#------------------------------------------------------------------------------
#$Date: 2016-03-24 14:34:44 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179668 $
#$URL: svn://www.crystallography.net/cod/cif/4/51/21/4512157.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4512157
loop_
_publ_author_name
'Zhao, Junwei'
'Li, Hailou'
'Li, Yanzhou'
'Li, Chunyang'
'Wang, Zhenling'
'Chen, Lijuan'
_publ_section_title
;
 Rectangle versus Square Oxalate-Connective Tetralanthanide Cluster
 Anchored in Lacunary Lindqvist Isopolytungstates: Syntheses, Structures,
 and Properties
;
_journal_issue                   11
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              5495
_journal_paper_doi               10.1021/cg500675g
_journal_volume                  14
_journal_year                    2014
_chemical_formula_sum            'C8 H120 Eu4 K4 Na16 O148 W20'
_chemical_formula_weight         7394.12
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   notdet
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.2040(10)
_cell_angle_beta                 93.0640(10)
_cell_angle_gamma                95.3570(10)
_cell_formula_units_Z            1
_cell_length_a                   9.9166(5)
_cell_length_b                   19.4656(10)
_cell_length_c                   19.4690(10)
_cell_measurement_reflns_used    12490
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      25.00
_cell_measurement_theta_min      1.31
_cell_volume                     3580.6(3)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean none
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0279
_diffrn_reflns_av_sigmaI/netI    0.0559
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            18430
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.31
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    18.003
_exptl_absorpt_correction_T_max  0.1097
_exptl_absorpt_correction_T_min  0.0891
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.429
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'quadrangular prism'
_exptl_crystal_F_000             3336
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.22
_refine_diff_density_max         2.227
_refine_diff_density_min         -3.634
_refine_diff_density_rms         0.288
_refine_ls_extinction_coef       0.000328(18)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     867
_refine_ls_number_reflns         12490
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0566
_refine_ls_R_factor_gt           0.0402
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0490P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0976
_refine_ls_wR_factor_ref         0.1039
_reflns_number_gt                9824
_reflns_number_total             12490
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg500675g_si_001.cif
_cod_data_source_block           2-Eu
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2827 2014-09-09 07:05:25Z andrius 

 Adding full bibliography for 4512153--4512160.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4512157
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
W1 W 1.41851(5) 0.68458(3) 1.13913(2) 0.02066(13) Uani 1 1 d .
W2 W 1.62310(5) 0.80920(3) 1.10060(3) 0.02148(13) Uani 1 1 d .
W3 W 1.69939(5) 0.63996(3) 1.05909(2) 0.02162(13) Uani 1 1 d .
W4 W 1.67152(5) 0.64408(3) 1.23011(2) 0.01952(12) Uani 1 1 d .
W5 W 1.87547(5) 0.76825(3) 1.19237(3) 0.02102(13) Uani 1 1 d .
W6 W 1.48776(5) 0.81290(3) 1.80160(2) 0.02127(13) Uani 1 1 d .
W7 W 1.76635(5) 0.76836(3) 1.72447(3) 0.02567(14) Uani 1 1 d .
W8 W 1.58527(6) 0.64720(3) 1.59239(3) 0.02668(14) Uani 1 1 d .
W9 W 1.30688(5) 0.69177(3) 1.66806(3) 0.02254(13) Uani 1 1 d .
W10 W 1.55385(5) 0.64209(3) 1.76059(3) 0.02303(13) Uani 1 1 d .
Eu1 Eu 1.58592(6) 0.83177(3) 1.29457(3) 0.01853(14) Uani 1 1 d .
Eu2 Eu 1.51722(6) 0.83649(3) 1.62000(3) 0.01847(14) Uani 1 1 d .
K1 K 1.4470(3) 0.53778(18) 0.91252(16) 0.0426(8) Uani 1 1 d .
K2 K 1.3972(4) 0.47680(19) 1.62145(18) 0.0594(11) Uani 1 1 d .
Na1 Na 0.9436(5) 0.5034(3) 0.7741(3) 0.0377(13) Uani 1 1 d .
Na2 Na 0.2538(6) 0.6201(3) 0.3705(3) 0.0448(15) Uani 1 1 d .
Na3 Na 0.1789(6) 0.7966(3) 0.4118(3) 0.0459(15) Uani 1 1 d .
Na4 Na 0.9360(9) 0.9379(7) 0.4018(9) 0.123(5) Uani 0.80 1 d P
Na4' Na 0.946(2) 0.9502(13) 0.3372(13) 0.025(6) Uiso 0.20 1 d P
Na5 Na 1.1347(6) 0.6378(3) 0.9076(3) 0.0437(15) Uani 1 1 d .
Na6 Na 1.0535(7) 0.8101(4) 0.9576(3) 0.0591(18) Uani 1 1 d .
Na7 Na 0.2637(9) 0.8655(6) 0.1541(5) 0.034(3) Uani 0.50 1 d P
Na8 Na 0.1476(15) 0.8692(8) 0.7071(9) 0.075(4) Uani 0.50 1 d PU
Na9 Na 0.1085(9) 0.7260(6) -0.1545(5) 0.032(3) Uani 0.50 1 d P
Na10 Na 0.087(2) 1.0666(16) 0.3711(15) 0.167(12) Uani 0.50 1 d P
O1 O 1.2504(9) 0.6461(5) 1.1118(5) 0.042(3) Uani 1 1 d .
O2 O 1.4020(8) 0.7522(5) 1.2197(4) 0.028(2) Uani 1 1 d .
O3 O 1.4847(8) 0.6206(4) 1.1905(4) 0.0200(18) Uani 1 1 d .
O4 O 1.5075(8) 0.6213(5) 1.0576(4) 0.024(2) Uani 1 1 d .
O5 O 1.6496(8) 0.7239(4) 1.1633(4) 0.0220(19) Uani 1 1 d .
O6 O 1.4438(8) 0.7558(4) 1.0846(4) 0.0227(19) Uani 1 1 d .
O7 O 1.6112(10) 0.8623(5) 1.0451(5) 0.042(3) Uani 1 1 d .
O8 O 1.5829(8) 0.8655(4) 1.1865(4) 0.026(2) Uani 1 1 d .
O9 O 1.8162(8) 0.8235(4) 1.1305(4) 0.026(2) Uani 1 1 d .
O10 O 1.6697(8) 0.7223(5) 1.0275(4) 0.027(2) Uani 1 1 d .
O11 O 1.7325(9) 0.5766(5) 0.9821(4) 0.033(2) Uani 1 1 d .
O12 O 1.8734(8) 0.6890(5) 1.0992(4) 0.024(2) Uani 1 1 d .
O13 O 1.7112(8) 0.5903(4) 1.1307(4) 0.027(2) Uani 1 1 d .
O14 O 1.6927(9) 0.5749(5) 1.2690(4) 0.034(2) Uani 1 1 d .
O15 O 1.6304(8) 0.7159(4) 1.3036(4) 0.0229(19) Uani 1 1 d .
O16 O 1.8554(8) 0.6893(4) 1.2346(4) 0.0239(19) Uani 1 1 d .
O17 O 2.0475(8) 0.7917(5) 1.2029(5) 0.037(2) Uani 1 1 d .
O18 O 1.8163(8) 0.8280(5) 1.2691(4) 0.027(2) Uani 1 1 d .
O19 O 1.6969(8) 0.8557(5) 1.4170(4) 0.032(2) Uani 1 1 d .
O20 O 1.4315(9) 0.8168(5) 1.3851(4) 0.031(2) Uani 1 1 d .
O21 O 1.4056(9) 0.8235(5) 1.5008(4) 0.029(2) Uani 1 1 d .
O22 O 1.6735(8) 0.8603(5) 1.5320(4) 0.032(2) Uani 1 1 d .
O23 O 1.4531(10) 0.8674(5) 1.8841(4) 0.039(2) Uani 1 1 d .
O24 O 1.4793(9) 0.8704(4) 1.7438(4) 0.028(2) Uani 1 1 d .
O25 O 1.3091(8) 0.7616(5) 1.7611(4) 0.025(2) Uani 1 1 d .
O26 O 1.5361(8) 0.7278(4) 1.6984(4) 0.0231(19) Uani 1 1 d .
O27 O 1.5110(8) 0.7237(4) 1.8322(4) 0.025(2) Uani 1 1 d .
O28 O 1.6826(8) 0.8238(5) 1.8078(4) 0.027(2) Uani 1 1 d .
O29 O 1.9360(9) 0.7890(6) 1.7504(5) 0.043(3) Uani 1 1 d .
O30 O 1.7349(9) 0.6889(5) 1.7709(5) 0.033(2) Uani 1 1 d .
O31 O 1.7311(8) 0.8311(5) 1.6752(4) 0.0248(19) Uani 1 1 d .
O32 O 1.7635(8) 0.6896(5) 1.6384(4) 0.030(2) Uani 1 1 d .
