#------------------------------------------------------------------------------
#$Date: 2019-11-22 18:49:30 +0200 (Fri, 22 Nov 2019) $
#$Revision: 231222 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/51/62/4516284.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4516284
loop_
_publ_author_name
'Dong, Yun-Bo'
'Shi, Hua-Yu'
'Yang, Jin'
'Liu, Ying-Ying'
'Ma, Jian-Fang'
_publ_section_title
;
 Molecular Dumbbell, Sandwich, and Paddle-Wheel Assembled with
 Methylresorcin[4]arene Cavitands and Organooxotin Clusters
;
_journal_issue                   3
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              1546
_journal_paper_doi               10.1021/acs.cgd.5b00099
_journal_volume                  15
_journal_year                    2015
_chemical_formula_moiety         'C134 H204 O42 Sn12'
_chemical_formula_sum            'C134 H204 O42 Sn12'
_chemical_formula_weight         3911.25
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 98.435(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   20.9661(12)
_cell_length_b                   15.8372(9)
_cell_length_c                   23.0081(15)
_cell_measurement_reflns_used    8646
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      29.1710
_cell_measurement_theta_min      2.9712
_cell_volume                     7557.1(8)
_computing_cell_refinement       CrysAlis
_computing_data_collection       'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction        CrysAlis
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.2375
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.848
_diffrn_measurement_device_type  'Oxford Diffraction Gemini R Ultra'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0512
_diffrn_reflns_av_sigmaI/netI    0.1076
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            32417
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         29.24
_diffrn_reflns_theta_min         3.01
_exptl_absorpt_coefficient_mu    2.021
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.95827
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
CrysAlis (Oxford Diffraction, 2006)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.719
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3888
_exptl_crystal_size_max          0.39
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.28
_refine_diff_density_max         1.557
_refine_diff_density_min         -1.147
_refine_diff_density_rms         0.137
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.026
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     856
_refine_ls_number_reflns         17414
_refine_ls_number_restraints     68
_refine_ls_restrained_S_all      3.975
_refine_ls_R_factor_all          0.1570
_refine_ls_R_factor_gt           0.0670
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0634P)²+10.7165P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1341
_refine_ls_wR_factor_ref         0.1729
_reflns_number_gt                8646
_reflns_number_total             17414
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            cg5b00099_si_002.cif
_cod_data_source_block           3
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4516284
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sn1 Sn 0.14880(11) 0.41662(15) 0.49532(12) 0.0509(7) Uani 1 1 d .
Sn2 Sn 0.08951(11) 0.57496(15) 0.41236(11) 0.0502(7) Uani 1 1 d .
Sn3 Sn 0.00115(12) 0.41373(15) 0.37545(11) 0.0523(7) Uani 1 1 d .
Sn4 Sn 0.09469(12) 0.42206(15) 0.62213(11) 0.0519(7) Uani 1 1 d .
Sn5 Sn 0.03063(12) 0.29012(14) 0.52068(12) 0.0526(7) Uani 1 1 d .
Sn6 Sn 0.10733(11) 0.63625(14) 0.54681(11) 0.0500(7) Uani 1 1 d .
C1 C 0.471(2) 0.318(3) 0.692(3) 0.090(16) Uani 1 1 d .
C2 C 0.503(2) 0.264(3) 0.660(2) 0.074(12) Uani 1 1 d .
C3 C 0.5196(17) 0.182(3) 0.677(2) 0.068(12) Uani 1 1 d .
C4 C 0.5020(18) 0.156(3) 0.7300(18) 0.064(11) Uani 1 1 d .
H4 H 0.5125 0.1017 0.7429 0.076 Uiso 1 1 calc R
C5 C 0.4697(19) 0.207(3) 0.7643(18) 0.068(11) Uani 1 1 d .
C6 C 0.454(2) 0.287(3) 0.744(2) 0.082(14) Uani 1 1 d .
C7 C 0.454(3) 0.406(3) 0.672(3) 0.13(2) Uani 1 1 d .
H7A H 0.4318 0.4335 0.7007 0.195 Uiso 1 1 calc R
H7B H 0.4258 0.4041 0.6350 0.195 Uiso 1 1 calc R
H7C H 0.4920 0.4368 0.6677 0.195 Uiso 1 1 calc R
C8 C 0.486(3) 0.279(3) 0.555(3) 0.097(17) Uani 1 1 d .
H8A H 0.4413 0.2735 0.5615 0.117 Uiso 1 1 calc R
H8B H 0.4885 0.3263 0.5290 0.117 Uiso 1 1 calc R
C9 C 0.474(2) 0.129(3) 0.5415(19) 0.071(11) Uani 1 1 d .
C10 C 0.4975(17) 0.084(3) 0.5914(17) 0.058(10) Uani 1 1 d .
C11 C 0.5513(19) 0.124(3) 0.6363(18) 0.072(12) Uani 1 1 d .
H11 H 0.5776 0.1596 0.6142 0.086 Uiso 1 1 calc R
C12 C 0.596(2) 0.058(3) 0.669(2) 0.090(15) Uani 1 1 d .
H12A H 0.6147 0.0241 0.6416 0.135 Uiso 1 1 calc R
H12B H 0.5713 0.0223 0.6916 0.135 Uiso 1 1 calc R
H12C H 0.6293 0.0856 0.6953 0.135 Uiso 1 1 calc R
C13 C 0.423(2) 0.101(3) 0.5018(17) 0.072(12) Uani 1 1 d .
C14 C 0.3967(19) 0.024(3) 0.5134(17) 0.067(11) Uani 1 1 d .
C15 C 0.4183(18) -0.024(3) 0.5614(16) 0.060(10) Uani 1 1 d .
C16 C 0.4694(18) 0.009(3) 0.6007(16) 0.059(10) Uani 1 1 d .
H16 H 0.4846 -0.0219 0.6344 0.071 Uiso 1 1 calc R
C17 C 0.398(3) 0.151(4) 0.446(2) 0.110(19) Uani 1 1 d .
H17A H 0.4219 0.2021 0.4455 0.165 Uiso 1 1 calc R
H17B H 0.3530 0.1644 0.4468 0.165 Uiso 1 1 calc R
H17C H 0.4016 0.1177 0.4122 0.165 Uiso 1 1 calc R
C18 C 0.282(2) 0.005(4) 0.4850(19) 0.088(15) Uani 1 1 d .
H18A H 0.2816 0.0545 0.5097 0.105 Uiso 1 1 calc R
H18B H 0.2536 0.0155 0.4488 0.105 Uiso 1 1 calc R
C19 C 0.2695(19) -0.062(2) 0.5741(19) 0.062(10) Uani 1 1 d .
C20 C 0.3290(17) -0.085(2) 0.6040(19) 0.058(10) Uani 1 1 d .
C21 C 0.3841(19) -0.104(3) 0.5731(19) 0.069(11) Uani 1 1 d .
H21 H 0.3659 -0.1273 0.5346 0.083 Uiso 1 1 calc R
C22 C 0.430(2) -0.171(3) 0.603(2) 0.083(13) Uani 1 1 d .
H22A H 0.4640 -0.1813 0.5799 0.125 Uiso 1 1 calc R
H22B H 0.4068 -0.2230 0.6064 0.125 Uiso 1 1 calc R
H22C H 0.4483 -0.1522 0.6414 0.125 Uiso 1 1 calc R
C23 C 0.2163(19) -0.044(2) 0.602(2) 0.066(11) Uani 1 1 d .
C24 C 0.2246(18) -0.044(2) 0.662(2) 0.061(10) Uani 1 1 d .
C25 C 0.2849(18) -0.065(2) 0.6957(18) 0.056(10) Uani 1 1 d .
C26 C 0.3351(18) -0.085(2) 0.664(2) 0.062(11) Uani 1 1 d .
H26 H 0.3751 -0.0981 0.6853 0.074 Uiso 1 1 calc R
C27 C 0.1512(19) -0.023(3) 0.567(2) 0.086(14) Uani 1 1 d .
H27A H 0.1537 -0.0267 0.5259 0.129 Uiso 1 1 calc R
H27B H 0.1388 0.0326 0.5768 0.129 Uiso 1 1 calc R
H27C H 0.1199 -0.0632 0.5769 0.129 Uiso 1 1 calc R
C28 C 0.1565(19) 0.041(2) 0.7170(19) 0.064(10) Uani 1 1 d .
H28 H 0.1119 0.0330 0.7242 0.077 Uiso 1 1 calc R
C29 C 0.2536(19) 0.086(3) 0.7825(16) 0.060(10) Uani 1 1 d .
C30 C 0.306(2) 0.029(3) 0.7810(16) 0.062(10) Uani 1 1 d .
C31 C 0.2939(19) -0.062(3) 0.7622(18) 0.069(12) Uani 1 1 d .
H31 H 0.2522 -0.0772 0.7736 0.083 Uiso 1 1 calc R
C32 C 0.342(2) -0.125(3) 0.792(2) 0.088(14) Uani 1 1 d .
H32A H 0.3300 -0.1812 0.7783 0.132 Uiso 1 1 calc R
H32B H 0.3435 -0.1225 0.8336 0.132 Uiso 1 1 calc R
H32C H 0.3844 -0.1126 0.7822 0.132 Uiso 1 1 calc R
C33 C 0.265(2) 0.167(3) 0.7972(18) 0.071(11) Uani 1 1 d .
C34 C 0.327(2) 0.197(3) 0.8085(17) 0.070(11) Uani 1 1 d .
C35 C 0.380(2) 0.142(3) 0.8080(15) 0.066(11) Uani 1 1 d .
C36 C 0.3682(19) 0.060(3) 0.7943(15) 0.061(10) Uani 1 1 d .
H36 H 0.4028 0.0233 0.7938 0.074 Uiso 1 1 calc R
C37 C 0.210(2) 0.225(3) 0.801(2) 0.096(16) Uani 1 1 d .
H37A H 0.2264 0.2807 0.8118 0.144 Uiso 1 1 calc R
H37B H 0.1856 0.2050 0.8304 0.144 Uiso 1 1 calc R
H37C H 0.1830 0.2278 0.7637 0.144 Uiso 1 1 calc R
C38 C 0.357(3) 0.336(3) 0.774(3) 0.102(17) Uani 1 1 d .
H38A H 0.3404 0.3115 0.7357 0.122 Uiso 1 1 calc R
H38B H 0.3382 0.3913 0.7757 0.122 Uiso 1 1 calc R
C39 C 0.449(2) 0.179(3) 0.8199(19) 0.080(13) Uani 1 1 d .
H39 H 0.4456 0.2296 0.8435 0.096 Uiso 1 1 calc R
C40 C 0.494(2) 0.120(3) 0.857(2) 0.095(15) Uani 1 1 d .
H40A H 0.4760 0.1058 0.8923 0.143 Uiso 1 1 calc R
H40B H 0.5347 0.1471 0.8680 0.143 Uiso 1 1 calc R
H40C H 0.4994 0.0693 0.8357 0.143 Uiso 1 1 calc R
C41 C 0.154(2) 0.122(3) 0.6801(19) 0.070(11) Uani 1 1 d .
