#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:15:55 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179621 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/85/4508568.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4508568
loop_
_publ_author_name
'Xu, Wentao'
'Zhou, Youfu'
'Huang, Decai'
'Xiong, Wei'
'Su, Mingyi'
'Wang, Kun'
'Han, Shuo'
'Hong, Maochun'
_publ_section_title
;
 Crystal Structure, Multiplex Photoluminescence, and Magnetic Properties
 of a Series of Lanthanide Coordination Polymers Based on Quinoline
 Carboxylate Ligand
;
_journal_issue                   12
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              5420
_journal_paper_doi               10.1021/cg401391b
_journal_volume                  13
_journal_year                    2013
_chemical_formula_moiety         'C32 H21 Dy1 N4 O10'
_chemical_formula_sum            'C32 H21 Dy N4 O10'
_chemical_formula_weight         784.03
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 94.575(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.029(3)
_cell_length_b                   16.490(4)
_cell_length_c                   17.307(4)
_cell_measurement_reflns_used    7480
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4816
_cell_measurement_theta_min      2.5854
_cell_volume                     2853.1(13)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku, 2000)'
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Saturn 70 CCD diffractometer'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0448
_diffrn_reflns_av_sigmaI/netI    0.0405
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            25129
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.04
_exptl_absorpt_coefficient_mu    2.690
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.8357
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(CrystalClear; Rigaku, 2000)'
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.825
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1548
_exptl_crystal_size_max          0.2500
_exptl_crystal_size_mid          0.1500
_exptl_crystal_size_min          0.1000
_refine_diff_density_max         1.170
_refine_diff_density_min         -0.776
_refine_diff_density_rms         0.093
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.235
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     428
_refine_ls_number_reflns         6520
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.235
_refine_ls_R_factor_all          0.0559
_refine_ls_R_factor_gt           0.0503
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0104P)²+4.7641P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0741
_refine_ls_wR_factor_ref         0.0760
_reflns_number_gt                6112
_reflns_number_total             6520
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg401391b_si_002.cif
_cod_data_source_block           5-Dy
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P21/C
_cod_database_code               4508568
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.75417(2) 0.020958(12) -0.011983(12) 0.03322(7) Uani 1 1 d .
O1 O 0.8904(3) 0.13322(18) 0.00134(18) 0.0400(8) Uani 1 1 d .
O2 O 1.0885(3) 0.07504(18) 0.0162(2) 0.0513(9) Uani 1 1 d .
O3 O 0.6070(3) -0.07672(18) 0.01820(19) 0.0444(8) Uani 1 1 d .
O4 O 0.4087(3) -0.11060(19) 0.05766(19) 0.0445(8) Uani 1 1 d .
O9 O 0.6608(4) 0.0829(2) 0.1008(2) 0.0564(10) Uani 1 1 d .
O8 O 0.8238(4) -0.0018(2) 0.1242(2) 0.0576(10) Uani 1 1 d .
O10 O 0.7158(5) 0.0443(3) 0.2194(2) 0.0910(16) Uani 1 1 d .
O6 O 0.8303(3) 0.0504(2) -0.14165(19) 0.0489(9) Uani 1 1 d .
O5 O 0.6865(4) -0.0450(2) -0.1386(2) 0.0556(9) Uani 1 1 d .
O7 O 0.7779(4) -0.0185(2) -0.2462(2) 0.0687(11) Uani 1 1 d .
N1 N 1.2168(4) 0.3674(2) 0.0363(2) 0.0414(9) Uani 1 1 d .
N2 N 0.6986(4) -0.3242(2) 0.1743(2) 0.0436(10) Uani 1 1 d .
N3 N 0.7316(5) 0.0422(3) 0.1507(3) 0.0575(12) Uani 1 1 d .
N4 N 0.7659(4) -0.0046(2) -0.1773(3) 0.0483(10) Uani 1 1 d .
C1 C 1.0153(4) 0.1362(3) 0.0087(3) 0.0338(10) Uani 1 1 d .
C2 C 1.0832(4) 0.2181(2) 0.0123(2) 0.0317(9) Uani 1 1 d .
