#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:54:37 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179603 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/67/4506709.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4506709
loop_
_publ_author_name
'Cheng, Ping-Shing'
'Marivel, Samipillai'
'Zang, Shuang-Quan'
'Gao, Guang-Gang'
'Mak, Thomas C. W.'
_publ_section_title
;
 Argentophilic Infinite Chain, Column, and Layer Structures Assembled with
 the Multinuclear Silver(I)--Phenylethynide Supramolecular Synthon
;
_journal_issue                   9
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              4519
_journal_paper_doi               10.1021/cg300691n
_journal_volume                  12
_journal_year                    2012
_chemical_formula_moiety         'C36 H32 Ag5 As F6 O2 S2'
_chemical_formula_sum            'C36 H32 Ag5 As F6 O2 S2'
_chemical_formula_weight         1289.01
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 102.692(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   8.4617(12)
_cell_length_b                   27.714(4)
_cell_length_c                   17.932(2)
_cell_measurement_temperature    296(2)
_cell_volume                     4102.4(9)
_computing_cell_refinement       SAINT(Bruker,2001)
_computing_data_collection       APEX2(Bruker,2003)
_computing_data_reduction        APEX2(Bruker,2003)
_computing_molecular_graphics    DIAMOND
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'SMART CCD APEX II'
_diffrn_measurement_method       'ω and φ'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0741
_diffrn_reflns_av_sigmaI/netI    0.0699
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            24429
_diffrn_reflns_theta_full        23.21
_diffrn_reflns_theta_max         23.21
_diffrn_reflns_theta_min         1.38
_exptl_absorpt_coefficient_mu    3.305
_exptl_absorpt_correction_T_max  0.5578
_exptl_absorpt_correction_T_min  0.2888
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.087
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             2472
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.335
_refine_diff_density_min         -0.921
_refine_diff_density_rms         0.119
_refine_ls_extinction_coef       0.00013(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.005
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     470
_refine_ls_number_reflns         5721
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.018
_refine_ls_R_factor_all          0.1051
_refine_ls_R_factor_gt           0.0503
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0564P)²+10.5589P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1099
_refine_ls_wR_factor_ref         0.1330
_reflns_number_gt                3378
_reflns_number_total             5721
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg300691n_si_001.cif
_cod_data_source_block           3d
_cod_original_cell_volume        4102.4(10)
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               4506709
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.14605(11) 0.49443(3) 0.58492(5) 0.0578(3) Uani 1 1 d .
Ag2 Ag 0.04573(12) 0.41825(4) 0.46797(5) 0.0661(3) Uani 1 1 d .
Ag3 Ag 0.40125(10) 0.44503(3) 0.50564(4) 0.0551(3) Uani 1 1 d .
Ag4 Ag 0.50509(12) 0.51737(4) 0.63410(5) 0.0645(3) Uani 1 1 d .
Ag5 Ag 0.21685(13) 0.53806(4) 0.44261(6) 0.0841(4) Uani 1 1 d .
C1 C 0.0462(14) 0.4274(5) 0.6014(6) 0.062(3) Uani 1 1 d .
C2 C 0.0131(16) 0.3884(5) 0.6262(6) 0.065(3) Uani 1 1 d .
C3 C -0.016(2) 0.3439(5) 0.6580(8) 0.087(4) Uani 1 1 d .
C4 C 0.086(2) 0.3263(7) 0.7219(12) 0.142(8) Uani 1 1 d .
H4 H 0.1781 0.3436 0.7451 0.170 Uiso 1 1 calc R
C5 C 0.054(4) 0.2833(11) 0.7513(18) 0.197(14) Uani 1 1 d .
H5 H 0.1277 0.2713 0.7934 0.237 Uiso 1 1 calc R
C6 C -0.082(5) 0.2566(10) 0.723(2) 0.225(17) Uani 1 1 d .
H6 H -0.1084 0.2287 0.7464 0.270 Uiso 1 1 calc R
C7 C -0.175(5) 0.2741(8) 0.6577(15) 0.213(16) Uani 1 1 d .
H7 H -0.2590 0.2547 0.6318 0.256 Uiso 1 1 calc R
C8 C -0.156(3) 0.3188(6) 0.6262(10) 0.137(8) Uani 1 1 d .
H8 H -0.2326 0.3312 0.5856 0.164 Uiso 1 1 calc R
C9 C 0.2412(14) 0.4472(4) 0.4016(7) 0.061(3) Uani 1 1 d .
C10 C 0.1708(14) 0.4334(4) 0.3392(7) 0.059(3) Uani 1 1 d .
C11 C 0.0838(15) 0.4163(4) 0.2640(6) 0.063(3) Uani 1 1 d .
C12 C -0.0566(16) 0.3903(5) 0.2561(7) 0.083(4) Uani 1 1 d .
H12 H -0.0995 0.3828 0.2982 0.100 Uiso 1 1 calc R
C13 C -0.133(2) 0.3754(6) 0.1822(9) 0.104(5) Uani 1 1 d .
H13 H -0.2288 0.3578 0.1753 0.125 Uiso 1 1 calc R
C14 C -0.072(2) 0.3857(6) 0.1217(8) 0.105(5) Uani 1 1 d .
H14 H -0.1279 0.3764 0.0733 0.127 Uiso 1 1 calc R
C15 C 0.071(2) 0.4095(8) 0.1291(8) 0.126(7) Uani 1 1 d .
H15 H 0.1158 0.4139 0.0867 0.151 Uiso 1 1 calc R
C16 C 0.1510(19) 0.4273(7) 0.2001(8) 0.110(6) Uani 1 1 d .
H16 H 0.2448 0.4457 0.2053 0.132 Uiso 1 1 calc R
C17 C 0.2536(15) 0.5606(5) 0.5816(6) 0.063(3) Uani 1 1 d .
C18 C 0.3209(15) 0.5978(5) 0.6071(6) 0.062(3) Uani 1 1 d .
C19 C 0.3949(16) 0.6429(5) 0.6391(7) 0.066(3) Uani 1 1 d .
C20 C 0.478(2) 0.6445(6) 0.7130(8) 0.100(5) Uani 1 1 d .
H20 H 0.4906 0.6166 0.7424 0.120 Uiso 1 1 calc R
C21 C 0.545(3) 0.6876(7) 0.7451(11) 0.130(7) Uani 1 1 d .
H21 H 0.6009 0.6887 0.7958 0.156 Uiso 1 1 calc R
C22 C 0.527(3) 0.7277(8) 0.7018(17) 0.141(8) Uani 1 1 d .
H22 H 0.5694 0.7568 0.7229 0.169 Uiso 1 1 calc R
C23 C 0.449(3) 0.7260(7) 0.6299(16) 0.148(9) Uani 1 1 d .
H23 H 0.4397 0.7538 0.6003 0.178 Uiso 1 1 calc R
C24 C 0.380(2) 0.6840(7) 0.5976(10) 0.113(6) Uani 1 1 d .
H24 H 0.3234 0.6837 0.5469 0.135 Uiso 1 1 calc R
C25 C 0.5625(14) 0.4347(4) 0.6104(6) 0.055(3) Uani 1 1 d .
C26 C 0.6454(15) 0.4249(4) 0.6710(6) 0.056(3) Uani 1 1 d .
C27 C 0.7315(17) 0.4110(5) 0.7447(6) 0.068(4) Uani 1 1 d .
C28 C 0.685(2) 0.3696(6) 0.7786(9) 0.109(6) Uani 1 1 d .
H28 H 0.5985 0.3510 0.7529 0.131 Uiso 1 1 calc R
C29 C 0.771(3) 0.3565(8) 0.8523(13) 0.140(8) Uani 1 1 d .
H29 H 0.7374 0.3302 0.8772 0.169 Uiso 1 1 calc R
C30 C 0.901(3) 0.3826(11) 0.8864(10) 0.138(9) Uani 1 1 d .
H30 H 0.9630 0.3722 0.9331 0.166 Uiso 1 1 calc R
C31 C 0.945(2) 0.4225(9) 0.8553(9) 0.127(7) Uani 1 1 d .
H31 H 1.0306 0.4411 0.8815 0.152 Uiso 1 1 calc R
C32 C 0.859(2) 0.4363(7) 0.7823(7) 0.103(5) Uani 1 1 d .
H32 H 0.8909 0.4636 0.7596 0.123 Uiso 1 1 calc R
O1 O 0.4877(14) 0.5233(3) 0.7574(4) 0.104(3) Uani 1 1 d D
S1 S 0.4338(10) 0.4864(2) 0.8102(3) 0.171(3) Uani 1 1 d D
C33 C 0.290(5) 0.5055(11) 0.856(2) 0.42(3) Uani 1 1 d D
H33A H 0.1872 0.5067 0.8206 0.632 Uiso 1 1 calc R
H33B H 0.3179 0.5371 0.8768 0.632 Uiso 1 1 calc R
H33C H 0.2844 0.4835 0.8967 0.632 Uiso 1 1 calc R
C34 C 0.559(4) 0.4943(9) 0.9005(9) 0.227(15) Uani 1 1 d D
H34A H 0.6679 0.4858 0.8990 0.341 Uiso 1 1 calc R
H34B H 0.5218 0.4740 0.9366 0.341 Uiso 1 1 calc R
H34C H 0.5551 0.5274 0.9157 0.341 Uiso 1 1 calc R
O2 O 0.0140(16) 0.3379(4) 0.4460(8) 0.142(5) Uani 1 1 d .
S2 S 0.1275(9) 0.2953(2) 0.4479(4) 0.162(2) Uani 1 1 d D
C35 C 0.285(3) 0.3009(9) 0.5303(13) 0.227(15) Uani 1 1 d D
H35A H 0.3554 0.3269 0.5233 0.340 Uiso 1 1 calc R
H35B H 0.3456 0.2714 0.5386 0.340 Uiso 1 1 calc R
H35C H 0.2396 0.3076 0.5738 0.340 Uiso 1 1 calc R
C36 C 0.014(3) 0.2467(8) 0.476(3) 0.34(3) Uani 1 1 d D
H36A H -0.0782 0.2397 0.4357 0.512 Uiso 1 1 calc R
H36B H -0.0228 0.2558 0.5213 0.512 Uiso 1 1 calc R
H36C H 0.0811 0.2186 0.4867 0.512 Uiso 1 1 calc R
As1 As 0.4244(2) 0.35592(6) 0.00075(9) 0.0916(5) Uani 1 1 d .
