#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:03:41 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180024 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/18/7031849.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7031849
loop_
_publ_author_name
'Sheikh, Javeed Ahmad'
'Goswami, Soumyabrata'
'Konar, Sanjit'
_publ_section_title
;
 Modulating the magnetic properties by structural modification in a family
 of Co-Ln (Ln = Gd, Dy) molecular aggregates.
;
_journal_issue                   39
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              14577
_journal_page_last               14585
_journal_paper_doi               10.1039/c4dt01791a
_journal_volume                  43
_journal_year                    2014
_chemical_formula_moiety         'C74 H136 Co5 Dy3 N2 O33, 2(O), 2(C H3)'
_chemical_formula_sum            'C76 H142 Co5 Dy3 N2 O35'
_chemical_formula_weight         2426.07
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 96.0392(15)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.1684(7)
_cell_length_b                   27.6583(16)
_cell_length_c                   25.4178(13)
_cell_measurement_reflns_used    8721
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      29.55
_cell_measurement_theta_min      2.78
_cell_volume                     9905.3(9)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      110(2)
_diffrn_measured_fraction_theta_full 1
_diffrn_measured_fraction_theta_max 1
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0199
_diffrn_reflns_av_sigmaI/netI    0.0269
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            8721
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.18
_exptl_absorpt_coefficient_mu    3.125
_exptl_absorpt_correction_T_max  0.404
_exptl_absorpt_correction_T_min  0.291
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   multi-scan
_exptl_crystal_colour            Purple
_exptl_crystal_density_diffrn    1.627
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             4900
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.34
_exptl_crystal_size_min          0.29
_platon_squeeze_details
; 
 ? 
;
_refine_diff_density_max         2.469
_refine_diff_density_min         -1.478
_refine_diff_density_rms         0.171
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.103
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     498
_refine_ls_number_reflns         8721
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.103
_refine_ls_R_factor_all          0.0587
_refine_ls_R_factor_gt           0.0513
_refine_ls_shift/su_max          0.044
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0551P)²+4.3761P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1500
_refine_ls_wR_factor_ref         0.1533
_reflns_number_gt                7648
_reflns_number_total             8721
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt01791a2.cif
_cod_data_source_block           complex2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 7031848--7031851.cif.
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7031849
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.7878(6) 0.2058(3) 0.3126(3) 0.0345(18) Uani 1 1 d .
C2 C 0.8577(11) 0.2438(6) 0.3341(6) 0.113(3) Uani 1 1 d .
C3 C 0.9323(10) 0.2472(5) 0.2996(6) 0.113(3) Uani 1 1 d .
H3A H 0.9819 0.2691 0.3153 0.169 Uiso 1 1 calc R
H3B H 0.9060 0.2598 0.2651 0.169 Uiso 1 1 calc R
H3C H 0.9594 0.2151 0.2951 0.169 Uiso 1 1 calc R
C4 C 0.8887(10) 0.2380(5) 0.3896(5) 0.113(3) Uani 1 1 d .
H4A H 0.9048 0.2040 0.3969 0.169 Uiso 1 1 calc R
H4B H 0.8376 0.2478 0.4105 0.169 Uiso 1 1 calc R
H4C H 0.9447 0.2582 0.3991 0.169 Uiso 1 1 calc R
C5 C 0.8072(10) 0.2933(5) 0.3344(6) 0.113(3) Uani 1 1 d .
H5A H 0.7663 0.2941 0.3632 0.169 Uiso 1 1 calc R
H5B H 0.7685 0.2982 0.3006 0.169 Uiso 1 1 calc R
H5C H 0.8547 0.3191 0.3397 0.169 Uiso 1 1 calc R
C6 C 0.7819(5) 0.0668(3) 0.3921(3) 0.0347(19) Uani 1 1 d .
C7 C 0.8228(8) 0.0500(5) 0.4463(4) 0.0785(18) Uani 1 1 d .
C8 C 0.7526(7) 0.0457(4) 0.4845(3) 0.066(3) Uani 1 1 d .
H8A H 0.7832 0.0325 0.5178 0.100 Uiso 1 1 calc R
H8B H 0.7014 0.0240 0.4703 0.100 Uiso 1 1 calc R
H8C H 0.7263 0.0776 0.4910 0.100 Uiso 1 1 calc R
C9 C 0.8514(8) -0.0053(5) 0.4398(4) 0.0785(18) Uani 1 1 d .
H9A H 0.8939 -0.0082 0.4119 0.118 Uiso 1 1 calc R
H9B H 0.7941 -0.0245 0.4302 0.118 Uiso 1 1 calc R
H9C H 0.8837 -0.0172 0.4733 0.118 Uiso 1 1 calc R
C10 C 0.9087(8) 0.0750(5) 0.4629(4) 0.0785(18) Uani 1 1 d .
H10A H 0.8943 0.1087 0.4709 0.118 Uiso 1 1 calc R
H10B H 0.9505 0.0740 0.4346 0.118 Uiso 1 1 calc R
H10C H 0.9402 0.0594 0.4946 0.118 Uiso 1 1 calc R
C11 C 0.4469(5) -0.0044(3) 0.3447(3) 0.0253(16) Uani 1 1 d .
