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#$Date: 2016-03-25 22:48:39 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180016 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/10/7031088.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7031088
loop_
_publ_author_name
'Zhao, Xiao-Li'
'Mak, Thomas C. W.'
_publ_section_title
;
 Silver cages with encapsulated acetylenediide as building blocks for
 hydrothermal synthesis of supramolecular complexes with n-cyanopyridine
 and pyridine-n-carboxamide (n=3, 4).
;
_journal_issue                   20
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3212
_journal_page_last               3217
_journal_paper_doi               10.1039/B406711H
_journal_year                    2004
_chemical_formula_sum            'C30 H20 Ag10 F24 N4 O22'
_chemical_formula_weight         2323.20
_chemical_name_systematic
;
?
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 100.7030(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   15.7063(8)
_cell_length_b                   8.5582(4)
_cell_length_c                   20.3643(10)
_cell_measurement_temperature    293(2)
_cell_volume                     2689.7(2)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0447
_diffrn_reflns_av_sigmaI/netI    0.0371
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            14568
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.51
_exptl_absorpt_coefficient_mu    3.717
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.632085
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.869
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2180
_exptl_crystal_size_max          0.46
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.24
_refine_diff_density_max         1.778
_refine_diff_density_min         -1.060
_refine_diff_density_rms         0.194
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.209
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     407
_refine_ls_number_reflns         4741
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.209
_refine_ls_R_factor_all          0.0700
_refine_ls_R_factor_gt           0.0567
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0444P)²+29.2181P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1244
_refine_ls_wR_factor_ref         0.1314
_reflns_number_gt                3867
_reflns_number_total             4741
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b406711h.txt
_cod_data_source_block           compound_1
_cod_original_sg_symbol_H-M      P2/n
_cod_database_code               7031088
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.15850(5) 0.56897(9) 0.73462(4) 0.0356(2) Uani 1 1 d .
Ag2 Ag 0.12757(5) 0.89475(9) 0.66045(4) 0.0350(2) Uani 1 1 d .
Ag3 Ag 0.17064(5) 1.11429(9) 0.77494(4) 0.0339(2) Uani 1 1 d .
Ag4 Ag 0.31498(6) 0.79161(10) 0.65425(4) 0.0387(2) Uani 1 1 d .
Ag5 Ag 0.40986(6) 0.52680(12) 0.42185(5) 0.0514(3) Uani 1 1 d .
C1 C 0.2500 0.7711(15) 0.7500 0.026(3) Uani 1 2 d S
C2 C 0.2500 0.9162(16) 0.7500 0.027(3) Uani 1 2 d S
O1 O 0.1699(5) 1.5509(8) 0.8982(3) 0.0365(17) Uani 1 1 d .
O2 O 0.2007(5) 1.3681(8) 0.8284(3) 0.0393(18) Uani 1 1 d .
C3 C 0.1878(6) 1.4187(11) 0.8828(4) 0.024(2) Uani 1 1 d .
C4 C 0.1963(8) 1.2980(12) 0.9405(5) 0.040(3) Uani 1 1 d .
F11 F 0.2542(7) 1.3450(11) 0.9921(4) 0.099(3) Uani 1 1 d .
F12 F 0.1229(6) 1.2865(11) 0.9619(5) 0.089(3) Uani 1 1 d .
F13 F 0.2188(6) 1.1586(8) 0.9250(4) 0.067(2) Uani 1 1 d .
O3 O 0.0409(5) 1.0937(9) 0.8166(4) 0.050(2) Uani 1 1 d .
O4 O 0.0698(5) 0.8851(9) 0.8841(4) 0.0428(19) Uani 1 1 d .
C5 C 0.0260(7) 0.9951(12) 0.8586(5) 0.035(2) Uani 1 1 d .
C6 C -0.0617(8) 1.0181(15) 0.8815(7) 0.053(3) Uani 1 1 d .
F21 F -0.0504(7) 1.1070(15) 0.9357(5) 0.109(4) Uani 1 1 d .
F22 F -0.1219(5) 1.0845(10) 0.8386(5) 0.077(2) Uani 1 1 d .
F23 F -0.0926(6) 0.8855(12) 0.8992(7) 0.127(5) Uani 1 1 d .
O5 O 0.0119(5) 0.6485(9) 0.7338(4) 0.0456(19) Uani 1 1 d .
O6 O -0.0146(4) 0.8261(9) 0.6521(4) 0.0411(18) Uani 1 1 d .
