#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:00:20 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179608 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/72/4507223.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4507223
loop_
_publ_author_name
'Stefanoski, S.'
'Blosser, M. C.'
'Nolas, G. S.'
_publ_section_title
;
 Pressure Effects on the Size of Type-I and Type-II Si-Clathrates
 Synthesized by Spark Plasma Sintering
;
_journal_issue                   1
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              195
_journal_paper_doi               10.1021/cg3013443
_journal_volume                  13
_journal_year                    2013
_chemical_formula_sum            'Na4 Si23'
_chemical_formula_weight         732.22
_chemical_name_systematic        ' ?'
_space_group_IT_number           223
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-P 4n 2 3'
_symmetry_space_group_name_H-M   'P m -3 n'
_audit_creation_date             2012-09-10T10:25
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2012-09-10T10:25  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   10.19979(12)
_cell_length_b                   10.19979
_cell_length_c                   10.19979
_cell_volume                     1061.142(12)
_computing_structure_refinement  GSAS
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id                     2012-09-10T10:25|MCB92SPSTYPEI_1|Mike|1
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.00997
_pd_meas_2theta_range_max        119.99504
_pd_meas_2theta_range_min        12.0
_pd_meas_number_of_points        10833
_pd_phase_name                   Na8Si46
_pd_proc_2theta_range_inc        0.00997
_pd_proc_2theta_range_max        119.99504
_pd_proc_2theta_range_min        12.0
_pd_proc_info_datetime           2012-09-10T10:25:26
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 20 terms.
 Shifted Chebyshev function of 1st kind
      1:    152.675     2:   -166.490     3:    134.806     4:   -91.5245    
      5:    66.2306     6:   -50.8591     7:    37.6062     8:   -30.8411    
      9:    26.1226    10:   -22.1911    11:    17.1105    12:   -13.1813    
     13:    10.3683    14:   -10.3013    15:    7.45623    16:   -5.72706    
     17:    1.70335    18:   -1.77144    19:    1.32271    20:   -1.22506    
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0809
_pd_proc_ls_prof_wR_expected     0.0922
_pd_proc_ls_prof_wR_factor       0.1056
_pd_proc_number_of_points        10833
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.15
_refine_ls_matrix_type           full
_refine_ls_number_parameters     31
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.23702
_refine_ls_shift/su_max          0.04
_refine_ls_shift/su_mean         0.00
_reflns_d_resolution_high        0.891
_reflns_d_resolution_low         7.212
_reflns_limit_h_max              11
_reflns_limit_h_min              1
_reflns_limit_k_max              8
_reflns_limit_k_min              0