F1 F 0.3012(15) 0.4041(4) -0.0231(6) 0.161(4) Uani 1 1 d .
F2 F 0.5749(16) 0.3881(6) -0.0154(7) 0.197(6) Uani 1 1 d .
F3 F 0.264(2) 0.3301(6) 0.0248(11) 0.259(8) Uani 1 1 d .
F4 F 0.544(3) 0.3114(5) 0.0257(9) 0.279(11) Uani 1 1 d .
F5 F 0.4717(17) 0.3771(5) 0.0907(5) 0.171(5) Uani 1 1 d .
F6 F 0.3766(19) 0.3347(6) -0.0858(7) 0.238(8) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C17 Ag1 C1 173.7(4) . .
C17 Ag1 Ag2 58.3(3) . 3_566
C1 Ag1 Ag2 124.3(3) . 3_566
C17 Ag1 Ag2 132.4(3) . .
C1 Ag1 Ag2 53.5(3) . .
Ag2 Ag1 Ag2 107.74(3) 3_566 .
C17 Ag1 Ag5 56.1(3) . .
C1 Ag1 Ag5 129.9(3) . .
Ag2 Ag1 Ag5 66.09(3) 3_566 .
Ag2 Ag1 Ag5 76.42(4) . .
C17 Ag1 Ag4 53.2(3) . .
C1 Ag1 Ag4 123.7(3) . .
Ag2 Ag1 Ag4 111.45(4) 3_566 .
Ag2 Ag1 Ag4 117.83(4) . .
Ag5 Ag1 Ag4 77.81(3) . .
C17 Ag1 Ag5 132.6(3) . 3_566
C1 Ag1 Ag5 49.7(3) . 3_566
Ag2 Ag1 Ag5 74.59(4) 3_566 3_566
Ag2 Ag1 Ag5 64.26(3) . 3_566
Ag5 Ag1 Ag5 110.71(3) . 3_566
Ag4 Ag1 Ag5 171.32(4) . 3_566
C17 Ag1 Ag3 91.3(3) . .
C1 Ag1 Ag3 90.9(3) . .
Ag2 Ag1 Ag3 126.50(4) 3_566 .
Ag2 Ag1 Ag3 59.28(3) . .
Ag5 Ag1 Ag3 60.41(3) . .
Ag4 Ag1 Ag3 58.72(3) . .
Ag5 Ag1 Ag3 123.35(4) 3_566 .
O2 Ag2 C9 108.2(5) . .
O2 Ag2 C1 104.5(5) . .
C9 Ag2 C1 127.8(4) . .
O2 Ag2 C17 95.4(5) . 3_566
C9 Ag2 C17 119.5(4) . 3_566
C1 Ag2 C17 96.1(4) . 3_566
O2 Ag2 Ag1 135.5(3) . 3_566
C9 Ag2 Ag1 87.5(3) . 3_566
C1 Ag2 Ag1 96.5(3) . 3_566
C17 Ag2 Ag1 43.0(3) 3_566 3_566
O2 Ag2 Ag1 145.8(3) . .
C9 Ag2 Ag1 89.5(3) . .
C1 Ag2 Ag1 44.3(3) . .
C17 Ag2 Ag1 101.0(3) 3_566 .
Ag1 Ag2 Ag1 72.26(4) 3_566 .
O2 Ag2 Ag3 110.7(3) . .
C9 Ag2 Ag3 42.5(3) . .
C1 Ag2 Ag3 88.2(3) . .
C17 Ag2 Ag3 151.6(3) 3_566 .
Ag1 Ag2 Ag3 108.66(4) 3_566 .
Ag1 Ag2 Ag3 63.36(3) . .
O2 Ag2 Ag5 112.6(4) . 3_566
C9 Ag2 Ag5 138.4(3) . 3_566
C1 Ag2 Ag5 47.2(3) . 3_566
C17 Ag2 Ag5 49.8(2) 3_566 3_566
Ag1 Ag2 Ag5 57.68(3) 3_566 3_566
Ag1 Ag2 Ag5 60.39(3) . 3_566
Ag3 Ag2 Ag5 123.56(4) . 3_566
C9 Ag3 C25 173.8(5) . .
C9 Ag3 Ag4 57.9(3) . 3_666
C25 Ag3 Ag4 124.3(3) . 3_666
C9 Ag3 Ag2 51.6(3) . .
C25 Ag3 Ag2 126.1(3) . .
Ag4 Ag3 Ag2 109.46(3) 3_666 .
C9 Ag3 Ag4 134.0(3) . .
C25 Ag3 Ag4 51.9(3) . .
Ag4 Ag3 Ag4 108.74(3) 3_666 .
Ag2 Ag3 Ag4 116.05(4) . .
C9 Ag3 Ag5 57.6(3) . .
C25 Ag3 Ag5 128.4(3) . .
Ag4 Ag3 Ag5 66.87(3) 3_666 .
Ag2 Ag3 Ag5 74.11(3) . .
Ag4 Ag3 Ag5 76.44(4) . .
C9 Ag3 Ag1 91.0(3) . .
C25 Ag3 Ag1 91.7(3) . .
Ag4 Ag3 Ag1 124.31(4) 3_666 .
Ag2 Ag3 Ag1 57.36(3) . .
Ag4 Ag3 Ag1 58.85(3) . .
Ag5 Ag3 Ag1 57.44(3) . .
C9 Ag3 Ag5 133.1(3) . 3_666
C25 Ag3 Ag5 48.6(3) . 3_666
Ag4 Ag3 Ag5 75.75(3) 3_666 3_666
Ag2 Ag3 Ag5 173.22(4) . 3_666
Ag4 Ag3 Ag5 64.97(3) . 3_666
Ag5 Ag3 Ag5 112.35(3) . 3_666
Ag1 Ag3 Ag5 123.75(4) . 3_666
O1 Ag4 C25 107.6(4) . .
O1 Ag4 C17 95.9(4) . .
C25 Ag4 C17 126.4(4) . .
O1 Ag4 C9 117.1(4) . 3_666
C25 Ag4 C9 96.2(4) . 3_666
C17 Ag4 C9 114.9(4) . 3_666
O1 Ag4 C18 87.5(4) . .
C25 Ag4 C18 152.5(4) . .
C17 Ag4 C18 26.8(4) . .
C9 Ag4 C18 96.9(4) 3_666 .
O1 Ag4 Ag3 152.5(2) . 3_666
C25 Ag4 Ag3 94.8(3) . 3_666
C17 Ag4 Ag3 82.8(3) . 3_666
C9 Ag4 Ag3 42.6(3) 3_666 3_666
C18 Ag4 Ag3 79.1(2) . 3_666
O1 Ag4 Ag3 136.2(2) . .
C25 Ag4 Ag3 43.2(3) . .
C17 Ag4 Ag3 87.1(3) . .
C9 Ag4 Ag3 100.5(3) 3_666 .
C18 Ag4 Ag3 110.5(3) . .
Ag3 Ag4 Ag3 71.26(3) 3_666 .
O1 Ag4 Ag1 91.3(3) . .
C25 Ag4 Ag1 88.7(3) . .
C17 Ag4 Ag1 42.3(3) . .
C9 Ag4 Ag1 147.7(3) 3_666 .
C18 Ag4 Ag1 67.7(3) . .
Ag3 Ag4 Ag1 105.25(3) 3_666 .
Ag3 Ag4 Ag1 62.43(3) . .
O1 Ag4 Ag5 129.8(3) . 3_666
C25 Ag4 Ag5 45.7(3) . 3_666
C17 Ag4 Ag5 134.3(3) . 3_666
C9 Ag4 Ag5 51.0(3) 3_666 3_666
C18 Ag4 Ag5 137.3(2) . 3_666
Ag3 Ag4 Ag5 58.25(3) 3_666 3_666
Ag3 Ag4 Ag5 59.83(3) . 3_666
Ag1 Ag4 Ag5 122.19(4) . 3_666
C1 Ag5 C25 119.5(4) 3_566 3_666
C1 Ag5 C17 97.5(4) 3_566 .
C25 Ag5 C17 112.1(4) 3_666 .
C1 Ag5 C9 114.4(4) 3_566 .
C25 Ag5 C9 94.3(4) 3_666 .
C17 Ag5 C9 120.7(4) . .
C1 Ag5 Ag1 95.5(3) 3_566 .
C25 Ag5 Ag1 141.5(3) 3_666 .
C17 Ag5 Ag1 42.6(3) . .
C9 Ag5 Ag1 84.0(2) . .
C1 Ag5 Ag3 144.2(3) 3_566 .
C25 Ag5 Ag3 91.9(3) 3_666 .
C17 Ag5 Ag3 84.4(3) . .
C9 Ag5 Ag3 40.9(3) . .
Ag1 Ag5 Ag3 62.14(3) . .
C1 Ag5 Ag1 41.8(3) 3_566 3_566
C25 Ag5 Ag1 148.2(3) 3_666 3_566
C17 Ag5 Ag1 97.5(3) . 3_566
C9 Ag5 Ag1 79.4(3) . 3_566
Ag1 Ag5 Ag1 69.29(3) . 3_566
Ag3 Ag5 Ag1 102.48(4) . 3_566
C1 Ag5 Ag3 147.7(3) 3_566 3_666
C25 Ag5 Ag3 40.7(3) 3_666 3_666
C17 Ag5 Ag3 77.3(3) . 3_666
C9 Ag5 Ag3 94.9(3) . 3_666
Ag1 Ag5 Ag3 100.97(4) . 3_666
Ag3 Ag5 Ag3 67.65(3) . 3_666
Ag1 Ag5 Ag3 169.03(4) 3_566 3_666
C1 Ag5 Ag2 47.6(3) 3_566 3_566
C25 Ag5 Ag2 139.1(3) 3_666 3_566
C17 Ag5 Ag2 50.8(3) . 3_566
C9 Ag5 Ag2 126.6(2) . 3_566
Ag1 Ag5 Ag2 56.23(3) . 3_566
Ag3 Ag5 Ag2 118.36(4) . 3_566
Ag1 Ag5 Ag2 55.36(3) 3_566 3_566
Ag3 Ag5 Ag2 124.07(4) 3_666 3_566
C1 Ag5 Ag4 137.3(3) 3_566 3_666
C25 Ag5 Ag4 45.7(3) 3_666 3_666
C17 Ag5 Ag4 125.1(3) . 3_666
C9 Ag5 Ag4 49.0(2) . 3_666
Ag1 Ag5 Ag4 117.01(4) . 3_666
Ag3 Ag5 Ag4 54.87(3) . 3_666
Ag1 Ag5 Ag4 123.80(5) 3_566 3_666
Ag3 Ag5 Ag4 55.20(3) 3_666 3_666
Ag2 Ag5 Ag4 173.23(4) 3_566 3_666
C2 C1 Ag1 165.6(10) . .