O33 O 1.6249(10) 0.5785(5) 1.5216(5) 0.041(3) Uani 1 1 d .
O34 O 1.5667(9) 0.7193(4) 1.5530(4) 0.029(2) Uani 1 1 d .
O35 O 1.5887(9) 0.5923(5) 1.6665(5) 0.034(2) Uani 1 1 d .
O36 O 1.3915(9) 0.6276(5) 1.5930(4) 0.029(2) Uani 1 1 d .
O37 O 1.3158(8) 0.7613(5) 1.6234(4) 0.026(2) Uani 1 1 d .
O38 O 1.1377(9) 0.6546(6) 1.6529(5) 0.045(3) Uani 1 1 d .
O39 O 1.3671(9) 0.6263(4) 1.7264(4) 0.030(2) Uani 1 1 d .
O40 O 1.5644(9) 0.5767(5) 1.8060(5) 0.037(2) Uani 1 1 d .
O41 O 1.6869(8) 0.9594(5) 1.3370(5) 0.029(2) Uani 1 1 d .
O42 O 1.4214(8) 0.9212(4) 1.3098(5) 0.032(2) Uani 1 1 d .
O43 O 1.3835(8) 1.0358(4) 1.3389(5) 0.029(2) Uani 1 1 d .
O44 O 1.6510(8) 1.0753(4) 1.3703(5) 0.030(2) Uani 1 1 d .
C1 C 1.4782(12) 0.8282(6) 1.4497(7) 0.023(3) Uani 1 1 d .
C2 C 1.6307(12) 0.8507(7) 1.4667(6) 0.024(3) Uani 1 1 d .
C3 C 1.4560(12) 0.9861(6) 1.3303(6) 0.019(3) Uani 1 1 d U
C4 C 1.6131(11) 1.0092(6) 1.3474(6) 0.019(3) Uani 1 1 d .
O1W O 1.1658(13) 0.5505(6) 0.9648(6) 0.062(3) Uani 1 1 d .
O2W O 1.3709(9) 0.6820(6) 0.9339(5) 0.041(3) Uani 1 1 d .
O3W O 1.0862(10) 0.7207(6) 1.0201(5) 0.046(3) Uani 1 1 d .
O4W O 1.1301(15) 0.4868(9) 1.5878(8) 0.104(5) Uiso 1 1 d .
O5W O 1.5045(10) 0.3438(5) 1.5984(5) 0.044(3) Uani 1 1 d .
O6W O 0.9124(11) 0.5786(7) 0.6989(7) 0.070(4) Uani 1 1 d .
O7W O 1.485(2) 0.9880(9) 1.1583(9) 0.068(6) Uani 0.60 1 d P
O7W' O 1.646(3) 1.0123(19) 1.1856(18) 0.081(10) Uiso 0.40 1 d P
O8W O 0.1539(10) 0.8817(6) 0.3381(5) 0.054(3) Uani 1 1 d .
O9W O 0.1830(10) 0.7044(6) 0.4743(5) 0.049(3) Uani 1 1 d .
O10W O 0.9777(11) 0.4266(7) 0.8484(7) 0.065(4) Uani 1 1 d .
O11W O 1.2279(14) 1.0615(8) 1.0434(8) 0.090 Uiso 1 1 d .
O12W O 1.2903(11) 0.8525(8) 0.9985(6) 0.071(4) Uani 1 1 d .
O13W O 0.9904(10) 0.4119(6) 0.6663(6) 0.057(3) Uani 1 1 d .
O14W O 0.8958(10) 0.5995(6) 0.8729(5) 0.050(3) Uani 1 1 d .
O15W O 0.2966(9) 0.5426(5) 0.2542(5) 0.038(2) Uani 1 1 d .
O16W O 1.4691(15) 0.9873(9) 1.0310(8) 0.100 Uiso 1 1 d .
O17W O -0.1227(15) 0.7599(8) 0.5284(8) 0.098 Uiso 1 1 d .
O18W O 0.9050(19) 0.9770(11) 0.2399(10) 0.135(7) Uiso 1 1 d .
O19W O 1.1929(14) 1.0173(8) 1.2117(8) 0.090 Uiso 1 1 d .
O20W O -0.033(2) 0.6262(12) 0.5287(11) 0.152(7) Uiso 1 1 d .
O21W O 0.8227(12) 0.7592(7) 0.9234(6) 0.067(3) Uiso 1 1 d .
O22W O 0.1336(15) 0.8922(9) 0.5165(8) 0.116(7) Uani 1 1 d .
O23W O 0.9983(13) 0.9019(7) 1.0645(7) 0.077(4) Uani 1 1 d .
O24W O -0.0625(11) 0.7579(9) 0.3896(6) 0.086(5) Uani 1 1 d .
O25W O 1.2364(16) 0.9507(8) 1.0949(10) 0.113(6) Uani 1 1 d .
O26W O 0.2663(17) 0.5419(10) 0.4405(9) 0.115(6) Uiso 1 1 d .
O27W O 1.0352(15) 0.8990(9) 0.8922(8) 0.099 Uiso 1 1 d .
O28W O 0.3769(15) 0.9951(9) 0.9398(8) 0.098 Uiso 1 1 d .
O29W O 0.2030(10) 0.7033(5) 0.3013(5) 0.047(3) Uani 1 1 d .
O30W O 1.1893(9) 0.5528(5) 0.7953(5) 0.034(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 W1 O2 103.0(4) . .
O1 W1 O3 102.0(4) . .
O2 W1 O3 92.5(4) . .
O1 W1 O6 102.7(4) . .
O2 W1 O6 92.3(4) . .
O3 W1 O6 153.0(3) . .
O1 W1 O4 97.5(4) . .
O2 W1 O4 159.5(4) . .
O3 W1 O4 82.6(3) . .
O6 W1 O4 83.7(3) . .
O1 W1 O5 172.6(4) . .
O2 W1 O5 84.4(3) . .
O3 W1 O5 76.5(3) . .
O6 W1 O5 77.6(3) . .
O4 W1 O5 75.2(3) . .
O1 W1 Eu1 134.7(3) . .
O2 W1 Eu1 31.7(3) . .
O3 W1 Eu1 85.0(2) . .
O6 W1 Eu1 85.1(2) . .
O4 W1 Eu1 127.8(2) . .
O5 W1 Eu1 52.64(18) . .
O7 W2 O8 103.9(4) . .
O7 W2 O6 102.2(4) . .
O8 W2 O6 91.3(4) . .
O7 W2 O9 102.6(4) . .
O8 W2 O9 92.2(4) . .
O6 W2 O9 153.3(4) . .
O7 W2 O10 97.0(4) . .
O8 W2 O10 159.1(4) . .
O6 W2 O10 83.2(3) . .
O9 W2 O10 84.2(3) . .
O7 W2 O5 171.9(4) . .
O8 W2 O5 84.2(3) . .
O6 W2 O5 77.8(3) . .
O9 W2 O5 76.2(3) . .
O10 W2 O5 75.0(3) . .
O7 W2 Eu1 135.4(3) . .
O8 W2 Eu1 31.5(3) . .
O6 W2 Eu1 85.7(2) . .
O9 W2 Eu1 83.6(2) . .
O10 W2 Eu1 127.6(2) . .
O5 W2 Eu1 52.67(18) . .
O11 W3 O4 101.5(4) . .
O11 W3 O12 104.4(4) . .
O4 W3 O12 154.1(3) . .
O11 W3 O13 103.2(4) . .
O4 W3 O13 86.9(4) . .
O12 W3 O13 86.5(3) . .
O11 W3 O10 103.9(4) . .
O4 W3 O10 87.5(4) . .
O12 W3 O10 87.0(3) . .
O13 W3 O10 152.9(3) . .
O11 W3 O5 178.6(4) . .
O4 W3 O5 77.2(3) . .
O12 W3 O5 76.9(3) . .
O13 W3 O5 76.2(3) . .
O10 W3 O5 76.7(3) . .
O11 W3 K1 54.1(3) . .
O4 W3 K1 49.5(2) . .
O12 W3 K1 154.9(2) . .
O13 W3 K1 109.5(3) . .
O10 W3 K1 86.5(2) . .
O5 W3 K1 124.8(2) . .
O11 W3 K1 76.7(3) . 2_867
O4 W3 K1 61.9(3) . 2_867
O12 W3 K1 124.0(3) . 2_867
O13 W3 K1 41.7(3) . 2_867
O10 W3 K1 148.4(2) . 2_867
O5 W3 K1 102.1(2) . 2_867
K1 W3 K1 67.98(8) . 2_867
O14 W4 O15 103.3(4) . .
O14 W4 O3 101.9(4) . .
O15 W4 O3 92.6(3) . .
O14 W4 O16 102.9(4) . .
O15 W4 O16 91.9(3) . .
O3 W4 O16 153.1(3) . .
O14 W4 O13 96.6(4) . .
O15 W4 O13 160.0(3) . .
O3 W4 O13 83.6(3) . .
O16 W4 O13 83.2(3) . .
