#------------------------------------------------------------------------------
#$Date: 2016-03-24 14:00:38 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179648 $
#$URL: svn://www.crystallography.net/cod/cif/4/51/01/4510168.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4510168
loop_
_publ_author_name
'Kennedy, Robert D.'
'Clingerman, Daniel J.'
'Morris, William'
'Wilmer, Christopher E.'
'Sarjeant, Amy A.'
'Stern, Charlotte L.'
'O’Keeffe, Michael'
'Snurr, Randall Q.'
'Hupp, Joseph T.'
'Farha, Omar K.'
'Mirkin, Chad A.'
_publ_section_title
;
 Metallacarborane-Based Metal--Organic Framework with a Complex Topology
;
_journal_issue                   3
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              1324
_journal_paper_doi               10.1021/cg401817g
_journal_volume                  14
_journal_year                    2014
_chemical_formula_moiety         'C66 H98 B36 Co2 Cs2 O23, 6(C3 H6 O)'
_chemical_formula_sum            'C84 H134 B36 Co2 Cs2 O29'
_chemical_formula_weight         2380.75
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                82.240(2)
_cell_angle_beta                 76.013(2)
_cell_angle_gamma                76.535(2)
_cell_formula_units_Z            1
_cell_length_a                   10.7991(5)
_cell_length_b                   13.1642(6)
_cell_length_c                   21.7471(9)
_cell_measurement_reflns_used    9926
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      67.10
_cell_measurement_theta_min      3.46
_cell_volume                     2907.3(2)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'MX optics'
_diffrn_radiation_source         microsource
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0552
_diffrn_reflns_av_sigmaI/netI    0.0581
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            32159
_diffrn_reflns_theta_full        65.08
_diffrn_reflns_theta_max         65.08
_diffrn_reflns_theta_min         2.10
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    7.593
_exptl_absorpt_correction_T_max  0.7529
_exptl_absorpt_correction_T_min  0.4824
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, Bruker'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.360
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1214
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.123
_exptl_crystal_size_min          0.050
_refine_diff_density_max         1.545
_refine_diff_density_min         -0.699
_refine_diff_density_rms         0.125
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     710
_refine_ls_number_reflns         9807
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0511
_refine_ls_R_factor_gt           0.0454
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0825P)²+1.2823P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1170
_refine_ls_wR_factor_ref         0.1241
_reflns_number_gt                8857
_reflns_number_total             9807
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            Cs[5].cif
_cod_data_source_block           n1571a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4510168
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cs1 Cs 0.487493(18) 0.186539(16) 0.461402(10) 0.03072(10) Uani 1 1 d .
Co1 Co 0.43511(5) 0.26284(4) 1.02005(2) 0.02037(13) Uani 1 1 d .
O1 O -0.3832(3) 0.4597(2) 1.43333(13) 0.0434(7) Uani 1 1 d .
H1O H -0.3382 0.4261 1.4024 0.065 Uiso 0.50 1 calc PR
O2 O -0.3690(2) 0.4647(2) 1.53351(12) 0.0381(6) Uani 1 1 d .
H2O H -0.3116 0.4725 1.5515 0.057 Uiso 0.50 1 calc PR
O3 O 0.0457(2) 0.37272(19) 1.59247(11) 0.0291(5) Uani 1 1 d .
H3 H 0.0955 0.3617 1.6180 0.044 Uiso 1 1 calc R
O4 O 0.2322(2) 0.3178(2) 1.52309(12) 0.0339(5) Uani 1 1 d .
O5 O 1.2803(3) 0.0646(2) 0.64308(12) 0.0376(6) Uani 1 1 d .
H5 H 1.3616 0.0431 0.6351 0.056 Uiso 1 1 calc R
O6 O 1.3061(2) 0.03895(19) 0.54050(11) 0.0325(5) Uani 1 1 d .
O7 O 0.7169(3) 0.2025(2) 0.50942(12) 0.0367(6) Uani 1 1 d .
O8 O 0.9120(2) 0.14149(19) 0.44766(11) 0.0307(5) Uani 1 1 d .
H8 H 0.8683 0.1528 0.4194 0.046 Uiso 1 1 calc R
O9 O 0.7628(3) 0.1721(2) 0.36021(12) 0.0354(6) Uani 1 1 d .
O10 O 0.4203(3) 0.3531(2) 0.35250(14) 0.0441(7) Uani 1 1 d .
O11 O 0.4687(3) 0.0237(2) 0.37341(14) 0.0447(7) Uani 1 1 d .
O12 O 0.1936(3) 0.3438(3) 0.67670(15) 0.0528(8) Uani 1 1 d .
O13 O 0.1207(4) 0.0634(3) 0.81036(18) 0.0679(10) Uani 1 1 d .
O14 O 0.7669(6) 0.2995(8) 0.1133(3) 0.175(4) Uani 1 1 d .
O15 O 0.4725(8) 0.2543(8) 0.6102(4) 0.084(3) Uani 0.50 1 d P
H15A H 0.5397 0.2848 0.6097 0.126 Uiso 0.50 1 d PR
H15B H 0.3969 0.2999 0.6238 0.126 Uiso 0.50 1 d PR
C1 C 0.3781(4) 0.3853(3) 1.07700(17) 0.0306(7) Uani 1 1 d .
H1 H 0.4194 0.4536 1.0510 0.037 Uiso 1 1 calc R
C2 C 0.4679(3) 0.2781(3) 1.10662(15) 0.0249(7) Uani 1 1 d .
H2 H 0.5754 0.2708 1.1008 0.030 Uiso 1 1 calc R
C3 C 0.4821(4) 0.1434(3) 0.96127(19) 0.0398(9) Uani 1 1 d .
H3A H 0.4352 0.0770 0.9858 0.048 Uiso 1 1 calc R
C4 C 0.6122(4) 0.1721(3) 0.98160(19) 0.0382(9) Uani 1 1 d .
H4 H 0.6559 0.1256 1.0211 0.046 Uiso 1 1 calc R
C5 C 0.1490(3) 0.3304(3) 1.25929(17) 0.0282(7) Uani 1 1 d .
C6 C 0.0882(3) 0.3485(3) 1.31196(16) 0.0275(7) Uani 1 1 d .
C7 C 0.0227(3) 0.3658(3) 1.37660(16) 0.0267(7) Uani 1 1 d .
C8 C -0.1132(3) 0.3973(3) 1.39395(16) 0.0259(7) Uani 1 1 d .
H8A H -0.1640 0.4077 1.3627 0.031 Uiso 1 1 calc R
C9 C -0.1739(3) 0.4135(3) 1.45728(16) 0.0254(7) Uani 1 1 d .
C10 C -0.1016(3) 0.3991(3) 1.50372(16) 0.0257(7) Uani 1 1 d .
H10 H -0.1438 0.4106 1.5467 0.031 Uiso 1 1 calc R
C11 C 0.0337(3) 0.3676(2) 1.48655(16) 0.0246(7) Uani 1 1 d .
C12 C 0.0951(3) 0.3510(2) 1.42377(16) 0.0255(7) Uani 1 1 d .
H12 H 0.1873 0.3293 1.4126 0.031 Uiso 1 1 calc R
C13 C -0.3183(3) 0.4481(3) 1.47628(16) 0.0289(7) Uani 1 1 d .
C14 C 0.1147(3) 0.3499(3) 1.53535(16) 0.0268(7) Uani 1 1 d .
C15 C 0.7316(4) 0.1967(3) 0.78320(17) 0.0294(7) Uani 1 1 d .
C16 C 0.8002(3) 0.1810(3) 0.73133(16) 0.0281(7) Uani 1 1 d .
C17 C 0.8807(3) 0.1603(3) 0.66932(16) 0.0266(7) Uani 1 1 d .
C18 C 1.0160(3) 0.1247(3) 0.66105(16) 0.0267(7) Uani 1 1 d .
H18 H 1.0559 0.1160 0.6964 0.032 Uiso 1 1 calc R
C19 C 1.0921(3) 0.1019(2) 0.60104(16) 0.0264(7) Uani 1 1 d .
C20 C 1.0349(3) 0.1132(2) 0.54907(16) 0.0262(7) Uani 1 1 d .
H20 H 1.0869 0.0960 0.5084 0.031 Uiso 1 1 calc R
C21 C 0.9005(3) 0.1500(3) 0.55701(16) 0.0266(7) Uani 1 1 d .
C22 C 0.8242(3) 0.1741(3) 0.61647(16) 0.0274(7) Uani 1 1 d .
H22 H 0.7329 0.2002 0.6213 0.033 Uiso 1 1 calc R
C23 C 1.2361(3) 0.0652(3) 0.59145(16) 0.0284(7) Uani 1 1 d .
C24 C 0.8337(4) 0.1669(3) 0.50277(16) 0.0284(7) Uani 1 1 d .
C25 C 0.9382(4) 0.1429(3) 0.2705(2) 0.0406(9) Uani 1 1 d .
H25A H 0.9550 0.2022 0.2396 0.061 Uiso 1 1 calc R
H25B H 0.9602 0.0787 0.2485 0.061 Uiso 1 1 calc R
H25C H 0.9918 0.1349 0.3020 0.061 Uiso 1 1 calc R
C26 C 0.7975(4) 0.1625(3) 0.30315(17) 0.0309(7) Uani 1 1 d .
C27 C 0.7008(4) 0.1680(4) 0.26355(19) 0.0427(9) Uani 1 1 d .
H27A H 0.7067 0.0980 0.2510 0.064 Uiso 1 1 calc R
H27B H 0.7194 0.2157 0.2254 0.064 Uiso 1 1 calc R
H27C H 0.6127 0.1939 0.2882 0.064 Uiso 1 1 calc R
C28 C 0.5700(5) 0.4529(4) 0.2898(2) 0.0524(11) Uani 1 1 d .
H28A H 0.6358 0.3951 0.3035 0.079 Uiso 1 1 calc R
H28B H 0.5807 0.5191 0.3016 0.079 Uiso 1 1 calc R
H28C H 0.5810 0.4562 0.2435 0.079 Uiso 1 1 calc R
C29 C 0.4354(4) 0.4349(3) 0.32173(17) 0.0367(8) Uani 1 1 d .
C30 C 0.3232(5) 0.5231(3) 0.3138(2) 0.0436(9) Uani 1 1 d .
H30A H 0.2415 0.4979 0.3280 0.065 Uiso 1 1 calc R
H30B H 0.3335 0.5494 0.2689 0.065 Uiso 1 1 calc R
H30C H 0.3210 0.5797 0.3393 0.065 Uiso 1 1 calc R
C31 C 0.4564(5) -0.0417(4) 0.2796(2) 0.0454(10) Uani 1 1 d .
H31A H 0.5517 -0.0613 0.2731 0.068 Uiso 1 1 calc R
H31B H 0.4326 0.0009 0.2420 0.068 Uiso 1 1 calc R
H31C H 0.4205 -0.1051 0.2865 0.068 Uiso 1 1 calc R
C32 C 0.4025(4) 0.0198(3) 0.33621(18) 0.0335(8) Uani 1 1 d .
C33 C 0.2638(4) 0.0774(3) 0.3462(2) 0.0443(9) Uani 1 1 d .
H33A H 0.2306 0.0898 0.3913 0.066 Uiso 1 1 calc R
H33B H 0.2115 0.0355 0.3336 0.066 Uiso 1 1 calc R
H33C H 0.2584 0.1447 0.3205 0.066 Uiso 1 1 calc R
C34 C 0.2383(8) 0.2891(6) 0.7763(3) 0.086(2) Uani 1 1 d .
H34A H 0.2350 0.2159 0.7912 0.129 Uiso 1 1 calc R
H34B H 0.2120 0.3315 0.8129 0.129 Uiso 1 1 calc R
H34C H 0.3275 0.2936 0.7539 0.129 Uiso 1 1 calc R
C35 C 0.1480(5) 0.3291(4) 0.7324(2) 0.0483(11) Uani 1 1 d .
C36 C 0.0019(5) 0.3461(4) 0.7584(2) 0.0572(12) Uani 1 1 d .
H36A H -0.0280 0.4104 0.7806 0.086 Uiso 1 1 calc R
H36B H -0.0183 0.2863 0.7882 0.086 Uiso 1 1 calc R
H36C H -0.0424 0.3525 0.7233 0.086 Uiso 1 1 calc R
C37 C 0.1640(14) 0.0513(14) 0.9116(5) 0.213(9) Uani 1 1 d .
H37A H 0.2015 -0.0144 0.9337 0.320 Uiso 1 1 calc R
H37B H 0.1009 0.0958 0.9427 0.320 Uiso 1 1 calc R
H37C H 0.2337 0.0879 0.8896 0.320 Uiso 1 1 calc R
C38 C 0.0981(5) 0.0284(4) 0.8654(3) 0.0534(11) Uani 1 1 d .
C39 C 0.0019(8) -0.0372(7) 0.8898(4) 0.103(3) Uani 1 1 d .
H39A H -0.0583 -0.0265 0.8612 0.155 Uiso 1 1 calc R
H39B H -0.0471 -0.0181 0.9322 0.155 Uiso 1 1 calc R
H39C H 0.0466 -0.1110 0.8923 0.155 Uiso 1 1 calc R
C40 C 0.8400(7) 0.4658(5) 0.1112(3) 0.0803(18) Uani 1 1 d .
H40A H 0.7892 0.5284 0.0920 0.121 Uiso 1 1 calc R
H40B H 0.9323 0.4700 0.1007 0.121 Uiso 1 1 calc R
H40C H 0.8084 0.4615 0.1575 0.121 Uiso 1 1 calc R
C41 C 0.8245(6) 0.3678(8) 0.0852(3) 0.102(3) Uani 1 1 d .
C42 C 0.9093(7) 0.3435(5) 0.0178(3) 0.0782(19) Uani 1 1 d .
H42A H 1.0013 0.3393 0.0175 0.117 Uiso 1 1 calc R
H42B H 0.8814 0.3993 -0.0137 0.117 Uiso 1 1 calc R
H42C H 0.8986 0.2764 0.0072 0.117 Uiso 1 1 calc R
B1 B 0.4080(4) 0.1716(3) 1.10569(16) 0.0232(7) Uani 1 1 d .