C3 C 1.0348(4) 0.2873(3) -0.0298(2) 0.0351(10) Uani 1 1 d .
C4 C 0.9218(5) 0.2881(3) -0.0845(3) 0.0433(11) Uani 1 1 d .
H4 H 0.8707 0.2401 -0.0937 0.052 Uiso 1 1 calc R
C5 C 0.8863(5) 0.3569(3) -0.1239(3) 0.0539(14) Uani 1 1 d .
H5 H 0.8110 0.3563 -0.1609 0.065 Uiso 1 1 calc R
C6 C 0.9587(6) 0.4283(3) -0.1109(3) 0.0622(16) Uani 1 1 d .
H6 H 0.9316 0.4761 -0.1385 0.075 Uiso 1 1 calc R
C7 C 1.0675(6) 0.4301(3) -0.0593(3) 0.0550(14) Uani 1 1 d .
H7 H 1.1172 0.4789 -0.0518 0.066 Uiso 1 1 calc R
C8 C 1.1078(5) 0.3603(3) -0.0165(3) 0.0395(11) Uani 1 1 d .
C9 C 1.1947(4) 0.2256(3) 0.0625(2) 0.0336(10) Uani 1 1 d .
H9 H 1.2301 0.1791 0.0893 0.040 Uiso 1 1 calc R
C10 C 1.2581(4) 0.3014(3) 0.0750(3) 0.0350(10) Uani 1 1 d .
C11 C 1.3715(4) 0.3094(3) 0.1346(3) 0.0370(10) Uani 1 1 d .
C12 C 1.4559(5) 0.2448(3) 0.1546(3) 0.0438(12) Uani 1 1 d .
H12 H 1.4414 0.1941 0.1291 0.053 Uiso 1 1 calc R
C13 C 1.5599(5) 0.2528(3) 0.2108(3) 0.0507(13) Uani 1 1 d .
H13 H 1.6164 0.2078 0.2239 0.061 Uiso 1 1 calc R
C14 C 1.5828(5) 0.3260(4) 0.2481(3) 0.0561(14) Uani 1 1 d .
H14 H 1.6559 0.3319 0.2860 0.067 Uiso 1 1 calc R
C15 C 1.4994(5) 0.3899(3) 0.2300(3) 0.0528(14) Uani 1 1 d .
H15 H 1.5138 0.4400 0.2566 0.063 Uiso 1 1 calc R
C16 C 1.3946(5) 0.3828(3) 0.1737(3) 0.0456(12) Uani 1 1 d .
H16 H 1.3379 0.4280 0.1615 0.055 Uiso 1 1 calc R
C17 C 0.5297(5) -0.1222(3) 0.0512(3) 0.0349(10) Uani 1 1 d .
C18 C 0.5900(4) -0.1980(2) 0.0895(2) 0.0333(10) Uani 1 1 d .
C19 C 0.5310(4) -0.2754(3) 0.0785(3) 0.0356(10) Uani 1 1 d .
C20 C 0.4208(5) -0.2935(3) 0.0252(3) 0.0452(12) Uani 1 1 d .
H20 H 0.3778 -0.2515 -0.0050 0.054 Uiso 1 1 calc R
C21 C 0.3765(6) -0.3715(3) 0.0172(3) 0.0559(14) Uani 1 1 d .
H21 H 0.3043 -0.3836 -0.0199 0.067 Uiso 1 1 calc R
C22 C 0.4347(6) -0.4333(3) 0.0621(3) 0.0597(15) Uani 1 1 d .
H22 H 0.4004 -0.4869 0.0561 0.072 Uiso 1 1 calc R
C23 C 0.5394(6) -0.4190(3) 0.1143(3) 0.0558(14) Uani 1 1 d .
H23 H 0.5781 -0.4620 0.1450 0.067 Uiso 1 1 calc R
C24 C 0.5901(5) -0.3402(3) 0.1226(3) 0.0407(11) Uani 1 1 d .
C25 C 0.7038(4) -0.1884(3) 0.1380(3) 0.0368(10) Uani 1 1 d .