O14 W4 O5 171.7(3) . .
O15 W4 O5 84.9(3) . .
O3 W4 O5 77.2(3) . .
O16 W4 O5 76.8(3) . .
O13 W4 O5 75.1(3) . .
O14 W4 Eu1 135.4(3) . .
O15 W4 Eu1 32.1(3) . .
O3 W4 Eu1 85.4(2) . .
O16 W4 Eu1 84.3(2) . .
O13 W4 Eu1 128.0(2) . .
O5 W4 Eu1 52.86(19) . .
O14 W4 K1 71.7(3) . 2_867
O15 W4 K1 148.0(3) . 2_867
O3 W4 K1 59.2(2) . 2_867
O16 W4 K1 120.1(2) . 2_867
O13 W4 K1 41.2(2) . 2_867
O5 W4 K1 101.2(2) . 2_867
Eu1 W4 K1 141.63(6) . 2_867
O17 W5 O18 103.5(4) . .
O17 W5 O9 102.2(4) . .
O18 W5 O9 92.1(4) . .
O17 W5 O16 102.3(4) . .
O18 W5 O16 91.5(4) . .
O9 W5 O16 153.6(3) . .
O17 W5 O12 96.3(4) . .
O18 W5 O12 160.2(4) . .
O9 W5 O12 83.8(3) . .
O16 W5 O12 84.0(3) . .
O17 W5 O5 171.6(4) . .
O18 W5 O5 84.9(3) . .
O9 W5 O5 77.5(3) . .
O16 W5 O5 76.8(3) . .
O12 W5 O5 75.4(3) . .
O17 W5 Eu1 135.1(3) . .
O18 W5 Eu1 31.7(3) . .
O9 W5 Eu1 84.6(2) . .
O16 W5 Eu1 84.9(2) . .
O12 W5 Eu1 128.6(2) . .
O5 W5 Eu1 53.25(19) . .
O23 W6 O24 103.6(4) . .
O23 W6 O28 102.6(4) . .
O24 W6 O28 91.9(4) . .
O23 W6 O25 102.9(4) . .
O24 W6 O25 91.3(4) . .
O28 W6 O25 152.8(3) . .
O23 W6 O27 97.4(4) . .
O24 W6 O27 159.1(3) . .
O28 W6 O27 83.8(4) . .
O25 W6 O27 83.6(3) . .
O23 W6 O26 172.3(4) . .
O24 W6 O26 84.1(3) . .
O28 W6 O26 77.0(3) . .
O25 W6 O26 76.5(3) . .
O27 W6 O26 75.0(3) . .
O23 W6 Eu2 135.1(3) . .
O24 W6 Eu2 31.6(3) . .
O28 W6 Eu2 84.4(2) . .
O25 W6 Eu2 84.4(2) . .
O27 W6 Eu2 127.5(2) . .
O26 W6 Eu2 52.54(19) . .
O29 W7 O31 103.8(4) . .
O29 W7 O32 102.5(4) . .
O31 W7 O32 92.9(4) . .
O29 W7 O28 102.8(4) . .
O31 W7 O28 91.6(4) . .
O32 W7 O28 152.4(4) . .
O29 W7 O30 96.6(4) . .
O31 W7 O30 159.7(4) . .
O32 W7 O30 83.2(4) . .
O28 W7 O30 83.2(4) . .
O29 W7 O26 171.6(4) . .
O31 W7 O26 84.7(3) . .
O32 W7 O26 77.0(3) . .
O28 W7 O26 76.3(3) . .
O30 W7 O26 75.0(3) . .
O29 W7 Eu2 135.3(3) . .
O31 W7 Eu2 31.6(3) . .
O32 W7 Eu2 85.0(3) . .
O28 W7 Eu2 84.7(2) . .
O30 W7 Eu2 128.1(3) . .
O26 W7 Eu2 53.08(19) . .
O33 W8 O34 103.3(4) . .
O33 W8 O36 103.5(4) . .
O34 W8 O36 91.8(4) . .
O33 W8 O32 101.9(4) . .
O34 W8 O32 92.7(4) . .
O36 W8 O32 152.4(3) . .
O33 W8 O35 96.6(4) . .
O34 W8 O35 160.1(3) . .
O36 W8 O35 83.0(4) . .
O32 W8 O35 83.5(4) . .
O33 W8 O26 171.2(4) . .
O34 W8 O26 85.5(3) . .
O36 W8 O26 76.4(3) . .
O32 W8 O26 76.9(3) . .
O35 W8 O26 74.6(3) . .
O33 W8 Eu2 136.1(3) . .
O34 W8 Eu2 32.8(2) . .
O36 W8 Eu2 84.9(3) . .
O32 W8 Eu2 84.3(3) . .
O35 W8 Eu2 127.3(2) . .
O26 W8 Eu2 52.72(19) . .
O33 W8 K2 76.1(3) . .
O34 W8 K2 143.6(3) . .
O36 W8 K2 54.3(3) . .
O32 W8 K2 123.4(3) . .
O35 W8 K2 42.1(3) . .
O26 W8 K2 97.2(2) . .
Eu2 W8 K2 135.91(7) . .
O38 W9 O37 104.7(4) . .
O38 W9 O36 102.5(4) . .
O37 W9 O36 92.4(4) . .
O38 W9 O25 102.0(4) . .
O37 W9 O25 91.8(4) . .
O36 W9 O25 153.2(4) . .
O38 W9 O39 95.5(4) . .
O37 W9 O39 159.8(4) . .
O36 W9 O39 83.1(4) . .
O25 W9 O39 83.9(3) . .
O38 W9 O26 170.7(4) . .
O37 W9 O26 84.6(3) . .
O36 W9 O26 76.7(3) . .
O25 W9 O26 77.3(3) . .
O39 W9 O26 75.2(3) . .
O38 W9 Eu2 136.6(3) . .
O37 W9 Eu2 31.9(3) . .
O36 W9 Eu2 84.8(2) . .
O25 W9 Eu2 84.8(2) . .
O39 W9 Eu2 127.9(2) . .
O26 W9 Eu2 52.7(2) . .
O40 W10 O35 102.5(4) . .
O40 W10 O27 103.7(4) . .
O35 W10 O27 153.8(4) . .
O40 W10 O39 101.8(4) . .
O35 W10 O39 86.6(4) . .
O27 W10 O39 87.3(4) . .
O40 W10 O30 104.3(4) . .
O35 W10 O30 86.9(4) . .
O27 W10 O30 87.4(4) . .
O39 W10 O30 153.9(4) . .
O40 W10 O26 178.8(4) . .
O35 W10 O26 76.8(3) . .
O27 W10 O26 76.9(3) . .
O39 W10 O26 77.2(3) . .
O30 W10 O26 76.7(3) . .
O40 W10 K2 78.4(3) . .
O35 W10 K2 44.2(3) . .
O27 W10 K2 142.7(3) . .
O39 W10 K2 56.4(3) . .
O30 W10 K2 128.7(3) . .
O26 W10 K2 100.5(2) . .
O18 Eu1 O8 78.8(3) . .
O18 Eu1 O15 77.2(3) . .
O8 Eu1 O15 124.4(3) . .
O18 Eu1 O2 123.3(3) . .
O8 Eu1 O2 76.2(3) . .
O15 Eu1 O2 76.7(3) . .
O18 Eu1 O20 141.7(3) . .
O8 Eu1 O20 139.4(3) . .
O15 Eu1 O20 79.4(3) . .
O2 Eu1 O20 79.3(3) . .
O18 Eu1 O42 136.3(3) . .
O8 Eu1 O42 75.6(3) . .
O15 Eu1 O42 146.3(3) . .
O2 Eu1 O42 83.7(3) . .
O20 Eu1 O42 70.1(3) . .
O18 Eu1 O19 79.6(3) . .
O8 Eu1 O19 145.7(3) . .
O15 Eu1 O19 75.5(3) . .
O2 Eu1 O19 138.1(3) . .
O20 Eu1 O19 65.3(3) . .
O42 Eu1 O19 103.2(3) . .
O18 Eu1 O41 75.6(3) . .
O8 Eu1 O41 77.9(3) . .
O15 Eu1 O41 139.9(3) . .
O2 Eu1 O41 143.3(3) . .
O20 Eu1 O41 105.3(3) . .
O42 Eu1 O41 64.9(3) . .
O19 Eu1 O41 71.1(3) . .
O18 Eu1 O5 61.9(2) . .
O8 Eu1 O5 62.6(2) . .
O15 Eu1 O5 61.9(2) . .
O2 Eu1 O5 61.5(2) . .
O20 Eu1 O5 129.1(3) . .
O42 Eu1 O5 129.9(3) . .
O19 Eu1 O5 126.8(3) . .
O41 Eu1 O5 125.6(3) . .
O18 Eu1 C2 97.7(3) . .
O8 Eu1 C2 158.0(3) . .
O15 Eu1 C2 74.8(3) . .
O2 Eu1 C2 122.1(3) . .