_reflns_limit_l_max              6
_reflns_limit_l_min              0
_reflns_number_total             322
_cod_data_source_file            cg3013443_si_001.cif
_cod_data_source_block           MCB92SPSTYPEI_1_publ
_cod_original_cell_volume        1061.14(4)
_cod_database_code               4507223
#BEGIN Tags that were not found in dictionaries:
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y+1/2,+x+1/2,+z+1/2
14 +z+1/2,+y+1/2,+x+1/2
15 +x+1/2,+z+1/2,+y+1/2
16 +y+1/2,+x+1/2,-z+1/2
17 -z+1/2,+y+1/2,+x+1/2
18 +x+1/2,-z+1/2,+y+1/2
19 -z+1/2,+y+1/2,-x+1/2
20 -x+1/2,-z+1/2,+y+1/2
21 +x+1/2,-z+1/2,-y+1/2
22 -y+1/2,+x+1/2,-z+1/2
23 -z+1/2,-y+1/2,+x+1/2
24 +y+1/2,-x+1/2,-z+1/2
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y+1/2,-x+1/2,-z+1/2
-14 -z+1/2,-y+1/2,-x+1/2
-15 -x+1/2,-z+1/2,-y+1/2
-16 -y+1/2,-x+1/2,+z+1/2
-17 +z+1/2,-y+1/2,-x+1/2
-18 -x+1/2,+z+1/2,-y+1/2
-19 +z+1/2,-y+1/2,+x+1/2
-20 +x+1/2,+z+1/2,-y+1/2
-21 -x+1/2,+z+1/2,+y+1/2
-22 +y+1/2,-x+1/2,+z+1/2
-23 +z+1/2,+y+1/2,-x+1/2
-24 -y+1/2,+x+1/2,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Na Na1 0.0 0.0 0.0 1.0 Uiso 0.00995 2
Na Na2 0.5 0.0 0.25 1.0 Uiso 0.07136 6
Si Si1 0.30817 0.1203 0.0 1.0 Uiso 0.01752 24
Si Si3 0.5 0.25 0.0 1.0 Uiso 0.01786 6
Si Si2 0.18049 0.18049 0.18049 1.0 Uiso 0.01223 16
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Na 8.0 0.000 0.000 4.76260 3.28500 3.17360 8.84220 1.26740 0.31360 1.11280
129.424 0.67600 International_Tables_Vol_C
Si 46.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100
81.6937 1.14070 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540600 1.000 K\a~1~ 1
1.544400 0.500 K\a~2~ 2
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
838.0 0.001193 849.51343 852.73145
880.0 0.001136 845.59320 849.03363
823.0 0.001215 841.70001 845.38672
845.0 0.001183 837.83484 841.79498
851.0 0.001175 833.99603 838.26129
880.0 0.001136 830.18457 834.79132
876.0 0.001142 826.39825 831.38928
824.0 0.001214 822.64032 828.06555
881.0 0.001135 818.90753 824.82599
878.0 0.001139 815.20099 821.68298
897.0 0.001115 811.52075 818.65027
870.0 0.001149 807.86591 815.74481
904.0 0.001106 804.23688 812.98926
850.0 0.001176 800.63239 810.41156
803.0 0.001245 797.05475 808.05103
803.0 0.001245 793.50110 805.95557
815.0 0.001227 789.97247 804.19330
843.0 0.001186 786.46924 802.85669
842.0 0.001188 782.98975 802.07446
816.0 0.001225 779.53522 802.03339
848.0 0.001179 776.10413 803.01337
837.0 0.001195 772.69861 805.46155
795.0 0.001258 769.31622 810.15942
801.0 0.001248 765.95673 818.55902
860.0 0.001163 762.62238 833.30194
854.0 0.001171 759.31073 858.76318
853.0 0.001172 756.02258 900.94495
865.0 0.001156 752.75708 965.66809
859.0 0.001164 749.51544 1051.03198
835.0 0.001198 746.29663 1128.65149
869.0 0.001151 743.09924 1148.50891
848.0 0.001179 739.92609 1114.31262
882.0 0.001134 736.77417 1065.36377
842.0 0.001188 733.64508 1003.48517
814.0 0.001229 730.53741 931.17261
779.0 0.001284 727.45239 868.24713
772.0 0.001295 724.38898 822.55371