C12 C 0.4750(9) -0.0472(6) 0.3797(7) 0.121(3) Uani 1 1 d .
C13 C 0.4001(9) -0.0718(6) 0.3990(6) 0.121(3) Uani 1 1 d .
H13A H 0.3784 -0.0977 0.3744 0.181 Uiso 1 1 calc R
H13B H 0.3478 -0.0493 0.4025 0.181 Uiso 1 1 calc R
H13C H 0.4215 -0.0857 0.4337 0.181 Uiso 1 1 calc R
C14 C 0.5780(9) -0.0500(6) 0.3907(6) 0.121(3) Uani 1 1 d .
H14A H 0.5948 -0.0766 0.4154 0.181 Uiso 1 1 calc R
H14B H 0.6023 -0.0195 0.4065 0.181 Uiso 1 1 calc R
H14C H 0.6061 -0.0558 0.3577 0.181 Uiso 1 1 calc R
C15 C 0.4763(9) -0.0196(5) 0.4436(6) 0.121(3) Uani 1 1 d .
H15A H 0.4170 -0.0018 0.4456 0.181 Uiso 1 1 calc R
H15B H 0.5301 0.0028 0.4491 0.181 Uiso 1 1 calc R
H15C H 0.4826 -0.0447 0.4710 0.181 Uiso 1 1 calc R
C16 C 0.2832(5) 0.0004(2) 0.2331(3) 0.0248(16) Uani 1 1 d .
H16A H 0.3132 -0.0257 0.2558 0.030 Uiso 1 1 calc R
H16B H 0.2838 -0.0093 0.1957 0.030 Uiso 1 1 calc R
C17 C 0.1813(5) 0.0089(3) 0.2457(3) 0.0294(17) Uani 1 1 d .
H17A H 0.1480 0.0305 0.2189 0.035 Uiso 1 1 calc R
H17B H 0.1466 -0.0223 0.2450 0.035 Uiso 1 1 calc R
C18 C 0.1113(5) 0.0713(3) 0.3017(3) 0.0285(17) Uani 1 1 d .
H18A H 0.1046 0.0790 0.3391 0.034 Uiso 1 1 calc R
H18B H 0.0488 0.0602 0.2849 0.034 Uiso 1 1 calc R
C19 C 0.1415(5) 0.1165(3) 0.2735(3) 0.0286(17) Uani 1 1 d .
H19A H 0.1086 0.1174 0.2372 0.034 Uiso 1 1 calc R
H19B H 0.1226 0.1455 0.2926 0.034 Uiso 1 1 calc R
C20 C 0.1707(5) -0.0056(3) 0.3400(3) 0.0287(17) Uani 1 1 d .
H20A H 0.1895 0.0088 0.3752 0.034 Uiso 1 1 calc R
H20B H 0.2143 -0.0329 0.3354 0.034 Uiso 1 1 calc R
C21 C 0.0700(5) -0.0256(3) 0.3393(3) 0.0382(19) Uani 1 1 d .
H21A H 0.0286 -0.0009 0.3533 0.046 Uiso 1 1 calc R
H21B H 0.0443 -0.0330 0.3024 0.046 Uiso 1 1 calc R
C22 C 0.0694(7) -0.0713(3) 0.3728(4) 0.051(2) Uani 1 1 d .
H22A H 0.1059 -0.0655 0.4076 0.061 Uiso 1 1 calc R
H22B H 0.0034 -0.0793 0.3789 0.061 Uiso 1 1 calc R
C23 C 0.1127(11) -0.1134(4) 0.3456(7) 0.115(6) Uani 1 1 d .
H23A H 0.0758 -0.1195 0.3115 0.172 Uiso 1 1 calc R
H23B H 0.1119 -0.1423 0.3679 0.172 Uiso 1 1 calc R
H23C H 0.1783 -0.1056 0.3399 0.172 Uiso 1 1 calc R
C24 C 0.2667(5) 0.1340(3) 0.3911(3) 0.0254(16) Uani 1 1 d .
C25 C 0.2297(6) 0.1411(3) 0.4448(3) 0.039(2) Uani 1 1 d .
C26 C 0.3011(8) 0.1164(5) 0.4865(4) 0.089(4) Uani 1 1 d .
H26A H 0.2725 0.1132 0.5199 0.133 Uiso 1 1 calc R
H26B H 0.3588 0.1360 0.4923 0.133 Uiso 1 1 calc R
H26C H 0.3171 0.0842 0.4739 0.133 Uiso 1 1 calc R
C27 C 0.1378(9) 0.1156(5) 0.4468(5) 0.088(4) Uani 1 1 d .
H27A H 0.1104 0.1247 0.4792 0.132 Uiso 1 1 calc R
H27B H 0.1484 0.0806 0.4466 0.132 Uiso 1 1 calc R
H27C H 0.0941 0.1247 0.4159 0.132 Uiso 1 1 calc R
C28 C 0.2233(10) 0.1929(4) 0.4581(4) 0.078(4) Uani 1 1 d .
H28A H 0.1719 0.2079 0.4350 0.118 Uiso 1 1 calc R
H28B H 0.2835 0.2089 0.4533 0.118 Uiso 1 1 calc R
H28C H 0.2103 0.1962 0.4951 0.118 Uiso 1 1 calc R
C29 C 0.5515(6) 0.2247(3) 0.3791(3) 0.041(2) Uani 1 1 d .