H1A H 0.4694 0.0908 1.0998 0.028 Uiso 1 1 calc R
B2 B 0.2677(4) 0.2115(3) 1.07441(17) 0.0228(7) Uani 1 1 d .
H2A H 0.2315 0.1605 1.0484 0.027 Uiso 1 1 calc R
B3 B 0.2491(4) 0.3510(3) 1.05518(18) 0.0244(7) Uani 1 1 d .
H3B H 0.2005 0.3938 1.0163 0.029 Uiso 1 1 calc R
B4 B 0.2262(4) 0.4099(3) 1.12790(18) 0.0260(8) Uani 1 1 d .
H4A H 0.1656 0.4907 1.1351 0.031 Uiso 1 1 calc R
B5 B 0.3686(4) 0.3642(3) 1.15891(18) 0.0277(8) Uani 1 1 d .
H5A H 0.4035 0.4141 1.1862 0.033 Uiso 1 1 calc R
B6 B 0.3877(4) 0.2275(3) 1.17736(17) 0.0269(8) Uani 1 1 d .
H6 H 0.4355 0.1868 1.2169 0.032 Uiso 1 1 calc R
B7 B 0.2573(4) 0.1863(3) 1.15834(17) 0.0246(7) Uani 1 1 d .
H7 H 0.2176 0.1184 1.1859 0.030 Uiso 1 1 calc R
B8 B 0.1569(4) 0.2992(3) 1.12756(17) 0.0247(7) Uani 1 1 d .
H8B H 0.0490 0.3062 1.1349 0.030 Uiso 1 1 calc R
B9 B 0.2292(4) 0.3092(3) 1.19155(18) 0.0254(7) Uani 1 1 d .
B10 B 0.6063(3) 0.3021(3) 0.96632(17) 0.0236(7) Uani 1 1 d .
H10A H 0.6451 0.3475 0.9947 0.028 Uiso 1 1 calc R
B11 B 0.4724(4) 0.3566(3) 0.93538(18) 0.0294(8) Uani 1 1 d .
H11 H 0.4186 0.4395 0.9417 0.035 Uiso 1 1 calc R
B12 B 0.3878(4) 0.2579(3) 0.93267(18) 0.0286(8) Uani 1 1 d .
H12A H 0.2799 0.2712 0.9366 0.034 Uiso 1 1 calc R
B13 B 0.6388(4) 0.1127(3) 0.91161(19) 0.0319(9) Uani 1 1 d .
H13 H 0.6943 0.0305 0.9043 0.038 Uiso 1 1 calc R
B14 B 0.7176(4) 0.2156(3) 0.91525(18) 0.0278(8) Uani 1 1 d .
H14 H 0.8257 0.2017 0.9104 0.033 Uiso 1 1 calc R
B15 B 0.6281(4) 0.3346(3) 0.88462(18) 0.0260(8) Uani 1 1 d .
H15 H 0.6768 0.3995 0.8592 0.031 Uiso 1 1 calc R
B16 B 0.4928(4) 0.3061(3) 0.86290(19) 0.0298(8) Uani 1 1 d .
H16 H 0.4522 0.3526 0.8225 0.036 Uiso 1 1 calc R
B17 B 0.4986(4) 0.1697(3) 0.87963(19) 0.0320(9) Uani 1 1 d .
H17 H 0.4616 0.1246 0.8503 0.038 Uiso 1 1 calc R
B18 B 0.6459(4) 0.2155(3) 0.84964(18) 0.0264(8) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.7457 7.9052 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O7 Cs1 O4 115.35(7) . 1_554
O7 Cs1 O10 115.31(8) . .
O4 Cs1 O10 76.96(7) 1_554 .
O7 Cs1 O11 128.22(7) . .
O4 Cs1 O11 115.48(7) 1_554 .
O10 Cs1 O11 85.23(8) . .
O7 Cs1 O6 118.01(7) . 1_455
O4 Cs1 O6 70.88(7) 1_554 1_455
O10 Cs1 O6 125.42(7) . 1_455
O11 Cs1 O6 71.15(7) . 1_455
O7 Cs1 O9 62.61(7) . .
O4 Cs1 O9 148.75(7) 1_554 .
O10 Cs1 O9 76.83(7) . .
O11 Cs1 O9 78.83(7) . .
O6 Cs1 O9 139.54(7) 1_455 .
O7 Cs1 O6 69.70(7) . 2_756
O4 Cs1 O6 148.04(7) 1_554 2_756
O10 Cs1 O6 131.48(7) . 2_756
O11 Cs1 O6 62.23(7) . 2_756
O6 Cs1 O6 79.06(7) 1_455 2_756
O9 Cs1 O6 62.96(7) . 2_756
O7 Cs1 O15 55.37(15) . .
O4 Cs1 O15 64.70(14) 1_554 .
O10 Cs1 O15 121.93(17) . .
O11 Cs1 O15 149.90(18) . .
O6 Cs1 O15 81.56(17) 1_455 .
O9 Cs1 O15 117.36(15) . .
O6 Cs1 O15 100.92(15) 2_756 .
O7 Cs1 C23 111.94(7) . 1_455
O4 Cs1 C23 58.60(7) 1_554 1_455
O10 Cs1 C23 125.25(7) . 1_455
O11 Cs1 C23 86.65(8) . 1_455
O6 Cs1 C23 16.04(7) 1_455 1_455
O9 Cs1 C23 152.65(7) . 1_455
O6 Cs1 C23 89.79(7) 2_756 1_455
O15 Cs1 C23 67.56(17) . 1_455
O7 Cs1 Cs1 93.91(5) . 2_656
O4 Cs1 Cs1 110.73(5) 1_554 2_656
O10 Cs1 Cs1 143.72(6) . 2_656
O11 Cs1 Cs1 59.11(6) . 2_656
O6 Cs1 Cs1 40.54(4) 1_455 2_656
O9 Cs1 Cs1 100.46(5) . 2_656
O6 Cs1 Cs1 38.52(4) 2_756 2_656
O15 Cs1 Cs1 91.85(16) . 2_656
C23 Cs1 Cs1 52.26(5) 1_455 2_656
C2 Co1 C4 99.26(15) . .
C2 Co1 C1 47.90(13) . .
C4 Co1 C1 134.08(16) . .
C2 Co1 C3 134.92(16) . .
C4 Co1 C3 49.01(16) . .
C1 Co1 C3 176.65(16) . .
C2 Co1 B10 96.41(14) . .
C4 Co1 B10 48.31(15) . .
C1 Co1 B10 97.74(15) . .
C3 Co1 B10 83.95(15) . .
C2 Co1 B1 48.20(13) . .
C4 Co1 B1 95.14(16) . .
C1 Co1 B1 83.89(14) . .
C3 Co1 B1 97.35(16) . .
B10 Co1 B1 128.25(15) . .
C2 Co1 B11 128.85(14) . .
C4 Co1 B11 83.31(17) . .
C1 Co1 B11 94.89(16) . .
C3 Co1 B11 84.05(17) . .
B10 Co1 B11 48.57(15) . .
B1 Co1 B11 176.47(14) . .
C2 Co1 B3 84.23(14) . .
C4 Co1 B3 176.12(15) . .
C1 Co1 B3 49.73(14) . .
C3 Co1 B3 127.16(15) . .
B10 Co1 B3 133.27(15) . .
B1 Co1 B3 85.91(15) . .
B11 Co1 B3 95.84(16) . .
C2 Co1 B12 175.10(15) . .
C4 Co1 B12 85.45(17) . .
C1 Co1 B12 127.50(16) . .
C3 Co1 B12 49.61(17) . .
B10 Co1 B12 85.71(15) . .
B1 Co1 B12 133.08(15) . .
B11 Co1 B12 50.07(15) . .
B3 Co1 B12 91.10(16) . .
C2 Co1 B2 84.01(14) . .
C4 Co1 B2 127.58(15) . .
C1 Co1 B2 85.58(14) . .
C3 Co1 B2 92.85(15) . .
B10 Co1 B2 175.89(14) . .
B1 Co1 B2 49.51(14) . .
B11 Co1 B2 133.78(15) . .
B3 Co1 B2 50.82(14) . .
B12 Co1 B2 94.19(15) . .
C13 O1 H1O 109.5 . .
C13 O2 H2O 109.5 . .
C14 O3 H3 109.5 . .
C14 O4 Cs1 156.9(2) . 1_556
C23 O5 H5 109.5 . .
C23 O6 Cs1 118.9(2) . 1_655
C23 O6 Cs1 118.3(2) . 2_756
Cs1 O6 Cs1 100.94(7) 1_655 2_756
C24 O7 Cs1 141.4(2) . .
C24 O8 H8 109.5 . .
C26 O9 Cs1 134.1(2) . .
C29 O10 Cs1 148.6(3) . .
C32 O11 Cs1 137.0(3) . .
Cs1 O15 H15A 110.5 . .
Cs1 O15 H15B 110.3 . .
H15A O15 H15B 108.5 . .
C2 C1 B4 108.3(3) . .
C2 C1 B3 108.9(3) . .
B4 C1 B3 62.2(2) . .
C2 C1 B5 60.1(2) . .
B4 C1 B5 61.3(2) . .
B3 C1 B5 112.3(3) . .
C2 C1 Co1 65.65(16) . .
B4 C1 Co1 122.0(2) . .
B3 C1 Co1 66.29(17) . .
B5 C1 Co1 121.4(2) . .
C2 C1 H1 123.3 . .
B4 C1 H1 118.4 . .
B3 C1 H1 120.1 . .
B5 C1 H1 117.7 . .
Co1 C1 H1 109.2 . .
C1 C2 B1 111.2(3) . .
C1 C2 B6 112.8(3) . .
B1 C2 B6 62.6(2) . .
C1 C2 B5 62.4(2) . .
B1 C2 B5 113.2(3) . .
B6 C2 B5 62.3(2) . .
C1 C2 Co1 66.45(16) . .
B1 C2 Co1 66.86(16) . .
B6 C2 Co1 124.5(2) . .
B5 C2 Co1 124.2(2) . .
C1 C2 H2 120.4 . .
B1 C2 H2 120.0 . .
B6 C2 H2 116.3 . .
B5 C2 H2 116.3 . .
Co1 C2 H2 107.6 . .
C4 C3 B17 108.3(3) . .
C4 C3 B12 109.6(3) . .
B17 C3 B12 61.5(2) . .
C4 C3 B13 60.1(2) . .
B17 C3 B13 61.3(2) . .
B12 C3 B13 111.9(3) . .
C4 C3 Co1 65.45(18) . .
B17 C3 Co1 121.0(3) . .
B12 C3 Co1 66.45(18) . .
B13 C3 Co1 120.7(2) . .
C4 C3 H3A 122.8 . .
B17 C3 H3A 119.0 . .
B12 C3 H3A 120.0 . .
B13 C3 H3A 118.0 . .
Co1 C3 H3A 109.8 . .
B10 C4 C3 108.9(3) . .
B10 C4 B14 61.3(2) . .
C3 C4 B14 111.0(3) . .
B10 C4 B13 110.8(3) . .
C3 C4 B13 61.7(2) . .
B14 C4 B13 61.7(2) . .
B10 C4 Co1 66.39(18) . .
C3 C4 Co1 65.54(19) . .
B14 C4 Co1 122.5(3) . .
B13 C4 Co1 122.2(3) . .
B10 C4 H4 121.6 . .
C3 C4 H4 121.7 . .
B14 C4 H4 117.4 . .
B13 C4 H4 117.5 . .
Co1 C4 H4 108.9 . .
C6 C5 B9 178.6(4) . .
C5 C6 C7 176.2(4) . .
C8 C7 C12 118.8(3) . .
C8 C7 C6 121.3(3) . .
C12 C7 C6 119.9(3) . .
C9 C8 C7 119.9(3) . .
C9 C8 H8A 120.1 . .
C7 C8 H8A 120.1 . .
C10 C9 C8 121.1(3) . .
C10 C9 C13 118.5(3) . .
C8 C9 C13 120.4(3) . .
C9 C10 C11 119.1(3) . .
C9 C10 H10 120.4 . .
C11 C10 H10 120.4 . .
C12 C11 C10 120.3(3) . .
C12 C11 C14 119.0(3) . .
C10 C11 C14 120.7(3) . .
C11 C12 C7 120.8(3) . .
C11 C12 H12 119.6 . .
C7 C12 H12 119.6 . .
O2 C13 O1 123.8(3) . .
O2 C13 C9 118.5(3) . .
O1 C13 C9 117.7(3) . .
O4 C14 O3 123.9(3) . .
O4 C14 C11 122.9(3) . .
O3 C14 C11 113.1(3) . .
C16 C15 B18 179.1(4) . .
C15 C16 C17 178.6(4) . .
C22 C17 C18 119.1(3) . .
C22 C17 C16 120.2(3) . .
C18 C17 C16 120.7(3) . .
C19 C18 C17 120.0(3) . .
C19 C18 H18 120.0 . .
C17 C18 H18 120.0 . .
C20 C19 C18 120.6(3) . .
C20 C19 C23 118.8(3) . .
C18 C19 C23 120.6(3) . .
C19 C20 C21 119.5(3) . .
C19 C20 H20 120.3 . .
C21 C20 H20 120.3 . .
C22 C21 C20 120.3(3) . .
C22 C21 C24 117.6(3) . .
C20 C21 C24 122.1(3) . .
C21 C22 C17 120.5(3) . .
C21 C22 H22 119.7 . .
C17 C22 H22 119.7 . .
O6 C23 O5 123.6(3) . .
O6 C23 C19 123.0(3) . .
O5 C23 C19 113.4(3) . .
O6 C23 Cs1 45.05(18) . 1_655
O5 C23 Cs1 102.0(2) . 1_655
C19 C23 Cs1 124.3(2) . 1_655
O7 C24 O8 123.6(3) . .
O7 C24 C21 122.0(3) . .