C42 C 0.009(2) 0.159(2) 0.516(2) 0.096(14) Uani 1 1 d U
H42A H -0.0123 0.1457 0.4771 0.116 Uiso 1 1 calc R
H42B H 0.0494 0.1275 0.5229 0.116 Uiso 1 1 calc R
C43 C -0.035(3) 0.132(4) 0.564(3) 0.125(19) Uani 1 1 d U
H43A H -0.0214 0.1629 0.5998 0.149 Uiso 1 1 calc R
H43B H -0.0792 0.1494 0.5495 0.149 Uiso 1 1 calc R
C44 C -0.036(4) 0.043(4) 0.578(3) 0.15(2) Uani 1 1 d U
H44A H -0.0475 0.0106 0.5420 0.176 Uiso 1 1 calc R
H44B H 0.0069 0.0254 0.5955 0.176 Uiso 1 1 calc R
C45 C -0.081(4) 0.025(5) 0.618(4) 0.19(3) Uani 1 1 d U
H45A H -0.0808 -0.0340 0.6261 0.290 Uiso 1 1 calc R
H45B H -0.1235 0.0420 0.5999 0.290 Uiso 1 1 calc R
H45C H -0.0691 0.0563 0.6534 0.290 Uiso 1 1 calc R
C46 C 0.005(3) 0.359(4) 0.2922(19) 0.111(15) Uani 1 1 d U
H46A H 0.0010 0.4041 0.2634 0.133 Uiso 1 1 calc R
H46B H 0.0484 0.3356 0.2930 0.133 Uiso 1 1 calc R
C47 C -0.041(4) 0.293(5) 0.270(4) 0.18(3) Uani 1 1 d U
H47A H -0.0841 0.3138 0.2711 0.220 Uiso 1 1 calc R
H47B H -0.0366 0.2809 0.2296 0.220 Uiso 1 1 calc R
C48 C -0.033(5) 0.217(7) 0.302(4) 0.21(3) Uani 1 1 d U
H48A H 0.0020 0.2294 0.3331 0.252 Uiso 1 1 calc R
H48B H -0.0714 0.2152 0.3213 0.252 Uiso 1 1 calc R
C49 C -0.023(5) 0.132(6) 0.290(4) 0.21(3) Uani 1 1 d U
H49A H -0.0345 0.0984 0.3220 0.318 Uiso 1 1 calc R
H49B H 0.0213 0.1235 0.2869 0.318 Uiso 1 1 calc R
H49C H -0.0497 0.1165 0.2544 0.318 Uiso 1 1 calc R
C50 C 0.146(2) 0.624(3) 0.353(2) 0.087(14) Uani 1 1 d .
H50A H 0.1717 0.5781 0.3414 0.105 Uiso 1 1 calc R
H50B H 0.1166 0.6409 0.3182 0.105 Uiso 1 1 calc R
C51 C 0.187(4) 0.692(5) 0.368(3) 0.16(2) Uani 1 1 d DU
H51A H 0.1609 0.7412 0.3707 0.194 Uiso 1 1 calc R
H51B H 0.2104 0.7011 0.3347 0.194 Uiso 1 1 calc R
C52 C 0.235(4) 0.690(5) 0.420(3) 0.18(3) Uani 1 1 d DU
H52A H 0.2553 0.6347 0.4211 0.217 Uiso 1 1 calc R
H52B H 0.2117 0.6925 0.4533 0.217 Uiso 1 1 calc R
C53 C 0.288(4) 0.752(5) 0.432(4) 0.19(3) Uani 1 1 d U
H53A H 0.3092 0.7462 0.4714 0.281 Uiso 1 1 calc R
H53B H 0.2709 0.8082 0.4259 0.281 Uiso 1 1 calc R
H53C H 0.3187 0.7426 0.4051 0.281 Uiso 1 1 calc R
C54 C 0.1742(19) 0.732(3) 0.5776(19) 0.074(12) Uani 1 1 d .
H54A H 0.1920 0.7544 0.5442 0.088 Uiso 1 1 calc R
H54B H 0.1507 0.7776 0.5931 0.088 Uiso 1 1 calc R
C55 C 0.227(3) 0.709(3) 0.622(4) 0.16(3) Uani 1 1 d DU
H55A H 0.2560 0.7568 0.6277 0.196 Uiso 1 1 calc R
H55B H 0.2096 0.7012 0.6584 0.196 Uiso 1 1 calc R
C56 C 0.266(3) 0.636(4) 0.615(4) 0.16(3) Uani 1 1 d DU
H56A H 0.2823 0.6413 0.5777 0.197 Uiso 1 1 calc R
H56B H 0.2378 0.5866 0.6115 0.197 Uiso 1 1 calc R
C57 C 0.322(3) 0.617(5) 0.661(3) 0.17(3) Uani 1 1 d .
H57A H 0.3440 0.5683 0.6498 0.249 Uiso 1 1 calc R
H57B H 0.3063 0.6069 0.6976 0.249 Uiso 1 1 calc R
H57C H 0.3503 0.6647 0.6649 0.249 Uiso 1 1 calc R
C58 C 0.135(2) 0.417(3) 0.7110(18) 0.085(14) Uani 1 1 d .
H58A H 0.1002 0.4136 0.7340 0.102 Uiso 1 1 calc R
H58B H 0.1596 0.3651 0.7172 0.102 Uiso 1 1 calc R
C59 C 0.178(4) 0.486(5) 0.736(3) 0.16(3) Uani 1 1 d U
H59A H 0.1528 0.5372 0.7279 0.198 Uiso 1 1 calc R
H59B H 0.2120 0.4885 0.7118 0.198 Uiso 1 1 calc R
C60 C 0.209(4) 0.492(6) 0.797(3) 0.17(3) Uani 1 1 d .
H60A H 0.1798 0.4716 0.8231 0.205 Uiso 1 1 calc R
H60B H 0.2470 0.4556 0.8029 0.205 Uiso 1 1 calc R
C61 C 0.229(5) 0.579(6) 0.814(4) 0.22(4) Uani 1 1 d .
H61A H 0.2501 0.5794 0.8543 0.328 Uiso 1 1 calc R
H61B H 0.1916 0.6145 0.8107 0.328 Uiso 1 1 calc R
H61C H 0.2581 0.5993 0.7890 0.328 Uiso 1 1 calc R
C62 C 0.2387(17) 0.404(3) 0.464(2) 0.072(12) Uani 1 1 d .
H62A H 0.2539 0.3466 0.4716 0.087 Uiso 1 1 calc R
H62B H 0.2315 0.4117 0.4217 0.087 Uiso 1 1 calc R
C63 C 0.2907(19) 0.462(3) 0.489(2) 0.090(15) Uani 1 1 d .
H63A H 0.3000 0.4517 0.5312 0.108 Uiso 1 1 calc R
H63B H 0.2744 0.5196 0.4842 0.108 Uiso 1 1 calc R
C64 C 0.352(2) 0.457(4) 0.465(2) 0.110(18) Uani 1 1 d .
H64A H 0.3427 0.4669 0.4225 0.132 Uiso 1 1 calc R
H64B H 0.3690 0.4006 0.4706 0.132 Uiso 1 1 calc R
C65 C 0.403(3) 0.518(5) 0.490(3) 0.16(3) Uani 1 1 d .
H65A H 0.4410 0.5105 0.4712 0.244 Uiso 1 1 calc R
H65B H 0.4141 0.5088 0.5313 0.244 Uiso 1 1 calc R
H65C H 0.3877 0.5751 0.4832 0.244 Uiso 1 1 calc R
C66 C 0.308(2) 0.247(4) 0.602(3) 0.107(17) Uani 1 1 d .
H66A H 0.3403 0.2908 0.6053 0.128 Uiso 1 1 calc R
H66B H 0.2954 0.2346 0.5605 0.128 Uiso 1 1 calc R
C67 C 0.337(2) 0.169(3) 0.632(2) 0.083(13) Uani 1 1 d .
H67A H 0.3730 0.1516 0.6141 0.124 Uiso 1 1 calc R
H67B H 0.3049 0.1249 0.6282 0.124 Uiso 1 1 calc R
H67C H 0.3503 0.1811 0.6728 0.124 Uiso 1 1 calc R
O1 O 0.1028(15) 0.164(2) 0.6772(15) 0.093(10) Uani 1 1 d .
O2 O 0.2003(16) 0.139(2) 0.6560(16) 0.102(11) Uani 1 1 d .
O3 O 0.1714(11) -0.0338(16) 0.6902(13) 0.068(7) Uani 1 1 d .
O4 O 0.1920(13) 0.0525(19) 0.7736(13) 0.077(8) Uani 1 1 d .
O5 O 0.2589(14) -0.063(2) 0.5131(14) 0.083(9) Uani 1 1 d .
O6 O 0.3457(16) -0.005(2) 0.4714(12) 0.089(10) Uani 1 1 d .
O7 O 0.5241(16) 0.297(2) 0.6099(17) 0.096(10) Uani 1 1 d .
O8 O 0.5047(16) 0.205(2) 0.5286(14) 0.093(10) Uani 1 1 d .
O9 O 0.4223(16) 0.343(2) 0.7780(15) 0.097(11) Uani 1 1 d .
O10 O 0.3383(15) 0.284(2) 0.8188(15) 0.093(10) Uani 1 1 d .
O11 O 0.0921(10) 0.5552(13) 0.6115(9) 0.046(5) Uani 1 1 d .
O12 O 0.0596(10) 0.6664(13) 0.4632(9) 0.048(6) Uani 1 1 d .
O13 O 0.0008(10) 0.5450(13) 0.3694(10) 0.051(6) Uani 1 1 d .
O14 O -0.0158(10) 0.3276(13) 0.4367(10) 0.048(5) Uani 1 1 d .
O17 O 0.0647(10) 0.4136(12) 0.5324(9) 0.043(5) Uani 1 1 d .
O19 O 0.0912(10) 0.4439(13) 0.4143(10) 0.050(6) Uani 1 1 d .
O20 O 0.1422(10) 0.5493(13) 0.4943(10) 0.049(6) Uani 1 1 d .
O21 O 0.2540(16) 0.277(2) 0.6248(19) 0.123(14) Uani 1 1 d .
H21A H 0.2402 0.3191 0.6068 0.185 Uiso 1 1 calc RD
O15 O 0.0687(13) 0.2954(15) 0.6097(11) 0.061(7) Uani 1 1 d D
H15 H 0.08(2) 0.254(16) 0.631(15) 0.091 Uiso 1 1 d D
O18 O 0.1201(12) 0.2884(14) 0.4886(12) 0.061(7) Uani 1 1 d D
H18 H 0.11(2) 0.332(16) 0.468(16) 0.092 Uiso 1 1 d D
O16 O 0.1819(11) 0.4145(15) 0.5861(11) 0.058(6) Uani 1 1 d D
H16A H 0.171(14) 0.452(17) 0.560(9) 0.087 Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O17 Sn1 O16 76.6(9) . .
O17 Sn1 O20 88.2(8) . .
O16 Sn1 O20 92.2(9) . .
O17 Sn1 O19 87.5(8) . .
O16 Sn1 O19 160.6(9) . .
O20 Sn1 O19 76.0(9) . .
O17 Sn1 O18 76.0(9) . .
O16 Sn1 O18 96.1(10) . .
O20 Sn1 O18 159.8(9) . .
O19 Sn1 O18 90.7(9) . .
O17 Sn1 C62 172.0(14) . .
O16 Sn1 C62 98.9(13) . .
O20 Sn1 C62 98.7(13) . .
O19 Sn1 C62 98.1(14) . .
O18 Sn1 C62 98.1(13) . .
O17 Sn1 Sn4 37.6(6) . .
O16 Sn1 Sn4 39.1(6) . .
O20 Sn1 Sn4 87.3(6) . .
O19 Sn1 Sn4 123.5(6) . .
O18 Sn1 Sn4 87.6(7) . .
C62 Sn1 Sn4 138.0(12) . .
O17 Sn1 Sn2 89.1(6) . .
O16 Sn1 Sn2 129.2(7) . .
O20 Sn1 Sn2 38.1(6) . .
O19 Sn1 Sn2 38.0(6) . .
O18 Sn1 Sn2 127.6(7) . .
C62 Sn1 Sn2 98.9(13) . .
Sn4 Sn1 Sn2 110.23(9) . .
O17 Sn1 H18 76(10) . .
O16 Sn1 H18 116(8) . .
O20 Sn1 H18 142(9) . .
O19 Sn1 H18 69(6) . .
O18 Sn1 H18 22(6) . .
C62 Sn1 H18 101(10) . .
Sn4 Sn1 H18 99(10) . .
Sn2 Sn1 H18 106(7) . .
O17 Sn1 H16A 77(9) . .
O16 Sn1 H16A 22(5) . .
O20 Sn1 H16A 71(5) . .
O19 Sn1 H16A 143(2) . .
O18 Sn1 H16A 116(8) . .
C62 Sn1 H16A 102(8) . .
Sn4 Sn1 H16A 41(10) . .
Sn2 Sn1 H16A 108(4) . .
H18 Sn1 H16A 135(10) . .
O12 Sn2 O13 96.3(9) . .
O12 Sn2 O19 135.3(9) . .
O13 Sn2 O19 77.8(8) . .
O12 Sn2 O20 77.5(8) . .
O13 Sn2 O20 136.2(9) . .
O19 Sn2 O20 77.3(8) . .
O12 Sn2 C50 111.4(15) . .
O13 Sn2 C50 109.6(15) . .
O19 Sn2 C50 112.3(15) . .
O20 Sn2 C50 113.0(15) . .