C30 C 0.5702(7) 0.2289(4) 0.4385(4) 0.063(3) Uani 1 1 d .
C31 C 0.4847(10) 0.2220(8) 0.4644(5) 0.155(9) Uani 1 1 d .
H31A H 0.4415 0.2492 0.4561 0.232 Uiso 1 1 calc R
H31B H 0.5013 0.2203 0.5028 0.232 Uiso 1 1 calc R
H31C H 0.4536 0.1919 0.4520 0.232 Uiso 1 1 calc R
C32 C 0.6539(11) 0.1981(6) 0.4581(5) 0.122(6) Uani 1 1 d .
H32A H 0.6317 0.1668 0.4697 0.183 Uiso 1 1 calc R
H32B H 0.6906 0.2143 0.4879 0.183 Uiso 1 1 calc R
H32C H 0.6943 0.1933 0.4295 0.183 Uiso 1 1 calc R
C33 C 0.6032(12) 0.2834(5) 0.4535(5) 0.120(6) Uani 1 1 d .
H33A H 0.6726 0.2853 0.4568 0.180 Uiso 1 1 calc R
H33B H 0.5803 0.2926 0.4871 0.180 Uiso 1 1 calc R
H33C H 0.5767 0.3055 0.4256 0.180 Uiso 1 1 calc R
C34 C 0.3559(11) 0.3027(4) 0.3079(6) 0.109(3) Uani 1 1 d .
C35 C 0.2917(8) 0.3366(5) 0.3347(4) 0.0785(18) Uani 1 1 d .
C36 C 0.2058(8) 0.3116(5) 0.3490(4) 0.0785(4) Uani 1 1 d .
H36A H 0.1794 0.3294 0.3774 0.118 Uiso 1 1 calc R
H36B H 0.2226 0.2788 0.3611 0.118 Uiso 1 1 calc R
H36C H 0.1586 0.3100 0.3180 0.118 Uiso 1 1 calc R
C37 C 0.2870(8) 0.3850(4) 0.3095(4) 0.0785(4) Uani 1 1 d .
H37A H 0.2547 0.3825 0.2736 0.118 Uiso 1 1 calc R
H37B H 0.3515 0.3973 0.3079 0.118 Uiso 1 1 calc R
H37C H 0.2518 0.4072 0.3304 0.118 Uiso 1 1 calc R
C38 C 0.3455(13) 0.3448(6) 0.3928(6) 0.148(8) Uani 1 1 d .
H38A H 0.3355 0.3782 0.4041 0.222 Uiso 1 1 calc R
H38B H 0.4136 0.3390 0.3921 0.222 Uiso 1 1 calc R
H38C H 0.3202 0.3224 0.4177 0.222 Uiso 1 1 calc R
Co1 Co 0.72313(6) 0.10509(3) 0.30747(3) 0.0218(2) Uani 1 1 d .
Co2 Co 0.30450(6) 0.06681(3) 0.31045(3) 0.0159(2) Uani 1 1 d .
Co3 Co 0.53253(15) 0.27992(7) 0.27903(8) 0.0331(5) Uani 0.50 1 d P
Dy1 Dy 0.5000 0.068455(15) 0.2500 0.01558(14) Uani 1 2 d S
Dy2 Dy 0.37378(2) 0.181791(11) 0.291510(12) 0.02199(13) Uani 1 1 d .
N1 N 0.1834(4) 0.0312(2) 0.2991(2) 0.0229(13) Uani 1 1 d .
O1 O 0.7872(4) 0.1660(2) 0.3368(2) 0.0371(13) Uani 1 1 d .
O2 O 0.8345(4) 0.0671(2) 0.35459(19) 0.0369(13) Uani 1 1 d .
O3 O 0.6982(3) 0.0801(2) 0.3834(2) 0.0344(13) Uani 1 1 d .
O4 O 0.5956(3) 0.13404(16) 0.28236(17) 0.0209(10) Uani 1 1 d .
O5 O 0.5022(3) 0.00842(17) 0.31285(18) 0.0234(11) Uani 1 1 d .
O6 O 0.3651(3) 0.01377(16) 0.34871(17) 0.0221(10) Uani 1 1 d .
O7 O 0.4188(3) 0.10320(15) 0.31686(16) 0.0162(9) Uani 1 1 d .
O8 O 0.3333(3) 0.04446(16) 0.24295(16) 0.0198(10) Uani 1 1 d .
O9 O 0.2417(3) 0.11713(16) 0.27111(17) 0.0194(10) Uani 1 1 d .
O10 O 0.2706(3) 0.08937(16) 0.37660(17) 0.0208(10) Uani 1 1 d .
O11 O 0.2922(3) 0.16919(17) 0.36617(18) 0.0253(11) Uani 1 1 d .
O12 O 0.5059(4) 0.18860(18) 0.3586(2) 0.0357(13) Uani 1 1 d .
O13 O 0.2638(4) 0.21530(19) 0.2291(2) 0.0397(14) Uani 1 1 d .
O14 O 0.5000 0.2213(3) 0.2500 0.047(2) Uani 1 2 d S
O15 O 0.3607(4) 0.25929(17) 0.3211(2) 0.0337(12) Uani 1 1 d .
