#------------------------------------------------------------------------------
#$Date: 2016-03-25 22:31:57 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180014 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/08/7030891.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7030891
loop_
_publ_author_name
'Fässler, Thomas F'
'Zeilinger, Michael'
_publ_section_title
;
 Structural and Thermodynamic Similarities of Phases in the Li--Tt (Tt =
 Si, Ge) Systems: Redetermination of the Lithium-Rich Side of the Li--Ge
 Phase Diagram and Crystal Structures of Li17Si4.0−xGex for x =
 2.3, 3.1, 3.5, and 4 as well as Li4.1Ge
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/c4dt00743c
_journal_year                    2014
_chemical_formula_analytical     'Ge Li4.096'
_chemical_formula_moiety         'Ge Li4.096'
_chemical_formula_sum            'Ge Li4.096'
_chemical_formula_weight         101.01
_chemical_melting_point          '900 K, peritectic decomposition'
_chemical_name_common            'Lithium Germanide'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   4.5511(2)
_cell_length_b                   22.0862(7)
_cell_length_c                   13.2751(4)
_cell_measurement_reflns_used    8466
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      42.2278
_cell_measurement_theta_min      3.5813
_cell_volume                     1334.37(8)
_citation_year                   2014
_computing_cell_refinement
'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. '
_computing_data_collection
;APEX suite of crystallographic software. APEX 2 Version 2008.4,
 Bruker AXS Inc., Madison, Wisconsin, USA, 2008.
;
_computing_data_reduction
'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. '
_computing_molecular_graphics    'Diamond 3.2i (Crystal Impact 2012)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      123(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'phi- and omega-rotation'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0234
_diffrn_reflns_av_sigmaI/netI    0.0166
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            15241
_diffrn_reflns_theta_full        40.25
_diffrn_reflns_theta_max         40.25
_diffrn_reflns_theta_min         1.84
_exptl_absorpt_coefficient_mu    8.860
_exptl_absorpt_correction_T_max  0.7483
_exptl_absorpt_correction_T_min  0.5989
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, Bruker, 2008b'
_exptl_crystal_colour            'metallic silver'
_exptl_crystal_density_diffrn    2.011
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             709
_exptl_crystal_size_max          0.37
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.23
_refine_diff_density_max         0.688
_refine_diff_density_min         -0.519
_refine_diff_density_rms         0.084
_refine_ls_extinction_coef       0.00152(7)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_matrix_type           full
_refine_ls_number_parameters     82
_refine_ls_number_reflns         2369
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0225
_refine_ls_R_factor_gt           0.0145
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0090P)²+0.2032P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0257
_refine_ls_wR_factor_ref         0.0270
_reflns_number_gt                1920
_reflns_number_total             2369
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt00743c6.cif
_cod_data_source_block           Li4Ge_123K
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               7030891
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Ge1 Ge 0.0000 0.256372(6) 0.2500 0.00783(3) Uani 1 4 d S .
Ge2 Ge 0.5000 0.454314(5) 0.2500 0.00635(3) Uani 1 4 d S .
Ge3 Ge 0.5000 0.105220(4) 0.067609(6) 0.00683(2) Uani 1 2 d S .
Li1 Li 0.5000 0.03326(11) 0.2500 0.0144(4) Uani 1 4 d S .
Li2 Li 0.5000 0.32965(10) 0.2500 0.0135(4) Uani 1 4 d S .
Li3 Li 0.0000 0.39223(11) 0.2500 0.0175(5) Uani 1 4 d S .
Li4A Li 0.5000 0.1476(2) 0.2500 0.052(3) Uani 0.616(8) 4 d SP 1
Li5A Li 0.0000 0.1741(3) 0.0842(7) 0.0139(11) Uani 0.75(4) 2 d SP 1
Li4B Li 0.2098(12) 0.1385(2) 0.2500 0.0210(16) Uani 0.384(8) 2 d SP 2
Li5B Li 0.0000 0.1641(10) 0.123(4) 0.024(6) Uani 0.25(4) 2 d SP 2
Li6 Li 0.0000 0.04650(7) 0.12254(14) 0.0139(3) Uani 1 2 d S .
Li7 Li 0.0000 0.31636(9) 0.07878(13) 0.0165(3) Uani 1 2 d S .
Li8 Li 0.0000 0.47089(9) 0.09082(14) 0.0187(3) Uani 1 2 d S .
Li9 Li 0.5000 0.23155(8) 0.13557(14) 0.0191(3) Uani 1 2 d S .
Li10 Li 0.5000 0.40425(8) 0.06385(12) 0.0145(3) Uani 1 2 d S .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Li7 Ge1 Li7 119.52(9) 10_556 .
Li7 Ge1 Li5B 159.8(12) 10_556 .
Li7 Ge1 Li5B 80.7(12) . .
Li7 Ge1 Li5B 80.7(12) 10_556 10_556
Li7 Ge1 Li5B 159.8(12) . 10_556
Li5B Ge1 Li5B 79(2) . 10_556
Li7 Ge1 Li4B 118.21(5) 10_556 3
Li7 Ge1 Li4B 118.22(5) . 3
Li7 Ge1 Li4B 118.22(5) 10_556 .
Li7 Ge1 Li4B 118.22(5) . .
Li7 Ge1 Li9 124.70(3) 10_556 1_455
Li7 Ge1 Li9 68.20(4) . 1_455
Li5B Ge1 Li9 60.1(4) . 1_455
Li5B Ge1 Li9 101.3(6) 10_556 1_455
Li4B Ge1 Li9 62.27(10) 3 1_455
Li4B Ge1 Li9 95.54(11) . 1_455
Li7 Ge1 Li9 68.20(5) 10_556 10_556
Li7 Ge1 Li9 124.70(3) . 10_556
Li5B Ge1 Li9 101.3(6) . 10_556
Li5B Ge1 Li9 60.1(4) 10_556 10_556
Li4B Ge1 Li9 95.54(11) 3 10_556
Li4B Ge1 Li9 62.27(10) . 10_556
Li9 Ge1 Li9 157.34(8) 1_455 10_556
Li7 Ge1 Li9 68.20(5) 10_556 10_456
Li7 Ge1 Li9 124.70(3) . 10_456
Li5B Ge1 Li9 101.3(6) . 10_456
Li5B Ge1 Li9 60.1(4) 10_556 10_456
Li4B Ge1 Li9 62.27(10) 3 10_456
Li4B Ge1 Li9 95.54(11) . 10_456
Li9 Ge1 Li9 65.97(7) 1_455 10_456
Li9 Ge1 Li9 109.27(6) 10_556 10_456
Li7 Ge1 Li9 124.70(3) 10_556 .
Li7 Ge1 Li9 68.20(5) . .
Li5B Ge1 Li9 60.1(4) . .
Li5B Ge1 Li9 101.3(6) 10_556 .
Li4B Ge1 Li9 95.54(11) 3 .
Li4B Ge1 Li9 62.27(10) . .
Li9 Ge1 Li9 109.27(6) 1_455 .
Li9 Ge1 Li9 65.97(7) 10_556 .
Li9 Ge1 Li9 157.34(8) 10_456 .
Li7 Ge1 Li2 73.03(3) 10_556 .
Li7 Ge1 Li2 73.03(3) . .
Li5B Ge1 Li2 116.5(5) . .
Li5B Ge1 Li2 116.5(5) 10_556 .
Li4B Ge1 Li2 145.57(12) 3 .
Li4B Ge1 Li2 105.27(13) . .
Li9 Ge1 Li2 141.12(4) 1_455 .
Li9 Ge1 Li2 56.59(4) 10_556 .
Li9 Ge1 Li2 141.12(4) 10_456 .
Li9 Ge1 Li2 56.59(4) . .
Li7 Ge1 Li2 73.03(3) 10_556 1_455
Li7 Ge1 Li2 73.03(3) . 1_455
Li5B Ge1 Li2 116.5(5) . 1_455
Li5B Ge1 Li2 116.5(5) 10_556 1_455
Li4B Ge1 Li2 105.27(12) 3 1_455
Li4B Ge1 Li2 145.57(12) . 1_455
Li9 Ge1 Li2 56.59(4) 1_455 1_455
Li9 Ge1 Li2 141.12(4) 10_556 1_455
Li9 Ge1 Li2 56.59(4) 10_456 1_455
Li9 Ge1 Li2 141.12(4) . 1_455
Li2 Ge1 Li2 109.16(8) . 1_455
Li6 Ge2 Li6 79.46(8) 14_556 5
Li6 Ge2 Li3 113.39(3) 14_556 .
Li6 Ge2 Li3 113.39(3) 5 .
