#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:14:46 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179620 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/84/4508486.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4508486
loop_
_publ_author_name
'Amo-Ochoa, Pilar'
'Jiménez-Aparicio, Reyes'
'Perles, Josefina'
'Torres, M. Rosario'
'Gennari, Marcello'
'Zamora, Félix'
_publ_section_title
;
 Structural Diversity in Paddlewheel Dirhodium(II) Compounds through Ionic
 Interactions: Electronic and Redox Properties
;
_journal_issue                   11
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              4977
_journal_paper_doi               10.1021/cg4011532
_journal_volume                  13
_journal_year                    2013
_chemical_formula_sum            'C36 H60 Br K O26 Rh6'
_chemical_formula_weight         1645.31
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.035(8)
_cell_angle_beta                 108.809(10)
_cell_angle_gamma                102.831(11)
_cell_formula_units_Z            2
_cell_length_a                   13.2906(14)
_cell_length_b                   13.844(2)
_cell_length_c                   16.453(2)
_cell_measurement_temperature    296(2)
_cell_volume                     2731.6(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.973
_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0271
_diffrn_reflns_av_sigmaI/netI    0.0390
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            21109
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.34
_exptl_absorpt_coefficient_mu    2.657
_exptl_absorpt_correction_T_max  0.6758
_exptl_absorpt_correction_T_min  0.3620
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    2.000
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             1616
_exptl_crystal_size_max          0.48
_exptl_crystal_size_mid          0.33
_exptl_crystal_size_min          0.16
_refine_diff_density_max         0.826
_refine_diff_density_min         -0.667
_refine_diff_density_rms         0.108
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.997
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     631
_refine_ls_number_reflns         9361
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      0.998
_refine_ls_R_factor_all          0.0503
_refine_ls_R_factor_gt           0.0320
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0399P)²+5.8216P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0754
_refine_ls_wR_factor_ref         0.0875
_reflns_number_gt                7224
_reflns_number_total             9361
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg4011532_si_001.cif
_cod_data_source_block           C5
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        2731.5(6)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4508486
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Br1 Br 0.92895(5) 0.89251(4) 0.34921(3) 0.03475(14) Uani 1 1 d .
C1 C 1.1560(5) 0.6734(5) 0.3995(4) 0.0419(14) Uani 1 1 d D
C2 C 1.2298(6) 0.6632(5) 0.3477(5) 0.065(2) Uani 1 1 d D
H2A H 1.2085 0.6946 0.2976 0.078 Uiso 1 1 calc R
H2B H 1.3056 0.6997 0.3843 0.078 Uiso 1 1 calc R
C3 C 1.2246(14) 0.5556(6) 0.3158(11) 0.207(8) Uani 1 1 d D
H3A H 1.2732 0.5540 0.2836 0.310 Uiso 1 1 calc R
H3B H 1.1502 0.5194 0.2782 0.310 Uiso 1 1 calc R
H3C H 1.2471 0.5244 0.3651 0.310 Uiso 1 1 calc R
C4 C 0.8760(5) 0.6994(5) 0.5558(4) 0.0471(15) Uani 1 1 d .
C5 C 0.7884(9) 0.6935(8) 0.5955(7) 0.099(3) Uani 1 1 d .
H5A H 0.7173 0.6561 0.5510 0.119 Uiso 1 1 calc R
H5B H 0.8037 0.6561 0.6421 0.119 Uiso 1 1 calc R
C6 C 0.7817(12) 0.7915(13) 0.6307(10) 0.188(7) Uani 1 1 d .
H6A H 0.7248 0.7830 0.6553 0.281 Uiso 1 1 calc R
H6B H 0.7645 0.8283 0.5845 0.281 Uiso 1 1 calc R
H6C H 0.8514 0.8286 0.6756 0.281 Uiso 1 1 calc R
C7 C 0.8297(5) 1.1645(4) 0.3959(3) 0.0346(13) Uani 1 1 d .
C8 C 0.7436(5) 1.0798(4) 0.3253(4) 0.0434(14) Uani 1 1 d .
H8A H 0.6962 1.0418 0.3514 0.052 Uiso 1 1 calc R
H8B H 0.7808 1.0345 0.3051 0.052 Uiso 1 1 calc R
C9 C 0.6710(6) 1.1085(6) 0.2464(4) 0.073(2) Uani 1 1 d .
H9A H 0.6195 1.0483 0.2060 0.110 Uiso 1 1 calc R
H9B H 0.7160 1.1440 0.2181 0.110 Uiso 1 1 calc R
H9C H 0.6312 1.1514 0.2647 0.110 Uiso 1 1 calc R
C10 C 0.8658(5) 0.5408(4) 0.3547(4) 0.0554(18) Uani 1 1 d D
C11 C 0.7918(9) 0.4537(6) 0.2779(6) 0.141(6) Uani 1 1 d D
H11A H 0.7780 0.4738 0.2218 0.170 Uiso 1 1 calc R
H11B H 0.8207 0.3953 0.2773 0.170 Uiso 1 1 calc R
C12 C 0.6922(11) 0.4364(11) 0.3035(9) 0.217(9) Uani 1 1 d D
H12A H 0.6340 0.3813 0.2615 0.325 Uiso 1 1 calc R
H12B H 0.6679 0.4967 0.3050 0.325 Uiso 1 1 calc R
H12C H 0.7107 0.4200 0.3606 0.325 Uiso 1 1 calc R
C13 C 0.5338(5) 0.8820(5) 0.3796(4) 0.0451(15) Uani 1 1 d .
C14 C 0.5530(6) 0.8133(6) 0.3109(5) 0.064(2) Uani 1 1 d .
H14A H 0.4961 0.8067 0.2543 0.076 Uiso 1 1 calc R
H14B H 0.6238 0.8447 0.3071 0.076 Uiso 1 1 calc R
C15 C 0.5523(13) 0.7152(9) 0.3276(8) 0.167(6) Uani 1 1 d .
H15A H 0.5648 0.6759 0.2814 0.251 Uiso 1 1 calc R
H15B H 0.4818 0.6826 0.3299 0.251 Uiso 1 1 calc R
H15C H 0.6097 0.7206 0.3827 0.251 Uiso 1 1 calc R
C16 C 0.5350(5) 1.1549(5) 0.4274(4) 0.0426(14) Uani 1 1 d .
C17 C 0.5544(6) 1.2480(6) 0.3888(5) 0.065(2) Uani 1 1 d .
H17A H 0.6313 1.2690 0.3943 0.079 Uiso 1 1 calc R
H17B H 0.5092 1.2312 0.3268 0.079 Uiso 1 1 calc R
C18 C 0.5271(12) 1.3336(9) 0.4336(10) 0.160(6) Uani 1 1 d .