C7 C -0.0332(7) 0.7367(12) 0.6950(6) 0.036(2) Uani 1 1 d .
C8 C -0.1306(8) 0.7361(14) 0.6986(8) 0.055(3) Uani 1 1 d .
F31 F -0.1790(6) 0.715(2) 0.6424(6) 0.152(6) Uani 1 1 d .
F32 F -0.1534(6) 0.6343(12) 0.7386(6) 0.112(4) Uani 1 1 d .
F33 F -0.1538(7) 0.8708(12) 0.7197(8) 0.133(5) Uani 1 1 d .
O7 O 0.1075(5) 1.3204(8) 0.6960(3) 0.0380(17) Uani 1 1 d .
O8 O 0.0770(5) 1.1391(8) 0.6162(3) 0.0389(18) Uani 1 1 d .
C9 C 0.0824(6) 1.2723(11) 0.6385(4) 0.027(2) Uani 1 1 d .
C10 C 0.0491(8) 1.4003(12) 0.5861(5) 0.042(3) Uani 1 1 d .
F41 F 0.0328(7) 1.3476(9) 0.5251(3) 0.085(3) Uani 1 1 d .
F42 F -0.0254(5) 1.4631(10) 0.5965(4) 0.075(2) Uani 1 1 d .
F43 F 0.1036(5) 1.5182(8) 0.5894(4) 0.071(2) Uani 1 1 d .
N1 N 0.2850(6) 0.6453(10) 0.4057(4) 0.035(2) Uani 1 1 d .
N2 N 0.1014(5) 1.0169(10) 0.4868(4) 0.033(2) Uani 1 1 d .
H2A H 0.0830 1.0633 0.5189 0.039 Uiso 1 1 calc R
H2B H 0.0852 1.0488 0.4463 0.039 Uiso 1 1 calc R
O9 O 0.1800(4) 0.8458(8) 0.5570(3) 0.0331(16) Uani 1 1 d .
C11 C 0.1540(6) 0.8980(11) 0.4994(5) 0.026(2) Uani 1 1 d .
C12 C 0.1827(6) 0.8192(11) 0.4415(4) 0.026(2) Uani 1 1 d .
C13 C 0.2525(7) 0.7211(12) 0.4533(5) 0.034(2) Uani 1 1 d .
H13A H 0.2795 0.7058 0.4974 0.041 Uiso 1 1 calc R
C14 C 0.2430(7) 0.6652(13) 0.3429(5) 0.038(3) Uani 1 1 d .
H14A H 0.2624 0.6114 0.3088 0.045 Uiso 1 1 calc R
C15 C 0.1738(7) 0.7599(14) 0.3270(5) 0.042(3) Uani 1 1 d .
H15A H 0.1472 0.7716 0.2825 0.050 Uiso 1 1 calc R
C16 C 0.1423(7) 0.8391(12) 0.3756(5) 0.037(2) Uani 1 1 d .
H16A H 0.0947 0.9050 0.3647 0.044 Uiso 1 1 calc R
O1W O 0.5278(5) 0.3763(9) 0.4538(4) 0.0430(18) Uani 1 1 d .
H1WA H 0.5645 0.3903 0.4285 0.064 Uiso 1 1 d R
H1WB H 0.5141 0.2801 0.4533 0.064 Uiso 1 1 d R
O2W O 0.4713(6) 0.5935(10) 0.3207(4) 0.060(2) Uani 1 1 d .
H2WA H 0.4916 0.6853 0.3194 0.091 Uiso 1 1 d R
H2WB H 0.4833 0.5220 0.2949 0.091 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Ag1 O7 156.4(2) . 1_545
C1 Ag1 O5 111.9(3) . .
O7 Ag1 O5 89.3(3) 1_545 .
C1 Ag1 O2 110.1(2) . 1_545
O7 Ag1 O2 70.6(2) 1_545 1_545
O5 Ag1 O2 108.1(2) . 1_545
C1 Ag1 Ag1 50.8(2) . 2_556
O7 Ag1 Ag1 110.05(18) 1_545 2_556
O5 Ag1 Ag1 159.6(2) . 2_556
O2 Ag1 Ag1 73.94(18) 1_545 2_556
C1 Ag1 Ag4 52.57(8) . 2_556
O7 Ag1 Ag4 146.75(17) 1_545 2_556
O5 Ag1 Ag4 79.6(2) . 2_556
O2 Ag1 Ag4 83.14(15) 1_545 2_556
Ag1 Ag1 Ag4 80.55(3) 2_556 2_556
C1 Ag1 Ag2 54.72(17) . .
