#------------------------------------------------------------------------------
#$Date: 2016-03-25 22:48:39 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180016 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/10/7031090.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7031090
loop_
_publ_author_name
'Zhao, Xiao-Li'
'Mak, Thomas C. W.'
_publ_section_title
;
 Silver cages with encapsulated acetylenediide as building blocks for
 hydrothermal synthesis of supramolecular complexes with n-cyanopyridine
 and pyridine-n-carboxamide (n=3, 4).
;
_journal_issue                   20
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3212
_journal_page_last               3217
_journal_paper_doi               10.1039/B406711H
_journal_year                    2004
_chemical_formula_sum            'C114 H70 Ag24 F54 N24 O48'
_chemical_formula_weight         6158.82
_chemical_name_systematic
;
?
;
_space_group_IT_number           9
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 94.2860(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.3822(11)
_cell_length_b                   55.376(3)
_cell_length_c                   15.8726(10)
_cell_measurement_temperature    123(2)
_cell_volume                     16112.1(16)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0265
_diffrn_reflns_av_sigmaI/netI    0.0430
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       65
_diffrn_reflns_limit_k_min       -64
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            57985
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         0.74
_exptl_absorpt_coefficient_mu    2.989
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.764866
_exptl_absorpt_correction_type   sadabs
_exptl_crystal_colour            block
_exptl_crystal_density_diffrn    2.539
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       colorless
_exptl_crystal_F_000             11680
_exptl_crystal_size_max          0.41
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.24
_refine_diff_density_max         1.657
_refine_diff_density_min         -1.006
_refine_diff_density_rms         0.133
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.010(14)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.048
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2377
_refine_ls_number_reflns         27674
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.0354
_refine_ls_R_factor_gt           0.0327
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0293P)²+17.9247P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0731
_refine_ls_wR_factor_ref         0.0752
_reflns_number_gt                26023
_reflns_number_total             27674
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b406711h.txt
_cod_data_source_block           z
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/automatic-downloads/retrospective/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_cell_volume        16112.1(17)
_cod_original_sg_symbol_H-M      Cc
_cod_database_code               7031090
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.82635(3) 0.107194(9) 0.97968(3) 0.01961(11) Uani 1 1 d .
Ag2 Ag -0.82383(3) 0.439223(9) -0.01603(3) 0.01999(11) Uani 1 1 d .
Ag3 Ag -0.82148(3) 0.227570(9) 0.47400(3) 0.02044(12) Uani 1 1 d .
Ag4 Ag -0.85424(3) 0.401150(9) 0.22755(3) 0.01991(11) Uani 1 1 d .
Ag5 Ag -0.71769(3) 0.288609(9) 0.65948(3) 0.02279(12) Uani 1 1 d .
Ag6 Ag -0.85375(3) 0.265061(9) 0.72052(3) 0.02062(12) Uani 1 1 d .
Ag7 Ag -0.69834(3) 0.096729(9) 1.22688(3) 0.01986(12) Uani 1 1 d .
Ag8 Ag -0.71881(3) 0.378249(9) 0.16229(3) 0.02190(12) Uani 1 1 d .
Ag9 Ag -0.70343(3) 0.433069(9) 0.21445(3) 0.02084(11) Uani 1 1 d .
Ag10 Ag -0.87517(3) 0.448229(9) 0.16358(3) 0.02332(12) Uani 1 1 d .
Ag11 Ag -0.70340(3) 0.234945(9) 0.70807(3) 0.02045(12) Uani 1 1 d .
Ag12 Ag -0.85193(3) 0.065409(9) 1.23463(3) 0.02200(12) Uani 1 1 d .
Ag13 Ag -0.71772(3) 0.043460(9) 1.17951(3) 0.02048(12) Uani 1 1 d .
Ag14 Ag -0.88317(3) 0.276228(9) 0.54289(3) 0.02227(12) Uani 1 1 d .
Ag15 Ag -0.88831(3) 0.060078(10) 1.05905(3) 0.02785(14) Uani 1 1 d .
Ag16 Ag -0.85906(3) 0.115386(9) 1.15733(3) 0.02221(12) Uani 1 1 d .
Ag17 Ag -0.72660(3) 0.278324(9) 0.48265(3) 0.02325(12) Uani 1 1 d .
Ag18 Ag -0.87277(3) 0.217671(9) 0.64638(3) 0.02460(13) Uani 1 1 d .
Ag19 Ag -0.87591(3) 0.388201(9) 0.05194(3) 0.02009(11) Uani 1 1 d .
Ag20 Ag -0.72268(3) 0.060240(9) 1.00566(3) 0.02424(12) Uani 1 1 d .
Ag21 Ag -0.66858(3) 0.440156(9) 0.03201(3) 0.02184(11) Uani 1 1 d .
Ag22 Ag -0.72148(3) 0.389827(9) -0.01162(3) 0.02252(12) Uani 1 1 d .
Ag23 Ag -0.66754(3) 0.227734(10) 0.52592(3) 0.02641(12) Uani 1 1 d .
Ag24 Ag -0.68258(3) 0.116279(12) 1.04765(4) 0.04090(17) Uani 1 1 d .
C1 C -0.7519(4) 0.41548(12) 0.0816(4) 0.0228(15) Uani 1 1 d .
C2 C -0.8042(3) 0.41902(11) 0.1246(4) 0.0183(14) Uani 1 1 d .
C3 C -0.7530(4) 0.25196(13) 0.5752(4) 0.0279(17) Uani 1 1 d .
C4 C -0.8035(4) 0.24783(13) 0.6150(4) 0.0274(16) Uani 1 1 d .
C5 C -0.7639(4) 0.09148(12) 1.0895(4) 0.0212(15) Uani 1 1 d .
C6 C -0.7866(4) 0.07627(13) 1.1344(4) 0.0289(17) Uani 1 1 d .
O1 O -0.9907(3) 0.38012(9) 0.1088(3) 0.0300(12) Uani 1 1 d .
O2 O -0.9619(3) 0.38253(9) 0.2487(3) 0.0308(12) Uani 1 1 d .
C7 C -1.0008(4) 0.37685(11) 0.1840(4) 0.0209(15) Uani 1 1 d .
C8 C -1.0703(4) 0.36213(13) 0.2008(5) 0.0318(17) Uani 1 1 d .
F11 F -1.1254(2) 0.36658(10) 0.1456(3) 0.0507(13) Uani 1 1 d .
F12 F -1.0554(3) 0.33873(8) 0.1984(3) 0.0528(13) Uani 1 1 d .
F13 F -1.0930(2) 0.36692(8) 0.2775(3) 0.0433(12) Uani 1 1 d .
O3 O -0.5492(2) 0.22349(9) 0.5933(3) 0.0295(12) Uani 1 1 d .
O4 O -0.5829(2) 0.22646(8) 0.7264(3) 0.0215(10) Uani 1 1 d .
C9 C -0.5400(4) 0.22410(11) 0.6717(4) 0.0216(15) Uani 1 1 d .
C10 C -0.4585(4) 0.22090(15) 0.7051(5) 0.0337(18) Uani 1 1 d .
F21 F -0.4470(3) 0.22309(10) 0.7882(3) 0.0558(15) Uani 1 1 d .
F22 F -0.4163(3) 0.23663(11) 0.6692(4) 0.0705(17) Uani 1 1 d .
F23 F -0.4340(3) 0.19891(9) 0.6855(3) 0.0507(13) Uani 1 1 d .
O5 O -0.7611(2) 0.27359(8) 0.3381(3) 0.0228(10) Uani 1 1 d .
O6 O -0.7832(2) 0.23341(8) 0.3385(3) 0.0245(11) Uani 1 1 d .
C11 C -0.7644(3) 0.25272(12) 0.3072(4) 0.0178(14) Uani 1 1 d .
C12 C -0.7393(4) 0.25098(12) 0.2170(4) 0.0238(15) Uani 1 1 d .
F31 F -0.7630(2) 0.23103(7) 0.1779(2) 0.0306(10) Uani 1 1 d .
F32 F -0.7642(2) 0.26954(7) 0.1695(2) 0.0347(10) Uani 1 1 d .
F33 F -0.6671(2) 0.25141(8) 0.2180(3) 0.0375(11) Uani 1 1 d .
O7 O -0.7589(2) 0.39301(8) -0.1555(3) 0.0216(10) Uani 1 1 d .
O8 O -0.7822(2) 0.43301(8) -0.1520(3) 0.0222(10) Uani 1 1 d .
C13 C -0.7644(3) 0.41398(12) -0.1856(4) 0.0191(14) Uani 1 1 d .
C14 C -0.7458(4) 0.41597(12) -0.2781(4) 0.0242(15) Uani 1 1 d .
F41 F -0.7731(2) 0.43604(7) -0.3142(2) 0.0357(10) Uani 1 1 d .
F42 F -0.7711(3) 0.39746(7) -0.3236(2) 0.0386(11) Uani 1 1 d .
F43 F -0.6737(2) 0.41676(8) -0.2824(3) 0.0395(11) Uani 1 1 d .
O9 O -0.8783(3) 0.47502(8) -0.0388(3) 0.0314(12) Uani 1 1 d .
O10 O -0.8915(3) 0.48576(9) 0.0968(3) 0.0303(12) Uani 1 1 d .
C15 C -0.8970(4) 0.48830(12) 0.0177(4) 0.0240(16) Uani 1 1 d .
C16 C -0.9341(5) 0.51172(14) -0.0135(5) 0.039(2) Uani 1 1 d .
F51 F -1.0069(3) 0.50859(11) -0.0169(4) 0.083(2) Uani 1 1 d .
F52 F -0.9154(3) 0.51894(8) -0.0876(3) 0.0492(13) Uani 1 1 d .
F53 F -0.9214(4) 0.53013(9) 0.0384(3) 0.0669(17) Uani 1 1 d .
O11 O -0.6986(3) 0.00591(9) 1.1201(3) 0.0330(12) Uani 1 1 d .
O12 O -0.6946(3) 0.02083(8) 0.9890(3) 0.0293(12) Uani 1 1 d .
C17 C -0.6912(4) 0.00451(12) 1.0437(4) 0.0246(16) Uani 1 1 d .
C18 C -0.6758(5) -0.02093(13) 1.0114(5) 0.0358(19) Uani 1 1 d .
F61 F -0.7266(4) -0.03639(9) 1.0301(4) 0.088(2) Uani 1 1 d .
F62 F -0.6737(4) -0.02175(9) 0.9284(3) 0.0727(18) Uani 1 1 d .
F63 F -0.6128(3) -0.02903(10) 1.0442(3) 0.0697(18) Uani 1 1 d .
O13 O -0.6836(3) 0.35183(9) -0.0293(3) 0.0306(12) Uani 1 1 d .
O14 O -0.7003(3) 0.33986(8) 0.1021(3) 0.0332(12) Uani 1 1 d .
C19 C -0.6842(4) 0.33688(13) 0.0292(4) 0.0250(16) Uani 1 1 d .
C20 C -0.6604(5) 0.31096(14) 0.0065(5) 0.039(2) Uani 1 1 d .
F71 F -0.6851(6) 0.29486(10) 0.0533(5) 0.160(5) Uani 1 1 d .
F72 F -0.5895(3) 0.30879(10) 0.0133(5) 0.091(2) Uani 1 1 d .
F73 F -0.6810(4) 0.30521(11) -0.0713(4) 0.088(2) Uani 1 1 d .
O15 O -1.0030(3) 0.05151(9) 1.1128(3) 0.0334(12) Uani 1 1 d .
O16 O -0.9643(3) 0.05040(9) 1.2500(3) 0.0318(12) Uani 1 1 d .
C21 C -1.0074(4) 0.04650(12) 1.1880(4) 0.0225(15) Uani 1 1 d .
C22 C -1.0778(4) 0.03262(14) 1.2083(5) 0.0372(19) Uani 1 1 d .
F81 F -1.0629(3) 0.00923(9) 1.2115(4) 0.0660(16) Uani 1 1 d .
F82 F -1.1005(3) 0.03926(10) 1.2825(3) 0.0530(13) Uani 1 1 d .
F83 F -1.1328(2) 0.03554(8) 1.1507(3) 0.0431(12) Uani 1 1 d .
O17 O -0.5613(3) 0.11811(9) 1.1037(3) 0.0342(12) Uani 1 1 d .
O18 O -0.5819(2) 0.10963(8) 1.2384(3) 0.0256(11) Uani 1 1 d .
C23 C -0.5448(4) 0.11520(13) 1.1796(5) 0.0265(16) Uani 1 1 d .
C24 C -0.4626(4) 0.11830(16) 1.2033(5) 0.040(2) Uani 1 1 d .
F91 F -0.4239(3) 0.10310(11) 1.1579(4) 0.0737(17) Uani 1 1 d .
F92 F -0.4427(3) 0.11417(10) 1.2835(3) 0.0584(15) Uani 1 1 d .
F93 F -0.4401(2) 0.14053(9) 1.1844(3) 0.0500(13) Uani 1 1 d .
O19 O -0.8317(2) 0.07996(8) 1.3721(3) 0.0203(10) Uani 1 1 d .
O20 O -0.7115(2) 0.08862(8) 1.3686(3) 0.0248(11) Uani 1 1 d .
C25 C -0.7701(4) 0.08706(11) 1.4019(4) 0.0192(14) Uani 1 1 d .
C26 C -0.7667(4) 0.09519(14) 1.4956(4) 0.0280(17) Uani 1 1 d .
F101 F -0.7658(3) 0.11904(8) 1.5004(3) 0.0480(12) Uani 1 1 d .
F102 F -0.7053(2) 0.08749(8) 1.5371(2) 0.0333(10) Uani 1 1 d .
F103 F -0.8223(2) 0.08710(9) 1.5354(3) 0.0449(13) Uani 1 1 d .