C2 C1 Ag5 101.7(9) . 3_566
Ag1 C1 Ag5 88.5(5) . 3_566
C2 C1 Ag2 108.5(9) . .
Ag1 C1 Ag2 82.3(4) . .
Ag5 C1 Ag2 85.2(4) 3_566 .
C1 C2 C3 176.5(15) . .
C4 C3 C8 119.5(16) . .
C4 C3 C2 121.4(17) . .
C8 C3 C2 119.1(15) . .
C5 C4 C3 120(2) . .
C5 C4 H4 120.2 . .
C3 C4 H4 120.2 . .
C4 C5 C6 124(3) . .
C4 C5 H5 118.1 . .
C6 C5 H5 118.1 . .
C7 C6 C5 114(3) . .
C7 C6 H6 122.9 . .
C5 C6 H6 122.9 . .
C6 C7 C8 125(3) . .
C6 C7 H7 117.4 . .
C8 C7 H7 117.4 . .
C3 C8 C7 117(2) . .
C3 C8 H8 121.6 . .
C7 C8 H8 121.6 . .
C10 C9 Ag3 157.8(11) . .
C10 C9 Ag2 95.8(8) . .
Ag3 C9 Ag2 85.8(4) . .
C10 C9 Ag4 99.2(8) . 3_666
Ag3 C9 Ag4 79.4(4) . 3_666
Ag2 C9 Ag4 164.9(6) . 3_666
C10 C9 Ag5 120.4(10) . .
Ag3 C9 Ag5 81.4(4) . .
Ag2 C9 Ag5 94.4(4) . .
Ag4 C9 Ag5 80.0(3) 3_666 .
C9 C10 C11 179.2(14) . .
C12 C11 C16 121.4(12) . .
C12 C11 C10 120.9(11) . .
C16 C11 C10 117.7(12) . .
C11 C12 C13 117.5(13) . .
C11 C12 H12 121.3 . .
C13 C12 H12 121.3 . .
C14 C13 C12 121.6(15) . .
C14 C13 H13 119.2 . .
C12 C13 H13 119.2 . .
C13 C14 C15 121.4(14) . .
C13 C14 H14 119.3 . .
C15 C14 H14 119.3 . .
C14 C15 C16 120.4(15) . .
C14 C15 H15 119.8 . .
C16 C15 H15 119.8 . .
C15 C16 C11 117.4(15) . .
C15 C16 H16 121.3 . .
C11 C16 H16 121.3 . .
C18 C17 Ag1 156.8(10) . .
C18 C17 Ag4 88.6(8) . .
Ag1 C17 Ag4 84.5(5) . .
C18 C17 Ag5 121.8(10) . .
Ag1 C17 Ag5 81.3(4) . .
Ag4 C17 Ag5 99.6(4) . .
C18 C17 Ag2 106.4(9) . 3_566
Ag1 C17 Ag2 78.7(4) . 3_566
Ag4 C17 Ag2 163.1(7) . 3_566
Ag5 C17 Ag2 79.4(3) . 3_566
C17 C18 C19 177.3(13) . .
C17 C18 Ag4 64.7(8) . .
C19 C18 Ag4 117.1(8) . .
C24 C19 C20 118.4(14) . .
C24 C19 C18 121.7(13) . .
C20 C19 C18 119.8(12) . .
C19 C20 C21 120.5(15) . .
C19 C20 H20 119.8 . .
C21 C20 H20 119.8 . .
C22 C21 C20 119.1(18) . .
C22 C21 H21 120.4 . .
C20 C21 H21 120.4 . .
C23 C22 C21 120.4(19) . .
C23 C22 H22 119.8 . .
C21 C22 H22 119.8 . .
C22 C23 C24 121.3(19) . .
C22 C23 H23 119.3 . .
C24 C23 H23 119.3 . .
C19 C24 C23 120.2(17) . .
C19 C24 H24 119.9 . .
C23 C24 H24 119.9 . .
C26 C25 Ag3 173.5(10) . .
C26 C25 Ag5 94.5(9) . 3_666
Ag3 C25 Ag5 90.7(4) . 3_666
C26 C25 Ag4 99.2(8) . .
Ag3 C25 Ag4 84.9(4) . .
Ag5 C25 Ag4 88.6(4) 3_666 .
C25 C26 C27 174.6(14) . .
C32 C27 C28 119.0(13) . .
C32 C27 C26 121.4(13) . .
C28 C27 C26 119.7(14) . .
C27 C28 C29 119.0(18) . .
C27 C28 H28 120.5 . .
C29 C28 H28 120.5 . .
C30 C29 C28 119.3(19) . .
C30 C29 H29 120.4 . .
C28 C29 H29 120.4 . .
C31 C30 C29 122.1(19) . .
C31 C30 H30 119.0 . .
C29 C30 H30 119.0 . .
C30 C31 C32 119(2) . .
C30 C31 H31 120.5 . .
C32 C31 H31 120.5 . .
C27 C32 C31 121.5(17) . .
C27 C32 H32 119.2 . .
C31 C32 H32 119.2 . .
S1 O1 Ag4 130.7(6) . .
O1 S1 C33 115.8(9) . .
O1 S1 C34 106.8(9) . .
C33 S1 C34 82(2) . .
S1 C33 H33A 109.5 . .
S1 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
S1 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
S1 C34 H34A 109.5 . .
S1 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
S1 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
S2 O2 Ag2 135.3(8) . .
O2 S2 C35 107.9(9) . .
O2 S2 C36 102.4(12) . .
C35 S2 C36 100.6(17) . .
S2 C35 H35A 109.5 . .
S2 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
S2 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
S2 C36 H36A 109.5 . .
S2 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
S2 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
F4 As1 F6 89.9(7) . .
F4 As1 F2 89.9(11) . .
F6 As1 F2 93.9(8) . .
F4 As1 F3 95.6(11) . .
F6 As1 F3 92.7(9) . .
F2 As1 F3 171.4(8) . .
F4 As1 F5 89.9(7) . .
F6 As1 F5 179.0(9) . .
F2 As1 F5 87.0(7) . .
F3 As1 F5 86.4(8) . .
F4 As1 F1 178.1(7) . .
F6 As1 F1 91.9(6) . .
F2 As1 F1 89.2(7) . .
F3 As1 F1 85.1(9) . .
F5 As1 F1 88.3(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C17 2.054(15) .
Ag1 C1 2.088(14) .
Ag1 Ag2 2.9518(14) 3_566
Ag1 Ag2 2.9652(13) .
Ag1 Ag5 3.0008(13) .
Ag1 Ag4 3.0389(14) .
Ag1 Ag5 3.1333(15) 3_566
Ag1 Ag3 3.1476(13) .
Ag2 O2 2.266(11) .
Ag2 C9 2.379(11) .
Ag2 C1 2.405(11) .
Ag2 C17 2.561(12) 3_566
Ag2 Ag1 2.9518(14) 3_566
Ag2 Ag3 3.0272(14) .
Ag2 Ag5 3.2464(14) 3_566
Ag3 C9 2.052(12) .
Ag3 C25 2.085(12) .
Ag3 Ag4 2.9775(12) 3_666
Ag3 Ag4 3.0345(13) .
Ag3 Ag5 3.0959(14) .
Ag3 Ag5 3.1946(15) 3_666
Ag4 O1 2.254(8) .
Ag4 C25 2.398(11) .
Ag4 C17 2.443(12) .
Ag4 C9 2.566(11) 3_666
Ag4 C18 2.702(12) .
Ag4 Ag3 2.9775(12) 3_666
Ag4 Ag5 3.3481(14) 3_666
Ag5 C1 2.392(12) 3_566
Ag5 C25 2.396(11) 3_666
Ag5 C17 2.521(11) .
Ag5 C9 2.644(12) .
Ag5 Ag1 3.1333(15) 3_566
Ag5 Ag3 3.1946(14) 3_666
Ag5 Ag2 3.2464(14) 3_566
Ag5 Ag4 3.3481(14) 3_666
C1 C2 1.223(16) .
C1 Ag5 2.392(12) 3_566
C2 C3 1.403(19) .
C3 C4 1.37(2) .
C3 C8 1.38(2) .
C4 C5 1.35(3) .
C4 H4 0.9300 .
C5 C6 1.37(4) .
C5 H5 0.9300 .
C6 C7 1.35(4) .
C6 H6 0.9300 .
C7 C8 1.39(3) .
C7 H7 0.9300 .
C8 H8 0.9300 .
C9 C10 1.208(14) .
C9 Ag4 2.566(11) 3_666
C10 C11 1.466(16) .
C11 C12 1.370(17) .
C11 C16 1.420(17) .
C12 C13 1.403(17) .
C12 H12 0.9300 .
C13 C14 1.33(2) .
C13 H13 0.9300 .
C14 C15 1.36(2) .
C14 H14 0.9300 .
C15 C16 1.393(19) .
C15 H15 0.9300 .
C16 H16 0.9300 .
C17 C18 1.218(16) .
C17 Ag2 2.561(12) 3_566
C18 C19 1.458(18) .
C19 C24 1.350(18) .
C19 C20 1.359(17) .
C20 C21 1.39(2) .
C20 H20 0.9300 .
C21 C22 1.34(3) .
C21 H21 0.9300 .
C22 C23 1.31(3) .
C22 H22 0.9300 .
C23 C24 1.37(2) .
C23 H23 0.9300 .
C24 H24 0.9300 .
C25 C26 1.187(13) .
C25 Ag5 2.396(11) 3_666
C26 C27 1.416(16) .
C27 C32 1.336(19) .
C27 C28 1.394(19) .
