . .
F2 P1 F5 88.6(10) . 4_575
F2 P1 F5 67.9(9) 4_575 4_575
F4 P1 F5 87.2(8) 4_575 4_575
F4 P1 F5 112.1(9) . 4_575
F3 P1 F5 118.3(11) 4_575 4_575
F3 P1 F5 179.3(12) . 4_575
F6 P1 F5 84.5(9) . 4_575
F6 P1 F5 31.1(8) 4_575 4_575
F1 P1 F5 90.9(11) 4_575 4_575
F1 P1 F5 142.1(9) . 4_575
F5 P1 F5 62.3(17) . 4_575
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N1 1.469(9) .
C1 C2 1.511(10) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C2 N2 1.498(8) .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C3 N1 1.458(14) .
C3 C4 1.510(19) .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C4 N2 1.500(14) .
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C5 N2 1.500(14) .
C5 C6 1.510(15) .
C5 H5A 0.9700 .
C5 H5B 0.9700 .
C6 C7 1.490(16) .
C6 H6A 0.9700 .
C6 H6B 0.9700 .
C7 C8 1.493(19) .
C7 H7A 0.9700 .
C7 H7B 0.9700 .
C8 C9 1.57(2) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C9 C10 1.40(3) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C10 C11 1.516(17) .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C11 C12 1.352(18) .
C11 H11A 0.9700 .
C11 H11B 0.9700 .
N1 C1 1.469(9) 4_575
N2 C2 1.498(8) 4_575
F1 F3 1.018(18) .
F1 F2 1.438(19) .
F1 P1 1.572(13) .
F2 F2 1.05(3) 4_575
F2 P1 1.536(11) .
F2 F5 1.74(2) .
F4 F4 1.28(2) 4_575
F4 F6 1.49(2) .
F4 P1 1.553(9) .
F4 F3 1.754(19) .
F5 F6 0.84(2) .
F5 P1 1.578(19) .
F5 F5 1.63(5) 4_575
F3 P1 1.562(16) .
F3 F3 1.59(4) 4_575
F6 P1 1.566(14) .
P1 F2 1.536(11) 4_575
P1 F4 1.553(9) 4_575
P1 F3 1.562(16) 4_575
P1 F6 1.566(14) 4_575
P1 F1 1.572(13) 4_575
P1 F5 1.578(19) 4_575
I1 I2 2.7620(16) .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N1 C1 C2 N2 -1.1(9) . .
N1 C3 C4 N2 0.000(4) . .
N2 C5 C6 C7 180.000(7) . .
C5 C6 C7 C8 180.000(7) . .
C6 C7 C8 C9 180.000(10) . .
C7 C8 C9 C10 180.000(13) . .
C8 C9 C10 C11 180.000(14) . .
C9 C10 C11 C12 0.00(2) . .
C4 C3 N1 C1 -59.0(5) . 4_575
C4 C3 N1 C1 59.0(5) . .
C2 C1 N1 C3 -58.7(9) . .
C2 C1 N1 C1 60.2(10) . 4_575
C1 C2 N2 C2 -58.0(10) . 4_575
C1 C2 N2 C4 59.0(9) . .
C1 C2 N2 C5 177.6(6) . .
C3 C4 N2 C2 58.8(5) . 4_575
C3 C4 N2 C2 -58.8(5) . .
C3 C4 N2 C5 180.000(5) . .
C6 C5 N2 C2 -61.3(5) . 4_575
C6 C5 N2 C2 61.3(5) . .
C6 C5 N2 C4 180.000(6) . .
F3 F1 F2 F2 -23(3) . 4_575
P1 F1 F2 F2 -47.3(6) . 4_575
F3 F1 F2 P1 25(2) . .
F3 F1 F2 F5 78(3) . .
P1 F1 F2 F5 53.2(9) . .
F2 F2 F5 F6 112(3) 4_575 .
F1 F2 F5 F6 -6(3) . .
P1 F2 F5 F6 53(3) . .
F2 F2 F5 P1 58.6(6) 4_575 .
F1 F2 F5 P1 -58.7(8) . .
F2 F2 F5 F5 0.000(7) 4_575 4_575
F1 F2 F5 F5 -117.2(7) . 4_575
P1 F2 F5 F5 -58.6(6) . 4_575
F2 F1 F3 P1 -23(2) . .
F2 F1 F3 F3 22(3) . 4_575
P1 F1 F3 F3 44.6(6) . 4_575
F2 F1 F3 F4 -69(3) . .
P1 F1 F3 F4 -45.6(10) . .
F4 F4 F3 F1 111.4(19) 4_575 .
F6 F4 F3 F1 1(2) . .
P1 F4 F3 F1 55.3(17) . .
F4 F4 F3 P1 56.0(6) 4_575 .
F6 F4 F3 P1 -54.2(8) . .
F4 F4 F3 F3 0.000(3) 4_575 4_575
F6 F4 F3 F3 -110.3(8) . 4_575
P1 F4 F3 F3 -56.0(6) . 4_575
P1 F5 F6 F4 -21(3) . .