O12 Sn2 Sn3 120.7(6) . .
O13 Sn2 Sn3 39.6(6) . .
O19 Sn2 Sn3 38.2(6) . .
O20 Sn2 Sn3 107.1(6) . .
C50 Sn2 Sn3 119.2(13) . .
O12 Sn2 Sn6 39.4(6) . .
O13 Sn2 Sn6 120.6(7) . .
O19 Sn2 Sn6 106.4(6) . .
O20 Sn2 Sn6 38.2(6) . .
C50 Sn2 Sn6 121.4(13) . .
Sn3 Sn2 Sn6 118.59(10) . .
O12 Sn2 Sn1 109.5(6) . .
O13 Sn2 Sn1 110.3(6) . .
O19 Sn2 Sn1 38.8(6) . .
O20 Sn2 Sn1 38.6(6) . .
C50 Sn2 Sn1 117.7(14) . .
Sn3 Sn2 Sn1 72.51(8) . .
Sn6 Sn2 Sn1 71.95(8) . .
O19 Sn3 O14 95.7(9) . .
O19 Sn3 O11 135.7(9) . 3_566
O14 Sn3 O11 78.2(8) . 3_566
O19 Sn3 O13 77.8(9) . .
O14 Sn3 O13 135.9(9) . .
O11 Sn3 O13 77.3(8) 3_566 .
O19 Sn3 C46 109.6(16) . .
O14 Sn3 C46 112.8(19) . .
O11 Sn3 C46 113.2(15) 3_566 .
O13 Sn3 C46 110.4(19) . .
O19 Sn3 Sn6 120.4(7) . 3_566
O14 Sn3 Sn6 39.9(6) . 3_566
O11 Sn3 Sn6 38.4(6) 3_566 3_566
O13 Sn3 Sn6 106.8(6) . 3_566
C46 Sn3 Sn6 122.3(16) . 3_566
O19 Sn3 Sn2 39.4(6) . .
O14 Sn3 Sn2 120.4(6) . .
O11 Sn3 Sn2 107.0(6) 3_566 .
O13 Sn3 Sn2 38.4(6) . .
C46 Sn3 Sn2 117.9(17) . .
Sn6 Sn3 Sn2 118.82(10) 3_566 .
O19 Sn3 Sn4 109.8(6) . 3_566
O14 Sn3 Sn4 110.5(6) . 3_566
O11 Sn3 Sn4 38.9(6) 3_566 3_566
O13 Sn3 Sn4 38.4(6) . 3_566
C46 Sn3 Sn4 116.5(16) . 3_566
Sn6 Sn3 Sn4 72.52(8) 3_566 3_566
Sn2 Sn3 Sn4 72.29(8) . 3_566
O17 Sn4 O15 76.5(9) . .
O17 Sn4 C58 171.5(16) . .
O15 Sn4 C58 99.2(15) . .
O17 Sn4 O13 87.4(8) . 3_566
O15 Sn4 O13 91.0(9) . 3_566
C58 Sn4 O13 100.0(16) . 3_566
O17 Sn4 O16 76.1(9) . .
O15 Sn4 O16 96.6(10) . .
C58 Sn4 O16 97.4(15) . .
O13 Sn4 O16 159.6(9) 3_566 .
O17 Sn4 O11 87.2(8) . .
O15 Sn4 O11 159.6(8) . .
C58 Sn4 O11 98.5(14) . .
O13 Sn4 O11 75.9(8) 3_566 .
O16 Sn4 O11 91.1(9) . .
O17 Sn4 Sn5 38.3(6) . .
O15 Sn4 Sn5 38.4(7) . .
C58 Sn4 Sn5 137.6(13) . .
O13 Sn4 Sn5 85.9(6) 3_566 .
O16 Sn4 Sn5 88.4(7) . .
O11 Sn4 Sn5 123.5(6) . .
O17 Sn4 Sn1 37.5(6) . .
O15 Sn4 Sn1 88.3(7) . .
C58 Sn4 Sn1 136.2(14) . .
O13 Sn4 Sn1 123.1(6) 3_566 .
O16 Sn4 Sn1 38.8(6) . .
O11 Sn4 Sn1 86.0(6) . .
Sn5 Sn4 Sn1 60.55(8) . .
O17 Sn4 Sn3 88.4(5) . 3_566
O15 Sn4 Sn3 127.8(7) . 3_566
C58 Sn4 Sn3 100.0(14) . 3_566
O13 Sn4 Sn3 38.0(6) 3_566 3_566
O16 Sn4 Sn3 128.0(7) . 3_566
O11 Sn4 Sn3 38.0(6) . 3_566
Sn5 Sn4 Sn3 109.21(9) . 3_566
Sn1 Sn4 Sn3 109.09(9) . 3_566
O17 Sn5 O15 76.2(9) . .
O17 Sn5 O12 88.3(8) . 3_566
O15 Sn5 O12 92.2(9) . 3_566
O17 Sn5 O18 75.7(9) . .
O15 Sn5 O18 96.5(11) . .
O12 Sn5 O18 159.3(9) 3_566 .
O17 Sn5 O14 87.6(8) . .
O15 Sn5 O14 160.5(9) . .
O12 Sn5 O14 76.3(8) 3_566 .
O18 Sn5 O14 89.9(9) . .
O17 Sn5 C42 171.4(15) . .
O15 Sn5 C42 97.7(16) . .
O12 Sn5 C42 98.1(15) 3_566 .
O18 Sn5 C42 99.2(15) . .
O14 Sn5 C42 99.5(16) . .
O17 Sn5 Sn4 38.0(6) . .
O15 Sn5 Sn4 38.4(6) . .
O12 Sn5 Sn4 87.2(6) 3_566 .
O18 Sn5 Sn4 88.0(7) . .
O14 Sn5 Sn4 123.9(6) . .
C42 Sn5 Sn4 136.1(15) . .
O17 Sn5 Sn6 89.4(6) . 3_566
O15 Sn5 Sn6 129.2(7) . 3_566
O12 Sn5 Sn6 38.1(6) 3_566 3_566
O18 Sn5 Sn6 127.1(7) . 3_566
O14 Sn5 Sn6 38.3(6) . 3_566
C42 Sn5 Sn6 99.2(13) . 3_566
Sn4 Sn5 Sn6 110.55(9) . 3_566
O11 Sn6 O20 96.7(9) . .
O11 Sn6 O12 135.7(8) . .
O20 Sn6 O12 76.9(9) . .
O11 Sn6 O14 78.0(9) . 3_566
O20 Sn6 O14 135.4(8) . 3_566
O12 Sn6 O14 77.0(9) . 3_566
O11 Sn6 C54 112.1(13) . .
O20 Sn6 C54 113.9(14) . .
O12 Sn6 C54 110.4(13) . .
O14 Sn6 C54 108.9(14) 3_566 .
O11 Sn6 Sn3 39.6(6) . 3_566
O20 Sn6 Sn3 120.8(6) . 3_566
O12 Sn6 Sn3 106.7(6) . 3_566
O14 Sn6 Sn3 38.5(6) 3_566 3_566
C54 Sn6 Sn3 118.8(13) . 3_566
O11 Sn6 Sn2 120.5(6) . .
O20 Sn6 Sn2 39.3(6) . .
O12 Sn6 Sn2 37.8(6) . .
O14 Sn6 Sn2 106.1(6) 3_566 .
C54 Sn6 Sn2 121.1(13) . .
Sn3 Sn6 Sn2 118.23(9) 3_566 .
O11 Sn6 Sn5 110.4(6) . 3_566
O20 Sn6 Sn5 109.1(6) . 3_566
O12 Sn6 Sn5 38.3(6) . 3_566
O14 Sn6 Sn5 38.8(6) 3_566 3_566
C54 Sn6 Sn5 113.4(11) . 3_566
Sn3 Sn6 Sn5 72.72(8) 3_566 3_566
Sn2 Sn6 Sn5 71.48(8) . 3_566
C2 C1 C6 117(5) . .
C2 C1 C7 122(6) . .
C6 C1 C7 121(6) . .
C1 C2 C3 123(5) . .
C1 C2 O7 117(5) . .
C3 C2 O7 120(5) . .
C4 C3 C2 117(4) . .
C4 C3 C11 124(4) . .
C2 C3 C11 119(4) . .
C5 C4 C3 123(4) . .
C5 C4 H4 118.4 . .
C3 C4 H4 118.4 . .
C6 C5 C4 117(4) . .
C6 C5 C39 120(4) . .
C4 C5 C39 123(4) . .
C5 C6 C1 123(5) . .
C5 C6 O9 119(5) . .
C1 C6 O9 118(5) . .
C1 C7 H7A 109.5 . .
C1 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C1 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
O8 C8 O7 113(4) . .
O8 C8 H8A 108.9 . .
O7 C8 H8A 108.9 . .
O8 C8 H8B 108.9 . .
O7 C8 H8B 108.9 . .
H8A C8 H8B 107.7 . .
C13 C9 C10 121(4) . .
C13 C9 O8 118(4) . .
C10 C9 O8 120(4) . .
C16 C10 C9 119(4) . .
C16 C10 C11 123(4) . .
C9 C10 C11 118(4) . .
C12 C11 C3 113(4) . .
C12 C11 C10 112(4) . .
C3 C11 C10 108(3) . .
C12 C11 H11 107.6 . .
C3 C11 H11 107.6 . .
C10 C11 H11 107.6 . .
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C14 C13 C9 118(4) . .
C14 C13 C17 121(4) . .
C9 C13 C17 122(4) . .
C15 C14 C13 123(4) . .
C15 C14 O6 120(4) . .
C13 C14 O6 116(4) . .
C14 C15 C16 117(4) . .
C14 C15 C21 120(4) . .
C16 C15 C21 122(4) . .
C10 C16 C15 122(4) . .
C10 C16 H16 119.0 . .
C15 C16 H16 119.0 . .
C13 C17 H17A 109.5 . .
C13 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C13 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
O5 C18 O6 116(4) . .
O5 C18 H18A 108.4 . .
O6 C18 H18A 108.4 . .
O5 C18 H18B 108.4 . .
O6 C18 H18B 108.4 . .
H18A C18 H18B 107.5 . .
C20 C19 O5 120(4) . .
C20 C19 C23 124(4) . .
O5 C19 C23 116(4) . .
C26 C20 C19 117(4) . .
C26 C20 C21 122(3) . .
C19 C20 C21 122(4) . .
C20 C21 C15 110(3) . .
C20 C21 C22 114(4) . .
C15 C21 C22 113(3) . .
C20 C21 H21 106.5 . .
C15 C21 H21 106.5 . .
C22 C21 H21 106.5 . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C24 C23 C19 118(4) . .
C24 C23 C27 120(4) . .
C19 C23 C27 122(4) . .
C23 C24 O3 119(4) . .
C23 C24 C25 121(4) . .
O3 C24 C25 119(4) . .
C26 C25 C24 116(4) . .
C26 C25 C31 123(3) . .
C24 C25 C31 121(4) . .
C20 C26 C25 124(4) . .
C20 C26 H26 118.1 . .
C25 C26 H26 118.1 . .
C23 C27 H27A 109.5 . .
C23 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C23 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
O3 C28 O4 113(3) . .
O3 C28 C41 117(4) . .
O4 C28 C41 112(3) . .
O3 C28 H28 104.4 . .
O4 C28 H28 104.4 . .
C41 C28 H28 104.4 . .
C33 C29 O4 122(4) . .
C33 C29 C30 120(4) . .
O4 C29 C30 118(4) . .
C36 C30 C29 118(4) . .
C36 C30 C31 121(4) . .
C29 C30 C31 121(4) . .
C30 C31 C25 108(3) . .
C30 C31 C32 115(4) . .
C25 C31 C32 114(3) . .
C30 C31 H31 106.2 . .
C25 C31 H31 106.2 . .
C32 C31 H31 106.2 . .
C31 C32 H32A 109.5 . .
C31 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C31 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
C29 C33 C34 120(4) . .
C29 C33 C37 120(4) . .
C34 C33 C37 120(4) . .
C33 C34 C35 120(4) . .
C33 C34 O10 120(4) . .
C35 C34 O10 120(4) . .
C36 C35 C34 119(4) . .
C36 C35 C39 122(4) . .
C34 C35 C39 118(4) . .
C35 C36 C30 122(4) . .
C35 C36 H36 119.1 . .