O20 Eu1 C2 46.7(3) . .
O42 Eu1 C2 93.4(3) . .
O19 Eu1 C2 18.7(3) . .
O41 Eu1 C2 80.2(3) . .
O5 Eu1 C2 134.8(3) . .
O18 Eu1 W5 23.3(2) . .
O8 Eu1 W5 69.50(19) . .
O15 Eu1 W5 68.81(18) . .
O2 Eu1 W5 100.07(19) . .
O20 Eu1 W5 147.3(2) . .
O42 Eu1 W5 142.6(2) . .
O19 Eu1 W5 98.3(2) . .
O41 Eu1 W5 94.66(19) . .
O5 Eu1 W5 38.60(16) . .
C2 Eu1 W5 114.5(2) . .
O18 Eu1 W4 68.2(2) . .
O8 Eu1 W4 100.9(2) . .
O15 Eu1 W4 23.51(18) . .
O2 Eu1 W4 67.9(2) . .
O20 Eu1 W4 99.0(2) . .
O42 Eu1 W4 151.26(19) . .
O19 Eu1 W4 95.4(2) . .
O41 Eu1 W4 143.20(19) . .
O5 Eu1 W4 38.38(15) . .
C2 Eu1 W4 97.7(2) . .
W5 Eu1 W4 52.460(14) . .
O31 Eu2 O24 77.5(3) . .
O31 Eu2 O37 124.8(3) . .
O24 Eu2 O37 77.2(3) . .
O31 Eu2 O34 78.8(3) . .
O24 Eu2 O34 124.8(3) . .
O37 Eu2 O34 77.0(3) . .
O31 Eu2 O21 140.3(3) . .
O24 Eu2 O21 142.0(3) . .
O37 Eu2 O21 79.7(3) . .
O34 Eu2 O21 77.7(3) . .
O31 Eu2 O43 76.7(3) . 2_878
O24 Eu2 O43 77.3(3) . 2_878
O37 Eu2 O43 141.2(3) . 2_878
O34 Eu2 O43 141.8(3) . 2_878
O21 Eu2 O43 103.9(3) . 2_878
O31 Eu2 O22 77.7(3) . .
O24 Eu2 O22 143.2(3) . .
O37 Eu2 O22 139.5(3) . .
O34 Eu2 O22 75.6(3) . .
O21 Eu2 O22 65.7(3) . .
O43 Eu2 O22 70.9(3) 2_878 .
O31 Eu2 O44 137.6(3) . 2_878
O24 Eu2 O44 76.2(3) . 2_878
O37 Eu2 O44 80.3(3) . 2_878
O34 Eu2 O44 143.6(3) . 2_878
O21 Eu2 O44 70.4(3) . 2_878
O43 Eu2 O44 65.5(3) 2_878 2_878
O22 Eu2 O44 105.7(3) . 2_878
O31 Eu2 O26 62.7(3) . .
O24 Eu2 O26 62.1(2) . .
O37 Eu2 O26 62.1(2) . .
O34 Eu2 O26 62.7(2) . .
O21 Eu2 O26 129.3(3) . .
O43 Eu2 O26 126.8(3) 2_878 .
O22 Eu2 O26 126.3(3) . .
O44 Eu2 O26 128.0(3) 2_878 .
O31 Eu2 W7 23.6(2) . .
O24 Eu2 W7 69.0(2) . .
O37 Eu2 W7 101.21(19) . .
O34 Eu2 W7 69.5(2) . .
O21 Eu2 W7 145.9(2) . .
O43 Eu2 W7 96.4(2) 2_878 .
O22 Eu2 W7 96.4(2) . .
O44 Eu2 W7 143.7(2) 2_878 .
O26 Eu2 W7 39.10(16) . .
O31 Eu2 W8 69.2(2) . .
O24 Eu2 W8 101.0(2) . .
O37 Eu2 W8 68.7(2) . .
O34 Eu2 W8 23.91(19) . .
O21 Eu2 W8 98.3(2) . .
O43 Eu2 W8 145.33(19) 2_878 .
O22 Eu2 W8 95.2(2) . .
O44 Eu2 W8 148.56(19) 2_878 .
O26 Eu2 W8 38.85(15) . .
W7 Eu2 W8 52.630(15) . .
O31 Eu2 W9 101.3(2) . .
O24 Eu2 W9 68.5(2) . .
O37 Eu2 W9 23.58(19) . .
O34 Eu2 W9 68.4(2) . .
O21 Eu2 W9 99.2(2) . .
O43 Eu2 W9 145.2(2) 2_878 .
O22 Eu2 W9 143.4(2) . .
O44 Eu2 W9 99.3(2) 2_878 .
O26 Eu2 W9 38.53(16) . .
W7 Eu2 W9 77.632(17) . .
W8 Eu2 W9 52.415(14) . .
O40 K1 O13 114.1(3) 1_554 2_867
O40 K1 O4 120.9(3) 1_554 .
O13 K1 O4 124.7(3) 2_867 .
O40 K1 O2W 78.4(3) 1_554 .
O13 K1 O2W 129.3(3) 2_867 .
O4 K1 O2W 69.0(3) . .
O40 K1 O11 81.8(3) 1_554 .
O13 K1 O11 130.9(3) 2_867 .
O4 K1 O11 57.4(2) . .
O2W K1 O11 98.6(3) . .
O40 K1 O1W 132.1(3) 1_554 .
O13 K1 O1W 68.4(3) 2_867 .
O4 K1 O1W 78.3(3) . .
O2W K1 O1W 68.3(3) . .
O11 K1 O1W 135.2(3) . .
O40 K1 O3 78.8(3) 1_554 2_867
O13 K1 O3 50.3(2) 2_867 2_867
O4 K1 O3 136.9(3) . 2_867
O2W K1 O3 152.6(2) . 2_867
O11 K1 O3 93.0(2) . 2_867
O1W K1 O3 118.7(3) . 2_867
O40 K1 O4 120.7(3) 1_554 2_867
O13 K1 O4 49.6(2) 2_867 2_867
O4 K1 O4 95.5(2) . 2_867
O2W K1 O4 160.5(2) . 2_867
O11 K1 O4 81.8(2) . 2_867
O1W K1 O4 97.6(3) . 2_867
O3 K1 O4 45.91(19) 2_867 2_867
O40 K1 O30W 73.3(3) 1_554 .
O13 K1 O30W 72.2(2) 2_867 .
O4 K1 O30W 127.2(3) . .
O2W K1 O30W 64.9(2) . .
O11 K1 O30W 152.2(3) . .
O1W K1 O30W 61.9(3) . .
O3 K1 O30W 94.0(2) 2_867 .
O4 K1 O30W 121.5(2) 2_867 .
O40 K1 W3 97.2(2) 1_554 .
O13 K1 W3 139.8(2) 2_867 .
O4 K1 W3 30.65(16) . .
O2W K1 W3 79.39(19) . .
O11 K1 W3 27.65(16) . .
O1W K1 W3 108.9(2) . .
O3 K1 W3 118.49(17) 2_867 .
O4 K1 W3 93.39(15) 2_867 .
O30W K1 W3 144.15(18) . .
O40 K1 Na5 96.2(2) 1_554 .
O13 K1 Na5 90.6(2) 2_867 .
O4 K1 Na5 88.0(2) . .
O2W K1 Na5 38.8(2) . .
O11 K1 Na5 135.6(2) . .
O1W K1 Na5 37.3(2) . .
O3 K1 Na5 130.44(18) 2_867 .
O4 K1 Na5 132.86(18) 2_867 .
O30W K1 Na5 39.34(17) . .
W3 K1 Na5 111.07(12) . .
O40 K1 W3 135.3(2) 1_554 2_867
O13 K1 W3 27.95(18) 2_867 2_867
O4 K1 W3 99.77(19) . 2_867
O2W K1 W3 138.0(2) . 2_867
O11 K1 W3 109.0(2) . 2_867
O1W K1 W3 69.8(2) . 2_867
O3 K1 W3 57.98(14) 2_867 2_867
O4 K1 W3 29.82(13) 2_867 2_867
O30W K1 W3 97.45(17) . 2_867
W3 K1 W3 112.02(8) . 2_867
Na5 K1 W3 103.23(12) . 2_867
O33 K2 O35 112.1(3) 2_868 .
O33 K2 O4W 78.3(4) 2_868 .
O35 K2 O4W 123.5(4) . .
O33 K2 O14 132.8(3) 2_868 2_868
O35 K2 O14 113.5(3) . 2_868
O4W K2 O14 86.1(4) . 2_868
O33 K2 O5W 75.7(3) 2_868 .
O35 K2 O5W 113.5(3) . .
O4W K2 O5W 122.7(4) . .
O14 K2 O5W 76.2(3) 2_868 .
O33 K2 O39 134.9(3) 2_868 .
O35 K2 O39 52.5(2) . .
O4W K2 O39 80.2(4) . .
O14 K2 O39 84.1(3) 2_868 .