F5 F5 F6 F4 23(4) 4_575 .
F2 F5 F6 F4 -64(5) . .
F5 F5 F6 P1 44.3(11) 4_575 .
F2 F5 F6 P1 -43.0(17) . .
F4 F4 F6 F5 -23(5) 4_575 .
P1 F4 F6 F5 23(4) . .
F3 F4 F6 F5 73(4) . .
F4 F4 F6 P1 -46.1(6) 4_575 .
F3 F4 F6 P1 49.7(8) . .
F1 F2 P1 F2 -135.8(7) . 4_575
F5 F2 P1 F2 116.5(9) . 4_575
F2 F2 P1 F4 -26(7) 4_575 4_575
F1 F2 P1 F4 -162(7) . 4_575
F5 F2 P1 F4 91(7) . 4_575
F2 F2 P1 F4 -177.0(10) 4_575 .
F1 F2 P1 F4 47.3(12) . .
F5 F2 P1 F4 -60.5(13) . .
F2 F2 P1 F3 64.0(8) 4_575 4_575
F1 F2 P1 F3 -71.8(10) . 4_575
F5 F2 P1 F3 -179.5(12) . 4_575
F2 F2 P1 F3 123.3(8) 4_575 .
F1 F2 P1 F3 -12.5(13) . .
F5 F2 P1 F3 -120.2(12) . .
F2 F2 P1 F6 -140.6(7) 4_575 .
F1 F2 P1 F6 83.7(10) . .
F5 F2 P1 F6 -24.1(12) . .
F2 F2 P1 F6 -46.1(8) 4_575 4_575
F1 F2 P1 F6 178.1(10) . 4_575
F5 F2 P1 F6 70.4(9) . 4_575
F2 F2 P1 F1 35.0(5) 4_575 4_575
F1 F2 P1 F1 -100.8(12) . 4_575
F5 F2 P1 F1 151.5(10) . 4_575
F2 F2 P1 F1 135.8(8) 4_575 .
F5 F2 P1 F1 -107.7(12) . .
F2 F2 P1 F5 -116.5(9) 4_575 .
F1 F2 P1 F5 107.7(12) . .
F2 F2 P1 F5 -56.0(10) 4_575 4_575
F1 F2 P1 F5 168.2(12) . 4_575
F5 F2 P1 F5 60.5(18) . 4_575
F4 F4 P1 F2 176.9(11) 4_575 .
F6 F4 P1 F2 44.9(13) . .
F3 F4 P1 F2 -68.2(13) . .
F4 F4 P1 F2 153(8) 4_575 4_575
F6 F4 P1 F2 21(8) . 4_575
F3 F4 P1 F2 -92(7) . 4_575
F6 F4 P1 F4 -132.0(8) . 4_575
F3 F4 P1 F4 115.0(8) . 4_575
F4 F4 P1 F3 -57.6(7) 4_575 4_575
F6 F4 P1 F3 170.4(11) . 4_575
F3 F4 P1 F3 57.3(15) . 4_575
F4 F4 P1 F3 -115.0(8) 4_575 .
F6 F4 P1 F3 113.0(12) . .
F4 F4 P1 F6 132.0(8) 4_575 .
F3 F4 P1 F6 -113.0(12) . .
F4 F4 P1 F6 38.8(7) 4_575 4_575
F6 F4 P1 F6 -93.2(14) . 4_575
F3 F4 P1 F6 153.7(10) . 4_575
F4 F4 P1 F1 -46.3(8) 4_575 4_575
F6 F4 P1 F1 -178.3(11) . 4_575
F3 F4 P1 F1 68.7(10) . 4_575
F4 F4 P1 F1 -146.1(6) 4_575 .
F6 F4 P1 F1 81.9(10) . .
F3 F4 P1 F1 -31.1(10) . .
F4 F4 P1 F5 123.1(9) 4_575 .
F6 F4 P1 F5 -8.9(16) . .
F3 F4 P1 F5 -121.9(13) . .
F4 F4 P1 F5 64.6(9) 4_575 4_575
F6 F4 P1 F5 -67.4(10) . 4_575
F3 F4 P1 F5 179.6(12) . 4_575
F1 F3 P1 F2 16.8(17) . .
F3 F3 P1 F2 -114.1(6) 4_575 .
F4 F3 P1 F2 139.6(8) . .
F1 F3 P1 F2 52(2) . 4_575
F3 F3 P1 F2 -78.9(8) 4_575 4_575
F4 F3 P1 F2 174.8(9) . 4_575
F1 F3 P1 F4 -165.7(17) . 4_575
F3 F3 P1 F4 63.4(5) 4_575 4_575
F4 F3 P1 F4 -42.9(9) . 4_575
F1 F3 P1 F4 -122.8(19) . .
F3 F3 P1 F4 106.3(7) 4_575 .
F1 F3 P1 F3 130.9(15) . 4_575
F4 F3 P1 F3 -106.3(7) . 4_575
F1 F3 P1 F6 -71.7(18) . .