O21 O -0.8819(3) 0.14335(9) 0.9522(3) 0.0295(11) Uani 1 1 d .
O22 O -0.8786(3) 0.15379(8) 1.0909(3) 0.0268(11) Uani 1 1 d .
C27 C -0.8912(4) 0.15661(12) 1.0125(4) 0.0242(16) Uani 1 1 d .
C28 C -0.9246(4) 0.18116(13) 0.9887(5) 0.0315(17) Uani 1 1 d .
F111 F -0.9987(3) 0.17927(10) 0.9849(4) 0.0620(15) Uani 1 1 d .
F112 F -0.9070(3) 0.18930(8) 0.9142(3) 0.0417(11) Uani 1 1 d .
F113 F -0.9092(3) 0.19856(8) 1.0437(3) 0.0557(15) Uani 1 1 d .
O23 O -0.6938(3) 0.31697(8) 0.4673(3) 0.0291(11) Uani 1 1 d .
O24 O -0.7010(3) 0.32786(8) 0.6030(3) 0.0304(12) Uani 1 1 d .
C29 C -0.6912(4) 0.33127(12) 0.5288(4) 0.0257(16) Uani 1 1 d .
C30 C -0.6689(5) 0.35720(13) 0.5062(5) 0.0336(18) Uani 1 1 d .
F121 F -0.7016(5) 0.37334(9) 0.5490(5) 0.123(3) Uani 1 1 d .
F122 F -0.6866(3) 0.36308(10) 0.4268(3) 0.0758(19) Uani 1 1 d .
F123 F -0.5991(3) 0.36080(10) 0.5185(4) 0.078(2) Uani 1 1 d .
O25 O -0.7155(2) 0.24261(8) 0.8530(3) 0.0253(11) Uani 1 1 d .
O26 O -0.8356(2) 0.24958(8) 0.8577(3) 0.0190(10) Uani 1 1 d .
C31 C -0.7744(4) 0.24336(11) 0.8867(4) 0.0200(14) Uani 1 1 d .
C32 C -0.7684(4) 0.23571(12) 0.9805(4) 0.0224(15) Uani 1 1 d .
F131 F -0.7658(2) 0.21194(8) 0.9867(3) 0.0381(11) Uani 1 1 d .
F132 F -0.7087(2) 0.24433(9) 1.0215(2) 0.0396(11) Uani 1 1 d .
F133 F -0.8266(2) 0.24305(8) 1.0197(2) 0.0326(10) Uani 1 1 d .
O27 O -0.9961(3) 0.28510(9) 0.6000(3) 0.0298(11) Uani 1 1 d .
O28 O -0.9618(3) 0.28346(9) 0.7386(3) 0.0294(12) Uani 1 1 d .
C33 C -1.0039(4) 0.28829(11) 0.6760(4) 0.0211(15) Uani 1 1 d .
C34 C -1.0738(4) 0.30145(13) 0.6974(5) 0.0295(17) Uani 1 1 d .
F141 F -1.0629(3) 0.32506(8) 0.6993(4) 0.0584(14) Uani 1 1 d .
F142 F -1.0966(2) 0.29463(9) 0.7708(3) 0.0501(13) Uani 1 1 d .
F143 F -1.1291(2) 0.29794(9) 0.6392(3) 0.0469(12) Uani 1 1 d .
O29 O -0.7835(3) 0.10408(8) 0.8451(3) 0.0248(11) Uani 1 1 d .
O30 O -0.7577(3) 0.06438(8) 0.8576(3) 0.0285(11) Uani 1 1 d .
C35 C -0.7613(4) 0.08436(12) 0.8212(4) 0.0216(15) Uani 1 1 d .
C36 C -0.7332(4) 0.08461(12) 0.7325(4) 0.0217(15) Uani 1 1 d .
F151 F -0.6610(2) 0.08607(9) 0.7369(3) 0.0419(11) Uani 1 1 d .
F152 F -0.7519(3) 0.06453(7) 0.6897(2) 0.0390(11) Uani 1 1 d .
F153 F -0.7591(2) 0.10308(7) 0.6867(2) 0.0341(10) Uani 1 1 d .
O31 O -0.8663(3) 0.19011(8) 0.4508(3) 0.0293(11) Uani 1 1 d .
O32 O -0.8881(3) 0.17910(9) 0.5833(3) 0.0303(12) Uani 1 1 d .
C37 C -0.8878(4) 0.17672(13) 0.5052(5) 0.0264(16) Uani 1 1 d .
C38 C -0.9220(4) 0.15350(14) 0.4706(5) 0.0359(19) Uani 1 1 d .
F161 F -0.9892(3) 0.15698(13) 0.4444(6) 0.149(4) Uani 1 1 d .
F162 F -0.9226(4) 0.13579(10) 0.5255(4) 0.091(2) Uani 1 1 d .
F163 F -0.8896(3) 0.14412(8) 0.4074(3) 0.0581(15) Uani 1 1 d .
O33 O -0.7148(3) 0.42323(8) 0.3597(3) 0.0243(10) Uani 1 1 d .
O34 O -0.8339(2) 0.41556(8) 0.3640(3) 0.0230(10) Uani 1 1 d .
C39 C -0.7737(4) 0.42254(11) 0.3932(4) 0.0181(14) Uani 1 1 d .
C40 C -0.7711(4) 0.43223(14) 0.4848(4) 0.0254(16) Uani 1 1 d .
F171 F -0.7094(2) 0.42585(9) 0.5289(2) 0.0397(11) Uani 1 1 d .
F172 F -0.7745(3) 0.45585(8) 0.4855(3) 0.0466(12) Uani 1 1 d .
F173 F -0.8267(2) 0.42375(9) 0.5254(3) 0.0397(11) Uani 1 1 d .
O35 O -0.5855(2) 0.44394(8) 0.2333(3) 0.0242(11) Uani 1 1 d .
O36 O -0.5503(2) 0.44525(9) 0.1005(3) 0.0268(11) Uani 1 1 d .
C41 C -0.5415(4) 0.44596(11) 0.1788(4) 0.0210(15) Uani 1 1 d .
C42 C -0.4623(4) 0.45183(13) 0.2122(4) 0.0272(16) Uani 1 1 d .
F181 F -0.4452(2) 0.47477(8) 0.1962(3) 0.0428(11) Uani 1 1 d .
F182 F -0.4144(2) 0.43811(9) 0.1743(4) 0.0564(14) Uani 1 1 d .
F183 F -0.4491(3) 0.44847(9) 0.2947(3) 0.0489(13) Uani 1 1 d .
O100 O -1.1086(4) 0.42591(15) 0.4641(5) 0.109(4) Uani 1 1 d .
N1 N -0.9733(3) 0.45382(10) 0.2414(3) 0.0247(13) Uani 1 1 d .
N2 N -1.0080(5) 0.40969(17) 0.4474(6) 0.107(4) Uani 1 1 d .
C100 C -1.0439(3) 0.44198(12) 0.3553(4) 0.0217(15) Uani 1 1 d .
C101 C -0.9862(4) 0.43934(12) 0.3049(4) 0.0235(15) Uani 1 1 d .
H10A H -0.9543 0.4265 0.3164 0.028 Uiso 1 1 calc R
C102 C -1.0177(4) 0.47272(12) 0.2259(4) 0.0241(15) Uani 1 1 d .
H10B H -1.0089 0.4833 0.1822 0.029 Uiso 1 1 calc R
C103 C -1.0768(4) 0.47696(13) 0.2738(4) 0.0285(17) Uani 1 1 d .
H10C H -1.1071 0.4902 0.2617 0.034 Uiso 1 1 calc R
C104 C -1.0904(4) 0.46163(12) 0.3390(4) 0.0251(16) Uani 1 1 d .
H10D H -1.1297 0.4643 0.3716 0.030 Uiso 1 1 calc R
C105 C -1.0560(4) 0.42520(12) 0.4263(4) 0.0227(15) Uani 1 1 d .
O101 O -0.6121(3) 0.25970(9) 0.4360(3) 0.0354(13) Uani 1 1 d .
C108 C -0.5713(4) 0.31358(13) 0.2567(5) 0.0329(18) Uani 1 1 d .
H10E H -0.6008 0.3270 0.2456 0.039 Uiso 1 1 calc R
N4 N -0.4947(3) 0.25022(10) 0.4437(4) 0.0309(15) Uani 1 1 d .
H4A H -0.4997 0.2409 0.4863 0.037 Uiso 1 1 calc R
H4B H -0.4525 0.2519 0.4242 0.037 Uiso 1 1 calc R
C106 C -0.5400(3) 0.27866(11) 0.3371(4) 0.0191(14) Uani 1 1 d .
C107 C -0.5851(4) 0.29818(13) 0.3208(4) 0.0282(16) Uani 1 1 d .
H10F H -0.6245 0.3009 0.3531 0.034 Uiso 1 1 calc R
C109 C -0.5132(4) 0.30907(12) 0.2081(4) 0.0265(16) Uani 1 1 d .
H10G H -0.5038 0.3198 0.1650 0.032 Uiso 1 1 calc R
N3 N -0.4703(3) 0.28976(10) 0.2215(3) 0.0250(13) Uani 1 1 d .
C110 C -0.4838(4) 0.27509(12) 0.2850(4) 0.0226(15) Uani 1 1 d .
H11A H -0.4538 0.2617 0.2949 0.027 Uiso 1 1 calc R
C111 C -0.5515(3) 0.26196(12) 0.4084(4) 0.0213(15) Uani 1 1 d .
O102 O -0.7964(3) 0.30464(9) -0.2408(3) 0.0324(12) Uani 1 1 d .
N5 N -0.8798(3) 0.35282(9) -0.0179(3) 0.0206(12) Uani 1 1 d .
N6 N -0.7742(3) 0.34467(10) -0.2440(3) 0.0255(13) Uani 1 1 d .
H6A H -0.7516 0.3434 -0.2893 0.031 Uiso 1 1 calc R
H6B H -0.7789 0.3586 -0.2208 0.031 Uiso 1 1 calc R
C112 C -0.8392(4) 0.32786(12) -0.1297(4) 0.0241(15) Uani 1 1 d .
C113 C -0.8503(3) 0.34986(11) -0.0928(4) 0.0198(14) Uani 1 1 d .
H11B H -0.8367 0.3636 -0.1211 0.024 Uiso 1 1 calc R
C114 C -0.8993(5) 0.33274(14) 0.0216(5) 0.041(2) Uani 1 1 d .
H11C H -0.9186 0.3343 0.0739 0.049 Uiso 1 1 calc R
C115 C -0.8922(5) 0.30984(14) -0.0114(5) 0.048(2) Uani 1 1 d .
H11D H -0.9068 0.2963 0.0177 0.057 Uiso 1 1 calc R
C116 C -0.8627(5) 0.30759(14) -0.0890(5) 0.043(2) Uani 1 1 d .
H11E H -0.8588 0.2924 -0.1136 0.051 Uiso 1 1 calc R
C117 C -0.8020(4) 0.32494(12) -0.2094(4) 0.0227(15) Uani 1 1 d .
O103 O -0.7681(3) 0.46969(8) 0.2571(3) 0.0308(12) Uani 1 1 d .
N7 N -0.6642(3) 0.52378(10) 0.4648(3) 0.0220(12) Uani 1 1 d .
N8 N -0.7947(3) 0.50857(11) 0.2417(4) 0.0358(16) Uani 1 1 d .
H8A H -0.8255 0.5055 0.1996 0.043 Uiso 1 1 calc R
H8B H -0.7877 0.5232 0.2584 0.043 Uiso 1 1 calc R
C118 C -0.7058(4) 0.49660(11) 0.3537(4) 0.0192(14) Uani 1 1 d .
C119 C -0.7097(4) 0.51780(13) 0.3986(4) 0.0257(16) Uani 1 1 d .
H11F H -0.7465 0.5287 0.3817 0.031 Uiso 1 1 calc R
C120 C -0.6107(4) 0.50826(13) 0.4866(4) 0.0280(16) Uani 1 1 d .
H12A H -0.5778 0.5121 0.5319 0.034 Uiso 1 1 calc R
C121 C -0.6022(4) 0.48699(14) 0.4455(5) 0.043(2) Uani 1 1 d .
H12B H -0.5645 0.4766 0.4635 0.051 Uiso 1 1 calc R
C122 C -0.6494(4) 0.48083(13) 0.3769(5) 0.0344(18) Uani 1 1 d .
H12C H -0.6434 0.4666 0.3473 0.041 Uiso 1 1 calc R
C123 C -0.7582(4) 0.49075(12) 0.2808(4) 0.0237(15) Uani 1 1 d .
O104 O -0.7602(3) 0.13605(9) 1.2549(3) 0.0324(12) Uani 1 1 d .
N9 N -0.6580(3) 0.19195(10) 1.4589(3) 0.0243(13) Uani 1 1 d .
N10 N -0.7847(3) 0.17520(10) 1.2339(4) 0.0314(15) Uani 1 1 d .
H10H H -0.8154 0.1720 1.1919 0.038 Uiso 1 1 calc R
H10I H -0.7767 0.1899 1.2489 0.038 Uiso 1 1 calc R
C124 C -0.6981(4) 0.16358(12) 1.3510(4) 0.0213(15) Uani 1 1 d .
C125 C -0.7027(4) 0.18529(12) 1.3920(4) 0.0226(15) Uani 1 1 d .
H12D H -0.7389 0.1961 1.3723 0.027 Uiso 1 1 calc R
C126 C -0.6058(4) 0.17631(13) 1.4843(5) 0.0321(18) Uani 1 1 d .
H12E H -0.5739 0.1805 1.5302 0.039 Uiso 1 1 calc R
C127 C -0.5967(4) 0.15438(13) 1.4466(5) 0.042(2) Uani 1 1 d .