O16 O 0.5829(4) 0.2572(2) 0.3520(2) 0.0547(17) Uani 1 1 d .
O17 O 0.4065(7) 0.3215(2) 0.2768(4) 0.109(3) Uani 1 1 d .
O18 O 0.5197(5) 0.0943(3) 0.4138(2) 0.067(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O13 C1 O1 124.2(7) 2_655 .
O13 C1 C2 117.6(10) 2_655 .
O1 C1 C2 118.1(10) . .
C4 C2 C3 115.7(14) . .
C4 C2 C1 113.4(12) . .
C3 C2 C1 108.7(10) . .
C4 C2 C5 100.7(12) . .
C3 C2 C5 108.3(14) . .
C1 C2 C5 109.5(12) . .
C2 C3 H3A 109.5 . .
C2 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C2 C3 H3C 109.4 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
C2 C4 H4A 109.4 . .
C2 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
C2 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
C2 C5 H5A 109.4 . .
C2 C5 H5B 109.5 . .
H5A C5 H5B 109.5 . .
C2 C5 H5C 109.5 . .
H5A C5 H5C 109.5 . .
H5B C5 H5C 109.5 . .
O3 C6 O2 119.3(7) . .
O3 C6 C7 121.5(8) . .
O2 C6 C7 119.2(8) . .
O3 C6 Co1 59.1(4) . .
O2 C6 Co1 60.8(4) . .
C7 C6 Co1 172.2(7) . .
C10 C7 C8 117.5(11) . .
C10 C7 C6 110.9(9) . .
C8 C7 C6 114.0(9) . .
C10 C7 C9 106.1(10) . .
C8 C7 C9 100.7(10) . .
C6 C7 C9 106.1(9) . .
C7 C8 H8A 109.5 . .
C7 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
C7 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
C7 C9 H9A 109.5 . .
C7 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C7 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
C7 C10 H10A 109.5 . .
C7 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C7 C10 H10C 109.4 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
O5 C11 O6 125.6(6) . .
O5 C11 C12 117.7(8) . .
O6 C11 C12 116.5(8) . .
C13 C12 C14 133.7(10) . .
C13 C12 C11 115.3(10) . .
C14 C12 C11 110.5(10) . .
C13 C12 C15 79.9(12) . .
C14 C12 C15 86.2(12) . .
C11 C12 C15 100.2(11) . .
C12 C13 H13A 109.3 . .
C12 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
C12 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
C12 C14 H14A 109.4 . .
C12 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C12 C14 H14C 109.4 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C12 C15 H15A 109.4 . .
C12 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C12 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
O8 C16 C17 107.3(5) . .
O8 C16 H16A 110.3 . .
C17 C16 H16A 110.3 . .
O8 C16 H16B 110.3 . .
C17 C16 H16B 110.3 . .
H16A C16 H16B 108.5 . .
N1 C17 C16 109.0(5) . .
N1 C17 H17A 109.9 . .
C16 C17 H17A 109.9 . .
N1 C17 H17B 109.9 . .
C16 C17 H17B 109.9 . .
H17A C17 H17B 108.3 . .
N1 C18 C19 110.8(6) . .
N1 C18 H18A 109.5 . .
C19 C18 H18A 109.5 . .
N1 C18 H18B 109.5 . .
C19 C18 H18B 109.5 . .
H18A C18 H18B 108.1 . .
O9 C19 C18 111.1(5) . .
O9 C19 H19A 109.4 . .
C18 C19 H19A 109.4 . .
O9 C19 H19B 109.4 . .
C18 C19 H19B 109.4 . .
H19A C19 H19B 108.0 . .
N1 C20 C21 115.1(6) . .
N1 C20 H20A 108.5 . .
C21 C20 H20A 108.5 . .
N1 C20 H20B 108.5 . .
C21 C20 H20B 108.5 . .
H20A C20 H20B 107.5 . .
C22 C21 C20 110.7(7) . .
C22 C21 H21A 109.5 . .
C20 C21 H21A 109.5 . .
C22 C21 H21B 109.5 . .
C20 C21 H21B 109.5 . .
H21A C21 H21B 108.1 . .
C23 C22 C21 110.9(8) . .
C23 C22 H22A 109.5 . .
C21 C22 H22A 109.4 . .
C23 C22 H22B 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 108.0 . .
C22 C23 H23A 109.5 . .
C22 C23 H23B 109.4 . .
H23A C23 H23B 109.5 . .
C22 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
O11 C24 O10 125.7(6) . .
O11 C24 C25 120.3(6) . .
O10 C24 C25 114.0(6) . .
C28 C25 C27 112.1(9) . .
C28 C25 C24 111.4(7) . .
C27 C25 C24 110.8(7) . .
C28 C25 C26 108.8(9) . .
C27 C25 C26 106.2(9) . .
C24 C25 C26 107.3(7) . .
C25 C26 H26A 109.5 . .
C25 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
C25 C26 H26C 109.4 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
C25 C27 H27A 109.5 . .
C25 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C25 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C25 C28 H28A 109.5 . .
C25 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C25 C28 H28C 109.4 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
O16 C29 O12 122.3(8) . .
O16 C29 C30 117.8(8) . .