F3 F3 P1 F6 157.5(8) 4_575 .
F4 F3 P1 F6 51.1(9) . .
F1 F3 P1 F6 178.4(16) . 4_575
F3 F3 P1 F6 47.6(16) 4_575 4_575
F4 F3 P1 F6 -59(2) . 4_575
F1 F3 P1 F1 103(2) . 4_575
F3 F3 P1 F1 -27.7(7) 4_575 4_575
F4 F3 P1 F1 -134.0(7) . 4_575
F3 F3 P1 F1 -130.9(15) 4_575 .
F4 F3 P1 F1 122.8(19) . .
F1 F3 P1 F5 -49(2) . .
F3 F3 P1 F5 -179.4(11) 4_575 .
F4 F3 P1 F5 74.2(11) . .
F1 F3 P1 F5 90(78) . 4_575
F3 F3 P1 F5 -41(78) 4_575 4_575
F4 F3 P1 F5 -148(78) . 4_575
F5 F6 P1 F2 47(3) . .
F4 F6 P1 F2 -150.5(9) . .
F5 F6 P1 F2 19(3) . 4_575
F4 F6 P1 F2 -178.0(7) . 4_575
F5 F6 P1 F4 -129(3) . 4_575
F4 F6 P1 F4 34.0(9) . 4_575
F5 F6 P1 F4 -163(3) . .
F5 F6 P1 F3 179(2) . 4_575
F4 F6 P1 F3 -19(2) . 4_575
F5 F6 P1 F3 138(3) . .
F4 F6 P1 F3 -59.5(9) . .
F5 F6 P1 F6 -71(3) . 4_575
F4 F6 P1 F6 91.4(10) . 4_575
F5 F6 P1 F1 7(10) . 4_575
F4 F6 P1 F1 169(7) . 4_575
F5 F6 P1 F1 102(3) . .
F4 F6 P1 F1 -95.4(9) . .
F4 F6 P1 F5 163(3) . .
F5 F6 P1 F5 -42(3) . 4_575
F4 F6 P1 F5 120.8(10) . 4_575
F3 F1 P1 F2 -159(2) . .
F3 F1 P1 F2 -132.8(19) . 4_575
F2 F1 P1 F2 26.6(9) . 4_575
F3 F1 P1 F4 19(2) . 4_575
F2 F1 P1 F4 178.0(8) . 4_575
F3 F1 P1 F4 51.5(18) . .
F2 F1 P1 F4 -149.1(8) . .
F3 F1 P1 F3 -41.5(18) . 4_575
F2 F1 P1 F3 117.9(10) . 4_575
F2 F1 P1 F3 159(2) . .
F3 F1 P1 F6 108.4(19) . .
F2 F1 P1 F6 -92.3(10) . .
F3 F1 P1 F6 -173(7) . 4_575
F2 F1 P1 F6 -14(8) . 4_575
F3 F1 P1 F1 -79(2) . 4_575
F2 F1 P1 F1 80.8(10) . 4_575
F3 F1 P1 F5 138.7(18) . .
F2 F1 P1 F5 -61.9(9) . .
F3 F1 P1 F5 -178.8(19) . 4_575
F2 F1 P1 F5 -19.4(19) . 4_575
F6 F5 P1 F2 -128(3) . .
F5 F5 P1 F2 100.6(10) 4_575 .
F6 F5 P1 F2 -163(3) . 4_575
F5 F5 P1 F2 65.6(6) 4_575 4_575
F2 F5 P1 F2 -35.0(11) . 4_575
F6 F5 P1 F4 57(3) . 4_575
F5 F5 P1 F4 -74.1(8) 4_575 4_575
F2 F5 P1 F4 -174.7(9) . 4_575
F6 F5 P1 F4 15(3) . .
F5 F5 P1 F4 -116.9(6) 4_575 .
F2 F5 P1 F4 142.5(9) . .
F6 F5 P1 F3 -90(78) . 4_575
F5 F5 P1 F3 138(78) 4_575 4_575
F2 F5 P1 F3 38(78) . 4_575
F6 F5 P1 F3 -49(3) . .
F5 F5 P1 F3 179.4(11) 4_575 .
F2 F5 P1 F3 78.8(10) . .
F5 F5 P1 F6 -131(2) 4_575 .
F2 F5 P1 F6 128(3) . .
F6 F5 P1 F6 109(3) . 4_575
F5 F5 P1 F6 -22.9(10) 4_575 4_575
F2 F5 P1 F6 -123.5(9) . 4_575
F6 F5 P1 F1 -178.7(19) . 4_575
F5 F5 P1 F1 49.8(13) 4_575 4_575
F2 F5 P1 F1 -50.8(19) . 4_575
F6 F5 P1 F1 -77(3) . .
F5 F5 P1 F1 152.0(8) 4_575 .
F2 F5 P1 F1 51.4(8) . .
F6 F5 P1 F5 131(2) . 4_575
F2 F5 P1 F5 -100.6(10) . 4_575