738.0 0.001355 721.34662 791.44257
772.0 0.001295 718.32703 770.34839
787.0 0.001271 715.32794 755.52295
700.0 0.001429 712.35022 744.48236
764.0 0.001309 709.39307 735.74506
753.0 0.001328 706.45764 728.48798
798.0 0.001253 703.54279 722.23816
776.0 0.001289 700.64807 716.71088
747.0 0.001339 697.77466 711.72363
724.0 0.001381 694.92102 707.14618
748.0 0.001337 692.08826 702.88995
732.0 0.001366 689.27435 698.88690
733.0 0.001364 686.48187 695.09143
689.0 0.001451 683.70862 691.46405
696.0 0.001437 680.95471 687.97681
726.0 0.001377 678.22089 684.60907
688.0 0.001453 675.50604 681.34229
720.0 0.001389 672.81061 678.16339
711.0 0.001406 670.13483 675.06195
726.0 0.001377 667.47760 672.02771
694.0 0.001441 664.83929 669.05414
676.0 0.001479 662.21948 666.13470
739.0 0.001353 659.61896 663.26544
695.0 0.001439 657.03644 660.44086
693.0 0.001443 654.47223 657.65802
686.0 0.001458 651.92706 654.91461
636.0 0.001572 649.39935 652.20654
711.0 0.001406 646.88983 649.53259
698.0 0.001433 644.39740 646.88977
666.0 0.001502 641.92413 644.27850
718.0 0.001393 639.46765 641.69525
719.0 0.001391 637.02875 639.13947
709.0 0.001410 634.60760 636.61047
649.0 0.001541 632.20337 634.10651
728.0 0.001374 629.81671 631.62726
689.0 0.001451 627.44617 629.17072
610.0 0.001639 625.09369 626.73834
649.0 0.001541 622.75732 624.32745
703.0 0.001422 620.43774 621.93829
605.0 0.001653 618.13501 619.57056
633.0 0.001580 615.84839 617.22302
678.0 0.001475 613.57831 614.89594
610.0 0.001639 611.32397 612.58789
649.0 0.001541 609.08667 610.30023
616.0 0.001623 606.86469 608.03082
654.0 0.001529 604.65863 605.78003
640.0 0.001563 602.46869 603.54791
616.0 0.001623 600.29407 601.33350
601.0 0.001664 598.13525 599.13696
618.0 0.001618 595.99133 596.95740
611.0 0.001637 593.86365 594.79596
633.0 0.001580 591.75079 592.65112
574.0 0.001742 589.65234 590.52222
596.0 0.001678 587.57013 588.41113
637.0 0.001570 585.50201 586.31549
605.0 0.001653 583.44910 584.23639
575.0 0.001739 581.41034 582.17273
575.0 0.001739 579.38690 580.12555
584.0 0.001712 577.37781 578.09387
619.0 0.001616 575.38232 576.07678
601.0 0.001664 573.40222 574.07605
583.0 0.001715 571.43573 572.08984
598.0 0.001672 569.48352 570.11865
605.0 0.001653 567.54492 568.16205
546.0 0.001832 565.62061 566.22046
577.0 0.001733 563.70996 564.29321
546.0 0.001832 561.81268 562.38000
561.0 0.001783 559.92975 560.48175
535.0 0.001869 558.05988 558.59729
544.0 0.001838 556.20331 556.72668
572.0 0.001748 554.35999 554.86981
531.0 0.001883 552.53021 553.02698
528.0 0.001894 550.71338 551.19763
597.0 0.001675 548.90936 549.38165
572.0 0.001748 547.11865 547.57935
533.0 0.001876 545.34039 545.78992
560.0 0.001786 543.57507 544.01379
553.0 0.001808 541.82263 542.25098
555.0 0.001802 540.08246 540.50079
543.0 0.001842 538.35486 538.76355
555.0 0.001802 536.63940 537.03870
578.0 0.001730 534.93665 535.32697
488.0 0.002049 533.24567 533.62732
535.0 0.001869 531.56702 531.69269
561.0 0.001783 529.90070 530.02362
471.0 0.002123 528.24585 528.36609