O12 C29 C30 119.9(8) . .
C31 C30 C32 116.3(12) . .
C31 C30 C29 112.1(9) . .
C32 C30 C29 109.8(9) . .
C31 C30 C33 104.5(12) . .
C32 C30 C33 104.6(11) . .
C29 C30 C33 108.8(9) . .
C30 C31 H31A 109.4 . .
C30 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C30 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C30 C32 H32A 109.5 . .
C30 C32 H32B 109.4 . .
H32A C32 H32B 109.5 . .
C30 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
C30 C33 H33A 109.5 . .
C30 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C30 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
O17 C34 O15 123.9(9) . .
O17 C34 C35 116.3(9) . .
O15 C34 C35 119.5(9) . .
C36 C35 C37 122.0(11) . .
C36 C35 C34 111.6(12) . .
C37 C35 C34 111.4(10) . .
C36 C35 C38 99.4(9) . .
C37 C35 C38 105.4(12) . .
C34 C35 C38 104.5(12) . .
C35 C36 H36A 109.5 . .
C35 C36 H36B 109.6 . .
H36A C36 H36B 109.4 . .
C35 C36 H36C 109.5 . .
H36A C36 H36C 109.4 . .
H36B C36 H36C 109.4 . .
C35 C37 H37A 109.5 . .
C35 C37 H37B 109.5 . .
H37A C37 H37B 109.5 . .
C35 C37 H37C 109.4 . .
H37A C37 H37C 109.5 . .
H37B C37 H37C 109.5 . .
C35 C38 H38A 109.4 . .
C35 C38 H38B 109.5 . .
H38A C38 H38B 109.5 . .
C35 C38 H38C 109.5 . .
H38A C38 H38C 109.5 . .
H38B C38 H38C 109.5 . .
O1 Co1 O4 98.0(2) . .
O1 Co1 O3 92.7(2) . .
O4 Co1 O3 100.85(19) . .
O1 Co1 O9 94.30(19) . 2_655
O4 Co1 O9 86.08(18) . 2_655
O3 Co1 O9 169.3(2) . 2_655
O1 Co1 O2 85.8(2) . .
O4 Co1 O2 161.7(2) . .
O3 Co1 O2 61.01(19) . .
O9 Co1 O2 111.55(18) 2_655 .
O1 Co1 O8 165.71(19) . 2_655
O4 Co1 O8 81.97(17) . 2_655
O3 Co1 O8 101.32(19) . 2_655
O9 Co1 O8 71.42(16) 2_655 2_655
O2 Co1 O8 98.71(19) . 2_655
O1 Co1 C6 86.5(2) . .
O4 Co1 C6 131.0(2) . .
O3 Co1 C6 30.2(2) . .
O9 Co1 C6 142.5(2) 2_655 .
O2 Co1 C6 31.0(2) . .
O8 Co1 C6 104.4(2) 2_655 .
O1 Co1 Dy2 83.43(15) . 2_655
O4 Co1 Dy2 41.72(13) . 2_655
O3 Co1 Dy2 140.53(14) . 2_655
O9 Co1 Dy2 48.58(12) 2_655 2_655
O2 Co1 Dy2 156.24(15) . 2_655
O8 Co1 Dy2 87.25(11) 2_655 2_655
C6 Co1 Dy2 165.9(2) . 2_655
O1 Co1 Dy1 138.52(16) . .
O4 Co1 Dy1 40.64(13) . .
O3 Co1 Dy1 93.21(14) . .
O9 Co1 Dy1 86.79(11) 2_655 .
O2 Co1 Dy1 132.05(15) . .
O8 Co1 Dy1 43.96(11) 2_655 .
C6 Co1 Dy1 116.67(18) . .
Dy2 Co1 Dy1 66.505(17) 2_655 .
O9 Co2 O7 90.29(19) . .
O9 Co2 O10 94.47(19) . .
O7 Co2 O10 92.44(19) . .
O9 Co2 O8 84.00(19) . .
O7 Co2 O8 89.29(18) . .
O10 Co2 O8 177.70(19) . .
O9 Co2 O6 177.6(2) . .
O7 Co2 O6 91.70(18) . .
O10 Co2 O6 86.77(19) . .
O8 Co2 O6 94.69(19) . .
O9 Co2 N1 86.3(2) . .
O7 Co2 N1 176.1(2) . .
O10 Co2 N1 89.8(2) . .
O8 Co2 N1 88.4(2) . .
O6 Co2 N1 91.6(2) . .
O9 Co2 Dy1 96.62(13) . .
O7 Co2 Dy1 44.27(13) . .
O10 Co2 Dy1 135.08(13) . .
O8 Co2 Dy1 46.97(13) . .
O6 Co2 Dy1 83.90(13) . .
N1 Co2 Dy1 134.18(17) . .
O9 Co2 Dy2 49.93(13) . .
O7 Co2 Dy2 41.87(13) . .
O10 Co2 Dy2 85.48(14) . .
O8 Co2 Dy2 94.82(13) . .
O6 Co2 Dy2 132.30(14) . .
N1 Co2 Dy2 135.27(17) . .
Dy1 Co2 Dy2 69.545(19) . .
Co3 Co3 O14 62.97(13) 2_655 .