C28 C29 1.41(2) .
C28 H28 0.9300 .
C29 C30 1.35(3) .
C29 H29 0.9300 .
C30 C31 1.33(3) .
C30 H30 0.9300 .
C31 C32 1.40(2) .
C31 H31 0.9300 .
C32 H32 0.9300 .
O1 S1 1.528(7) .
S1 C33 1.695(15) .
S1 C34 1.742(16) .
C33 H33A 0.9600 .
C33 H33B 0.9600 .
C33 H33C 0.9600 .
C34 H34A 0.9600 .
C34 H34B 0.9600 .
C34 H34C 0.9600 .
O2 S2 1.519(12) .
S2 C35 1.766(15) .
S2 C36 1.792(17) .
C35 H35A 0.9600 .
C35 H35B 0.9600 .
C35 H35C 0.9600 .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
As1 F4 1.598(12) .
As1 F6 1.625(10) .
As1 F2 1.632(12) .
As1 F3 1.669(16) .
As1 F5 1.680(9) .
As1 F1 1.690(10) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C17 Ag1 Ag2 O2 147.5(8) . .
C1 Ag1 Ag2 O2 -29.6(7) . .
Ag2 Ag1 Ag2 O2 -149.5(6) 3_566 .
Ag5 Ag1 Ag2 O2 151.5(6) . .
Ag4 Ag1 Ag2 O2 83.4(6) . .
Ag5 Ag1 Ag2 O2 -87.2(6) 3_566 .
Ag3 Ag1 Ag2 O2 88.0(6) . .
C17 Ag1 Ag2 C9 24.6(5) . .
C1 Ag1 Ag2 C9 -152.5(5) . .
Ag2 Ag1 Ag2 C9 87.5(3) 3_566 .
Ag5 Ag1 Ag2 C9 28.5(3) . .
Ag4 Ag1 Ag2 C9 -39.6(3) . .
Ag5 Ag1 Ag2 C9 149.9(3) 3_566 .
Ag3 Ag1 Ag2 C9 -34.9(3) . .
C17 Ag1 Ag2 C1 177.1(6) . .
Ag2 Ag1 Ag2 C1 -120.0(4) 3_566 .
Ag5 Ag1 Ag2 C1 -179.0(4) . .
Ag4 Ag1 Ag2 C1 112.9(4) . .
Ag5 Ag1 Ag2 C1 -57.6(4) 3_566 .
Ag3 Ag1 Ag2 C1 117.6(4) . .
C17 Ag1 Ag2 C17 -95.4(5) . 3_566
C1 Ag1 Ag2 C17 87.5(5) . 3_566
Ag2 Ag1 Ag2 C17 -32.5(3) 3_566 3_566
Ag5 Ag1 Ag2 C17 -91.5(3) . 3_566
Ag4 Ag1 Ag2 C17 -159.6(3) . 3_566
Ag5 Ag1 Ag2 C17 29.9(3) 3_566 3_566
Ag3 Ag1 Ag2 C17 -154.9(3) . 3_566
C17 Ag1 Ag2 Ag1 -62.9(4) . 3_566
C1 Ag1 Ag2 Ag1 120.0(4) . 3_566
Ag2 Ag1 Ag2 Ag1 0.0 3_566 3_566
Ag5 Ag1 Ag2 Ag1 -59.00(3) . 3_566
Ag4 Ag1 Ag2 Ag1 -127.09(5) . 3_566
Ag5 Ag1 Ag2 Ag1 62.36(3) 3_566 3_566
Ag3 Ag1 Ag2 Ag1 -122.43(4) . 3_566
C17 Ag1 Ag2 Ag3 59.5(4) . .
C1 Ag1 Ag2 Ag3 -117.6(4) . .
Ag2 Ag1 Ag2 Ag3 122.43(4) 3_566 .
Ag5 Ag1 Ag2 Ag3 63.43(3) . .
Ag4 Ag1 Ag2 Ag3 -4.65(4) . .
Ag5 Ag1 Ag2 Ag3 -175.21(4) 3_566 .
C17 Ag1 Ag2 Ag5 -125.3(4) . 3_566
C1 Ag1 Ag2 Ag5 57.6(4) . 3_566
Ag2 Ag1 Ag2 Ag5 -62.36(3) 3_566 3_566
Ag5 Ag1 Ag2 Ag5 -121.36(3) . 3_566
Ag4 Ag1 Ag2 Ag5 170.55(4) . 3_566
Ag3 Ag1 Ag2 Ag5 175.21(4) . 3_566
O2 Ag2 Ag3 C9 94.8(6) . .
C1 Ag2 Ag3 C9 -160.4(5) . .
C17 Ag2 Ag3 C9 -60.9(7) 3_566 .
Ag1 Ag2 Ag3 C9 -64.1(4) 3_566 .
Ag1 Ag2 Ag3 C9 -122.2(4) . .
Ag5 Ag2 Ag3 C9 -127.2(4) 3_566 .
O2 Ag2 Ag3 C25 -78.0(5) . .
C9 Ag2 Ag3 C25 -172.8(6) . .
C1 Ag2 Ag3 C25 26.8(5) . .
C17 Ag2 Ag3 C25 126.3(6) 3_566 .
Ag1 Ag2 Ag3 C25 123.1(4) 3_566 .
Ag1 Ag2 Ag3 C25 65.0(4) . .
Ag5 Ag2 Ag3 C25 60.0(4) 3_566 .
O2 Ag2 Ag3 Ag4 98.0(4) . 3_666
C9 Ag2 Ag3 Ag4 3.2(4) . 3_666
C1 Ag2 Ag3 Ag4 -157.2(3) . 3_666
C17 Ag2 Ag3 Ag4 -57.7(5) 3_566 3_666
Ag1 Ag2 Ag3 Ag4 -60.87(5) 3_566 3_666
Ag1 Ag2 Ag3 Ag4 -118.92(4) . 3_666
Ag5 Ag2 Ag3 Ag4 -123.92(5) 3_566 3_666
O2 Ag2 Ag3 Ag4 -138.5(4) . .
C9 Ag2 Ag3 Ag4 126.8(4) . .
C1 Ag2 Ag3 Ag4 -33.6(3) . .
C17 Ag2 Ag3 Ag4 65.8(5) 3_566 .
Ag1 Ag2 Ag3 Ag4 62.64(5) 3_566 .
Ag1 Ag2 Ag3 Ag4 4.59(4) . .
Ag5 Ag2 Ag3 Ag4 -0.41(6) 3_566 .
O2 Ag2 Ag3 Ag5 155.8(4) . .
C9 Ag2 Ag3 Ag5 61.0(4) . .
C1 Ag2 Ag3 Ag5 -99.4(3) . .
C17 Ag2 Ag3 Ag5 0.1(5) 3_566 .
Ag1 Ag2 Ag3 Ag5 -3.13(4) 3_566 .
Ag1 Ag2 Ag3 Ag5 -61.18(3) . .
Ag5 Ag2 Ag3 Ag5 -66.18(5) 3_566 .
O2 Ag2 Ag3 Ag1 -143.1(4) . .
C9 Ag2 Ag3 Ag1 122.2(4) . .
C1 Ag2 Ag3 Ag1 -38.2(3) . .
C17 Ag2 Ag3 Ag1 61.2(5) 3_566 .
Ag1 Ag2 Ag3 Ag1 58.05(4) 3_566 .
Ag5 Ag2 Ag3 Ag1 -5.00(4) 3_566 .
O2 Ag2 Ag3 Ag5 -41.5(5) . 3_666
C9 Ag2 Ag3 Ag5 -136.3(6) . 3_666
C1 Ag2 Ag3 Ag5 63.3(5) . 3_666
C17 Ag2 Ag3 Ag5 162.8(6) 3_566 3_666
Ag1 Ag2 Ag3 Ag5 159.6(3) 3_566 3_666
Ag1 Ag2 Ag3 Ag5 101.6(3) . 3_666
Ag5 Ag2 Ag3 Ag5 96.6(3) 3_566 3_666
C17 Ag1 Ag3 C9 -98.9(4) . .
C1 Ag1 Ag3 C9 87.0(4) . .
Ag2 Ag1 Ag3 C9 -48.5(3) 3_566 .
Ag2 Ag1 Ag3 C9 41.6(3) . .
Ag5 Ag1 Ag3 C9 -49.7(3) . .
Ag4 Ag1 Ag3 C9 -143.2(3) . .
Ag5 Ag1 Ag3 C9 46.8(3) 3_566 .
C17 Ag1 Ag3 C25 86.6(4) . .
C1 Ag1 Ag3 C25 -87.4(4) . .
Ag2 Ag1 Ag3 C25 137.1(3) 3_566 .
Ag2 Ag1 Ag3 C25 -132.8(3) . .
Ag5 Ag1 Ag3 C25 135.8(3) . .
Ag4 Ag1 Ag3 C25 42.3(3) . .
Ag5 Ag1 Ag3 C25 -127.7(3) 3_566 .
C17 Ag1 Ag3 Ag4 -48.1(3) . 3_666
C1 Ag1 Ag3 Ag4 137.8(3) . 3_666
Ag2 Ag1 Ag3 Ag4 2.33(7) 3_566 3_666
Ag2 Ag1 Ag3 Ag4 92.40(5) . 3_666
Ag5 Ag1 Ag3 Ag4 1.07(5) . 3_666
Ag4 Ag1 Ag3 Ag4 -92.41(5) . 3_666
Ag5 Ag1 Ag3 Ag4 97.57(5) 3_566 3_666
C17 Ag1 Ag3 Ag2 -140.5(3) . .
C1 Ag1 Ag3 Ag2 45.4(3) . .
Ag2 Ag1 Ag3 Ag2 -90.07(5) 3_566 .
Ag5 Ag1 Ag3 Ag2 -91.33(4) . .
Ag4 Ag1 Ag3 Ag2 175.18(4) . .
Ag5 Ag1 Ag3 Ag2 5.17(4) 3_566 .
C17 Ag1 Ag3 Ag4 44.3(3) . .
C1 Ag1 Ag3 Ag4 -129.8(3) . .
Ag2 Ag1 Ag3 Ag4 94.75(5) 3_566 .
Ag2 Ag1 Ag3 Ag4 -175.18(4) . .
Ag5 Ag1 Ag3 Ag4 93.49(4) . .
