#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/97/4509758.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4509758
loop_
_publ_author_name
'Wang, Hailong'
'Zhang, Daopeng'
'Sun, Daofeng'
'Chen, Yuting'
'Zhang, Li-Fang'
'Tian, Laijin'
'Jiang, Jianzhuang'
'Ni, Zhong-Hai'
_publ_section_title
;
 Co(II) Metal−Organic Frameworks (MOFs) Assembled from Asymmetric
 Semirigid Multicarboxylate Ligands: Synthesis, Crystal Structures, and
 Magnetic Properties
;
_journal_issue                   12
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              5273
_journal_paper_doi               10.1021/cg900788h
_journal_volume                  9
_journal_year                    2009
_chemical_formula_moiety         'C25 H22 Co N2 O10, 2(C5 H4 N),2(H2 O) '
_chemical_formula_sum            'C35 H34 Co N4 O12'
_chemical_formula_weight         761.59
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                110.2710(10)
_cell_angle_beta                 94.099(2)
_cell_angle_gamma                94.9960(10)
_cell_formula_units_Z            2
_cell_length_a                   10.7673(10)
_cell_length_b                   11.7146(11)
_cell_length_c                   14.4532(13)
_cell_measurement_reflns_used    4216
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      27.40
_cell_measurement_theta_min      2.30
_cell_volume                     1693.5(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      298(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Bruker APEX CCD area-detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0140
_diffrn_reflns_av_sigmaI/netI    0.0312
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            8439
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.51
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.579
_exptl_absorpt_correction_T_max  0.944
_exptl_absorpt_correction_T_min  0.895
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2003)'
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.494
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             790
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.08
_refine_diff_density_max         0.297
_refine_diff_density_min         -0.217
_refine_diff_density_rms         0.049
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.094
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     469
_refine_ls_number_reflns         5875
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.150
_refine_ls_R_factor_all          0.0400
_refine_ls_R_factor_gt           0.0327
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0635P)²+0.0083P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0970
_refine_ls_wR_factor_ref         0.1015
_reflns_number_gt                5063
_reflns_number_total             5875
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg900788hsup1.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_Hall     -P1
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4509758
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.2174(2) 0.3832(2) 0.09128(16) 0.0394(5) Uani 1 1 d .
C2 C 0.21566(19) 0.3222(2) 0.16797(15) 0.0353(5) Uani 1 1 d .
C3 C 0.3021(2) 0.2416(2) 0.16786(17) 0.0454(6) Uani 1 1 d .
H3 H 0.3580 0.2252 0.1201 0.055 Uiso 1 1 calc R
C4 C 0.3072(2) 0.1849(2) 0.2370(2) 0.0548(6) Uani 1 1 d .
H4 H 0.3641 0.1289 0.2346 0.066 Uiso 1 1 calc R
C5 C 0.2273(2) 0.2121(2) 0.30931(19) 0.0512(6) Uani 1 1 d .
H5 H 0.2306 0.1759 0.3573 0.061 Uiso 1 1 calc R
C6 C 0.14256(19) 0.2931(2) 0.31036(15) 0.0381(5) Uani 1 1 d .
C7 C 0.13189(18) 0.34833(19) 0.24009(14) 0.0321(4) Uani 1 1 d .
C8 C 0.03739(19) 0.43907(19) 0.25004(14) 0.0319(4) Uani 1 1 d .
C9 C -0.0389(2) 0.2649(2) 0.38914(16) 0.0373(5) Uani 1 1 d .
C10 C -0.1059(2) 0.3147(2) 0.46849(17) 0.0484(6) Uani 1 1 d .
H10 H -0.0727 0.3863 0.5203 0.058 Uiso 1 1 calc R
C11 C -0.2227(2) 0.2571(2) 0.47006(19) 0.0510(6) Uani 1 1 d .
H11 H -0.2686 0.2902 0.5232 0.061 Uiso 1 1 calc R
C12 C -0.2720(2) 0.1507(2) 0.39345(17) 0.0410(5) Uani 1 1 d .
C13 C -0.2003(2) 0.0994(2) 0.31780(17) 0.0436(5) Uani 1 1 d .