O7 Ag1 Ag2 128.55(17) 1_545 .
O5 Ag1 Ag2 71.61(19) . .
O2 Ag1 Ag2 160.35(15) 1_545 .
Ag1 Ag1 Ag2 99.52(3) 2_556 .
Ag4 Ag1 Ag2 77.46(3) 2_556 .
O6 Ag2 O8 86.8(3) . .
O6 Ag2 C2 135.3(2) . .
O8 Ag2 C2 112.9(4) . .
O6 Ag2 O9 112.0(3) . .
O8 Ag2 O9 88.1(2) . .
C2 Ag2 O9 108.59(17) . .
O6 Ag2 C1 122.0(2) . .
O8 Ag2 C1 141.1(3) . .
C2 Ag2 C1 28.3(4) . .
O9 Ag2 C1 102.17(18) . .
O6 Ag2 Ag3 107.3(2) . .
O8 Ag2 Ag3 75.54(16) . .
C2 Ag2 Ag3 47.3(3) . .
O9 Ag2 Ag3 136.27(18) . .
C1 Ag2 Ag3 71.2(2) . .
O6 Ag2 Ag4 147.84(19) . .
O8 Ag2 Ag4 119.5(2) . .
C2 Ag2 Ag4 54.50(13) . .
O9 Ag2 Ag4 55.92(16) . .
C1 Ag2 Ag4 48.09(2) . .
Ag3 Ag2 Ag4 97.61(3) . .
O6 Ag2 Ag1 82.54(18) . .
O8 Ag2 Ag1 167.24(19) . .
C2 Ag2 Ag1 71.0(3) . .
O9 Ag2 Ag1 102.41(16) . .
C1 Ag2 Ag1 44.2(2) . .
Ag3 Ag2 Ag1 100.95(3) . .
Ag4 Ag2 Ag1 72.88(3) . .
C2 Ag3 O3 125.9(3) . .
C2 Ag3 O2 135.5(3) . .
O3 Ag3 O2 90.8(3) . .
C2 Ag3 O7 124.9(2) . .
O3 Ag3 O7 91.0(3) . .
O2 Ag3 O7 71.0(2) . .
C2 Ag3 Ag3 49.8(2) . 2_556
O3 Ag3 Ag3 175.69(19) . 2_556
O2 Ag3 Ag3 92.83(18) . 2_556
O7 Ag3 Ag3 92.30(18) . 2_556
C2 Ag3 Ag2 52.64(8) . .
O3 Ag3 Ag2 98.6(2) . .
O2 Ag3 Ag2 155.64(16) . .
O7 Ag3 Ag2 86.28(16) . .
Ag3 Ag3 Ag2 78.93(3) 2_556 .
C2 Ag3 Ag4 55.3(2) . 2_556
O3 Ag3 Ag4 76.06(18) . 2_556
O2 Ag3 Ag4 126.46(16) . 2_556
O7 Ag3 Ag4 157.58(17) . 2_556
Ag3 Ag3 Ag4 99.90(3) 2_556 2_556
Ag2 Ag3 Ag4 77.79(3) . 2_556
O4 Ag4 O1 89.9(3) 2_556 2_546
O4 Ag4 C1 144.1(3) 2_556 .
O1 Ag4 C1 113.8(3) 2_546 .
O4 Ag4 C2 124.7(3) 2_556 .
O1 Ag4 C2 142.1(3) 2_546 .
C1 Ag4 C2 28.5(4) . .
O4 Ag4 Ag1 119.5(2) 2_556 2_556
O1 Ag4 Ag1 76.67(17) 2_546 2_556
C1 Ag4 Ag1 48.5(2) . 2_556
C2 Ag4 Ag1 72.9(2) . 2_556
O4 Ag4 Ag2 138.2(2) 2_556 .
O1 Ag4 Ag2 116.40(19) 2_546 .
C1 Ag4 Ag2 55.24(12) . .
C2 Ag4 Ag2 48.88(2) . .
Ag1 Ag4 Ag2 98.84(3) 2_556 .