O8 C24 C21 114.4(3) . .
C26 C25 H25A 109.5 . .
C26 C25 H25B 109.5 . .
H25A C25 H25B 109.5 . .
C26 C25 H25C 109.5 . .
H25A C25 H25C 109.5 . .
H25B C25 H25C 109.5 . .
O9 C26 C27 121.2(3) . .
O9 C26 C25 121.4(3) . .
C27 C26 C25 117.3(3) . .
C26 C27 H27A 109.5 . .
C26 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C26 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C29 C28 H28A 109.5 . .
C29 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C29 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
O10 C29 C30 122.3(4) . .
O10 C29 C28 121.1(4) . .
C30 C29 C28 116.6(4) . .
C29 C30 H30A 109.5 . .
C29 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C29 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C32 C31 H31A 109.5 . .
C32 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C32 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
O11 C32 C31 121.5(4) . .
O11 C32 C33 120.4(4) . .
C31 C32 C33 118.0(4) . .
C32 C33 H33A 109.5 . .
C32 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C32 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
C35 C34 H34A 109.5 . .
C35 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
C35 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
O12 C35 C34 118.6(5) . .
O12 C35 C36 121.7(4) . .
C34 C35 C36 119.6(5) . .
C35 C36 H36A 109.5 . .
C35 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C35 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C38 C37 H37A 109.5 . .
C38 C37 H37B 109.5 . .
H37A C37 H37B 109.5 . .
C38 C37 H37C 109.5 . .
H37A C37 H37C 109.5 . .
H37B C37 H37C 109.5 . .
O13 C38 C39 122.2(6) . .
O13 C38 C37 121.7(5) . .
C39 C38 C37 116.1(6) . .
C38 C39 H39A 109.5 . .
C38 C39 H39B 109.5 . .
H39A C39 H39B 109.5 . .
C38 C39 H39C 109.5 . .
H39A C39 H39C 109.5 . .
H39B C39 H39C 109.5 . .
C41 C40 H40A 109.5 . .
C41 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
C41 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
O14 C41 C40 128.2(8) . .
O14 C41 C42 115.3(10) . .
C40 C41 C42 115.8(5) . .
C41 C42 H42A 109.5 . .
C41 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C41 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
C2 B1 B7 107.4(3) . .
C2 B1 B2 108.1(3) . .
B7 B1 B2 61.9(2) . .
C2 B1 B6 59.4(2) . .
B7 B1 B6 61.1(2) . .
B2 B1 B6 111.4(3) . .
C2 B1 Co1 64.94(16) . .
B7 B1 Co1 121.3(2) . .
B2 B1 Co1 66.30(17) . .
B6 B1 Co1 119.9(2) . .
C2 B1 H1A 124.0 . .
B7 B1 H1A 118.7 . .
B2 B1 H1A 120.5 . .
B6 B1 H1A 118.5 . .
Co1 B1 H1A 109.9 . .
B1 B2 B8 105.5(3) . .
B1 B2 B7 58.6(2) . .
B8 B2 B7 59.8(2) . .
B1 B2 B3 106.0(2) . .
B8 B2 B3 60.1(2) . .
B7 B2 B3 107.8(2) . .
B1 B2 Co1 64.19(16) . .
B8 B2 Co1 116.8(2) . .
B7 B2 Co1 116.6(2) . .
B3 B2 Co1 64.16(16) . .
B1 B2 H2A 124.3 . .
B8 B2 H2A 120.8 . .
B7 B2 H2A 120.4 . .
B3 B2 H2A 122.6 . .
Co1 B2 H2A 112.8 . .
C1 B3 B8 105.0(3) . .
C1 B3 B4 58.5(2) . .
B8 B3 B4 59.9(2) . .
C1 B3 B2 105.7(3) . .
B8 B3 B2 59.2(2) . .
B4 B3 B2 107.4(3) . .
C1 B3 Co1 63.98(17) . .
B8 B3 Co1 116.8(2) . .
B4 B3 Co1 116.7(2) . .
B2 B3 Co1 65.01(16) . .
C1 B3 H3B 124.7 . .
B8 B3 H3B 121.2 . .
B4 B3 H3B 120.4 . .
B2 B3 H3B 122.8 . .
Co1 B3 H3B 112.4 . .
C1 B4 B5 59.8(2) . .
C1 B4 B9 106.6(3) . .
B5 B4 B9 59.9(2) . .
C1 B4 B8 105.6(3) . .
B5 B4 B8 107.5(3) . .
B9 B4 B8 59.9(2) . .
C1 B4 B3 59.3(2) . .
B5 B4 B3 108.8(3) . .
B9 B4 B3 108.7(3) . .
B8 B4 B3 59.9(2) . .
C1 B4 H4A 123.4 . .
B5 B4 H4A 121.4 . .
B9 B4 H4A 121.8 . .
B8 B4 H4A 122.7 . .
B3 B4 H4A 121.1 . .
C2 B5 C1 57.5(2) . .
C2 B5 B6 58.8(2) . .
C1 B5 B6 106.1(3) . .
C2 B5 B4 104.3(3) . .
C1 B5 B4 58.9(2) . .
B6 B5 B4 108.3(3) . .
C2 B5 B9 105.0(3) . .
C1 B5 B9 106.2(3) . .
B6 B5 B9 60.3(2) . .
B4 B5 B9 60.4(2) . .
C2 B5 H5A 124.8 . .
C1 B5 H5A 123.5 . .
B6 B5 H5A 121.6 . .
B4 B5 H5A 122.3 . .
B9 B5 H5A 122.3 . .
C2 B6 B1 58.02(19) . .
C2 B6 B5 59.0(2) . .
B1 B6 B5 106.9(3) . .
C2 B6 B7 104.5(3) . .
B1 B6 B7 58.8(2) . .
B5 B6 B7 108.6(3) . .
C2 B6 B9 105.0(3) . .
B1 B6 B9 106.6(3) . .
B5 B6 B9 60.1(2) . .
B7 B6 B9 60.6(2) . .
C2 B6 H6 124.7 . .
B1 B6 H6 123.0 . .
B5 B6 H6 121.3 . .
B7 B6 H6 122.2 . .
B9 B6 H6 122.3 . .
B1 B7 B6 60.1(2) . .
B1 B7 B8 106.0(3) . .
B6 B7 B8 107.6(3) . .
B1 B7 B9 107.0(3) . .
B6 B7 B9 59.8(2) . .
B8 B7 B9 60.0(2) . .
B1 B7 B2 59.5(2) . .
B6 B7 B2 108.7(3) . .
B8 B7 B2 59.6(2) . .
B9 B7 B2 108.3(3) . .
B1 B7 H7 122.9 . .
B6 B7 H7 121.4 . .
B8 B7 H7 122.6 . .
B9 B7 H7 121.8 . .
B2 B7 H7 121.3 . .
B2 B8 B7 60.6(2) . .
B2 B8 B9 109.4(3) . .
B7 B8 B9 60.3(2) . .
B2 B8 B4 108.8(3) . .
B7 B8 B4 108.0(3) . .
B9 B8 B4 59.9(2) . .
B2 B8 B3 60.8(2) . .
B7 B8 B3 109.0(3) . .
B9 B8 B3 108.8(3) . .
B4 B8 B3 60.1(2) . .
B2 B8 H8B 120.7 . .
B7 B8 H8B 121.4 . .
B9 B8 H8B 121.2 . .
B4 B8 H8B 121.8 . .
B3 B8 H8B 121.1 . .
C5 B9 B5 120.6(3) . .
C5 B9 B6 122.2(3) . .
B5 B9 B6 59.6(2) . .
C5 B9 B4 121.0(3) . .
B5 B9 B4 59.8(2) . .
B6 B9 B4 107.3(3) . .
C5 B9 B8 123.0(3) . .
B5 B9 B8 107.6(3) . .
B6 B9 B8 107.1(3) . .
B4 B9 B8 60.2(2) . .
C5 B9 B7 123.5(3) . .
B5 B9 B7 107.4(3) . .
B6 B9 B7 59.6(2) . .
B4 B9 B7 107.7(3) . .
B8 B9 B7 59.6(2) . .
C4 B10 B11 108.1(3) . .
C4 B10 B14 60.6(2) . .
B11 B10 B14 110.4(3) . .
C4 B10 B15 109.3(3) . .
B11 B10 B15 61.3(2) . .
B14 B10 B15 61.3(2) . .
C4 B10 Co1 65.30(18) . .
B11 B10 Co1 66.07(17) . .
B14 B10 Co1 120.9(2) . .
B15 B10 Co1 121.6(2) . .
C4 B10 H10A 122.7 . .
B11 B10 H10A 121.6 . .
B14 B10 H10A 118.2 . .
B15 B10 H10A 118.1 . .
Co1 B10 H10A 109.6 . .
B10 B11 B16 108.6(3) . .
B10 B11 B15 60.3(2) . .
B16 B11 B15 60.8(2) . .
B10 B11 B12 109.2(3) . .
B16 B11 B12 61.7(2) . .
B15 B11 B12 111.2(3) . .
B10 B11 Co1 65.36(18) . .
B16 B11 Co1 120.2(3) . .
B15 B11 Co1 120.2(3) . .
B12 B11 Co1 65.39(18) . .
B10 B11 H11 122.4 . .
B16 B11 H11 118.9 . .
B15 B11 H11 118.3 . .
B12 B11 H11 120.6 . .
Co1 B11 H11 110.6 . .
C3 B12 B11 104.2(3) . .
C3 B12 B17 59.1(2) . .
B11 B12 B17 105.1(3) . .
C3 B12 B16 105.4(3) . .
B11 B12 B16 58.3(2) . .
B17 B12 B16 59.4(2) . .
C3 B12 Co1 63.94(18) . .
B11 B12 Co1 64.54(17) . .
B17 B12 Co1 116.7(3) . .
B16 B12 Co1 116.6(2) . .
C3 B12 H12A 124.5 . .
B11 B12 H12A 124.7 . .
B17 B12 H12A 121.0 . .
B16 B12 H12A 121.2 . .
Co1 B12 H12A 112.4 . .
C4 B13 C3 58.3(2) . .
C4 B13 B18 105.7(3) . .
C3 B13 B18 106.1(3) . .
C4 B13 B14 58.9(2) . .
C3 B13 B14 106.1(3) . .
B18 B13 B14 60.1(2) . .
C4 B13 B17 104.8(3) . .
C3 B13 B17 58.6(2) . .
B18 B13 B17 59.9(2) . .
B14 B13 B17 107.4(3) . .
C4 B13 H13 124.0 . .
C3 B13 H13 123.4 . .
B18 B13 H13 122.4 . .
B14 B13 H13 122.0 . .
B17 B13 H13 122.8 . .
C4 B14 B10 58.2(2) . .
C4 B14 B15 105.9(3) . .
B10 B14 B15 59.4(2) . .
C4 B14 B13 59.3(2) . .
B10 B14 B13 106.4(3) . .
B15 B14 B13 108.3(3) . .
C4 B14 B18 105.8(3) . .
B10 B14 B18 106.4(3) . .
B15 B14 B18 60.2(2) . .
B13 B14 B18 59.9(2) . .
C4 B14 H14 123.7 . .
B10 B14 H14 123.2 . .
B15 B14 H14 121.8 . .
B13 B14 H14 121.7 . .
B18 B14 H14 122.4 . .
B10 B15 B11 58.4(2) . .
B10 B15 B16 105.7(3) . .
B11 B15 B16 59.0(2) . .
B10 B15 B14 59.3(2) . .
B11 B15 B14 106.5(3) . .
B16 B15 B14 108.0(3) . .
B10 B15 B18 106.2(3) . .
B11 B15 B18 106.6(3) . .
B16 B15 B18 60.2(2) . .
B14 B15 B18 60.0(2) . .
B10 B15 H15 123.5 . .
B11 B15 H15 123.1 . .
B16 B15 H15 122.2 . .
B14 B15 H15 121.8 . .
B18 B15 H15 122.2 . .
B11 B16 B15 60.1(2) . .
B11 B16 B17 106.5(3) . .
B15 B16 B17 108.1(3) . .
B11 B16 B18 107.5(3) . .
B15 B16 B18 60.3(2) . .
B17 B16 B18 60.0(2) . .
B11 B16 B12 60.0(2) . .
B15 B16 B12 109.3(3) . .
B17 B16 B12 59.7(2) . .
B18 B16 B12 108.5(3) . .
B11 B16 H16 122.5 . .
B15 B16 H16 121.0 . .
B17 B16 H16 122.4 . .
B18 B16 H16 121.6 . .
B12 B16 H16 121.1 . .
C3 B17 B16 106.8(3) . .
C3 B17 B18 107.3(3) . .
B16 B17 B18 60.3(2) . .
C3 B17 B12 59.4(2) . .
B16 B17 B12 60.9(2) . .
B18 B17 B12 109.8(3) . .
C3 B17 B13 60.1(2) . .
B16 B17 B13 108.3(3) . .
B18 B17 B13 59.9(2) . .
B12 B17 B13 109.4(3) . .
C3 B17 H17 122.9 . .
B16 B17 H17 121.8 . .
B18 B17 H17 121.3 . .
B12 B17 H17 120.4 . .
B13 B17 H17 121.2 . .
C15 B18 B17 123.6(3) . .
C15 B18 B13 121.5(3) . .
B17 B18 B13 60.2(2) . .
C15 B18 B14 120.6(3) . .
B17 B18 B14 107.5(3) . .
B13 B18 B14 60.0(2) . .
C15 B18 B16 123.0(3) . .
B17 B18 B16 59.7(2) . .
B13 B18 B16 108.0(3) . .
B14 B18 B16 107.2(3) . .
C15 B18 B15 121.1(3) . .
B17 B18 B15 107.3(3) . .
B13 B18 B15 108.0(3) . .
B14 B18 B15 59.8(2) . .
B16 B18 B15 59.5(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cs1 O7 2.971(3) .
Cs1 O4 3.001(2) 1_554
Cs1 O10 3.103(3) .
Cs1 O11 3.130(3) .