H13 H -0.2312 0.0254 0.2679 0.052 Uiso 1 1 calc R
C14 C -0.0835(2) 0.1555(2) 0.31463(17) 0.0430(5) Uani 1 1 d .
H14 H -0.0358 0.1202 0.2632 0.052 Uiso 1 1 calc R
C15 C -0.4015(2) 0.0924(2) 0.3899(2) 0.0474(6) Uani 1 1 d .
C16 C -0.2710(2) 0.5192(2) 0.38808(16) 0.0424(5) Uani 1 1 d .
H16 H -0.1839 0.5322 0.3975 0.051 Uiso 1 1 calc R
C17 C -0.3344(2) 0.5192(2) 0.46770(16) 0.0428(5) Uani 1 1 d .
H17 H -0.2896 0.5309 0.5284 0.051 Uiso 1 1 calc R
C18 C -0.46399(18) 0.50189(18) 0.45787(14) 0.0325(4) Uani 1 1 d .
C19 C -0.5221(2) 0.4873(2) 0.36543(16) 0.0452(6) Uani 1 1 d .
H19 H -0.6092 0.4775 0.3547 0.054 Uiso 1 1 calc R
C20 C -0.4528(2) 0.4872(2) 0.28925(16) 0.0420(5) Uani 1 1 d .
H20 H -0.4953 0.4764 0.2280 0.050 Uiso 1 1 calc R
C21 C -0.3353(2) 0.2208(2) 0.15345(16) 0.0404(5) Uani 1 1 d .
H21 H -0.2924 0.2464 0.2167 0.048 Uiso 1 1 calc R
C22 C -0.4006(2) 0.10527(19) 0.11621(16) 0.0390(5) Uani 1 1 d .
H22 H -0.4025 0.0560 0.1547 0.047 Uiso 1 1 calc R
C23 C -0.46373(17) 0.06214(18) 0.02144(15) 0.0316(4) Uani 1 1 d .
C24 C -0.4568(2) 0.1427(2) -0.02995(17) 0.0446(5) Uani 1 1 d .
H24 H -0.4968 0.1188 -0.0941 0.054 Uiso 1 1 calc R
C25 C -0.3911(2) 0.2576(2) 0.01335(17) 0.0437(5) Uani 1 1 d .
H25 H -0.3894 0.3099 -0.0226 0.052 Uiso 1 1 calc R
C26 C -0.1422(3) -0.1446(3) 0.1089(2) 0.0708(8) Uani 1 1 d .
H26 H -0.2228 -0.1648 0.1220 0.085 Uiso 1 1 calc R
C27 C -0.1280(3) -0.0701(2) 0.0527(2) 0.0605(7) Uani 1 1 d .
H27 H -0.1975 -0.0412 0.0303 0.073 Uiso 1 1 calc R
C28 C -0.0100(2) -0.0391(2) 0.03030(18) 0.0507(6) Uani 1 1 d .
C29 C 0.0867(3) -0.0861(3) 0.0670(3) 0.0839(10) Uani 1 1 d .
H29 H 0.1681 -0.0695 0.0536 0.101 Uiso 1 1 calc R
C30 C 0.0636(4) -0.1582(3) 0.1239(3) 0.0906(11) Uani 1 1 d .
H30 H 0.1315 -0.1868 0.1488 0.109 Uiso 1 1 calc R
C31 C 0.2652(2) 0.1360(2) 0.5464(2) 0.0558(7) Uani 1 1 d .
H31 H 0.3138 0.2047 0.5918 0.067 Uiso 1 1 calc R
C32 C 0.1416(2) 0.1153(2) 0.55984(19) 0.0529(6) Uani 1 1 d .
H32 H 0.1082 0.1694 0.6131 0.063 Uiso 1 1 calc R
C33 C 0.0668(2) 0.0134(2) 0.49372(16) 0.0394(5) Uani 1 1 d .
C34 C 0.1230(2) -0.0624(2) 0.41567(19) 0.0518(6) Uani 1 1 d .