Li6 Ge2 Li3 113.39(3) 14_556 1_655
Li6 Ge2 Li3 113.39(3) 5 1_655
Li3 Ge2 Li3 117.86(9) . 1_655
Li6 Ge2 Li10 153.83(6) 14_556 .
Li6 Ge2 Li10 74.38(5) 5 .
Li3 Ge2 Li10 77.83(2) . .
Li3 Ge2 Li10 77.83(2) 1_655 .
Li6 Ge2 Li10 74.38(5) 14_556 10_556
Li6 Ge2 Li10 153.83(6) 5 10_556
Li3 Ge2 Li10 77.83(2) . 10_556
Li3 Ge2 Li10 77.83(2) 1_655 10_556
Li10 Ge2 Li10 131.79(8) . 10_556
Li6 Ge2 Li2 140.27(4) 14_556 .
Li6 Ge2 Li2 140.27(4) 5 .
Li3 Ge2 Li2 58.93(4) . .
Li3 Ge2 Li2 58.93(4) 1_655 .
Li10 Ge2 Li2 65.89(4) . .
Li10 Ge2 Li2 65.89(4) 10_556 .
Li6 Ge2 Li1 62.11(3) 14_556 5
Li6 Ge2 Li1 62.11(3) 5 5
Li3 Ge2 Li1 173.61(6) . 5
Li3 Ge2 Li1 68.53(6) 1_655 5
Li10 Ge2 Li1 104.38(3) . 5
Li10 Ge2 Li1 104.38(3) 10_556 5
Li2 Ge2 Li1 127.46(4) . 5
Li6 Ge2 Li1 62.11(3) 14_556 5_455
Li6 Ge2 Li1 62.11(3) 5 5_455
Li3 Ge2 Li1 68.53(6) . 5_455
Li3 Ge2 Li1 173.61(6) 1_655 5_455
Li10 Ge2 Li1 104.38(3) . 5_455
Li10 Ge2 Li1 104.38(3) 10_556 5_455
Li2 Ge2 Li1 127.46(4) . 5_455
Li1 Ge2 Li1 105.08(8) 5 5_455
Li6 Ge2 Li8 109.99(4) 14_556 .
Li6 Ge2 Li8 58.53(4) 5 .
Li3 Ge2 Li8 55.74(4) . .
Li3 Ge2 Li8 133.14(3) 1_655 .
Li10 Ge2 Li8 55.32(3) . .
Li10 Ge2 Li8 131.66(3) 10_556 .
Li2 Ge2 Li8 96.72(3) . .
Li1 Ge2 Li8 120.43(4) 5 .
Li1 Ge2 Li8 49.54(4) 5_455 .
Li6 Ge2 Li8 58.54(4) 14_556 10_656
Li6 Ge2 Li8 109.99(4) 5 10_656
Li3 Ge2 Li8 133.14(3) . 10_656
Li3 Ge2 Li8 55.74(4) 1_655 10_656
Li10 Ge2 Li8 131.66(3) . 10_656
Li10 Ge2 Li8 55.32(3) 10_556 10_656
Li2 Ge2 Li8 96.72(3) . 10_656
Li1 Ge2 Li8 49.54(4) 5 10_656
Li1 Ge2 Li8 120.43(4) 5_455 10_656
Li8 Ge2 Li8 166.55(7) . 10_656
Li6 Ge2 Li8 109.99(4) 14_556 1_655
Li6 Ge2 Li8 58.54(4) 5 1_655
Li3 Ge2 Li8 133.14(3) . 1_655
Li3 Ge2 Li8 55.74(4) 1_655 1_655
Li10 Ge2 Li8 55.32(3) . 1_655
Li10 Ge2 Li8 131.66(3) 10_556 1_655
Li2 Ge2 Li8 96.72(3) . 1_655
Li1 Ge2 Li8 49.54(4) 5 1_655
Li1 Ge2 Li8 120.43(4) 5_455 1_655
Li8 Ge2 Li8 93.39(5) . 1_655
Li8 Ge2 Li8 85.03(5) 10_656 1_655
Li4A Ge3 Li7 117.14(11) . 13
Li4A Ge3 Li8 162.52(11) . 13
Li7 Ge3 Li8 80.34(6) 13 13
Li4A Ge3 Li6 85.53(7) . .
Li7 Ge3 Li6 121.17(3) 13 .
Li8 Ge3 Li6 84.93(4) 13 .
Li4A Ge3 Li6 85.53(7) . 1_655
Li7 Ge3 Li6 121.17(3) 13 1_655
Li8 Ge3 Li6 84.93(4) 13 1_655
Li6 Ge3 Li6 113.64(6) . 1_655
Li4A Ge3 Li5B 64.8(9) . 1_655
Li7 Ge3 Li5B 83.4(11) 13 1_655
Li8 Ge3 Li5B 120.7(7) 13 1_655
Li6 Ge3 Li5B 148.7(11) . 1_655
Li6 Ge3 Li5B 57.0(5) 1_655 1_655
Li4A Ge3 Li5B 64.8(9) . .
Li7 Ge3 Li5B 83.4(11) 13 .
Li8 Ge3 Li5B 120.7(7) 13 .
Li6 Ge3 Li5B 57.0(5) . .
Li6 Ge3 Li5B 148.7(11) 1_655 .
Li5B Ge3 Li5B 113.3(5) 1_655 .
Li4A Ge3 Li5A 74.05(18) . .
Li7 Ge3 Li5A 72.0(2) 13 .
Li8 Ge3 Li5A 114.13(13) 13 .
Li6 Ge3 Li5A 63.22(15) . .
Li6 Ge3 Li5A 159.43(19) 1_655 .
Li5B Ge3 Li5A 113.93(19) 1_655 .
Li4A Ge3 Li5A 74.05(18) . 1_655
Li7 Ge3 Li5A 72.0(2) 13 1_655
Li8 Ge3 Li5A 114.13(13) 13 1_655
Li6 Ge3 Li5A 159.43(19) . 1_655
Li6 Ge3 Li5A 63.22(15) 1_655 1_655
Li5B Ge3 Li5A 113.93(19) . 1_655
Li5A Ge3 Li5A 111.89(17) . 1_655
Li7 Ge3 Li4B 117.50(9) 13 .
Li8 Ge3 Li4B 145.44(11) 13 .
Li6 Ge3 Li4B 60.54(11) . .
Li6 Ge3 Li4B 106.42(9) 1_655 .
Li5B Ge3 Li4B 91.9(9) 1_655 .
Li5A Ge3 Li4B 53.5(2) . .
Li5A Ge3 Li4B 99.92(18) 1_655 .
Li7 Ge3 Li4B 117.50(9) 13 3_655
Li8 Ge3 Li4B 145.44(11) 13 3_655
Li6 Ge3 Li4B 106.42(9) . 3_655
Li6 Ge3 Li4B 60.54(11) 1_655 3_655
Li5B Ge3 Li4B 91.9(9) . 3_655
Li5A Ge3 Li4B 99.92(18) . 3_655
Li5A Ge3 Li4B 53.5(2) 1_655 3_655
Li4B Ge3 Li4B 55.1(2) . 3_655
Li4A Ge3 Li10 126.32(3) . 13
Li7 Ge3 Li10 66.13(4) 13 13
Li8 Ge3 Li10 58.70(3) 13 13
Li6 Ge3 Li10 57.70(4) . 13
Li6 Ge3 Li10 142.23(5) 1_655 13
Li5B Ge3 Li10 149.4(11) 1_655 13
Li5B Ge3 Li10 62.5(8) . 13
Li5A Ge3 Li10 55.48(12) . 13
Li5A Ge3 Li10 138.1(2) 1_655 13
Li4B Ge3 Li10 99.64(10) . 13
Li4B Ge3 Li10 154.12(11) 3_655 13
Li8 Li1 Li8 113.80(13) 5_545 14_546
Li8 Li1 Li4A 123.10(7) 5_545 .
Li8 Li1 Li4A 123.10(7) 14_546 .
Li8 Li1 Li4B 118.35(6) 5_545 .
Li8 Li1 Li4B 118.35(6) 14_546 .
Li4A Li1 Li4B 29.60(12) . .