520.0 0.001923 526.60315 526.60449
518.0 0.001931 524.97180 524.97321
533.0 0.001876 523.35254 523.35394
464.0 0.002155 521.74475 521.74622
563.0 0.001776 520.14832 520.14978
493.0 0.002028 518.56372 518.56519
523.0 0.001912 516.99011 516.99158
519.0 0.001927 515.42792 515.42938
545.0 0.001835 513.87634 513.87793
505.0 0.001980 512.33673 512.33826
519.0 0.001927 510.80771 510.80927
532.0 0.001880 509.28958 509.29117
497.0 0.002012 507.78259 507.78418
511.0 0.001957 506.28607 506.28769
479.0 0.002088 504.80051 504.80212
484.0 0.002066 503.32504 503.32669
481.0 0.002079 501.86087 501.86252
495.0 0.002020 500.40671 500.40839
489.0 0.002045 498.96289 498.96457
493.0 0.002028 497.52960 497.53128
517.0 0.001934 496.10638 496.10809
445.0 0.002247 494.69333 494.69504
459.0 0.002179 493.29016 493.29190
484.0 0.002066 491.89755 491.89932
470.0 0.002128 490.51465 490.51642
527.0 0.001898 489.14127 489.14304
479.0 0.002088 487.77808 487.77988
443.0 0.002257 486.42435 486.42615
470.0 0.002128 485.08038 485.08218
483.0 0.002070 483.74570 483.74753
451.0 0.002217 482.42105 482.42288
479.0 0.002088 481.10550 481.10733
450.0 0.002222 479.79910 479.80093
415.0 0.002410 478.50250 478.50436
490.0 0.002041 477.21472 477.21658
449.0 0.002227 475.93628 475.93817
472.0 0.002119 474.66656 474.66846
455.0 0.002198 473.40628 473.40820
499.0 0.002004 472.15488 472.15680
462.0 0.002165 470.91196 470.91388
467.0 0.002141 469.67850 469.68045
438.0 0.002283 468.45334 468.45529
425.0 0.002353 467.23697 467.23892
462.0 0.002165 466.02905 466.03101
445.0 0.002247 464.82993 464.83188
441.0 0.002268 463.63916 463.64114
437.0 0.002288 462.45667 462.45865
446.0 0.002242 461.28287 461.28485
433.0 0.002309 460.11707 460.11905
441.0 0.002268 458.95966 458.96164
459.0 0.002179 457.81018 457.81216
461.0 0.002169 456.66904 456.67105
440.0 0.002273 455.53589 455.53790
433.0 0.002309 454.41049 454.41251
411.0 0.002433 453.29337 453.29541
489.0 0.002045 452.18387 452.18588
436.0 0.002294 451.08215 451.08420
424.0 0.002358 449.98846 449.99051
434.0 0.002304 448.90216 448.90424
433.0 0.002309 447.82355 447.82562
437.0 0.002288 446.75238 446.75443
448.0 0.002232 445.68893 445.69098
411.0 0.002433 444.63275 444.63483
437.0 0.002288 443.58398 443.58606
397.0 0.002519 442.54272 442.54483
433.0 0.002309 441.50858 441.51065
440.0 0.002273 440.48166 440.48373
439.0 0.002278 439.46182 439.46390
403.0 0.002481 438.44928 438.45135
456.0 0.002193 437.44363 437.44571
446.0 0.002242 436.44501 436.44708
402.0 0.002488 435.45346 435.45557
419.0 0.002387 434.46857 434.47067
404.0 0.002475 433.49066 433.49277
422.0 0.002370 432.51926 432.52136
433.0 0.002309 431.55502 431.55713
429.0 0.002331 430.59726 430.59937
456.0 0.002193 429.64606 429.64816
421.0 0.002375 428.70160 428.70370
434.0 0.002304 427.76343 427.76553
431.0 0.002320 426.83197 426.83408
411.0 0.002433 425.90652 425.90863
457.0 0.002188 424.98795 424.99005
386.0 0.002591 424.07541 424.07751
413.0 0.002421 423.16916 423.17126