H34 H 0.0770 -0.1319 0.3689 0.062 Uiso 1 1 calc R
C35 C 0.2481(2) -0.0334(3) 0.4082(2) 0.0581(7) Uani 1 1 d .
H35 H 0.2847 -0.0847 0.3554 0.070 Uiso 1 1 calc R
N1 N -0.32987(15) 0.29785(16) 0.10419(13) 0.0348(4) Uani 1 1 d .
N2 N -0.32771(15) 0.50164(15) 0.29854(12) 0.0332(4) Uani 1 1 d .
N3 N -0.0497(3) -0.1886(2) 0.14487(19) 0.0739(7) Uani 1 1 d .
N4 N 0.31850(18) 0.0637(2) 0.47255(17) 0.0513(5) Uani 1 1 d .
O1 O 0.31716(17) 0.3896(2) 0.05437(15) 0.0702(6) Uani 1 1 d .
O2 O 0.12057(15) 0.42443(17) 0.07134(13) 0.0540(5) Uani 1 1 d .
O3 O 0.07927(15) 0.55000(14) 0.28947(13) 0.0527(4) Uani 1 1 d .
O4 O -0.07499(12) 0.39703(13) 0.22174(11) 0.0356(3) Uani 1 1 d .
O5 O 0.07250(14) 0.33241(15) 0.39142(10) 0.0444(4) Uani 1 1 d .
O6 O -0.45119(17) 0.00458(18) 0.31943(15) 0.0629(5) Uani 1 1 d .
O7 O -0.45508(16) 0.14630(19) 0.46884(15) 0.0689(5) Uani 1 1 d D
H7A H -0.5291 0.1083 0.4634 0.103 Uiso 1 1 d RD
O8 O -0.11375(15) 0.64893(13) 0.24243(12) 0.0446(4) Uani 1 1 d D
H8B H -0.0956 0.6874 0.2011 0.067 Uiso 1 1 d RD
H8A H -0.0376 0.6305 0.2684 0.067 Uiso 1 1 d RD
O9 O -0.13426(13) 0.43848(14) 0.04101(11) 0.0404(4) Uani 1 1 d D
H9A H -0.0509 0.4194 0.0505 0.061 Uiso 1 1 d RD
H9B H -0.1281 0.4888 0.0076 0.061 Uiso 1 1 d RD
O10 O -0.35301(14) 0.56096(15) 0.10879(12) 0.0470(4) Uani 1 1 d D
H10A H -0.4027 0.6247 0.1458 0.070 Uiso 1 1 d RD
H10B H -0.3384 0.5721 0.0582 0.070 Uiso 1 1 d RD
O11 O 0.4806(2) 0.2552(2) 0.77318(17) 0.0814(6) Uani 1 1 d D
H11B H 0.5597 0.2749 0.7675 0.122 Uiso 1 1 d RD
H11A H 0.4605 0.1797 0.7474 0.122 Uiso 1 1 d RD
O12 O 0.7389(2) 0.3241(2) 0.7804(2) 0.1108(9) Uani 1 1 d D
H12A H 0.7498 0.3572 0.7379 0.166 Uiso 1 1 d RD
H12B H 0.7542 0.3767 0.8380 0.166 Uiso 1 1 d RD
Co1 Co -0.22362(2) 0.47810(2) 0.171235(18) 0.02765(11) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O1 C1 O2 125.2(2) .
O1 C1 C2 116.77(19) .
O2 C1 C2 118.02(18) .
C3 C2 C7 119.7(2) .
C3 C2 C1 118.58(19) .
C7 C2 C1 121.70(19) .
C4 C3 C2 121.5(2) .
C4 C3 H3 119.3 .
C2 C3 H3 119.3 .
C5 C4 C3 119.2(2) .
C5 C4 H4 120.4 .
C3 C4 H4 120.4 .
C6 C5 C4 119.4(2) .
C6 C5 H5 120.3 .
C4 C5 H5 120.3 .
C5 C6 C7 122.9(2) .
C5 C6 O5 119.0(2) .
C7 C6 O5 117.79(19) .
C6 C7 C2 117.25(19) .
C6 C7 C8 118.39(18) .
C2 C7 C8 124.22(18) .