C30 C36 H36 119.1 . .
C33 C37 H37A 109.5 . .
C33 C37 H37B 109.5 . .
H37A C37 H37B 109.5 . .
C33 C37 H37C 109.5 . .
H37A C37 H37C 109.5 . .
H37B C37 H37C 109.5 . .
O9 C38 O10 112(5) . .
O9 C38 H38A 109.1 . .
O10 C38 H38A 109.1 . .
O9 C38 H38B 109.1 . .
O10 C38 H38B 109.1 . .
H38A C38 H38B 107.9 . .
C5 C39 C40 116(4) . .
C5 C39 C35 111(3) . .
C40 C39 C35 111(4) . .
C5 C39 H39 106.0 . .
C40 C39 H39 106.0 . .
C35 C39 H39 106.0 . .
C39 C40 H40A 109.5 . .
C39 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
C39 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
O2 C41 O1 126(4) . .
O2 C41 C28 118(4) . .
O1 C41 C28 115(4) . .
C43 C42 Sn5 112(3) . .
C43 C42 H42A 109.3 . .
Sn5 C42 H42A 109.3 . .
C43 C42 H42B 109.3 . .
Sn5 C42 H42B 109.3 . .
H42A C42 H42B 107.9 . .
C44 C43 C42 116(5) . .
C44 C43 H43A 108.3 . .
C42 C43 H43A 108.3 . .
C44 C43 H43B 108.3 . .
C42 C43 H43B 108.3 . .
H43A C43 H43B 107.4 . .
C45 C44 C43 111(7) . .
C45 C44 H44A 109.5 . .
C43 C44 H44A 109.5 . .
C45 C44 H44B 109.5 . .
C43 C44 H44B 109.5 . .
H44A C44 H44B 108.0 . .
C44 C45 H45A 109.5 . .
C44 C45 H45B 109.5 . .
H45A C45 H45B 109.5 . .
C44 C45 H45C 109.5 . .
H45A C45 H45C 109.5 . .
H45B C45 H45C 109.5 . .
C47 C46 Sn3 119(5) . .
C47 C46 H46A 107.5 . .
Sn3 C46 H46A 107.5 . .
C47 C46 H46B 107.5 . .
Sn3 C46 H46B 107.5 . .
H46A C46 H46B 107.0 . .
C48 C47 C46 114(8) . .
C48 C47 H47A 108.6 . .
C46 C47 H47A 108.6 . .
C48 C47 H47B 108.6 . .
C46 C47 H47B 108.6 . .
H47A C47 H47B 107.6 . .
C49 C48 C47 137(10) . .
C49 C48 H48A 102.8 . .
C47 C48 H48A 102.8 . .
C49 C48 H48B 102.8 . .
C47 C48 H48B 102.8 . .
H48A C48 H48B 105.0 . .
C48 C49 H49A 109.5 . .
C48 C49 H49B 109.5 . .
H49A C49 H49B 109.5 . .
C48 C49 H49C 109.5 . .
H49A C49 H49C 109.5 . .
H49B C49 H49C 109.5 . .
C51 C50 Sn2 122(4) . .
C51 C50 H50A 106.9 . .
Sn2 C50 H50A 106.9 . .
C51 C50 H50B 106.9 . .
Sn2 C50 H50B 106.9 . .
H50A C50 H50B 106.7 . .
C50 C51 C52 121(7) . .
C50 C51 H51A 107.0 . .
C52 C51 H51A 107.0 . .
C50 C51 H51B 107.0 . .
C52 C51 H51B 107.0 . .
H51A C51 H51B 106.7 . .
C51 C52 C53 123(7) . .
C51 C52 H52A 106.5 . .
C53 C52 H52A 106.5 . .
C51 C52 H52B 106.5 . .
C53 C52 H52B 106.5 . .
H52A C52 H52B 106.5 . .
C52 C53 H53A 109.5 . .
C52 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
C52 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C55 C54 Sn6 117(3) . .
C55 C54 H54A 108.0 . .
Sn6 C54 H54A 108.0 . .
C55 C54 H54B 108.0 . .
Sn6 C54 H54B 108.0 . .
H54A C54 H54B 107.3 . .
C56 C55 C54 121(6) . .
C56 C55 H55A 107.1 . .
C54 C55 H55A 107.1 . .
C56 C55 H55B 107.1 . .
C54 C55 H55B 107.1 . .
H55A C55 H55B 106.8 . .
C55 C56 C57 118(7) . .
C55 C56 H56A 107.7 . .
C57 C56 H56A 107.7 . .
C55 C56 H56B 107.7 . .
C57 C56 H56B 107.7 . .
H56A C56 H56B 107.1 . .
C56 C57 H57A 109.5 . .
C56 C57 H57B 109.5 . .
H57A C57 H57B 109.5 . .
C56 C57 H57C 109.5 . .
H57A C57 H57C 109.5 . .
H57B C57 H57C 109.5 . .
C59 C58 Sn4 119(4) . .
C59 C58 H58A 107.5 . .
Sn4 C58 H58A 107.5 . .
C59 C58 H58B 107.5 . .
Sn4 C58 H58B 107.5 . .
H58A C58 H58B 107.0 . .
C58 C59 C60 126(7) . .
C58 C59 H59A 105.9 . .
C60 C59 H59A 105.9 . .
C58 C59 H59B 105.9 . .
C60 C59 H59B 105.9 . .
H59A C59 H59B 106.3 . .
C61 C60 C59 113(8) . .
C61 C60 H60A 109.1 . .
C59 C60 H60A 109.1 . .
C61 C60 H60B 109.1 . .
C59 C60 H60B 109.1 . .
H60A C60 H60B 107.8 . .
C60 C61 H61A 109.5 . .
C60 C61 H61B 109.5 . .
H61A C61 H61B 109.5 . .
C60 C61 H61C 109.5 . .
H61A C61 H61C 109.5 . .
H61B C61 H61C 109.5 . .
C63 C62 Sn1 116(3) . .
C63 C62 H62A 108.2 . .
Sn1 C62 H62A 108.2 . .
C63 C62 H62B 108.2 . .
Sn1 C62 H62B 108.2 . .
H62A C62 H62B 107.3 . .
C62 C63 C64 117(4) . .
C62 C63 H63A 108.2 . .
C64 C63 H63A 108.2 . .
C62 C63 H63B 108.2 . .
C64 C63 H63B 108.2 . .
H63A C63 H63B 107.3 . .
C63 C64 C65 116(5) . .
C63 C64 H64A 108.4 . .
C65 C64 H64A 108.4 . .
C63 C64 H64B 108.4 . .
C65 C64 H64B 108.4 . .
H64A C64 H64B 107.4 . .
C64 C65 H65A 109.5 . .
C64 C65 H65B 109.5 . .
H65A C65 H65B 109.5 . .
C64 C65 H65C 109.5 . .
H65A C65 H65C 109.5 . .
H65B C65 H65C 109.5 . .
O21 C66 C67 114(4) . .
O21 C66 H66A 108.9 . .
C67 C66 H66A 108.9 . .
O21 C66 H66B 108.9 . .
C67 C66 H66B 108.9 . .
H66A C66 H66B 107.7 . .
C66 C67 H67A 109.5 . .
C66 C67 H67B 109.5 . .
H67A C67 H67B 109.5 . .
C66 C67 H67C 109.5 . .
H67A C67 H67C 109.5 . .
H67B C67 H67C 109.5 . .
C24 O3 C28 124(3) . .
C29 O4 C28 123(3) . .
C18 O5 C19 117(3) . .
C14 O6 C18 117(3) . .
C2 O7 C8 117(3) . .
C9 O8 C8 117(3) . .
C38 O9 C6 117(3) . .
C34 O10 C38 120(3) . .
Sn6 O11 Sn3 102.1(9) . 3_566
Sn6 O11 Sn4 135.3(11) . .
Sn3 O11 Sn4 103.1(9) 3_566 .
Sn2 O12 Sn6 102.8(9) . .
Sn2 O12 Sn5 134.7(11) . 3_566
Sn6 O12 Sn5 103.6(10) . 3_566
Sn2 O13 Sn3 101.9(9) . .
Sn2 O13 Sn4 135.4(11) . 3_566
Sn3 O13 Sn4 103.6(10) . 3_566
Sn3 O14 Sn6 101.5(9) . 3_566
Sn3 O14 Sn5 135.9(10) . .
Sn6 O14 Sn5 102.9(10) 3_566 .
Sn1 O17 Sn4 104.9(9) . .
Sn1 O17 Sn5 105.4(9) . .
Sn4 O17 Sn5 103.7(9) . .
Sn3 O19 Sn2 102.4(9) . .
Sn3 O19 Sn1 135.8(12) . .
Sn2 O19 Sn1 103.3(9) . .
Sn6 O20 Sn2 102.5(9) . .
Sn6 O20 Sn1 134.2(12) . .
Sn2 O20 Sn1 103.3(9) . .
C66 O21 H21A 109.5 . .
Sn4 O15 Sn5 103.2(9) . .
Sn4 O15 H15 130(10) . .
Sn5 O15 H15 125(10) . .
Sn5 O18 Sn1 102.7(10) . .
Sn5 O18 H18 91(10) . .
Sn1 O18 H18 45(10) . .
Sn1 O16 Sn4 102.1(9) . .
Sn1 O16 H16A 44(10) . .
Sn4 O16 H16A 94(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sn1 O17 2.07(2) .
Sn1 O16 2.10(2) .
Sn1 O20 2.11(2) .
Sn1 O19 2.11(2) .
Sn1 O18 2.12(2) .
Sn1 C62 2.12(4) .
Sn1 Sn4 3.283(4) .
Sn1 Sn2 3.283(3) .
Sn1 H18 1.6(4) .
Sn1 H16A 1.6(3) .
Sn2 O12 2.02(2) .
Sn2 O13 2.03(2) .
Sn2 O19 2.08(2) .
Sn2 O20 2.08(2) .
Sn2 C50 2.08(4) .
Sn2 Sn3 3.195(3) .
Sn2 Sn6 3.211(4) .
Sn3 O19 2.02(2) .
Sn3 O14 2.03(2) .
Sn3 O11 2.08(2) 3_566
Sn3 O13 2.08(2) .
Sn3 C46 2.12(4) .
Sn3 Sn6 3.193(4) 3_566
Sn3 Sn4 3.292(3) 3_566
Sn4 O17 2.07(2) .
Sn4 O15 2.09(2) .
Sn4 C58 2.10(4) .
Sn4 O13 2.11(2) 3_566
Sn4 O16 2.12(2) .
Sn4 O11 2.12(2) .
Sn4 Sn5 3.271(3) .
Sn4 Sn3 3.292(3) 3_566
Sn5 O17 2.09(2) .
Sn5 O15 2.09(2) .
Sn5 O12 2.10(2) 3_566
Sn5 O18 2.11(3) .
Sn5 O14 2.12(2) .
Sn5 C42 2.12(4) .
Sn5 Sn6 3.289(3) 3_566
Sn6 O11 2.03(2) .
Sn6 O20 2.04(2) .
Sn6 O12 2.09(2) .
Sn6 O14 2.09(2) 3_566
Sn6 C54 2.12(3) .
Sn6 Sn3 3.193(4) 3_566
Sn6 Sn5 3.289(3) 3_566
C1 C2 1.37(7) .
C1 C6 1.38(7) .
C1 C7 1.50(6) .
C2 C3 1.39(6) .
C2 O7 1.39(5) .
C3 C4 1.38(6) .
C3 C11 1.54(6) .
C4 C5 1.38(5) .
C4 H4 0.9300 .
C5 C6 1.37(6) .
C5 C39 1.49(6) .
C6 O9 1.42(5) .
C7 H7A 0.9600 .
C7 H7B 0.9600 .
C7 H7C 0.9600 .
C8 O8 1.41(6) .
C8 O7 1.41(6) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C9 C13 1.38(6) .
C9 C10 1.38(5) .
C9 O8 1.40(5) .
C10 C16 1.36(5) .
C10 C11 1.55(5) .
C11 C12 1.53(6) .
C11 H11 0.9800 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 C14 1.38(6) .
C13 C17 1.53(6) .
C14 C15 1.36(5) .
C14 O6 1.41(4) .
C15 C16 1.39(5) .
C15 C21 1.51(6) .
C16 H16 0.9300 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C18 O5 1.38(6) .