H12F H -0.5594 0.1441 1.4665 0.051 Uiso 1 1 calc R
C128 C -0.6437(4) 0.14787(13) 1.3785(5) 0.0337(18) Uani 1 1 d .
H12G H -0.6386 0.1331 1.3518 0.040 Uiso 1 1 calc R
C129 C -0.7494(3) 0.15737(13) 1.2757(4) 0.0221(15) Uani 1 1 d .
O105 O -0.7628(3) 0.19665(8) 0.7368(3) 0.0300(12) Uani 1 1 d .
N11 N -0.6655(3) 0.14842(11) 0.9661(4) 0.0322(15) Uani 1 1 d .
N12 N -0.7961(3) 0.15821(10) 0.7394(4) 0.0309(14) Uani 1 1 d .
H12H H -0.8267 0.1602 0.6963 0.037 Uiso 1 1 calc R
H12I H -0.7911 0.1443 0.7629 0.037 Uiso 1 1 calc R
C130 C -0.7030(4) 0.17225(11) 0.8437(4) 0.0192(14) Uani 1 1 d .
C131 C -0.7125(4) 0.15379(12) 0.8996(4) 0.0266(16) Uani 1 1 d .
H13A H -0.7542 0.1443 0.8909 0.032 Uiso 1 1 calc R
C132 C -0.6070(4) 0.16221(13) 0.9782(4) 0.0278(16) Uani 1 1 d .
H13B H -0.5736 0.1589 1.0237 0.033 Uiso 1 1 calc R
C133 C -0.5935(4) 0.18140(13) 0.9257(5) 0.0334(18) Uani 1 1 d .
H13C H -0.5519 0.1908 0.9366 0.040 Uiso 1 1 calc R
C134 C -0.6414(4) 0.18658(12) 0.8577(4) 0.0242(15) Uani 1 1 d .
H13D H -0.6327 0.1994 0.8218 0.029 Uiso 1 1 calc R
C135 C -0.7565(4) 0.17668(12) 0.7694(4) 0.0209(14) Uani 1 1 d .
O106 O -0.9443(3) 0.08747(9) 0.9522(3) 0.0317(12) Uani 1 1 d .
N13 N -1.1018(3) 0.11904(9) 0.7256(3) 0.0215(12) Uani 1 1 d .
N14 N -1.0642(3) 0.07977(10) 0.9533(3) 0.0257(13) Uani 1 1 d .
H14A H -1.0582 0.0715 0.9991 0.031 Uiso 1 1 calc R
H14B H -1.1072 0.0817 0.9290 0.031 Uiso 1 1 calc R
C136 C -1.0194(4) 0.10306(12) 0.8371(4) 0.0238(15) Uani 1 1 d .
C137 C -1.0895(4) 0.10929(11) 0.8043(4) 0.0190(14) Uani 1 1 d .
H13F H -1.1288 0.1067 0.8370 0.023 Uiso 1 1 calc R
C138 C -1.0443(4) 0.12374(13) 0.6813(5) 0.0324(18) Uani 1 1 d .
H13G H -1.0522 0.1303 0.6275 0.039 Uiso 1 1 calc R
C139 C -0.9731(4) 0.11911(15) 0.7127(5) 0.040(2) Uani 1 1 d .
H13H H -0.9342 0.1231 0.6810 0.048 Uiso 1 1 calc R
C140 C -0.9604(4) 0.10857(13) 0.7917(5) 0.0312(18) Uani 1 1 d .
H14C H -0.9131 0.1053 0.8137 0.037 Uiso 1 1 calc R
C141 C -1.0064(4) 0.08973(11) 0.9196(4) 0.0241(16) Uani 1 1 d .
O107 O -0.9385(2) 0.41765(9) -0.0472(3) 0.0281(11) Uani 1 1 d .
N15 N -1.1006(3) 0.45462(10) -0.2584(3) 0.0225(12) Uani 1 1 d .
N16 N -1.0588(3) 0.41175(10) -0.0395(3) 0.0271(13) Uani 1 1 d .
H16A H -1.0519 0.4027 0.0043 0.033 Uiso 1 1 calc R
H16B H -1.1024 0.4146 -0.0605 0.033 Uiso 1 1 calc R
C142 C -1.0169(4) 0.43616(11) -0.1538(4) 0.0209(15) Uani 1 1 d .
C143 C -1.0863(4) 0.44356(11) -0.1830(4) 0.0219(15) Uani 1 1 d .
H14D H -1.1247 0.4408 -0.1492 0.026 Uiso 1 1 calc R
C144 C -1.0451(4) 0.45948(13) -0.3046(5) 0.0329(18) Uani 1 1 d .
H14E H -1.0547 0.4668 -0.3569 0.040 Uiso 1 1 calc R
C145 C -0.9737(4) 0.45406(15) -0.2782(5) 0.042(2) Uani 1 1 d .
H14F H -0.9359 0.4583 -0.3111 0.050 Uiso 1 1 calc R
C146 C -0.9593(4) 0.44233(14) -0.2025(5) 0.0315(18) Uani 1 1 d .
H14G H -0.9115 0.4385 -0.1838 0.038 Uiso 1 1 calc R
C147 C -1.0016(4) 0.42136(11) -0.0753(4) 0.0203(14) Uani 1 1 d .
O108 O -0.9450(2) 0.24457(9) 0.4527(3) 0.0290(12) Uani 1 1 d .
N17 N -1.1037(3) 0.21125(9) 0.2306(3) 0.0201(12) Uani 1 1 d .
N18 N -1.0640(3) 0.25426(10) 0.4486(4) 0.0270(13) Uani 1 1 d .
H18A H -1.0576 0.2632 0.4929 0.032 Uiso 1 1 calc R
H18B H -1.1069 0.2527 0.4235 0.032 Uiso 1 1 calc R
C148 C -1.0214(4) 0.22721(12) 0.3405(4) 0.0232(15) Uani 1 1 d .
C149 C -1.0907(4) 0.22267(11) 0.3041(4) 0.0202(15) Uani 1 1 d .
H14H H -1.1304 0.2279 0.3324 0.024 Uiso 1 1 calc R
C150 C -1.0465(4) 0.20331(14) 0.1929(5) 0.0333(18) Uani 1 1 d .
H15B H -1.0546 0.1956 0.1410 0.040 Uiso 1 1 calc R
C151 C -0.9756(4) 0.20590(16) 0.2261(5) 0.045(2) Uani 1 1 d .
H15C H -0.9372 0.1993 0.1987 0.054 Uiso 1 1 calc R
C152 C -0.9624(4) 0.21844(14) 0.3011(4) 0.0309(17) Uani 1 1 d .
H15D H -0.9150 0.2209 0.3244 0.037 Uiso 1 1 calc R
C153 C -1.0069(4) 0.24275(12) 0.4184(4) 0.0209(15) Uani 1 1 d .
O109 O -0.6094(3) 0.40957(9) -0.0614(3) 0.0317(12) Uani 1 1 d .
N19 N -0.4604(3) 0.38009(10) -0.2717(3) 0.0211(12) Uani 1 1 d .
N20 N -0.4905(3) 0.41804(11) -0.0453(4) 0.0290(14) Uani 1 1 d .
H20A H -0.4965 0.4270 -0.0020 0.035 Uiso 1 1 calc R
H20B H -0.4477 0.4162 -0.0627 0.035 Uiso 1 1 calc R
C154 C -0.5349(3) 0.39180(12) -0.1587(4) 0.0209(15) Uani 1 1 d .
C155 C -0.4727(4) 0.39356(12) -0.2030(4) 0.0221(15) Uani 1 1 d .
H15E H -0.4373 0.4047 -0.1842 0.027 Uiso 1 1 calc R
C156 C -0.5098(4) 0.36351(13) -0.2963(5) 0.0296(17) Uani 1 1 d .
H15F H -0.5017 0.3538 -0.3426 0.035 Uiso 1 1 calc R
C157 C -0.5737(4) 0.36017(13) -0.2547(4) 0.0326(18) Uani 1 1 d .
H15G H -0.6076 0.3485 -0.2734 0.039 Uiso 1 1 calc R
C158 C -0.5857(4) 0.37439(13) -0.1858(4) 0.0290(17) Uani 1 1 d .
H15H H -0.6277 0.3723 -0.1575 0.035 Uiso 1 1 calc R
C159 C -0.5466(3) 0.40729(12) -0.0849(4) 0.0203(15) Uani 1 1 d .
O111 O -0.8009(3) 0.02436(9) 1.2717(3) 0.0391(14) Uani 1 1 d .
N23 N -0.8878(3) -0.02391(9) 1.4908(3) 0.0199(12) Uani 1 1 d .
N24 N -0.7742(3) -0.01499(10) 1.2709(3) 0.0253(13) Uani 1 1 d .
H24A H -0.7515 -0.0137 1.2257 0.030 Uiso 1 1 calc R
H24B H -0.7775 -0.0288 1.2949 0.030 Uiso 1 1 calc R
C166 C -0.8456(4) 0.00099(12) 1.3804(4) 0.0256(16) Uani 1 1 d .
C167 C -0.8556(3) -0.02109(11) 1.4179(4) 0.0181(14) Uani 1 1 d .
H16C H -0.8391 -0.0348 1.3914 0.022 Uiso 1 1 calc R
C168 C -0.9124(4) -0.00423(14) 1.5261(5) 0.041(2) Uani 1 1 d .
H16D H -0.9356 -0.0058 1.5760 0.049 Uiso 1 1 calc R
C169 C -0.9055(5) 0.01869(13) 1.4927(6) 0.055(3) Uani 1 1 d .
H16E H -0.9225 0.0322 1.5202 0.066 Uiso 1 1 calc R
C170 C -0.8734(5) 0.02112(14) 1.4189(6) 0.049(2) Uani 1 1 d .
H17B H -0.8700 0.0363 1.3942 0.059 Uiso 1 1 calc R
C171 C -0.8045(4) 0.00455(13) 1.3041(4) 0.0259(16) Uani 1 1 d .
O110 O -0.7967(3) 0.36138(9) 0.2581(3) 0.0367(13) Uani 1 1 d .
N21 N -0.8868(3) 0.31182(9) 0.4731(3) 0.0205(12) Uani 1 1 d .
N22 N -0.7734(3) 0.32166(9) 0.2527(3) 0.0220(13) Uani 1 1 d .
H22A H -0.7494 0.3234 0.2086 0.026 Uiso 1 1 calc R
H22B H -0.7783 0.3076 0.2742 0.026 Uiso 1 1 calc R
C160 C -0.8422(4) 0.33742(12) 0.3664(4) 0.0219(15) Uani 1 1 d .
C161 C -0.8572(3) 0.31507(11) 0.3991(4) 0.0168(13) Uani 1 1 d .
H16F H -0.8462 0.3015 0.3682 0.020 Uiso 1 1 calc R
C162 C -0.9024(4) 0.33169(13) 0.5155(4) 0.0296(17) Uani 1 1 d .
H16G H -0.9216 0.3299 0.5677 0.036 Uiso 1 1 calc R
C163 C -0.8917(4) 0.35482(13) 0.4866(5) 0.0358(19) Uani 1 1 d .
H16H H -0.9048 0.3682 0.5177 0.043 Uiso 1 1 calc R
C164 C -0.8613(4) 0.35772(13) 0.4102(5) 0.0375(19) Uani 1 1 d .
H16I H -0.8538 0.3731 0.3887 0.045 Uiso 1 1 calc R
C165 C -0.8029(4) 0.34079(12) 0.2877(4) 0.0240(15) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C5 Ag1 O21 134.6(2) . .
C5 Ag1 O29 120.3(2) . .
O21 Ag1 O29 93.81(16) . .
C5 Ag1 O106 111.7(2) . .
O21 Ag1 O106 88.83(17) . .
O29 Ag1 O106 99.17(17) . .
C5 Ag1 Ag24 49.31(16) . .
O21 Ag1 Ag24 108.07(13) . .
O29 Ag1 Ag24 89.58(11) . .
O106 Ag1 Ag24 160.49(11) . .
C5 Ag1 Ag16 55.67(18) . .
O21 Ag1 Ag16 85.86(12) . .
O29 Ag1 Ag16 170.95(12) . .
O106 Ag1 Ag16 89.88(12) . .
Ag24 Ag1 Ag16 81.94(2) . .
C5 Ag1 Ag15 62.41(17) . .
O21 Ag1 Ag15 129.49(13) . .
O29 Ag1 Ag15 117.48(11) . .
O106 Ag1 Ag15 49.96(11) . .
Ag24 Ag1 Ag15 110.55(2) . .
Ag16 Ag1 Ag15 68.936(18) . .
C5 Ag1 Ag20 46.44(18) . .
O21 Ag1 Ag20 169.88(13) . .
O29 Ag1 Ag20 79.72(11) . .
O106 Ag1 Ag20 99.82(12) . .
Ag24 Ag1 Ag20 64.44(2) . .
Ag16 Ag1 Ag20 99.293(19) . .
Ag15 Ag1 Ag20 60.632(17) . .
O9 Ag2 C1 145.2(2) . .
O9 Ag2 O8 98.80(16) . .
C1 Ag2 O8 108.3(2) . .
O9 Ag2 O107 91.81(17) . .
C1 Ag2 O107 107.05(19) . .
O8 Ag2 O107 94.43(16) . .
O9 Ag2 C2 125.00(19) . .
C1 Ag2 C2 29.3(2) . .
O8 Ag2 C2 135.57(18) . .
O107 Ag2 C2 91.54(17) . .
O9 Ag2 Ag21 116.52(14) . .
C1 Ag2 Ag21 49.10(16) . .
O8 Ag2 Ag21 82.17(11) . .
O107 Ag2 Ag21 151.67(11) . .
C2 Ag2 Ag21 72.49(15) . .
O9 Ag2 Ag10 80.96(12) . .
C1 Ag2 Ag10 71.38(16) . .
O8 Ag2 Ag10 178.57(12) . .