430.0 0.002326 422.26917 422.27127
441.0 0.002268 421.37531 421.37744
426.0 0.002347 420.48764 420.48975
430.0 0.002326 419.60583 419.60794
406.0 0.002463 418.73041 418.73251
430.0 0.002326 417.86075 417.86285
427.0 0.002342 416.99698 416.99908
439.0 0.002278 416.13910 416.14124
435.0 0.002299 415.28714 415.28925
404.0 0.002475 414.44095 414.44305
392.0 0.002551 413.60019 413.60229
392.0 0.002551 412.76569 412.76776
412.0 0.002427 411.93655 411.93866
418.0 0.002392 411.11276 411.11484
447.0 0.002237 410.29498 410.29706
357.0 0.002801 409.48254 409.48462
395.0 0.002532 408.67557 408.67767
386.0 0.002591 407.87384 407.87592
385.0 0.002597 407.07776 407.07983
394.0 0.002538 406.28702 406.28909
386.0 0.002591 405.50125 405.50333
367.0 0.002725 404.72113 404.72321
429.0 0.002331 403.94604 403.94812
388.0 0.002577 403.17621 403.17828
394.0 0.002538 402.41129 402.41336
418.0 0.002392 401.65167 401.65372
425.0 0.002353 400.89709 400.89917
392.0 0.002551 400.14737 400.14941
347.0 0.002882 399.40277 399.40482
425.0 0.002353 398.66299 398.66504
374.0 0.002674 397.92819 397.93024
375.0 0.002667 397.19809 397.20013
396.0 0.002525 396.47290 396.47491
367.0 0.002725 395.75250 395.75452
407.0 0.002457 395.03668 395.03873
415.0 0.002410 394.32568 394.32770
390.0 0.002564 393.61929 393.62131
396.0 0.002525 392.91748 392.91949
401.0 0.002494 392.22040 392.22238
396.0 0.002525 391.52771 391.52969
349.0 0.002865 390.83954 390.84152
403.0 0.002481 390.15573 390.15771
390.0 0.002564 389.47656 389.47855
424.0 0.002358 388.80167 388.80365
382.0 0.002618 388.13107 388.13303
392.0 0.002551 387.46494 387.46689
365.0 0.002740 386.80295 386.80490
413.0 0.002421 386.14523 386.14719
385.0 0.002597 385.49176 385.49371
357.0 0.002801 384.84247 384.84442
357.0 0.002801 384.19724 384.19916
386.0 0.002591 383.55615 383.55807
351.0 0.002849 382.91922 382.92114
383.0 0.002611 382.28625 382.28818
364.0 0.002747 381.65735 381.65927
396.0 0.002525 381.03217 381.03409
415.0 0.002410 380.41129 380.41318
369.0 0.002710 379.79413 379.79602
378.0 0.002646 379.18082 379.18271
381.0 0.002625 378.57141 378.57327
379.0 0.002639 377.96579 377.96765
361.0 0.002770 377.36398 377.36584
399.0 0.002506 376.76575 376.76761
395.0 0.002532 376.17151 376.17334
378.0 0.002646 375.58078 375.58261
412.0 0.002427 374.99368 374.99551
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80.0 0.01250 69.75669 92.91949
98.0 0.01020 69.75301 94.36163
112.0 0.00893 69.74863 95.62057
93.0 0.01075 69.74355 96.60084
91.0 0.01099 69.73774 97.21323
97.0 0.01031 69.73121 97.39151
108.0 0.00926 69.72392 97.11365
82.0 0.01220 69.71590 96.40488
94.0 0.01064 69.70710 95.32711
111.0 0.00901 69.69754 93.97424
94.0 0.01064 69.68718 92.43811
85.0 0.01176 69.67604 90.81419
80.0 0.01250 69.66407 89.17010
84.0 0.01190 69.65130 87.56755
87.0 0.01149 69.63767 86.03859
84.0 0.01190 69.62321 84.61183
68.0 0.01471 69.60793 83.30146
88.0 0.01136 69.59172 82.10683
108.0 0.00926 69.57468 81.03407
88.0 0.01136 69.55670 80.05495