Li8 Li1 Li4B 118.35(6) 5_545 3_655
Li8 Li1 Li4B 118.35(6) 14_546 3_655
Li4A Li1 Li4B 29.59(12) . 3_655
Li4B Li1 Li4B 59.2(2) . 3_655
Li8 Li1 Li6 123.59(5) 5_545 10_656
Li8 Li1 Li6 63.82(4) 14_546 10_656
Li4A Li1 Li6 84.11(6) . 10_656
Li4B Li1 Li6 107.76(12) . 10_656
Li4B Li1 Li6 61.09(10) 3_655 10_656
Li8 Li1 Li6 63.82(4) 5_545 1_655
Li8 Li1 Li6 123.59(5) 14_546 1_655
Li4A Li1 Li6 84.11(6) . 1_655
Li4B Li1 Li6 107.76(12) . 1_655
Li4B Li1 Li6 61.09(10) 3_655 1_655
Li6 Li1 Li6 72.82(6) 10_656 1_655
Li8 Li1 Li6 123.59(5) 5_545 10_556
Li8 Li1 Li6 63.82(4) 14_546 10_556
Li4A Li1 Li6 84.11(6) . 10_556
Li4B Li1 Li6 61.09(10) . 10_556
Li4B Li1 Li6 107.76(12) 3_655 10_556
Li6 Li1 Li6 105.92(6) 10_656 10_556
Li6 Li1 Li6 168.23(12) 1_655 10_556
Li8 Li1 Li6 63.82(4) 5_545 .
Li8 Li1 Li6 123.59(5) 14_546 .
Li4A Li1 Li6 84.11(6) . .
Li4B Li1 Li6 61.09(10) . .
Li4B Li1 Li6 107.76(12) 3_655 .
Li6 Li1 Li6 168.22(12) 10_656 .
Li6 Li1 Li6 105.92(6) 1_655 .
Li6 Li1 Li6 72.82(6) 10_556 .
Li8 Li1 Ge2 70.60(5) 5_545 5_445
Li8 Li1 Ge2 70.60(5) 14_546 5_445
Li4A Li1 Ge2 127.46(4) . 5_445
Li4B Li1 Ge2 97.86(12) . 5_445
Li4B Li1 Ge2 157.05(14) 3_655 5_445
Li6 Li1 Ge2 134.11(7) 10_656 5_445
Li6 Li1 Ge2 134.11(7) 1_655 5_445
Li6 Li1 Ge2 55.16(3) 10_556 5_445
Li6 Li1 Ge2 55.16(3) . 5_445
Li8 Li1 Ge2 70.60(5) 5_545 5_545
Li8 Li1 Ge2 70.60(5) 14_546 5_545
Li4A Li1 Ge2 127.46(4) . 5_545
Li4B Li1 Ge2 157.06(14) . 5_545
Li4B Li1 Ge2 97.87(12) 3_655 5_545
Li6 Li1 Ge2 55.16(3) 10_656 5_545
Li6 Li1 Ge2 55.16(3) 1_655 5_545
Li6 Li1 Ge2 134.11(7) 10_556 5_545
Li6 Li1 Ge2 134.11(7) . 5_545
Ge2 Li1 Ge2 105.08(8) 5_445 5_545
Li8 Li1 Ge3 179.82(10) 5_545 10_556
Li8 Li1 Ge3 66.38(5) 14_546 10_556
Li4A Li1 Ge3 56.72(4) . 10_556
Li4B Li1 Ge3 61.50(6) . 10_556
Li4B Li1 Ge3 61.50(6) 3_655 10_556
Li6 Li1 Ge3 56.46(3) 10_656 10_556
Li6 Li1 Ge3 116.10(6) 1_655 10_556
Li6 Li1 Ge3 56.46(3) 10_556 10_556
Li6 Li1 Ge3 116.10(6) . 10_556
Ge2 Li1 Ge3 109.495(4) 5_445 10_556
Ge2 Li1 Ge3 109.495(5) 5_545 10_556
Li9 Li2 Li9 70.07(10) 10_556 .
Li9 Li2 Li3 115.16(5) 10_556 1_655
Li9 Li2 Li3 115.16(5) . 1_655
Li9 Li2 Li3 115.16(5) 10_556 .
Li9 Li2 Li3 115.16(5) . .
Li3 Li2 Li3 117.45(12) 1_655 .
Li9 Li2 Ge2 144.97(5) 10_556 .
Li9 Li2 Ge2 144.97(5) . .
Li3 Li2 Ge2 58.72(6) 1_655 .
Li3 Li2 Ge2 58.72(6) . .
Li9 Li2 Ge1 61.67(4) 10_556 .
Li9 Li2 Ge1 61.67(4) . .
Li3 Li2 Ge1 175.85(9) 1_655 .
Li3 Li2 Ge1 66.70(4) . .
Ge2 Li2 Ge1 125.42(4) . .
Li9 Li2 Ge1 61.67(4) 10_556 1_655
Li9 Li2 Ge1 61.67(4) . 1_655
Li3 Li2 Ge1 66.70(4) 1_655 1_655
Li3 Li2 Ge1 175.85(9) . 1_655
Ge2 Li2 Ge1 125.42(4) . 1_655
Ge1 Li2 Ge1 109.16(8) . 1_655
Li9 Li2 Li10 88.66(5) 10_556 10_556
Li9 Li2 Li10 158.73(9) . 10_556
Li3 Li2 Li10 73.26(5) 1_655 10_556
Li3 Li2 Li10 73.26(5) . 10_556
Ge2 Li2 Li10 56.31(5) . 10_556
Ge1 Li2 Li10 108.756(17) . 10_556
Ge1 Li2 Li10 108.755(17) 1_655 10_556
Li9 Li2 Li10 158.73(9) 10_556 .
Li9 Li2 Li10 88.66(5) . .
Li3 Li2 Li10 73.26(5) 1_655 .
Li3 Li2 Li10 73.26(5) . .
Ge2 Li2 Li10 56.31(5) . .
Ge1 Li2 Li10 108.756(17) . .
Ge1 Li2 Li10 108.757(17) 1_655 .
Li10 Li2 Li10 112.61(10) 10_556 .
Li9 Li2 Li7 61.42(5) 10_556 10_656
Li9 Li2 Li7 109.24(7) . 10_656
Li3 Li2 Li7 56.29(4) 1_655 10_656
Li3 Li2 Li7 130.49(5) . 10_656
Ge2 Li2 Li7 95.21(6) . 10_656
Ge1 Li2 Li7 121.43(6) . 10_656
Ge1 Li2 Li7 51.18(3) 1_655 10_656
Li10 Li2 Li7 57.65(4) 10_556 10_656
Li10 Li2 Li7 129.49(6) . 10_656
Li9 Li2 Li7 109.24(7) 10_556 1_655
Li9 Li2 Li7 61.42(5) . 1_655
Li3 Li2 Li7 56.29(4) 1_655 1_655
Li3 Li2 Li7 130.49(5) . 1_655
Ge2 Li2 Li7 95.21(6) . 1_655
Ge1 Li2 Li7 121.43(6) . 1_655
Ge1 Li2 Li7 51.18(3) 1_655 1_655
Li10 Li2 Li7 129.49(6) 10_556 1_655
Li10 Li2 Li7 57.65(4) . 1_655
Li7 Li2 Li7 89.46(4) 10_656 1_655
Li9 Li2 Li7 61.42(5) 10_556 10_556
Li9 Li2 Li7 109.24(7) . 10_556
Li3 Li2 Li7 130.49(5) 1_655 10_556
Li3 Li2 Li7 56.29(4) . 10_556
Ge2 Li2 Li7 95.21(6) . 10_556
Ge1 Li2 Li7 51.18(3) . 10_556
Ge1 Li2 Li7 121.43(6) 1_655 10_556
Li10 Li2 Li7 57.65(4) 10_556 10_556
Li10 Li2 Li7 129.49(6) . 10_556
Li7 Li2 Li7 89.59(4) 10_656 10_556
Li7 Li2 Li7 169.57(12) 1_655 10_556
Ge2 Li3 Ge2 117.86(9) . 1_455
Ge2 Li3 Li2 179.79(10) . 1_455
Ge2 Li3 Li2 62.35(4) 1_455 1_455
Ge2 Li3 Li2 62.35(4) . .
Ge2 Li3 Li2 179.80(10) 1_455 .
Li2 Li3 Li2 117.45(13) 1_455 .
Ge2 Li3 Li8 70.87(5) . 10_556
Ge2 Li3 Li8 70.87(5) 1_455 10_556
Li2 Li3 Li8 109.25(3) 1_455 10_556
Li2 Li3 Li8 109.25(3) . 10_556
Ge2 Li3 Li8 70.87(5) . .
Ge2 Li3 Li8 70.87(5) 1_455 .
Li2 Li3 Li8 109.25(3) 1_455 .
Li2 Li3 Li8 109.25(3) . .
Li8 Li3 Li8 101.15(11) 10_556 .