H18A H 0.5402 1.3910 0.4072 0.240 Uiso 1 1 calc R
H18B H 0.5730 1.3515 0.4947 0.240 Uiso 1 1 calc R
H18C H 0.4507 1.3134 0.4276 0.240 Uiso 1 1 calc R
C19 C 0.7001(4) 0.8925(4) 0.0719(4) 0.0427(14) Uani 1 1 d D
C20 C 0.5766(4) 0.8679(5) 0.0496(3) 0.0535(17) Uani 1 1 d D
H20A H 0.5522 0.8028 0.0638 0.064 Uiso 1 1 calc R
H20B H 0.5619 0.9182 0.0873 0.064 Uiso 1 1 calc R
C21 C 0.5076(6) 0.8635(8) -0.0441(4) 0.092(3) Uani 1 1 d D
H21A H 0.4308 0.8471 -0.0511 0.138 Uiso 1 1 calc R
H21B H 0.5193 0.8125 -0.0824 0.138 Uiso 1 1 calc R
H21C H 0.5286 0.9282 -0.0587 0.138 Uiso 1 1 calc R
C22 C 1.1322(4) 0.9982(4) 0.1611(3) 0.0370(13) Uani 1 1 d D
C23 C 1.2555(4) 1.0255(5) 0.1827(4) 0.0572(19) Uani 1 1 d D
H23A H 1.2933 1.0499 0.2456 0.069 Uiso 1 1 calc R
H23B H 1.2766 1.0797 0.1541 0.069 Uiso 1 1 calc R
C24 C 1.2910(8) 0.9354(7) 0.1530(6) 0.109(3) Uani 1 1 d D
H24A H 1.3698 0.9548 0.1679 0.164 Uiso 1 1 calc R
H24B H 1.2550 0.9121 0.0906 0.164 Uiso 1 1 calc R
H24C H 1.2709 0.8820 0.1818 0.164 Uiso 1 1 calc R
C25 C 0.9210(5) 1.1310(4) 0.1651(4) 0.0458(15) Uani 1 1 d D
C26 C 0.9243(7) 1.2401(4) 0.1909(4) 0.066(2) Uani 1 1 d D
H26A H 0.8494 1.2461 0.1703 0.079 Uiso 1 1 calc R
H26B H 0.9536 1.2601 0.2545 0.079 Uiso 1 1 calc R
C27 C 0.9934(9) 1.3115(6) 0.1550(7) 0.116(4) Uani 1 1 d D
H27A H 0.9924 1.3795 0.1739 0.173 Uiso 1 1 calc R
H27B H 0.9638 1.2934 0.0920 0.173 Uiso 1 1 calc R
H27C H 1.0682 1.3071 0.1761 0.173 Uiso 1 1 calc R
C28 C 0.9091(5) 0.7553(4) 0.0697(4) 0.0450(15) Uani 1 1 d D
C29 C 0.9055(6) 0.6463(4) 0.0427(4) 0.0633(19) Uani 1 1 d D
H29A H 0.8288 0.6063 0.0153 0.076 Uiso 1 1 calc R
H29B H 0.9399 0.6413 -0.0008 0.076 Uiso 1 1 calc R
C30 C 0.9626(9) 0.6019(8) 0.1177(6) 0.117(4) Uani 1 1 d D
H30A H 0.9569 0.5325 0.0960 0.176 Uiso 1 1 calc R
H30B H 0.9281 0.6051 0.1606 0.176 Uiso 1 1 calc R
H30C H 1.0392 0.6397 0.1442 0.176 Uiso 1 1 calc R
C31 C 0.5775(6) 0.6109(5) 0.9055(4) 0.0526(17) Uani 1 1 d D
C32 C 0.6246(7) 0.6734(6) 0.8504(4) 0.084(3) Uani 1 1 d D
H32A H 0.5689 0.7021 0.8159 0.100 Uiso 1 1 calc R
H32B H 0.6873 0.7290 0.8887 0.100 Uiso 1 1 calc R
C33 C 0.6611(11) 0.6112(8) 0.7898(7) 0.145(5) Uani 1 1 d D
H33A H 0.6906 0.6533 0.7560 0.217 Uiso 1 1 calc R
H33B H 0.5990 0.5569 0.7510 0.217 Uiso 1 1 calc R
H33C H 0.7171 0.5837 0.8238 0.217 Uiso 1 1 calc R
C34 C 0.6332(6) 0.3919(6) 0.9881(6) 0.0634(19) Uani 1 1 d D
C35 C 0.7111(8) 0.3297(8) 0.9804(7) 0.110(4) Uani 1 1 d D
H35A H 0.7719 0.3434 1.0361 0.132 Uiso 1 1 calc R
H35B H 0.6722 0.2582 0.9657 0.132 Uiso 1 1 calc R
C36 C 0.7552(11) 0.3563(11) 0.9100(9) 0.206(8) Uani 1 1 d D
H36A H 0.8045 0.3166 0.9050 0.308 Uiso 1 1 calc R
H36B H 0.7946 0.4270 0.9252 0.308 Uiso 1 1 calc R
H36C H 0.6948 0.3423 0.8550 0.308 Uiso 1 1 calc R
K1 K 0.84458(11) 0.95104(10) 0.50535(8) 0.0421(3) Uani 1 1 d .
O1 O 1.1016(3) 0.7375(3) 0.3809(2) 0.0408(9) Uani 1 1 d .
O2 O 0.8817(3) 0.7578(3) 0.5027(3) 0.0437(10) Uani 1 1 d .
O3 O 0.8896(3) 1.1391(3) 0.4621(2) 0.0360(9) Uani 1 1 d .
O4 O 0.8734(3) 0.6314(3) 0.3447(2) 0.0492(11) Uani 1 1 d .
O5 O 1.1626(3) 0.7455(3) 0.6147(2) 0.0403(9) Uani 1 1 d .
O6 O 0.9278(3) 0.5181(3) 0.4224(2) 0.0407(10) Uani 1 1 d .
O7 O 0.9358(3) 0.6408(3) 0.5778(3) 0.0450(10) Uani 1 1 d .
O8 O 1.1536(3) 0.6208(3) 0.4563(3) 0.0431(10) Uani 1 1 d .
O9 O 0.5632(3) 1.1119(3) 0.6347(2) 0.0454(10) Uani 1 1 d .
O10 O 0.6179(3) 0.9296(3) 0.4478(2) 0.0412(9) Uani 1 1 d .
O11 O 0.6191(3) 1.1409(3) 0.4837(2) 0.0408(9) Uani 1 1 d .
O12 O 0.5625(3) 0.9013(3) 0.5988(2) 0.0453(10) Uani 1 1 d .
O13 O 0.7849(3) 1.0679(3) 0.6235(2) 0.0361(9) Uani 1 1 d .
O14 O 0.7570(3) 0.8912(3) 0.1501(2) 0.0459(10) Uani 1 1 d .
O15 O 1.0938(3) 0.9709(3) 0.2178(2) 0.0419(10) Uani 1 1 d .
O16 O 0.9327(3) 1.0793(3) 0.2236(2) 0.0437(10) Uani 1 1 d .
O17 O 0.9163(4) 0.7842(3) 0.1478(2) 0.0495(11) Uani 1 1 d .
O18 O 0.9050(3) 0.8091(3) 0.0129(2) 0.0467(10) Uani 1 1 d .
O19 O 0.9050(4) 1.1004(3) 0.0849(2) 0.0484(11) Uani 1 1 d .
O20 O 1.0731(3) 1.0021(3) 0.0842(2) 0.0424(10) Uani 1 1 d .
O21 O 0.7387(3) 0.9124(3) 0.0130(2) 0.0481(11) Uani 1 1 d .
O22 O 0.6255(3) 0.6394(3) 0.9877(3) 0.0515(11) Uani 1 1 d .
O23 O 0.6696(4) 0.4659(4) 1.0527(3) 0.0637(13) Uani 1 1 d .
O24 O 0.4942(4) 0.5358(4) 0.8651(3) 0.0616(13) Uani 1 1 d .
O25 O 0.4624(4) 0.6361(4) 1.0698(3) 0.0629(13) Uani 1 1 d .
O26 O 0.7066(4) 0.6702(3) 1.1891(3) 0.0613(13) Uani 1 1 d .
Rh1 Rh 0.99019(3) 0.75128(3) 0.43875(2) 0.02879(11) Uani 1 1 d .
Rh2 Rh 1.04715(3) 0.62894(3) 0.52040(3) 0.03116(11) Uani 1 1 d .
Rh3 Rh 0.59589(3) 1.02272(3) 0.54387(3) 0.03299(11) Uani 1 1 d .
Rh4 Rh 0.92430(4) 0.92999(3) 0.18952(2) 0.03390(12) Uani 1 1 d .
Rh5 Rh 0.90485(4) 0.95574(3) 0.04505(2) 0.03683(12) Uani 1 1 d .
Rh6 Rh 0.57012(4) 0.55457(4) 1.06479(3) 0.04212(13) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Rh1 Br1 Rh4 133.45(3) . .
Rh1 Br1 K1 83.49(3) . .
Rh4 Br1 K1 142.47(3) . .
Rh1 Br1 K1 84.92(3) . 2_776
Rh4 Br1 K1 106.48(3) . 2_776
K1 Br1 K1 79.11(4) . 2_776
O8 C1 O1 125.8(5) . .
O8 C1 C2 119.3(6) . .
O1 C1 C2 114.8(5) . .
C3 C2 C1 113.3(7) . .
C3 C2 H2A 108.9 . .
C1 C2 H2A 108.9 . .
C3 C2 H2B 108.9 . .
C1 C2 H2B 108.9 . .
H2A C2 H2B 107.7 . .
C2 C3 H3A 109.5 . .
C2 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C2 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
O7 C4 O2 126.2(5) . .
O7 C4 C5 114.3(6) . .
O2 C4 C5 119.4(6) . .
C6 C5 C4 113.2(9) . .
C6 C5 H5A 108.9 . .
C4 C5 H5A 108.9 . .
C6 C5 H5B 108.9 . .
C4 C5 H5B 108.9 . .
H5A C5 H5B 107.8 . .
C5 C6 K1 108.0(7) . .
C5 C6 H6A 109.5 . .
K1 C6 H6A 130.5 . .
C5 C6 H6B 109.5 . .
K1 C6 H6B 25.6 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
K1 C6 H6C 86.8 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
O5 C7 O3 125.2(5) 2_776 .
O5 C7 C8 118.5(5) 2_776 .
O3 C7 C8 116.3(5) . .
C7 C8 C9 117.1(5) . .
C7 C8 H8A 108.0 . .
C9 C8 H8A 108.0 . .
C7 C8 H8B 108.0 . .
C9 C8 H8B 108.0 . .
H8A C8 H8B 107.3 . .
C8 C9 H9A 109.5 . .
C8 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C8 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
O4 C10 O6 123.1(5) . .
O4 C10 C11 119.2(5) . .
O6 C10 C11 117.1(6) . .
C12 C11 C10 96.8(9) . .
C12 C11 H11A 112.4 . .
C10 C11 H11A 112.4 . .
C12 C11 H11B 112.4 . .
C10 C11 H11B 112.4 . .
H11A C11 H11B 109.9 . .
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
O9 C13 O10 125.1(5) 2_676 .
O9 C13 C14 117.9(5) 2_676 .