O107 Ag2 Ag10 86.98(11) . .
C2 Ag2 Ag10 44.46(14) . .
Ag21 Ag2 Ag10 96.673(19) . .
O9 Ag2 Ag19 134.08(13) . .
C1 Ag2 Ag19 56.85(16) . .
O8 Ag2 Ag19 107.73(11) . .
O107 Ag2 Ag19 50.20(11) . .
C2 Ag2 Ag19 47.92(14) . .
Ag21 Ag2 Ag19 103.93(2) . .
Ag10 Ag2 Ag19 73.335(17) . .
O9 Ag2 Ag22 168.50(13) . .
C1 Ag2 Ag22 40.37(16) . .
O8 Ag2 Ag22 71.23(11) . .
O107 Ag2 Ag22 94.63(12) . .
C2 Ag2 Ag22 64.41(14) . .
Ag21 Ag2 Ag22 57.559(16) . .
Ag10 Ag2 Ag22 108.864(18) . .
Ag19 Ag2 Ag22 56.482(15) . .
O31 Ag3 O6 96.24(16) . .
O31 Ag3 C3 143.1(2) . .
O6 Ag3 C3 111.2(2) . .
O31 Ag3 O108 90.41(17) . .
O6 Ag3 O108 99.18(16) . .
C3 Ag3 O108 108.1(2) . .
O31 Ag3 C4 125.5(2) . .
O6 Ag3 C4 137.1(2) . .
C3 Ag3 C4 27.9(2) . .
O108 Ag3 C4 90.57(19) . .
O31 Ag3 Ag23 112.86(13) . .
O6 Ag3 Ag23 84.60(11) . .
C3 Ag3 Ag23 49.42(17) . .
O108 Ag3 Ag23 156.01(11) . .
C4 Ag3 Ag23 71.49(16) . .
O31 Ag3 Ag18 81.11(12) . .
O6 Ag3 Ag18 177.34(12) . .
C3 Ag3 Ag18 71.10(17) . .
O108 Ag3 Ag18 81.12(11) . .
C4 Ag3 Ag18 45.43(16) . .
Ag23 Ag3 Ag18 96.20(2) . .
O31 Ag3 Ag14 135.04(13) . .
O6 Ag3 Ag14 110.02(11) . .
C3 Ag3 Ag14 57.81(17) . .
O108 Ag3 Ag14 50.76(11) . .
C4 Ag3 Ag14 48.19(16) . .
Ag23 Ag3 Ag14 105.59(2) . .
Ag18 Ag3 Ag14 72.241(17) . .
O31 Ag3 Ag17 167.29(12) . .
O6 Ag3 Ag17 74.10(11) . .
C3 Ag3 Ag17 40.55(16) . .
O108 Ag3 Ag17 99.17(12) . .
C4 Ag3 Ag17 63.12(16) . .
Ag23 Ag3 Ag17 58.845(17) . .
Ag18 Ag3 Ag17 108.497(19) . .
Ag14 Ag3 Ag17 57.376(16) . .
C2 Ag4 O2 137.6(2) . .
C2 Ag4 O34 120.0(2) . .
O2 Ag4 O34 95.72(17) . .
C2 Ag4 O110 110.7(2) . .
O2 Ag4 O110 86.07(18) . .
O34 Ag4 O110 94.97(17) . .
C2 Ag4 Ag10 50.27(16) . .
O2 Ag4 Ag10 112.06(13) . .
O34 Ag4 Ag10 91.51(11) . .
O110 Ag4 Ag10 160.05(11) . .
C2 Ag4 Ag19 54.60(16) . .
O2 Ag4 Ag19 88.32(12) . .
O34 Ag4 Ag19 174.02(12) . .
O110 Ag4 Ag19 89.68(12) . .
Ag10 Ag4 Ag19 82.879(19) . .
C2 Ag4 Ag8 62.00(16) . .
O2 Ag4 Ag8 127.08(14) . .
O34 Ag4 Ag8 112.56(11) . .
O110 Ag4 Ag8 49.29(11) . .
Ag10 Ag4 Ag8 110.89(2) . .
Ag19 Ag4 Ag8 67.914(17) . .
C2 Ag4 Ag9 45.98(16) . .
O2 Ag4 Ag9 172.96(13) . .
O34 Ag4 Ag9 78.29(12) . .
O110 Ag4 Ag9 98.04(12) . .
Ag10 Ag4 Ag9 64.836(17) . .
Ag19 Ag4 Ag9 97.372(18) . .
Ag8 Ag4 Ag9 59.372(16) . .
N17 Ag5 O24 92.46(18) 4 .
N17 Ag5 O102 104.30(18) 4 1_556
O24 Ag5 O102 90.68(16) . 1_556
N17 Ag5 C3 117.2(2) 4 .
O24 Ag5 C3 125.32(19) . .
O102 Ag5 C3 120.7(2) 1_556 .
N17 Ag5 Ag17 117.73(14) 4 .
O24 Ag5 Ag17 79.15(11) . .
O102 Ag5 Ag17 136.95(13) 1_556 .
C3 Ag5 Ag17 46.86(15) . .
N17 Ag5 Ag6 125.76(13) 4 .
O24 Ag5 Ag6 130.08(13) . .
O102 Ag5 Ag6 52.88(11) 1_556 .
C3 Ag5 Ag6 68.53(16) . .
Ag17 Ag5 Ag6 103.84(2) . .
N17 Ag5 Ag11 79.80(13) 4 .
O24 Ag5 Ag11 164.94(12) . .
O102 Ag5 Ag11 103.70(12) 1_556 .
C3 Ag5 Ag11 50.31(15) . .
Ag17 Ag5 Ag11 92.94(2) . .
Ag6 Ag5 Ag11 64.089(16) . .
C4 Ag6 O28 135.6(2) . .
C4 Ag6 O26 120.8(2) . .
O28 Ag6 O26 96.43(16) . .
C4 Ag6 O102 112.2(2) . 1_556
O28 Ag6 O102 86.10(17) . 1_556
O26 Ag6 O102 93.70(16) . 1_556
C4 Ag6 Ag18 48.50(19) . .
O28 Ag6 Ag18 112.29(13) . .
O26 Ag6 Ag18 92.91(11) . .
O102 Ag6 Ag18 159.60(11) 1_556 .
C4 Ag6 Ag14 53.69(17) . .
O28 Ag6 Ag14 85.74(12) . .
O26 Ag6 Ag14 170.59(11) . .
O102 Ag6 Ag14 95.58(12) 1_556 .
Ag18 Ag6 Ag14 77.833(19) . .
C4 Ag6 Ag5 62.60(19) . .
O28 Ag6 Ag5 126.58(13) . .
O26 Ag6 Ag5 112.95(11) . .
O102 Ag6 Ag5 50.07(11) 1_556 .
Ag18 Ag6 Ag5 109.71(2) . .
Ag14 Ag6 Ag5 72.349(18) . .
C4 Ag6 Ag11 47.18(18) . .
O28 Ag6 Ag11 174.47(13) . .
O26 Ag6 Ag11 78.80(11) . .
O102 Ag6 Ag11 96.92(12) 1_556 .
Ag18 Ag6 Ag11 65.538(17) . .
Ag14 Ag6 Ag11 98.524(19) . .
Ag5 Ag6 Ag11 58.463(16) . .
O18 Ag7 O20 98.63(16) . .
O18 Ag7 C6 142.9(2) . .
O20 Ag7 C6 112.8(2) . .
O18 Ag7 C5 121.05(19) . .
O20 Ag7 C5 139.93(19) . .
C6 Ag7 C5 28.8(2) . .
O18 Ag7 O104 98.67(17) . .
O20 Ag7 O104 85.09(16) . .
C6 Ag7 O104 103.0(2) . .
C5 Ag7 O104 93.57(19) . .
O18 Ag7 Ag13 114.76(12) . .
O20 Ag7 Ag13 91.89(12) . .
C6 Ag7 Ag13 47.98(18) . .
C5 Ag7 Ag13 67.85(15) . .
O104 Ag7 Ag13 146.49(12) . .
O18 Ag7 Ag24 78.98(11) . .
O20 Ag7 Ag24 170.53(12) . .
C6 Ag7 Ag24 72.86(16) . .
C5 Ag7 Ag24 44.50(15) . .
O104 Ag7 Ag24 86.22(12) . .
Ag13 Ag7 Ag24 97.43(2) . .
O18 Ag7 Ag16 139.71(12) . .
O20 Ag7 Ag16 103.44(11) . .
C6 Ag7 Ag16 51.92(18) . .
C5 Ag7 Ag16 49.81(16) . .
O104 Ag7 Ag16 51.06(11) . .
Ag13 Ag7 Ag16 97.880(19) . .
Ag24 Ag7 Ag16 73.725(18) . .
O18 Ag7 Ag12 165.43(12) . .
O20 Ag7 Ag12 73.32(11) . .
C6 Ag7 Ag12 40.21(16) . .
C5 Ag7 Ag12 66.74(15) . .
O104 Ag7 Ag12 92.80(12) . .
Ag13 Ag7 Ag12 54.698(15) . .
Ag24 Ag7 Ag12 110.898(19) . .
Ag16 Ag7 Ag12 54.853(15) . .
N13 Ag8 O110 109.61(19) 4_554 .
N13 Ag8 O14 94.42(18) 4_554 .
O110 Ag8 O14 90.99(17) . .
N13 Ag8 C1 110.8(2) 4_554 .
O110 Ag8 C1 121.68(19) . .
O14 Ag8 C1 125.16(19) . .
N13 Ag8 Ag22 110.93(14) 4_554 .
O110 Ag8 Ag22 138.73(14) . .
O14 Ag8 Ag22 78.58(11) . .
C1 Ag8 Ag22 47.33(15) . .
N13 Ag8 Ag4 125.70(13) 4_554 .
O110 Ag8 Ag4 52.70(12) . .
O14 Ag8 Ag4 131.12(13) . .
C1 Ag8 Ag4 69.74(15) . .
Ag22 Ag8 Ag4 106.41(2) . .
N13 Ag8 Ag9 76.17(13) 4_554 .
O110 Ag8 Ag9 104.99(12) . .
O14 Ag8 Ag9 163.39(13) . .
C1 Ag8 Ag9 49.36(15) . .
Ag22 Ag8 Ag9 91.870(19) . .
Ag4 Ag8 Ag9 64.480(16) . .
N13 Ag8 Ag19 165.16(13) 4_554 .
O110 Ag8 Ag19 81.93(14) . .
O14 Ag8 Ag19 94.69(13) . .
C1 Ag8 Ag19 54.36(15) . .
Ag22 Ag8 Ag19 59.694(16) . .
Ag4 Ag8 Ag19 53.647(15) . .
Ag9 Ag8 Ag19 92.074(18) . .
O35 Ag9 C2 149.98(19) . .
O35 Ag9 O33 94.92(16) . .
C2 Ag9 O33 112.47(19) . .
O35 Ag9 C1 120.67(19) . .
C2 Ag9 C1 29.7(2) . .
O33 Ag9 C1 133.75(19) . .
O35 Ag9 O103 102.87(16) . .
C2 Ag9 O103 93.65(18) . .
O33 Ag9 O103 81.06(16) . .
C1 Ag9 O103 114.44(19) . .
O35 Ag9 Ag21 79.76(11) . .
C2 Ag9 Ag21 71.42(15) . .
O33 Ag9 Ag21 170.96(11) . .
C1 Ag9 Ag21 46.74(15) . .
O103 Ag9 Ag21 107.16(12) . .
O35 Ag9 Ag8 111.06(12) . .
C2 Ag9 Ag8 58.53(15) . .
O33 Ag9 Ag8 91.21(11) . .
C1 Ag9 Ag8 50.70(16) . .
O103 Ag9 Ag8 145.74(12) . .
Ag21 Ag9 Ag8 83.989(18) . .
O35 Ag9 Ag4 159.91(12) . .
C2 Ag9 Ag4 40.99(15) . .
O33 Ag9 Ag4 71.56(11) . .
C1 Ag9 Ag4 65.52(15) . .
O103 Ag9 Ag4 89.93(12) . .
Ag21 Ag9 Ag4 111.497(19) . .
Ag8 Ag9 Ag4 56.148(15) . .
O35 Ag9 Ag10 149.06(12) . .
C2 Ag9 Ag10 41.55(15) . .
O33 Ag9 Ag10 98.18(11) . .
C1 Ag9 Ag10 66.95(16) . .
O103 Ag9 Ag10 52.31(11) . .
Ag21 Ag9 Ag10 89.998(18) . .
Ag8 Ag9 Ag10 96.604(18) . .
Ag4 Ag9 Ag10 50.344(15) . .
C2 Ag10 N1 139.7(2) . .
C2 Ag10 O10 125.8(2) . .
N1 Ag10 O10 92.56(19) . .
C2 Ag10 Ag4 49.54(16) . .
N1 Ag10 Ag4 91.30(14) . .
O10 Ag10 Ag4 174.24(11) . .
C2 Ag10 Ag2 52.86(16) . .
N1 Ag10 Ag2 145.52(14) . .
O10 Ag10 Ag2 76.40(12) . .
Ag4 Ag10 Ag2 98.02(2) . .
C2 Ag10 Ag9 46.00(16) . .
N1 Ag10 Ag9 132.90(14) . .
O10 Ag10 Ag9 115.05(13) . .
Ag4 Ag10 Ag9 64.820(17) . .
Ag2 Ag10 Ag9 80.419(17) . .
O4 Ag11 O25 94.28(15) . .
O4 Ag11 C4 147.78(19) . .
O25 Ag11 C4 115.1(2) . .
O4 Ag11 C3 119.6(2) . .
O25 Ag11 C3 136.0(2) . .
C4 Ag11 C3 28.5(2) . .
O4 Ag11 O105 104.03(16) . .