Ge2 Li3 Li7 107.834(16) . 10_556
Ge2 Li3 Li7 107.834(16) 1_455 10_556
Li2 Li3 Li7 72.06(5) 1_455 10_556
Li2 Li3 Li7 72.06(5) . 10_556
Li8 Li3 Li7 75.82(5) 10_556 10_556
Li8 Li3 Li7 176.97(10) . 10_556
Ge2 Li3 Li7 107.833(16) . .
Ge2 Li3 Li7 107.835(16) 1_455 .
Li2 Li3 Li7 72.06(5) 1_455 .
Li2 Li3 Li7 72.06(5) . .
Li8 Li3 Li7 176.98(10) 10_556 .
Li8 Li3 Li7 75.82(5) . .
Li7 Li3 Li7 107.20(11) 10_556 .
Ge2 Li3 Ge1 121.07(4) . .
Ge2 Li3 Ge1 121.07(4) 1_455 .
Li2 Li3 Ge1 58.72(6) 1_455 .
Li2 Li3 Ge1 58.72(6) . .
Li8 Li3 Ge1 129.42(6) 10_556 .
Li8 Li3 Ge1 129.43(6) . .
Li7 Li3 Ge1 53.60(5) 10_556 .
Li7 Li3 Ge1 53.60(5) . .
Ge2 Li3 Li1 58.93(4) . 5_455
Ge2 Li3 Li1 58.93(4) 1_455 5_455
Li2 Li3 Li1 121.28(6) 1_455 5_455
Li2 Li3 Li1 121.28(6) . 5_455
Li8 Li3 Li1 50.58(6) 10_556 5_455
Li8 Li3 Li1 50.58(6) . 5_455
Li7 Li3 Li1 126.40(5) 10_556 5_455
Li7 Li3 Li1 126.40(5) . 5_455
Ge1 Li3 Li1 180.0 . 5_455
Ge2 Li3 Li10 51.75(3) . 10_556
Ge2 Li3 Li10 122.53(5) 1_455 10_556
Li2 Li3 Li10 128.17(5) 1_455 10_556
Li2 Li3 Li10 57.57(3) . 10_556
Li8 Li3 Li10 51.94(3) 10_556 10_556
Li8 Li3 Li10 121.09(7) . 10_556
Li7 Li3 Li10 57.08(4) 10_556 10_556
Li7 Li3 Li10 129.57(6) . 10_556
Ge1 Li3 Li10 94.52(5) . 10_556
Li1 Li3 Li10 85.48(5) 5_455 10_556
Ge2 Li3 Li10 122.53(5) . 1_455
Ge2 Li3 Li10 51.75(3) 1_455 1_455
Li2 Li3 Li10 57.57(3) 1_455 1_455
Li2 Li3 Li10 128.17(5) . 1_455
Li8 Li3 Li10 121.09(7) 10_556 1_455
Li8 Li3 Li10 51.94(3) . 1_455
Li7 Li3 Li10 129.57(6) 10_556 1_455
Li7 Li3 Li10 57.08(4) . 1_455
Ge1 Li3 Li10 94.52(5) . 1_455
Li1 Li3 Li10 85.48(5) 5_455 1_455
Li10 Li3 Li10 170.96(10) 10_556 1_455
Li9 Li4A Li9 78.68(18) . 10_556
Li9 Li4A Li1 140.66(9) . .
Li9 Li4A Li1 140.66(9) 10_556 .
Li9 Li4A Ge3 150.50(19) . 10_556
Li9 Li4A Ge3 71.81(5) 10_556 10_556
Li1 Li4A Ge3 68.84(11) . 10_556
Li9 Li4A Ge3 71.81(5) . .
Li9 Li4A Ge3 150.50(19) 10_556 .
Li1 Li4A Ge3 68.85(11) . .
Ge3 Li4A Ge3 137.7(2) 10_556 .
Li9 Li4A Li5A 54.97(14) . .
Li9 Li4A Li5A 107.02(15) 10_556 .
Li1 Li4A Li5A 100.47(13) . .
Ge3 Li4A Li5A 134.68(14) 10_556 .
Ge3 Li4A Li5A 55.11(8) . .
Li9 Li4A Li5A 107.02(15) . 10_656
Li9 Li4A Li5A 54.97(14) 10_556 10_656
Li1 Li4A Li5A 100.48(13) . 10_656
Ge3 Li4A Li5A 55.12(8) 10_556 10_656
Ge3 Li4A Li5A 134.68(14) . 10_656
Li5A Li4A Li5A 159.0(3) . 10_656
Li9 Li4A Li5A 54.97(14) . 1_655
Li9 Li4A Li5A 107.02(15) 10_556 1_655
Li1 Li4A Li5A 100.48(13) . 1_655
Ge3 Li4A Li5A 134.68(14) 10_556 1_655
Ge3 Li4A Li5A 55.12(8) . 1_655
Li5A Li4A Li5A 90.0(3) . 1_655
Li5A Li4A Li5A 86.3(2) 10_656 1_655
Li9 Li4A Li5A 107.02(15) . 10_556
Li9 Li4A Li5A 54.97(14) 10_556 10_556
Li1 Li4A Li5A 100.48(13) . 10_556
Ge3 Li4A Li5A 55.12(8) 10_556 10_556
Ge3 Li4A Li5A 134.68(14) . 10_556
Li5A Li4A Li5A 86.3(2) . 10_556
Li5A Li4A Li5A 90.0(3) 10_656 10_556
Li5A Li4A Li5A 159.0(3) 1_655 10_556
Li10 Li5A Li9 120.08(15) 13 .
Li10 Li5A Li9 120.08(15) 13 1_455
Li9 Li5A Li9 115.36(14) . 1_455
Li10 Li5A Ge3 64.75(7) 13 .
Li9 Li5A Ge3 65.24(4) . .
Li9 Li5A Ge3 168.9(4) 1_455 .
Li10 Li5A Ge3 64.75(7) 13 1_455
Li9 Li5A Ge3 168.9(4) . 1_455
Li9 Li5A Ge3 65.24(4) 1_455 1_455
Ge3 Li5A Ge3 111.89(17) . 1_455
Li10 Li5A Ge1 178.2(4) 13 .
Li9 Li5A Ge1 60.33(9) . .
Li9 Li5A Ge1 60.33(9) 1_455 .
Ge3 Li5A Ge1 114.5(2) . .
Ge3 Li5A Ge1 114.5(2) 1_455 .
Li10 Li5A Li6 58.85(10) 13 .
Li9 Li5A Li6 114.7(2) . .
Li9 Li5A Li6 114.7(2) 1_455 .
Ge3 Li5A Li6 57.92(12) . .
Ge3 Li5A Li6 57.92(12) 1_455 .
Ge1 Li5A Li6 119.3(4) . .
Li10 Li5A Li7 130.1(4) 13 .
Li9 Li5A Li7 62.30(11) . .
Li9 Li5A Li7 62.29(11) 1_455 .
Ge3 Li5A Li7 123.52(13) . .
Ge3 Li5A Li7 123.52(13) 1_455 .
Ge1 Li5A Li7 51.79(7) . .
Li6 Li5A Li7 171.1(3) . .
Li10 Li5A Li7 61.84(15) 13 13_455
Li9 Li5A Li7 138.9(4) . 13_455
Li9 Li5A Li7 62.07(11) 1_455 13_455
Ge3 Li5A Li7 125.5(2) . 13_455
Ge3 Li5A Li7 51.88(8) 1_455 13_455
Ge1 Li5A Li7 119.20(13) . 13_455
Li6 Li5A Li7 100.82(10) . 13_455
Li7 Li5A Li7 85.3(2) . 13_455
Li10 Li5A Li7 61.84(15) 13 13
Li9 Li5A Li7 62.07(11) . 13
Li9 Li5A Li7 138.9(4) 1_455 13
Ge3 Li5A Li7 51.88(8) . 13
Ge3 Li5A Li7 125.5(2) 1_455 13
Ge1 Li5A Li7 119.20(13) . 13
Li6 Li5A Li7 100.82(10) . 13
Li7 Li5A Li7 85.3(2) . 13
Li7 Li5A Li7 92.6(3) 13_455 13
Li10 Li5A Li4A 113.13(17) 13 .
Li9 Li5A Li4A 46.78(13) . .
Li9 Li5A Li4A 120.7(3) 1_455 .
Ge3 Li5A Li4A 50.84(12) . .
Ge3 Li5A Li4A 122.7(3) 1_455 .
Ge1 Li5A Li4A 65.70(17) . .
Li6 Li5A Li4A 72.5(2) . .
Li7 Li5A Li4A 101.39(13) . .
Li7 Li5A Li4A 173.3(2) 13_455 .
Li7 Li5A Li4A 88.34(3) 13 .