O10 C13 C14 117.0(6) . .
C15 C14 C13 114.1(7) . .
C15 C14 H14A 108.7 . .
C13 C14 H14A 108.7 . .
C15 C14 H14B 108.7 . .
C13 C14 H14B 108.7 . .
H14A C14 H14B 107.6 . .
C14 C15 H15A 109.5 . .
C14 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C14 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
O12 C16 O11 126.0(5) 2_676 .
O12 C16 C17 117.2(6) 2_676 .
O11 C16 C17 116.8(6) . .
C18 C17 C16 112.0(7) . .
C18 C17 H17A 109.2 . .
C16 C17 H17A 109.2 . .
C18 C17 H17B 109.2 . .
C16 C17 H17B 109.2 . .
H17A C17 H17B 107.9 . .
C17 C18 H18A 109.5 . .
C17 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C17 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
O21 C19 O14 125.3(5) . .
O21 C19 C20 118.9(5) . .
O14 C19 C20 115.8(5) . .
C21 C20 C19 116.4(5) . .
C21 C20 H20A 108.2 . .
C19 C20 H20A 108.2 . .
C21 C20 H20B 108.2 . .
C19 C20 H20B 108.2 . .
H20A C20 H20B 107.3 . .
C20 C21 H21A 109.5 . .
C20 C21 H21B 109.5 . .
H21A C21 H21B 109.5 . .
C20 C21 H21C 109.5 . .
H21A C21 H21C 109.5 . .
H21B C21 H21C 109.5 . .
O15 C22 O20 124.1(4) . .
O15 C22 C23 119.3(4) . .
O20 C22 C23 116.5(4) . .
C22 C23 C24 111.2(6) . .
C22 C23 H23A 109.4 . .
C24 C23 H23A 109.4 . .
C22 C23 H23B 109.4 . .
C24 C23 H23B 109.4 . .
H23A C23 H23B 108.0 . .
C23 C24 H24A 109.5 . .
C23 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C23 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
O16 C25 O19 126.7(5) . .
O16 C25 C26 117.8(5) . .
O19 C25 C26 115.5(5) . .
C27 C26 C25 113.6(6) . .
C27 C26 H26A 108.9 . .
C25 C26 H26A 108.9 . .
C27 C26 H26B 108.9 . .
C25 C26 H26B 108.9 . .
H26A C26 H26B 107.7 . .
C26 C27 H27A 109.5 . .
C26 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C26 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
O18 C28 O17 126.2(5) . .
O18 C28 C29 117.3(5) . .
O17 C28 C29 116.5(5) . .
C30 C29 C28 113.8(6) . .
C30 C29 H29A 108.8 . .
C28 C29 H29A 108.8 . .
C30 C29 H29B 108.8 . .
C28 C29 H29B 108.8 . .
H29A C29 H29B 107.7 . .
C29 C30 H30A 109.5 . .
C29 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C29 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
O24 C31 O22 126.5(5) . .
O24 C31 C32 117.0(6) . .
O22 C31 C32 116.4(6) . .
C33 C32 C31 111.8(7) . .
C33 C32 H32A 109.3 . .
C31 C32 H32A 109.3 . .
C33 C32 H32B 109.3 . .
C31 C32 H32B 109.3 . .
H32A C32 H32B 107.9 . .
C32 C33 H33A 109.5 . .
C32 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C32 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
O25 C34 O23 126.3(6) 2_667 .
O25 C34 C35 116.7(8) 2_667 .
O23 C34 C35 117.0(8) . .
C36 C35 C34 109.5(8) . .
C36 C35 H35A 109.8 . .
C34 C35 H35A 109.8 . .
C36 C35 H35B 109.8 . .
C34 C35 H35B 109.8 . .
H35A C35 H35B 108.2 . .
C35 C36 H36A 109.5 . .
C35 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C35 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
O3 K1 O10 92.61(12) . .
O3 K1 O13 78.34(11) . .
O10 K1 O13 67.32(11) . .
O3 K1 O2 148.44(12) . .
O10 K1 O2 109.40(12) . .
O13 K1 O2 130.50(12) . .
O3 K1 Br1 81.27(8) . .
O10 K1 Br1 113.18(9) . .
O13 K1 Br1 159.60(9) . .
O2 K1 Br1 69.52(8) . .
O3 K1 Br1 68.18(8) . 2_776
O10 K1 Br1 137.91(9) . 2_776
O13 K1 Br1 72.13(8) . 2_776
O2 K1 Br1 105.11(9) . 2_776
Br1 K1 Br1 100.89(4) . 2_776
O3 K1 C6 154.4(3) . .
O10 K1 C6 82.3(3) . .
O13 K1 C6 76.6(3) . .
O2 K1 C6 54.7(3) . .
Br1 K1 C6 123.8(3) . .
Br1 K1 C6 99.2(3) 2_776 .
O3 K1 Rh3 84.96(9) . .
O10 K1 Rh3 30.81(8) . .
O13 K1 Rh3 36.51(7) . .
O2 K1 Rh3 125.35(9) . .
Br1 K1 Rh3 140.56(4) . .
Br1 K1 Rh3 107.89(4) 2_776 .
C6 K1 Rh3 77.9(3) . .
O3 K1 Rh1 118.68(9) . .
O10 K1 Rh1 126.40(9) . .
O13 K1 Rh1 154.18(8) . .
O2 K1 Rh1 29.76(8) . .
Br1 K1 Rh1 42.80(2) . .
Br1 K1 Rh1 95.33(3) 2_776 .
C6 K1 Rh1 83.5(3) . .
Rh3 K1 Rh1 152.15(4) . .
O3 K1 Rh1 27.40(7) . 2_776
O10 K1 Rh1 109.34(9) . 2_776
O13 K1 Rh1 67.43(8) . 2_776
O2 K1 Rh1 141.26(9) . 2_776
Br1 K1 Rh1 94.40(3) . 2_776
Br1 K1 Rh1 41.63(2) 2_776 2_776
C6 K1 Rh1 132.7(3) . 2_776
Rh3 K1 Rh1 89.80(3) . 2_776
Rh1 K1 Rh1 118.01(3) . 2_776
O3 K1 K1 65.63(9) . 2_776
O10 K1 K1 153.42(10) . 2_776
O13 K1 K1 119.05(9) . 2_776
O2 K1 K1 86.25(9) . 2_776
Br1 K1 K1 51.12(3) . 2_776
Br1 K1 K1 49.78(3) 2_776 2_776
C6 K1 K1 124.0(3) . 2_776
Rh3 K1 K1 147.57(5) . 2_776
Rh1 K1 K1 60.20(3) . 2_776
Rh1 K1 K1 57.80(3) 2_776 2_776
C1 O1 Rh1 119.0(3) . .
C4 O2 Rh1 118.1(4) . .
C4 O2 K1 129.3(4) . .
Rh1 O2 K1 107.16(15) . .
C7 O3 Rh1 119.3(3) . 2_776
C7 O3 K1 125.4(3) . .
Rh1 O3 K1 113.85(14) 2_776 .
C10 O4 Rh1 120.9(3) . .
C7 O5 Rh2 119.6(3) 2_776 .
C10 O6 Rh2 120.3(3) . .
C10 O6 Rh2 139.0(3) . 2_766
Rh2 O6 Rh2 100.70(14) . 2_766
C4 O7 Rh2 119.3(4) . .
C1 O8 Rh2 119.0(3) . .
C13 O9 Rh3 120.0(4) 2_676 .
C13 O10 Rh3 118.5(4) . .
C13 O10 K1 136.2(4) . .
Rh3 O10 K1 105.18(15) . .
C16 O11 Rh3 118.3(4) . .
C16 O12 Rh3 119.2(4) 2_676 .
Rh3 O13 K1 97.73(12) . .
C19 O14 Rh4 119.4(3) . .
C22 O15 Rh4 120.4(3) . .
C25 O16 Rh4 118.6(3) . .
C28 O17 Rh4 118.8(3) . .
C28 O18 Rh5 118.8(3) . .
C25 O19 Rh5 118.2(3) . .
C22 O20 Rh5 119.6(3) . .
C22 O20 Rh5 139.3(3) . 2_775
Rh5 O20 Rh5 101.05(14) . 2_775
C19 O21 Rh5 119.0(3) . .
C31 O22 Rh6 118.1(4) . .
C34 O23 Rh6 118.8(4) . .
C31 O24 Rh6 119.1(4) . 2_667
C34 O25 Rh6 118.8(4) 2_667 .
O1 Rh1 O3 89.70(16) . 2_776
O1 Rh1 O2 175.74(15) . .
O3 Rh1 O2 89.92(16) 2_776 .
O1 Rh1 O4 89.96(17) . .
O3 Rh1 O4 174.96(14) 2_776 .
O2 Rh1 O4 90.05(18) . .
O1 Rh1 Rh2 87.88(11) . .
O3 Rh1 Rh2 87.92(10) 2_776 .
O2 Rh1 Rh2 87.87(11) . .
O4 Rh1 Rh2 87.04(11) . .
O1 Rh1 Br1 92.16(11) . .