Cs1 O6 3.132(3) 1_455
Cs1 O9 3.226(3) .
Cs1 O6 3.269(2) 2_756
Cs1 O15 3.428(10) .
Cs1 C23 3.874(3) 1_455
Cs1 Cs1 4.9383(5) 2_656
Co1 C2 2.041(3) .
Co1 C4 2.053(4) .
Co1 C1 2.054(3) .
Co1 C3 2.055(4) .
Co1 B10 2.071(4) .
Co1 B1 2.072(4) .
Co1 B11 2.082(4) .
Co1 B3 2.093(4) .
Co1 B12 2.097(4) .
Co1 B2 2.108(4) .
O1 C13 1.271(4) .
O1 H1O 0.8400 .
O2 C13 1.259(4) .
O2 H2O 0.8400 .
O3 C14 1.318(4) .
O3 H3 0.8400 .
O4 C14 1.215(4) .
O4 Cs1 3.001(2) 1_556
O5 C23 1.321(4) .
O5 H5 0.8400 .
O6 C23 1.223(4) .
O6 Cs1 3.132(3) 1_655
O6 Cs1 3.269(2) 2_756
O7 C24 1.219(5) .
O8 C24 1.322(4) .
O8 H8 0.8400 .
O9 C26 1.222(4) .
O10 C29 1.212(5) .
O11 C32 1.214(5) .
O12 C35 1.201(6) .
O13 C38 1.212(6) .
O14 C41 1.224(9) .
O15 H15A 0.9052 .
O15 H15B 0.9048 .
C1 C2 1.663(5) .
C1 B4 1.730(5) .
C1 B3 1.744(5) .
C1 B5 1.747(5) .
C1 H1 1.1200 .
C2 B1 1.680(5) .
C2 B6 1.705(5) .
C2 B5 1.709(5) .
C2 H2 1.1200 .
C3 C4 1.704(6) .
C3 B17 1.736(6) .
C3 B12 1.742(6) .
C3 B13 1.763(5) .
C3 H3A 1.1200 .
C4 B10 1.687(5) .
C4 B14 1.730(5) .
C4 B13 1.737(5) .
C4 H4 1.1200 .
C5 C6 1.199(5) .
C5 B9 1.543(5) .
C6 C7 1.435(5) .
C7 C8 1.399(5) .
C7 C12 1.402(5) .
C8 C9 1.396(5) .
C8 H8A 0.9500 .
C9 C10 1.388(5) .
C9 C13 1.490(5) .
C10 C11 1.394(5) .
C10 H10 0.9500 .
C11 C12 1.388(5) .
C11 C14 1.494(5) .
C12 H12 0.9500 .
C15 C16 1.205(5) .
C15 B18 1.533(5) .
C16 C17 1.439(5) .
C17 C22 1.399(5) .
C17 C18 1.402(5) .
C18 C19 1.393(5) .
C18 H18 0.9500 .
C19 C20 1.390(5) .
C19 C23 1.488(5) .
C20 C21 1.394(5) .
C20 H20 0.9500 .
C21 C22 1.388(5) .
C21 C24 1.492(5) .
C22 H22 0.9500 .
C23 Cs1 3.874(3) 1_655
C25 C26 1.491(5) .
C25 H25A 0.9800 .
C25 H25B 0.9800 .
C25 H25C 0.9800 .
C26 C27 1.490(5) .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 C29 1.510(6) .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 C30 1.496(6) .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 C32 1.487(6) .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C32 C33 1.491(6) .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
C34 C35 1.489(7) .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
C35 C36 1.515(7) .
C36 H36A 0.9800 .
C36 H36B 0.9800 .
C36 H36C 0.9800 .
C37 C38 1.461(10) .
C37 H37A 0.9800 .
C37 H37B 0.9800 .
C37 H37C 0.9800 .
C38 C39 1.461(8) .
C39 H39A 0.9800 .
C39 H39B 0.9800 .
C39 H39C 0.9800 .
C40 C41 1.534(12) .
C40 H40A 0.9800 .
C40 H40B 0.9800 .
C40 H40C 0.9800 .
C41 C42 1.559(11) .
C42 H42A 0.9800 .
C42 H42B 0.9800 .
C42 H42C 0.9800 .
B1 B7 1.734(5) .
B1 B2 1.751(5) .
B1 B6 1.758(5) .
B1 H1A 1.1200 .
B2 B8 1.774(5) .
B2 B7 1.791(5) .
B2 B3 1.803(5) .
B2 H2A 1.1200 .
B3 B8 1.790(5) .
B3 B4 1.793(5) .
B3 H3B 1.1200 .
B4 B5 1.773(5) .
B4 B9 1.784(5) .
B4 B8 1.790(5) .
B4 H4A 1.1200 .
B5 B6 1.765(6) .
B5 B9 1.775(5) .
B5 H5A 1.1200 .
B6 B7 1.774(5) .
B6 B9 1.777(5) .
B6 H6 1.1200 .
B7 B8 1.778(5) .
B7 B9 1.791(5) .
B7 H7 1.1200 .
B8 B9 1.785(5) .
B8 H8B 1.1200 .
B10 B11 1.708(5) .
B10 B14 1.741(5) .
B10 B15 1.742(5) .
B10 H10A 1.1200 .
B11 B16 1.739(5) .
B11 B15 1.758(5) .
B11 B12 1.768(5) .
B11 H11 1.1200 .
B12 B17 1.777(6) .
B12 B16 1.798(5) .
B12 H12A 1.1200 .
B13 B18 1.778(5) .
B13 B14 1.779(6) .
B13 B17 1.783(6) .
B13 H13 1.1200 .
B14 B15 1.776(5) .
B14 B18 1.781(5) .
B14 H14 1.1200 .
B15 B16 1.770(5) .
B15 B18 1.785(5) .
B15 H15 1.1200 .
B16 B17 1.772(6) .
B16 B18 1.784(6) .
B16 H16 1.1200 .
B17 B18 1.777(5) .
B17 H17 1.1200 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O4 Cs1 O7 C24 177.5(4) 1_554 .
O10 Cs1 O7 C24 -95.5(4) . .
O11 Cs1 O7 C24 9.3(4) . .
O6 Cs1 O7 C24 96.6(4) 1_455 .
O9 Cs1 O7 C24 -37.4(4) . .
O6 Cs1 O7 C24 31.8(4) 2_756 .
O15 Cs1 O7 C24 151.9(4) . .
C23 Cs1 O7 C24 113.0(4) 1_455 .
Cs1 Cs1 O7 C24 62.4(4) 2_656 .
O7 Cs1 O9 C26 -178.7(3) . .
O4 Cs1 O9 C26 -84.4(3) 1_554 .
O10 Cs1 O9 C26 -50.7(3) . .
O11 Cs1 O9 C26 36.9(3) . .
O6 Cs1 O9 C26 79.3(3) 1_455 .
O6 Cs1 O9 C26 101.3(3) 2_756 .
O15 Cs1 O9 C26 -170.1(3) . .
C23 Cs1 O9 C26 96.2(3) 1_455 .
Cs1 Cs1 O9 C26 92.3(3) 2_656 .
O7 Cs1 O10 C29 -13.6(5) . .
O4 Cs1 O10 C29 98.6(5) 1_554 .
O11 Cs1 O10 C29 -143.9(5) . .
O6 Cs1 O10 C29 153.3(5) 1_455 .
O9 Cs1 O10 C29 -64.3(5) . .
O6 Cs1 O10 C29 -98.1(5) 2_756 .
O15 Cs1 O10 C29 50.0(6) . .
C23 Cs1 O10 C29 133.6(5) 1_455 .
Cs1 Cs1 O10 C29 -154.1(5) 2_656 .
O7 Cs1 O11 C32 -155.0(4) . .
O4 Cs1 O11 C32 36.8(4) 1_554 .
O10 Cs1 O11 C32 -36.3(4) . .
O6 Cs1 O11 C32 93.7(4) 1_455 .
O9 Cs1 O11 C32 -113.8(4) . .
O6 Cs1 O11 C32 -179.0(4) 2_756 .
O15 Cs1 O11 C32 119.8(4) . .
C23 Cs1 O11 C32 89.5(4) 1_455 .
Cs1 Cs1 O11 C32 136.7(4) 2_656 .
C4 Co1 C1 C2 -55.0(3) . .
C3 Co1 C1 C2 148(3) . .
B10 Co1 C1 C2 -91.66(19) . .
B1 Co1 C1 C2 36.21(18) . .
B11 Co1 C1 C2 -140.46(19) . .
B3 Co1 C1 C2 126.0(2) . .
B12 Co1 C1 C2 177.82(18) . .
B2 Co1 C1 C2 85.92(19) . .
C2 Co1 C1 B4 -97.1(3) . .
C4 Co1 C1 B4 -152.1(3) . .
C3 Co1 C1 B4 51(3) . .
B10 Co1 C1 B4 171.3(3) . .
B1 Co1 C1 B4 -60.9(3) . .
B11 Co1 C1 B4 122.5(3) . .
B3 Co1 C1 B4 28.9(2) . .
B12 Co1 C1 B4 80.7(3) . .
B2 Co1 C1 B4 -11.2(3) . .
C2 Co1 C1 B3 -126.0(2) . .
C4 Co1 C1 B3 178.9(2) . .
C3 Co1 C1 B3 22(3) . .
B10 Co1 C1 B3 142.33(18) . .
B1 Co1 C1 B3 -89.80(19) . .
B11 Co1 C1 B3 93.52(19) . .
B12 Co1 C1 B3 51.8(2) . .
B2 Co1 C1 B3 -40.10(19) . .
C2 Co1 C1 B5 -23.5(2) . .
C4 Co1 C1 B5 -78.5(3) . .
C3 Co1 C1 B5 125(3) . .
B10 Co1 C1 B5 -115.1(3) . .
B1 Co1 C1 B5 12.7(3) . .
B11 Co1 C1 B5 -163.9(3) . .
B3 Co1 C1 B5 102.6(3) . .
B12 Co1 C1 B5 154.4(2) . .
B2 Co1 C1 B5 62.5(3) . .
B4 C1 C2 B1 66.5(3) . .
B3 C1 C2 B1 0.5(3) . .
B5 C1 C2 B1 105.9(3) . .
Co1 C1 C2 B1 -51.0(2) . .
B4 C1 C2 B6 -1.6(3) . .
B3 C1 C2 B6 -67.6(3) . .
B5 C1 C2 B6 37.8(3) . .
Co1 C1 C2 B6 -119.1(2) . .
B4 C1 C2 B5 -39.4(2) . .
B3 C1 C2 B5 -105.4(3) . .
Co1 C1 C2 B5 -156.9(2) . .
B4 C1 C2 Co1 117.5(2) . .
B3 C1 C2 Co1 51.5(2) . .
B5 C1 C2 Co1 156.9(2) . .
C4 Co1 C2 C1 143.37(19) . .
C3 Co1 C2 C1 -177.5(2) . .
B10 Co1 C2 C1 94.7(2) . .
B1 Co1 C2 C1 -128.0(3) . .
B11 Co1 C2 C1 54.5(3) . .
B3 Co1 C2 C1 -38.34(19) . .
B12 Co1 C2 C1 -20.7(17) . .
B2 Co1 C2 C1 -89.45(19) . .
C4 Co1 C2 B1 -88.6(2) . .
C1 Co1 C2 B1 128.0(2) . .
C3 Co1 C2 B1 -49.5(3) . .
B10 Co1 C2 B1 -137.34(19) . .
B11 Co1 C2 B1 -177.5(2) . .
B3 Co1 C2 B1 89.66(19) . .
B12 Co1 C2 B1 107.3(16) . .
B2 Co1 C2 B1 38.55(19) . .
C4 Co1 C2 B6 -114.2(3) . .
C1 Co1 C2 B6 102.4(3) . .
C3 Co1 C2 B6 -75.1(3) . .
B10 Co1 C2 B6 -163.0(3) . .
B1 Co1 C2 B6 -25.6(2) . .
B11 Co1 C2 B6 156.9(3) . .
B3 Co1 C2 B6 64.0(3) . .
B12 Co1 C2 B6 81.7(17) . .
B2 Co1 C2 B6 12.9(3) . .
C4 Co1 C2 B5 168.2(3) . .
C1 Co1 C2 B5 24.9(2) . .
C3 Co1 C2 B5 -152.7(3) . .
B10 Co1 C2 B5 119.5(3) . .
B1 Co1 C2 B5 -103.1(3) . .
B11 Co1 C2 B5 79.4(3) . .
B3 Co1 C2 B5 -13.5(3) . .
B12 Co1 C2 B5 4.1(18) . .
B2 Co1 C2 B5 -64.6(3) . .
C2 Co1 C3 C4 -55.6(3) . .
C1 Co1 C3 C4 158(3) . .
B10 Co1 C3 C4 37.4(2) . .
B1 Co1 C3 C4 -90.4(2) . .
B11 Co1 C3 C4 86.3(2) . .
B3 Co1 C3 C4 179.1(2) . .
B12 Co1 C3 C4 127.0(3) . .
B2 Co1 C3 C4 -140.0(2) . .
C2 Co1 C3 B17 -152.9(3) . .
C4 Co1 C3 B17 -97.4(3) . .
C1 Co1 C3 B17 61(3) . .
B10 Co1 C3 B17 -59.9(3) . .
B1 Co1 C3 B17 172.2(3) . .
B11 Co1 C3 B17 -11.1(3) . .
B3 Co1 C3 B17 81.8(3) . .
B12 Co1 C3 B17 29.6(3) . .
B2 Co1 C3 B17 122.7(3) . .
C2 Co1 C3 B12 177.47(19) . .
C4 Co1 C3 B12 -127.0(3) . .
C1 Co1 C3 B12 31(3) . .
B10 Co1 C3 B12 -89.5(2) . .
B1 Co1 C3 B12 142.6(2) . .
B11 Co1 C3 B12 -40.66(19) . .
B3 Co1 C3 B12 52.2(3) . .
B2 Co1 C3 B12 93.1(2) . .