Li10 Li5A Li4A 113.13(17) 13 1_455
Li9 Li5A Li4A 120.7(3) . 1_455
Li9 Li5A Li4A 46.78(13) 1_455 1_455
Ge3 Li5A Li4A 122.7(3) . 1_455
Ge3 Li5A Li4A 50.84(12) 1_455 1_455
Ge1 Li5A Li4A 65.70(17) . 1_455
Li6 Li5A Li4A 72.5(2) . 1_455
Li7 Li5A Li4A 101.39(13) . 1_455
Li7 Li5A Li4A 88.34(3) 13_455 1_455
Li7 Li5A Li4A 173.3(2) 13 1_455
Li4A Li5A Li4A 90.0(3) . 1_455
Li4B Li4B Li5B 61.7(8) 3 10_556
Li4B Li4B Li5B 61.7(8) 3 .
Li5B Li4B Li5B 113.2(13) 10_556 .
Li4B Li4B Li4B 179.996(2) 3 3_655
Li5B Li4B Li4B 118.3(8) 10_556 3_655
Li5B Li4B Li4B 118.3(8) . 3_655
Li4B Li4B Li1 119.60(12) 3 .
Li5B Li4B Li1 118.6(4) 10_556 .
Li5B Li4B Li1 118.6(4) . .
Li4B Li4B Li1 60.41(12) 3_655 .
Li4B Li4B Ge1 69.85(12) 3 .
Li5B Li4B Ge1 64.7(3) 10_556 .
Li5B Li4B Ge1 64.7(3) . .
Li4B Li4B Ge1 110.15(12) 3_655 .
Li1 Li4B Ge1 170.6(2) . .
Li4B Li4B Li6 70.15(11) 3 .
Li5B Li4B Li6 123.0(7) 10_556 .
Li5B Li4B Li6 62.6(4) . .
Li4B Li4B Li6 109.86(11) 3_655 .
Li1 Li4B Li6 62.56(9) . .
Ge1 Li4B Li6 124.17(15) . .
Li4B Li4B Li6 70.15(11) 3 10_556
Li5B Li4B Li6 62.6(4) 10_556 10_556
Li5B Li4B Li6 123.0(7) . 10_556
Li4B Li4B Li6 109.85(11) 3_655 10_556
Li1 Li4B Li6 62.56(9) . 10_556
Ge1 Li4B Li6 124.17(15) . 10_556
Li6 Li4B Li6 73.99(14) . 10_556
Li4B Li4B Ge3 117.56(10) 3 10_556
Li5B Li4B Ge3 65.4(6) 10_556 10_556
Li5B Li4B Ge3 178.4(4) . 10_556
Li4B Li4B Ge3 62.44(10) 3_655 10_556
Li1 Li4B Ge3 63.09(8) . 10_556
Ge1 Li4B Ge3 113.66(10) . 10_556
Li6 Li4B Ge3 118.77(15) . 10_556
Li6 Li4B Ge3 57.34(5) 10_556 10_556
Li4B Li4B Ge3 117.56(10) 3 .
Li5B Li4B Ge3 178.4(4) 10_556 .
Li5B Li4B Ge3 65.4(6) . .
Li4B Li4B Ge3 62.44(10) 3_655 .
Li1 Li4B Ge3 63.09(8) . .
Ge1 Li4B Ge3 113.66(10) . .
Li6 Li4B Ge3 57.34(5) . .
Li6 Li4B Ge3 118.77(15) 10_556 .
Ge3 Li4B Ge3 116.04(17) 10_556 .
Li4B Li4B Li9 117.33(10) 3 .
Li5B Li4B Li9 117.3(4) 10_556 .
Li5B Li4B Li9 64.9(7) . .
Li4B Li4B Li9 62.67(10) 3_655 .
Li1 Li4B Li9 113.22(17) . .
Ge1 Li4B Li9 59.18(9) . .
Li6 Li4B Li9 110.76(5) . .
Li6 Li4B Li9 171.94(19) 10_556 .
Ge3 Li4B Li9 114.82(18) 10_556 .
Ge3 Li4B Li9 61.55(8) . .
Li4B Li4B Li9 117.33(10) 3 10_556
Li5B Li4B Li9 64.9(7) 10_556 10_556
Li5B Li4B Li9 117.3(4) . 10_556
Li4B Li4B Li9 62.67(10) 3_655 10_556
Li1 Li4B Li9 113.23(17) . 10_556
Ge1 Li4B Li9 59.18(9) . 10_556
Li6 Li4B Li9 171.94(19) . 10_556
Li6 Li4B Li9 110.76(5) 10_556 10_556
Ge3 Li4B Li9 61.55(8) 10_556 10_556
Ge3 Li4B Li9 114.82(18) . 10_556
Li9 Li4B Li9 63.76(13) . 10_556
Li4B Li5B Li4B 56.6(16) . 3
Li4B Li5B Li6 73.9(12) . .
Li4B Li5B Li6 73.9(12) 3 .
Li4B Li5B Ge1 71.6(11) . .
Li4B Li5B Ge1 71.6(11) 3 .
Li6 Li5B Ge1 141(2) . .
Li4B Li5B Li9 73.0(5) . .
Li4B Li5B Li9 119.9(17) 3 .
Li6 Li5B Li9 123.1(5) . .
Ge1 Li5B Li9 62.6(2) . .
Li4B Li5B Li9 119.9(17) . 1_455
Li4B Li5B Li9 73.0(5) 3 1_455
Li6 Li5B Li9 123.1(5) . 1_455
Ge1 Li5B Li9 62.6(2) . 1_455
Li9 Li5B Li9 113.3(6) . 1_455
Li4B Li5B Ge3 119.2(18) . 1_455
Li4B Li5B Ge3 72.3(6) 3 1_455
Li6 Li5B Ge3 61.4(3) . 1_455
Ge1 Li5B Ge3 122.8(6) . 1_455
Li9 Li5B Ge3 167(2) . 1_455
Li9 Li5B Ge3 65.13(17) 1_455 1_455
Li4B Li5B Ge3 72.3(6) . .
Li4B Li5B Ge3 119.2(18) 3 .
Li6 Li5B Ge3 61.4(3) . .
Ge1 Li5B Ge3 122.8(6) . .
Li9 Li5B Ge3 65.13(17) . .
Li9 Li5B Ge3 167(2) 1_455 .
Ge3 Li5B Ge3 113.3(5) 1_455 .
Li4B Li5B Li10 124.6(6) . 13
Li4B Li5B Li10 124.6(6) 3 13
Li6 Li5B Li10 58.5(4) . 13
Ge1 Li5B Li10 161(2) . 13
Li9 Li5B Li10 109.6(12) . 13
Li9 Li5B Li10 109.6(12) 1_455 13
Ge3 Li5B Li10 61.3(6) 1_455 13
Ge3 Li5B Li10 61.3(6) . 13
Li4B Li5B Li5B 33.4(6) . 10_556
Li4B Li5B Li5B 33.4(6) 3 10_556
Li6 Li5B Li5B 90.2(12) . 10_556
Ge1 Li5B Li5B 50.5(12) . 10_556
Li9 Li5B Li5B 86.6(11) . 10_556
Li9 Li5B Li5B 86.6(11) 1_455 10_556
Ge3 Li5B Li5B 105.7(11) 1_455 10_556
Ge3 Li5B Li5B 105.7(11) . 10_556
Li10 Li5B Li5B 148.7(9) 13 10_556
Li4B Li5B Li7 114.9(6) . .
Li4B Li5B Li7 114.9(6) 3 .
Li6 Li5B Li7 170(2) . .
Ge1 Li5B Li7 49.5(4) . .
Li9 Li5B Li7 58.1(5) . .
Li9 Li5B Li7 58.1(5) 1_455 .
Ge3 Li5B Li7 115.1(10) 1_455 .
Ge3 Li5B Li7 115.1(10) . .
Li10 Li5B Li7 111.3(17) 13 .
Li5B Li5B Li7 100.0(8) 10_556 .
Li5B Li6 Ge2 140.1(12) . 5_445
Li5B Li6 Li10 66.5(12) . 13
Ge2 Li6 Li10 153.46(8) 5_445 13
Li5B Li6 Ge3 61.6(4) . 1_455
Ge2 Li6 Ge3 122.57(3) 5_445 1_455
Li10 Li6 Ge3 64.06(4) 13 1_455
Li5B Li6 Ge3 61.6(4) . .
Ge2 Li6 Ge3 122.57(3) 5_445 .
Li10 Li6 Ge3 64.06(4) 13 .
Ge3 Li6 Ge3 113.65(6) 1_455 .
Li5B Li6 Li4B 43.5(10) . .