C18 O6 1.41(5) .
C18 H18A 0.9700 .
C18 H18B 0.9700 .
C19 C20 1.38(5) .
C19 O5 1.39(5) .
C19 C23 1.39(5) .
C20 C26 1.37(5) .
C20 C21 1.48(5) .
C21 C22 1.53(6) .
C21 H21 0.9800 .
C22 H22A 0.9600 .
C22 H22B 0.9600 .
C22 H22C 0.9600 .
C23 C24 1.38(6) .
C23 C27 1.51(5) .
C24 O3 1.38(4) .
C24 C25 1.42(5) .
C25 C26 1.40(5) .
C25 C31 1.51(5) .
C26 H26 0.9300 .
C27 H27A 0.9600 .
C27 H27B 0.9600 .
C27 H27C 0.9600 .
C28 O3 1.39(4) .
C28 O4 1.41(5) .
C28 C41 1.54(5) .
C28 H28 0.9800 .
C29 C33 1.34(5) .
C29 O4 1.38(5) .
C29 C30 1.43(5) .
C30 C36 1.38(5) .
C30 C31 1.51(6) .
C31 C32 1.52(5) .
C31 H31 0.9800 .
C32 H32A 0.9600 .
C32 H32B 0.9600 .
C32 H32C 0.9600 .
C33 C34 1.38(6) .
C33 C37 1.49(6) .
C34 C35 1.40(5) .
C34 O10 1.41(5) .
C35 C36 1.35(5) .
C35 C39 1.54(6) .
C36 H36 0.9300 .
C37 H37A 0.9600 .
C37 H37B 0.9600 .
C37 H37C 0.9600 .
C38 O9 1.36(6) .
C38 O10 1.42(6) .
C38 H38A 0.9700 .
C38 H38B 0.9700 .
C39 C40 1.51(6) .
C39 H39 0.9800 .
C40 H40A 0.9600 .
C40 H40B 0.9600 .
C40 H40C 0.9600 .
C41 O2 1.21(5) .
C41 O1 1.26(5) .
C42 C43 1.60(8) .
C42 H42A 0.9700 .
C42 H42B 0.9700 .
C43 C44 1.45(8) .
C43 H43A 0.9700 .
C43 H43B 0.9700 .
C44 C45 1.44(9) .
C44 H44A 0.9700 .
C44 H44B 0.9700 .
C45 H45A 0.9600 .
C45 H45B 0.9600 .
C45 H45C 0.9600 .
C46 C47 1.47(8) .
C46 H46A 0.9700 .
C46 H46B 0.9700 .
C47 C48 1.40(10) .
C47 H47A 0.9700 .
C47 H47B 0.9700 .
C48 C49 1.39(11) .
C48 H48A 0.9700 .
C48 H48B 0.9700 .
C49 H49A 0.9600 .
C49 H49B 0.9600 .
C49 H49C 0.9600 .
C50 C51 1.39(7) .
C50 H50A 0.9700 .
C50 H50B 0.9700 .
C51 C52 1.45(4) .
C51 H51A 0.9700 .
C51 H51B 0.9700 .
C52 C53 1.48(9) .
C52 H52A 0.9700 .
C52 H52B 0.9700 .
C53 H53A 0.9600 .
C53 H53B 0.9600 .
C53 H53C 0.9600 .
C54 C55 1.44(7) .
C54 H54A 0.9700 .
C54 H54B 0.9700 .
C55 C56 1.44(4) .
C55 H55A 0.9700 .
C55 H55B 0.9700 .
C56 C57 1.48(8) .
C56 H56A 0.9700 .
C56 H56B 0.9700 .
C57 H57A 0.9600 .
C57 H57B 0.9600 .
C57 H57C 0.9600 .
C58 C59 1.46(8) .
C58 H58A 0.9700 .
C58 H58B 0.9700 .
C59 C60 1.48(8) .
C59 H59A 0.9700 .
C59 H59B 0.9700 .
C60 C61 1.47(10) .
C60 H60A 0.9700 .
C60 H60B 0.9700 .
C61 H61A 0.9600 .
C61 H61B 0.9600 .
C61 H61C 0.9600 .
C62 C63 1.48(5) .
C62 H62A 0.9700 .
C62 H62B 0.9700 .
C63 C64 1.48(6) .
C63 H63A 0.9700 .
C63 H63B 0.9700 .
C64 C65 1.50(7) .
C64 H64A 0.9700 .
C64 H64B 0.9700 .
C65 H65A 0.9600 .
C65 H65B 0.9600 .
C65 H65C 0.9600 .
C66 O21 1.39(5) .
C66 C67 1.49(6) .
C66 H66A 0.9700 .
C66 H66B 0.9700 .
C67 H67A 0.9600 .
C67 H67B 0.9600 .
C67 H67C 0.9600 .
O11 Sn3 2.08(2) 3_566
O12 Sn5 2.10(2) 3_566
O13 Sn4 2.11(2) 3_566
O14 Sn6 2.09(2) 3_566
O21 H21A 0.8200 .
O15 H15 0.820(4) .
O18 H18 0.850(4) .
O16 H16A 0.851(4) .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
O21 H21A O16 0.82 1.96 2.73(4) 156.6
O15 H15 O1 0.820(4) 1.81(4) 2.63(4) 179(47)
O18 H18 O19 0.850(4) 2.16(3) 3.01(3) 176(4)
O16 H16A O20 0.851(4) 2.18(3) 3.03(3) 180(57)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O17 Sn1 Sn2 O12 52.5(9) . .
O16 Sn1 Sn2 O12 -19.2(10) . .
O20 Sn1 Sn2 O12 -35.7(11) . .
O19 Sn1 Sn2 O12 139.7(12) . .
O18 Sn1 Sn2 O12 124.0(11) . .
C62 Sn1 Sn2 O12 -128.5(13) . .
Sn4 Sn1 Sn2 O12 20.8(7) . .
O17 Sn1 Sn2 O13 -52.2(9) . .
O16 Sn1 Sn2 O13 -124.0(11) . .
O20 Sn1 Sn2 O13 -140.5(12) . .
O19 Sn1 Sn2 O13 34.9(12) . .
O18 Sn1 Sn2 O13 19.2(11) . .
C62 Sn1 Sn2 O13 126.7(13) . .
Sn4 Sn1 Sn2 O13 -84.0(7) . .
O17 Sn1 Sn2 O19 -87.1(11) . .
O16 Sn1 Sn2 O19 -158.9(13) . .
O20 Sn1 Sn2 O19 -175.4(14) . .
O18 Sn1 Sn2 O19 -15.7(13) . .
C62 Sn1 Sn2 O19 91.8(15) . .
Sn4 Sn1 Sn2 O19 -118.9(10) . .
O17 Sn1 Sn2 O20 88.3(11) . .
O16 Sn1 Sn2 O20 16.5(12) . .
O19 Sn1 Sn2 O20 175.4(14) . .
O18 Sn1 Sn2 O20 159.7(13) . .
C62 Sn1 Sn2 O20 -92.8(14) . .
Sn4 Sn1 Sn2 O20 56.5(10) . .
O17 Sn1 Sn2 C50 -178.9(16) . .
O16 Sn1 Sn2 C50 109.4(17) . .
O20 Sn1 Sn2 C50 92.9(18) . .
O19 Sn1 Sn2 C50 -91.7(18) . .
O18 Sn1 Sn2 C50 -107.4(17) . .
C62 Sn1 Sn2 C50 0.1(18) . .
Sn4 Sn1 Sn2 C50 149.4(15) . .
O17 Sn1 Sn2 Sn3 -64.6(6) . .
O16 Sn1 Sn2 Sn3 -136.3(8) . .
O20 Sn1 Sn2 Sn3 -152.8(10) . .
O19 Sn1 Sn2 Sn3 22.6(10) . .
O18 Sn1 Sn2 Sn3 6.9(9) . .
C62 Sn1 Sn2 Sn3 114.4(11) . .
Sn4 Sn1 Sn2 Sn3 -96.33(10) . .
O17 Sn1 Sn2 Sn6 64.5(6) . .
O16 Sn1 Sn2 Sn6 -7.3(8) . .
O20 Sn1 Sn2 Sn6 -23.7(10) . .
O19 Sn1 Sn2 Sn6 151.7(10) . .
O18 Sn1 Sn2 Sn6 136.0(9) . .
C62 Sn1 Sn2 Sn6 -116.5(11) . .
Sn4 Sn1 Sn2 Sn6 32.75(9) . .
O12 Sn2 Sn3 O19 -125.6(12) . .
O13 Sn2 Sn3 O19 175.4(14) . .
O20 Sn2 Sn3 O19 -40.2(12) . .
C50 Sn2 Sn3 O19 89.6(19) . .
Sn6 Sn2 Sn3 O19 -80.1(10) . .
Sn1 Sn2 Sn3 O19 -22.9(10) . .
O12 Sn2 Sn3 O14 -67.9(10) . .
O13 Sn2 Sn3 O14 -126.9(12) . .
O19 Sn2 Sn3 O14 57.7(12) . .
O20 Sn2 Sn3 O14 17.5(10) . .
C50 Sn2 Sn3 O14 147.3(18) . .
Sn6 Sn2 Sn3 O14 -22.4(7) . .
Sn1 Sn2 Sn3 O14 34.9(7) . .
O12 Sn2 Sn3 O11 18.1(9) . 3_566
O13 Sn2 Sn3 O11 -40.8(12) . 3_566
O19 Sn2 Sn3 O11 143.8(12) . 3_566
O20 Sn2 Sn3 O11 103.5(9) . 3_566
C50 Sn2 Sn3 O11 -126.7(18) . 3_566
Sn6 Sn2 Sn3 O11 63.7(6) . 3_566
Sn1 Sn2 Sn3 O11 120.9(6) . 3_566
O12 Sn2 Sn3 O13 58.9(12) . .
O19 Sn2 Sn3 O13 -175.4(14) . .
O20 Sn2 Sn3 O13 144.3(12) . .
C50 Sn2 Sn3 O13 -85.8(19) . .
Sn6 Sn2 Sn3 O13 104.5(10) . .
Sn1 Sn2 Sn3 O13 161.7(10) . .
O12 Sn2 Sn3 C46 147.1(19) . .
O13 Sn2 Sn3 C46 88(2) . .
O19 Sn2 Sn3 C46 -87(2) . .
O20 Sn2 Sn3 C46 -127.5(18) . .
C50 Sn2 Sn3 C46 2(2) . .
Sn6 Sn2 Sn3 C46 -167.4(17) . .
Sn1 Sn2 Sn3 C46 -110.1(17) . .
O12 Sn2 Sn3 Sn6 -21.7(7) . 3_566
O13 Sn2 Sn3 Sn6 -80.7(10) . 3_566
O19 Sn2 Sn3 Sn6 103.9(10) . 3_566
O20 Sn2 Sn3 Sn6 63.7(6) . 3_566
C50 Sn2 Sn3 Sn6 -166.5(17) . 3_566
Sn6 Sn2 Sn3 Sn6 23.83(16) . 3_566
Sn1 Sn2 Sn3 Sn6 81.04(11) . 3_566
O12 Sn2 Sn3 Sn4 35.9(7) . 3_566
O13 Sn2 Sn3 Sn4 -23.1(10) . 3_566
O19 Sn2 Sn3 Sn4 161.5(10) . 3_566
O20 Sn2 Sn3 Sn4 121.3(6) . 3_566
C50 Sn2 Sn3 Sn4 -108.9(17) . 3_566
Sn6 Sn2 Sn3 Sn4 81.45(11) . 3_566
Sn1 Sn2 Sn3 Sn4 138.65(9) . 3_566
O16 Sn1 Sn4 O17 -172.5(14) . .
O20 Sn1 Sn4 O17 90.6(11) . .
O19 Sn1 Sn4 O17 19.4(11) . .
O18 Sn1 Sn4 O17 -69.9(11) . .
C62 Sn1 Sn4 O17 -169.4(19) . .
Sn2 Sn1 Sn4 O17 59.6(9) . .
O17 Sn1 Sn4 O15 69.8(11) . .
O16 Sn1 Sn4 O15 -102.8(13) . .
O20 Sn1 Sn4 O15 160.4(9) . .
O19 Sn1 Sn4 O15 89.2(10) . .
O18 Sn1 Sn4 O15 -0.1(9) . .
C62 Sn1 Sn4 O15 -99.6(18) . .