O3 Rh1 Br1 90.91(10) 2_776 .
O2 Rh1 Br1 92.09(11) . .
O4 Rh1 Br1 94.13(11) . .
Rh2 Rh1 Br1 178.83(2) . .
O1 Rh1 K1 140.58(11) . .
O3 Rh1 K1 73.71(11) 2_776 .
O2 Rh1 K1 43.09(11) . .
O4 Rh1 K1 109.50(13) . .
Rh2 Rh1 K1 125.82(3) . .
Br1 Rh1 K1 53.71(2) . .
O1 Rh1 K1 82.55(11) . 2_776
O3 Rh1 K1 38.75(10) 2_776 2_776
O2 Rh1 K1 99.76(12) . 2_776
O4 Rh1 K1 146.09(11) . 2_776
Rh2 Rh1 K1 125.41(3) . 2_776
Br1 Rh1 K1 53.45(3) . 2_776
K1 Rh1 K1 61.99(3) . 2_776
O7 Rh2 O5 90.17(17) . .
O7 Rh2 O8 176.29(16) . .
O5 Rh2 O8 91.00(16) . .
O7 Rh2 O6 89.27(17) . .
O5 Rh2 O6 176.70(15) . .
O8 Rh2 O6 89.36(16) . .
O7 Rh2 O6 90.66(15) . 2_766
O5 Rh2 O6 103.97(13) . 2_766
O8 Rh2 O6 92.48(15) . 2_766
O6 Rh2 O6 79.30(14) . 2_766
O7 Rh2 Rh1 88.41(11) . .
O5 Rh2 Rh1 88.02(10) . .
O8 Rh2 Rh1 88.11(11) . .
O6 Rh2 Rh1 88.71(10) . .
O6 Rh2 Rh1 167.98(8) 2_766 .
O11 Rh3 O12 176.37(15) . .
O11 Rh3 O9 89.43(16) . .
O12 Rh3 O9 90.83(17) . .
O11 Rh3 O10 90.83(16) . .
O12 Rh3 O10 88.67(16) . .
O9 Rh3 O10 176.27(15) . .
O11 Rh3 O13 89.62(14) . .
O12 Rh3 O13 93.97(14) . .
O9 Rh3 O13 93.97(14) . .
O10 Rh3 O13 89.76(14) . .
O11 Rh3 Rh3 88.50(11) . 2_676
O12 Rh3 Rh3 87.89(11) . 2_676
O9 Rh3 Rh3 87.99(11) . 2_676
O10 Rh3 Rh3 88.29(11) . 2_676
O13 Rh3 Rh3 177.27(9) . 2_676
O11 Rh3 K1 89.89(11) . .
O12 Rh3 K1 92.25(12) . .
O9 Rh3 K1 139.72(12) . .
O10 Rh3 K1 44.01(11) . .
O13 Rh3 K1 45.75(9) . .
Rh3 Rh3 K1 132.25(3) 2_676 .
O17 Rh4 O14 89.49(18) . .
O17 Rh4 O16 176.06(14) . .
O14 Rh4 O16 90.86(17) . .
O17 Rh4 O15 90.01(17) . .
O14 Rh4 O15 174.57(13) . .
O16 Rh4 O15 89.28(16) . .
O17 Rh4 Rh5 88.39(10) . .
O14 Rh4 Rh5 87.81(10) . .
O16 Rh4 Rh5 87.71(10) . .
O15 Rh4 Rh5 86.77(9) . .
O17 Rh4 Br1 90.39(10) . .
O14 Rh4 Br1 87.76(10) . .
O16 Rh4 Br1 93.54(10) . .
O15 Rh4 Br1 97.65(9) . .
Rh5 Rh4 Br1 175.42(2) . .
O21 Rh5 O19 88.95(18) . .
O21 Rh5 O18 90.68(17) . .
O19 Rh5 O18 176.32(14) . .
O21 Rh5 O20 176.89(15) . .
O19 Rh5 O20 89.51(17) . .
O18 Rh5 O20 90.69(17) . .
O21 Rh5 O20 103.74(14) . 2_775
O19 Rh5 O20 89.29(14) . 2_775
O18 Rh5 O20 94.36(14) . 2_775
O20 Rh5 O20 78.95(14) . 2_775
O21 Rh5 Rh4 88.35(10) . .
O19 Rh5 Rh4 88.60(10) . .
O18 Rh5 Rh4 87.73(10) . .
O20 Rh5 Rh4 88.91(9) . .
O20 Rh5 Rh4 167.69(9) 2_775 .
O25 Rh6 O22 91.18(19) . .
O25 Rh6 O23 176.09(19) . .
O22 Rh6 O23 89.1(2) . .
O25 Rh6 O24 88.2(2) . 2_667
O22 Rh6 O24 176.19(16) . 2_667
O23 Rh6 O24 91.3(2) . 2_667
O25 Rh6 O26 89.64(19) . .
O22 Rh6 O26 88.81(16) . .
O23 Rh6 O26 94.27(19) . .
O24 Rh6 O26 94.94(16) 2_667 .
O25 Rh6 Rh6 88.24(14) . 2_667
O22 Rh6 Rh6 88.75(12) . 2_667
O23 Rh6 Rh6 87.86(14) . 2_667
O24 Rh6 Rh6 87.48(12) 2_667 2_667
O26 Rh6 Rh6 176.73(12) . 2_667
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Br1 Rh1 2.7008(7) .
Br1 Rh4 2.7239(7) .
Br1 K1 3.2038(14) .
Br1 K1 3.2662(15) 2_776
C1 O8 1.257(7) .
C1 O1 1.269(7) .
C1 C2 1.510(4) .
C2 C3 1.496(5) .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C3 H3A 0.9600 .
C3 H3B 0.9600 .
C3 H3C 0.9600 .
C4 O7 1.263(7) .
C4 O2 1.269(7) .
C4 C5 1.499(10) .
C5 C6 1.442(17) .
C5 H5A 0.9700 .
C5 H5B 0.9700 .
C6 K1 3.351(13) .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
C7 O5 1.266(6) 2_776
C7 O3 1.265(6) .
C7 C8 1.498(8) .
C8 C9 1.504(8) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C9 H9A 0.9600 .
C9 H9B 0.9600 .
C9 H9C 0.9600 .
C10 O4 1.272(7) .
C10 O6 1.275(7) .
C10 C11 1.522(5) .
C11 C12 1.494(5) .
C11 H11A 0.9700 .
C11 H11B 0.9700 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 O9 1.259(7) 2_676
C13 O10 1.275(7) .
C13 C14 1.510(9) .
C14 C15 1.416(12) .
C14 H14A 0.9700 .
C14 H14B 0.9700 .
C15 H15A 0.9600 .
C15 H15B 0.9600 .
C15 H15C 0.9600 .
C16 O12 1.257(7) 2_676
C16 O11 1.271(7) .
C16 C17 1.512(8) .
C17 C18 1.493(13) .
C17 H17A 0.9700 .
C17 H17B 0.9700 .
C18 H18A 0.9600 .
C18 H18B 0.9600 .
C18 H18C 0.9600 .
C19 O21 1.265(6) .
C19 O14 1.270(6) .
C19 C20 1.508(4) .
C20 C21 1.505(4) .
C20 H20A 0.9700 .
C20 H20B 0.9700 .
C21 H21A 0.9600 .
C21 H21B 0.9600 .
C21 H21C 0.9600 .
C22 O15 1.257(6) .
C22 O20 1.271(6) .
C22 C23 1.507(4) .
C23 C24 1.509(5) .
C23 H23A 0.9700 .
C23 H23B 0.9700 .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
C25 O16 1.259(6) .
C25 O19 1.268(7) .
C25 C26 1.505(4) .
C26 C27 1.503(5) .
C26 H26A 0.9700 .
C26 H26B 0.9700 .
C27 H27A 0.9600 .
C27 H27B 0.9600 .
C27 H27C 0.9600 .
C28 O18 1.261(7) .
C28 O17 1.264(7) .
C28 C29 1.506(4) .
C29 C30 1.504(5) .
C29 H29A 0.9700 .
C29 H29B 0.9700 .
C30 H30A 0.9600 .
C30 H30B 0.9600 .
C30 H30C 0.9600 .
C31 O24 1.261(7) .
C31 O22 1.262(7) .
C31 C32 1.511(4) .
C32 C33 1.502(5) .
C32 H32A 0.9700 .
C32 H32B 0.9700 .
C33 H33A 0.9600 .
C33 H33B 0.9600 .
C33 H33C 0.9600 .
C34 O25 1.258(9) 2_667
C34 O23 1.263(9) .
C34 C35 1.511(5) .
C35 C36 1.506(5) .
C35 H35A 0.9700 .
C35 H35B 0.9700 .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
K1 O3 2.772(4) .
K1 O10 2.785(4) .
K1 O13 2.797(4) .
K1 O2 2.823(4) .
K1 Br1 3.2661(15) 2_776
K1 Rh3 3.8684(14) .
K1 Rh1 3.9491(14) .