C2 Co1 C3 B13 -80.1(4) . .
C4 Co1 C3 B13 -24.6(3) . .
C1 Co1 C3 B13 133(3) . .
B10 Co1 C3 B13 12.9(3) . .
B1 Co1 C3 B13 -115.0(3) . .
B11 Co1 C3 B13 61.7(3) . .
B3 Co1 C3 B13 154.6(3) . .
B12 Co1 C3 B13 102.4(4) . .
B2 Co1 C3 B13 -164.5(3) . .
B17 C3 C4 B10 64.8(3) . .
B12 C3 C4 B10 -0.6(4) . .
B13 C3 C4 B10 104.0(3) . .
Co1 C3 C4 B10 -51.6(2) . .
B17 C3 C4 B14 -0.8(4) . .
B12 C3 C4 B14 -66.2(3) . .
B13 C3 C4 B14 38.4(3) . .
Co1 C3 C4 B14 -117.2(3) . .
B17 C3 C4 B13 -39.2(3) . .
B12 C3 C4 B13 -104.6(3) . .
Co1 C3 C4 B13 -155.7(3) . .
B17 C3 C4 Co1 116.4(3) . .
B12 C3 C4 Co1 51.0(2) . .
B13 C3 C4 Co1 155.7(3) . .
C2 Co1 C4 B10 -90.4(2) . .
C1 Co1 C4 B10 -52.3(3) . .
C3 Co1 C4 B10 125.9(3) . .
B1 Co1 C4 B10 -138.8(2) . .
B11 Co1 C4 B10 38.0(2) . .
B3 Co1 C4 B10 116(2) . .
B12 Co1 C4 B10 88.3(2) . .
B2 Co1 C4 B10 -179.91(18) . .
C2 Co1 C4 C3 143.7(2) . .
C1 Co1 C4 C3 -178.3(2) . .
B10 Co1 C4 C3 -125.9(3) . .
B1 Co1 C4 C3 95.3(2) . .
B11 Co1 C4 C3 -87.9(2) . .
B3 Co1 C4 C3 -10(2) . .
B12 Co1 C4 C3 -37.6(2) . .
B2 Co1 C4 C3 54.2(3) . .
C2 Co1 C4 B14 -116.1(3) . .
C1 Co1 C4 B14 -78.0(4) . .
C3 Co1 C4 B14 100.2(4) . .
B10 Co1 C4 B14 -25.7(3) . .
B1 Co1 C4 B14 -164.5(3) . .
B11 Co1 C4 B14 12.3(3) . .
B3 Co1 C4 B14 90(2) . .
B12 Co1 C4 B14 62.6(3) . .
B2 Co1 C4 B14 154.4(3) . .
C2 Co1 C4 B13 169.1(3) . .
C1 Co1 C4 B13 -152.9(3) . .
C3 Co1 C4 B13 25.4(3) . .
B10 Co1 C4 B13 -100.5(3) . .
B1 Co1 C4 B13 120.7(3) . .
B11 Co1 C4 B13 -62.5(3) . .
B3 Co1 C4 B13 15(2) . .
B12 Co1 C4 B13 -12.2(3) . .
B2 Co1 C4 B13 79.6(3) . .
B9 C5 C6 C7 -78(19) . .
C5 C6 C7 C8 -159(5) . .
C5 C6 C7 C12 21(6) . .
C12 C7 C8 C9 0.1(5) . .
C6 C7 C8 C9 180.0(3) . .
C7 C8 C9 C10 0.2(5) . .
C7 C8 C9 C13 179.4(3) . .
C8 C9 C10 C11 -0.2(5) . .
C13 C9 C10 C11 -179.5(3) . .
C9 C10 C11 C12 0.1(5) . .
C9 C10 C11 C14 -179.2(3) . .
C10 C11 C12 C7 0.2(5) . .
C14 C11 C12 C7 179.4(3) . .
C8 C7 C12 C11 -0.3(5) . .
C6 C7 C12 C11 179.8(3) . .
C10 C9 C13 O2 1.3(5) . .
C8 C9 C13 O2 -178.0(3) . .
C10 C9 C13 O1 -179.2(3) . .
C8 C9 C13 O1 1.5(5) . .
Cs1 O4 C14 O3 140.3(5) 1_556 .
Cs1 O4 C14 C11 -39.8(8) 1_556 .
C12 C11 C14 O4 -2.7(5) . .
C10 C11 C14 O4 176.5(3) . .
C12 C11 C14 O3 177.2(3) . .
C10 C11 C14 O3 -3.6(4) . .
B18 C15 C16 C17 94(31) . .
C15 C16 C17 C22 64(17) . .
C15 C16 C17 C18 -115(17) . .
C22 C17 C18 C19 -1.0(5) . .
C16 C17 C18 C19 178.0(3) . .
C17 C18 C19 C20 -0.6(5) . .
C17 C18 C19 C23 179.3(3) . .
C18 C19 C20 C21 1.4(5) . .
C23 C19 C20 C21 -178.4(3) . .
C19 C20 C21 C22 -0.6(5) . .
C19 C20 C21 C24 178.1(3) . .
C20 C21 C22 C17 -1.0(5) . .
C24 C21 C22 C17 -179.8(3) . .
C18 C17 C22 C21 1.9(5) . .
C16 C17 C22 C21 -177.2(3) . .
Cs1 O6 C23 O5 -71.9(4) 1_655 .
Cs1 O6 C23 O5 51.1(4) 2_756 .
Cs1 O6 C23 C19 107.6(3) 1_655 .
Cs1 O6 C23 C19 -129.5(3) 2_756 .
Cs1 O6 C23 Cs1 123.0(3) 2_756 1_655
C20 C19 C23 O6 -4.1(5) . .
C18 C19 C23 O6 176.0(3) . .
C20 C19 C23 O5 175.4(3) . .
C18 C19 C23 O5 -4.5(5) . .
C20 C19 C23 Cs1 50.7(4) . 1_655
C18 C19 C23 Cs1 -129.2(3) . 1_655
Cs1 O7 C24 O8 35.4(6) . .
Cs1 O7 C24 C21 -145.5(3) . .
C22 C21 C24 O7 1.4(5) . .
C20 C21 C24 O7 -177.4(3) . .
C22 C21 C24 O8 -179.5(3) . .
C20 C21 C24 O8 1.7(5) . .
Cs1 O9 C26 C27 7.7(5) . .
Cs1 O9 C26 C25 -171.1(3) . .
Cs1 O10 C29 C30 -126.2(5) . .
Cs1 O10 C29 C28 53.3(7) . .
Cs1 O11 C32 C31 148.0(3) . .
Cs1 O11 C32 C33 -31.9(6) . .
C1 C2 B1 B7 -66.2(3) . .
B6 C2 B1 B7 39.3(2) . .
B5 C2 B1 B7 1.8(4) . .
Co1 C2 B1 B7 -117.0(2) . .
C1 C2 B1 B2 -0.9(3) . .
B6 C2 B1 B2 104.6(3) . .
B5 C2 B1 B2 67.1(3) . .
Co1 C2 B1 B2 -51.7(2) . .
C1 C2 B1 B6 -105.5(3) . .
B5 C2 B1 B6 -37.5(3) . .
Co1 C2 B1 B6 -156.3(2) . .
C1 C2 B1 Co1 50.8(2) . .
B6 C2 B1 Co1 156.3(2) . .
B5 C2 B1 Co1 118.8(3) . .
C4 Co1 B1 C2 97.83(19) . .
C1 Co1 B1 C2 -36.02(18) . .
C3 Co1 B1 C2 147.11(19) . .
B10 Co1 B1 C2 59.0(2) . .
B11 Co1 B1 C2 34(3) . .
B3 Co1 B1 C2 -85.92(19) . .
B12 Co1 B1 C2 -173.6(2) . .
B2 Co1 B1 C2 -125.4(2) . .
C2 Co1 B1 B7 95.8(3) . .
C4 Co1 B1 B7 -166.3(3) . .
C1 Co1 B1 B7 59.8(3) . .
C3 Co1 B1 B7 -117.0(3) . .
B10 Co1 B1 B7 154.9(2) . .
B11 Co1 B1 B7 130(3) . .
B3 Co1 B1 B7 9.9(3) . .
B12 Co1 B1 B7 -77.7(3) . .
B2 Co1 B1 B7 -29.6(2) . .
C2 Co1 B1 B2 125.4(2) . .
C4 Co1 B1 B2 -136.75(19) . .
C1 Co1 B1 B2 89.40(19) . .
C3 Co1 B1 B2 -87.47(19) . .
B10 Co1 B1 B2 -175.54(18) . .
B11 Co1 B1 B2 159(3) . .
B3 Co1 B1 B2 39.50(18) . .
B12 Co1 B1 B2 -48.2(3) . .
C2 Co1 B1 B6 23.5(2) . .
C4 Co1 B1 B6 121.3(3) . .
C1 Co1 B1 B6 -12.5(3) . .
C3 Co1 B1 B6 170.6(3) . .
B10 Co1 B1 B6 82.6(3) . .
B11 Co1 B1 B6 57(3) . .
B3 Co1 B1 B6 -62.4(3) . .
B12 Co1 B1 B6 -150.1(2) . .
B2 Co1 B1 B6 -101.9(3) . .
C2 B1 B2 B8 -61.7(3) . .
B7 B1 B2 B8 38.8(2) . .
B6 B1 B2 B8 1.7(3) . .
Co1 B1 B2 B8 -112.7(2) . .
C2 B1 B2 B7 -100.5(3) . .
B6 B1 B2 B7 -37.0(2) . .
Co1 B1 B2 B7 -151.4(2) . .
C2 B1 B2 B3 0.9(3) . .
B7 B1 B2 B3 101.4(3) . .
B6 B1 B2 B3 64.4(3) . .
Co1 B1 B2 B3 -50.02(19) . .
C2 B1 B2 Co1 51.0(2) . .
B7 B1 B2 Co1 151.4(2) . .
B6 B1 B2 Co1 114.4(2) . .
C2 Co1 B2 B1 -37.65(18) . .
C4 Co1 B2 B1 59.4(2) . .
C1 Co1 B2 B1 -85.74(19) . .
C3 Co1 B2 B1 97.2(2) . .
B10 Co1 B2 B1 58(2) . .
B11 Co1 B2 B1 -178.3(2) . .
B3 Co1 B2 B1 -125.1(2) . .
B12 Co1 B2 B1 146.92(19) . .
C2 Co1 B2 B8 57.4(2) . .
C4 Co1 B2 B8 154.5(2) . .
C1 Co1 B2 B8 9.3(2) . .
C3 Co1 B2 B8 -167.7(3) . .
B10 Co1 B2 B8 153.5(19) . .
B1 Co1 B2 B8 95.1(3) . .
B11 Co1 B2 B8 -83.2(3) . .
B3 Co1 B2 B8 -30.0(2) . .
B12 Co1 B2 B8 -118.0(3) . .
C2 Co1 B2 B7 -10.5(2) . .
C4 Co1 B2 B7 86.6(3) . .
C1 Co1 B2 B7 -58.6(2) . .
C3 Co1 B2 B7 124.4(3) . .
B10 Co1 B2 B7 86(2) . .
B1 Co1 B2 B7 27.2(2) . .
B11 Co1 B2 B7 -151.1(2) . .
B3 Co1 B2 B7 -97.9(3) . .
B12 Co1 B2 B7 174.1(2) . .
C2 Co1 B2 B3 87.43(18) . .
C4 Co1 B2 B3 -175.5(2) . .
C1 Co1 B2 B3 39.34(18) . .
C3 Co1 B2 B3 -137.7(2) . .
B10 Co1 B2 B3 -176(32) . .
B1 Co1 B2 B3 125.1(2) . .
B11 Co1 B2 B3 -53.2(3) . .
B12 Co1 B2 B3 -88.00(19) . .
C2 C1 B3 B8 61.7(3) . .
B4 C1 B3 B8 -39.5(2) . .
B5 C1 B3 B8 -2.9(3) . .
Co1 C1 B3 B8 112.9(2) . .
C2 C1 B3 B4 101.2(3) . .
B5 C1 B3 B4 36.6(3) . .
Co1 C1 B3 B4 152.3(2) . .
C2 C1 B3 B2 0.1(3) . .
B4 C1 B3 B2 -101.1(3) . .
B5 C1 B3 B2 -64.5(3) . .
Co1 C1 B3 B2 51.27(19) . .
C2 C1 B3 Co1 -51.2(2) . .
B4 C1 B3 Co1 -152.3(2) . .
B5 C1 B3 Co1 -115.8(3) . .
B1 B2 B3 C1 -0.6(3) . .
B8 B2 B3 C1 98.3(3) . .
B7 B2 B3 C1 60.9(3) . .
Co1 B2 B3 C1 -50.66(19) . .
B1 B2 B3 B8 -98.9(3) . .
B7 B2 B3 B8 -37.4(2) . .
Co1 B2 B3 B8 -149.0(2) . .
B1 B2 B3 B4 -61.9(3) . .
B8 B2 B3 B4 37.0(2) . .
B7 B2 B3 B4 -0.4(3) . .
Co1 B2 B3 B4 -112.0(2) . .
B1 B2 B3 Co1 50.04(19) . .
B8 B2 B3 Co1 149.0(2) . .
B7 B2 B3 Co1 111.6(2) . .
C2 Co1 B3 C1 37.10(18) . .
C4 Co1 B3 C1 -169(2) . .
C3 Co1 B3 C1 -178.4(2) . .
B10 Co1 B3 C1 -56.3(3) . .
B1 Co1 B3 C1 85.46(19) . .
B11 Co1 B3 C1 -91.47(19) . .
B12 Co1 B3 C1 -141.42(19) . .
B2 Co1 B3 C1 124.1(2) . .
C2 Co1 B3 B8 -57.2(2) . .
C4 Co1 B3 B8 97(2) . .
C1 Co1 B3 B8 -94.3(3) . .
C3 Co1 B3 B8 87.2(3) . .
B10 Co1 B3 B8 -150.6(2) . .