Ag5 Ag1 Ag3 Ag4 -170.01(5) 3_566 .
C17 Ag1 Ag3 Ag5 -49.2(3) . .
C1 Ag1 Ag3 Ag5 136.8(3) . .
Ag2 Ag1 Ag3 Ag5 1.26(5) 3_566 .
Ag2 Ag1 Ag3 Ag5 91.33(4) . .
Ag4 Ag1 Ag3 Ag5 -93.49(4) . .
Ag5 Ag1 Ag3 Ag5 96.50(5) 3_566 .
C17 Ag1 Ag3 Ag5 47.5(3) . 3_666
C1 Ag1 Ag3 Ag5 -126.6(3) . 3_666
Ag2 Ag1 Ag3 Ag5 97.93(5) 3_566 3_666
Ag2 Ag1 Ag3 Ag5 -172.00(5) . 3_666
Ag5 Ag1 Ag3 Ag5 96.67(4) . 3_666
Ag4 Ag1 Ag3 Ag5 3.18(4) . 3_666
Ag5 Ag1 Ag3 Ag5 -166.83(5) 3_566 3_666
C9 Ag3 Ag4 O1 115.8(6) . .
C25 Ag3 Ag4 O1 -61.7(6) . .
Ag4 Ag3 Ag4 O1 178.9(4) 3_666 .
Ag2 Ag3 Ag4 O1 55.0(4) . .
Ag5 Ag3 Ag4 O1 119.5(4) . .
Ag1 Ag3 Ag4 O1 59.5(4) . .
Ag5 Ag3 Ag4 O1 -117.6(4) 3_666 .
C9 Ag3 Ag4 C25 177.5(6) . .
Ag4 Ag3 Ag4 C25 -119.4(4) 3_666 .
Ag2 Ag3 Ag4 C25 116.7(4) . .
Ag5 Ag3 Ag4 C25 -178.8(4) . .
Ag1 Ag3 Ag4 C25 121.2(4) . .
Ag5 Ag3 Ag4 C25 -55.8(4) 3_666 .
C9 Ag3 Ag4 C17 20.2(5) . .
C25 Ag3 Ag4 C17 -157.2(5) . .
Ag4 Ag3 Ag4 C17 83.4(3) 3_666 .
Ag2 Ag3 Ag4 C17 -40.5(3) . .
Ag5 Ag3 Ag4 C17 23.9(3) . .
Ag1 Ag3 Ag4 C17 -36.0(3) . .
Ag5 Ag3 Ag4 C17 146.9(3) 3_666 .
C9 Ag3 Ag4 C9 -94.6(5) . 3_666
C25 Ag3 Ag4 C9 87.9(5) . 3_666
Ag4 Ag3 Ag4 C9 -31.5(3) 3_666 3_666
Ag2 Ag3 Ag4 C9 -155.4(3) . 3_666
Ag5 Ag3 Ag4 C9 -90.9(3) . 3_666
Ag1 Ag3 Ag4 C9 -150.8(3) . 3_666
Ag5 Ag3 Ag4 C9 32.1(3) 3_666 3_666
C9 Ag3 Ag4 C18 6.9(5) . .
C25 Ag3 Ag4 C18 -170.5(5) . .
Ag4 Ag3 Ag4 C18 70.1(3) 3_666 .
Ag2 Ag3 Ag4 C18 -53.8(3) . .
Ag5 Ag3 Ag4 C18 10.6(3) . .
Ag1 Ag3 Ag4 C18 -49.3(3) . .
Ag5 Ag3 Ag4 C18 133.6(3) 3_666 .
C9 Ag3 Ag4 Ag3 -63.1(4) . 3_666
C25 Ag3 Ag4 Ag3 119.4(4) . 3_666
Ag4 Ag3 Ag4 Ag3 0.0 3_666 3_666
Ag2 Ag3 Ag4 Ag3 -123.88(5) . 3_666
Ag5 Ag3 Ag4 Ag3 -59.44(3) . 3_666
Ag1 Ag3 Ag4 Ag3 -119.37(4) . 3_666
Ag5 Ag3 Ag4 Ag3 63.55(3) 3_666 3_666
C9 Ag3 Ag4 Ag1 56.2(4) . .
C25 Ag3 Ag4 Ag1 -121.2(4) . .
Ag4 Ag3 Ag4 Ag1 119.37(4) 3_666 .
Ag2 Ag3 Ag4 Ag1 -4.51(4) . .
Ag5 Ag3 Ag4 Ag1 59.93(3) . .
Ag5 Ag3 Ag4 Ag1 -177.08(4) 3_666 .
C9 Ag3 Ag4 Ag5 -126.7(4) . 3_666
C25 Ag3 Ag4 Ag5 55.8(4) . 3_666
Ag4 Ag3 Ag4 Ag5 -63.55(3) 3_666 3_666
Ag2 Ag3 Ag4 Ag5 172.57(4) . 3_666
Ag5 Ag3 Ag4 Ag5 -122.99(3) . 3_666
Ag1 Ag3 Ag4 Ag5 177.08(4) . 3_666
C17 Ag1 Ag4 O1 97.4(4) . .
C1 Ag1 Ag4 O1 -75.9(4) . .
Ag2 Ag1 Ag4 O1 96.0(2) 3_566 .
Ag2 Ag1 Ag4 O1 -138.7(2) . .
Ag5 Ag1 Ag4 O1 154.0(2) . .
Ag5 Ag1 Ag4 O1 -37.0(4) 3_566 .
Ag3 Ag1 Ag4 O1 -143.4(2) . .
C17 Ag1 Ag4 C25 -155.1(5) . .
C1 Ag1 Ag4 C25 31.7(5) . .
Ag2 Ag1 Ag4 C25 -156.4(3) 3_566 .
Ag2 Ag1 Ag4 C25 -31.1(3) . .
Ag5 Ag1 Ag4 C25 -98.5(3) . .
Ag5 Ag1 Ag4 C25 70.6(4) 3_566 .
Ag3 Ag1 Ag4 C25 -35.8(3) . .
C1 Ag1 Ag4 C17 -173.3(5) . .
Ag2 Ag1 Ag4 C17 -1.4(4) 3_566 .
Ag2 Ag1 Ag4 C17 123.9(4) . .
Ag5 Ag1 Ag4 C17 56.6(4) . .
Ag5 Ag1 Ag4 C17 -134.4(5) 3_566 .
Ag3 Ag1 Ag4 C17 119.2(4) . .
C17 Ag1 Ag4 C9 -55.5(6) . 3_666
C1 Ag1 Ag4 C9 131.3(6) . 3_666
Ag2 Ag1 Ag4 C9 -56.8(5) 3_566 3_666
Ag2 Ag1 Ag4 C9 68.5(5) . 3_666
Ag5 Ag1 Ag4 C9 1.1(5) . 3_666
Ag5 Ag1 Ag4 C9 170.2(6) 3_566 3_666
Ag3 Ag1 Ag4 C9 63.8(5) . 3_666
C17 Ag1 Ag4 C18 10.6(5) . .
C1 Ag1 Ag4 C18 -162.6(4) . .
Ag2 Ag1 Ag4 C18 9.3(3) 3_566 .
Ag2 Ag1 Ag4 C18 134.5(2) . .
Ag5 Ag1 Ag4 C18 67.2(2) . .
Ag5 Ag1 Ag4 C18 -123.8(4) 3_566 .
Ag3 Ag1 Ag4 C18 129.9(2) . .
C17 Ag1 Ag4 Ag3 -60.4(4) . 3_666
C1 Ag1 Ag4 Ag3 126.3(4) . 3_666
Ag2 Ag1 Ag4 Ag3 -61.80(5) 3_566 3_666
Ag2 Ag1 Ag4 Ag3 63.48(5) . 3_666
Ag5 Ag1 Ag4 Ag3 -3.83(4) . 3_666
Ag5 Ag1 Ag4 Ag3 165.2(3) 3_566 3_666
Ag3 Ag1 Ag4 Ag3 58.80(4) . 3_666
C17 Ag1 Ag4 Ag3 -119.2(4) . .
C1 Ag1 Ag4 Ag3 67.5(4) . .
Ag2 Ag1 Ag4 Ag3 -120.60(4) 3_566 .
Ag2 Ag1 Ag4 Ag3 4.68(4) . .
Ag5 Ag1 Ag4 Ag3 -62.63(3) . .
Ag5 Ag1 Ag4 Ag3 106.4(3) 3_566 .
C17 Ag1 Ag4 Ag5 -122.2(4) . 3_666
C1 Ag1 Ag4 Ag5 64.5(4) . 3_666
Ag2 Ag1 Ag4 Ag5 -123.58(4) 3_566 3_666
Ag2 Ag1 Ag4 Ag5 1.70(6) . 3_666
Ag5 Ag1 Ag4 Ag5 -65.61(5) . 3_666
Ag5 Ag1 Ag4 Ag5 103.4(3) 3_566 3_666
Ag3 Ag1 Ag4 Ag5 -2.98(4) . 3_666
C17 Ag1 Ag5 C1 -95.1(5) . 3_566
C1 Ag1 Ag5 C1 87.3(5) . 3_566
Ag2 Ag1 Ag5 C1 -28.3(3) 3_566 3_566
Ag2 Ag1 Ag5 C1 88.4(3) . 3_566
Ag4 Ag1 Ag5 C1 -148.7(3) . 3_566
Ag5 Ag1 Ag5 C1 33.1(3) 3_566 3_566
Ag3 Ag1 Ag5 C1 150.6(3) . 3_566
C17 Ag1 Ag5 C25 61.6(6) . 3_666
C1 Ag1 Ag5 C25 -115.9(6) . 3_666
Ag2 Ag1 Ag5 C25 128.4(4) 3_566 3_666
Ag2 Ag1 Ag5 C25 -114.9(4) . 3_666
Ag4 Ag1 Ag5 C25 8.1(4) . 3_666
Ag5 Ag1 Ag5 C25 -170.2(4) 3_566 3_666
Ag3 Ag1 Ag5 C25 -52.7(4) . 3_666
C1 Ag1 Ag5 C17 -177.6(6) . .
Ag2 Ag1 Ag5 C17 66.7(4) 3_566 .
Ag2 Ag1 Ag5 C17 -176.5(4) . .