Co3 Co3 O16 158.4(2) 2_655 .
O14 Co3 O16 98.3(2) . .
Co3 Co3 O17 68.0(3) 2_655 2_655
O14 Co3 O17 108.7(2) . 2_655
O16 Co3 O17 131.8(4) . 2_655
Co3 Co3 O17 65.6(3) 2_655 .
O14 Co3 O17 107.2(3) . .
O16 Co3 O17 114.2(3) . .
O17 Co3 O17 95.2(4) 2_655 .
O5 Dy1 O5 87.7(2) . 2_655
O5 Dy1 O7 145.40(15) . 2_655
O5 Dy1 O7 76.43(15) 2_655 2_655
O5 Dy1 O7 76.43(15) . .
O5 Dy1 O7 145.40(15) 2_655 .
O7 Dy1 O7 131.8(2) 2_655 .
O5 Dy1 O4 139.62(16) . 2_655
O5 Dy1 O4 110.33(16) 2_655 2_655
O7 Dy1 O4 74.97(15) 2_655 2_655
O7 Dy1 O4 68.40(15) . 2_655
O5 Dy1 O4 110.33(16) . .
O5 Dy1 O4 139.62(16) 2_655 .
O7 Dy1 O4 68.40(15) 2_655 .
O7 Dy1 O4 74.97(15) . .
O4 Dy1 O4 79.5(2) 2_655 .
O5 Dy1 O8 78.30(15) . .
O5 Dy1 O8 79.09(15) 2_655 .
O7 Dy1 O8 126.87(14) 2_655 .
O7 Dy1 O8 67.77(14) . .
O4 Dy1 O8 70.61(15) 2_655 .
O4 Dy1 O8 138.57(15) . .
O5 Dy1 O8 79.09(15) . 2_655
O5 Dy1 O8 78.30(15) 2_655 2_655
O7 Dy1 O8 67.77(14) 2_655 2_655
O7 Dy1 O8 126.87(14) . 2_655
O4 Dy1 O8 138.57(15) 2_655 2_655
O4 Dy1 O8 70.61(15) . 2_655
O8 Dy1 O8 148.5(2) . 2_655
O5 Dy1 Co2 111.21(11) . 2_655
O5 Dy1 Co2 67.56(11) 2_655 2_655
O7 Dy1 Co2 34.26(10) 2_655 2_655
O7 Dy1 Co2 146.90(10) . 2_655
O4 Dy1 Co2 109.07(11) 2_655 2_655
O4 Dy1 Co2 72.21(11) . 2_655
O8 Dy1 Co2 144.43(10) . 2_655
O8 Dy1 Co2 34.83(10) 2_655 2_655
O5 Dy1 Co2 67.56(11) . .
O5 Dy1 Co2 111.21(11) 2_655 .
O7 Dy1 Co2 146.90(10) 2_655 .
O7 Dy1 Co2 34.26(10) . .
O4 Dy1 Co2 72.21(11) 2_655 .
O4 Dy1 Co2 109.07(11) . .
O8 Dy1 Co2 34.83(10) . .
O8 Dy1 Co2 144.43(10) 2_655 .
Co2 Dy1 Co2 178.42(3) 2_655 .
O5 Dy1 Co1 116.44(11) . 2_655
O5 Dy1 Co1 88.48(11) 2_655 2_655
O7 Dy1 Co1 93.97(10) 2_655 2_655
O7 Dy1 Co1 72.18(10) . 2_655
O4 Dy1 Co1 33.86(11) 2_655 2_655
O4 Dy1 Co1 112.58(11) . 2_655
O8 Dy1 Co1 38.89(10) . 2_655
O8 Dy1 Co1 159.42(10) 2_655 2_655
Co2 Dy1 Co1 125.15(2) 2_655 2_655
Co2 Dy1 Co1 55.41(2) . 2_655
O5 Dy1 Co1 88.48(11) . .
O5 Dy1 Co1 116.44(11) 2_655 .
O7 Dy1 Co1 72.18(10) 2_655 .
O7 Dy1 Co1 93.97(10) . .
O4 Dy1 Co1 112.58(11) 2_655 .
O4 Dy1 Co1 33.86(11) . .
O8 Dy1 Co1 159.42(10) . .
O8 Dy1 Co1 38.89(10) 2_655 .
Co2 Dy1 Co1 55.41(2) 2_655 .
Co2 Dy1 Co1 125.15(2) . .
Co1 Dy1 Co1 146.25(3) 2_655 .
O15 Dy2 O13 77.07(19) . .
O15 Dy2 O7 144.18(16) . .
O13 Dy2 O7 135.32(17) . .
O15 Dy2 O11 79.00(17) . .
O13 Dy2 O11 105.15(18) . .
O7 Dy2 O11 77.45(16) . .
O15 Dy2 O4 144.15(17) . 2_655
O13 Dy2 O4 81.14(17) . 2_655
O7 Dy2 O4 68.46(14) . 2_655
O11 Dy2 O4 134.68(16) . 2_655
O15 Dy2 O12 77.13(18) . .
O13 Dy2 O12 151.51(18) . .
O7 Dy2 O12 73.00(16) . .
O11 Dy2 O12 81.46(18) . .
O4 Dy2 O12 114.28(16) 2_655 .