Ge2 Li6 Li4B 99.86(8) 5_445 .
Li10 Li6 Li4B 105.07(9) 13 .
Ge3 Li6 Li4B 95.79(11) 1_455 .
Ge3 Li6 Li4B 62.12(9) . .
Li5B Li6 Li4B 43.5(10) . 3
Ge2 Li6 Li4B 99.86(8) 5_445 3
Li10 Li6 Li4B 105.07(9) 13 3
Ge3 Li6 Li4B 62.12(9) 1_455 3
Ge3 Li6 Li4B 95.79(11) . 3
Li4B Li6 Li4B 39.7(2) . 3
Li5B Li6 Li1 95.8(7) . .
Ge2 Li6 Li1 62.72(5) 5_445 .
Li10 Li6 Li1 125.78(4) 13 .
Ge3 Li6 Li1 151.19(8) 1_455 .
Ge3 Li6 Li1 62.61(3) . .
Li4B Li6 Li1 56.35(11) . .
Li4B Li6 Li1 89.32(11) 3 .
Li5B Li6 Li1 95.8(7) . 1_455
Ge2 Li6 Li1 62.72(5) 5_445 1_455
Li10 Li6 Li1 125.78(4) 13 1_455
Ge3 Li6 Li1 62.61(3) 1_455 1_455
Ge3 Li6 Li1 151.19(8) . 1_455
Li4B Li6 Li1 89.32(11) . 1_455
Li4B Li6 Li1 56.35(11) 3 1_455
Li1 Li6 Li1 105.92(6) . 1_455
Li5B Li6 Li8 125.9(2) . 5_445
Ge2 Li6 Li8 69.16(5) 5_445 5_445
Li10 Li6 Li8 95.76(7) 13 5_445
Ge3 Li6 Li8 64.67(3) 1_455 5_445
Ge3 Li6 Li8 155.09(8) . 5_445
Li4B Li6 Li8 141.50(12) . 5_445
Li4B Li6 Li8 103.94(11) 3 5_445
Li1 Li6 Li8 131.61(8) . 5_445
Li1 Li6 Li8 52.49(5) 1_455 5_445
Li5B Li6 Li8 125.9(2) . 5_545
Ge2 Li6 Li8 69.16(5) 5_445 5_545
Li10 Li6 Li8 95.76(7) 13 5_545
Ge3 Li6 Li8 155.09(8) 1_455 5_545
Ge3 Li6 Li8 64.67(3) . 5_545
Li4B Li6 Li8 103.94(11) . 5_545
Li4B Li6 Li8 141.50(12) 3 5_545
Li1 Li6 Li8 52.49(5) . 5_545
Li1 Li6 Li8 131.61(8) 1_455 5_545
Li8 Li6 Li8 105.76(8) 5_445 5_545
Li5B Li6 Li5A 10.4(10) . .
Ge2 Li6 Li5A 150.50(19) 5_445 .
Li10 Li6 Li5A 56.04(18) 13 .
Ge3 Li6 Li5A 58.87(5) 1_455 .
Ge3 Li6 Li5A 58.87(5) . .
Li4B Li6 Li5A 52.81(17) . .
Li4B Li6 Li5A 52.81(17) 3 .
Li1 Li6 Li5A 101.91(12) . .
Li1 Li6 Li5A 101.91(12) 1_455 .
Li8 Li6 Li5A 123.34(7) 5_445 .
Li8 Li6 Li5A 123.34(7) 5_545 .
Ge3 Li7 Ge1 168.53(9) 13 .
Ge3 Li7 Li3 101.89(8) 13 .
Ge1 Li7 Li3 66.64(5) . .
Ge3 Li7 Li10 61.30(4) 13 1_455
Ge1 Li7 Li10 112.54(5) . 1_455
Li3 Li7 Li10 70.67(6) . 1_455
Ge3 Li7 Li10 61.30(4) 13 .
Ge1 Li7 Li10 112.54(5) . .
Li3 Li7 Li10 70.67(6) . .
Li10 Li7 Li10 98.78(8) 1_455 .
Ge3 Li7 Li9 62.11(5) 13 13
Ge1 Li7 Li9 129.36(8) . 13
Li3 Li7 Li9 164.00(9) . 13
Li10 Li7 Li9 99.42(5) 1_455 13
Li10 Li7 Li9 99.42(5) . 13
Ge3 Li7 Li9 126.49(4) 13 1_455
Ge1 Li7 Li9 58.39(4) . 1_455
Li3 Li7 Li9 99.55(6) . 1_455
Li10 Li7 Li9 81.22(4) 1_455 1_455
Li10 Li7 Li9 169.40(8) . 1_455
Li9 Li7 Li9 91.01(6) 13 1_455
Ge3 Li7 Li9 126.49(4) 13 .
Ge1 Li7 Li9 58.39(4) . .
Li3 Li7 Li9 99.55(6) . .
Li10 Li7 Li9 169.40(8) 1_455 .
Li10 Li7 Li9 81.22(4) . .
Li9 Li7 Li9 91.01(6) 13 .
Li9 Li7 Li9 96.83(8) 1_455 .
Ge3 Li7 Li5A 133.02(19) 13 .
Ge1 Li7 Li5A 58.44(18) . .
Li3 Li7 Li5A 125.08(19) . .
Li10 Li7 Li5A 130.46(4) 1_455 .
Li10 Li7 Li5A 130.46(4) . .
Li9 Li7 Li5A 70.92(18) 13 .
Li9 Li7 Li5A 51.59(6) 1_455 .
Li9 Li7 Li5A 51.59(6) . .
Ge3 Li7 Li5A 56.11(15) 13 13_455
Ge1 Li7 Li5A 128.87(16) . 13_455
Li3 Li7 Li5A 120.92(8) . 13_455
Li10 Li7 Li5A 50.39(7) 1_455 13_455
Li10 Li7 Li5A 117.41(16) . 13_455
Li9 Li7 Li5A 51.59(9) 13 13_455
Li9 Li7 Li5A 70.77(16) 1_455 13_455
Li9 Li7 Li5A 138.78(10) . 13_455
Li5A Li7 Li5A 94.7(2) . 13_455
Ge3 Li7 Li5A 56.11(15) 13 13
Ge1 Li7 Li5A 128.87(16) . 13
Li3 Li7 Li5A 120.92(8) . 13
Li10 Li7 Li5A 117.41(16) 1_455 13
Li10 Li7 Li5A 50.39(7) . 13
Li9 Li7 Li5A 51.59(9) 13 13
Li9 Li7 Li5A 138.78(10) 1_455 13
Li9 Li7 Li5A 70.77(16) . 13
Li5A Li7 Li5A 94.7(2) . 13
Li5A Li7 Li5A 92.6(3) 13_455 13
Ge3 Li7 Li2 117.71(6) 13 .
Ge1 Li7 Li2 55.79(4) . .
Li3 Li7 Li2 51.66(4) . .
Li10 Li7 Li2 121.50(8) 1_455 .
Li10 Li7 Li2 56.83(5) . .
Li9 Li7 Li2 133.73(4) 13 .
Li9 Li7 Li2 114.11(7) 1_455 .
Li9 Li7 Li2 49.80(5) . .
Li5A Li7 Li2 94.28(13) . .
Li5A Li7 Li2 170.86(13) 13_455 .
Li5A Li7 Li2 88.19(12) 13 .
Li1 Li8 Ge3 174.47(10) 5_455 13
Li1 Li8 Li10 113.81(6) 5_455 .
Ge3 Li8 Li10 63.99(5) 13 .
Li1 Li8 Li10 113.81(6) 5_455 1_455
Ge3 Li8 Li10 63.99(5) 13 1_455
Li10 Li8 Li10 112.70(8) . 1_455
Li1 Li8 Li8 118.84(12) 5_455 9_565
Ge3 Li8 Li8 66.70(7) 13 9_565
Li10 Li8 Li8 97.92(7) . 9_565
Li10 Li8 Li8 97.92(7) 1_455 9_565
Li1 Li8 Li3 72.52(7) 5_455 .
Ge3 Li8 Li3 101.94(8) 13 .
Li10 Li8 Li3 76.07(6) . .
Li10 Li8 Li3 76.07(6) 1_455 .
Li8 Li8 Li3 168.64(12) 9_565 .