Sn2 Sn1 Sn4 O15 129.4(7) . .
O17 Sn1 Sn4 C58 171(2) . .
O16 Sn1 Sn4 C58 -1(2) . .
O20 Sn1 Sn4 C58 -98(2) . .
O19 Sn1 Sn4 C58 -169(2) . .
O18 Sn1 Sn4 C58 101(2) . .
C62 Sn1 Sn4 C58 2(3) . .
Sn2 Sn1 Sn4 C58 -129.0(19) . .
O17 Sn1 Sn4 O13 -20.3(11) . 3_566
O16 Sn1 Sn4 O13 167.1(13) . 3_566
O20 Sn1 Sn4 O13 70.3(9) . 3_566
O19 Sn1 Sn4 O13 -0.9(10) . 3_566
O18 Sn1 Sn4 O13 -90.2(10) . 3_566
C62 Sn1 Sn4 O13 170.2(18) . 3_566
Sn2 Sn1 Sn4 O13 39.3(7) . 3_566
O17 Sn1 Sn4 O16 172.5(14) . .
O20 Sn1 Sn4 O16 -96.9(12) . .
O19 Sn1 Sn4 O16 -168.1(13) . .
O18 Sn1 Sn4 O16 102.7(13) . .
C62 Sn1 Sn4 O16 3(2) . .
Sn2 Sn1 Sn4 O16 -127.8(11) . .
O17 Sn1 Sn4 O11 -90.6(10) . .
O16 Sn1 Sn4 O11 96.9(12) . .
O20 Sn1 Sn4 O11 0.0(8) . .
O19 Sn1 Sn4 O11 -71.2(9) . .
O18 Sn1 Sn4 O11 -160.5(9) . .
C62 Sn1 Sn4 O11 100.0(18) . .
Sn2 Sn1 Sn4 O11 -31.0(6) . .
O17 Sn1 Sn4 Sn5 41.8(9) . .
O16 Sn1 Sn4 Sn5 -130.7(11) . .
O20 Sn1 Sn4 Sn5 132.4(6) . .
O19 Sn1 Sn4 Sn5 61.2(7) . .
O18 Sn1 Sn4 Sn5 -28.0(7) . .
C62 Sn1 Sn4 Sn5 -127.6(17) . .
Sn2 Sn1 Sn4 Sn5 101.46(10) . .
O17 Sn1 Sn4 Sn3 -59.9(9) . 3_566
O16 Sn1 Sn4 Sn3 127.5(11) . 3_566
O20 Sn1 Sn4 Sn3 30.7(6) . 3_566
O19 Sn1 Sn4 Sn3 -40.6(7) . 3_566
O18 Sn1 Sn4 Sn3 -129.8(7) . 3_566
C62 Sn1 Sn4 Sn3 130.6(17) . 3_566
Sn2 Sn1 Sn4 Sn3 -0.33(12) . 3_566
O15 Sn4 Sn5 O17 -172.1(15) . .
C58 Sn4 Sn5 O17 -169(2) . .
O13 Sn4 Sn5 O17 91.1(11) 3_566 .
O16 Sn4 Sn5 O17 -69.3(11) . .
O11 Sn4 Sn5 O17 21.0(11) . .
Sn1 Sn4 Sn5 O17 -41.0(9) . .
Sn3 Sn4 Sn5 O17 60.6(9) 3_566 .
O17 Sn4 Sn5 O15 172.1(15) . .
C58 Sn4 Sn5 O15 4(2) . .
O13 Sn4 Sn5 O15 -96.9(13) 3_566 .
O16 Sn4 Sn5 O15 102.7(14) . .
O11 Sn4 Sn5 O15 -166.9(14) . .
Sn1 Sn4 Sn5 O15 131.1(12) . .
Sn3 Sn4 Sn5 O15 -127.3(12) 3_566 .
O17 Sn4 Sn5 O12 -90.9(11) . 3_566
O15 Sn4 Sn5 O12 97.1(13) . 3_566
C58 Sn4 Sn5 O12 101(2) . 3_566
O13 Sn4 Sn5 O12 0.2(8) 3_566 3_566
O16 Sn4 Sn5 O12 -160.2(9) . 3_566
O11 Sn4 Sn5 O12 -69.9(9) . 3_566
Sn1 Sn4 Sn5 O12 -131.8(6) . 3_566
Sn3 Sn4 Sn5 O12 -30.2(6) 3_566 3_566
O17 Sn4 Sn5 O18 69.1(11) . .
O15 Sn4 Sn5 O18 -103.0(14) . .
C58 Sn4 Sn5 O18 -99(2) . .
O13 Sn4 Sn5 O18 160.1(9) 3_566 .
O16 Sn4 Sn5 O18 -0.3(9) . .
O11 Sn4 Sn5 O18 90.1(10) . .
Sn1 Sn4 Sn5 O18 28.1(7) . .
Sn3 Sn4 Sn5 O18 129.7(7) 3_566 .
O17 Sn4 Sn5 O14 -19.4(11) . .
O15 Sn4 Sn5 O14 168.5(14) . .
C58 Sn4 Sn5 O14 172(2) . .
O13 Sn4 Sn5 O14 71.6(9) 3_566 .
O16 Sn4 Sn5 O14 -88.8(10) . .
O11 Sn4 Sn5 O14 1.6(10) . .
Sn1 Sn4 Sn5 O14 -60.4(7) . .
Sn3 Sn4 Sn5 O14 41.2(7) 3_566 .
O17 Sn4 Sn5 C42 170(2) . .
O15 Sn4 Sn5 C42 -2(2) . .
C58 Sn4 Sn5 C42 2(3) . .
O13 Sn4 Sn5 C42 -99(2) 3_566 .
O16 Sn4 Sn5 C42 101(2) . .
O11 Sn4 Sn5 C42 -169(2) . .
Sn1 Sn4 Sn5 C42 129(2) . .
Sn3 Sn4 Sn5 C42 -129(2) 3_566 .
O17 Sn4 Sn5 Sn6 -60.1(9) . 3_566
O15 Sn4 Sn5 Sn6 127.8(12) . 3_566
C58 Sn4 Sn5 Sn6 131(2) . 3_566
O13 Sn4 Sn5 Sn6 30.9(6) 3_566 3_566
O16 Sn4 Sn5 Sn6 -129.5(7) . 3_566
O11 Sn4 Sn5 Sn6 -39.1(7) . 3_566
Sn1 Sn4 Sn5 Sn6 -101.10(10) . 3_566
Sn3 Sn4 Sn5 Sn6 0.50(13) 3_566 3_566
O12 Sn2 Sn6 O11 126.5(12) . .
O13 Sn2 Sn6 O11 67.8(10) . .
O19 Sn2 Sn6 O11 -17.5(9) . .
O20 Sn2 Sn6 O11 -59.5(12) . .
C50 Sn2 Sn6 O11 -147.4(18) . .
Sn3 Sn2 Sn6 O11 22.0(7) . .
Sn1 Sn2 Sn6 O11 -35.5(7) . .
O12 Sn2 Sn6 O20 -174.0(14) . .
O13 Sn2 Sn6 O20 127.3(12) . .
O19 Sn2 Sn6 O20 42.0(11) . .
C50 Sn2 Sn6 O20 -88.0(19) . .
Sn3 Sn2 Sn6 O20 81.4(10) . .
Sn1 Sn2 Sn6 O20 23.9(9) . .
O13 Sn2 Sn6 O12 -58.7(12) . .
O19 Sn2 Sn6 O12 -144.0(12) . .
O20 Sn2 Sn6 O12 174.0(14) . .
C50 Sn2 Sn6 O12 86.0(19) . .
Sn3 Sn2 Sn6 O12 -104.6(10) . .
Sn1 Sn2 Sn6 O12 -162.0(10) . .
O12 Sn2 Sn6 O14 41.1(11) . 3_566
O13 Sn2 Sn6 O14 -17.6(9) . 3_566
O19 Sn2 Sn6 O14 -102.9(9) . 3_566
O20 Sn2 Sn6 O14 -144.8(11) . 3_566
C50 Sn2 Sn6 O14 127.2(18) . 3_566
Sn3 Sn2 Sn6 O14 -63.4(6) . 3_566
Sn1 Sn2 Sn6 O14 -120.9(6) . 3_566
O12 Sn2 Sn6 C54 -83.4(17) . .
O13 Sn2 Sn6 C54 -142.2(15) . .
O19 Sn2 Sn6 C54 132.6(15) . .
O20 Sn2 Sn6 C54 90.6(17) . .
C50 Sn2 Sn6 C54 3(2) . .
Sn3 Sn2 Sn6 C54 172.0(14) . .
Sn1 Sn2 Sn6 C54 114.5(14) . .
O12 Sn2 Sn6 Sn3 80.9(10) . 3_566
O13 Sn2 Sn6 Sn3 22.1(7) . 3_566
O19 Sn2 Sn6 Sn3 -63.1(6) . 3_566
O20 Sn2 Sn6 Sn3 -105.1(10) . 3_566
C50 Sn2 Sn6 Sn3 166.9(17) . 3_566
Sn3 Sn2 Sn6 Sn3 -23.69(16) . 3_566
Sn1 Sn2 Sn6 Sn3 -81.18(10) . 3_566
O12 Sn2 Sn6 Sn5 23.2(9) . 3_566
O13 Sn2 Sn6 Sn5 -35.5(7) . 3_566
O19 Sn2 Sn6 Sn5 -120.8(6) . 3_566
O20 Sn2 Sn6 Sn5 -162.8(10) . 3_566
C50 Sn2 Sn6 Sn5 109.3(17) . 3_566
Sn3 Sn2 Sn6 Sn5 -81.33(11) . 3_566
Sn1 Sn2 Sn6 Sn5 -138.82(9) . 3_566
C6 C1 C2 C3 -1(7) . .
C7 C1 C2 C3 -180(4) . .
C6 C1 C2 O7 -176(4) . .
C7 C1 C2 O7 6(7) . .
C1 C2 C3 C4 0(6) . .
O7 C2 C3 C4 174(3) . .
C1 C2 C3 C11 176(4) . .
O7 C2 C3 C11 -10(5) . .
C2 C3 C4 C5 0(5) . .
C11 C3 C4 C5 -175(4) . .
C3 C4 C5 C6 1(6) . .
C3 C4 C5 C39 178(3) . .
C4 C5 C6 C1 -2(6) . .
C39 C5 C6 C1 -179(4) . .
C4 C5 C6 O9 -178(3) . .
C39 C5 C6 O9 5(6) . .
C2 C1 C6 C5 2(7) . .
C7 C1 C6 C5 -179(4) . .
C2 C1 C6 O9 178(4) . .
C7 C1 C6 O9 -3(7) . .
C13 C9 C10 C16 1(6) . .
O8 C9 C10 C16 -176(4) . .
C13 C9 C10 C11 -175(4) . .
O8 C9 C10 C11 8(6) . .
C4 C3 C11 C12 -34(5) . .
C2 C3 C11 C12 151(4) . .
C4 C3 C11 C10 92(4) . .
C2 C3 C11 C10 -84(4) . .
C16 C10 C11 C12 34(5) . .
C9 C10 C11 C12 -150(4) . .
C16 C10 C11 C3 -91(5) . .
C9 C10 C11 C3 85(4) . .
C10 C9 C13 C14 -1(6) . .
O8 C9 C13 C14 176(4) . .
C10 C9 C13 C17 180(4) . .
O8 C9 C13 C17 -3(7) . .
C9 C13 C14 C15 0(7) . .
C17 C13 C14 C15 179(4) . .
C9 C13 C14 O6 -178(4) . .
C17 C13 C14 O6 1(6) . .
C13 C14 C15 C16 1(6) . .
O6 C14 C15 C16 179(3) . .
C13 C14 C15 C21 176(4) . .
O6 C14 C15 C21 -6(6) . .
C9 C10 C16 C15 0(6) . .
C11 C10 C16 C15 176(3) . .
C14 C15 C16 C10 -1(6) . .
C21 C15 C16 C10 -176(4) . .
O5 C19 C20 C26 -179(3) . .
C23 C19 C20 C26 -3(5) . .
O5 C19 C20 C21 4(5) . .
C23 C19 C20 C21 180(3) . .
C26 C20 C21 C15 -92(4) . .
C19 C20 C21 C15 85(4) . .