O4 Ag4 Ag3 81.41(19) 2_556 2_556
O1 Ag4 Ag3 170.10(18) 2_546 2_556
C1 Ag4 Ag3 71.9(3) . 2_556
C2 Ag4 Ag3 44.7(3) . 2_556
Ag1 Ag4 Ag3 103.42(3) 2_556 2_556
Ag2 Ag4 Ag3 73.46(3) . 2_556
N1 Ag5 O1W 168.4(3) . .
N1 Ag5 O2W 104.1(3) . .
O1W Ag5 O2W 86.9(3) . .
C2 C1 Ag1 140.8(2) . .
C2 C1 Ag1 140.8(2) . 2_556
Ag1 C1 Ag1 78.5(4) . 2_556
C2 C1 Ag4 85.7(3) . 2_556
Ag1 C1 Ag4 78.96(17) . 2_556
Ag1 C1 Ag4 107.8(3) 2_556 2_556
C2 C1 Ag4 85.7(3) . .
Ag1 C1 Ag4 107.8(3) . .
Ag1 C1 Ag4 78.96(17) 2_556 .
Ag4 C1 Ag4 171.5(6) 2_556 .
C2 C1 Ag2 66.1(3) . 2_556
Ag1 C1 Ag2 141.4(3) . 2_556
Ag1 C1 Ag2 81.08(7) 2_556 2_556
Ag4 C1 Ag2 76.67(12) 2_556 2_556
Ag4 C1 Ag2 99.82(17) . 2_556
C2 C1 Ag2 66.1(3) . .
Ag1 C1 Ag2 81.08(7) . .
Ag1 C1 Ag2 141.4(3) 2_556 .
Ag4 C1 Ag2 99.82(17) 2_556 .
Ag4 C1 Ag2 76.67(12) . .
Ag2 C1 Ag2 132.3(5) 2_556 .
C1 C2 Ag3 139.8(2) . 2_556
C1 C2 Ag3 139.8(2) . .
Ag3 C2 Ag3 80.3(5) 2_556 .
C1 C2 Ag2 85.6(3) . .
Ag3 C2 Ag2 106.8(3) 2_556 .
Ag3 C2 Ag2 80.06(18) . .
C1 C2 Ag2 85.6(3) . 2_556
Ag3 C2 Ag2 80.06(18) 2_556 2_556
Ag3 C2 Ag2 106.8(3) . 2_556
Ag2 C2 Ag2 171.2(6) . 2_556
C1 C2 Ag4 65.7(3) . .
Ag3 C2 Ag4 79.96(7) 2_556 .
Ag3 C2 Ag4 143.4(3) . .
Ag2 C2 Ag4 76.62(13) . .
Ag2 C2 Ag4 99.69(18) 2_556 .
C1 C2 Ag4 65.7(3) . 2_556
Ag3 C2 Ag4 143.4(3) 2_556 2_556
Ag3 C2 Ag4 79.96(7) . 2_556
Ag2 C2 Ag4 99.69(18) . 2_556
Ag2 C2 Ag4 76.62(13) 2_556 2_556
Ag4 C2 Ag4 131.4(5) . 2_556
C3 O1 Ag4 130.4(6) . 2_566
C3 O2 Ag3 131.3(6) . .
C3 O2 Ag1 111.6(6) . 1_565
Ag3 O2 Ag1 105.3(2) . 1_565
O1 C3 O2 129.5(9) . .
O1 C3 C4 114.5(8) . .
O2 C3 C4 116.0(8) . .
F13 C4 F12 107.9(10) . .
F13 C4 F11 107.2(10) . .
F12 C4 F11 106.1(10) . .
F13 C4 C3 114.6(9) . .
F12 C4 C3 110.2(9) . .
F11 C4 C3 110.4(9) . .
C5 O3 Ag3 125.5(7) . .
C5 O4 Ag4 123.6(7) . 2_556
O4 C5 O3 130.1(10) . .
O4 C5 C6 115.7(9) . .
O3 C5 C6 114.2(9) . .
F22 C6 F23 107.7(12) . .
F22 C6 F21 106.2(11) . .
F23 C6 F21 105.5(12) . .
F22 C6 C5 115.6(10) . .
F23 C6 C5 111.6(10) . .
F21 C6 C5 109.6(11) . .
C7 O5 Ag1 128.4(7) . .
C7 O6 Ag2 117.6(7) . .
O5 C7 O6 130.9(10) . .
O5 C7 C8 115.4(10) . .
O6 C7 C8 113.7(10) . .
F31 C8 F32 106.5(13) . .
F31 C8 F33 105.4(14) . .