H25 H 0.7465 -0.1370 0.1412 0.044 Uiso 1 1 calc R
C26 C 0.7584(4) -0.2523(3) 0.1827(3) 0.0374(10) Uani 1 1 d .
C27 C 0.8790(5) -0.2420(3) 0.2374(3) 0.0416(11) Uani 1 1 d .
C28 C 0.9465(5) -0.3084(3) 0.2692(3) 0.0548(14) Uani 1 1 d .
H28 H 0.9153 -0.3615 0.2566 0.066 Uiso 1 1 calc R
C29 C 1.0590(6) -0.2978(4) 0.3190(3) 0.0671(18) Uani 1 1 d .
H29 H 1.1038 -0.3438 0.3416 0.080 Uiso 1 1 calc R
C30 C 1.1070(5) -0.2219(5) 0.3363(3) 0.0670(18) Uani 1 1 d .
H30 H 1.1852 -0.2153 0.3704 0.080 Uiso 1 1 calc R
C31 C 1.0417(6) -0.1546(4) 0.3041(4) 0.0729(18) Uani 1 1 d .
H31 H 1.0747 -0.1017 0.3158 0.088 Uiso 1 1 calc R
C32 C 0.9274(5) -0.1653(3) 0.2544(3) 0.0571(15) Uani 1 1 d .
H32 H 0.8821 -0.1193 0.2320 0.069 Uiso 1 1 calc R
HN2 H 0.726(5) -0.368(3) 0.202(3) 0.073(19) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Dy1 O3 88.78(12) 3_755 .
O2 Dy1 O4 157.98(13) 3_755 3_655
O3 Dy1 O4 94.48(11) . 3_655
O2 Dy1 O1 99.07(11) 3_755 .
O3 Dy1 O1 159.71(12) . .
O4 Dy1 O1 85.24(11) 3_655 .
O2 Dy1 O8 76.97(14) 3_755 .
O3 Dy1 O8 79.02(12) . .
O4 Dy1 O8 125.04(13) 3_655 .
O1 Dy1 O8 84.54(11) . .
O2 Dy1 O9 129.38(13) 3_755 .
O3 Dy1 O9 79.40(12) . .
O4 Dy1 O9 72.55(12) 3_655 .
O1 Dy1 O9 81.19(12) . .
O8 Dy1 O9 52.54(13) . .
O2 Dy1 O6 80.80(13) 3_755 .
O3 Dy1 O6 126.88(11) . .
O4 Dy1 O6 79.85(12) 3_655 .
O1 Dy1 O6 73.11(11) . .
O8 Dy1 O6 145.39(12) . .
O9 Dy1 O6 143.55(12) . .
O2 Dy1 O5 78.81(12) 3_755 .
O3 Dy1 O5 75.92(12) . .
O4 Dy1 O5 80.89(12) 3_655 .
O1 Dy1 O5 123.84(12) . .
O8 Dy1 O5 145.25(12) . .
O9 Dy1 O5 141.89(12) . .
O6 Dy1 O5 50.97(11) . .
O2 Dy1 N3 103.30(15) 3_755 .
O3 Dy1 N3 75.95(12) . .
O4 Dy1 N3 98.61(14) 3_655 .
O1 Dy1 N3 84.02(12) . .
O8 Dy1 N3 26.59(13) . .
O9 Dy1 N3 26.08(13) . .
O6 Dy1 N3 157.13(11) . .
O5 Dy1 N3 151.73(12) . .
O2 Dy1 N4 77.35(12) 3_755 .
O3 Dy1 N4 101.63(12) . .
O4 Dy1 N4 80.66(12) 3_655 .
O1 Dy1 N4 98.34(12) . .
O8 Dy1 N4 154.29(13) . .
O9 Dy1 N4 153.17(12) . .
O6 Dy1 N4 25.25(10) . .
O5 Dy1 N4 25.78(11) . .
N3 Dy1 N4 177.44(12) . .
C1 O1 Dy1 128.6(3) . .
C1 O2 Dy1 167.8(3) . 3_755
C17 O3 Dy1 165.6(3) . .