Li1 Li8 Li6 63.70(6) 5_455 5
Ge3 Li8 Li6 118.72(6) 13 5
Li10 Li8 Li6 70.77(4) . 5
Li10 Li8 Li6 176.52(7) 1_455 5
Li8 Li8 Li6 81.66(7) 9_565 5
Li3 Li8 Li6 104.93(6) . 5
Li1 Li8 Li6 63.70(6) 5_455 5_455
Ge3 Li8 Li6 118.72(6) 13 5_455
Li10 Li8 Li6 176.52(7) . 5_455
Li10 Li8 Li6 70.77(4) 1_455 5_455
Li8 Li8 Li6 81.66(7) 9_565 5_455
Li3 Li8 Li6 104.93(6) . 5_455
Li6 Li8 Li6 105.76(8) 5 5_455
Li1 Li8 Ge3 62.83(7) 5_455 5_455
Ge3 Li8 Ge3 122.70(7) 13 5_455
Li10 Li8 Ge3 121.47(5) . 5_455
Li10 Li8 Ge3 121.47(5) 1_455 5_455
Li8 Li8 Ge3 56.00(7) 9_565 5_455
Li3 Li8 Ge3 135.36(8) . 5_455
Li6 Li8 Ge3 55.47(4) 5 5_455
Li6 Li8 Ge3 55.47(4) 5_455 5_455
Li1 Li8 Ge2 59.86(4) 5_455 .
Ge3 Li8 Ge2 117.05(4) 13 .
Li10 Li8 Ge2 54.53(4) . .
Li10 Li8 Ge2 129.14(8) 1_455 .
Li8 Li8 Ge2 130.65(4) 9_565 .
Li3 Li8 Ge2 53.39(3) . .
Li6 Li8 Ge2 52.30(4) 5 .
Li6 Li8 Ge2 123.31(7) 5_455 .
Ge3 Li8 Ge2 100.74(4) 5_455 .
Li1 Li8 Ge2 59.85(4) 5_455 1_455
Ge3 Li8 Ge2 117.05(4) 13 1_455
Li10 Li8 Ge2 129.14(8) . 1_455
Li10 Li8 Ge2 54.53(4) 1_455 1_455
Li8 Li8 Ge2 130.65(4) 9_565 1_455
Li3 Li8 Ge2 53.39(3) . 1_455
Li6 Li8 Ge2 123.30(7) 5 1_455
Li6 Li8 Ge2 52.30(4) 5_455 1_455
Ge3 Li8 Ge2 100.74(4) 5_455 1_455
Ge2 Li8 Ge2 93.39(5) . 1_455
Li1 Li8 Li7 125.78(9) 5_455 .
Ge3 Li8 Li7 48.69(4) 13 .
Li10 Li8 Li7 57.05(4) . .
Li10 Li8 Li7 57.05(4) 1_455 .
Li8 Li8 Li7 115.38(10) 9_565 .
Li3 Li8 Li7 53.26(6) . .
Li6 Li8 Li7 126.26(4) 5 .
Li6 Li8 Li7 126.26(4) 5_455 .
Ge3 Li8 Li7 171.39(7) 5_455 .
Ge2 Li8 Li7 85.10(5) . .
Ge2 Li8 Li7 85.11(5) 1_455 .
Li4A Li9 Li2 105.62(11) . .
Li4A Li9 Li5A 78.3(2) . 1_655
Li2 Li9 Li5A 122.06(8) . 1_655
Li4A Li9 Li5A 78.2(2) . .
Li2 Li9 Li5A 122.07(8) . .
Li5A Li9 Li5A 115.37(14) 1_655 .
Li4A Li9 Li5B 67.4(10) . .
Li2 Li9 Li5B 118.8(5) . .
Li5A Li9 Li5B 115.68(17) 1_655 .
Li5A Li9 Li5B 11.9(10) . .
Li4A Li9 Li5B 67.4(10) . 1_655
Li2 Li9 Li5B 118.8(5) . 1_655
Li5A Li9 Li5B 11.9(10) 1_655 1_655
Li5A Li9 Li5B 115.68(17) . 1_655
Li5B Li9 Li5B 113.3(6) . 1_655
Li4A Li9 Ge1 78.86(6) . .
Li2 Li9 Ge1 61.74(3) . .
Li5A Li9 Ge1 156.9(2) 1_655 .
Li5A Li9 Ge1 62.69(11) . .
Li5B Li9 Ge1 57.2(6) . .
Li5B Li9 Ge1 145.2(12) 1_655 .
Li4A Li9 Ge1 78.86(6) . 1_655
Li2 Li9 Ge1 61.74(3) . 1_655
Li5A Li9 Ge1 62.69(11) 1_655 1_655
Li5A Li9 Ge1 156.9(2) . 1_655
Li5B Li9 Ge1 145.2(12) . 1_655
Li5B Li9 Ge1 57.2(6) 1_655 1_655
Ge1 Li9 Ge1 109.27(6) . 1_655
Li4A Li9 Li4B 27.47(10) . 3_655
Li2 Li9 Li4B 106.36(8) . 3_655
Li5A Li9 Li4B 53.8(2) 1_655 3_655
Li5A Li9 Li4B 100.7(2) . 3_655
Li5B Li9 Li4B 91.4(9) . 3_655
Li5B Li9 Li4B 42.1(11) 1_655 3_655
Ge1 Li9 Li4B 103.13(10) . 3_655
Ge1 Li9 Li4B 58.56(9) 1_655 3_655
Li4A Li9 Li4B 27.47(10) . .
Li2 Li9 Li4B 106.36(8) . .
Li5A Li9 Li4B 100.7(2) 1_655 .
Li5A Li9 Li4B 53.8(2) . .
Li5B Li9 Li4B 42.1(11) . .
Li5B Li9 Li4B 91.4(9) 1_655 .
Ge1 Li9 Li4B 58.56(9) . .
Ge1 Li9 Li4B 103.13(10) 1_655 .
Li4B Li9 Li4B 54.7(2) 3_655 .
Li4A Li9 Ge3 57.26(9) . .
Li2 Li9 Ge3 162.88(9) . .
Li5A Li9 Ge3 58.27(9) 1_655 .
Li5A Li9 Ge3 58.27(9) . .
Li5B Li9 Ge3 57.4(2) . .
Li5B Li9 Ge3 57.4(2) 1_655 .
Ge1 Li9 Ge3 110.76(4) . .
Ge1 Li9 Ge3 110.76(4) 1_655 .
Li4B Li9 Ge3 58.86(7) 3_655 .
Li4B Li9 Ge3 58.86(7) . .
Li4A Li9 Li7 108.94(11) . 13
Li2 Li9 Li7 145.43(9) . 13
Li5A Li9 Li7 66.33(17) 1_655 13
Li5A Li9 Li7 66.33(17) . 13
Li5B Li9 Li7 75.7(10) . 13
Li5B Li9 Li7 75.7(10) 1_655 13
Ge1 Li9 Li7 125.36(3) . 13
Ge1 Li9 Li7 125.36(3) 1_655 13
Li4B Li9 Li7 104.25(8) 3_655 13
Li4B Li9 Li7 104.25(8) . 13
Ge3 Li9 Li7 51.68(5) . 13
Li5A Li10 Li6 65.1(2) 13 13
Li5A Li10 Ge2 162.7(2) 13 .
Li6 Li10 Ge2 132.17(8) 13 .
Li5A Li10 Li8 117.01(9) 13 1_655
Li6 Li10 Li8 84.45(6) 13 1_655
Ge2 Li10 Li8 70.16(5) . 1_655
Li5A Li10 Li8 117.01(9) 13 .
Li6 Li10 Li8 84.45(6) 13 .
Ge2 Li10 Li8 70.16(5) . .
Li8 Li10 Li8 112.70(8) 1_655 .
Li5A Li10 Ge3 59.77(9) 13 13
Li6 Li10 Ge3 58.24(3) 13 13
Ge2 Li10 Ge3 125.71(3) . 13
Li8 Li10 Ge3 141.03(8) 1_655 13
Li8 Li10 Ge3 57.31(4) . 13
Li5A Li10 Ge3 59.77(9) 13 13_655
Li6 Li10 Ge3 58.24(3) 13 13_655
Ge2 Li10 Ge3 125.71(3) . 13_655
Li8 Li10 Ge3 57.31(4) 1_655 13_655
Li8 Li10 Ge3 141.03(8) . 13_655
Ge3 Li10 Ge3 104.63(5) 13 13_655
Li5A Li10 Li5B 10.1(7) 13 13
Li6 Li10 Li5B 55.0(9) 13 13
Ge2 Li10 Li5B 172.8(9) . 13
Li8 Li10 Li5B 113.1(4) 1_655 13
Li8 Li10 Li5B 113.1(4) . 13
Ge3 Li10 Li5B 56.2(3) 13 13
Ge3 Li10 Li5B 56.2(3) 13_655 13
Li5A Li10 Li2 104.9(2) 13 .