O4 C8 O3 126.02(19) .
O4 C8 C7 117.59(18) .
O3 C8 C7 116.34(18) .
O5 C9 C14 124.0(2) .
O5 C9 C10 114.86(19) .
C14 C9 C10 121.1(2) .
C9 C10 C11 119.2(2) .
C9 C10 H10 120.4 .
C11 C10 H10 120.4 .
C12 C11 C10 120.6(2) .
C12 C11 H11 119.7 .
C10 C11 H11 119.7 .
C13 C12 C11 119.0(2) .
C13 C12 C15 119.6(2) .
C11 C12 C15 121.4(2) .
C14 C13 C12 121.3(2) .
C14 C13 H13 119.3 .
C12 C13 H13 119.3 .
C9 C14 C13 118.6(2) .
C9 C14 H14 120.7 .
C13 C14 H14 120.7 .
O6 C15 O7 124.4(2) .
O6 C15 C12 122.8(2) .
O7 C15 C12 112.8(2) .
N2 C16 C17 123.63(19) .
N2 C16 H16 118.2 .
C17 C16 H16 118.2 .
C16 C17 C18 120.4(2) .
C16 C17 H17 119.8 .
C18 C17 H17 119.8 .
C17 C18 C19 115.57(19) .
C17 C18 C18 121.9(2) 2_466
C19 C18 C18 122.5(2) 2_466
C20 C19 C18 120.76(19) .
C20 C19 H19 119.6 .
C18 C19 H19 119.6 .
N2 C20 C19 123.5(2) .
N2 C20 H20 118.3 .
C19 C20 H20 118.3 .
N1 C21 C22 123.8(2) .
N1 C21 H21 118.1 .
C22 C21 H21 118.1 .
C21 C22 C23 120.13(19) .
C21 C22 H22 119.9 .
C23 C22 H22 119.9 .
C22 C23 C24 115.80(19) .
C22 C23 C23 121.8(2) 2_455
C24 C23 C23 122.4(2) 2_455
C25 C24 C23 120.4(2) .
C25 C24 H24 119.8 .
C23 C24 H24 119.8 .
N1 C25 C24 123.3(2) .
N1 C25 H25 118.4 .
C24 C25 H25 118.4 .
N3 C26 C27 124.7(3) .
N3 C26 H26 117.7 .
C27 C26 H26 117.7 .
C28 C27 C26 119.6(3) .
C28 C27 H27 120.2 .
C26 C27 H27 120.2 .
C29 C28 C27 115.8(3) .
C29 C28 C28 122.5(3) 2
C27 C28 C28 121.7(3) 2
C28 C29 C30 120.5(3) .
C28 C29 H29 119.8 .
C30 C29 H29 119.8 .
N3 C30 C29 123.8(3) .
N3 C30 H30 118.1 .
C29 C30 H30 118.1 .
N4 C31 C32 123.5(2) .
N4 C31 H31 118.3 .
C32 C31 H31 118.3 .
C31 C32 C33 119.7(2) .
C31 C32 H32 120.2 .
C33 C32 H32 120.2 .
C32 C33 C34 116.8(2) .
C32 C33 C33 121.4(3) 2_556
C34 C33 C33 121.7(3) 2_556
C35 C34 C33 119.2(2) .
C35 C34 H34 120.4 .
C33 C34 H34 120.4 .
N4 C35 C34 123.2(2) .
N4 C35 H35 118.4 .
C34 C35 H35 118.4 .
C21 N1 C25 116.54(18) .
C21 N1 Co1 120.27(14) .
C25 N1 Co1 123.18(14) .
C16 N2 C20 116.12(17) .
C16 N2 Co1 121.93(13) .
C20 N2 Co1 121.63(14) .
C26 N3 C30 115.7(3) .
C31 N4 C35 117.7(2) .
C8 O4 Co1 129.49(13) .
C9 O5 C6 118.73(16) .
C15 O7 H7A 109.0 .
Co1 O8 H8B 112.9 .
Co1 O8 H8A 105.3 .
H8B O8 H8A 108.2 .
Co1 O9 H9A 112.0 .
Co1 O9 H9B 122.7 .