C17 O4 Dy1 137.9(3) . 3_655
N3 O9 Dy1 95.4(3) . .
N3 O8 Dy1 95.7(3) . .
N4 O6 Dy1 96.9(3) . .
N4 O5 Dy1 95.5(3) . .
C10 N1 C8 117.9(4) . .
C26 N2 C24 124.6(4) . .
C26 N2 HN2 123(4) . .
C24 N2 HN2 113(4) . .
O10 N3 O9 123.0(6) . .
O10 N3 O8 121.3(5) . .
O9 N3 O8 115.7(4) . .
O10 N3 Dy1 173.9(4) . .
O9 N3 Dy1 58.5(2) . .
O8 N3 Dy1 57.7(2) . .
O7 N4 O6 121.9(5) . .
O7 N4 O5 121.8(4) . .
O6 N4 O5 116.3(4) . .
O7 N4 Dy1 175.9(4) . .
O6 N4 Dy1 57.8(2) . .
O5 N4 Dy1 58.7(2) . .
O2 C1 O1 123.7(4) . .
O2 C1 C2 117.3(4) . .
O1 C1 C2 118.9(4) . .
C9 C2 C3 118.9(4) . .
C9 C2 C1 116.7(4) . .
C3 C2 C1 124.3(4) . .
C4 C3 C8 118.5(4) . .
C4 C3 C2 124.9(4) . .
C8 C3 C2 116.6(4) . .
C5 C4 C3 120.4(5) . .
C5 C4 H4 119.8 . .
C3 C4 H4 119.8 . .
C4 C5 C6 120.9(5) . .
C4 C5 H5 119.6 . .
C6 C5 H5 119.6 . .
C7 C6 C5 120.5(5) . .
C7 C6 H6 119.7 . .
C5 C6 H6 119.7 . .
C6 C7 C8 120.7(5) . .
C6 C7 H7 119.6 . .
C8 C7 H7 119.6 . .
N1 C8 C7 117.4(4) . .
N1 C8 C3 123.6(4) . .
C7 C8 C3 118.9(4) . .
C2 C9 C10 120.8(4) . .
C2 C9 H9 119.6 . .
C10 C9 H9 119.6 . .
N1 C10 C9 122.0(4) . .
N1 C10 C11 118.1(4) . .
C9 C10 C11 119.8(4) . .
C12 C11 C16 118.1(4) . .
C12 C11 C10 121.7(4) . .
C16 C11 C10 120.2(4) . .
C13 C12 C11 121.1(5) . .
C13 C12 H12 119.5 . .
C11 C12 H12 119.5 . .
C12 C13 C14 120.2(5) . .
C12 C13 H13 119.9 . .
C14 C13 H13 119.9 . .
C15 C14 C13 119.5(5) . .
C15 C14 H14 120.2 . .
C13 C14 H14 120.2 . .
C14 C15 C16 120.9(5) . .
C14 C15 H15 119.5 . .
C16 C15 H15 119.5 . .
C15 C16 C11 120.2(5) . .
C15 C16 H16 119.9 . .
C11 C16 H16 119.9 . .
O4 C17 O3 126.5(4) . .
O4 C17 C18 116.5(4) . .
O3 C17 C18 117.0(4) . .
C25 C18 C19 120.4(4) . .
C25 C18 C17 117.2(4) . .
C19 C18 C17 122.4(4) . .
C20 C19 C18 125.2(4) . .
C20 C19 C24 117.7(4) . .
C18 C19 C24 117.1(4) . .
C21 C20 C19 119.8(5) . .
C21 C20 H20 120.1 . .
C19 C20 H20 120.1 . .
C20 C21 C22 121.2(5) . .
C20 C21 H21 119.4 . .
C22 C21 H21 119.4 . .
C23 C22 C21 121.2(5) . .
C23 C22 H22 119.4 . .
C21 C22 H22 119.4 . .
C22 C23 C24 119.2(5) . .
C22 C23 H23 120.4 . .
C24 C23 H23 120.4 . .
N2 C24 C23 120.5(4) . .
N2 C24 C19 118.7(4) . .