B1 Co1 B3 B8 -8.9(2) . .
B11 Co1 B3 B8 174.2(2) . .
B12 Co1 B3 B8 124.2(2) . .
B2 Co1 B3 B8 29.7(2) . .
C2 Co1 B3 B4 10.8(2) . .
C4 Co1 B3 B4 165(2) . .
C1 Co1 B3 B4 -26.3(2) . .
C3 Co1 B3 B4 155.3(2) . .
B10 Co1 B3 B4 -82.6(3) . .
B1 Co1 B3 B4 59.1(2) . .
B11 Co1 B3 B4 -117.8(3) . .
B12 Co1 B3 B4 -167.7(2) . .
B2 Co1 B3 B4 97.7(3) . .
C2 Co1 B3 B2 -86.97(18) . .
C4 Co1 B3 B2 67(2) . .
C1 Co1 B3 B2 -124.1(2) . .
C3 Co1 B3 B2 57.5(2) . .
B10 Co1 B3 B2 179.65(19) . .
B1 Co1 B3 B2 -38.61(17) . .
B11 Co1 B3 B2 144.47(18) . .
B12 Co1 B3 B2 94.51(19) . .
C2 C1 B4 B5 38.8(2) . .
B3 C1 B4 B5 141.1(3) . .
Co1 C1 B4 B5 111.0(3) . .
C2 C1 B4 B9 0.0(3) . .
B3 C1 B4 B9 102.3(3) . .
B5 C1 B4 B9 -38.8(2) . .
Co1 C1 B4 B9 72.2(3) . .
C2 C1 B4 B8 -62.6(3) . .
B3 C1 B4 B8 39.6(2) . .
B5 C1 B4 B8 -101.5(3) . .
Co1 C1 B4 B8 9.6(4) . .
C2 C1 B4 B3 -102.3(3) . .
B5 C1 B4 B3 -141.1(3) . .
Co1 C1 B4 B3 -30.1(2) . .
B8 B3 B4 C1 134.8(3) . .
B2 B3 B4 C1 98.1(3) . .
Co1 B3 B4 C1 27.9(2) . .
C1 B3 B4 B5 -35.0(3) . .
B8 B3 B4 B5 99.8(3) . .
B2 B3 B4 B5 63.1(3) . .
Co1 B3 B4 B5 -7.2(3) . .
C1 B3 B4 B9 -98.6(3) . .
B8 B3 B4 B9 36.2(2) . .
B2 B3 B4 B9 -0.5(3) . .
Co1 B3 B4 B9 -70.7(3) . .
C1 B3 B4 B8 -134.8(3) . .
B2 B3 B4 B8 -36.7(2) . .
Co1 B3 B4 B8 -106.9(3) . .
B1 C2 B5 C1 -102.7(3) . .
B6 C2 B5 C1 -140.4(3) . .
Co1 C2 B5 C1 -25.8(2) . .
C1 C2 B5 B6 140.4(3) . .
B1 C2 B5 B6 37.6(3) . .
Co1 C2 B5 B6 114.6(3) . .
C1 C2 B5 B4 37.3(2) . .
B1 C2 B5 B4 -65.4(3) . .
B6 C2 B5 B4 -103.0(3) . .
Co1 C2 B5 B4 11.6(4) . .
C1 C2 B5 B9 100.0(3) . .
B1 C2 B5 B9 -2.8(4) . .
B6 C2 B5 B9 -40.4(2) . .
Co1 C2 B5 B9 74.2(3) . .
B4 C1 B5 C2 136.6(3) . .
B3 C1 B5 C2 99.7(3) . .
Co1 C1 B5 C2 24.7(2) . .
C2 C1 B5 B6 -34.6(2) . .
B4 C1 B5 B6 102.0(3) . .
B3 C1 B5 B6 65.1(3) . .
Co1 C1 B5 B6 -9.9(4) . .
C2 C1 B5 B4 -136.6(3) . .
B3 C1 B5 B4 -36.9(3) . .
Co1 C1 B5 B4 -111.9(3) . .
C2 C1 B5 B9 -97.6(3) . .
B4 C1 B5 B9 39.0(2) . .
B3 C1 B5 B9 2.1(4) . .
Co1 C1 B5 B9 -72.9(3) . .
C1 B4 B5 C2 -36.7(2) . .
B9 B4 B5 C2 99.3(3) . .
B8 B4 B5 C2 61.5(3) . .
B3 B4 B5 C2 -1.9(3) . .
B9 B4 B5 C1 136.0(3) . .
B8 B4 B5 C1 98.2(3) . .
B3 B4 B5 C1 34.8(2) . .
C1 B4 B5 B6 -98.1(3) . .
B9 B4 B5 B6 37.9(2) . .
B8 B4 B5 B6 0.1(3) . .
B3 B4 B5 B6 -63.3(3) . .
C1 B4 B5 B9 -136.0(3) . .
B8 B4 B5 B9 -37.8(2) . .
B3 B4 B5 B9 -101.2(3) . .
C1 C2 B6 B1 102.9(3) . .
B5 C2 B6 B1 140.8(3) . .
Co1 C2 B6 B1 26.6(2) . .
C1 C2 B6 B5 -37.9(3) . .
B1 C2 B6 B5 -140.8(3) . .
Co1 C2 B6 B5 -114.2(3) . .
C1 C2 B6 B7 65.3(3) . .
B1 C2 B6 B7 -37.6(2) . .
B5 C2 B6 B7 103.2(3) . .
Co1 C2 B6 B7 -11.0(4) . .
C1 C2 B6 B9 2.4(3) . .
B1 C2 B6 B9 -100.5(3) . .
B5 C2 B6 B9 40.3(2) . .
Co1 C2 B6 B9 -73.9(3) . .
B7 B1 B6 C2 -136.3(3) . .
B2 B1 B6 C2 -99.0(3) . .
Co1 B1 B6 C2 -24.8(2) . .
C2 B1 B6 B5 34.5(2) . .
B7 B1 B6 B5 -101.9(3) . .
B2 B1 B6 B5 -64.5(3) . .
Co1 B1 B6 B5 9.7(4) . .
C2 B1 B6 B7 136.3(3) . .
B2 B1 B6 B7 37.4(2) . .
Co1 B1 B6 B7 111.5(3) . .
C2 B1 B6 B9 97.6(3) . .
B7 B1 B6 B9 -38.8(3) . .
B2 B1 B6 B9 -1.4(4) . .
Co1 B1 B6 B9 72.8(3) . .
C1 B5 B6 C2 34.1(2) . .
B4 B5 B6 C2 95.9(3) . .
B9 B5 B6 C2 133.9(3) . .
C2 B5 B6 B1 -34.1(2) . .
C1 B5 B6 B1 0.0(3) . .
B4 B5 B6 B1 61.9(3) . .
B9 B5 B6 B1 99.8(3) . .
C2 B5 B6 B7 -96.1(3) . .
C1 B5 B6 B7 -62.1(3) . .
B4 B5 B6 B7 -0.2(3) . .
B9 B5 B6 B7 37.8(2) . .
C2 B5 B6 B9 -133.9(3) . .
C1 B5 B6 B9 -99.8(3) . .
B4 B5 B6 B9 -38.0(2) . .
C2 B1 B7 B6 -38.5(2) . .
B2 B1 B7 B6 -140.2(3) . .
Co1 B1 B7 B6 -109.3(3) . .
C2 B1 B7 B8 62.9(3) . .
B2 B1 B7 B8 -38.8(2) . .
B6 B1 B7 B8 101.4(3) . .
Co1 B1 B7 B8 -7.9(3) . .
C2 B1 B7 B9 0.0(3) . .
B2 B1 B7 B9 -101.6(3) . .
B6 B1 B7 B9 38.5(2) . .
Co1 B1 B7 B9 -70.8(3) . .
C2 B1 B7 B2 101.6(3) . .
B6 B1 B7 B2 140.2(3) . .
Co1 B1 B7 B2 30.8(2) . .
C2 B6 B7 B1 37.2(2) . .
B5 B6 B7 B1 98.9(3) . .
B9 B6 B7 B1 136.5(3) . .
C2 B6 B7 B8 -61.5(3) . .
B1 B6 B7 B8 -98.7(3) . .
B5 B6 B7 B8 0.2(3) . .
B9 B6 B7 B8 37.7(2) . .
C2 B6 B7 B9 -99.2(3) . .
B1 B6 B7 B9 -136.5(3) . .
B5 B6 B7 B9 -37.6(2) . .
C2 B6 B7 B2 1.6(3) . .
B1 B6 B7 B2 -35.7(2) . .
B5 B6 B7 B2 63.2(3) . .
B9 B6 B7 B2 100.8(3) . .
B8 B2 B7 B1 -135.7(3) . .
B3 B2 B7 B1 -98.2(3) . .
Co1 B2 B7 B1 -28.8(2) . .
B1 B2 B7 B6 35.9(2) . .
B8 B2 B7 B6 -99.8(3) . .
B3 B2 B7 B6 -62.3(3) . .
Co1 B2 B7 B6 7.1(3) . .
B1 B2 B7 B8 135.7(3) . .
B3 B2 B7 B8 37.5(2) . .
Co1 B2 B7 B8 107.0(3) . .
B1 B2 B7 B9 99.4(3) . .
B8 B2 B7 B9 -36.4(2) . .
B3 B2 B7 B9 1.1(3) . .
Co1 B2 B7 B9 70.6(3) . .
B1 B2 B8 B7 -38.2(2) . .
B3 B2 B8 B7 -138.0(3) . .
Co1 B2 B8 B7 -106.7(3) . .
B1 B2 B8 B9 -1.4(3) . .
B7 B2 B8 B9 36.8(2) . .
B3 B2 B8 B9 -101.2(3) . .
Co1 B2 B8 B9 -69.9(3) . .
B1 B2 B8 B4 62.4(3) . .
B7 B2 B8 B4 100.6(3) . .
B3 B2 B8 B4 -37.5(2) . .
Co1 B2 B8 B4 -6.1(3) . .
B1 B2 B8 B3 99.8(3) . .
B7 B2 B8 B3 138.0(3) . .
Co1 B2 B8 B3 31.3(2) . .
B1 B7 B8 B2 38.7(2) . .
B6 B7 B8 B2 101.8(3) . .
B9 B7 B8 B2 139.5(3) . .
B1 B7 B8 B9 -100.7(3) . .
B6 B7 B8 B9 -37.7(2) . .
B2 B7 B8 B9 -139.5(3) . .
B1 B7 B8 B4 -63.2(3) . .
B6 B7 B8 B4 -0.1(3) . .
B9 B7 B8 B4 37.6(2) . .
B2 B7 B8 B4 -101.9(3) . .
B1 B7 B8 B3 0.6(3) . .
B6 B7 B8 B3 63.7(3) . .
B9 B7 B8 B3 101.3(3) . .
B2 B7 B8 B3 -38.1(2) . .
C1 B4 B8 B2 -1.6(3) . .
B5 B4 B8 B2 -64.2(3) . .
B9 B4 B8 B2 -102.0(3) . .
B3 B4 B8 B2 37.7(2) . .
C1 B4 B8 B7 62.6(3) . .
B5 B4 B8 B7 0.0(3) . .
B9 B4 B8 B7 -37.8(2) . .
B3 B4 B8 B7 101.9(3) . .
C1 B4 B8 B9 100.4(3) . .
B5 B4 B8 B9 37.8(2) . .
B3 B4 B8 B9 139.7(3) . .
C1 B4 B8 B3 -39.3(2) . .
B5 B4 B8 B3 -102.0(3) . .
B9 B4 B8 B3 -139.7(3) . .
C1 B3 B8 B2 -99.6(3) . .
B4 B3 B8 B2 -138.4(3) . .
Co1 B3 B8 B2 -31.6(2) . .
C1 B3 B8 B7 -61.6(3) . .
B4 B3 B8 B7 -100.4(3) . .
B2 B3 B8 B7 38.0(2) . .
Co1 B3 B8 B7 6.5(3) . .
C1 B3 B8 B9 2.6(3) . .
B4 B3 B8 B9 -36.2(2) . .
B2 B3 B8 B9 102.2(3) . .
Co1 B3 B8 B9 70.6(3) . .
C1 B3 B8 B4 38.8(2) . .
B2 B3 B8 B4 138.4(3) . .
Co1 B3 B8 B4 106.9(3) . .
C6 C5 B9 B5 8(17) . .
C6 C5 B9 B6 80(17) . .
C6 C5 B9 B4 -62(17) . .
C6 C5 B9 B8 -135(17) . .
C6 C5 B9 B7 152(17) . .
C2 B5 B9 C5 151.4(3) . .
C1 B5 B9 C5 -148.7(3) . .
B6 B5 B9 C5 111.8(3) . .
B4 B5 B9 C5 -110.4(4) . .
C2 B5 B9 B6 39.6(2) . .
C1 B5 B9 B6 99.5(3) . .
B4 B5 B9 B6 137.8(3) . .
C2 B5 B9 B4 -98.2(3) . .
C1 B5 B9 B4 -38.3(2) . .
B6 B5 B9 B4 -137.8(3) . .
C2 B5 B9 B8 -60.3(3) . .
C1 B5 B9 B8 -0.3(3) . .
B6 B5 B9 B8 -99.9(3) . .
B4 B5 B9 B8 37.9(2) . .
C2 B5 B9 B7 2.6(3) . .
C1 B5 B9 B7 62.5(3) . .
B6 B5 B9 B7 -37.0(2) . .
B4 B5 B9 B7 100.8(3) . .
C2 B6 B9 C5 -148.8(3) . .
B1 B6 B9 C5 150.7(3) . .
B5 B6 B9 C5 -109.1(3) . .
B7 B6 B9 C5 112.7(3) . .
C2 B6 B9 B5 -39.7(2) . .
B1 B6 B9 B5 -100.2(3) . .
B7 B6 B9 B5 -138.2(3) . .
C2 B6 B9 B4 -2.3(3) . .
B1 B6 B9 B4 -62.8(3) . .
B5 B6 B9 B4 37.4(2) . .