O15 Dy2 O14 79.1(2) . .
O13 Dy2 O14 89.77(16) . .
O7 Dy2 O14 110.22(18) . .
O11 Dy2 O14 149.86(14) . .
O4 Dy2 O14 72.66(17) 2_655 .
O12 Dy2 O14 73.66(14) . .
O15 Dy2 O9 128.95(16) . .
O13 Dy2 O9 73.64(17) . .
O7 Dy2 O9 65.49(13) . .
O11 Dy2 O9 69.77(15) . .
O4 Dy2 O9 69.34(14) 2_655 .
O12 Dy2 O9 133.30(16) . .
O14 Dy2 O9 140.31(13) . .
O15 Dy2 Co2 143.23(13) . .
O13 Dy2 Co2 106.97(14) . .
O7 Dy2 Co2 32.85(10) . .
O11 Dy2 Co2 64.54(12) . .
O4 Dy2 Co2 70.66(11) 2_655 .
O12 Dy2 Co2 100.90(13) . .
O14 Dy2 Co2 136.33(16) . .
O9 Dy2 Co2 33.61(9) . .
O15 Dy2 Co1 140.72(13) . 2_655
O13 Dy2 Co1 63.74(14) . 2_655
O7 Dy2 Co1 72.92(10) . 2_655
O11 Dy2 Co1 107.75(11) . 2_655
O4 Dy2 Co1 34.47(10) 2_655 2_655
O12 Dy2 Co1 141.56(12) . 2_655
O14 Dy2 Co1 102.33(9) . 2_655
O9 Dy2 Co1 37.99(10) . 2_655
Co2 Dy2 Co1 55.09(2) . 2_655
O15 Dy2 Dy1 156.77(14) . .
O13 Dy2 Dy1 116.39(13) . .
O7 Dy2 Dy1 35.81(10) . .
O11 Dy2 Dy1 112.74(12) . .
O4 Dy2 Dy1 36.20(10) 2_655 .
O12 Dy2 Dy1 84.70(12) . .
O14 Dy2 Dy1 82.01(16) . .
O9 Dy2 Dy1 74.22(9) . .
Co2 Dy2 Dy1 54.346(16) . .
Co1 Dy2 Dy1 57.098(16) 2_655 .
C20 N1 C17 111.2(6) . .
C20 N1 C18 109.9(5) . .
C17 N1 C18 113.2(5) . .
C20 N1 Co2 114.1(4) . .
C17 N1 Co2 106.0(4) . .
C18 N1 Co2 102.1(4) . .
C1 O1 Co1 125.1(5) . .
C6 O2 Co1 88.1(4) . .
C6 O3 Co1 90.7(5) . .
Co1 O4 Dy1 105.50(19) . .
Co1 O4 Dy2 103.81(19) . 2_655
Dy1 O4 Dy2 107.36(16) . 2_655
C11 O5 Dy1 134.3(4) . .
C11 O6 Co2 128.6(4) . .
Co2 O7 Dy2 105.28(18) . .
Co2 O7 Dy1 101.47(17) . .
Dy2 O7 Dy1 108.70(16) . .
C16 O8 Co2 106.6(4) . .
C16 O8 Co1 114.0(4) . 2_655
Co2 O8 Co1 100.21(19) . 2_655
C16 O8 Dy1 135.1(4) . .
Co2 O8 Dy1 98.20(17) . .
Co1 O8 Dy1 97.15(16) 2_655 .
C19 O9 Co2 112.6(4) . .
C19 O9 Co1 111.7(4) . 2_655
Co2 O9 Co1 103.76(19) . 2_655
C19 O9 Dy2 134.3(4) . .
Co2 O9 Dy2 96.46(17) . .
Co1 O9 Dy2 93.43(15) 2_655 .
C24 O10 Co2 126.0(4) . .
C24 O11 Dy2 136.5(4) . .
C29 O12 Dy2 132.6(6) . .
C1 O13 Dy2 142.5(5) 2_655 .
Co3 O14 Co3 54.1(3) 2_655 .
Co3 O14 Dy2 114.19(13) 2_655 .
Co3 O14 Dy2 113.01(13) . .
Co3 O14 Dy2 113.01(13) 2_655 2_655
Co3 O14 Dy2 114.19(13) . 2_655
Dy2 O14 Dy2 126.6(3) . 2_655
C34 O15 Dy2 144.9(8) . .
C29 O16 Co3 128.6(5) . .
C34 O17 Co3 120.9(8) . 2_655
C34 O17 Co3 107.4(8) . .
Co3 O17 Co3 46.41(18) 2_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O13 1.251(9) 2_655
C1 O1 1.262(10) .
C1 C2 1.506(13) .
C2 C4 1.443(19) .
C2 C3 1.445(18) .
C2 C5 1.55(2) .
C3 H3A 0.9800 .
C3 H3B 0.9800 .
C3 H3C 0.9800 .
C4 H4A 0.9800 .
C4 H4B 0.9800 .
C4 H4C 0.9800 .
C5 H5A 0.9800 .
C5 H5B 0.9800 .
C5 H5C 0.9800 .
C6 O3 1.240(9) .
C6 O2 1.270(9) .
C6 C7 1.510(13) .