C23 C24 C19 120.8(5) . .
C18 C25 C26 121.6(4) . .
C18 C25 H25 119.2 . .
C26 C25 H25 119.2 . .
N2 C26 C25 117.4(4) . .
N2 C26 C27 120.5(4) . .
C25 C26 C27 122.1(4) . .
C28 C27 C32 119.4(5) . .
C28 C27 C26 120.9(5) . .
C32 C27 C26 119.7(4) . .
C29 C28 C27 120.1(6) . .
C29 C28 H28 119.9 . .
C27 C28 H28 119.9 . .
C30 C29 C28 120.7(5) . .
C30 C29 H29 119.7 . .
C28 C29 H29 119.7 . .
C29 C30 C31 120.0(5) . .
C29 C30 H30 120.0 . .
C31 C30 H30 120.0 . .
C30 C31 C32 119.3(6) . .
C30 C31 H31 120.3 . .
C32 C31 H31 120.3 . .
C27 C32 C31 120.5(5) . .
C27 C32 H32 119.8 . .
C31 C32 H32 119.8 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O2 2.240(3) 3_755
Dy1 O3 2.274(3) .
Dy1 O4 2.296(3) 3_655
Dy1 O1 2.301(3) .
Dy1 O8 2.433(4) .
Dy1 O9 2.454(4) .
Dy1 O6 2.475(3) .
Dy1 O5 2.492(4) .
Dy1 N3 2.864(5) .
Dy1 N4 2.903(5) .
O1 C1 1.249(5) .
O2 C1 1.249(5) .
O2 Dy1 2.240(3) 3_755
O3 C17 1.249(5) .
O4 C17 1.242(5) .
O4 Dy1 2.296(3) 3_655
O9 N3 1.265(5) .
O8 N3 1.289(6) .
O10 N3 1.212(6) .
O6 N4 1.248(5) .
O5 N4 1.269(5) .
O7 N4 1.231(5) .
N1 C10 1.326(6) .
N1 C8 1.372(6) .
N2 C26 1.331(6) .
N2 C24 1.378(6) .
N2 HN2 0.89(6) .
C1 C2 1.512(6) .
C2 C9 1.366(6) .
C2 C3 1.419(6) .
C3 C4 1.417(6) .
C3 C8 1.418(6) .
C4 C5 1.357(7) .
C4 H4 0.9500 .
C5 C6 1.392(8) .
C5 H5 0.9500 .
C6 C7 1.355(7) .
C6 H6 0.9500 .
C7 C8 1.410(6) .
C7 H7 0.9500 .
C9 C10 1.412(6) .
C9 H9 0.9500 .
C10 C11 1.480(6) .
C11 C12 1.388(6) .
C11 C16 1.397(6) .
C12 C13 1.374(6) .
C12 H12 0.9500 .
C13 C14 1.379(7) .
C13 H13 0.9500 .
C14 C15 1.367(7) .
C14 H14 0.9500 .
C15 C16 1.381(7) .
C15 H15 0.9500 .
C16 H16 0.9500 .
C17 C18 1.517(6) .
C18 C25 1.371(6) .
C18 C19 1.414(6) .
C19 C20 1.414(6) .
C19 C24 1.416(6) .
C20 C21 1.363(7) .
C20 H20 0.9500 .
C21 C22 1.383(7) .
C21 H21 0.9500 .
C22 C23 1.350(7) .
C22 H22 0.9500 .
C23 C24 1.398(6) .
C23 H23 0.9500 .
C25 C26 1.393(6) .
C25 H25 0.9500 .
C26 C27 1.485(6) .
C27 C28 1.377(6) .
C27 C32 1.379(7) .
C28 C29 1.376(8) .
C28 H28 0.9500 .
C29 C30 1.366(9) .
C29 H29 0.9500 .
C30 C31 1.382(8) .
C30 H30 0.9500 .
C31 C32 1.388(7) .
C31 H31 0.9500 .
C32 H32 0.9500 .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
N2 HN2 O7 0.89(6) 2.13(6) 3.012(5) 171(5) 4_556