F32 C8 F33 105.2(13) . .
F31 C8 C7 113.1(12) . .
F32 C8 C7 115.2(11) . .
F33 C8 C7 110.7(10) . .
C9 O7 Ag1 130.3(6) . 1_565
C9 O7 Ag3 113.5(6) . .
Ag1 O7 Ag3 110.9(3) 1_565 .
C9 O8 Ag2 133.6(6) . .
O8 C9 O7 130.5(9) . .
O8 C9 C10 114.4(8) . .
O7 C9 C10 115.1(8) . .
F41 C10 F43 108.9(10) . .
F41 C10 F42 105.5(10) . .
F43 C10 F42 105.3(9) . .
F41 C10 C9 113.1(8) . .
F43 C10 C9 112.0(9) . .
F42 C10 C9 111.6(9) . .
C14 N1 C13 116.3(9) . .
C14 N1 Ag5 118.3(7) . .
C13 N1 Ag5 124.6(7) . .
C11 O9 Ag2 130.2(6) . .
O9 C11 N2 123.2(9) . .
O9 C11 C12 118.9(8) . .
N2 C11 C12 117.9(8) . .
C13 C12 C16 117.0(9) . .
C13 C12 C11 119.2(8) . .
C16 C12 C11 123.8(9) . .
N1 C13 C12 124.8(9) . .
N1 C14 C15 122.6(9) . .
C14 C15 C16 120.6(9) . .
C15 C16 C12 118.6(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C1 2.234(10) .
Ag1 O7 2.357(7) 1_545
Ag1 O5 2.398(7) .
Ag1 O2 2.563(7) 1_545
Ag1 Ag1 2.8258(16) 2_556
Ag1 Ag4 2.9284(11) 2_556
Ag1 Ag2 3.1652(11) .
Ag2 O6 2.284(7) .
Ag2 O8 2.356(7) .
Ag2 C2 2.3989(14) .
Ag2 O9 2.437(6) .
Ag2 C1 2.616(5) .
Ag2 Ag3 2.9728(11) .
Ag2 Ag4 3.0980(12) .
Ag3 C2 2.218(10) .
Ag3 O3 2.355(7) .
Ag3 O2 2.436(7) .
Ag3 O7 2.468(7) .
Ag3 Ag3 2.8611(15) 2_556
Ag3 Ag4 3.1042(11) 2_556
Ag4 O4 2.247(7) 2_556
Ag4 O1 2.353(7) 2_546
Ag4 C1 2.3694(12) .
Ag4 C2 2.592(6) .
Ag4 Ag1 2.9284(11) 2_556
Ag4 Ag3 3.1042(11) 2_556
Ag5 N1 2.178(8) .
Ag5 O1W 2.251(8) .
Ag5 O2W 2.498(8) .
C1 C2 1.242(19) .
C1 Ag1 2.234(10) 2_556
C1 Ag4 2.3694(12) 2_556
C1 Ag2 2.616(5) 2_556
C2 Ag3 2.218(10) 2_556
C2 Ag2 2.3989(13) 2_556
C2 Ag4 2.592(6) 2_556
O1 C3 1.220(11) .
O1 Ag4 2.353(7) 2_566
O2 C3 1.241(11) .
O2 Ag1 2.563(7) 1_565
C3 C4 1.551(14) .
C4 F13 1.300(12) .
C4 F12 1.309(14) .
C4 F11 1.319(13) .
O3 C5 1.255(12) .
O4 C5 1.223(12) .
O4 Ag4 2.247(7) 2_556
C5 C6 1.545(15) .
C6 F22 1.294(15) .
C6 F23 1.311(15) .
C6 F21 1.325(17) .
O5 C7 1.220(12) .
O6 C7 1.237(13) .
C7 C8 1.545(16) .
C8 F31 1.266(17) .
C8 F32 1.288(15) .
C8 F33 1.305(16) .
O7 C9 1.234(11) .
O7 Ag1 2.357(7) 1_565
O8 C9 1.224(11) .
C9 C10 1.550(14) .
C10 F41 1.303(12) .
C10 F43 1.317(13) .
C10 F42 1.340(14) .
N1 C14 1.337(13) .
N1 C13 1.343(12) .
N2 C11 1.306(12) .
O9 C11 1.250(11) .
C11 C12 1.498(13) .
C12 C13 1.366(14) .
C12 C16 1.385(13) .
C14 C15 1.347(15) .
C15 C16 1.368(15) .