C6 Co1 2.463(8) .
C7 C10 1.423(16) .
C7 C8 1.467(14) .
C7 C9 1.596(17) .
C8 H8A 0.9800 .
C8 H8B 0.9800 .
C8 H8C 0.9800 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 O5 1.236(8) .
C11 O6 1.277(8) .
C11 C12 1.510(12) .
C12 C13 1.391(17) .
C12 C14 1.459(17) .
C13 H13A 0.9800 .
C13 H13B 0.9800 .
C13 H13C 0.9800 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 O8 1.420(8) .
C16 C17 1.530(10) .
C16 H16A 0.9900 .
C16 H16B 0.9900 .
C17 N1 1.488(9) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 N1 1.514(9) .
C18 C19 1.524(10) .
C18 H18A 0.9900 .
C18 H18B 0.9900 .
C19 O9 1.427(8) .
C19 H19A 0.9900 .
C19 H19B 0.9900 .
C20 N1 1.479(9) .
C20 C21 1.529(10) .
C20 H20A 0.9900 .
C20 H20B 0.9900 .
C21 C22 1.525(12) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 C23 1.516(16) .
C22 H22A 0.9900 .
C22 H22B 0.9900 .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
C24 O11 1.235(8) .
C24 O10 1.292(8) .
C24 C25 1.525(10) .
C25 C28 1.478(13) .
C25 C27 1.486(13) .
C25 C26 1.547(13) .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 O16 1.243(10) .
C29 O12 1.273(9) .
C29 C30 1.509(12) .
C30 C31 1.452(16) .
C30 C32 1.501(17) .
C30 C33 1.613(17) .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
C34 O17 1.237(12) .
C34 O15 1.248(11) .
C34 C35 1.517(16) .
C35 C36 1.478(16) .
C35 C37 1.481(16) .
C35 C38 1.605(19) .
C36 H36A 0.9807 .
C36 H36B 0.9807 .
C36 H36C 0.9807 .
C37 H37A 0.9800 .
C37 H37B 0.9800 .
C37 H37C 0.9800 .
C38 H38A 0.9800 .
C38 H38B 0.9800 .
C38 H38C 0.9800 .
Co1 O1 2.018(5) .
Co1 O4 2.018(4) .
Co1 O3 2.114(5) .
Co1 O9 2.135(4) 2_655
Co1 O2 2.152(5) .
Co1 O8 2.208(4) 2_655
Co1 Dy2 3.4624(10) 2_655
Co1 Dy1 3.4904(9) .
Co2 O9 1.882(4) .
Co2 O7 1.899(4) .
Co2 O10 1.902(4) .
Co2 O8 1.908(4) .
Co2 O6 1.913(4) .
Co2 N1 1.973(5) .
Co2 Dy1 3.3062(8) .
Co2 Dy2 3.3776(9) .
Co3 Co3 1.656(4) 2_655
Co3 O14 1.822(7) .
Co3 O16 2.015(7) .
Co3 O17 2.082(8) 2_655
Co3 O17 2.119(8) .
Dy1 O5 2.302(4) .
Dy1 O5 2.302(4) 2_655
Dy1 O7 2.355(4) 2_655
Dy1 O7 2.355(4) .
Dy1 O4 2.359(4) 2_655
Dy1 O4 2.359(4) .
Dy1 O8 2.442(4) .
Dy1 O8 2.442(4) 2_655
Dy1 Co2 3.3062(8) 2_655
Dy1 Co1 3.4903(9) 2_655
Dy2 O15 2.286(5) .
Dy2 O13 2.298(5) .
Dy2 O7 2.337(4) .
Dy2 O11 2.350(5) .
Dy2 O4 2.373(4) 2_655
Dy2 O12 2.403(5) .
Dy2 O14 2.429(3) .
Dy2 O9 2.601(4) .
Dy2 Co1 3.4624(10) 2_655
O4 Dy2 2.373(4) 2_655
O8 Co1 2.208(4) 2_655
O9 Co1 2.135(4) 2_655
O13 C1 1.251(9) 2_655
O14 Co3 1.822(7) 2_655
O14 Dy2 2.429(3) 2_655
O17 Co3 2.082(8) 2_655
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.380 0.250 76 4 ' '
2 0.000 0.620 0.750 76 4 ' '
3 0.027 0.340 0.423 13 0 ' '
4 0.027 0.660 0.923 13 0 ' '
5 0.215 0.351 0.061 9 0 ' '
6 0.215 0.649 0.561 9 0 ' '
7 0.285 0.149 0.939 9 0 ' '
8 0.285 0.851 0.439 9 0 ' '
9 0.500 0.120 0.750 76 4 ' '
10 0.500 0.880 0.250 76 4 ' '
11 0.472 0.160 0.577 13 0 ' '
12 0.472 0.840 0.077 12 0 ' '
13 0.527 0.160 0.923 13 0 ' '
14 0.527 0.840 0.423 13 0 ' '
15 0.715 0.149 0.561 9 0 ' '
16 0.715 0.851 0.061 9 0 ' '
17 0.785 0.351 0.439 9 0 ' '
18 0.785 0.649 0.939 9 0 ' '
19 0.972 0.340 0.077 12 0 ' '
20 0.972 0.660 0.577 13 0 ' '