O5W K2 O39 147.8(3) . .
O33 K2 O36 86.2(3) 2_868 .
O35 K2 O36 52.5(2) . .
O4W K2 O36 74.5(4) . .
O14 K2 O36 131.8(3) 2_868 .
O5W K2 O36 150.6(3) . .
O39 K2 O36 49.8(2) . .
O33 K2 W10 139.2(2) 2_868 .
O35 K2 W10 29.00(19) . .
O4W K2 W10 110.8(4) . .
O14 K2 W10 88.0(2) 2_868 .
O5W K2 W10 122.2(2) . .
O39 K2 W10 30.67(17) . .
O36 K2 W10 60.38(16) . .
O33 K2 W8 87.1(2) 2_868 .
O35 K2 W8 30.01(19) . .
O4W K2 W8 103.9(4) . .
O14 K2 W8 140.1(2) 2_868 .
O5W K2 W8 124.5(2) . .
O39 K2 W8 60.51(17) . .
O36 K2 W8 29.85(16) . .
W10 K2 W8 52.23(5) . .
O33 K2 Na2 88.7(2) 2_868 2_767
O35 K2 Na2 78.3(2) . 2_767
O4W K2 Na2 157.5(4) . 2_767
O14 K2 Na2 89.5(2) 2_868 2_767
O5W K2 Na2 35.2(2) . 2_767
O39 K2 Na2 121.3(2) . 2_767
O36 K2 Na2 123.4(2) . 2_767
W10 K2 Na2 90.99(12) . 2_767
W8 K2 Na2 93.58(12) . 2_767
O6W Na1 O14W 88.3(5) . .
O6W Na1 O10W 179.0(5) . .
O14W Na1 O10W 92.6(4) . .
O6W Na1 O13W 86.7(5) . .
O14W Na1 O13W 175.0(5) . .
O10W Na1 O13W 92.4(5) . .
O6W Na1 O15W 88.1(4) . 2_666
O14W Na1 O15W 92.3(4) . 2_666
O10W Na1 O15W 92.4(4) . 2_666
O13W Na1 O15W 87.7(4) . 2_666
O6W Na1 O30W 88.4(4) . .
O14W Na1 O30W 89.2(4) . .
O10W Na1 O30W 91.1(4) . .
O13W Na1 O30W 90.5(4) . .
O15W Na1 O30W 176.1(4) 2_666 .
O6W Na1 Na5 93.8(4) . .
O14W Na1 Na5 44.4(3) . .
O10W Na1 Na5 86.5(4) . .
O13W Na1 Na5 135.9(3) . .
O15W Na1 Na5 136.4(3) 2_666 .
O30W Na1 Na5 45.5(2) . .
O6W Na1 Na2 80.5(4) . 2_666
O14W Na1 Na2 134.5(3) . 2_666
O10W Na1 Na2 99.2(4) . 2_666
O13W Na1 Na2 44.5(3) . 2_666
O15W Na1 Na2 43.8(2) 2_666 2_666
O30W Na1 Na2 133.8(3) . 2_666
Na5 Na1 Na2 174.3(2) . 2_666
O26W Na2 O9W 86.7(5) . .
O26W Na2 O5W 88.0(5) . 2_767
O9W Na2 O5W 95.3(4) . 2_767
O26W Na2 O15W 100.9(5) . .
O9W Na2 O15W 170.1(4) . .
O5W Na2 O15W 91.2(4) 2_767 .
O26W Na2 O29W 170.9(6) . .
O9W Na2 O29W 88.2(4) . .
O5W Na2 O29W 100.0(4) 2_767 .
O15W Na2 O29W 83.4(4) . .
O26W Na2 O13W 95.6(6) . 2_666
O9W Na2 O13W 85.4(4) . 2_666
O5W Na2 O13W 176.4(5) 2_767 2_666
O15W Na2 O13W 87.6(4) . 2_666
O29W Na2 O13W 76.4(4) . 2_666
O26W Na2 Na3 131.2(5) . .
O9W Na2 Na3 44.6(3) . .
O5W Na2 Na3 92.9(3) 2_767 .
O15W Na2 Na3 127.8(3) . .
O29W Na2 Na3 44.7(3) . .
O13W Na2 Na3 85.2(3) 2_666 .
O26W Na2 Na1 95.6(5) . 2_666
O9W Na2 Na1 129.5(3) . 2_666
O5W Na2 Na1 135.1(3) 2_767 2_666
O15W Na2 Na1 44.1(3) . 2_666
O29W Na2 Na1 81.8(3) . 2_666
O13W Na2 Na1 44.1(3) 2_666 2_666
Na3 Na2 Na1 116.4(2) . 2_666
O26W Na2 K2 61.4(4) . 2_767
O9W Na2 K2 122.0(3) . 2_767
O5W Na2 K2 42.0(3) 2_767 2_767
O15W Na2 K2 67.6(3) . 2_767
O29W Na2 K2 127.7(3) . 2_767
O13W Na2 K2 140.0(3) 2_666 2_767
Na3 Na2 K2 134.84(19) . 2_767
Na1 Na2 K2 102.37(17) 2_666 2_767
O24W Na3 O9W 84.9(5) . .
O24W Na3 O29W 86.2(4) . .
O9W Na3 O29W 87.8(4) . .
O24W Na3 O22W 89.2(5) . .
O9W Na3 O22W 95.3(6) . .
O29W Na3 O22W 174.2(5) . .
O24W Na3 O8W 89.7(5) . .
O9W Na3 O8W 173.5(4) . .
O29W Na3 O8W 88.1(4) . .
O22W Na3 O8W 88.3(5) . .
O24W Na3 O20 158.9(4) . 1_454
O9W Na3 O20 102.5(4) . 1_454
O29W Na3 O20 74.5(3) . 1_454
O22W Na3 O20 109.4(5) . 1_454
O8W Na3 O20 81.3(3) . 1_454
O24W Na3 O21 148.8(4) . 1_454
O9W Na3 O21 70.6(3) . 1_454
O29W Na3 O21 111.0(4) . 1_454
O22W Na3 O21 74.7(4) . 1_454
O8W Na3 O21 115.7(4) . 1_454
O20 Na3 O21 50.4(3) 1_454 1_454
O24W Na3 C1 172.0(5) . 1_454
O9W Na3 C1 87.0(4) . 1_454
O29W Na3 C1 93.4(4) . 1_454
O22W Na3 C1 91.7(4) . 1_454
O8W Na3 C1 98.3(4) . 1_454
O20 Na3 C1 25.1(3) 1_454 1_454
O21 Na3 C1 25.3(3) 1_454 1_454
O24W Na3 Na2 91.6(4) . .
O9W Na3 Na2 44.0(3) . .
O29W Na3 Na2 45.0(3) . .
O22W Na3 Na2 138.9(5) . .
O8W Na3 Na2 132.8(3) . .
O20 Na3 Na2 80.9(3) 1_454 .
O21 Na3 Na2 84.0(3) 1_454 .
C1 Na3 Na2 82.5(3) 1_454 .
O24W Na3 Na4 61.6(4) . 1_455
O9W Na3 Na4 134.3(4) . 1_455
O29W Na3 Na4 117.5(4) . 1_455
O22W Na3 Na4 56.9(4) . 1_455
O8W Na3 Na4 44.5(3) . 1_455
O20 Na3 Na4 120.0(3) 1_454 1_455
O21 Na3 Na4 124.3(3) 1_454 1_455
C1 Na3 Na4 125.1(3) 1_454 1_455
Na2 Na3 Na4 151.2(2) . 1_455
Na4' Na4 O8W 68.8(12) . 1_655
Na4' Na4 O19 115.9(12) . 1_454
O8W Na4 O19 124.4(5) 1_655 1_454
Na4' Na4 O41 65.8(11) . 1_454
O8W Na4 O41 128.8(7) 1_655 1_454
O19 Na4 O41 61.3(3) 1_454 1_454
Na4' Na4 O18 59.6(12) . 1_454
O8W Na4 O18 75.7(4) 1_655 1_454
O19 Na4 O18 64.9(3) 1_454 1_454
O41 Na4 O18 61.7(3) 1_454 1_454
Na4' Na4 Na10 52.8(13) . 1_655
O8W Na4 Na10 77.8(7) 1_655 1_655
O19 Na4 Na10 152.5(7) 1_454 1_655
O41 Na4 Na10 92.6(6) 1_454 1_655
O18 Na4 Na10 112.3(8) 1_454 1_655
Na4' Na4 Na3 106.9(12) . 1_655
O8W Na4 Na3 40.1(3) 1_655 1_655
O19 Na4 Na3 96.4(4) 1_454 1_655
O41 Na4 Na3 144.3(4) 1_454 1_655
O18 Na4 Na3 84.1(3) 1_454 1_655
Na10 Na4 Na3 110.8(6) 1_655 1_655
Na4' Na4 Na4 130.6(14) . 2_776
O8W Na4 Na4 108.1(4) 1_655 2_776
O19 Na4 Na4 105.9(6) 1_454 2_776
O41 Na4 Na4 118.9(5) 1_454 2_776
O18 Na4 Na4 169.7(8) 1_454 2_776
Na10 Na4 Na4 78.0(6) 1_655 2_776
Na3 Na4 Na4 92.9(4) 1_655 2_776
Na4' Na4 Eu1 78.5(11) . 1_454
O8W Na4 Eu1 111.1(4) 1_655 1_454
O19 Na4 Eu1 37.4(2) 1_454 1_454
O41 Na4 Eu1 37.7(2) 1_454 1_454
O18 Na4 Eu1 35.75(19) 1_454 1_454
Na10 Na4 Eu1 124.3(6) 1_655 1_454
Na3 Na4 Eu1 107.6(3) 1_655 1_454
Na4 Na4 Eu1 138.0(5) 2_776 1_454
Na4 Na4' O18W 163.9(18) . .