Ag4 Ag1 Ag5 C17 -53.6(4) . .
Ag5 Ag1 Ag5 C17 128.2(4) 3_566 .
Ag3 Ag1 Ag5 C17 -114.4(4) . .
C17 Ag1 Ag5 C9 150.9(5) . .
C1 Ag1 Ag5 C9 -26.7(5) . .
Ag2 Ag1 Ag5 C9 -142.3(3) 3_566 .
Ag2 Ag1 Ag5 C9 -25.6(3) . .
Ag4 Ag1 Ag5 C9 97.3(3) . .
Ag5 Ag1 Ag5 C9 -80.9(3) 3_566 .
Ag3 Ag1 Ag5 C9 36.5(3) . .
C17 Ag1 Ag5 Ag3 114.4(4) . .
C1 Ag1 Ag5 Ag3 -63.2(4) . .
Ag2 Ag1 Ag5 Ag3 -178.89(4) 3_566 .
Ag2 Ag1 Ag5 Ag3 -62.15(3) . .
Ag4 Ag1 Ag5 Ag3 60.78(3) . .
Ag5 Ag1 Ag5 Ag3 -117.46(4) 3_566 .
C17 Ag1 Ag5 Ag1 -128.2(4) . 3_566
C1 Ag1 Ag5 Ag1 54.2(4) . 3_566
Ag2 Ag1 Ag5 Ag1 -61.43(3) 3_566 3_566
Ag2 Ag1 Ag5 Ag1 55.31(3) . 3_566
Ag4 Ag1 Ag5 Ag1 178.24(5) . 3_566
Ag5 Ag1 Ag5 Ag1 0.0 3_566 3_566
Ag3 Ag1 Ag5 Ag1 117.46(4) . 3_566
C17 Ag1 Ag5 Ag3 57.1(4) . 3_666
C1 Ag1 Ag5 Ag3 -120.5(4) . 3_666
Ag2 Ag1 Ag5 Ag3 123.84(4) 3_566 3_666
Ag2 Ag1 Ag5 Ag3 -119.42(4) . 3_666
Ag4 Ag1 Ag5 Ag3 3.50(4) . 3_666
Ag5 Ag1 Ag5 Ag3 -174.73(5) 3_566 3_666
Ag3 Ag1 Ag5 Ag3 -57.27(4) . 3_666
C17 Ag1 Ag5 Ag2 -66.7(4) . 3_566
C1 Ag1 Ag5 Ag2 115.7(4) . 3_566
Ag2 Ag1 Ag5 Ag2 116.74(3) . 3_566
Ag4 Ag1 Ag5 Ag2 -120.33(4) . 3_566
Ag5 Ag1 Ag5 Ag2 61.43(3) 3_566 3_566
Ag3 Ag1 Ag5 Ag2 178.89(4) . 3_566
C17 Ag1 Ag5 Ag4 113.5(4) . 3_666
C1 Ag1 Ag5 Ag4 -64.1(4) . 3_666
Ag2 Ag1 Ag5 Ag4 -179.78(5) 3_566 3_666
Ag2 Ag1 Ag5 Ag4 -63.03(5) . 3_666
Ag4 Ag1 Ag5 Ag4 59.89(5) . 3_666
Ag5 Ag1 Ag5 Ag4 -118.35(5) 3_566 3_666
Ag3 Ag1 Ag5 Ag4 -0.88(4) . 3_666
C9 Ag3 Ag5 C1 58.5(6) . 3_566
C25 Ag3 Ag5 C1 -119.5(6) . 3_566
Ag4 Ag3 Ag5 C1 124.1(5) 3_666 3_566
Ag2 Ag3 Ag5 C1 4.2(5) . 3_566
Ag4 Ag3 Ag5 C1 -118.3(5) . 3_566
Ag1 Ag3 Ag5 C1 -56.8(5) . 3_566
Ag5 Ag3 Ag5 C1 -173.6(5) 3_666 3_566
C9 Ag3 Ag5 C25 -94.3(5) . 3_666
C25 Ag3 Ag5 C25 87.7(5) . 3_666
Ag4 Ag3 Ag5 C25 -28.7(3) 3_666 3_666
Ag2 Ag3 Ag5 C25 -148.6(3) . 3_666
Ag4 Ag3 Ag5 C25 88.8(3) . 3_666
Ag1 Ag3 Ag5 C25 150.3(3) . 3_666
Ag5 Ag3 Ag5 C25 33.6(3) 3_666 3_666
C9 Ag3 Ag5 C17 153.6(5) . .
C25 Ag3 Ag5 C17 -24.4(5) . .
Ag4 Ag3 Ag5 C17 -140.8(3) 3_666 .
Ag2 Ag3 Ag5 C17 99.3(3) . .
Ag4 Ag3 Ag5 C17 -23.2(3) . .
Ag1 Ag3 Ag5 C17 38.3(3) . .
Ag5 Ag3 Ag5 C17 -78.5(3) 3_666 .
C25 Ag3 Ag5 C9 -178.0(5) . .
Ag4 Ag3 Ag5 C9 65.6(4) 3_666 .
Ag2 Ag3 Ag5 C9 -54.3(4) . .
Ag4 Ag3 Ag5 C9 -176.9(4) . .
Ag1 Ag3 Ag5 C9 -115.4(4) . .
Ag5 Ag3 Ag5 C9 127.9(4) 3_666 .
C9 Ag3 Ag5 Ag1 115.4(4) . .
C25 Ag3 Ag5 Ag1 -62.7(4) . .
Ag4 Ag3 Ag5 Ag1 -179.04(4) 3_666 .
Ag2 Ag3 Ag5 Ag1 61.08(3) . .
Ag4 Ag3 Ag5 Ag1 -61.49(3) . .
Ag5 Ag3 Ag5 Ag1 -116.75(4) 3_666 .
C9 Ag3 Ag5 Ag1 57.1(4) . 3_566
C25 Ag3 Ag5 Ag1 -120.9(4) . 3_566
Ag4 Ag3 Ag5 Ag1 122.75(4) 3_666 3_566
Ag2 Ag3 Ag5 Ag1 2.86(3) . 3_566
Ag4 Ag3 Ag5 Ag1 -119.71(4) . 3_566
Ag1 Ag3 Ag5 Ag1 -58.22(4) . 3_566
Ag5 Ag3 Ag5 Ag1 -174.97(4) 3_666 3_566
C9 Ag3 Ag5 Ag3 -127.9(4) . 3_666
C25 Ag3 Ag5 Ag3 54.1(4) . 3_666
Ag4 Ag3 Ag5 Ag3 -62.28(3) 3_666 3_666
Ag2 Ag3 Ag5 Ag3 177.83(4) . 3_666
Ag4 Ag3 Ag5 Ag3 55.26(3) . 3_666
Ag1 Ag3 Ag5 Ag3 116.75(4) . 3_666
Ag5 Ag3 Ag5 Ag3 0.0 3_666 3_666
C9 Ag3 Ag5 Ag2 114.3(4) . 3_566
C25 Ag3 Ag5 Ag2 -63.7(4) . 3_566
Ag4 Ag3 Ag5 Ag2 179.92(5) 3_666 3_566
Ag2 Ag3 Ag5 Ag2 60.03(5) . 3_566
Ag4 Ag3 Ag5 Ag2 -62.54(5) . 3_566
Ag1 Ag3 Ag5 Ag2 -1.05(4) . 3_566
Ag5 Ag3 Ag5 Ag2 -117.80(5) 3_666 3_566
C9 Ag3 Ag5 Ag4 -65.6(4) . 3_666
C25 Ag3 Ag5 Ag4 116.4(4) . 3_666
Ag2 Ag3 Ag5 Ag4 -119.89(3) . 3_666
Ag4 Ag3 Ag5 Ag4 117.54(3) . 3_666
Ag1 Ag3 Ag5 Ag4 179.04(4) . 3_666
Ag5 Ag3 Ag5 Ag4 62.28(3) 3_666 3_666
C17 Ag1 C1 C2 -21(7) . .
Ag2 Ag1 C1 C2 -133(4) 3_566 .
Ag2 Ag1 C1 C2 139(4) . .
Ag5 Ag1 C1 C2 141(4) . .
Ag4 Ag1 C1 C2 38(4) . .
Ag5 Ag1 C1 C2 -135(4) 3_566 .
Ag3 Ag1 C1 C2 90(4) . .
C17 Ag1 C1 Ag5 114(4) . 3_566
Ag2 Ag1 C1 Ag5 2.0(5) 3_566 3_566
Ag2 Ag1 C1 Ag5 -85.3(3) . 3_566
Ag5 Ag1 C1 Ag5 -84.0(4) . 3_566
Ag4 Ag1 C1 Ag5 172.87(8) . 3_566
Ag3 Ag1 C1 Ag5 -135.0(3) . 3_566
C17 Ag1 C1 Ag2 -160(4) . .
Ag2 Ag1 C1 Ag2 87.3(3) 3_566 .
Ag5 Ag1 C1 Ag2 1.3(5) . .
Ag4 Ag1 C1 Ag2 -101.8(3) . .
Ag5 Ag1 C1 Ag2 85.3(3) 3_566 .
Ag3 Ag1 C1 Ag2 -49.6(2) . .
O2 Ag2 C1 C2 -6.8(10) . .
C9 Ag2 C1 C2 -134.4(9) . .
C17 Ag2 C1 C2 90.4(10) 3_566 .
Ag1 Ag2 C1 C2 133.7(9) 3_566 .
Ag1 Ag2 C1 C2 -170.2(11) . .
Ag3 Ag2 C1 C2 -117.7(9) . .
Ag5 Ag2 C1 C2 100.7(10) 3_566 .
O2 Ag2 C1 Ag1 163.3(4) . .
C9 Ag2 C1 Ag1 35.8(6) . .
C17 Ag2 C1 Ag1 -99.5(4) 3_566 .
Ag1 Ag2 C1 Ag1 -56.1(3) 3_566 .
Ag3 Ag2 C1 Ag1 52.4(3) . .
Ag5 Ag2 C1 Ag1 -89.1(4) 3_566 .