K1 Rh1 4.0498(15) 2_776
K1 K1 4.120(3) 2_776
O1 Rh1 2.031(4) .
O2 Rh1 2.051(4) .
O3 Rh1 2.038(3) 2_776
O4 Rh1 2.058(4) .
O5 C7 1.266(6) 2_776
O5 Rh2 2.029(4) .
O6 Rh2 2.033(3) .
O6 Rh2 2.390(4) 2_766
O7 Rh2 2.020(4) .
O8 Rh2 2.032(4) .
O9 C13 1.259(7) 2_676
O9 Rh3 2.037(4) .
O10 Rh3 2.053(4) .
O11 Rh3 2.031(4) .
O12 C16 1.257(7) 2_676
O12 Rh3 2.034(4) .
O13 Rh3 2.323(3) .
O14 Rh4 2.026(4) .
O15 Rh4 2.075(4) .
O16 Rh4 2.043(4) .
O17 Rh4 2.019(4) .
O18 Rh5 2.034(4) .
O19 Rh5 2.028(4) .
O20 Rh5 2.040(4) .
O20 Rh5 2.361(3) 2_775
O21 Rh5 2.025(4) .
O22 Rh6 2.028(4) .
O23 Rh6 2.031(5) .
O24 Rh6 2.035(4) 2_667
O25 C34 1.258(9) 2_667
O25 Rh6 2.025(5) .
O26 Rh6 2.356(4) .
Rh1 O3 2.038(3) 2_776
Rh1 Rh2 2.3910(6) .
Rh1 K1 4.0498(15) 2_776
Rh2 O6 2.390(4) 2_766
Rh3 Rh3 2.3810(9) 2_676
Rh4 Rh5 2.3867(6) .
Rh5 O20 2.361(3) 2_775
Rh6 O24 2.035(4) 2_667
Rh6 Rh6 2.3875(10) 2_667
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O8 C1 C2 C3 44.2(12) . .
O1 C1 C2 C3 -136.6(10) . .
O7 C4 C5 C6 134.2(10) . .
O2 C4 C5 C6 -48.1(14) . .
C4 C5 C6 K1 33.3(12) . .
O5 C7 C8 C9 -0.6(9) 2_776 .
O3 C7 C8 C9 179.5(6) . .
O4 C10 C11 C12 -96.0(10) . .
O6 C10 C11 C12 92.7(10) . .
O9 C13 C14 C15 -95.7(10) 2_676 .
O10 C13 C14 C15 84.3(10) . .
O12 C16 C17 C18 81.9(9) 2_676 .
O11 C16 C17 C18 -97.9(9) . .
O21 C19 C20 C21 3.1(10) . .
O14 C19 C20 C21 -176.7(6) . .
O15 C22 C23 C24 93.3(7) . .
O20 C22 C23 C24 -84.8(7) . .
O16 C25 C26 C27 135.4(8) . .
O19 C25 C26 C27 -45.5(9) . .
O18 C28 C29 C30 152.5(7) . .
O17 C28 C29 C30 -27.4(10) . .
O24 C31 C32 C33 -59.7(11) . .
O22 C31 C32 C33 120.5(9) . .
O25 C34 C35 C36 77.4(11) 2_667 .
O23 C34 C35 C36 -103.6(10) . .
Rh1 Br1 K1 O3 151.70(8) . .
Rh4 Br1 K1 O3 -37.28(10) . .
K1 Br1 K1 O3 65.64(8) 2_776 .
Rh1 Br1 K1 O10 -119.19(10) . .
Rh4 Br1 K1 O10 51.82(12) . .
K1 Br1 K1 O10 154.75(11) 2_776 .
Rh1 Br1 K1 O13 153.8(2) . .
Rh4 Br1 K1 O13 -35.2(3) . .
K1 Br1 K1 O13 67.7(2) 2_776 .
Rh1 Br1 K1 O2 -16.15(9) . .
Rh4 Br1 K1 O2 154.86(10) . .
K1 Br1 K1 O2 -102.21(10) 2_776 .
Rh1 Br1 K1 Br1 86.06(3) . 2_776
Rh4 Br1 K1 Br1 -102.93(5) . 2_776
K1 Br1 K1 Br1 0.0 2_776 2_776
Rh1 Br1 K1 C6 -22.8(3) . .
Rh4 Br1 K1 C6 148.2(3) . .
K1 Br1 K1 C6 -108.9(3) 2_776 .
Rh1 Br1 K1 Rh3 -137.36(6) . .
Rh4 Br1 K1 Rh3 33.66(10) . .
K1 Br1 K1 Rh3 136.58(8) 2_776 .
Rh4 Br1 K1 Rh1 171.01(5) . .
K1 Br1 K1 Rh1 -86.06(3) 2_776 .
Rh1 Br1 K1 Rh1 127.59(3) . 2_776
Rh4 Br1 K1 Rh1 -61.40(6) . 2_776
K1 Br1 K1 Rh1 41.53(2) 2_776 2_776
Rh1 Br1 K1 K1 86.06(3) . 2_776
Rh4 Br1 K1 K1 -102.93(5) . 2_776
C5 C6 K1 O3 -173.3(6) . .
C5 C6 K1 O10 106.9(10) . .
C5 C6 K1 O13 175.3(10) . .
C5 C6 K1 O2 -13.6(8) . .
C5 C6 K1 Br1 -5.9(11) . .
C5 C6 K1 Br1 -115.7(9) . 2_776
C5 C6 K1 Rh3 137.8(10) . .
C5 C6 K1 Rh1 -21.3(9) . .
C5 C6 K1 Rh1 -143.9(8) . 2_776
C5 C6 K1 K1 -68.5(10) . 2_776
O8 C1 O1 Rh1 -5.5(8) . .
C2 C1 O1 Rh1 175.3(4) . .
O7 C4 O2 Rh1 4.5(9) . .
C5 C4 O2 Rh1 -172.8(6) . .
O7 C4 O2 K1 -145.9(5) . .
C5 C4 O2 K1 36.7(9) . .
O3 K1 O2 C4 151.8(5) . .
O10 K1 O2 C4 -76.4(5) . .
O13 K1 O2 C4 -0.1(6) . .
Br1 K1 O2 C4 175.3(5) . .
Br1 K1 O2 C4 79.1(5) 2_776 .
C6 K1 O2 C4 -11.5(6) . .
Rh3 K1 O2 C4 -46.5(5) . .
Rh1 K1 O2 C4 152.9(6) . .
Rh1 K1 O2 C4 104.8(5) 2_776 .
K1 K1 O2 C4 125.6(5) 2_776 .
O3 K1 O2 Rh1 -1.0(3) . .
O10 K1 O2 Rh1 130.68(15) . .
O13 K1 O2 Rh1 -153.02(14) . .
Br1 K1 O2 Rh1 22.38(12) . .
Br1 K1 O2 Rh1 -73.82(15) 2_776 .
C6 K1 O2 Rh1 -164.4(4) . .
Rh3 K1 O2 Rh1 160.61(10) . .
Rh1 K1 O2 Rh1 -48.1(2) 2_776 .
K1 K1 O2 Rh1 -27.30(14) 2_776 .
O5 C7 O3 Rh1 -0.4(7) 2_776 2_776
C8 C7 O3 Rh1 179.6(4) . 2_776
O5 C7 O3 K1 164.9(4) 2_776 .
C8 C7 O3 K1 -15.2(7) . .
O10 K1 O3 C7 -36.8(4) . .
O13 K1 O3 C7 -103.0(4) . .
O2 K1 O3 C7 98.4(5) . .
Br1 K1 O3 C7 76.3(4) . .
Br1 K1 O3 C7 -178.2(4) 2_776 .
C6 K1 O3 C7 -114.3(7) . .
Rh3 K1 O3 C7 -66.6(4) . .
Rh1 K1 O3 C7 97.8(4) . .
Rh1 K1 O3 C7 -166.0(5) 2_776 .
K1 K1 O3 C7 127.4(4) 2_776 .
O10 K1 O3 Rh1 129.22(17) . 2_776
O13 K1 O3 Rh1 63.02(17) . 2_776
O2 K1 O3 Rh1 -95.6(3) . 2_776
Br1 K1 O3 Rh1 -117.72(16) . 2_776
Br1 K1 O3 Rh1 -12.21(13) 2_776 2_776
C6 K1 O3 Rh1 51.7(7) . 2_776
Rh3 K1 O3 Rh1 99.35(16) . 2_776
Rh1 K1 O3 Rh1 -96.18(16) . 2_776
K1 K1 O3 Rh1 -66.59(15) 2_776 2_776
O6 C10 O4 Rh1 0.6(10) . .
C11 C10 O4 Rh1 -170.1(7) . .
O4 C10 O6 Rh2 -0.8(10) . .
C11 C10 O6 Rh2 170.1(7) . .
O4 C10 O6 Rh2 178.8(4) . 2_766
C11 C10 O6 Rh2 -10.2(12) . 2_766
O2 C4 O7 Rh2 -3.7(9) . .
C5 C4 O7 Rh2 173.7(6) . .