Na4 Na4' Na10 101.1(15) . 1_655
O18W Na4' Na10 82.9(11) . 1_655
Na4 Na4' O8W 81.7(12) . 1_655
O18W Na4' O8W 113.9(11) . 1_655
Na10 Na4' O8W 92.1(10) 1_655 1_655
Na4 Na4' O18 93.3(14) . 1_454
O18W Na4' O18 84.3(10) . 1_454
Na10 Na4' O18 165.0(13) 1_655 1_454
O8W Na4' O18 86.0(8) 1_655 1_454
Na4 Na4' O41 85.8(12) . 1_454
O18W Na4' O41 78.4(9) . 1_454
Na10 Na4' O41 114.2(12) 1_655 1_454
O8W Na4' O41 152.6(11) 1_655 1_454
O18 Na4' O41 70.5(7) 1_454 1_454
Na4 Na4' Eu1 82.0(11) . 1_454
O18W Na4' Eu1 87.1(9) . 1_454
Na10 Na4' Eu1 151.5(11) 1_655 1_454
O8W Na4' Eu1 116.3(8) 1_655 1_454
O18 Na4' Eu1 34.6(4) 1_454 1_454
O41 Na4' Eu1 37.4(4) 1_454 1_454
Na4 Na4' Na8 124.2(14) . 2_676
O18W Na4' Na8 46.5(7) . 2_676
Na10 Na4' Na8 53.6(8) 1_655 2_676
O8W Na4' Na8 137.9(9) 1_655 2_676
O18 Na4' Na8 120.4(8) 1_454 2_676
O41 Na4' Na8 68.6(6) 1_454 2_676
Eu1 Na4' Na8 101.0(6) 1_454 2_676
O1W Na5 Na9 177.9(5) . 1_656
O1W Na5 O2W 89.9(4) . .
Na9 Na5 O2W 89.0(4) 1_656 .
O1W Na5 O14W 95.2(5) . .
Na9 Na5 O14W 85.8(4) 1_656 .
O2W Na5 O14W 174.6(5) . .
O1W Na5 O3W 90.5(4) . .
Na9 Na5 O3W 91.4(4) 1_656 .
O2W Na5 O3W 89.5(4) . .
O14W Na5 O3W 91.9(4) . .
O1W Na5 O30W 88.4(4) . .
Na9 Na5 O30W 89.8(4) 1_656 .
O2W Na5 O30W 89.4(4) . .
O14W Na5 O30W 89.3(4) . .
O3W Na5 O30W 178.4(4) . .
O1W Na5 Na6 135.7(4) . .
Na9 Na5 Na6 46.2(3) 1_656 .
O2W Na5 Na6 89.9(3) . .
O14W Na5 Na6 87.4(3) . .
O3W Na5 Na6 45.2(3) . .
O30W Na5 Na6 135.9(3) . .
O1W Na5 Na1 86.6(4) . .
Na9 Na5 Na1 92.9(3) 1_656 .
O2W Na5 Na1 135.7(3) . .
O14W Na5 Na1 43.6(3) . .
O3W Na5 Na1 134.7(3) . .
O30W Na5 Na1 46.4(2) . .
Na6 Na5 Na1 122.1(2) . .
O1W Na5 K1 52.4(3) . .
Na9 Na5 K1 125.7(3) 1_656 .
O2W Na5 K1 49.3(3) . .
O14W Na5 K1 133.8(3) . .
O3W Na5 K1 116.8(3) . .
O30W Na5 K1 61.6(3) . .
Na6 Na5 K1 138.6(2) . .
Na1 Na5 K1 96.61(16) . .
O21W Na6 O3W 90.0(5) . .
O21W Na6 O12W 174.2(6) . .
O3W Na6 O12W 84.2(4) . .
O21W Na6 O27W 92.8(5) . .
O3W Na6 O27W 176.3(5) . .
O12W Na6 O27W 92.9(5) . .
O21W Na6 Na9 86.3(4) . 1_656
O3W Na6 Na9 89.9(4) . 1_656
O12W Na6 Na9 93.6(4) . 1_656
O27W Na6 Na9 87.9(5) . 1_656
O21W Na6 O23W 94.2(5) . .
O3W Na6 O23W 94.8(4) . .
O12W Na6 O23W 86.3(5) . .
O27W Na6 O23W 87.4(5) . .
Na9 Na6 O23W 175.3(5) 1_656 .
O21W Na6 Na5 86.5(4) . .
O3W Na6 Na5 45.5(3) . .
O12W Na6 Na5 89.5(4) . .
O27W Na6 Na5 132.3(4) . .
Na9 Na6 Na5 44.4(3) 1_656 .
O23W Na6 Na5 140.3(4) . .
O21W Na6 Na7 129.4(4) . 1_656
O3W Na6 Na7 59.2(3) . 1_656
O12W Na6 Na7 47.0(3) . 1_656
O27W Na6 Na7 120.3(5) . 1_656
Na9 Na6 Na7 128.1(3) 1_656 1_656
O23W Na6 Na7 54.6(4) . 1_656
Na5 Na6 Na7 95.3(2) . 1_656
O25W Na7 O17 124.0(6) 1_454 1_354
O25W Na7 O6 113.8(6) 1_454 1_454
O17 Na7 O6 106.9(4) 1_354 1_454
O25W Na7 O12W 51.9(5) 1_454 1_454
O17 Na7 O12W 123.0(5) 1_354 1_454
O6 Na7 O12W 66.2(4) 1_454 1_454
O25W Na7 O19W 50.7(5) 1_454 1_454
O17 Na7 O19W 99.1(4) 1_354 1_454
O6 Na7 O19W 153.7(5) 1_454 1_454
O12W Na7 O19W 102.6(5) 1_454 1_454
O25W Na7 Na6 59.6(5) 1_454 1_454
O17 Na7 Na6 88.5(3) 1_354 1_454
O6 Na7 Na6 85.0(3) 1_454 1_454
O12W Na7 Na6 36.4(3) 1_454 1_454
O19W Na7 Na6 99.5(4) 1_454 1_454
O25W Na7 Eu1 133.9(5) 1_454 1_454
O17 Na7 Eu1 97.5(3) 1_354 1_454
O6 Na7 Eu1 64.7(2) 1_454 1_454
O12W Na7 Eu1 123.2(3) 1_454 1_454
O19W Na7 Eu1 108.8(4) 1_454 1_454
Na6 Na7 Eu1 149.6(3) 1_454 1_454
O29 Na8 O44 166.0(7) 1_354 2_777
O29 Na8 O37 105.5(5) 1_354 1_454
O44 Na8 O37 64.7(3) 2_777 1_454
O29 Na8 O18W 106.0(6) 1_354 2_676
O44 Na8 O18W 83.8(5) 2_777 2_676
O37 Na8 O18W 148.4(6) 1_454 2_676
O29 Na8 Na10 86.7(6) 1_354 2_576
O44 Na8 Na10 90.2(6) 2_777 2_576
O37 Na8 Na10 121.6(8) 1_454 2_576
O18W Na8 Na10 58.3(7) 2_676 2_576
O29 Na8 Na4' 116.2(6) 1_354 2_676
O44 Na8 Na4' 67.4(5) 2_777 2_676
O37 Na8 Na4' 126.7(5) 1_454 2_676
O18W Na8 Na4' 31.2(5) 2_676 2_676
Na10 Na8 Na4' 37.5(6) 2_576 2_676
O29 Na8 Eu2 138.1(5) 1_354 1_454
O44 Na8 Eu2 35.9(2) 2_777 1_454
O37 Na8 Eu2 34.3(2) 1_454 1_454
O18W Na8 Eu2 115.2(5) 2_676 1_454
Na10 Na8 Eu2 120.8(6) 2_576 1_454
Na4' Na8 Eu2 103.3(4) 2_676 1_454
Na5 Na9 Na6 89.5(4) 1_454 1_454
Na5 Na9 O25 121.4(4) 1_454 1_453
Na6 Na9 O25 123.0(5) 1_454 1_453
Na4' Na10 O31 147.0(14) 1_455 2_777
Na4' Na10 O22 138.9(12) 1_455 2_777
O31 Na10 O22 62.3(5) 2_777 2_777
Na4' Na10 Na4 26.1(6) 1_455 1_455
O31 Na10 Na4 167.8(13) 2_777 1_455
O22 Na10 Na4 117.4(9) 2_777 1_455
Na4' Na10 Na8 88.9(8) 1_455 2_576
O31 Na10 Na8 83.5(7) 2_777 2_576
O22 Na10 Na8 130.8(10) 2_777 2_576
Na4 Na10 Na8 103.4(6) 1_455 2_576
Na4' Na10 Eu2 143.3(12) 1_455 2_777
O31 Na10 Eu2 33.2(3) 2_777 2_777
O22 Na10 Eu2 35.8(3) 2_777 2_777
Na4 Na10 Eu2 139.8(8) 1_455 2_777
Na8 Na10 Eu2 116.4(7) 2_576 2_777
W1 O2 Eu1 125.5(4) . .