O25 Ag11 O105 84.17(16) . .
C4 Ag11 O105 92.3(2) . .
C3 Ag11 O105 110.8(2) . .
O4 Ag11 Ag23 79.34(11) . .
O25 Ag11 Ag23 172.42(11) . .
C4 Ag11 Ag23 70.24(16) . .
C3 Ag11 Ag23 47.00(16) . .
O105 Ag11 Ag23 101.27(12) . .
O4 Ag11 Ag5 107.30(11) . .
O25 Ag11 Ag5 93.32(11) . .
C4 Ag11 Ag5 60.50(18) . .
C3 Ag11 Ag5 52.20(17) . .
O105 Ag11 Ag5 148.67(11) . .
Ag23 Ag11 Ag5 84.777(18) . .
O4 Ag11 Ag6 158.27(11) . .
O25 Ag11 Ag6 72.93(11) . .
C4 Ag11 Ag6 42.43(16) . .
C3 Ag11 Ag6 65.58(16) . .
O105 Ag11 Ag6 92.31(12) . .
Ag23 Ag11 Ag6 111.807(19) . .
Ag5 Ag11 Ag6 57.448(15) . .
O4 Ag11 Ag18 149.58(11) . .
O25 Ag11 Ag18 100.58(11) . .
C4 Ag11 Ag18 40.73(17) . .
C3 Ag11 Ag18 64.75(17) . .
O105 Ag11 Ag18 52.08(11) . .
Ag23 Ag11 Ag18 86.965(18) . .
Ag5 Ag11 Ag18 98.230(18) . .
Ag6 Ag11 Ag18 52.019(15) . .
C6 Ag12 O16 138.5(2) . .
C6 Ag12 O19 122.5(2) . .
O16 Ag12 O19 96.32(17) . .
C6 Ag12 O111 101.9(2) . .
O16 Ag12 O111 88.32(18) . .
O19 Ag12 O111 93.61(17) . .
C6 Ag12 Ag15 53.47(18) . .
O16 Ag12 Ag15 85.24(12) . .
O19 Ag12 Ag15 165.25(11) . .
O111 Ag12 Ag15 101.11(13) . .
C6 Ag12 Ag13 50.79(19) . .
O16 Ag12 Ag13 132.44(14) . .
O19 Ag12 Ag13 110.03(11) . .
O111 Ag12 Ag13 52.32(11) . .
Ag15 Ag12 Ag13 78.80(2) . .
C6 Ag12 Ag16 56.9(2) . .
O16 Ag12 Ag16 111.60(13) . .
O19 Ag12 Ag16 93.58(11) . .
O111 Ag12 Ag16 157.89(11) . .
Ag15 Ag12 Ag16 72.332(19) . .
Ag13 Ag12 Ag16 105.61(2) . .
C6 Ag12 Ag7 45.85(18) . .
O16 Ag12 Ag7 169.47(14) . .
O19 Ag12 Ag7 77.13(11) . .
O111 Ag12 Ag7 100.21(12) . .
Ag15 Ag12 Ag7 99.015(19) . .
Ag13 Ag12 Ag7 58.057(16) . .
Ag16 Ag12 Ag7 61.244(16) . .
C6 Ag13 N15 124.9(2) . 4_556
C6 Ag13 O11 132.7(2) . .
N15 Ag13 O11 92.87(19) 4_556 .
C6 Ag13 O111 100.1(2) . .
N15 Ag13 O111 111.82(19) 4_556 .
O11 Ag13 O111 88.63(17) . .
C6 Ag13 Ag20 58.24(17) . .
N15 Ag13 Ag20 110.71(14) 4_556 .
O11 Ag13 Ag20 84.00(12) . .
O111 Ag13 Ag20 137.12(14) . .
C6 Ag13 Ag12 46.49(17) . .
N15 Ag13 Ag12 129.19(14) 4_556 .
O11 Ag13 Ag12 130.32(13) . .
O111 Ag13 Ag12 54.74(12) . .
Ag20 Ag13 Ag12 100.54(2) . .
C6 Ag13 Ag7 50.61(17) . .
N15 Ag13 Ag7 76.24(13) 4_556 .
O11 Ag13 Ag7 161.01(12) . .
O111 Ag13 Ag7 109.76(12) . .
Ag20 Ag13 Ag7 85.403(19) . .
Ag12 Ag13 Ag7 67.245(17) . .
N21 Ag14 O27 90.70(18) . .
N21 Ag14 C4 143.7(2) . .
O27 Ag14 C4 118.4(2) . .
N21 Ag14 O108 109.76(18) . .
O27 Ag14 O108 89.45(16) . .
C4 Ag14 O108 92.8(2) . .
N21 Ag14 Ag6 131.26(14) . .
O27 Ag14 Ag6 77.16(11) . .
C4 Ag14 Ag6 47.80(16) . .
O108 Ag14 Ag6 117.00(12) . .
N21 Ag14 Ag17 79.06(13) . .
O27 Ag14 Ag17 165.09(12) . .
C4 Ag14 Ag17 67.78(16) . .
O108 Ag14 Ag17 104.14(11) . .
Ag6 Ag14 Ag17 101.41(2) . .
N21 Ag14 Ag3 125.04(13) . .
O27 Ag14 Ag3 131.01(12) . .
C4 Ag14 Ag3 51.55(17) . .
O108 Ag14 Ag3 50.04(10) . .
Ag6 Ag14 Ag3 96.276(19) . .
Ag17 Ag14 Ag3 63.816(16) . .
N23 Ag15 C6 123.5(2) 2_554 .
N23 Ag15 O15 91.72(18) 2_554 .
C6 Ag15 O15 126.4(2) . .
N23 Ag15 O106 103.42(18) 2_554 .
C6 Ag15 O106 113.5(2) . .
O15 Ag15 O106 91.96(17) . .
N23 Ag15 Ag12 123.41(13) 2_554 .
C6 Ag15 Ag12 48.07(17) . .
O15 Ag15 Ag12 79.54(12) . .
O106 Ag15 Ag12 132.39(13) . .
N23 Ag15 Ag1 121.63(13) 2_554 .
C6 Ag15 Ag1 65.45(17) . .
O15 Ag15 Ag1 131.72(13) . .
O106 Ag15 Ag1 49.78(11) . .
Ag12 Ag15 Ag1 103.98(2) . .
N23 Ag15 Ag20 80.80(13) 2_554 .
C6 Ag15 Ag20 52.68(17) . .
O15 Ag15 Ag20 167.10(13) . .
O106 Ag15 Ag20 99.97(11) . .
Ag12 Ag15 Ag20 95.75(2) . .
Ag1 Ag15 Ag20 60.981(16) . .
N19 Ag16 O22 91.11(18) 4_456 .
N19 Ag16 C5 154.4(2) 4_456 .
O22 Ag16 C5 111.59(18) . .
N19 Ag16 O104 102.84(18) 4_456 .
O22 Ag16 O104 86.88(15) . .
C5 Ag16 O104 90.54(19) . .
N19 Ag16 C6 128.0(2) 4_456 .
O22 Ag16 C6 138.26(19) . .
C5 Ag16 C6 27.2(2) . .
O104 Ag16 C6 96.29(18) . .
N19 Ag16 Ag1 136.45(14) 4_456 .
O22 Ag16 Ag1 75.56(11) . .
C5 Ag16 Ag1 46.41(14) . .
O104 Ag16 Ag1 117.24(12) . .
C6 Ag16 Ag1 66.02(15) . .
N19 Ag16 Ag12 84.92(14) 4_456 .
O22 Ag16 Ag12 173.54(11) . .
C5 Ag16 Ag12 71.34(14) . .
O104 Ag16 Ag12 98.96(11) . .
C6 Ag16 Ag12 44.21(15) . .
Ag1 Ag16 Ag12 103.90(2) . .
N19 Ag16 Ag7 128.94(13) 4_456 .
O22 Ag16 Ag7 122.44(11) . .
C5 Ag16 Ag7 47.90(14) . .
O104 Ag16 Ag7 49.54(10) . .
C6 Ag16 Ag7 46.75(15) . .
Ag1 Ag16 Ag7 91.755(19) . .
Ag12 Ag16 Ag7 63.903(16) . .
C3 Ag17 O23 142.9(2) . .
C3 Ag17 O5 122.2(2) . .
O23 Ag17 O5 93.20(16) . .
C3 Ag17 O101 99.2(2) . .
O23 Ag17 O101 97.02(17) . .
O5 Ag17 O101 80.58(16) . .
C3 Ag17 Ag5 57.58(19) . .
O23 Ag17 Ag5 85.42(11) . .
O5 Ag17 Ag5 166.77(11) . .
O101 Ag17 Ag5 112.65(12) . .
C3 Ag17 Ag23 47.24(18) . .
O23 Ag17 Ag23 143.47(13) . .
O5 Ag17 Ag23 100.49(11) . .
O101 Ag17 Ag23 53.02(11) . .
Ag5 Ag17 Ag23 88.21(2) . .
C3 Ag17 Ag14 60.14(19) . .
O23 Ag17 Ag14 109.42(13) . .
O5 Ag17 Ag14 96.20(11) . .
O101 Ag17 Ag14 153.52(12) . .
Ag5 Ag17 Ag14 72.001(18) . .
Ag23 Ag17 Ag14 102.60(2) . .
C3 Ag17 Ag3 46.06(19) . .
O23 Ag17 Ag3 162.32(13) . .
O5 Ag17 Ag3 76.20(11) . .
O101 Ag17 Ag3 95.16(12) . .
Ag5 Ag17 Ag3 101.63(2) . .
Ag23 Ag17 Ag3 53.759(16) . .
Ag14 Ag17 Ag3 58.808(16) . .
C4 Ag18 N3 139.3(2) . 4_455
C4 Ag18 O32 130.4(2) . .
N3 Ag18 O32 89.14(18) 4_455 .
C4 Ag18 Ag6 48.82(18) . .
N3 Ag18 Ag6 91.55(14) 4_455 .
O32 Ag18 Ag6 179.03(12) . .
C4 Ag18 Ag3 54.90(18) . .
N3 Ag18 Ag3 145.71(14) 4_455 .
O32 Ag18 Ag3 79.36(12) . .
Ag6 Ag18 Ag3 99.69(2) . .
C4 Ag18 Ag11 45.47(18) . .
N3 Ag18 Ag11 131.02(14) 4_455 .
O32 Ag18 Ag11 117.52(12) . .
Ag6 Ag18 Ag11 62.443(16) . .
Ag3 Ag18 Ag11 82.278(18) . .
N5 Ag19 O1 91.53(17) . .
N5 Ag19 C2 148.5(2) . .
O1 Ag19 C2 114.78(19) . .
N5 Ag19 O107 105.25(18) . .
O1 Ag19 O107 88.96(16) . .
C2 Ag19 O107 92.84(18) . .
N5 Ag19 Ag4 133.76(14) . .
O1 Ag19 Ag4 75.15(11) . .
C2 Ag19 Ag4 47.58(15) . .
O107 Ag19 Ag4 118.25(12) . .
N5 Ag19 Ag22 81.98(13) . .
O1 Ag19 Ag22 170.31(12) . .
C2 Ag19 Ag22 69.52(15) . .
O107 Ag19 Ag22 99.65(11) . .
Ag4 Ag19 Ag22 104.21(2) . .
N5 Ag19 Ag2 127.06(13) . .
O1 Ag19 Ag2 125.87(12) . .
C2 Ag19 Ag2 50.64(15) . .
O107 Ag19 Ag2 48.94(10) . .
Ag4 Ag19 Ag2 94.785(18) . .
Ag22 Ag19 Ag2 63.742(16) . .
N5 Ag19 Ag8 96.33(14) . .
O1 Ag19 Ag8 121.81(12) . .
C2 Ag19 Ag8 55.76(15) . .
O107 Ag19 Ag8 141.99(10) . .
Ag4 Ag19 Ag8 58.439(16) . .
Ag22 Ag19 Ag8 52.408(15) . .
Ag2 Ag19 Ag8 93.112(18) . .
O12 Ag20 C5 149.89(19) . .
O12 Ag20 O100 93.8(2) . 4
C5 Ag20 O100 104.4(2) . 4
O12 Ag20 O30 91.38(16) . .
C5 Ag20 O30 114.27(19) . .
O100 Ag20 O30 82.8(2) 4 .
O12 Ag20 C6 123.0(2) . .
C5 Ag20 C6 27.6(2) . .
O100 Ag20 C6 124.8(2) 4 .
O30 Ag20 C6 129.47(19) . .
O12 Ag20 Ag13 79.14(11) . .
C5 Ag20 Ag13 71.67(15) . .
O100 Ag20 Ag13 113.7(2) 4 .
O30 Ag20 Ag13 161.25(12) . .
C6 Ag20 Ag13 49.02(16) . .
O12 Ag20 Ag15 104.84(12) . .
C5 Ag20 Ag15 60.03(16) . .
O100 Ag20 Ag15 161.2(2) 4 .
O30 Ag20 Ag15 93.92(12) . .
C6 Ag20 Ag15 45.55(15) . .
Ag13 Ag20 Ag15 73.292(18) . .
O12 Ag20 Ag1 153.94(12) . .
C5 Ag20 Ag1 42.75(15) . .
O100 Ag20 Ag1 103.3(2) 4 .
O30 Ag20 Ag1 71.70(11) . .
C6 Ag20 Ag1 61.76(16) . .
Ag13 Ag20 Ag1 110.77(2) . .
Ag15 Ag20 Ag1 58.387(16) . .
O12 Ag20 Ag24 153.60(13) . .
C5 Ag20 Ag24 41.90(15) . .
O100 Ag20 Ag24 63.66(18) 4 .
O30 Ag20 Ag24 98.62(11) . .
C6 Ag20 Ag24 67.65(16) . .
Ag13 Ag20 Ag24 96.90(2) . .