O2 Ag2 C1 Ag5 -107.5(5) . 3_566
C9 Ag2 C1 Ag5 124.9(4) . 3_566
C17 Ag2 C1 Ag5 -10.3(5) 3_566 3_566
Ag1 Ag2 C1 Ag5 33.0(3) 3_566 3_566
Ag1 Ag2 C1 Ag5 89.1(4) . 3_566
Ag3 Ag2 C1 Ag5 141.5(3) . 3_566
Ag1 C1 C2 C3 -13(25) . .
Ag5 C1 C2 C3 -147(21) 3_566 .
Ag2 C1 C2 C3 124(21) . .
C1 C2 C3 C4 4(22) . .
C1 C2 C3 C8 -180(100) . .
C8 C3 C4 C5 3(3) . .
C2 C3 C4 C5 179.4(19) . .
C3 C4 C5 C6 -3(5) . .
C4 C5 C6 C7 6(6) . .
C5 C6 C7 C8 -10(6) . .
C4 C3 C8 C7 -6(3) . .
C2 C3 C8 C7 177.4(17) . .
C6 C7 C8 C3 10(5) . .
C25 Ag3 C9 C10 -25(6) . .
Ag4 Ag3 C9 C10 88(3) 3_666 .
Ag2 Ag3 C9 C10 -95(3) . .
Ag4 Ag3 C9 C10 174(2) . .
Ag5 Ag3 C9 C10 170(3) . .
Ag1 Ag3 C9 C10 -141(3) . .
Ag5 Ag3 C9 C10 78(3) 3_666 .
C25 Ag3 C9 Ag2 70(4) . .
Ag4 Ag3 C9 Ag2 -176.4(5) 3_666 .
Ag4 Ag3 C9 Ag2 -90.8(4) . .
Ag5 Ag3 C9 Ag2 -95.1(3) . .
Ag1 Ag3 C9 Ag2 -45.5(3) . .
Ag5 Ag3 C9 Ag2 173.58(8) 3_666 .
C25 Ag3 C9 Ag4 -113(4) . 3_666
Ag2 Ag3 C9 Ag4 176.4(5) . 3_666
Ag4 Ag3 C9 Ag4 85.6(4) . 3_666
Ag5 Ag3 C9 Ag4 81.3(3) . 3_666
Ag1 Ag3 C9 Ag4 130.9(2) . 3_666
Ag5 Ag3 C9 Ag4 -10.0(5) 3_666 3_666
C25 Ag3 C9 Ag5 165(4) . .
Ag4 Ag3 C9 Ag5 -81.3(3) 3_666 .
Ag2 Ag3 C9 Ag5 95.1(3) . .
Ag4 Ag3 C9 Ag5 4.3(5) . .
Ag1 Ag3 C9 Ag5 49.6(2) . .
Ag5 Ag3 C9 Ag5 -91.3(4) 3_666 .
O2 Ag2 C9 C10 56.7(10) . .
C1 Ag2 C9 C10 -177.2(8) . .
C17 Ag2 C9 C10 -50.8(10) 3_566 .
Ag1 Ag2 C9 C10 -80.8(8) 3_566 .
Ag1 Ag2 C9 C10 -153.1(8) . .
Ag3 Ag2 C9 C10 157.7(11) . .
Ag5 Ag2 C9 C10 -112.0(8) 3_566 .
O2 Ag2 C9 Ag3 -101.0(5) . .
C1 Ag2 C9 Ag3 25.1(7) . .
C17 Ag2 C9 Ag3 151.5(4) 3_566 .
Ag1 Ag2 C9 Ag3 121.4(3) 3_566 .
Ag1 Ag2 C9 Ag3 49.2(3) . .
Ag5 Ag2 C9 Ag3 90.2(5) 3_566 .
O2 Ag2 C9 Ag4 -115(2) . 3_666
C1 Ag2 C9 Ag4 11(2) . 3_666
C17 Ag2 C9 Ag4 138(2) 3_566 3_666
Ag1 Ag2 C9 Ag4 108(2) 3_566 3_666
Ag1 Ag2 C9 Ag4 35(2) . 3_666
Ag3 Ag2 C9 Ag4 -13.7(18) . 3_666
Ag5 Ag2 C9 Ag4 77(2) 3_566 3_666
O2 Ag2 C9 Ag5 177.9(4) . .
C1 Ag2 C9 Ag5 -56.0(6) . .
C17 Ag2 C9 Ag5 70.4(5) 3_566 .
Ag1 Ag2 C9 Ag5 40.4(3) 3_566 .
Ag1 Ag2 C9 Ag5 -31.9(3) . .
Ag3 Ag2 C9 Ag5 -81.1(4) . .
Ag5 Ag2 C9 Ag5 9.2(6) 3_566 .
C1 Ag5 C9 C10 37.7(11) 3_566 .
C25 Ag5 C9 C10 -87.5(10) 3_666 .
C17 Ag5 C9 C10 153.6(9) . .
Ag1 Ag5 C9 C10 131.1(10) . .
Ag3 Ag5 C9 C10 -175.5(12) . .
Ag1 Ag5 C9 C10 61.1(10) 3_566 .
Ag3 Ag5 C9 C10 -128.4(10) 3_666 .
Ag2 Ag5 C9 C10 91.8(10) 3_566 .
Ag4 Ag5 C9 C10 -94.8(10) 3_666 .
C1 Ag5 C9 Ag3 -146.8(4) 3_566 .
C25 Ag5 C9 Ag3 88.0(4) 3_666 .
C17 Ag5 C9 Ag3 -31.0(5) . .
Ag1 Ag5 C9 Ag3 -53.5(3) . .
Ag1 Ag5 C9 Ag3 -123.4(3) 3_566 .
Ag3 Ag5 C9 Ag3 47.1(3) 3_666 .
Ag2 Ag5 C9 Ag3 -92.7(3) 3_566 .
Ag4 Ag5 C9 Ag3 80.7(3) 3_666 .
C1 Ag5 C9 Ag2 -61.7(5) 3_566 .
C25 Ag5 C9 Ag2 173.1(4) 3_666 .
C17 Ag5 C9 Ag2 54.2(5) . .
Ag1 Ag5 C9 Ag2 31.7(3) . .
Ag3 Ag5 C9 Ag2 85.1(4) . .
Ag1 Ag5 C9 Ag2 -38.3(3) 3_566 .
Ag3 Ag5 C9 Ag2 132.2(3) 3_666 .
Ag2 Ag5 C9 Ag2 -7.6(5) 3_566 .
Ag4 Ag5 C9 Ag2 165.8(5) 3_666 .
C1 Ag5 C9 Ag4 132.5(4) 3_566 3_666
C25 Ag5 C9 Ag4 7.3(4) 3_666 3_666
C17 Ag5 C9 Ag4 -111.7(4) . 3_666
Ag1 Ag5 C9 Ag4 -134.2(2) . 3_666
Ag3 Ag5 C9 Ag4 -80.7(3) . 3_666
Ag1 Ag5 C9 Ag4 155.8(3) 3_566 3_666
Ag3 Ag5 C9 Ag4 -33.6(2) 3_666 3_666
Ag2 Ag5 C9 Ag4 -173.39(6) 3_566 3_666
Ag3 C9 C10 C11 84(100) . .
Ag2 C9 C10 C11 -9(100) . .
Ag4 C9 C10 C11 169(100) 3_666 .
Ag5 C9 C10 C11 -108(100) . .
C9 C10 C11 C12 6(100) . .
C9 C10 C11 C16 -174(100) . .
C16 C11 C12 C13 -1(2) . .
C10 C11 C12 C13 179.8(12) . .
C11 C12 C13 C14 0(2) . .
C12 C13 C14 C15 3(3) . .
C13 C14 C15 C16 -5(3) . .
C14 C15 C16 C11 5(3) . .
C12 C11 C16 C15 -2(2) . .
C10 C11 C16 C15 177.7(15) . .
C1 Ag1 C17 C18 -11(6) . .
Ag2 Ag1 C17 C18 105(3) 3_566 .
Ag2 Ag1 C17 C18 -169(2) . .
Ag5 Ag1 C17 C18 -174(3) . .
Ag4 Ag1 C17 C18 -73(3) . .
Ag5 Ag1 C17 C18 98(3) 3_566 .
Ag3 Ag1 C17 C18 -122(3) . .
C1 Ag1 C17 Ag4 62(4) . .
Ag2 Ag1 C17 Ag4 178.5(4) 3_566 .
Ag2 Ag1 C17 Ag4 -96.0(3) . .
Ag5 Ag1 C17 Ag4 -100.6(4) . .
Ag5 Ag1 C17 Ag4 171.57(8) 3_566 .
Ag3 Ag1 C17 Ag4 -48.2(2) . .
C1 Ag1 C17 Ag5 163(4) . .
Ag2 Ag1 C17 Ag5 -80.8(3) 3_566 .
Ag2 Ag1 C17 Ag5 4.6(5) . .
Ag4 Ag1 C17 Ag5 100.6(3) . .
Ag5 Ag1 C17 Ag5 -87.8(4) 3_566 .
Ag3 Ag1 C17 Ag5 52.4(2) . .
C1 Ag1 C17 Ag2 -116(4) . 3_566
Ag2 Ag1 C17 Ag2 85.4(4) . 3_566
Ag5 Ag1 C17 Ag2 80.8(3) . 3_566
Ag4 Ag1 C17 Ag2 -178.5(4) . 3_566
Ag5 Ag1 C17 Ag2 -7.0(5) 3_566 3_566
Ag3 Ag1 C17 Ag2 133.25(18) . 3_566
O1 Ag4 C17 C18 72.4(8) . .
C25 Ag4 C17 C18 -170.7(7) . .
C9 Ag4 C17 C18 -51.2(9) 3_666 .
Ag3 Ag4 C17 C18 -80.0(8) 3_666 .
Ag3 Ag4 C17 C18 -151.5(8) . .
Ag1 Ag4 C17 C18 157.8(10) . .
Ag5 Ag4 C17 C18 -110.2(8) 3_666 .
O1 Ag4 C17 Ag1 -85.4(4) . .
C25 Ag4 C17 Ag1 31.6(6) . .
C9 Ag4 C17 Ag1 151.0(4) 3_666 .
C18 Ag4 C17 Ag1 -157.8(10) . .
Ag3 Ag4 C17 Ag1 122.2(3) 3_666 .
Ag3 Ag4 C17 Ag1 50.8(3) . .
Ag5 Ag4 C17 Ag1 92.0(4) 3_666 .