C26 C20 C21 C22 36(5) . .
C19 C20 C21 C22 -147(4) . .
C14 C15 C21 C20 -84(5) . .
C16 C15 C21 C20 91(5) . .
C14 C15 C21 C22 147(4) . .
C16 C15 C21 C22 -38(5) . .
C20 C19 C23 C24 4(6) . .
O5 C19 C23 C24 179(3) . .
C20 C19 C23 C27 -177(4) . .
O5 C19 C23 C27 -1(5) . .
C19 C23 C24 O3 -174(3) . .
C27 C23 C24 O3 7(5) . .
C19 C23 C24 C25 -2(5) . .
C27 C23 C24 C25 178(3) . .
C23 C24 C25 C26 1(5) . .
O3 C24 C25 C26 173(3) . .
C23 C24 C25 C31 178(3) . .
O3 C24 C25 C31 -11(5) . .
C19 C20 C26 C25 2(5) . .
C21 C20 C26 C25 179(3) . .
C24 C25 C26 C20 -1(5) . .
C31 C25 C26 C20 -177(4) . .
C33 C29 C30 C36 -1(6) . .
O4 C29 C30 C36 -175(3) . .
C33 C29 C30 C31 -178(4) . .
O4 C29 C30 C31 8(5) . .
C36 C30 C31 C25 -93(4) . .
C29 C30 C31 C25 83(4) . .
C36 C30 C31 C32 36(5) . .
C29 C30 C31 C32 -148(4) . .
C26 C25 C31 C30 96(4) . .
C24 C25 C31 C30 -81(4) . .
C26 C25 C31 C32 -34(5) . .
C24 C25 C31 C32 149(4) . .
O4 C29 C33 C34 177(4) . .
C30 C29 C33 C34 3(6) . .
O4 C29 C33 C37 -4(6) . .
C30 C29 C33 C37 -177(4) . .
C29 C33 C34 C35 -4(6) . .
C37 C33 C34 C35 177(4) . .
C29 C33 C34 O10 174(4) . .
C37 C33 C34 O10 -5(6) . .
C33 C34 C35 C36 2(6) . .
O10 C34 C35 C36 -176(3) . .
C33 C34 C35 C39 179(4) . .
O10 C34 C35 C39 1(6) . .
C34 C35 C36 C30 0(6) . .
C39 C35 C36 C30 -177(4) . .
C29 C30 C36 C35 0(6) . .
C31 C30 C36 C35 176(3) . .
C6 C5 C39 C40 -146(4) . .
C4 C5 C39 C40 37(6) . .
C6 C5 C39 C35 86(5) . .
C4 C5 C39 C35 -91(5) . .
C36 C35 C39 C5 88(5) . .
C34 C35 C39 C5 -89(5) . .
C36 C35 C39 C40 -43(5) . .
C34 C35 C39 C40 141(4) . .
O3 C28 C41 O2 -52(6) . .
O4 C28 C41 O2 81(5) . .
O3 C28 C41 O1 127(4) . .
O4 C28 C41 O1 -100(4) . .
O17 Sn5 C42 C43 99(11) . .
O15 Sn5 C42 C43 55(4) . .
O12 Sn5 C42 C43 -39(4) 3_566 .
O18 Sn5 C42 C43 153(3) . .
O14 Sn5 C42 C43 -116(3) . .
Sn4 Sn5 C42 C43 56(4) . .
Sn6 Sn5 C42 C43 -77(4) 3_566 .
Sn5 C42 C43 C44 -161(4) . .
C42 C43 C44 C45 -176(6) . .
O19 Sn3 C46 C47 146(5) . .
O14 Sn3 C46 C47 41(6) . .
O11 Sn3 C46 C47 -45(6) 3_566 .
O13 Sn3 C46 C47 -130(6) . .
Sn6 Sn3 C46 C47 -3(6) 3_566 .
Sn2 Sn3 C46 C47 -171(5) . .
Sn4 Sn3 C46 C47 -88(6) 3_566 .
Sn3 C46 C47 C48 -67(10) . .
C46 C47 C48 C49 -123(14) . .
O12 Sn2 C50 C51 35(6) . .
O13 Sn2 C50 C51 141(5) . .
O19 Sn2 C50 C51 -135(5) . .
O20 Sn2 C50 C51 -50(6) . .
Sn3 Sn2 C50 C51 -177(5) . .
Sn6 Sn2 C50 C51 -8(6) . .
Sn1 Sn2 C50 C51 -92(5) . .
Sn2 C50 C51 C52 53(10) . .
C50 C51 C52 C53 168(7) . .
O11 Sn6 C54 C55 36(5) . .
O20 Sn6 C54 C55 -73(5) . .
O12 Sn6 C54 C55 -157(5) . .
O14 Sn6 C54 C55 120(5) 3_566 .
Sn3 Sn6 C54 C55 79(5) 3_566 .
Sn2 Sn6 C54 C55 -116(5) . .
Sn5 Sn6 C54 C55 162(4) 3_566 .
Sn6 C54 C55 C56 50(9) . .
C54 C55 C56 C57 177(6) . .
O17 Sn4 C58 C59 103(10) . .
O15 Sn4 C58 C59 162(5) . .
O13 Sn4 C58 C59 -105(5) 3_566 .
O16 Sn4 C58 C59 64(5) . .
O11 Sn4 C58 C59 -28(5) . .
Sn5 Sn4 C58 C59 160(4) . .
Sn1 Sn4 C58 C59 65(6) . .
Sn3 Sn4 C58 C59 -67(5) 3_566 .
Sn4 C58 C59 C60 179(6) . .
C58 C59 C60 C61 -159(8) . .
O17 Sn1 C62 C63 -105(9) . .
O16 Sn1 C62 C63 -50(4) . .
O20 Sn1 C62 C63 43(4) . .
O19 Sn1 C62 C63 120(4) . .
O18 Sn1 C62 C63 -148(4) . .
Sn4 Sn1 C62 C63 -52(4) . .
Sn2 Sn1 C62 C63 82(4) . .
Sn1 C62 C63 C64 -176(4) . .
C62 C63 C64 C65 179(5) . .
C23 C24 O3 C28 -104(4) . .
C25 C24 O3 C28 84(4) . .
O4 C28 O3 C24 -81(4) . .
C41 C28 O3 C24 52(5) . .
C33 C29 O4 C28 100(5) . .
C30 C29 O4 C28 -86(4) . .
O3 C28 O4 C29 83(4) . .
C41 C28 O4 C29 -52(5) . .
O6 C18 O5 C19 91(4) . .
C20 C19 O5 C18 -78(5) . .
C23 C19 O5 C18 106(4) . .
C15 C14 O6 C18 80(5) . .
C13 C14 O6 C18 -102(5) . .
O5 C18 O6 C14 -92(5) . .
C1 C2 O7 C8 -100(5) . .
C3 C2 O7 C8 85(5) . .
O8 C8 O7 C2 -91(5) . .
C13 C9 O8 C8 98(5) . .
C10 C9 O8 C8 -85(5) . .
O7 C8 O8 C9 91(5) . .
O10 C38 O9 C6 95(5) . .
C5 C6 O9 C38 -83(6) . .
C1 C6 O9 C38 101(6) . .
C33 C34 O10 C38 -103(5) . .
C35 C34 O10 C38 75(5) . .
O9 C38 O10 C34 -93(5) . .
O20 Sn6 O11 Sn3 -131.9(9) . 3_566
O12 Sn6 O11 Sn3 -53.8(15) . 3_566
O14 Sn6 O11 Sn3 3.2(8) 3_566 3_566
C54 Sn6 O11 Sn3 108.9(15) . 3_566
Sn2 Sn6 O11 Sn3 -98.6(8) . 3_566
Sn5 Sn6 O11 Sn3 -18.6(9) 3_566 3_566
O20 Sn6 O11 Sn4 -8.8(16) . .
O12 Sn6 O11 Sn4 69.3(19) . .
O14 Sn6 O11 Sn4 126.2(15) 3_566 .
C54 Sn6 O11 Sn4 -128.1(18) . .
Sn3 Sn6 O11 Sn4 123.0(18) 3_566 .
Sn2 Sn6 O11 Sn4 24.4(17) . .
Sn5 Sn6 O11 Sn4 104.4(13) 3_566 .
O17 Sn4 O11 Sn6 -31.7(15) . .
O15 Sn4 O11 Sn6 -68(3) . .
C58 Sn4 O11 Sn6 142.0(19) . .
O13 Sn4 O11 Sn6 -119.8(16) 3_566 .
O16 Sn4 O11 Sn6 44.3(15) . .
Sn5 Sn4 O11 Sn6 -44.5(17) . .
Sn1 Sn4 O11 Sn6 5.9(13) . .
Sn3 Sn4 O11 Sn6 -122.7(19) 3_566 .
O17 Sn4 O11 Sn3 91.0(9) . 3_566
O15 Sn4 O11 Sn3 54(3) . 3_566
C58 Sn4 O11 Sn3 -95.4(16) . 3_566
O13 Sn4 O11 Sn3 2.9(9) 3_566 3_566
O16 Sn4 O11 Sn3 167.0(10) . 3_566
Sn5 Sn4 O11 Sn3 78.1(9) . 3_566
Sn1 Sn4 O11 Sn3 128.5(8) . 3_566
O13 Sn2 O12 Sn6 132.3(9) . .
O19 Sn2 O12 Sn6 53.3(15) . .
O20 Sn2 O12 Sn6 -3.8(9) . .
C50 Sn2 O12 Sn6 -113.8(16) . .
Sn3 Sn2 O12 Sn6 98.9(8) . .
Sn1 Sn2 O12 Sn6 18.1(9) . .
O13 Sn2 O12 Sn5 7.9(16) . 3_566
O19 Sn2 O12 Sn5 -71.1(19) . 3_566
O20 Sn2 O12 Sn5 -128.1(16) . 3_566
C50 Sn2 O12 Sn5 122(2) . 3_566
Sn3 Sn2 O12 Sn5 -25.4(17) . 3_566
Sn6 Sn2 O12 Sn5 -124.3(19) . 3_566
Sn1 Sn2 O12 Sn5 -106.2(14) . 3_566
O11 Sn6 O12 Sn2 -82.3(14) . .
O20 Sn6 O12 Sn2 3.9(9) . .
O14 Sn6 O12 Sn2 -139.6(10) 3_566 .
C54 Sn6 O12 Sn2 114.9(15) . .
Sn3 Sn6 O12 Sn2 -114.7(7) 3_566 .
Sn5 Sn6 O12 Sn2 -142.9(14) 3_566 .
O11 Sn6 O12 Sn5 60.6(14) . 3_566
O20 Sn6 O12 Sn5 146.7(10) . 3_566
O14 Sn6 O12 Sn5 3.3(8) 3_566 3_566
C54 Sn6 O12 Sn5 -102.3(15) . 3_566
Sn3 Sn6 O12 Sn5 28.2(9) 3_566 3_566
Sn2 Sn6 O12 Sn5 142.9(14) . 3_566
O12 Sn2 O13 Sn3 -132.1(10) . .
O19 Sn2 O13 Sn3 2.9(9) . .
O20 Sn2 O13 Sn3 -53.6(15) . .
C50 Sn2 O13 Sn3 112.4(16) . .
Sn6 Sn2 O13 Sn3 -99.1(8) . .
Sn1 Sn2 O13 Sn3 -18.6(10) . .
O12 Sn2 O13 Sn4 -8.3(17) . 3_566
O19 Sn2 O13 Sn4 126.7(17) . 3_566
O20 Sn2 O13 Sn4 70.2(19) . 3_566
C50 Sn2 O13 Sn4 -124(2) . 3_566
Sn3 Sn2 O13 Sn4 124(2) . 3_566
Sn6 Sn2 O13 Sn4 24.7(18) . 3_566
Sn1 Sn2 O13 Sn4 105.2(14) . 3_566
O19 Sn3 O13 Sn2 -3.0(9) . .
O14 Sn3 O13 Sn2 82.5(14) . .
O11 Sn3 O13 Sn2 140.2(11) 3_566 .
C46 Sn3 O13 Sn2 -109.5(17) . .
Sn6 Sn3 O13 Sn2 115.4(7) 3_566 .
Sn4 Sn3 O13 Sn2 143.1(15) 3_566 .