Ag15 Ag20 Ag24 98.81(2) . .
Ag1 Ag20 Ag24 51.681(17) . .
C1 Ag21 N7 138.7(2) . 2_564
C1 Ag21 O36 122.6(2) . .
N7 Ag21 O36 92.72(17) 2_564 .
C1 Ag21 O109 97.6(2) . .
N7 Ag21 O109 106.24(18) 2_564 .
O36 Ag21 O109 85.94(16) . .
C1 Ag21 Ag2 52.82(17) . .
N7 Ag21 Ag2 87.74(14) 2_564 .
O36 Ag21 Ag2 166.54(11) . .
O109 Ag21 Ag2 106.86(11) . .
C1 Ag21 Ag22 45.52(17) . .
N7 Ag21 Ag22 136.71(14) 2_564 .
O36 Ag21 Ag22 118.92(12) . .
O109 Ag21 Ag22 52.88(10) . .
Ag2 Ag21 Ag22 68.214(17) . .
C1 Ag21 Ag9 52.22(17) . .
N7 Ag21 Ag9 125.41(14) 2_564 .
O36 Ag21 Ag9 80.20(11) . .
O109 Ag21 Ag9 126.78(12) . .
Ag2 Ag21 Ag9 88.561(19) . .
Ag22 Ag21 Ag9 90.697(18) . .
C1 Ag22 O13 143.5(2) . .
C1 Ag22 O7 123.2(2) . .
O13 Ag22 O7 91.13(16) . .
C1 Ag22 O109 101.0(2) . .
O13 Ag22 O109 95.68(17) . .
O7 Ag22 O109 81.26(16) . .
C1 Ag22 Ag8 57.73(17) . .
O13 Ag22 Ag8 85.80(12) . .
O7 Ag22 Ag8 161.89(11) . .
O109 Ag22 Ag8 116.79(12) . .
C1 Ag22 Ag21 47.85(17) . .
O13 Ag22 Ag21 143.01(13) . .
O7 Ag22 Ag21 102.74(11) . .
O109 Ag22 Ag21 53.99(11) . .
Ag8 Ag22 Ag21 90.206(19) . .
C1 Ag22 Ag19 60.14(17) . .
O13 Ag22 Ag19 108.42(13) . .
O7 Ag22 Ag19 96.37(11) . .
O109 Ag22 Ag19 155.84(12) . .
Ag8 Ag22 Ag19 67.899(18) . .
Ag21 Ag22 Ag19 103.93(2) . .
C1 Ag22 Ag2 45.18(17) . .
O13 Ag22 Ag2 162.31(13) . .
O7 Ag22 Ag2 78.03(11) . .
O109 Ag22 Ag2 96.42(12) . .
Ag8 Ag22 Ag2 100.127(19) . .
Ag21 Ag22 Ag2 54.227(16) . .
Ag19 Ag22 Ag2 59.776(16) . .
C3 Ag23 N9 140.0(2) . 1_554
C3 Ag23 O3 123.0(2) . .
N9 Ag23 O3 91.39(18) 1_554 .
C3 Ag23 O101 95.7(2) . .
N9 Ag23 O101 107.35(18) 1_554 .
O3 Ag23 O101 85.94(16) . .
C3 Ag23 Ag3 53.57(18) . .
N9 Ag23 Ag3 88.40(14) 1_554 .
O3 Ag23 Ag3 168.05(12) . .
O101 Ag23 Ag3 105.53(11) . .
C3 Ag23 Ag11 52.00(17) . .
N9 Ag23 Ag11 126.33(13) 1_554 .
O3 Ag23 Ag11 80.83(11) . .
O101 Ag23 Ag11 124.67(12) . .
Ag3 Ag23 Ag11 89.67(2) . .
C3 Ag23 Ag17 44.60(17) . .
N9 Ag23 Ag17 137.25(13) 1_554 .
O3 Ag23 Ag17 119.42(12) . .
O101 Ag23 Ag17 52.10(11) . .
Ag3 Ag23 Ag17 67.397(18) . .
Ag11 Ag23 Ag17 89.696(18) . .
C5 Ag24 N11 144.1(2) . .
C5 Ag24 O17 124.7(2) . .
N11 Ag24 O17 90.84(19) . .
C5 Ag24 Ag1 50.04(17) . .
N11 Ag24 Ag1 95.09(14) . .
O17 Ag24 Ag1 172.20(13) . .
C5 Ag24 Ag7 51.69(17) . .
N11 Ag24 Ag7 147.32(16) . .
O17 Ag24 Ag7 79.42(11) . .
Ag1 Ag24 Ag7 98.07(2) . .
C5 Ag24 Ag20 46.13(18) . .
N11 Ag24 Ag20 132.95(16) . .
O17 Ag24 Ag20 108.34(13) . .
Ag1 Ag24 Ag20 63.882(18) . .
Ag7 Ag24 Ag20 79.510(18) . .
C2 C1 Ag22 137.5(5) . .
C2 C1 Ag21 132.7(5) . .
Ag22 C1 Ag21 86.6(2) . .
C2 C1 Ag2 81.6(4) . .
Ag22 C1 Ag2 94.4(2) . .
Ag21 C1 Ag2 78.1(2) . .
C2 C1 Ag9 73.0(4) . .
Ag22 C1 Ag9 139.7(3) . .
Ag21 C1 Ag9 81.0(2) . .
Ag2 C1 Ag9 119.8(3) . .
C2 C1 Ag8 91.0(4) . .
Ag22 C1 Ag8 74.9(2) . .
Ag21 C1 Ag8 122.8(3) . .
Ag2 C1 Ag8 155.0(3) . .
Ag9 C1 Ag8 79.94(19) . .
C1 C2 Ag4 137.2(5) . .
C1 C2 Ag10 140.9(5) . .
Ag4 C2 Ag10 80.2(2) . .
C1 C2 Ag9 77.3(4) . .
Ag4 C2 Ag9 93.0(2) . .
Ag10 C2 Ag9 92.4(2) . .
C1 C2 Ag19 92.5(4) . .
Ag4 C2 Ag19 77.82(19) . .
Ag10 C2 Ag19 110.0(3) . .
Ag9 C2 Ag19 153.5(3) . .
C1 C2 Ag2 69.1(4) . .
Ag4 C2 Ag2 146.6(3) . .
Ag10 C2 Ag2 82.7(2) . .
Ag9 C2 Ag2 116.3(2) . .
Ag19 C2 Ag2 81.44(19) . .
C4 C3 Ag17 136.2(6) . .
C4 C3 Ag23 131.8(6) . .
Ag17 C3 Ag23 88.2(2) . .
C4 C3 Ag3 81.7(5) . .
Ag17 C3 Ag3 93.4(2) . .
Ag23 C3 Ag3 77.0(2) . .
C4 C3 Ag11 73.7(5) . .
Ag17 C3 Ag11 140.1(3) . .
Ag23 C3 Ag11 81.0(2) . .
Ag3 C3 Ag11 120.7(3) . .
C4 C3 Ag5 93.1(5) . .
Ag17 C3 Ag5 75.6(2) . .
Ag23 C3 Ag5 120.8(3) . .
Ag3 C3 Ag5 158.0(3) . .
Ag11 C3 Ag5 77.5(2) . .
C3 C4 Ag18 139.9(6) . .
C3 C4 Ag6 135.7(6) . .
Ag18 C4 Ag6 82.7(2) . .
C3 C4 Ag11 77.8(5) . .
Ag18 C4 Ag11 93.8(2) . .
Ag6 C4 Ag11 90.4(2) . .
C3 C4 Ag14 95.4(5) . .
Ag18 C4 Ag14 105.5(3) . .
Ag6 C4 Ag14 78.5(2) . .
Ag11 C4 Ag14 156.1(3) . .
C3 C4 Ag3 70.5(5) . .
Ag18 C4 Ag3 79.7(2) . .
Ag6 C4 Ag3 147.5(3) . .
Ag11 C4 Ag3 117.7(3) . .
Ag14 C4 Ag3 80.3(2) . .
C6 C5 Ag24 154.8(6) . .
C6 C5 Ag1 124.5(5) . .
Ag24 C5 Ag1 80.6(2) . .
C6 C5 Ag20 87.7(5) . .
Ag24 C5 Ag20 92.0(2) . .
Ag1 C5 Ag20 90.8(2) . .
C6 C5 Ag7 73.8(4) . .
Ag24 C5 Ag7 83.8(2) . .
Ag1 C5 Ag7 149.4(3) . .
Ag20 C5 Ag7 116.0(3) . .
C6 C5 Ag16 80.2(5) . .
Ag24 C5 Ag16 108.5(3) . .
Ag1 C5 Ag16 77.9(2) . .
Ag20 C5 Ag16 154.4(3) . .
Ag7 C5 Ag16 82.3(2) . .
C5 C6 Ag12 151.1(6) . .
C5 C6 Ag13 122.2(6) . .
Ag12 C6 Ag13 82.7(2) . .
C5 C6 Ag15 105.5(5) . .
Ag12 C6 Ag15 78.5(2) . .
Ag13 C6 Ag15 105.0(3) . .
C5 C6 Ag7 77.4(5) . .
Ag12 C6 Ag7 93.9(3) . .
Ag13 C6 Ag7 81.4(2) . .
Ag15 C6 Ag7 169.2(3) . .
C5 C6 Ag16 72.6(5) . .
Ag12 C6 Ag16 78.9(2) . .
Ag13 C6 Ag16 153.7(3) . .
Ag15 C6 Ag16 89.6(2) . .
Ag7 C6 Ag16 81.3(2) . .
C5 C6 Ag20 64.7(5) . .
Ag12 C6 Ag20 143.1(3) . .
Ag13 C6 Ag20 72.7(2) . .
Ag15 C6 Ag20 81.8(2) . .
Ag7 C6 Ag20 108.7(2) . .
Ag16 C6 Ag20 131.9(3) . .
C7 O1 Ag19 126.2(4) . .
C7 O2 Ag4 116.4(4) . .
O1 C7 O2 129.8(6) . .
O1 C7 C8 115.3(6) . .
O2 C7 C8 114.8(6) . .
F11 C8 F12 108.4(6) . .
F11 C8 F13 107.0(6) . .
F12 C8 F13 107.4(6) . .
F11 C8 C7 113.0(6) . .
F12 C8 C7 109.5(6) . .
F13 C8 C7 111.5(6) . .
C9 O3 Ag23 120.1(4) . .
C9 O4 Ag11 127.5(4) . .
O4 C9 O3 131.9(6) . .
O4 C9 C10 115.1(6) . .
O3 C9 C10 113.0(6) . .
F22 C10 F21 108.3(7) . .
F22 C10 F23 106.3(6) . .
F21 C10 F23 106.4(6) . .
F22 C10 C9 110.9(6) . .
F21 C10 C9 113.9(6) . .
F23 C10 C9 110.7(6) . .
C11 O5 Ag17 119.1(4) . .
C11 O6 Ag3 127.0(4) . .
O6 C11 O5 130.1(6) . .
O6 C11 C12 115.5(6) . .
O5 C11 C12 114.3(6) . .
F31 C12 F33 108.3(6) . .
F31 C12 F32 106.8(5) . .
F33 C12 F32 107.1(5) . .
F31 C12 C11 112.1(5) . .
F33 C12 C11 110.9(5) . .
F32 C12 C11 111.3(5) . .
C13 O7 Ag22 116.8(4) . .
C13 O8 Ag2 129.1(4) . .
O8 C13 O7 129.8(6) . .
O8 C13 C14 115.9(6) . .
O7 C13 C14 114.3(6) . .
F42 C14 F41 107.9(6) . .
F42 C14 F43 108.0(6) . .
F41 C14 F43 107.1(5) . .
F42 C14 C13 111.9(5) . .
F41 C14 C13 111.6(6) . .
F43 C14 C13 110.2(6) . .
C15 O9 Ag2 124.0(4) . .
C15 O10 Ag10 123.2(4) . .
O9 C15 O10 130.9(7) . .
O9 C15 C16 114.4(6) . .
O10 C15 C16 114.7(6) . .
F52 C16 F53 106.2(6) . .
F52 C16 F51 109.1(7) . .
F53 C16 F51 104.7(7) . .
F52 C16 C15 114.1(6) . .
F53 C16 C15 113.6(7) . .
F51 C16 C15 108.7(6) . .
C17 O11 Ag13 119.2(4) . .
C17 O12 Ag20 127.9(4) . .
O11 C17 O12 129.3(6) . .
O11 C17 C18 115.1(6) . .
O12 C17 C18 115.6(6) . .
F63 C18 F61 107.9(7) . .
F63 C18 F62 107.0(7) . .
F61 C18 F62 106.1(7) . .
F63 C18 C17 111.1(6) . .
F61 C18 C17 111.7(7) . .
F62 C18 C17 112.7(6) . .
C19 O13 Ag22 120.7(4) . .
C19 O14 Ag8 123.6(5) . .
O14 C19 O13 129.1(7) . .
O14 C19 C20 115.8(6) . .
O13 C19 C20 115.1(6) . .
F71 C20 F73 107.0(8) . .
F71 C20 F72 106.6(9) . .
F73 C20 F72 105.9(7) . .
F71 C20 C19 113.3(6) . .
F73 C20 C19 112.3(7) . .
F72 C20 C19 111.3(6) . .
C21 O15 Ag15 121.1(4) . .
C21 O16 Ag12 121.1(4) . .
O15 C21 O16 130.2(7) . .
O15 C21 C22 115.3(6) . .
O16 C21 C22 114.4(6) . .
F83 C22 F81 106.9(7) . .
F83 C22 F82 107.7(6) . .
F81 C22 F82 108.4(7) . .
F83 C22 C21 113.6(6) . .
F81 C22 C21 108.5(6) . .
F82 C22 C21 111.6(6) . .