B7 B6 B9 B4 -100.8(3) . .
C2 B6 B9 B8 61.0(3) . .
B1 B6 B9 B8 0.5(3) . .
B5 B6 B9 B8 100.7(3) . .
B7 B6 B9 B8 -37.5(2) . .
C2 B6 B9 B7 98.5(3) . .
B1 B6 B9 B7 38.0(2) . .
B5 B6 B9 B7 138.2(3) . .
C1 B4 B9 C5 148.4(3) . .
B5 B4 B9 C5 109.6(3) . .
B8 B4 B9 C5 -112.8(3) . .
B3 B4 B9 C5 -149.1(3) . .
C1 B4 B9 B5 38.8(2) . .
B8 B4 B9 B5 137.5(3) . .
B3 B4 B9 B5 101.3(3) . .
C1 B4 B9 B6 1.5(3) . .
B5 B4 B9 B6 -37.3(2) . .
B8 B4 B9 B6 100.2(3) . .
B3 B4 B9 B6 64.0(3) . .
C1 B4 B9 B8 -98.7(3) . .
B5 B4 B9 B8 -137.5(3) . .
B3 B4 B9 B8 -36.2(2) . .
C1 B4 B9 B7 -61.3(3) . .
B5 B4 B9 B7 -100.1(3) . .
B8 B4 B9 B7 37.4(2) . .
B3 B4 B9 B7 1.2(3) . .
B2 B8 B9 C5 -149.3(3) . .
B7 B8 B9 C5 -112.4(4) . .
B4 B8 B9 C5 109.7(4) . .
B3 B8 B9 C5 146.0(3) . .
B2 B8 B9 B5 63.3(3) . .
B7 B8 B9 B5 100.2(3) . .
B4 B8 B9 B5 -37.7(2) . .
B3 B8 B9 B5 -1.4(3) . .
B2 B8 B9 B6 0.6(3) . .
B7 B8 B9 B6 37.5(2) . .
B4 B8 B9 B6 -100.5(3) . .
B3 B8 B9 B6 -64.1(3) . .
B2 B8 B9 B4 101.0(3) . .
B7 B8 B9 B4 137.9(3) . .
B3 B8 B9 B4 36.3(2) . .
B2 B8 B9 B7 -36.9(2) . .
B4 B8 B9 B7 -137.9(3) . .
B3 B8 B9 B7 -101.6(3) . .
B1 B7 B9 C5 -149.3(3) . .
B6 B7 B9 C5 -110.7(4) . .
B8 B7 B9 C5 111.7(4) . .
B2 B7 B9 C5 147.9(3) . .
B1 B7 B9 B5 -1.6(3) . .
B6 B7 B9 B5 37.0(2) . .
B8 B7 B9 B5 -100.6(3) . .
B2 B7 B9 B5 -64.4(3) . .
B1 B7 B9 B6 -38.7(2) . .
B8 B7 B9 B6 -137.6(3) . .
B2 B7 B9 B6 -101.4(3) . .
B1 B7 B9 B4 61.4(3) . .
B6 B7 B9 B4 100.0(3) . .
B8 B7 B9 B4 -37.6(2) . .
B2 B7 B9 B4 -1.4(3) . .
B1 B7 B9 B8 99.0(3) . .
B6 B7 B9 B8 137.6(3) . .
B2 B7 B9 B8 36.2(2) . .
C3 C4 B10 B11 -0.5(4) . .
B14 C4 B10 B11 103.7(3) . .
B13 C4 B10 B11 65.5(4) . .
Co1 C4 B10 B11 -51.7(2) . .
C3 C4 B10 B14 -104.2(3) . .
B13 C4 B10 B14 -38.2(3) . .
Co1 C4 B10 B14 -155.3(2) . .
C3 C4 B10 B15 -65.6(3) . .
B14 C4 B10 B15 38.6(3) . .
B13 C4 B10 B15 0.4(4) . .
Co1 C4 B10 B15 -116.8(2) . .
C3 C4 B10 Co1 51.2(2) . .
B14 C4 B10 Co1 155.3(2) . .
B13 C4 B10 Co1 117.2(3) . .
C2 Co1 B10 C4 96.7(2) . .
C1 Co1 B10 C4 145.0(2) . .
C3 Co1 B10 C4 -37.9(2) . .
B1 Co1 B10 C4 56.7(3) . .
B11 Co1 B10 C4 -125.3(3) . .
B3 Co1 B10 C4 -175.2(2) . .
B12 Co1 B10 C4 -87.7(2) . .
B2 Co1 B10 C4 1(2) . .
C2 Co1 B10 B11 -138.0(2) . .
C4 Co1 B10 B11 125.3(3) . .
C1 Co1 B10 B11 -89.7(2) . .
C3 Co1 B10 B11 87.4(2) . .
B1 Co1 B10 B11 -178.0(2) . .
B3 Co1 B10 B11 -49.9(3) . .
B12 Co1 B10 B11 37.6(2) . .
B2 Co1 B10 B11 126.4(19) . .
C2 Co1 B10 B14 121.8(3) . .
C4 Co1 B10 B14 25.1(3) . .
C1 Co1 B10 B14 170.0(3) . .
C3 Co1 B10 B14 -12.9(3) . .
B1 Co1 B10 B14 81.7(3) . .
B11 Co1 B10 B14 -100.3(3) . .
B3 Co1 B10 B14 -150.1(2) . .
B12 Co1 B10 B14 -62.7(3) . .
B2 Co1 B10 B14 26(2) . .
C2 Co1 B10 B15 -165.0(3) . .
C4 Co1 B10 B15 98.3(3) . .
C1 Co1 B10 B15 -116.7(3) . .
C3 Co1 B10 B15 60.4(3) . .
B1 Co1 B10 B15 155.0(2) . .
B11 Co1 B10 B15 -27.0(3) . .
B3 Co1 B10 B15 -76.9(3) . .
B12 Co1 B10 B15 10.6(3) . .
B2 Co1 B10 B15 99.4(19) . .
C4 B10 B11 B16 -64.2(3) . .
B14 B10 B11 B16 0.3(4) . .
B15 B10 B11 B16 38.4(3) . .
Co1 B10 B11 B16 -115.5(3) . .
C4 B10 B11 B15 -102.6(3) . .
B14 B10 B11 B15 -38.1(3) . .
Co1 B10 B11 B15 -153.9(2) . .
C4 B10 B11 B12 1.4(4) . .
B14 B10 B11 B12 66.0(3) . .
B15 B10 B11 B12 104.0(3) . .
Co1 B10 B11 B12 -49.8(2) . .
C4 B10 B11 Co1 51.3(2) . .
B14 B10 B11 Co1 115.8(3) . .
B15 B10 B11 Co1 153.9(2) . .
C2 Co1 B11 B10 58.7(3) . .
C4 Co1 B11 B10 -37.8(2) . .
C1 Co1 B11 B10 96.0(2) . .
C3 Co1 B11 B10 -87.2(2) . .
B1 Co1 B11 B10 26(3) . .
B3 Co1 B11 B10 146.0(2) . .
B12 Co1 B11 B10 -127.5(3) . .
B2 Co1 B11 B10 -175.42(19) . .
C2 Co1 B11 B16 156.7(2) . .
C4 Co1 B11 B16 60.2(3) . .
C1 Co1 B11 B16 -166.0(3) . .
C3 Co1 B11 B16 10.8(3) . .
B10 Co1 B11 B16 98.0(3) . .
B1 Co1 B11 B16 124(3) . .
B3 Co1 B11 B16 -116.0(3) . .
B12 Co1 B11 B16 -29.5(3) . .
B2 Co1 B11 B16 -77.4(3) . .
C2 Co1 B11 B15 85.0(3) . .
C4 Co1 B11 B15 -11.6(3) . .
C1 Co1 B11 B15 122.3(3) . .
C3 Co1 B11 B15 -60.9(3) . .
B10 Co1 B11 B15 26.3(2) . .
B1 Co1 B11 B15 53(3) . .
B3 Co1 B11 B15 172.3(3) . .
B12 Co1 B11 B15 -101.2(3) . .
B2 Co1 B11 B15 -149.1(2) . .
C2 Co1 B11 B12 -173.82(19) . .
C4 Co1 B11 B12 89.7(2) . .
C1 Co1 B11 B12 -136.5(2) . .
C3 Co1 B11 B12 40.3(2) . .
B10 Co1 B11 B12 127.5(3) . .
B1 Co1 B11 B12 154(3) . .
B3 Co1 B11 B12 -86.5(2) . .
B2 Co1 B11 B12 -47.9(3) . .
C4 C3 B12 B11 1.4(3) . .
B17 C3 B12 B11 -99.3(3) . .
B13 C3 B12 B11 -63.3(3) . .
Co1 C3 B12 B11 51.9(2) . .
C4 C3 B12 B17 100.7(3) . .
B13 C3 B12 B17 36.0(3) . .
Co1 C3 B12 B17 151.2(2) . .
C4 C3 B12 B16 61.9(3) . .
B17 C3 B12 B16 -38.8(3) . .
B13 C3 B12 B16 -2.8(4) . .
Co1 C3 B12 B16 112.4(2) . .
C4 C3 B12 Co1 -50.5(2) . .
B17 C3 B12 Co1 -151.2(2) . .
B13 C3 B12 Co1 -115.2(3) . .
B10 B11 B12 C3 -1.7(3) . .
B16 B11 B12 C3 99.6(3) . .
B15 B11 B12 C3 63.0(3) . .
Co1 B11 B12 C3 -51.5(2) . .
B10 B11 B12 B17 -63.0(3) . .
B16 B11 B12 B17 38.3(3) . .
B15 B11 B12 B17 1.7(4) . .
Co1 B11 B12 B17 -112.8(3) . .
B10 B11 B12 B16 -101.3(3) . .
B15 B11 B12 B16 -36.6(3) . .
Co1 B11 B12 B16 -151.1(3) . .
B10 B11 B12 Co1 49.8(2) . .
B16 B11 B12 Co1 151.1(3) . .
B15 B11 B12 Co1 114.5(3) . .
C2 Co1 B12 C3 -158.5(16) . .
C4 Co1 B12 C3 37.2(2) . .
C1 Co1 B12 C3 -177.83(19) . .
B10 Co1 B12 C3 85.7(2) . .
B1 Co1 B12 C3 -55.6(3) . .
B11 Co1 B12 C3 122.3(3) . .
B3 Co1 B12 C3 -141.0(2) . .
B2 Co1 B12 C3 -90.2(2) . .
C2 Co1 B12 B11 79.2(17) . .
C4 Co1 B12 B11 -85.1(2) . .
C1 Co1 B12 B11 59.9(3) . .
C3 Co1 B12 B11 -122.3(3) . .
B10 Co1 B12 B11 -36.6(2) . .
B1 Co1 B12 B11 -177.9(2) . .
B3 Co1 B12 B11 96.7(2) . .
B2 Co1 B12 B11 147.5(2) . .
C2 Co1 B12 B17 173.9(15) . .
C4 Co1 B12 B17 9.7(3) . .
C1 Co1 B12 B17 154.6(2) . .
C3 Co1 B12 B17 -27.6(2) . .
B10 Co1 B12 B17 58.1(3) . .
B1 Co1 B12 B17 -83.1(3) . .
B11 Co1 B12 B17 94.7(3) . .
B3 Co1 B12 B17 -168.6(3) . .
B2 Co1 B12 B17 -117.8(3) . .
C2 Co1 B12 B16 106.6(16) . .
C4 Co1 B12 B16 -57.7(3) . .
C1 Co1 B12 B16 87.2(3) . .
C3 Co1 B12 B16 -94.9(3) . .
B10 Co1 B12 B16 -9.2(3) . .
B1 Co1 B12 B16 -150.5(2) . .
B11 Co1 B12 B16 27.4(2) . .
B3 Co1 B12 B16 124.1(3) . .
B2 Co1 B12 B16 174.9(3) . .
B10 C4 B13 C3 -100.9(3) . .
B14 C4 B13 C3 -138.8(3) . .
Co1 C4 B13 C3 -26.3(3) . .
B10 C4 B13 B18 -1.4(4) . .
C3 C4 B13 B18 99.5(3) . .
B14 C4 B13 B18 -39.3(3) . .
Co1 C4 B13 B18 73.2(3) . .
B10 C4 B13 B14 38.0(3) . .
C3 C4 B13 B14 138.8(3) . .
Co1 C4 B13 B14 112.5(3) . .
B10 C4 B13 B17 -63.6(4) . .
C3 C4 B13 B17 37.2(3) . .
B14 C4 B13 B17 -101.6(3) . .
Co1 C4 B13 B17 10.9(4) . .
B17 C3 B13 C4 136.8(3) . .
B12 C3 B13 C4 100.7(3) . .
Co1 C3 B13 C4 25.9(3) . .
C4 C3 B13 B18 -98.7(3) . .
B17 C3 B13 B18 38.0(3) . .
B12 C3 B13 B18 1.9(4) . .
Co1 C3 B13 B18 -72.9(4) . .
C4 C3 B13 B14 -35.9(3) . .
B17 C3 B13 B14 100.8(3) . .
B12 C3 B13 B14 64.7(4) . .
Co1 C3 B13 B14 -10.1(4) . .
C4 C3 B13 B17 -136.8(3) . .
B12 C3 B13 B17 -36.1(3) . .
Co1 C3 B13 B17 -110.9(3) . .
C3 C4 B14 B10 100.6(3) . .
B13 C4 B14 B10 139.0(3) . .
Co1 C4 B14 B10 27.0(3) . .
B10 C4 B14 B15 -36.8(3) . .
C3 C4 B14 B15 63.8(3) . .
B13 C4 B14 B15 102.2(3) . .
Co1 C4 B14 B15 -9.9(4) . .
B10 C4 B14 B13 -139.0(3) . .
C3 C4 B14 B13 -38.4(3) . .
Co1 C4 B14 B13 -112.0(3) . .
B10 C4 B14 B18 -99.7(3) . .
C3 C4 B14 B18 0.9(4) . .