O1 Ag4 C17 Ag5 -165.6(4) . .
C25 Ag4 C17 Ag5 -48.6(6) . .
C9 Ag4 C17 Ag5 70.8(6) 3_666 .
C18 Ag4 C17 Ag5 122.0(10) . .
Ag3 Ag4 C17 Ag5 42.1(4) 3_666 .
Ag3 Ag4 C17 Ag5 -29.4(4) . .
Ag1 Ag4 C17 Ag5 -80.2(5) . .
Ag5 Ag4 C17 Ag5 11.8(7) 3_666 .
O1 Ag4 C17 Ag2 -80.4(17) . 3_566
C25 Ag4 C17 Ag2 36.6(19) . 3_566
C9 Ag4 C17 Ag2 156.0(16) 3_666 3_566
C18 Ag4 C17 Ag2 -153(2) . 3_566
Ag3 Ag4 C17 Ag2 127.2(17) 3_666 3_566
Ag3 Ag4 C17 Ag2 55.8(17) . 3_566
Ag1 Ag4 C17 Ag2 5.0(14) . 3_566
Ag5 Ag4 C17 Ag2 97.0(17) 3_666 3_566
C1 Ag5 C17 C18 -92.8(11) 3_566 .
C25 Ag5 C17 C18 33.4(12) 3_666 .
C9 Ag5 C17 C18 143.0(10) . .
Ag1 Ag5 C17 C18 177.2(13) . .
Ag3 Ag5 C17 C18 123.2(11) . .
Ag1 Ag5 C17 C18 -134.9(11) 3_566 .
Ag3 Ag5 C17 C18 54.9(10) 3_666 .
Ag2 Ag5 C17 C18 -102.8(12) 3_566 .
Ag4 Ag5 C17 C18 84.0(11) 3_666 .
C1 Ag5 C17 Ag1 90.0(5) 3_566 .
C25 Ag5 C17 Ag1 -143.8(4) 3_666 .
C9 Ag5 C17 Ag1 -34.2(5) . .
Ag3 Ag5 C17 Ag1 -54.0(3) . .
Ag1 Ag5 C17 Ag1 47.9(3) 3_566 .
Ag3 Ag5 C17 Ag1 -122.3(3) 3_666 .
Ag2 Ag5 C17 Ag1 80.0(4) 3_566 .
Ag4 Ag5 C17 Ag1 -93.2(4) 3_666 .
C1 Ag5 C17 Ag4 172.9(5) 3_566 .
C25 Ag5 C17 Ag4 -60.9(6) 3_666 .
C9 Ag5 C17 Ag4 48.7(6) . .
Ag1 Ag5 C17 Ag4 82.9(5) . .
Ag3 Ag5 C17 Ag4 28.9(4) . .
Ag1 Ag5 C17 Ag4 130.8(4) 3_566 .
Ag3 Ag5 C17 Ag4 -39.4(3) 3_666 .
Ag2 Ag5 C17 Ag4 162.9(7) 3_566 .
Ag4 Ag5 C17 Ag4 -10.3(6) 3_666 .
C1 Ag5 C17 Ag2 10.0(5) 3_566 3_566
C25 Ag5 C17 Ag2 136.2(4) 3_666 3_566
C9 Ag5 C17 Ag2 -114.2(4) . 3_566
Ag1 Ag5 C17 Ag2 -80.0(4) . 3_566
Ag3 Ag5 C17 Ag2 -134.0(3) . 3_566
Ag1 Ag5 C17 Ag2 -32.1(3) 3_566 3_566
Ag3 Ag5 C17 Ag2 157.7(3) 3_666 3_566
Ag4 Ag5 C17 Ag2 -173.23(7) 3_666 3_566
Ag1 C17 C18 C19 -60(29) . .
Ag4 C17 C18 C19 -133(28) . .
Ag5 C17 C18 C19 127(28) . .
Ag2 C17 C18 C19 39(28) 3_566 .
Ag1 C17 C18 Ag4 73(2) . .
Ag5 C17 C18 Ag4 -100.4(8) . .
Ag2 C17 C18 Ag4 172.1(7) 3_566 .
O1 Ag4 C18 C17 -108.4(8) . .
C25 Ag4 C18 C17 16.5(13) . .
C9 Ag4 C18 C17 134.6(8) 3_666 .
Ag3 Ag4 C18 C17 95.7(8) 3_666 .
Ag3 Ag4 C18 C17 30.6(9) . .
Ag1 Ag4 C18 C17 -16.0(7) . .
Ag5 Ag4 C18 C17 97.9(9) 3_666 .
O1 Ag4 C18 C19 69.4(9) . .
C25 Ag4 C18 C19 -165.7(8) . .
C17 Ag4 C18 C19 177.8(14) . .
C9 Ag4 C18 C19 -47.6(9) 3_666 .
Ag3 Ag4 C18 C19 -86.5(8) 3_666 .
Ag3 Ag4 C18 C19 -151.6(8) . .
Ag1 Ag4 C18 C19 161.8(9) . .
Ag5 Ag4 C18 C19 -84.3(9) 3_666 .
C17 C18 C19 C24 -93(28) . .
Ag4 C18 C19 C24 134.8(13) . .
C17 C18 C19 C20 85(28) . .
Ag4 C18 C19 C20 -46.7(15) . .
C24 C19 C20 C21 1(2) . .
C18 C19 C20 C21 -177.8(16) . .
C19 C20 C21 C22 0(3) . .
C20 C21 C22 C23 -1(4) . .
C21 C22 C23 C24 2(4) . .
C20 C19 C24 C23 0(3) . .
C18 C19 C24 C23 178.7(17) . .
C22 C23 C24 C19 -1(4) . .
C9 Ag3 C25 C26 -34(12) . .
Ag4 Ag3 C25 C26 -144(9) 3_666 .
Ag2 Ag3 C25 C26 32(9) . .
Ag4 Ag3 C25 C26 129(9) . .
Ag5 Ag3 C25 C26 130(9) . .
Ag1 Ag3 C25 C26 81(9) . .
Ag5 Ag3 C25 C26 -143(9) 3_666 .
C9 Ag3 C25 Ag5 109(4) . 3_666
Ag4 Ag3 C25 Ag5 -0.8(5) 3_666 3_666
Ag2 Ag3 C25 Ag5 174.62(7) . 3_666
Ag4 Ag3 C25 Ag5 -88.5(4) . 3_666
Ag5 Ag3 C25 Ag5 -87.1(4) . 3_666
Ag1 Ag3 C25 Ag5 -135.6(3) . 3_666
C9 Ag3 C25 Ag4 -163(4) . .
Ag4 Ag3 C25 Ag4 87.7(3) 3_666 .
Ag2 Ag3 C25 Ag4 -96.9(3) . .
Ag5 Ag3 C25 Ag4 1.4(5) . .
Ag1 Ag3 C25 Ag4 -47.1(2) . .
Ag5 Ag3 C25 Ag4 88.5(4) 3_666 .
O1 Ag4 C25 C26 -34.6(9) . .
C17 Ag4 C25 C26 -146.2(8) . .
C9 Ag4 C25 C26 86.4(9) 3_666 .
C18 Ag4 C25 C26 -155.3(8) . .
Ag3 Ag4 C25 C26 129.3(8) 3_666 .
Ag3 Ag4 C25 C26 -174.8(11) . .
Ag1 Ag4 C25 C26 -125.5(9) . .
Ag5 Ag4 C25 C26 94.4(9) 3_666 .
O1 Ag4 C25 Ag3 140.3(4) . .
C17 Ag4 C25 Ag3 28.7(6) . .
C9 Ag4 C25 Ag3 -98.7(4) 3_666 .
C18 Ag4 C25 Ag3 19.5(9) . .
Ag3 Ag4 C25 Ag3 -55.9(3) 3_666 .
Ag1 Ag4 C25 Ag3 49.3(3) . .
Ag5 Ag4 C25 Ag3 -90.8(4) 3_666 .
O1 Ag4 C25 Ag5 -128.9(4) . 3_666
C17 Ag4 C25 Ag5 119.5(4) . 3_666
C9 Ag4 C25 Ag5 -7.9(4) 3_666 3_666
C18 Ag4 C25 Ag5 110.3(7) . 3_666
Ag3 Ag4 C25 Ag5 34.9(3) 3_666 3_666
Ag3 Ag4 C25 Ag5 90.8(4) . 3_666
Ag1 Ag4 C25 Ag5 140.1(3) . 3_666
Ag3 C25 C26 C27 -25(21) . .
Ag5 C25 C26 C27 -168(13) 3_666 .
Ag4 C25 C26 C27 103(14) . .
C25 C26 C27 C32 -154(13) . .
C25 C26 C27 C28 27(14) . .
C32 C27 C28 C29 2(2) . .
C26 C27 C28 C29 -179.3(15) . .
C27 C28 C29 C30 -4(3) . .
C28 C29 C30 C31 5(4) . .
C29 C30 C31 C32 -5(3) . .
C28 C27 C32 C31 -1(2) . .
C26 C27 C32 C31 -179.9(14) . .
C30 C31 C32 C27 2(3) . .
C25 Ag4 O1 S1 -30.0(10) . .
C17 Ag4 O1 S1 101.2(10) . .
C9 Ag4 O1 S1 -136.9(9) 3_666 .
C18 Ag4 O1 S1 126.6(10) . .
Ag3 Ag4 O1 S1 -173.1(5) 3_666 .
Ag3 Ag4 O1 S1 9.2(12) . .
Ag1 Ag4 O1 S1 59.0(9) . .
Ag5 Ag4 O1 S1 -76.4(10) 3_666 .
Ag4 O1 S1 C33 -128(2) . .
Ag4 O1 S1 C34 142.4(14) . .
C9 Ag2 O2 S2 47.2(13) . .
C1 Ag2 O2 S2 -91.5(12) . .
C17 Ag2 O2 S2 170.7(12) 3_566 .
Ag1 Ag2 O2 S2 152.9(9) 3_566 .
Ag1 Ag2 O2 S2 -70.7(15) . .
Ag3 Ag2 O2 S2 2.1(13) . .
Ag5 Ag2 O2 S2 -140.8(11) 3_566 .
Ag2 O2 S2 C35 43.0(18) . .
Ag2 O2 S2 C36 148.6(17) . .