O1 C1 O8 Rh2 4.5(8) . .
C2 C1 O8 Rh2 -176.4(4) . .
O9 C13 O10 Rh3 0.8(8) 2_676 .
C14 C13 O10 Rh3 -179.3(4) . .
O9 C13 O10 K1 -175.7(4) 2_676 .
C14 C13 O10 K1 4.2(9) . .
O3 K1 O10 C13 101.2(5) . .
O13 K1 O10 C13 177.4(6) . .
O2 K1 O10 C13 -55.8(6) . .
Br1 K1 O10 C13 19.5(6) . .
Br1 K1 O10 C13 160.9(5) 2_776 .
C6 K1 O10 C13 -104.0(6) . .
Rh3 K1 O10 C13 176.8(6) . .
Rh1 K1 O10 C13 -27.9(6) . .
Rh1 K1 O10 C13 123.4(5) 2_776 .
K1 K1 O10 C13 67.5(6) 2_776 .
O3 K1 O10 Rh3 -75.64(16) . .
O13 K1 O10 Rh3 0.58(13) . .
O2 K1 O10 Rh3 127.39(15) . .
Br1 K1 O10 Rh3 -157.26(11) . .
Br1 K1 O10 Rh3 -15.9(2) 2_776 .
C6 K1 O10 Rh3 79.2(3) . .
Rh1 K1 O10 Rh3 155.27(9) . .
Rh1 K1 O10 Rh3 -53.44(15) 2_776 .
K1 K1 O10 Rh3 -109.3(2) 2_776 .
O12 C16 O11 Rh3 -4.1(8) 2_676 .
C17 C16 O11 Rh3 175.7(4) . .
O3 K1 O13 Rh3 97.36(13) . .
O10 K1 O13 Rh3 -0.50(11) . .
O2 K1 O13 Rh3 -97.18(16) . .
Br1 K1 O13 Rh3 95.3(3) . .
Br1 K1 O13 Rh3 167.96(12) 2_776 .
C6 K1 O13 Rh3 -87.6(3) . .
Rh1 K1 O13 Rh3 -128.31(15) . .
Rh1 K1 O13 Rh3 123.72(12) 2_776 .
K1 K1 O13 Rh3 150.74(9) 2_776 .
O21 C19 O14 Rh4 3.2(8) . .
C20 C19 O14 Rh4 -176.9(4) . .
O20 C22 O15 Rh4 -0.8(8) . .
C23 C22 O15 Rh4 -178.8(4) . .
O19 C25 O16 Rh4 -0.6(9) . .
C26 C25 O16 Rh4 178.4(5) . .
O18 C28 O17 Rh4 -0.9(9) . .
C29 C28 O17 Rh4 178.9(4) . .
O17 C28 O18 Rh5 -2.0(9) . .
C29 C28 O18 Rh5 178.1(4) . .
O16 C25 O19 Rh5 -3.2(9) . .
C26 C25 O19 Rh5 177.8(4) . .
O15 C22 O20 Rh5 -3.0(8) . .
C23 C22 O20 Rh5 175.1(4) . .
O15 C22 O20 Rh5 -179.7(4) . 2_775
C23 C22 O20 Rh5 -1.6(9) . 2_775
O14 C19 O21 Rh5 -4.7(8) . .
C20 C19 O21 Rh5 175.5(4) . .
O24 C31 O22 Rh6 3.0(10) . .
C32 C31 O22 Rh6 -177.2(5) . .
O25 C34 O23 Rh6 -2.8(10) 2_667 .
C35 C34 O23 Rh6 178.4(6) . .
O22 C31 O24 Rh6 -2.4(10) . 2_667
C32 C31 O24 Rh6 177.9(5) . 2_667
C1 O1 Rh1 O3 91.2(4) . 2_776
C1 O1 Rh1 O2 6(2) . .
C1 O1 Rh1 O4 -83.8(4) . .
C1 O1 Rh1 Rh2 3.2(4) . .
C1 O1 Rh1 Br1 -177.9(4) . .
C1 O1 Rh1 K1 154.5(3) . .
C1 O1 Rh1 K1 129.4(4) . 2_776
C4 O2 Rh1 O1 -6(2) . .
K1 O2 Rh1 O1 151(2) . .
C4 O2 Rh1 O3 -90.6(5) . 2_776
K1 O2 Rh1 O3 65.86(16) . 2_776
C4 O2 Rh1 O4 84.4(5) . .
K1 O2 Rh1 O4 -119.18(16) . .
C4 O2 Rh1 Rh2 -2.7(4) . .
K1 O2 Rh1 Rh2 153.78(13) . .
C4 O2 Rh1 Br1 178.5(4) . .
K1 O2 Rh1 Br1 -25.05(13) . .
C4 O2 Rh1 K1 -156.4(5) . .
C4 O2 Rh1 K1 -128.2(4) . 2_776
K1 O2 Rh1 K1 28.19(14) . 2_776
C10 O4 Rh1 O1 87.7(5) . .
C10 O4 Rh1 O3 2(2) . 2_776
C10 O4 Rh1 O2 -88.0(5) . .
C10 O4 Rh1 Rh2 -0.1(5) . .
C10 O4 Rh1 Br1 179.9(5) . .
C10 O4 Rh1 K1 -127.2(5) . .
C10 O4 Rh1 K1 164.2(4) . 2_776
Rh4 Br1 Rh1 O1 28.88(12) . .
K1 Br1 Rh1 O1 -158.65(11) . .
K1 Br1 Rh1 O1 -79.07(11) 2_776 .
Rh4 Br1 Rh1 O3 118.61(11) . 2_776
K1 Br1 Rh1 O3 -68.92(11) . 2_776
K1 Br1 Rh1 O3 10.66(11) 2_776 2_776
Rh4 Br1 Rh1 O2 -151.44(12) . .
K1 Br1 Rh1 O2 21.03(12) . .
K1 Br1 Rh1 O2 100.61(12) 2_776 .
Rh4 Br1 Rh1 O4 -61.23(14) . .
K1 Br1 Rh1 O4 111.24(13) . .
K1 Br1 Rh1 O4 -169.18(13) 2_776 .
Rh4 Br1 Rh1 Rh2 120.9(12) . .
K1 Br1 Rh1 Rh2 -66.6(12) . .
K1 Br1 Rh1 Rh2 12.9(12) 2_776 .
Rh4 Br1 Rh1 K1 -172.47(5) . .
K1 Br1 Rh1 K1 79.58(4) 2_776 .
Rh4 Br1 Rh1 K1 107.95(4) . 2_776
K1 Br1 Rh1 K1 -79.58(4) . 2_776
O3 K1 Rh1 O1 2.7(2) . .
O10 K1 Rh1 O1 120.6(2) . .
O13 K1 Rh1 O1 -124.3(3) . .
O2 K1 Rh1 O1 -176.7(2) . .
Br1 K1 Rh1 O1 34.95(18) . .
Br1 K1 Rh1 O1 -65.34(18) 2_776 .
C6 K1 Rh1 O1 -164.0(3) . .
Rh3 K1 Rh1 O1 147.87(18) . .
Rh1 K1 Rh1 O1 -28.54(18) 2_776 .
K1 K1 Rh1 O1 -28.54(18) 2_776 .
O3 K1 Rh1 O3 71.31(15) . 2_776
O10 K1 Rh1 O3 -170.78(15) . 2_776
O13 K1 Rh1 O3 -55.7(2) . 2_776
O2 K1 Rh1 O3 -108.07(19) . 2_776
Br1 K1 Rh1 O3 103.60(10) . 2_776
Br1 K1 Rh1 O3 3.30(10) 2_776 2_776
C6 K1 Rh1 O3 -95.3(3) . 2_776
Rh3 K1 Rh1 O3 -143.48(13) . 2_776
Rh1 K1 Rh1 O3 40.10(10) 2_776 2_776
K1 K1 Rh1 O3 40.10(10) 2_776 2_776
O3 K1 Rh1 O2 179.38(19) . .
O10 K1 Rh1 O2 -62.7(2) . .
O13 K1 Rh1 O2 52.4(3) . .
Br1 K1 Rh1 O2 -148.33(17) . .
Br1 K1 Rh1 O2 111.37(17) 2_776 .
C6 K1 Rh1 O2 12.7(3) . .
Rh3 K1 Rh1 O2 -35.41(18) . .
Rh1 K1 Rh1 O2 148.17(17) 2_776 .
K1 K1 Rh1 O2 148.18(17) 2_776 .
O3 K1 Rh1 O4 -112.77(15) . .
O10 K1 Rh1 O4 5.13(16) . .
O13 K1 Rh1 O4 120.2(2) . .
O2 K1 Rh1 O4 67.8(2) . .
Br1 K1 Rh1 O4 -80.49(12) . .
Br1 K1 Rh1 O4 179.22(12) 2_776 .
C6 K1 Rh1 O4 80.6(3) . .
Rh3 K1 Rh1 O4 32.43(14) . .
Rh1 K1 Rh1 O4 -143.98(12) 2_776 .
K1 K1 Rh1 O4 -143.98(12) 2_776 .