B13 C4 B14 B18 39.3(3) . .
Co1 C4 B14 B18 -72.8(3) . .
B11 B10 B14 C4 -99.9(3) . .
B15 B10 B14 C4 -137.9(3) . .
Co1 B10 B14 C4 -26.2(3) . .
C4 B10 B14 B15 137.9(3) . .
B11 B10 B14 B15 38.0(3) . .
Co1 B10 B14 B15 111.7(3) . .
C4 B10 B14 B13 36.0(3) . .
B11 B10 B14 B13 -63.8(3) . .
B15 B10 B14 B13 -101.9(3) . .
Co1 B10 B14 B13 9.8(4) . .
C4 B10 B14 B18 98.8(3) . .
B11 B10 B14 B18 -1.1(4) . .
B15 B10 B14 B18 -39.1(2) . .
Co1 B10 B14 B18 72.5(3) . .
C3 B13 B14 C4 35.6(3) . .
B18 B13 B14 C4 135.2(3) . .
B17 B13 B14 C4 97.1(3) . .
C4 B13 B14 B10 -35.5(3) . .
C3 B13 B14 B10 0.1(4) . .
B18 B13 B14 B10 99.7(3) . .
B17 B13 B14 B10 61.6(3) . .
C4 B13 B14 B15 -98.0(3) . .
C3 B13 B14 B15 -62.3(3) . .
B18 B13 B14 B15 37.3(3) . .
B17 B13 B14 B15 -0.9(3) . .
C4 B13 B14 B18 -135.2(3) . .
C3 B13 B14 B18 -99.6(3) . .
B17 B13 B14 B18 -38.1(3) . .
C4 B10 B15 B11 100.5(3) . .
B14 B10 B15 B11 138.8(3) . .
Co1 B10 B15 B11 28.2(3) . .
C4 B10 B15 B16 63.7(3) . .
B11 B10 B15 B16 -36.9(3) . .
B14 B10 B15 B16 101.9(3) . .
Co1 B10 B15 B16 -8.7(4) . .
C4 B10 B15 B14 -38.2(3) . .
B11 B10 B15 B14 -138.8(3) . .
Co1 B10 B15 B14 -110.5(3) . .
C4 B10 B15 B18 0.8(4) . .
B11 B10 B15 B18 -99.8(3) . .
B14 B10 B15 B18 39.0(3) . .
Co1 B10 B15 B18 -71.6(3) . .
B16 B11 B15 B10 -137.6(3) . .
B12 B11 B15 B10 -100.7(3) . .
Co1 B11 B15 B10 -27.6(2) . .
B10 B11 B15 B16 137.6(3) . .
B12 B11 B15 B16 36.9(3) . .
Co1 B11 B15 B16 110.0(3) . .
B10 B11 B15 B14 36.2(3) . .
B16 B11 B15 B14 -101.4(3) . .
B12 B11 B15 B14 -64.5(3) . .
Co1 B11 B15 B14 8.6(4) . .
B10 B11 B15 B18 99.1(3) . .
B16 B11 B15 B18 -38.5(3) . .
B12 B11 B15 B18 -1.6(4) . .
Co1 B11 B15 B18 71.5(3) . .
C4 B14 B15 B10 36.3(2) . .
B13 B14 B15 B10 98.6(3) . .
B18 B14 B15 B10 135.7(3) . .
C4 B14 B15 B11 0.5(3) . .
B10 B14 B15 B11 -35.8(2) . .
B13 B14 B15 B11 62.8(3) . .
B18 B14 B15 B11 99.9(3) . .
C4 B14 B15 B16 -61.6(3) . .
B10 B14 B15 B16 -97.9(3) . .
B13 B14 B15 B16 0.7(3) . .
B18 B14 B15 B16 37.8(3) . .
C4 B14 B15 B18 -99.4(3) . .
B10 B14 B15 B18 -135.7(3) . .
B13 B14 B15 B18 -37.1(2) . .
B10 B11 B16 B15 -38.2(3) . .
B12 B11 B16 B15 -140.5(3) . .
Co1 B11 B16 B15 -109.9(3) . .
B10 B11 B16 B17 63.6(3) . .
B15 B11 B16 B17 101.8(3) . .
B12 B11 B16 B17 -38.7(3) . .
Co1 B11 B16 B17 -8.2(4) . .
B10 B11 B16 B18 0.6(4) . .
B15 B11 B16 B18 38.8(3) . .
B12 B11 B16 B18 -101.7(3) . .
Co1 B11 B16 B18 -71.2(3) . .
B10 B11 B16 B12 102.3(3) . .
B15 B11 B16 B12 140.5(3) . .
Co1 B11 B16 B12 30.6(3) . .
B10 B15 B16 B11 36.6(3) . .
B14 B15 B16 B11 98.8(3) . .
B18 B15 B16 B11 136.5(3) . .
B10 B15 B16 B17 -62.5(3) . .
B11 B15 B16 B17 -99.1(3) . .
B14 B15 B16 B17 -0.3(4) . .
B18 B15 B16 B17 37.5(3) . .
B10 B15 B16 B18 -99.9(3) . .
B11 B15 B16 B18 -136.5(3) . .
B14 B15 B16 B18 -37.7(2) . .
B10 B15 B16 B12 0.9(4) . .
B11 B15 B16 B12 -35.7(3) . .
B14 B15 B16 B12 63.1(3) . .
B18 B15 B16 B12 100.9(3) . .
C3 B12 B16 B11 -97.4(3) . .
B17 B12 B16 B11 -136.0(3) . .
Co1 B12 B16 B11 -29.2(3) . .
C3 B12 B16 B15 -61.6(3) . .
B11 B12 B16 B15 35.8(3) . .
B17 B12 B16 B15 -100.2(3) . .
Co1 B12 B16 B15 6.6(4) . .
C3 B12 B16 B17 38.6(3) . .
B11 B12 B16 B17 136.0(3) . .
Co1 B12 B16 B17 106.8(3) . .
C3 B12 B16 B18 2.5(3) . .
B11 B12 B16 B18 99.9(3) . .
B17 B12 B16 B18 -36.1(3) . .
Co1 B12 B16 B18 70.7(3) . .
C4 C3 B17 B16 -63.1(4) . .
B12 C3 B17 B16 39.8(3) . .
B13 C3 B17 B16 -101.8(3) . .
Co1 C3 B17 B16 8.8(4) . .
C4 C3 B17 B18 0.4(4) . .
B12 C3 B17 B18 103.2(3) . .
B13 C3 B17 B18 -38.3(3) . .
Co1 C3 B17 B18 72.2(4) . .
C4 C3 B17 B12 -102.8(3) . .
B13 C3 B17 B12 -141.5(3) . .
Co1 C3 B17 B12 -31.0(3) . .
C4 C3 B17 B13 38.7(3) . .
B12 C3 B17 B13 141.5(3) . .
Co1 C3 B17 B13 110.5(3) . .
B11 B16 B17 C3 -0.2(4) . .
B15 B16 B17 C3 63.1(3) . .
B18 B16 B17 C3 100.7(3) . .
B12 B16 B17 C3 -39.1(3) . .
B11 B16 B17 B18 -100.9(3) . .
B15 B16 B17 B18 -37.6(3) . .
B12 B16 B17 B18 -139.8(3) . .
B11 B16 B17 B12 38.9(3) . .
B15 B16 B17 B12 102.2(3) . .
B18 B16 B17 B12 139.8(3) . .
B11 B16 B17 B13 -63.6(3) . .
B15 B16 B17 B13 -0.3(4) . .
B18 B16 B17 B13 37.3(3) . .
B12 B16 B17 B13 -102.5(3) . .
B11 B12 B17 C3 97.7(3) . .
B16 B12 B17 C3 135.5(3) . .
Co1 B12 B17 C3 29.0(2) . .
C3 B12 B17 B16 -135.5(3) . .
B11 B12 B17 B16 -37.8(3) . .
Co1 B12 B17 B16 -106.5(3) . .
C3 B12 B17 B18 -98.9(3) . .
B11 B12 B17 B18 -1.2(4) . .
B16 B12 B17 B18 36.6(3) . .
Co1 B12 B17 B18 -69.9(3) . .
C3 B12 B17 B13 -34.9(3) . .
B11 B12 B17 B13 62.9(3) . .
B16 B12 B17 B13 100.6(3) . .
Co1 B12 B17 B13 -5.9(4) . .
C4 B13 B17 C3 -37.0(3) . .
B18 B13 B17 C3 -136.8(3) . .
B14 B13 B17 C3 -98.6(3) . .
C4 B13 B17 B16 62.3(3) . .
C3 B13 B17 B16 99.3(3) . .
B18 B13 B17 B16 -37.5(3) . .
B14 B13 B17 B16 0.7(4) . .
C4 B13 B17 B18 99.8(3) . .
C3 B13 B17 B18 136.8(3) . .
B14 B13 B17 B18 38.2(3) . .
C4 B13 B17 B12 -2.5(4) . .
C3 B13 B17 B12 34.6(3) . .
B18 B13 B17 B12 -102.2(3) . .
B14 B13 B17 B12 -64.0(3) . .
C16 C15 B18 B17 -112(26) . .
C16 C15 B18 B13 -39(26) . .
C16 C15 B18 B14 32(26) . .
C16 C15 B18 B16 175(100) . .
C16 C15 B18 B15 103(26) . .
C3 B17 B18 C15 148.4(3) . .
B16 B17 B18 C15 -111.7(4) . .
B12 B17 B18 C15 -148.6(3) . .
B13 B17 B18 C15 110.0(4) . .
C3 B17 B18 B13 38.4(3) . .
B16 B17 B18 B13 138.3(3) . .
B12 B17 B18 B13 101.4(3) . .
C3 B17 B18 B14 0.2(4) . .
B16 B17 B18 B14 100.0(3) . .
B12 B17 B18 B14 63.2(4) . .
B13 B17 B18 B14 -38.2(3) . .
C3 B17 B18 B16 -99.8(3) . .
B12 B17 B18 B16 -36.8(3) . .
B13 B17 B18 B16 -138.3(3) . .
C3 B17 B18 B15 -62.8(4) . .
B16 B17 B18 B15 37.1(3) . .
B12 B17 B18 B15 0.2(4) . .
B13 B17 B18 B15 -101.2(3) . .
C4 B13 B18 C15 148.4(3) . .
C3 B13 B18 C15 -150.8(3) . .
B14 B13 B18 C15 109.6(4) . .
B17 B13 B18 C15 -113.4(4) . .
C4 B13 B18 B17 -98.3(3) . .
C3 B13 B18 B17 -37.4(3) . .
B14 B13 B18 B17 -137.0(3) . .
C4 B13 B18 B14 38.8(3) . .
C3 B13 B18 B14 99.6(3) . .
B17 B13 B18 B14 137.0(3) . .
C4 B13 B18 B16 -61.1(3) . .
C3 B13 B18 B16 -0.3(4) . .
B14 B13 B18 B16 -99.9(3) . .
B17 B13 B18 B16 37.2(3) . .
C4 B13 B18 B15 1.8(4) . .
C3 B13 B18 B15 62.6(3) . .
B14 B13 B18 B15 -37.0(3) . .
B17 B13 B18 B15 100.0(3) . .
C4 B14 B18 C15 -150.0(3) . .
B10 B14 B18 C15 149.2(3) . .
B15 B14 B18 C15 110.4(3) . .
B13 B14 B18 C15 -111.0(4) . .
C4 B14 B18 B17 -0.7(4) . .
B10 B14 B18 B17 -61.5(3) . .
B15 B14 B18 B17 -100.2(3) . .
B13 B14 B18 B17 38.3(3) . .
C4 B14 B18 B13 -39.0(3) . .
B10 B14 B18 B13 -99.8(3) . .
B15 B14 B18 B13 -138.5(3) . .
C4 B14 B18 B16 62.2(3) . .
B10 B14 B18 B16 1.4(3) . .
B15 B14 B18 B16 -37.3(2) . .
B13 B14 B18 B16 101.2(3) . .
C4 B14 B18 B15 99.5(3) . .
B10 B14 B18 B15 38.7(2) . .
B13 B14 B18 B15 138.5(3) . .
B11 B16 B18 C15 -148.0(3) . .
B15 B16 B18 C15 -109.3(4) . .
B17 B16 B18 C15 112.6(4) . .
B12 B16 B18 C15 148.6(3) . .
B11 B16 B18 B17 99.4(3) . .
B15 B16 B18 B17 138.1(3) . .
B12 B16 B18 B17 36.0(3) . .
B11 B16 B18 B13 62.0(3) . .
B15 B16 B18 B13 100.7(3) . .
B17 B16 B18 B13 -37.4(3) . .
B12 B16 B18 B13 -1.4(4) . .
B11 B16 B18 B14 -1.3(4) . .
B15 B16 B18 B14 37.4(3) . .
B17 B16 B18 B14 -100.6(3) . .
B12 B16 B18 B14 -64.6(3) . .
B11 B16 B18 B15 -38.7(3) . .
B17 B16 B18 B15 -138.1(3) . .
B12 B16 B18 B15 -102.1(3) . .
B10 B15 B18 C15 -148.3(3) . .
B11 B15 B18 C15 150.5(3) . .
B16 B15 B18 C15 112.6(4) . .
B14 B15 B18 C15 -109.7(4) . .
B10 B15 B18 B17 61.9(3) . .
B11 B15 B18 B17 0.8(4) . .
B16 B15 B18 B17 -37.2(3) . .
B14 B15 B18 B17 100.6(3) . .
B10 B15 B18 B13 -1.6(4) . .
B11 B15 B18 B13 -62.7(3) . .
B16 B15 B18 B13 -100.7(3) . .
B14 B15 B18 B13 37.1(3) . .
B10 B15 B18 B14 -38.7(3) . .
B11 B15 B18 B14 -99.8(3) . .
B16 B15 B18 B14 -137.8(3) . .
B10 B15 B18 B16 99.1(3) . .
B11 B15 B18 B16 38.0(2) . .
B14 B15 B18 B16 137.8(3) . .