77.0 0.01299 69.53785 79.20894
87.0 0.01149 69.51804 78.46474
63.0 0.01587 69.49734 77.81732
76.0 0.01316 69.47566 77.25601
91.0 0.01099 69.45308 76.77492
83.0 0.01205 69.42944 76.36446
88.0 0.01136 69.40491 76.01937
66.0 0.01515 69.37932 75.73199
72.0 0.01389 69.35275 75.49815
68.0 0.01471 69.32512 75.31266
70.0 0.01429 69.29649 75.17291
77.0 0.01299 69.26684 75.07626
71.0 0.01408 69.23603 75.02126
78.0 0.01282 69.20423 75.00775
69.0 0.01449 69.17127 75.03603
74.0 0.01351 69.13725 75.10709
78.0 0.01282 69.10205 75.22296
66.0 0.01515 69.06577 75.38528
91.0 0.01099 69.02828 75.59714
69.0 0.01449 68.98971 75.86021
84.0 0.01190 68.94984 76.17773
79.0 0.01266 68.90889 76.55039
92.0 0.01087 68.86664 76.98049
82.0 0.01220 68.82319 77.46635
86.0 0.01163 68.77856 78.00444
79.0 0.01266 68.73257 78.69003
89.0 0.01124 68.68542 79.31357
64.0 0.01563 68.63687 79.95860
97.0 0.01031 68.58708 80.59878
84.0 0.01190 68.53590 81.20477
83.0 0.01205 68.48345 81.73544
84.0 0.01190 68.42957 82.15058
59.0 0.01695 68.37439 82.40874
96.0 0.01042 68.31775 82.48135
82.0 0.01220 68.25982 82.35538
75.0 0.01333 68.20034 82.03780
96.0 0.01042 68.13951 81.55548
76.0 0.01316 68.07713 80.94463
82.0 0.01220 68.01337 80.24995
79.0 0.01266 67.94816 79.51067
86.0 0.01163 67.88125 78.75919
66.0 0.01515 67.81300 78.02476
76.0 0.01316 67.74306 77.32303
80.0 0.01250 67.67166 76.66891
64.0 0.01563 67.59856 76.06712
83.0 0.01205 67.52398 75.52358
79.0 0.01266 67.44765 75.03721
74.0 0.01351 67.36987 74.60910
64.0 0.01563 67.29018 74.23549
74.0 0.01351 67.20906 73.91510
67.0 0.01493 67.12606 73.64307
75.0 0.01333 67.04140 73.41621
84.0 0.01190 66.95513 73.23001
80.0 0.01250 66.86691 73.07858
83.0 0.01205 66.77712 72.95694
60.0 0.01667 66.68526 72.85793
86.0 0.01163 66.59185 72.77478
79.0 0.01266 66.49640 72.69912
80.0 0.01250 66.39922 72.62312
64.0 0.01563 66.30003 72.53922
68.0 0.01471 66.19908 72.44206
57.0 0.01754 66.09606 72.32842
83.0 0.01205 65.99133 72.19883
69.0 0.01449 65.88432 72.05543
81.0 0.01235 65.77563 71.90364
64.0 0.01563 65.66470 71.74818
72.0 0.01389 65.55190 71.59483
70.0 0.01429 65.43706 71.44784
69.0 0.01449 65.31996 71.31055
72.0 0.01389 65.20103 71.18609
98.0 0.01020 65.07970 71.07576
79.0 0.01266 64.95643 70.98122
71.0 0.01408 64.83080 70.90315
70.0 0.01429 64.70316 70.84242
74.0 0.01351 64.57311 70.79946
57.0 0.01754 64.44102 70.77495
67.0 0.01493 64.30647 71.88057
79.0 0.01266 64.16995 71.90359
64.0 0.01563 64.03080 71.94782
90.0 0.01111 63.88941 72.01454
67.0 0.01493 63.74589 72.10534
80.0 0.01250 63.59966 72.22315
63.0 0.01587 63.45135 72.37019
75.0 0.01333 63.30015 72.55028
83.0 0.01205 63.14695 72.76727
77.0 0.01299 62.99092 73.02671
75.0 0.01333 62.83260 73.33343
73.0 0.01370 62.67151 73.69550
84.0 0.01190 62.50810 74.11902
71.0 0.01408 62.34184 74.61437
62.0 0.01613 62.17336 75.18895
72.0 0.01389 62.00170 75.85492
85.0 0.01176 61.82763 76.62142
79.0 0.01266 61.65127 77.49819
83.0 0.01205 61.47164 78.50067
82.0 0.01220 61.28953 79.63460
62.0 . . .