O3 K1 Rh1 Rh2 146.39(9) . .
O10 K1 Rh1 Rh2 -95.70(11) . .
O13 K1 Rh1 Rh2 19.4(2) . .
O2 K1 Rh1 Rh2 -32.99(17) . .
Br1 K1 Rh1 Rh2 178.68(3) . .
Br1 K1 Rh1 Rh2 78.38(4) 2_776 .
C6 K1 Rh1 Rh2 -20.3(3) . .
Rh3 K1 Rh1 Rh2 -68.40(9) . .
Rh1 K1 Rh1 Rh2 115.18(4) 2_776 .
K1 K1 Rh1 Rh2 115.19(4) 2_776 .
O3 K1 Rh1 Br1 -32.28(9) . .
O10 K1 Rh1 Br1 85.62(11) . .
O13 K1 Rh1 Br1 -159.3(2) . .
O2 K1 Rh1 Br1 148.33(17) . .
Br1 K1 Rh1 Br1 -100.29(3) 2_776 .
C6 K1 Rh1 Br1 161.1(3) . .
Rh3 K1 Rh1 Br1 112.92(8) . .
Rh1 K1 Rh1 Br1 -63.49(3) 2_776 .
K1 K1 Rh1 Br1 -63.49(3) 2_776 .
O3 K1 Rh1 K1 31.21(8) . 2_776
O10 K1 Rh1 K1 149.11(12) . 2_776
O13 K1 Rh1 K1 -95.8(2) . 2_776
O2 K1 Rh1 K1 -148.18(17) . 2_776
Br1 K1 Rh1 K1 63.49(3) . 2_776
Br1 K1 Rh1 K1 -36.80(2) 2_776 2_776
C6 K1 Rh1 K1 -135.4(3) . 2_776
Rh3 K1 Rh1 K1 176.41(11) . 2_776
Rh1 K1 Rh1 K1 0.0 2_776 2_776
C4 O7 Rh2 O5 89.1(5) . .
C4 O7 Rh2 O8 -19(3) . .
C4 O7 Rh2 O6 -87.7(5) . .
C4 O7 Rh2 O6 -167.0(5) . 2_766
C4 O7 Rh2 Rh1 1.1(4) . .
C7 O5 Rh2 O7 -88.9(4) 2_776 .
C7 O5 Rh2 O8 87.6(4) 2_776 .
C7 O5 Rh2 O6 -9(3) 2_776 .
C7 O5 Rh2 O6 -179.6(4) 2_776 2_766
C7 O5 Rh2 Rh1 -0.5(4) 2_776 .
C1 O8 Rh2 O7 19(3) . .
C1 O8 Rh2 O5 -89.3(4) . .
C1 O8 Rh2 O6 87.4(4) . .
C1 O8 Rh2 O6 166.7(4) . 2_766
C1 O8 Rh2 Rh1 -1.3(4) . .
C10 O6 Rh2 O7 89.0(5) . .
Rh2 O6 Rh2 O7 -90.81(17) 2_766 .
C10 O6 Rh2 O5 9(3) . .
Rh2 O6 Rh2 O5 -171(3) 2_766 .
C10 O6 Rh2 O8 -87.6(5) . .
Rh2 O6 Rh2 O8 92.64(16) 2_766 .
C10 O6 Rh2 O6 179.8(6) . 2_766
Rh2 O6 Rh2 O6 0.0 2_766 2_766
C10 O6 Rh2 Rh1 0.5(5) . .
Rh2 O6 Rh2 Rh1 -179.23(13) 2_766 .
O1 Rh1 Rh2 O7 -179.54(16) . .
O3 Rh1 Rh2 O7 90.69(16) 2_776 .
O2 Rh1 Rh2 O7 0.69(16) . .
O4 Rh1 Rh2 O7 -89.47(18) . .
Br1 Rh1 Rh2 O7 88.4(12) . .
K1 Rh1 Rh2 O7 22.54(12) . .
K1 Rh1 Rh2 O7 101.16(12) 2_776 .
O1 Rh1 Rh2 O5 90.24(16) . .
O3 Rh1 Rh2 O5 0.47(15) 2_776 .
O2 Rh1 Rh2 O5 -89.53(16) . .
O4 Rh1 Rh2 O5 -179.69(17) . .
Br1 Rh1 Rh2 O5 -1.8(12) . .
K1 Rh1 Rh2 O5 -67.68(12) . .
K1 Rh1 Rh2 O5 10.94(12) 2_776 .
O1 Rh1 Rh2 O8 -0.82(16) . .
O3 Rh1 Rh2 O8 -90.60(16) 2_776 .
O2 Rh1 Rh2 O8 179.41(16) . .
O4 Rh1 Rh2 O8 89.24(17) . .
Br1 Rh1 Rh2 O8 -92.9(12) . .
K1 Rh1 Rh2 O8 -158.74(12) . .
K1 Rh1 Rh2 O8 -80.13(12) 2_776 .
O1 Rh1 Rh2 O6 -90.23(16) . .
O3 Rh1 Rh2 O6 180.00(16) 2_776 .
O2 Rh1 Rh2 O6 90.00(16) . .
O4 Rh1 Rh2 O6 -0.17(17) . .
Br1 Rh1 Rh2 O6 178(100) . .
K1 Rh1 Rh2 O6 111.85(12) . .
K1 Rh1 Rh2 O6 -169.53(12) 2_776 .
O1 Rh1 Rh2 O6 -93.9(5) . 2_766
O3 Rh1 Rh2 O6 176.4(5) 2_776 2_766
O2 Rh1 Rh2 O6 86.4(5) . 2_766
O4 Rh1 Rh2 O6 -3.8(5) . 2_766
Br1 Rh1 Rh2 O6 174(36) . 2_766
K1 Rh1 Rh2 O6 108.2(5) . 2_766
K1 Rh1 Rh2 O6 -173.2(5) 2_776 2_766
C16 O11 Rh3 O12 8(3) . .
C16 O11 Rh3 O9 -85.8(4) . .
C16 O11 Rh3 O10 90.5(4) . .
C16 O11 Rh3 O13 -179.8(4) . .
C16 O11 Rh3 Rh3 2.2(4) . 2_676
C16 O11 Rh3 K1 134.5(4) . .
C16 O12 Rh3 O11 -5(3) 2_676 .
C16 O12 Rh3 O9 89.3(4) 2_676 .
C16 O12 Rh3 O10 -87.0(4) 2_676 .
C16 O12 Rh3 O13 -176.7(4) 2_676 .
C16 O12 Rh3 Rh3 1.3(4) 2_676 2_676
C16 O12 Rh3 K1 -130.9(4) 2_676 .
C13 O9 Rh3 O11 87.6(5) 2_676 .
C13 O9 Rh3 O12 -88.8(5) 2_676 .
C13 O9 Rh3 O10 -6(3) 2_676 .
C13 O9 Rh3 O13 177.2(4) 2_676 .
C13 O9 Rh3 Rh3 -0.9(4) 2_676 2_676
C13 O9 Rh3 K1 176.8(4) 2_676 .
C13 O10 Rh3 O11 -88.5(4) . .
K1 O10 Rh3 O11 88.97(16) . .
C13 O10 Rh3 O12 87.9(4) . .
K1 O10 Rh3 O12 -94.62(16) . .
C13 O10 Rh3 O9 5(3) . .
K1 O10 Rh3 O9 -177(2) . .
C13 O10 Rh3 O13 -178.1(4) . .
K1 O10 Rh3 O13 -0.64(15) . .
C13 O10 Rh3 Rh3 0.0(4) . 2_676
K1 O10 Rh3 Rh3 177.45(12) . 2_676
C13 O10 Rh3 K1 -177.5(5) . .
K1 O13 Rh3 O11 -90.21(14) . .
K1 O13 Rh3 O12 89.28(15) . .
K1 O13 Rh3 O9 -179.61(14) . .
K1 O13 Rh3 O10 0.62(14) . .
K1 O13 Rh3 Rh3 -44(2) . 2_676
O3 K1 Rh3 O11 12.40(13) . .
O10 K1 Rh3 O11 -91.32(19) . .
O13 K1 Rh3 O11 89.58(17) . .
O2 K1 Rh3 O11 -158.08(15) . .
Br1 K1 Rh3 O11 -57.30(13) . .
Br1 K1 Rh3 O11 77.54(11) 2_776 .
C6 K1 Rh3 O11 173.4(3) . .
Rh1 K1 Rh3 O11 -137.43(13) . .
Rh1 K1 Rh3 O11 39.40(11) 2_776 .
K1 K1 Rh3 O11 36.76(15) 2_776 .
O3 K1 Rh3 O12 -170.53(13) . .
O10 K1 Rh3 O12 85.75(19) . .
O13 K1 Rh3 O12 -93.35(17) . .
O2 K1 Rh3 O12 18.99(16) . .
Br1 K1 Rh3 O12 119.77(13) . .
Br1 K1 Rh3 O12 -105.40(12) 2_776 .
C6 K1 Rh3 O12 -9.6(3) . .