W4 O3 W1 115.7(4) . .
W4 O3 K1 90.9(3) . 2_867
W1 O3 K1 115.2(3) . 2_867
W3 O4 W1 116.3(4) . .
W3 O4 K1 99.8(3) . .
W1 O4 K1 140.4(4) . .
W3 O4 K1 88.3(3) . 2_867
W1 O4 K1 111.0(3) . 2_867
K1 O4 K1 84.5(2) . 2_867
W5 O5 W4 90.5(3) . .
W5 O5 W1 176.8(4) . .
W4 O5 W1 90.0(3) . .
W5 O5 W3 91.9(3) . .
W4 O5 W3 92.0(3) . .
W1 O5 W3 91.3(3) . .
W5 O5 W2 89.9(3) . .
W4 O5 W2 177.0(4) . .
W1 O5 W2 89.5(3) . .
W3 O5 W2 91.0(3) . .
W5 O5 Eu1 88.2(2) . .
W4 O5 Eu1 88.8(2) . .
W1 O5 Eu1 88.7(2) . .
W3 O5 Eu1 179.3(3) . .
W2 O5 Eu1 88.3(2) . .
W2 O6 W1 114.5(4) . .
W2 O6 Na7 103.9(4) . 1_656
W1 O6 Na7 102.2(3) . 1_656
W2 O8 Eu1 124.9(4) . .
W5 O9 W2 116.0(4) . .
W3 O10 W2 117.4(4) . .
W3 O11 K1 98.3(3) . .
W3 O12 W5 115.9(4) . .
W3 O13 W4 116.8(4) . .
W3 O13 K1 110.4(4) . 2_867
W4 O13 K1 109.6(3) . 2_867
W4 O14 K2 140.8(4) . 2_868
W4 O15 Eu1 124.4(4) . .
W5 O16 W4 115.4(4) . .
W5 O17 Na7 143.9(5) . 1_756
W5 O18 Eu1 125.1(4) . .
W5 O18 Na4' 123.3(7) . 1_656
Eu1 O18 Na4' 107.6(6) . 1_656
W5 O18 Na4 137.5(4) . 1_656
Eu1 O18 Na4 97.3(3) . 1_656
Na4' O18 Na4 27.1(6) 1_656 1_656
C2 O19 Eu1 120.8(8) . .
C2 O19 Na4 135.7(9) . 1_656
Eu1 O19 Na4 98.9(4) . 1_656
C1 O20 Eu1 119.6(7) . .
C1 O20 Na3 94.6(7) . 1_656
Eu1 O20 Na3 145.4(4) . 1_656
C1 O21 Eu2 119.3(8) . .
C1 O21 Na3 90.7(7) . 1_656
Eu2 O21 Na3 149.9(4) . 1_656
C2 O22 Eu2 120.9(8) . .
C2 O22 Na10 137.6(10) . 2_777
Eu2 O22 Na10 100.3(6) . 2_777
W6 O24 Eu2 125.1(4) . .
W9 O25 W6 115.3(4) . .
W9 O25 Na9 113.4(4) . 1_657
W6 O25 Na9 123.0(4) . 1_657
W9 O26 W8 89.9(3) . .
W9 O26 W6 90.5(3) . .
W8 O26 W6 177.1(4) . .
W9 O26 W7 176.6(4) . .
W8 O26 W7 89.6(3) . .
W6 O26 W7 89.9(3) . .
W9 O26 W10 91.9(3) . .
W8 O26 W10 91.5(3) . .
W6 O26 W10 91.4(3) . .
W7 O26 W10 91.5(3) . .
W9 O26 Eu2 88.8(2) . .
W8 O26 Eu2 88.4(2) . .
W6 O26 Eu2 88.7(2) . .
W7 O26 Eu2 87.8(2) . .
W10 O26 Eu2 179.3(4) . .
W10 O27 W6 116.7(4) . .
W6 O28 W7 116.1(4) . .
W7 O29 Na8 133.5(6) . 1_756
W10 O30 W7 116.8(4) . .
W7 O31 Eu2 124.8(4) . .
W7 O31 Na10 130.9(6) . 2_777
Eu2 O31 Na10 104.0(5) . 2_777
W7 O32 W8 116.0(4) . .
W8 O33 K2 145.2(5) . 2_868
W8 O34 Eu2 123.3(4) . .
W10 O35 W8 117.1(4) . .
W10 O35 K2 106.8(4) . .
W8 O35 K2 107.9(4) . .
W8 O36 W9 116.4(4) . .
W8 O36 K2 95.8(3) . .
W9 O36 K2 110.4(3) . .
W9 O37 Eu2 124.5(4) . .
W9 O37 Na8 103.8(4) . 1_656
Eu2 O37 Na8 100.8(4) . 1_656
W10 O39 W9 115.7(4) . .
W10 O39 K2 92.9(3) . .
W9 O39 K2 108.5(3) . .
W10 O40 K1 138.4(5) . 1_556
C4 O41 Eu1 120.7(7) . .
C4 O41 Na4' 135.8(10) . 1_656
Eu1 O41 Na4' 103.3(6) . 1_656
C4 O41 Na4 135.2(8) . 1_656
Eu1 O41 Na4 98.1(4) . 1_656
Na4' O41 Na4 28.4(6) 1_656 1_656
C3 O42 Eu1 122.6(8) . .
C3 O43 Eu2 121.4(8) . 2_878
C4 O44 Eu2 120.2(8) . 2_878
C4 O44 Na8 116.1(8) . 2_777
Eu2 O44 Na8 101.4(4) 2_878 2_777
O20 C1 O21 124.2(11) . .
O20 C1 C2 117.0(10) . .
O21 C1 C2 118.8(11) . .
O20 C1 Na3 60.4(6) . 1_656
O21 C1 Na3 63.9(6) . 1_656
C2 C1 Na3 174.6(9) . 1_656
O19 C2 O22 127.9(12) . .
O19 C2 C1 117.2(10) . .
O22 C2 C1 114.8(10) . .
O19 C2 Eu1 40.5(6) . .
O22 C2 Eu1 168.4(9) . .
C1 C2 Eu1 76.7(6) . .
O42 C3 O43 128.4(11) . .
O42 C3 C4 115.7(10) . .
O43 C3 C4 115.9(10) . .
O41 C4 O44 126.8(11) . .
O41 C4 C3 116.2(10) . .
O44 C4 C3 116.9(10) . .
Na5 O1W K1 90.3(4) . .
Na5 O2W K1 91.9(4) . .
Na6 O3W Na5 89.2(4) . .
Na2 O5W K2 102.8(4) 2_767 .
Na3 O8W Na4' 122.9(7) . 1_455
Na3 O8W Na4 95.4(5) . 1_455
Na4' O8W Na4 29.5(6) 1_455 1_455
Na2 O9W Na3 91.4(4) . .
Na6 O12W Na7 96.7(4) . 1_656
Na1 O13W Na2 91.4(4) . 2_666
Na1 O14W Na5 92.1(4) . .
Na2 O15W Na1 92.1(3) . 2_666
O16W O16W O28W 79.5(13) 2_877 2_777
Na4' O18W Na8 102.3(10) . 2_676
Na3 O29W Na2 90.3(4) . .
Na5 O30W Na1 88.1(3) . .
Na5 O30W K1 79.0(3) . .
Na1 O30W K1 132.6(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O1 1.753(9) .
W1 O2 1.771(8) .
W1 O3 1.938(8) .
W1 O6 1.974(8) .
W1 O4 2.020(8) .
W1 O5 2.327(8) .
W1 Eu1 3.7229(8) .
W2 O7 1.698(9) .
W2 O8 1.812(8) .
W2 O6 1.937(8) .
W2 O9 1.942(8) .
W2 O10 1.993(8) .
W2 O5 2.344(8) .
W2 Eu1 3.7208(8) .
W3 O11 1.723(8) .
W3 O4 1.901(8) .
W3 O12 1.905(8) .
W3 O13 1.910(8) .