C23 O17 Ag24 121.6(4) . .
C23 O18 Ag7 126.4(4) . .
O17 C23 O18 131.5(7) . .
O17 C23 C24 112.9(6) . .
O18 C23 C24 115.5(6) . .
F92 C24 F93 107.9(7) . .
F92 C24 F91 106.8(7) . .
F93 C24 F91 105.7(7) . .
F92 C24 C23 114.4(6) . .
F93 C24 C23 111.2(7) . .
F91 C24 C23 110.4(7) . .
C25 O19 Ag12 122.5(4) . .
C25 O20 Ag7 125.7(4) . .
O20 C25 O19 130.5(6) . .
O20 C25 C26 114.5(6) . .
O19 C25 C26 115.0(6) . .
F103 C26 F101 108.6(6) . .
F103 C26 F102 108.2(6) . .
F101 C26 F102 106.5(6) . .
F103 C26 C25 112.5(6) . .
F101 C26 C25 110.1(6) . .
F102 C26 C25 110.7(6) . .
C27 O21 Ag1 117.5(4) . .
C27 O22 Ag16 123.9(4) . .
O21 C27 O22 132.1(7) . .
O21 C27 C28 114.5(6) . .
O22 C27 C28 113.3(6) . .
F113 C28 F112 106.7(6) . .
F113 C28 F111 104.5(6) . .
F112 C28 F111 107.2(6) . .
F113 C28 C27 115.1(6) . .
F112 C28 C27 113.8(6) . .
F111 C28 C27 108.9(6) . .
C29 O23 Ag17 120.8(4) . .
C29 O24 Ag5 122.5(4) . .
O24 C29 O23 130.9(7) . .
O24 C29 C30 115.4(6) . .
O23 C29 C30 113.7(6) . .
F123 C30 F121 107.9(8) . .
F123 C30 F122 106.1(7) . .
F121 C30 F122 103.8(7) . .
F123 C30 C29 112.6(6) . .
F121 C30 C29 112.1(7) . .
F122 C30 C29 113.6(7) . .
C31 O25 Ag11 124.9(4) . .
C31 O26 Ag6 120.8(4) . .
O26 C31 O25 130.5(6) . .
O26 C31 C32 115.7(6) . .
O25 C31 C32 113.8(6) . .
F131 C32 F132 107.4(5) . .
F131 C32 F133 107.1(5) . .
F132 C32 F133 108.9(5) . .
F131 C32 C31 110.1(5) . .
F132 C32 C31 111.8(5) . .
F133 C32 C31 111.2(5) . .
C33 O27 Ag14 124.7(4) . .
C33 O28 Ag6 119.6(4) . .
O27 C33 O28 129.7(7) . .
O27 C33 C34 116.3(6) . .
O28 C33 C34 113.9(6) . .
F142 C34 F141 108.7(6) . .
F142 C34 F143 107.1(6) . .
F141 C34 F143 105.4(6) . .
F142 C34 C33 112.6(6) . .
F141 C34 C33 110.2(6) . .
F143 C34 C33 112.6(6) . .
C35 O29 Ag1 119.2(4) . .
C35 O30 Ag20 122.7(4) . .
O29 C35 O30 130.4(6) . .
O29 C35 C36 114.6(6) . .
O30 C35 C36 115.1(6) . .
F153 C36 F151 107.4(5) . .
F153 C36 F152 107.2(5) . .
F151 C36 F152 107.2(6) . .
F153 C36 C35 112.3(5) . .
F151 C36 C35 110.9(5) . .
F152 C36 C35 111.6(5) . .
C37 O31 Ag3 125.1(4) . .
C37 O32 Ag18 120.4(5) . .
O31 C37 O32 131.4(7) . .
O31 C37 C38 113.8(6) . .
O32 C37 C38 114.7(7) . .
F161 C38 F163 106.9(7) . .
F161 C38 F162 105.7(8) . .
F163 C38 F162 103.8(6) . .
F161 C38 C37 110.5(7) . .
F163 C38 C37 114.5(6) . .
F162 C38 C37 114.6(7) . .
C39 O33 Ag9 124.2(4) . .
C39 O34 Ag4 122.6(4) . .
O34 C39 O33 129.5(6) . .
O34 C39 C40 115.2(6) . .
O33 C39 C40 115.2(6) . .
F172 C40 F173 108.0(6) . .
F172 C40 F171 107.4(6) . .
F173 C40 F171 107.8(5) . .
F172 C40 C39 110.9(5) . .
F173 C40 C39 111.2(6) . .
F171 C40 C39 111.5(6) . .
C41 O35 Ag9 127.4(4) . .
C41 O36 Ag21 120.6(4) . .
O35 C41 O36 130.9(6) . .
O35 C41 C42 115.4(6) . .
O36 C41 C42 113.5(6) . .
F183 C42 F181 107.0(6) . .
F183 C42 F182 106.6(6) . .
F181 C42 F182 106.3(6) . .
F183 C42 C41 114.0(6) . .
F181 C42 C41 111.3(6) . .
F182 C42 C41 111.1(6) . .
C105 O100 Ag20 158.5(6) . 4_454
C101 N1 C102 118.2(6) . .
C101 N1 Ag10 121.6(4) . .
C102 N1 Ag10 120.2(5) . .
C101 C100 C104 117.5(6) . .
C101 C100 C105 122.4(6) . .
C104 C100 C105 120.1(6) . .
N1 C101 C100 124.4(6) . .
N1 C102 C103 121.5(6) . .
C104 C103 C102 120.0(6) . .
C103 C104 C100 118.5(6) . .
O100 C105 N2 118.3(7) . .
O100 C105 C100 122.7(7) . .
N2 C105 C100 119.0(6) . .
C111 O101 Ag17 149.8(5) . .
C111 O101 Ag23 133.0(4) . .
Ag17 O101 Ag23 74.88(13) . .
C107 C108 C109 119.7(6) . .
C107 C106 C110 117.8(6) . .
C107 C106 C111 120.9(6) . .
C110 C106 C111 121.3(6) . .
C108 C107 C106 119.2(6) . .
N3 C109 C108 121.7(6) . .
C110 N3 C109 117.9(6) . .
C110 N3 Ag18 119.2(4) . 4_554
C109 N3 Ag18 122.8(5) . 4_554
N3 C110 C106 123.6(6) . .
O101 C111 N4 120.5(6) . .
O101 C111 C106 121.1(6) . .
N4 C111 C106 118.4(6) . .
C117 O102 Ag5 132.5(4) . 1_554
C117 O102 Ag6 148.6(5) . 1_554
Ag5 O102 Ag6 77.05(14) 1_554 1_554
C114 N5 C113 116.8(6) . .
C114 N5 Ag19 119.5(5) . .
C113 N5 Ag19 122.6(4) . .
C113 C112 C116 117.4(6) . .
C113 C112 C117 123.4(6) . .
C116 C112 C117 119.2(6) . .
N5 C113 C112 124.4(6) . .
N5 C114 C115 123.2(7) . .
C114 C115 C116 118.2(7) . .
C112 C116 C115 119.9(7) . .
O102 C117 N6 122.0(6) . .
O102 C117 C112 119.8(6) . .
N6 C117 C112 118.2(6) . .
C123 O103 Ag9 142.7(5) . .
C120 N7 C119 116.8(6) . .
C120 N7 Ag21 119.8(4) . 2_565
C119 N7 Ag21 123.1(5) . 2_565
C119 C118 C122 117.8(6) . .
C119 C118 C123 122.3(6) . .
C122 C118 C123 119.9(6) . .
N7 C119 C118 124.4(6) . .
N7 C120 C121 122.9(7) . .
C120 C121 C122 120.2(7) . .
C121 C122 C118 117.8(7) . .
O103 C123 N8 120.3(6) . .
O103 C123 C118 121.1(6) . .
N8 C123 C118 118.7(6) . .
C129 O104 Ag7 143.9(5) . .
C129 O104 Ag16 132.7(4) . .
Ag7 O104 Ag16 79.40(14) . .
C126 N9 C125 116.4(6) . .
C126 N9 Ag23 120.5(5) . 1_556
C125 N9 Ag23 123.2(5) . 1_556
C128 C124 C125 118.3(6) . .
C128 C124 C129 120.4(6) . .
C125 C124 C129 121.3(6) . .
N9 C125 C124 124.0(6) . .
N9 C126 C127 123.6(7) . .
C126 C127 C128 118.9(7) . .
C124 C128 C127 118.8(7) . .
O104 C129 N10 120.8(6) . .
O104 C129 C124 120.5(6) . .
N10 C129 C124 118.6(6) . .
C135 O105 Ag11 146.6(4) . .
C132 N11 C131 117.0(6) . .
C132 N11 Ag24 121.6(4) . .
C131 N11 Ag24 121.3(5) . .
C131 C130 C134 117.7(6) . .
C131 C130 C135 121.5(6) . .
C134 C130 C135 120.9(6) . .
N11 C131 C130 124.5(6) . .
N11 C132 C133 122.5(6) . .
C134 C133 C132 120.1(7) . .
C133 C134 C130 118.3(6) . .
O105 C135 N12 121.0(6) . .
O105 C135 C130 121.1(6) . .
N12 C135 C130 117.9(6) . .
C141 O106 Ag1 145.0(5) . .
C141 O106 Ag15 133.5(4) . .
Ag1 O106 Ag15 80.27(14) . .
C138 N13 C137 118.3(6) . .
C138 N13 Ag8 120.4(4) . 4_455
C137 N13 Ag8 120.6(4) . 4_455
C140 C136 C137 119.4(6) . .
C140 C136 C141 118.8(6) . .
C137 C136 C141 121.8(6) . .
N13 C137 C136 121.6(6) . .
N13 C138 C139 122.4(7) . .
C140 C139 C138 119.5(7) . .
C136 C140 C139 118.6(7) . .
O106 C141 N14 122.0(6) . .
O106 C141 C136 120.0(6) . .
N14 C141 C136 117.9(6) . .
C147 O107 Ag2 140.3(4) . .
C147 O107 Ag19 136.0(4) . .
Ag2 O107 Ag19 80.85(13) . .
C144 N15 C143 118.3(6) . .
C144 N15 Ag13 119.1(5) . 4_453
C143 N15 Ag13 120.9(4) . 4_453
C143 C142 C146 117.3(6) . .
C143 C142 C147 123.3(6) . .
C146 C142 C147 119.4(6) . .
N15 C143 C142 122.9(6) . .
N15 C144 C145 122.7(7) . .
C146 C145 C144 119.0(7) . .
C145 C146 C142 119.6(7) . .
O107 C147 N16 121.9(6) . .
O107 C147 C142 120.4(6) . .
N16 C147 C142 117.7(6) . .
C153 O108 Ag3 147.7(4) . .
C153 O108 Ag14 133.0(4) . .
Ag3 O108 Ag14 79.20(13) . .
C150 N17 C149 117.3(6) . .
C150 N17 Ag5 120.2(4) . 4_454
C149 N17 Ag5 121.6(4) . 4_454
C152 C148 C149 118.6(6) . .
C152 C148 C153 118.3(6) . .
C149 C148 C153 123.0(6) . .
N17 C149 C148 123.4(6) . .
N17 C150 C151 123.6(7) . .
C150 C151 C152 118.8(7) . .
C148 C152 C151 118.3(7) . .
O108 C153 N18 121.6(6) . .
O108 C153 C148 120.6(6) . .
N18 C153 C148 117.8(6) . .
C159 O109 Ag22 148.2(5) . .
C159 O109 Ag21 133.4(4) . .
Ag22 O109 Ag21 73.13(12) . .
C156 N19 C155 117.7(6) . .
C156 N19 Ag16 120.0(4) . 4_553
C155 N19 Ag16 122.3(4) . 4_553
C158 C154 C155 116.9(6) . .
C158 C154 C159 120.8(6) . .
C155 C154 C159 122.3(6) . .
N19 C155 C154 124.2(6) . .
N19 C156 C157 122.1(7) . .
C158 C157 C156 119.2(7) . .
C157 C158 C154 120.0(6) . .
O109 C159 N20 121.7(6) . .
O109 C159 C154 119.3(6) . .
N20 C159 C154 119.0(6) . .
C171 O111 Ag13 134.7(5) . .
C171 O111 Ag12 152.1(5) . .
Ag13 O111 Ag12 72.94(13) . .
C168 N23 C167 117.1(6) . .
C168 N23 Ag15 120.7(5) . 2
C167 N23 Ag15 121.8(4) . 2
C167 C166 C170 117.2(6) . .
C167 C166 C171 124.1(6) . .
C170 C166 C171 118.6(6) . .
N23 C167 C166 123.7(6) . .
N23 C168 C169 123.3(7) . .
C170 C169 C168 118.7(7) . .
C169 C170 C166 119.9(7) . .
O111 C171 N24 121.6(6) . .
O111 C171 C166 120.8(6) . .
N24 C171 C166 117.6(6) . .
C165 O110 Ag8 133.2(4) . .
C165 O110 Ag4 147.3(5) . .
Ag8 O110 Ag4 78.01(14) . .
C162 N21 C161 116.6(6) . .
C162 N21 Ag14 118.2(4) . .
C161 N21 Ag14 123.1(4) . .
C161 C160 C164 118.4(6) . .
C161 C160 C165 123.2(6) . .
C164 C160 C165 118.3(6) . .
N21 C161 C160 123.7(6) . .
N21 C162 C163 123.9(6) . .
C162 C163 C164 118.5(7) . .
C160 C164 C163 118.8(7) . .
O110 C165 N22 121.5(6) . .
O110 C165 C160 119.5(6) . .
N22 C165 C160 119.0(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C5 2.194(6) .
Ag1 O21 2.275(5) .
Ag1 O29 2.337(4) .
Ag1 O106 2.438(5) .
Ag1 Ag24 2.8240(8) .