H9A O9 H9B 105.0 .
Co1 O10 H10A 125.7 .
Co1 O10 H10B 118.0 .
H10A O10 H10B 108.4 .
H11B O11 H11A 110.9 .
H12A O12 H12B 110.4 .
O10 Co1 O9 88.27(6) .
O10 Co1 O8 90.43(6) .
O9 Co1 O8 93.73(6) .
O10 Co1 O4 172.45(5) .
O9 Co1 O4 84.71(6) .
O8 Co1 O4 87.26(6) .
O10 Co1 N1 93.10(6) .
O9 Co1 N1 87.31(6) .
O8 Co1 N1 176.35(6) .
O4 Co1 N1 89.35(6) .
O10 Co1 N2 91.58(6) .
O9 Co1 N2 174.25(6) .
O8 Co1 N2 92.01(6) .
O4 Co1 N2 95.68(6) .
N1 Co1 N2 86.96(6) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.240(3) .
C1 O2 1.243(3) .
C1 C2 1.513(3) .
C2 C3 1.382(3) .
C2 C7 1.398(3) .
C3 C4 1.378(3) .
C3 H3 0.9300 .
C4 C5 1.371(3) .
C4 H4 0.9300 .
C5 C6 1.369(3) .
C5 H5 0.9300 .
C6 C7 1.383(3) .
C6 O5 1.402(3) .
C7 C8 1.513(3) .
C8 O4 1.249(2) .
C8 O3 1.251(3) .
C9 O5 1.370(2) .
C9 C14 1.376(3) .
C9 C10 1.380(3) .
C10 C11 1.381(3) .
C10 H10 0.9300 .
C11 C12 1.381(3) .
C11 H11 0.9300 .
C12 C13 1.379(3) .
C12 C15 1.487(3) .
C13 C14 1.379(3) .
C13 H13 0.9300 .
C14 H14 0.9300 .
C15 O6 1.218(3) .
C15 O7 1.300(3) .
C16 N2 1.330(3) .
C16 C17 1.379(3) .
C16 H16 0.9300 .
C17 C18 1.382(3) .
C17 H17 0.9300 .
C18 C19 1.382(3) .
C18 C18 1.501(4) 2_466
C19 C20 1.374(3) .
C19 H19 0.9300 .
C20 N2 1.334(3) .
C20 H20 0.9300 .
C21 N1 1.330(3) .
C21 C22 1.375(3) .
C21 H21 0.9300 .
C22 C23 1.386(3) .
C22 H22 0.9300 .
C23 C24 1.389(3) .
C23 C23 1.490(4) 2_455
C24 C25 1.375(3) .
C24 H24 0.9300 .
C25 N1 1.332(3) .
C25 H25 0.9300 .
C26 N3 1.315(4) .
C26 C27 1.389(4) .
C26 H26 0.9300 .
C27 C28 1.382(4) .
C27 H27 0.9300 .
C28 C29 1.375(4) .
C28 C28 1.484(5) 2
C29 C30 1.387(5) .
C29 H29 0.9300 .
C30 N3 1.326(4) .
C30 H30 0.9300 .
C31 N4 1.316(3) .
C31 C32 1.371(3) .
C31 H31 0.9300 .
C32 C33 1.385(3) .
C32 H32 0.9300 .
C33 C34 1.387(3) .
C33 C33 1.484(4) 2_556
C34 C35 1.381(4) .
C34 H34 0.9300 .
C35 N4 1.323(3) .
C35 H35 0.9300 .
N1 Co1 2.1701(17) .
N2 Co1 2.1713(16) .
O4 Co1 2.1387(14) .
O7 H7A 0.8624 .
O8 Co1 2.1095(15) .
O8 H8B 0.8862 .
O8 H8A 0.9501 .
O9 Co1 2.1012(14) .
O9 H9A 0.9554 .
O9 H9B 0.8831 .
O10 Co1 2.0881(15) .
O10 H10A 0.9816 .
O10 H10B 0.8098 .
O11 H11B 0.8801 .
O11 H11A 0.8339 .
O12 H12A 0.8420 .
O12 H12B 0.8409 .