W3 O10 1.911(9) .
W3 O5 2.332(7) .
W3 K1 3.675(3) .
W3 K1 3.821(3) 2_867
W4 O14 1.743(8) .
W4 O15 1.795(8) .
W4 O3 1.931(8) .
W4 O16 1.936(8) .
W4 O13 2.006(8) .
W4 O5 2.305(8) .
W4 Eu1 3.7120(8) .
W4 K1 3.874(3) 2_867
W5 O17 1.711(8) .
W5 O18 1.783(8) .
W5 O9 1.929(9) .
W5 O16 1.935(8) .
W5 O12 2.025(8) .
W5 O5 2.305(8) .
W5 Eu1 3.6924(8) .
W6 O23 1.733(8) .
W6 O24 1.799(8) .
W6 O28 1.918(8) .
W6 O25 1.959(9) .
W6 O27 2.016(8) .
W6 O26 2.325(7) .
W6 Eu2 3.7132(7) .
W7 O29 1.708(9) .
W7 O31 1.798(8) .
W7 O32 1.926(9) .
W7 O28 1.955(8) .
W7 O30 2.008(9) .
W7 O26 2.326(8) .
W7 Eu2 3.6850(8) .
W8 O33 1.723(9) .
W8 O34 1.796(8) .
W8 O36 1.925(9) .
W8 O32 1.937(9) .
W8 O35 2.022(9) .
W8 O26 2.324(8) .
W8 Eu2 3.7038(8) .
W8 K2 3.848(4) .
W9 O38 1.739(9) .
W9 O37 1.799(8) .
W9 O36 1.926(8) .
W9 O25 1.935(8) .
W9 O39 2.037(9) .
W9 O26 2.310(8) .
W9 Eu2 3.7075(8) .
W10 O40 1.748(9) .
W10 O35 1.885(9) .
W10 O27 1.897(8) .
W10 O39 1.901(9) .
W10 O30 1.909(9) .
W10 O26 2.332(8) .
W10 K2 3.723(4) .
Eu1 O18 2.368(8) .
Eu1 O8 2.373(8) .
Eu1 O15 2.390(8) .
Eu1 O2 2.404(9) .
Eu1 O20 2.455(8) .
Eu1 O42 2.464(8) .
Eu1 O19 2.472(8) .
Eu1 O41 2.481(9) .
Eu1 O5 2.960(7) .
Eu1 C2 3.269(11) .
Eu2 O31 2.350(8) .
Eu2 O24 2.375(8) .
Eu2 O37 2.379(8) .
Eu2 O34 2.401(8) .
Eu2 O21 2.454(8) .
Eu2 O43 2.477(9) 2_878
Eu2 O22 2.478(8) .
Eu2 O44 2.481(8) 2_878
Eu2 O26 2.948(8) .
K1 O40 2.684(9) 1_554
K1 O13 2.710(9) 2_867
K1 O4 2.837(8) .
K1 O2W 2.898(11) .
K1 O11 3.007(10) .
K1 O1W 3.028(13) .
K1 O3 3.328(8) 2_867
K1 O4 3.371(9) 2_867
K1 O30W 3.422(10) .
K1 Na5 3.819(7) .
K1 W3 3.821(3) 2_867
K2 O33 2.680(9) 2_868
K2 O35 2.712(10) .
K2 O4W 2.732(16) .
K2 O14 2.754(9) 2_868
K2 O5W 2.820(11) .
K2 O39 3.105(9) .
K2 O36 3.141(9) .
K2 Na2 4.109(7) 2_767
Na1 O6W 2.370(12) .
Na1 O14W 2.382(11) .
Na1 O10W 2.386(12) .
Na1 O13W 2.442(12) .
Na1 O15W 2.443(11) 2_666
Na1 O30W 2.503(10) .
Na1 Na5 3.456(8) .
Na1 Na2 3.507(8) 2_666
Na2 O26W 2.316(19) .
Na2 O9W 2.405(11) .
Na2 O5W 2.428(11) 2_767
Na2 O15W 2.430(11) .
Na2 O29W 2.448(12) .
Na2 O13W 2.460(11) 2_666
Na2 Na3 3.464(8) .
Na2 Na1 3.507(8) 2_666
Na2 K2 4.109(7) 2_767
Na3 O24W 2.419(13) .
Na3 O9W 2.434(12) .
Na3 O29W 2.437(11) .
Na3 O22W 2.440(15) .
Na3 O8W 2.498(13) .
Na3 O20 2.602(10) 1_454
Na3 O21 2.681(10) 1_454
Na3 C1 2.984(13) 1_454
Na3 Na4 3.859(13) 1_455
Na4 Na4' 1.35(3) .
Na4 O8W 2.716(15) 1_655
Na4 O19 2.811(14) 1_454
Na4 O41 2.833(13) 1_454
Na4 O18 2.963(15) 1_454
Na4 Na10 3.02(3) 1_655
Na4 Na3 3.859(13) 1_655
Na4 Na4 3.98(3) 2_776
Na4 Eu1 4.020(9) 1_454
Na4' O18W 2.13(3) .
Na4' Na10 2.45(3) 1_655
Na4' O8W 2.56(3) 1_655
Na4' O18 2.56(3) 1_454
Na4' O41 2.59(2) 1_454
Na4' Eu1 3.98(2) 1_454
Na4' Na8 4.02(3) 2_676
Na5 O1W 2.312(13) .
Na5 Na9 2.384(12) 1_656
Na5 O2W 2.395(11) .
Na5 O14W 2.418(12) .
Na5 O3W 2.433(11) .
Na5 O30W 2.466(10) .
Na5 Na6 3.408(9) .
Na6 O21W 2.390(14) .
Na6 O3W 2.419(13) .
Na6 O12W 2.429(13) .
Na6 O27W 2.431(18) .
Na6 Na9 2.458(12) 1_656
Na6 O23W 2.460(14) .
Na6 Na7 4.070(12) 1_656
Na7 O25W 2.294(19) 1_454
Na7 O17 2.823(13) 1_354
Na7 O6 2.991(13) 1_454
Na7 O12W 2.996(15) 1_454
Na7 O19W 3.016(18) 1_454
Na7 Na6 4.070(12) 1_454
Na7 Eu1 4.311(9) 1_454
Na8 O29 2.805(15) 1_354
Na8 O44 2.872(14) 2_777
Na8 O37 2.981(16) 1_454
Na8 O18W 2.99(2) 2_676
Na8 Na10 3.24(3) 2_576
Na8 Na4' 4.02(3) 2_676
Na8 Eu2 4.149(12) 1_454
Na9 Na5 2.384(12) 1_454
Na9 Na6 2.458(12) 1_454
Na9 O25 2.805(12) 1_453
Na10 Na4' 2.45(3) 1_455
Na10 O31 2.92(2) 2_777
Na10 O22 2.94(2) 2_777
Na10 Na4 3.02(3) 1_455
Na10 Na8 3.24(3) 2_576
Na10 Eu2 4.169(19) 2_777
O3 K1 3.328(8) 2_867
O4 K1 3.371(9) 2_867
O6 Na7 2.991(13) 1_656
O13 K1 2.710(9) 2_867
O14 K2 2.754(9) 2_868
O17 Na7 2.823(14) 1_756
O18 Na4' 2.56(3) 1_656
O18 Na4 2.963(15) 1_656
O19 C2 1.219(14) .
O19 Na4 2.811(14) 1_656
O20 C1 1.269(14) .
O20 Na3 2.602(10) 1_656
O21 C1 1.276(14) .
O21 Na3 2.681(10) 1_656
O22 C2 1.275(13) .
O22 Na10 2.94(2) 2_777
O25 Na9 2.805(12) 1_657
O29 Na8 2.805(15) 1_756
O31 Na10 2.92(3) 2_777
O33 K2 2.680(9) 2_868
O37 Na8 2.981(16) 1_656
O40 K1 2.684(9) 1_556
O41 C4 1.247(14) .
O41 Na4' 2.59(2) 1_656
O41 Na4 2.833(13) 1_656
O42 C3 1.223(14) .
O43 C3 1.240(14) .
O43 Eu2 2.477(8) 2_878
O44 C4 1.252(14) .
O44 Eu2 2.481(8) 2_878
O44 Na8 2.872(14) 2_777
C1 C2 1.526(17) .
C1 Na3 2.984(13) 1_656
C3 C4 1.572(16) .
O5W Na2 2.428(11) 2_767
O7W O7W' 1.64(4) .
O8W Na4' 2.56(3) 1_455
O8W Na4 2.716(15) 1_455
O12W Na7 2.996(15) 1_656
O13W Na2 2.460(11) 2_666
O15W Na1 2.443(11) 2_666
O16W O16W 1.56(3) 2_877
O16W O28W 1.573(19) 2_777
O18W Na8 2.99(2) 2_676
O19W Na7 3.016(18) 1_656
O25W Na7 2.294(19) 1_656
O28W O16W 1.573(19) 2_777