O19 Sn3 O13 Sn4 -146.1(11) . 3_566
O14 Sn3 O13 Sn4 -60.6(15) . 3_566
O11 Sn3 O13 Sn4 -2.9(9) 3_566 3_566
C46 Sn3 O13 Sn4 107.3(17) . 3_566
Sn6 Sn3 O13 Sn4 -27.7(10) 3_566 3_566
Sn2 Sn3 O13 Sn4 -143.1(15) . 3_566
O19 Sn3 O14 Sn6 132.4(9) . 3_566
O11 Sn3 O14 Sn6 -3.2(8) 3_566 3_566
O13 Sn3 O14 Sn6 54.2(14) . 3_566
C46 Sn3 O14 Sn6 -113.6(17) . 3_566
Sn2 Sn3 O14 Sn6 99.8(7) . 3_566
Sn4 Sn3 O14 Sn6 18.8(9) 3_566 3_566
O19 Sn3 O14 Sn5 9.8(16) . .
O11 Sn3 O14 Sn5 -125.8(16) 3_566 .
O13 Sn3 O14 Sn5 -68(2) . .
C46 Sn3 O14 Sn5 124(2) . .
Sn6 Sn3 O14 Sn5 -122.6(19) 3_566 .
Sn2 Sn3 O14 Sn5 -22.8(18) . .
Sn4 Sn3 O14 Sn5 -103.7(14) 3_566 .
O17 Sn5 O14 Sn3 30.0(15) . .
O15 Sn5 O14 Sn3 64(3) . .
O12 Sn5 O14 Sn3 118.9(16) 3_566 .
O18 Sn5 O14 Sn3 -45.6(16) . .
C42 Sn5 O14 Sn3 -145(2) . .
Sn4 Sn5 O14 Sn3 41.9(18) . .
Sn6 Sn5 O14 Sn3 122.1(19) 3_566 .
O17 Sn5 O14 Sn6 -92.1(9) . 3_566
O15 Sn5 O14 Sn6 -59(3) . 3_566
O12 Sn5 O14 Sn6 -3.3(8) 3_566 3_566
O18 Sn5 O14 Sn6 -167.8(9) . 3_566
C42 Sn5 O14 Sn6 92.9(16) . 3_566
Sn4 Sn5 O14 Sn6 -80.3(9) . 3_566
O16 Sn1 O17 Sn4 4.8(9) . .
O20 Sn1 O17 Sn4 -87.9(9) . .
O19 Sn1 O17 Sn4 -163.9(9) . .
O18 Sn1 O17 Sn4 104.7(11) . .
C62 Sn1 O17 Sn4 61(9) . .
Sn2 Sn1 O17 Sn4 -126.0(7) . .
O16 Sn1 O17 Sn5 -104.3(10) . .
O20 Sn1 O17 Sn5 163.0(10) . .
O19 Sn1 O17 Sn5 87.0(9) . .
O18 Sn1 O17 Sn5 -4.4(9) . .
C62 Sn1 O17 Sn5 -48(9) . .
Sn4 Sn1 O17 Sn5 -109.1(12) . .
Sn2 Sn1 O17 Sn5 124.9(8) . .
O15 Sn4 O17 Sn1 -105.3(11) . .
C58 Sn4 O17 Sn1 -45(10) . .
O13 Sn4 O17 Sn1 163.1(9) 3_566 .
O16 Sn4 O17 Sn1 -4.8(9) . .
O11 Sn4 O17 Sn1 87.1(9) . .
Sn5 Sn4 O17 Sn1 -110.3(12) . .
Sn3 Sn4 O17 Sn1 125.1(7) 3_566 .
O15 Sn4 O17 Sn5 5.1(9) . .
C58 Sn4 O17 Sn5 65(10) . .
O13 Sn4 O17 Sn5 -86.6(9) 3_566 .
O16 Sn4 O17 Sn5 105.5(10) . .
O11 Sn4 O17 Sn5 -162.6(9) . .
Sn1 Sn4 O17 Sn5 110.3(12) . .
Sn3 Sn4 O17 Sn5 -124.6(7) 3_566 .
O15 Sn5 O17 Sn1 104.9(11) . .
O12 Sn5 O17 Sn1 -162.5(10) 3_566 .
O18 Sn5 O17 Sn1 4.4(10) . .
O14 Sn5 O17 Sn1 -86.1(10) . .
C42 Sn5 O17 Sn1 59(11) . .
Sn4 Sn5 O17 Sn1 109.9(12) . .
Sn6 Sn5 O17 Sn1 -124.3(8) 3_566 .
O15 Sn5 O17 Sn4 -5.1(9) . .
O12 Sn5 O17 Sn4 87.6(9) 3_566 .
O18 Sn5 O17 Sn4 -105.6(11) . .
O14 Sn5 O17 Sn4 164.0(9) . .
C42 Sn5 O17 Sn4 -51(11) . .
Sn6 Sn5 O17 Sn4 125.7(7) 3_566 .
O14 Sn3 O19 Sn2 -132.9(10) . .
O11 Sn3 O19 Sn2 -54.0(16) 3_566 .
O13 Sn3 O19 Sn2 2.9(9) . .
C46 Sn3 O19 Sn2 110(2) . .
Sn6 Sn3 O19 Sn2 -99.6(8) 3_566 .
Sn4 Sn3 O19 Sn2 -18.7(10) 3_566 .
O14 Sn3 O19 Sn1 -8.6(16) . .
O11 Sn3 O19 Sn1 70(2) 3_566 .
O13 Sn3 O19 Sn1 127.2(17) . .
C46 Sn3 O19 Sn1 -125(2) . .
Sn6 Sn3 O19 Sn1 24.7(18) 3_566 .
Sn2 Sn3 O19 Sn1 124(2) . .
Sn4 Sn3 O19 Sn1 105.6(14) 3_566 .
O12 Sn2 O19 Sn3 83.6(14) . .
O13 Sn2 O19 Sn3 -3.0(9) . .
O20 Sn2 O19 Sn3 140.8(11) . .
C50 Sn2 O19 Sn3 -109.4(17) . .
Sn6 Sn2 O19 Sn3 115.6(7) . .
Sn1 Sn2 O19 Sn3 143.7(15) . .
O12 Sn2 O19 Sn1 -60.1(15) . .
O13 Sn2 O19 Sn1 -146.7(11) . .
O20 Sn2 O19 Sn1 -2.9(9) . .
C50 Sn2 O19 Sn1 107.0(17) . .
Sn3 Sn2 O19 Sn1 -143.7(15) . .
Sn6 Sn2 O19 Sn1 -28.1(9) . .
O17 Sn1 O19 Sn3 -32.3(16) . .
O16 Sn1 O19 Sn3 -67(3) . .
O20 Sn1 O19 Sn3 -121.0(17) . .
O18 Sn1 O19 Sn3 43.6(16) . .
C62 Sn1 O19 Sn3 142.0(18) . .
Sn4 Sn1 O19 Sn3 -44.0(18) . .
Sn2 Sn1 O19 Sn3 -124(2) . .
O17 Sn1 O19 Sn2 91.7(9) . .
O16 Sn1 O19 Sn2 57(3) . .
O20 Sn1 O19 Sn2 2.9(9) . .
O18 Sn1 O19 Sn2 167.6(10) . .
C62 Sn1 O19 Sn2 -94.1(14) . .
Sn4 Sn1 O19 Sn2 80.0(9) . .
O11 Sn6 O20 Sn2 131.7(9) . .
O12 Sn6 O20 Sn2 -3.8(8) . .
O14 Sn6 O20 Sn2 51.9(15) 3_566 .
C54 Sn6 O20 Sn2 -110.5(14) . .
Sn3 Sn6 O20 Sn2 98.1(8) 3_566 .
Sn5 Sn6 O20 Sn2 17.3(9) 3_566 .
O11 Sn6 O20 Sn1 8.7(16) . .
O12 Sn6 O20 Sn1 -126.7(16) . .
O14 Sn6 O20 Sn1 -71.0(19) 3_566 .
C54 Sn6 O20 Sn1 126.5(18) . .
Sn3 Sn6 O20 Sn1 -24.8(17) 3_566 .
Sn2 Sn6 O20 Sn1 -123.0(19) . .
Sn5 Sn6 O20 Sn1 -105.7(14) 3_566 .
O12 Sn2 O20 Sn6 3.9(9) . .
O13 Sn2 O20 Sn6 -82.2(13) . .
O19 Sn2 O20 Sn6 -138.9(11) . .
C50 Sn2 O20 Sn6 112.1(16) . .
Sn3 Sn2 O20 Sn6 -114.7(7) . .
Sn1 Sn2 O20 Sn6 -141.8(14) . .
O12 Sn2 O20 Sn1 145.7(11) . .
O13 Sn2 O20 Sn1 59.7(15) . .
O19 Sn2 O20 Sn1 3.0(9) . .
C50 Sn2 O20 Sn1 -106.1(17) . .
Sn3 Sn2 O20 Sn1 27.1(9) . .
Sn6 Sn2 O20 Sn1 141.8(14) . .
O17 Sn1 O20 Sn6 31.9(15) . .
O16 Sn1 O20 Sn6 -44.6(15) . .
O19 Sn1 O20 Sn6 119.8(16) . .
O18 Sn1 O20 Sn6 70(3) . .
C62 Sn1 O20 Sn6 -144.0(18) . .
Sn4 Sn1 O20 Sn6 -5.8(14) . .
Sn2 Sn1 O20 Sn6 122.7(19) . .
O17 Sn1 O20 Sn2 -90.8(9) . .
O16 Sn1 O20 Sn2 -167.3(10) . .
O19 Sn1 O20 Sn2 -2.9(9) . .
O18 Sn1 O20 Sn2 -53(3) . .
C62 Sn1 O20 Sn2 93.3(14) . .
Sn4 Sn1 O20 Sn2 -128.5(8) . .
O17 Sn4 O15 Sn5 -5.0(9) . .
C58 Sn4 O15 Sn5 -177.6(16) . .
O13 Sn4 O15 Sn5 82.1(11) 3_566 .
O16 Sn4 O15 Sn5 -79.0(11) . .
O11 Sn4 O15 Sn5 33(3) . .
Sn1 Sn4 O15 Sn5 -41.0(9) . .
Sn3 Sn4 O15 Sn5 72.0(13) 3_566 .
O17 Sn5 O15 Sn4 5.0(9) . .
O12 Sn5 O15 Sn4 -82.7(11) 3_566 .
O18 Sn5 O15 Sn4 78.5(11) . .
O14 Sn5 O15 Sn4 -30(3) . .
C42 Sn5 O15 Sn4 178.8(16) . .
Sn6 Sn5 O15 Sn4 -72.6(13) 3_566 .
O17 Sn5 O18 Sn1 -4.2(9) . .
O15 Sn5 O18 Sn1 -78.2(11) . .
O12 Sn5 O18 Sn1 36(3) 3_566 .
O14 Sn5 O18 Sn1 83.3(11) . .
C42 Sn5 O18 Sn1 -177.1(17) . .
Sn4 Sn5 O18 Sn1 -40.6(9) . .
Sn6 Sn5 O18 Sn1 73.8(12) 3_566 .
O17 Sn1 O18 Sn5 4.3(9) . .
O16 Sn1 O18 Sn5 78.7(11) . .
O20 Sn1 O18 Sn5 -35(3) . .
O19 Sn1 O18 Sn5 -83.0(11) . .
C62 Sn1 O18 Sn5 178.7(14) . .
Sn4 Sn1 O18 Sn5 40.5(9) . .
Sn2 Sn1 O18 Sn5 -73.4(12) . .
O17 Sn1 O16 Sn4 -4.7(9) . .
O20 Sn1 O16 Sn4 83.0(10) . .
O19 Sn1 O16 Sn4 31(3) . .
O18 Sn1 O16 Sn4 -78.6(11) . .
C62 Sn1 O16 Sn4 -177.9(14) . .
Sn2 Sn1 O16 Sn4 72.9(11) . .
O17 Sn4 O16 Sn1 4.7(9) . .
O15 Sn4 O16 Sn1 78.9(11) . .
C58 Sn4 O16 Sn1 179.2(15) . .
O13 Sn4 O16 Sn1 -32(3) 3_566 .
O11 Sn4 O16 Sn1 -82.1(10) . .
Sn5 Sn4 O16 Sn1 41.3(8) . .
Sn3 Sn4 O16 Sn1 -72.0(11) 3_566 .