Ag1 Ag16 2.9618(7) .
Ag1 Ag15 3.1475(7) .
Ag1 Ag20 3.2319(7) .
Ag2 O9 2.238(5) .
Ag2 C1 2.361(6) .
Ag2 O8 2.368(4) .
Ag2 O107 2.441(4) .
Ag2 C2 2.499(6) .
Ag2 Ag21 2.8988(7) .
Ag2 Ag10 3.1096(7) .
Ag2 Ag19 3.1965(7) .
Ag2 Ag22 3.3177(7) .
Ag3 O31 2.252(5) .
Ag3 O6 2.334(4) .
Ag3 C3 2.384(7) .
Ag3 O108 2.458(4) .
Ag3 C4 2.503(7) .
Ag3 Ag23 2.8875(7) .
Ag3 Ag18 3.0102(7) .
Ag3 Ag14 3.1507(7) .
Ag3 Ag17 3.3052(7) .
Ag4 C2 2.173(6) .
Ag4 O2 2.278(5) .
Ag4 O34 2.312(4) .
Ag4 O110 2.475(5) .
Ag4 Ag10 2.8137(7) .
Ag4 Ag19 2.8769(7) .
Ag4 Ag8 3.0437(7) .
Ag4 Ag9 3.3075(7) .
Ag5 N17 2.305(5) 4
Ag5 O24 2.380(5) .
Ag5 O102 2.394(5) 1_556
Ag5 C3 2.490(7) .
Ag5 Ag17 2.8567(7) .
Ag5 Ag6 3.0425(7) .
Ag5 Ag11 3.0764(7) .
Ag6 C4 2.190(7) .
Ag6 O28 2.270(5) .
Ag6 O26 2.340(4) .
Ag6 O102 2.489(5) 1_556
Ag6 Ag18 2.8865(7) .
Ag6 Ag14 2.8976(7) .
Ag6 Ag11 3.2467(7) .
Ag7 O18 2.251(5) .
Ag7 O20 2.325(4) .
Ag7 C6 2.390(7) .
Ag7 C5 2.429(6) .
Ag7 O104 2.511(5) .
Ag7 Ag13 3.0584(7) .
Ag7 Ag24 3.0777(7) .
Ag7 Ag16 3.2445(7) .
Ag7 Ag12 3.3236(7) .
Ag8 N13 2.309(6) 4_554
Ag8 O110 2.358(5) .
Ag8 O14 2.366(5) .
Ag8 C1 2.479(6) .
Ag8 Ag22 2.8307(7) .
Ag8 Ag9 3.1538(7) .
Ag8 Ag19 3.3100(7) .
Ag9 O35 2.249(5) .
Ag9 C2 2.382(6) .
Ag9 O33 2.394(4) .
Ag9 C1 2.430(7) .
Ag9 O103 2.470(4) .
Ag9 Ag21 3.0376(7) .
Ag9 Ag10 3.3079(7) .
Ag10 C2 2.196(6) .
Ag10 N1 2.283(5) .
Ag10 O10 2.342(5) .
Ag11 O4 2.261(4) .
Ag11 O25 2.366(4) .
Ag11 C4 2.382(7) .
Ag11 C3 2.425(7) .
Ag11 O105 2.444(5) .
Ag11 Ag23 3.0395(7) .
Ag11 Ag18 3.3334(7) .
Ag12 C6 2.151(7) .
Ag12 O16 2.257(5) .
Ag12 O19 2.330(4) .
Ag12 O111 2.512(5) .
Ag12 Ag15 2.8325(7) .
Ag12 Ag13 2.9414(7) .
Ag12 Ag16 3.0262(7) .
Ag13 C6 2.298(7) .
Ag13 N15 2.303(5) 4_556
Ag13 O11 2.321(5) .
Ag13 O111 2.435(5) .
Ag13 Ag20 2.9066(7) .
Ag14 N21 2.259(5) .
Ag14 O27 2.377(5) .
Ag14 C4 2.383(7) .
Ag14 O108 2.484(5) .
Ag14 Ag17 3.1021(7) .
Ag15 N23 2.277(5) 2_554
Ag15 C6 2.323(7) .
Ag15 O15 2.380(5) .
Ag15 O106 2.445(5) .
Ag15 Ag20 3.2209(8) .
Ag16 N19 2.261(5) 4_456
Ag16 O22 2.389(5) .
Ag16 C5 2.501(7) .
Ag16 O104 2.567(5) .
Ag16 C6 2.584(7) .
Ag17 C3 2.152(7) .
Ag17 O23 2.242(5) .
Ag17 O5 2.349(4) .
Ag17 O101 2.504(5) .
Ag17 Ag23 3.0638(8) .
Ag18 C4 2.180(7) .
Ag18 N3 2.264(6) 4_455
Ag18 O32 2.367(5) .
Ag19 N5 2.250(5) .
Ag19 O1 2.399(5) .
Ag19 C2 2.399(6) .
Ag19 O107 2.488(5) .
Ag19 Ag22 3.0843(7) .
Ag20 O12 2.263(5) .
Ag20 C5 2.342(7) .
Ag20 O100 2.372(6) 4
Ag20 O30 2.400(5) .
Ag20 C6 2.588(7) .
Ag20 Ag24 3.2471(8) .
Ag21 C1 2.239(6) .
Ag21 N7 2.269(5) 2_564
Ag21 O36 2.374(5) .
Ag21 O109 2.549(5) .
Ag21 Ag22 3.0153(7) .
Ag22 C1 2.155(7) .
Ag22 O13 2.241(5) .
Ag22 O7 2.341(4) .
Ag22 O109 2.513(5) .
Ag23 C3 2.251(7) .
Ag23 N9 2.262(6) 1_554
Ag23 O3 2.363(5) .
Ag23 O101 2.535(5) .
Ag24 C5 2.170(6) .
Ag24 N11 2.237(6) .
Ag24 O17 2.340(5) .
C1 C2 1.235(9) .
C3 C4 1.183(9) .
C5 C6 1.198(9) .
O1 C7 1.234(8) .
O2 C7 1.247(8) .
C7 C8 1.556(10) .
C8 F11 1.312(9) .
C8 F12 1.326(8) .
C8 F13 1.342(8) .
O3 C9 1.244(8) .
O4 C9 1.223(8) .
C9 C10 1.562(10) .
C10 F22 1.322(9) .
C10 F21 1.326(8) .
C10 F23 1.342(9) .
O5 C11 1.255(7) .
O6 C11 1.239(7) .
C11 C12 1.539(9) .
C12 F31 1.325(7) .
C12 F33 1.326(8) .
C12 F32 1.335(8) .
O7 C13 1.257(8) .
O8 C13 1.236(7) .
C13 C14 1.536(9) .
C14 F42 1.318(8) .
C14 F41 1.332(8) .
C14 F43 1.333(8) .
O9 C15 1.228(8) .
O10 C15 1.260(8) .
C15 C16 1.530(10) .
C16 F52 1.313(8) .
C16 F53 1.320(10) .
C16 F51 1.347(10) .
O11 C17 1.232(8) .
O12 C17 1.252(8) .
C17 C18 1.533(9) .
C18 F63 1.314(9) .
C18 F61 1.317(10) .
C18 F62 1.320(9) .
O13 C19 1.244(8) .
O14 C19 1.227(8) .
C19 C20 1.551(10) .
C20 F71 1.266(10) .
C20 F73 1.303(9) .
C20 F72 1.305(10) .
O15 C21 1.234(8) .
O16 C21 1.235(8) .
C21 C22 1.559(10) .
C22 F83 1.322(9) .
C22 F81 1.324(9) .
C22 F82 1.330(9) .
O17 C23 1.230(8) .
O18 C23 1.235(8) .
C23 C24 1.540(10) .
C24 F92 1.319(9) .
C24 F93 1.340(9) .
C24 F91 1.346(10) .
O19 C25 1.257(8) .
O20 C25 1.237(8) .
C25 C26 1.551(9) .
C26 F103 1.319(8) .
C26 F101 1.323(9) .
C26 F102 1.333(8) .
O21 C27 1.229(8) .
O22 C27 1.258(8) .
C27 C28 1.528(10) .
C28 F113 1.317(9) .
C28 F112 1.327(8) .
C28 F111 1.363(9) .
O23 C29 1.254(8) .
O24 C29 1.220(8) .
C29 C30 1.543(10) .
C30 F123 1.298(9) .
C30 F121 1.298(9) .
C30 F122 1.318(9) .
O25 C31 1.244(7) .
O26 C31 1.233(8) .
C31 C32 1.545(9) .
C32 F131 1.320(8) .
C32 F132 1.322(8) .
C32 F133 1.340(7) .
O27 C33 1.237(8) .
O28 C33 1.242(8) .
C33 C34 1.538(10) .
C34 F142 1.321(8) .
C34 F141 1.323(8) .
C34 F143 1.336(9) .
O29 C35 1.236(8) .
O30 C35 1.248(8) .
C35 C36 1.534(9) .
C36 F153 1.322(7) .
C36 F151 1.328(8) .
C36 F152 1.335(7) .
O31 C37 1.227(8) .
O32 C37 1.247(8) .
C37 C38 1.516(10) .
C38 F161 1.288(10) .
C38 F163 1.311(9) .
C38 F162 1.313(9) .
O33 C39 1.241(8) .
O34 C39 1.231(8) .
C39 C40 1.546(9) .
C40 F172 1.310(8) .
C40 F173 1.334(8) .
C40 F171 1.336(8) .
O35 C41 1.232(8) .
O36 C41 1.242(8) .
C41 C42 1.545(9) .
C42 F183 1.327(8) .
C42 F181 1.337(8) .
C42 F182 1.340(9) .
O100 C105 1.176(8) .
O100 Ag20 2.372(6) 4_454
N1 C101 1.322(8) .
N1 C102 1.339(8) .
N2 C105 1.259(10) .
C100 C101 1.384(9) .
C100 C104 1.395(9) .
C100 C105 1.491(9) .
C102 C103 1.390(9) .
C103 C104 1.377(9) .
O101 C111 1.233(8) .
C108 C107 1.366(10) .
C108 C109 1.387(9) .
N4 C111 1.320(8) .
C106 C107 1.375(9) .
C106 C110 1.386(9) .
C106 C111 1.489(9) .
C109 N3 1.336(8) .
N3 C110 1.332(8) .
N3 Ag18 2.264(6) 4_554
O102 C117 1.237(8) .
O102 Ag5 2.394(5) 1_554
O102 Ag6 2.489(5) 1_554
N5 C114 1.339(9) .
N5 C113 1.352(8) .
N6 C117 1.341(8) .
C112 C113 1.374(9) .
C112 C116 1.380(10) .
C112 C117 1.491(9) .
C114 C115 1.382(11) .
C115 C116 1.390(11) .
O103 C123 1.235(8) .
N7 C120 1.332(8) .
N7 C119 1.334(8) .
N7 Ag21 2.269(5) 2_565
N8 C123 1.322(9) .
C118 C119 1.378(9) .
C118 C122 1.385(10) .
C118 C123 1.484(9) .
C120 C121 1.361(10) .
C121 C122 1.383(10) .
O104 C129 1.238(8) .
N9 C126 1.332(9) .
N9 C125 1.345(8) .
N9 Ag23 2.262(6) 1_556
N10 C129 1.330(8) .
C124 C128 1.372(9) .
C124 C125 1.373(9) .
C124 C129 1.506(9) .
C126 C127 1.370(10) .
C127 C128 1.380(10) .
O105 C135 1.223(8) .
N11 C132 1.322(9) .
N11 C131 1.346(8) .
N12 C135 1.323(8) .
C130 C131 1.373(9) .
C130 C134 1.387(9) .
C130 C135 1.498(9) .
C132 C133 1.384(9) .
C133 C134 1.371(9) .
O106 C141 1.224(8) .
N13 C138 1.339(9) .
N13 C137 1.365(8) .
N13 Ag8 2.309(6) 4_455
N14 C141 1.343(9) .
C136 C140 1.380(9) .
C136 C137 1.397(9) .
C136 C141 1.507(9) .
C138 C139 1.389(10) .
C139 C140 1.387(10) .
O107 C147 1.228(7) .
N15 C144 1.327(9) .
N15 C143 1.353(8) .
N15 Ag13 2.303(5) 4_453
N16 C147 1.341(8) .
C142 C143 1.386(9) .
C142 C146 1.399(10) .
C142 C147 1.500(9) .
C144 C145 1.381(10) .
C145 C146 1.373(10) .
O108 C153 1.229(8) .
N17 C150 1.324(9) .
N17 C149 1.332(8) .
N17 Ag5 2.305(5) 4_454
N18 C153 1.346(8) .
C148 C152 1.379(9) .
C148 C149 1.383(9) .
C148 C153 1.514(9) .
C150 C151 1.377(10) .
C151 C152 1.384(10) .
O109 C159 1.244(7) .
N19 C156 1.330(8) .
N19 C155 1.354(8) .
N19 Ag16 2.261(5) 4_553
N20 C159 1.310(8) .
C154 C158 1.388(9) .
C154 C155 1.389(9) .
C154 C159 1.481(9) .
C156 C157 1.402(9) .
C157 C158 1.378(9) .
O111 C171 1.216(8) .
N23 C168 1.320(9) .
N23 C167 1.348(8) .
N23 Ag15 2.277(5) 2
N24 C171 1.342(9) .
C166 C167 1.378(9) .
C166 C170 1.387(10) .
C166 C171 1.488(9) .
C168 C169 1.386(10) .
C169 C170 1.357(11) .
O110 C165 1.241(8) .
N21 C162 1.332(8) .
N21 C161 1.343(8) .
N22 C165 1.330(8) .
C160 C161 1.378(9) .
C160 C164 1.381(10) .
C160 C165 1.501(9) .
C162 C163 1.380(10) .
C163 C164 1.382(10) .