Li6 Li10 Li2 170.03(9) 13 .
Ge2 Li10 Li2 57.80(5) . .
Li8 Li10 Li2 100.94(6) 1_655 .
Li8 Li10 Li2 100.94(6) . .
Ge3 Li10 Li2 117.69(4) 13 .
Ge3 Li10 Li2 117.69(4) 13_655 .
Li5B Li10 Li2 115.0(9) 13 .
Li5A Li10 Li7 67.76(14) 13 .
Li6 Li10 Li7 108.73(5) 13 .
Ge2 Li10 Li7 101.78(5) . .
Li8 Li10 Li7 166.39(8) 1_655 .
Li8 Li10 Li7 73.03(5) . .
Ge3 Li10 Li7 52.57(3) 13 .
Ge3 Li10 Li7 126.43(7) 13_655 .
Li5B Li10 Li7 73.7(5) 13 .
Li2 Li10 Li7 65.53(5) . .
Li5A Li10 Li7 67.76(14) 13 1_655
Li6 Li10 Li7 108.73(5) 13 1_655
Ge2 Li10 Li7 101.78(5) . 1_655
Li8 Li10 Li7 73.03(5) 1_655 1_655
Li8 Li10 Li7 166.39(8) . 1_655
Ge3 Li10 Li7 126.43(7) 13 1_655
Ge3 Li10 Li7 52.57(3) 13_655 1_655
Li5B Li10 Li7 73.7(5) 13 1_655
Li2 Li10 Li7 65.53(5) . 1_655
Li7 Li10 Li7 98.77(8) . 1_655
Li5A Li10 Li6 145.3(2) 13 5
Li6 Li10 Li6 80.20(7) 13 5
Ge2 Li10 Li6 51.97(5) . 5
Li8 Li10 Li6 56.35(4) 1_655 5
Li8 Li10 Li6 56.35(4) . 5
Ge3 Li10 Li6 102.51(5) 13 5
Ge3 Li10 Li6 102.51(5) 13_655 5
Li5B Li10 Li6 135.2(9) 13 5
Li2 Li10 Li6 109.77(7) . 5
Li7 Li10 Li6 127.78(4) . 5
Li7 Li10 Li6 127.78(4) 1_655 5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ge1 Li7 2.6309(16) 10_556
Ge1 Li7 2.6309(16) .
Ge1 Li5B 2.64(2) .
Ge1 Li5B 2.64(2) 10_556
Ge1 Li4B 2.772(4) 3
Ge1 Li4B 2.772(4) .
Ge1 Li9 2.7904(10) 1_455
Ge1 Li9 2.7904(11) 10_556
Ge1 Li9 2.7904(10) 10_456
Ge1 Li9 2.7904(11) .
Ge1 Li2 2.7924(13) .
Ge1 Li2 2.7924(13) 1_455
Ge2 Li6 2.6473(16) 14_556
Ge2 Li6 2.6473(16) 5
Ge2 Li3 2.6567(12) .
Ge2 Li3 2.6567(12) 1_655
Ge2 Li10 2.7072(17) .
Ge2 Li10 2.7072(17) 10_556
Ge2 Li2 2.753(2) .
Ge2 Li1 2.8668(15) 5
Ge2 Li1 2.8668(15) 5_455
Ge2 Li8 3.1269(13) .
Ge2 Li8 3.1269(13) 10_656
Ge2 Li8 3.1269(13) 1_655
Ge3 Li4A 2.5962(18) .
Ge3 Li7 2.6031(17) 13
Ge3 Li8 2.6925(18) 13
Ge3 Li6 2.7188(9) .
Ge3 Li6 2.7188(9) 1_655
Ge3 Li5B 2.723(8) 1_655
Ge3 Li5B 2.723(8) .
Ge3 Li5A 2.747(3) .
Ge3 Li5A 2.747(3) 1_655
Ge3 Li4B 2.854(3) .
Ge3 Li4B 2.854(3) 3_655
Ge3 Li10 2.8753(10) 13
Li1 Li8 2.522(2) 5_545
Li1 Li8 2.522(2) 14_546
Li1 Li4A 2.526(6) .
Li1 Li4B 2.674(5) .
Li1 Li4B 2.674(5) 3_655
Li1 Li6 2.8507(11) 10_656
Li1 Li6 2.8507(11) 1_655
Li1 Li6 2.8507(11) 10_556
Li1 Li6 2.8507(11) .
Li1 Ge2 2.8667(15) 5_445
Li1 Ge2 2.8667(15) 5_545
Li1 Ge3 2.8962(13) 10_556
Li2 Li9 2.646(3) 10_556
Li2 Li9 2.646(3) .
Li2 Li3 2.6624(18) 1_655
Li2 Li3 2.6625(18) .
Li2 Ge1 2.7924(13) 1_655
Li2 Li10 2.970(2) 10_556
Li2 Li10 2.970(2) .
Li2 Li7 3.2296(13) 10_656
Li2 Li7 3.2296(13) 1_655
Li2 Li7 3.2296(12) 10_556
Li3 Ge2 2.6567(12) 1_455
Li3 Li2 2.6625(18) 1_455
Li3 Li8 2.735(3) 10_556
Li3 Li8 2.736(3) .
Li3 Li7 2.824(2) 10_556
Li3 Li7 2.824(2) .
Li3 Li1 3.115(3) 5_455
Li3 Li10 3.3697(12) 10_556
Li3 Li10 3.3697(12) 1_455
Li4A Li9 2.396(5) .
Li4A Li9 2.396(5) 10_556
Li4A Ge3 2.5962(18) 10_556
Li4A Li5A 3.219(7) .
Li4A Li5A 3.219(7) 10_656
Li4A Li5A 3.219(7) 1_655
Li4A Li5A 3.219(7) 10_556
Li5A Li10 2.619(5) 13
Li5A Li9 2.693(2) .
Li5A Li9 2.693(2) 1_455
Li5A Ge3 2.747(3) 1_455
Li5A Li6 2.865(7) .
Li5A Li7 3.142(6) .
Li5A Li7 3.147(7) 13_455
Li5A Li7 3.147(7) 13
Li5A Li4A 3.219(7) 1_455
Li4B Li4B 1.910(11) 3
Li4B Li5B 2.02(5) 10_556
Li4B Li5B 2.02(5) .
Li4B Li4B 2.641(11) 3_655
Li4B Li6 2.812(4) .
Li4B Li6 2.812(4) 10_556
Li4B Ge3 2.854(3) 10_556
Li4B Li9 2.876(5) .
Li4B Li9 2.876(5) 10_556
Li5B Li4B 2.02(5) 3
Li5B Li6 2.60(2) .
Li5B Li9 2.724(9) .
Li5B Li9 2.724(9) 1_455
Li5B Ge3 2.723(8) 1_455
Li5B Li10 2.91(4) 13
Li5B Li5B 3.36(11) 10_556
Li5B Li7 3.41(3) .
Li6 Ge2 2.6474(16) 5_445
Li6 Li10 2.703(2) 13
Li6 Ge3 2.7188(9) 1_455
Li6 Li4B 2.812(4) 3
Li6 Li1 2.8508(11) 1_455
Li6 Li8 2.8538(15) 5_445
Li6 Li8 2.8538(15) 5_545
Li7 Ge3 2.6032(17) 13
Li7 Li10 2.9976(18) 1_455
Li7 Li10 2.9976(18) .
Li7 Li9 3.036(3) 13
Li7 Li9 3.0423(18) 1_455
Li7 Li9 3.0423(18) .
Li7 Li5A 3.147(7) 13_455
Li7 Li5A 3.147(7) 13
Li8 Li1 2.522(2) 5_455
Li8 Ge3 2.6924(18) 13
Li8 Li10 2.7336(13) .
Li8 Li10 2.7336(13) 1_455
Li8 Li8 2.733(4) 9_565
Li8 Li6 2.8537(15) 5
Li8 Li6 2.8537(15) 5_455
Li8 Ge3 2.9827(19) 5_455
Li8 Ge2 3.1269(13) 1_455
Li9 Li5A 2.693(2) 1_655
Li9 Li5B 2.724(9) 1_655
Li9 Ge1 2.7904(10) 1_655
Li9 Li4B 2.876(5) 3_655
Li9 Li7 3.036(3) 13
Li10 Li5A 2.619(5) 13
Li10 Li6 2.703(2) 13
Li10 Li8 2.7336(13) 1_655
Li10 Ge3 2.8753(10) 13
Li10 Ge3 2.8753(10) 13_655
Li10 Li5B 2.91(4) 13
Li10 Li7 2.9976(18) 1_655
Li10 Li6 3.237(2) 5