Rh1 K1 Rh3 O12 39.64(14) . .
Rh1 K1 Rh3 O12 -143.53(11) 2_776 .
K1 K1 Rh3 O12 -146.17(15) 2_776 .
O3 K1 Rh3 O9 -76.6(2) . .
O10 K1 Rh3 O9 179.7(2) . .
O13 K1 Rh3 O9 0.6(2) . .
O2 K1 Rh3 O9 112.9(2) . .
Br1 K1 Rh3 O9 -146.28(19) . .
Br1 K1 Rh3 O9 -11.44(19) 2_776 .
C6 K1 Rh3 O9 84.4(4) . .
Rh1 K1 Rh3 O9 133.59(19) . .
Rh1 K1 Rh3 O9 -49.58(18) 2_776 .
K1 K1 Rh3 O9 -52.2(2) 2_776 .
O3 K1 Rh3 O10 103.72(18) . .
O13 K1 Rh3 O10 -179.1(2) . .
O2 K1 Rh3 O10 -66.76(19) . .
Br1 K1 Rh3 O10 34.02(16) . .
Br1 K1 Rh3 O10 168.85(16) 2_776 .
C6 K1 Rh3 O10 -95.3(3) . .
Rh1 K1 Rh3 O10 -46.11(17) . .
Rh1 K1 Rh3 O10 130.72(16) 2_776 .
K1 K1 Rh3 O10 128.08(19) 2_776 .
O3 K1 Rh3 O13 -77.18(14) . .
O10 K1 Rh3 O13 179.1(2) . .
O2 K1 Rh3 O13 112.34(17) . .
Br1 K1 Rh3 O13 -146.88(15) . .
Br1 K1 Rh3 O13 -12.05(13) 2_776 .
C6 K1 Rh3 O13 83.8(3) . .
Rh1 K1 Rh3 O13 132.99(15) . .
Rh1 K1 Rh3 O13 -50.18(13) 2_776 .
K1 K1 Rh3 O13 -52.82(15) 2_776 .
O3 K1 Rh3 Rh3 100.27(8) . 2_676
O10 K1 Rh3 Rh3 -3.45(16) . 2_676
O13 K1 Rh3 Rh3 177.45(13) . 2_676
O2 K1 Rh3 Rh3 -70.21(12) . 2_676
Br1 K1 Rh3 Rh3 30.57(9) . 2_676
Br1 K1 Rh3 Rh3 165.40(4) 2_776 2_676
C6 K1 Rh3 Rh3 -98.8(3) . 2_676
Rh1 K1 Rh3 Rh3 -49.56(10) . 2_676
Rh1 K1 Rh3 Rh3 127.27(4) 2_776 2_676
K1 K1 Rh3 Rh3 124.63(9) 2_776 2_676
C28 O17 Rh4 O14 90.4(5) . .
C28 O17 Rh4 O16 -5(3) . .
C28 O17 Rh4 O15 -84.2(5) . .
C28 O17 Rh4 Rh5 2.6(4) . .
C28 O17 Rh4 Br1 178.2(4) . .
C19 O14 Rh4 O17 -88.8(4) . .
C19 O14 Rh4 O16 87.3(4) . .
C19 O14 Rh4 O15 -4(2) . .
C19 O14 Rh4 Rh5 -0.4(4) . .
C19 O14 Rh4 Br1 -179.2(4) . .
C25 O16 Rh4 O17 10(3) . .
C25 O16 Rh4 O14 -84.6(4) . .
C25 O16 Rh4 O15 89.9(4) . .
C25 O16 Rh4 Rh5 3.1(4) . .
C25 O16 Rh4 Br1 -172.4(4) . .
C22 O15 Rh4 O17 91.5(4) . .
C22 O15 Rh4 O14 7(2) . .
C22 O15 Rh4 O16 -84.6(4) . .
C22 O15 Rh4 Rh5 3.1(4) . .
C22 O15 Rh4 Br1 -178.1(4) . .
Rh1 Br1 Rh4 O17 23.71(13) . .
K1 Br1 Rh4 O17 -143.95(14) . .
K1 Br1 Rh4 O17 122.52(13) 2_776 .
Rh1 Br1 Rh4 O14 113.18(13) . .
K1 Br1 Rh4 O14 -54.48(14) . .
K1 Br1 Rh4 O14 -148.01(13) 2_776 .
Rh1 Br1 Rh4 O16 -156.10(12) . .
K1 Br1 Rh4 O16 36.24(13) . .
K1 Br1 Rh4 O16 -57.29(12) 2_776 .
Rh1 Br1 Rh4 O15 -66.35(12) . .
K1 Br1 Rh4 O15 125.99(13) . .
K1 Br1 Rh4 O15 32.46(12) 2_776 .
Rh1 Br1 Rh4 Rh5 98.2(3) . .
K1 Br1 Rh4 Rh5 -69.4(3) . .
K1 Br1 Rh4 Rh5 -162.9(3) 2_776 .
C19 O21 Rh5 O19 -85.4(4) . .
C19 O21 Rh5 O18 91.0(4) . .
C19 O21 Rh5 O20 -25(3) . .
C19 O21 Rh5 O20 -174.4(4) . 2_775
C19 O21 Rh5 Rh4 3.2(4) . .
C25 O19 Rh5 O21 92.7(5) . .
C25 O19 Rh5 O18 8(3) . .
C25 O19 Rh5 O20 -84.6(4) . .
C25 O19 Rh5 O20 -163.6(5) . 2_775
C25 O19 Rh5 Rh4 4.3(4) . .
C28 O18 Rh5 O21 -85.2(4) . .
C28 O18 Rh5 O19 -1(3) . .
C28 O18 Rh5 O20 92.0(4) . .
C28 O18 Rh5 O20 170.9(4) . 2_775
C28 O18 Rh5 Rh4 3.1(4) . .
C22 O20 Rh5 O21 33(3) . .
Rh5 O20 Rh5 O21 -150(3) 2_775 .
C22 O20 Rh5 O19 92.8(4) . .
Rh5 O20 Rh5 O19 -89.37(16) 2_775 .
C22 O20 Rh5 O18 -83.5(4) . .
Rh5 O20 Rh5 O18 94.31(16) 2_775 .
C22 O20 Rh5 O20 -177.8(5) . 2_775
Rh5 O20 Rh5 O20 0.0 2_775 2_775
C22 O20 Rh5 Rh4 4.2(4) . .
Rh5 O20 Rh5 Rh4 -177.98(13) 2_775 .
O17 Rh4 Rh5 O21 88.33(18) . .
O14 Rh4 Rh5 O21 -1.22(17) . .
O16 Rh4 Rh5 O21 -92.16(17) . .
O15 Rh4 Rh5 O21 178.43(17) . .
Br1 Rh4 Rh5 O21 13.7(4) . .
O17 Rh4 Rh5 O19 177.32(17) . .
O14 Rh4 Rh5 O19 87.78(18) . .
O16 Rh4 Rh5 O19 -3.17(17) . .
O15 Rh4 Rh5 O19 -92.58(17) . .
Br1 Rh4 Rh5 O19 102.7(4) . .
O17 Rh4 Rh5 O18 -2.41(17) . .
O14 Rh4 Rh5 O18 -91.96(17) . .
O16 Rh4 Rh5 O18 177.09(16) . .
O15 Rh4 Rh5 O18 87.69(17) . .
Br1 Rh4 Rh5 O18 -77.0(4) . .
O17 Rh4 Rh5 O20 -93.14(17) . .
O14 Rh4 Rh5 O20 177.31(17) . .
O16 Rh4 Rh5 O20 86.36(17) . .
O15 Rh4 Rh5 O20 -3.04(16) . .
Br1 Rh4 Rh5 O20 -167.8(3) . .
O17 Rh4 Rh5 O20 -102.5(5) . 2_775
O14 Rh4 Rh5 O20 168.0(5) . 2_775
O16 Rh4 Rh5 O20 77.0(5) . 2_775
O15 Rh4 Rh5 O20 -12.4(5) . 2_775
Br1 Rh4 Rh5 O20 -177.1(5) . 2_775
C34 O25 Rh6 O22 89.5(5) 2_667 .
C34 O25 Rh6 O23 -4(3) 2_667 .
C34 O25 Rh6 O24 -86.8(5) 2_667 2_667
C34 O25 Rh6 O26 178.3(5) 2_667 .
C34 O25 Rh6 Rh6 0.7(5) 2_667 2_667
C31 O22 Rh6 O25 -90.0(5) . .
C31 O22 Rh6 O23 86.1(5) . .
C31 O22 Rh6 O24 -10(3) . 2_667
C31 O22 Rh6 O26 -179.6(5) . .
C31 O22 Rh6 Rh6 -1.8(5) . 2_667
C34 O23 Rh6 O25 7(3) . .
C34 O23 Rh6 O22 -87.2(5) . .
C34 O23 Rh6 O24 89.0(5) . 2_667
C34 O23 Rh6 O26 -176.0(5) . .
C34 O23 Rh6 Rh6 1.6(5) . 2_667
